phase ii environmental assessment

By

P. O. Box 295

2561 Stouffville Road, Suite 202

Gormley, Ontario

L0H 1G0

Telephone (905) 887-6661

BARENCO INC.

Phase IIEnvironmental Assessment

Thirteen Properties, High Park Project

Toronto, Ontario

March 5, 2008

Daniels HR Corporation20 Queen Street West

Suite 3400

Toronto, Ontario

M5H 3R3

For

07126

ENVIRONMENTAL ENGINEERING AND SITE REMEDIATION SERVICES

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any decision made or any action taken based on this report or the work referredto in this report.

The investigation undertaken by Barenco Inc. with respect to this report andany conclusions or recommendations made in this report reflect Barenco Inc.'sjudgement based on the site conditions observed at the time of the siteinspection on the date(s) set out in this report and on information available atthe time of preparation of this report. This report has been prepared for specificapplication to this site and it is based, in part, upon visual observatiou of, thesite, subsurface investigation at discrete locations and depths, and specificanalysis of specific chemical parameters and materials during a specific timeinterval, all as described in this report. Unless otherwise stated, the findingscannot be extended to previous or future site conditions, portions of the sitewhich were unavailable for direct investigation, subsurface locations whichwere not investigated directly, or chemical parameters, materials or analysiswhich were not addressed. Substances other than those addressed by theinvestigation described in this report may exist within the site, substancesaddressed by the investigation may exist in areas of the site not investigated andconcentrations of substances addressed which are different than those reportedmay exist in areas other than the locations from which the samples were taken.

If site conditions or applicable standards change or if any additional informationbecomes available at a future date, modifications to the findings, conclusionsand recommendations in this report may be necessary.

Other than by Daniels HR Corporation, copying or distribution of this report orthe use of or reliance on the information contained herein, in whole or in part, isnot permitted without the express written permission of Barenco Inc. Nothingin this report is intended to constitute or provide a legal opinion.

Respectfully submitted,BARENCO INC.

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/I Jim Phimister, P .Eng, !.. '-

Principal, Hydrogeologist

March 5, 20088

Phase II Environmental AssessmentThirteen Properties, High Park Project, Toronto, Ontario

FIGURES

SITE

SITE

SITE

SITE

1FIGURE

SCALE: NOTES:

SOURCE:

DRAWN BY

07126-LOCALITY

C.D. V.K.

CHECKED BY

BARENCO JOB #: 07126 DATE: DECEMBER 2007

N

THIRTEEN PROPERTIES,HIGH PARK PROJECTTORONTO, ONTARIO

1:25000

LOCALITY PLAN

MAPART PUBLISHING 2005

SITE

SITE

SITE

SITE

SITE

2FIGURE

SCALE: SOURCE:

DRAWN BY

07126-SITE PLAN1-JAN08

M.A. B.C.

CHECKED BY

BARENCO JOB #: 07126 DATE: JANUARY 2008

N

THIRTEEN PROPERTIES,HIGH PARK PROJECTTORONTO, ONTARIO

SITE PLANCITY OF TORONTO PLANFIELD OBSERVATIONS BYBARENCO STAFF

SITE

0 20m

( APPROXIMATE)

10TEST HOLE WITHMONITOR DRILLEDIN JANUARY 2008

TEST HOLE DRILLED IN DECEMBER 2007

LEGEND:

BLOOR STREET WEST

PA

CIF

IC A

VE

NU

E

OA

KM

OU

NT

RO

AD

8

6

10

12

14

184418461848185018521854

35

37

GARAGE

SHED

TH106

TH101

TH104

TH105

TH102

TH103

FORMER USTEXCAVATION

TH3

TABLES

Table 1

SITE ENVIRONMENTAL SETTING DATA

Site Location: Thirteen Properties, High Park Project, Toronto, Ontario Date: January 24, 2008

NATIVE SOIL

Silty sandType:(select range)Hydraulic Conductivity

> 10-3 cm/s: Estimated to be 10-5 cm/s<10-3 to >10-6 cm/s:

< 10-6 cm/s: Estimated to be less than 50% Soil Particles < 75 Microns:

GROUND WATER

Approximately 15.6 to 15.9 metres below gradeDepth to Water Table: Measured from onsite monitorsEstimated or Measured: SouthDirection of Flow: Estimated based on topographyEstimated or Measured:

MUNICIPAL SERVICES

YesPiped Water: NoGround Water Source: NADistance to Well: Yes - Lake OntarioSurface Water Source: YesSanitary Sewer: YesStorm Sewer:

PRIVATE SERVICES

NADistance to Nearest Well: NAApproximate Depth of Well: NoPrivate Sanitary Sewage:

SURFACE WATER

Lake OntarioName of water body: Approximately 2 kilometres to the southDistance from site: UnknownElevation drop from site: NoDirect Drainage from site:

07126 BARENCO INC.

Table 2

DARCY'S LAW CALCULATIONS

Site Location: Thirteen Properties, High Park Project, Toronto, Ontario Date: January 24, 2008 v=ki/n

1.00E-07Permeability k (m/sec) =1.00E-05(cm/sec) =

0.010Gradient i (m/m) =2.50E-09Velocity v (m/sec) =0.4Porosity* n =8.20E-09(feet/sec) =7.08E-04(feet/day) =

0.259(feet/year) =0.079(metres/year) = * (from Freeze & Cherry, 1979)

Hydraulic conductivity for silty sandbased on published valuesGradient estimated based on slope of land

07126 BARENCO INC.

Table 3

SOIL CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario

Page 1 of 2Test HoleTest HoleTest HoleTest HoleTest HoleTest HoleSampleTH103-17TH103-8TH102-15TH102-14TH101-15TH101-13

MOE15.8 to 16.59.0 to 9.615.2 to 15.814.5 to 15.115.2 to 15.813.7 to 14.3Depth (m)Table 3Silty sandSilty sandSilty sandSilty sandSilty sandSilty sandRDL*Soil Type

Soil1/17/20081/17/20081/17/20081/17/20081/16/20081/16/2008Sample DateStandards**W85486W85485W85484W85483W80998W80997Maxxam I.D.

100 ppm425 ppm25 ppm25 ppm150 ppm175 ppmField Vapour Reading

5.3ndndndndndnd0.02Benzene

34ndndndndndnd0.02Toluene

290ndndndndndnd0.02Ethylbenzene

34nd1.48ndndnd0.620.04Xylenes

30nd220ndndnd9210F1 (C6 to C10 - BTEX)No valuend6.7ndnd<0.1370.2Aliphatic >C6 to C8No valuend170ndnd<0.414000.7Aliphatic >C8 to C10No valuend16ndnd<0.22000.1Aromatics >C8 to C10

150161900ndndnd290010F2 (C10 to C16)No valuena563nanana24605Aliphatic >C10 to C12No valuena54nanana925Aromatic >C10 to C12No valuena1800nanana757010Aliphatic >C12 to C16No valuena208nanana52515Aromatic >C12 to C16

400161400ndndnd220010F3 (C16 to C34)No valuena1320nanana608010Aliphatic >C16 to C21No valuena252nanana76210Aromatic >C16 to C21No valuena141nananand10Aliphatic >C21 to <C34No valuena161nanana35510Aromatic >C21 to <C34

2800ndndndndndnd10F4 (C34 to C50)No valuenandnananand10Aliphatic >C34No valuena58nanana4110Aromatic >C34

***7.917.897.787.967.967.80-pH

Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). na means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.

07126 BARENCO INC.

Table 3

SOIL CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario

Page 2 of 2Test HoleTest HoleTest HoleTest HoleTest HoleTest HoleSampleTH106-15TH106-14TH105-15TH105-14TH104-14TH104-12

MOE16.0 to 16.615.2 to 15.816.0 to 16.615.2 to 15.815.2 to 15.813.7 to 14.3Depth (m)Table 3Silty sandSilty sandSilty sandSilty sandSilty sandSilty sandRDL*Soil Type

Soil1/21/20081/21/20081/21/20081/21/20081/18/20081/18/2008Sample DateStandards**W837394W837393W837392W837391W85489W85488Maxxam I.D.

50 ppm50 ppm100 ppm100 ppm50 ppm50 ppmField Vapour Reading

5.3ndndndndndnd0.02Benzene



34ndndndndndnd0.04Xylenes

30ndndndndndnd10F1 (C6 to C10 - BTEX)No valuendndndndndnd0.2Aliphatic >C6 to C8No valuendndndndndnd0.7Aliphatic >C8 to C10No valuendndndndndnd0.1Aromatics >C8 to C10

150ndndndndnd1210F2 (C10 to C16)No valuenananananana5Aliphatic >C10 to C12No valuenananananana5Aromatic >C10 to C12No valuenananananana10Aliphatic >C12 to C16No valuenananananana15Aromatic >C12 to C16

400ndndndndnd1210F3 (C16 to C34)No valuenananananana10Aliphatic >C16 to C21No valuenananananana10Aromatic >C16 to C21No valuenananananana10Aliphatic >C21 to <C34No valuenananananana10Aromatic >C21 to <C34

2800ndndndndndnd10F4 (C34 to C50)No valuenananananana10Aliphatic >C34No valuenananananana10Aromatic >C34

***7.958.028.027.947.957.91-pH

Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). na means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.

07126 BARENCO INC.

Table 4

SOIL CHEMICAL ANALYSIS - Polycyclic Aromatic Hydrocarbons Thirteen Properties, High Park Project, Toronto, Ontario

Page 1 of 1Test HoleTest HoleTest HoleSample

OntarioTH105-2TH104-2TH101-15Regulation 153/040.8 to 1.40.8 to 1.415.2 to 15.8Depth (m)

Table 3Silty sandSilty sandSilty sandRDL*Soil TypeSoil1/21/20081/18/20081/16/2008Sample Date

Standards**W87390W85487W80998Maxxam I.D.

1000ndndnd0.01Acenaphthene100ndndnd0.005Acenaphthylene28ndndnd0.005Anthracene40ndndnd0.01Benzo(a)anthracene1.2ndndnd0.005Benzo(a)pyrene12ndndnd0.005Benzo(b/j)fluoranthene40ndndnd0.02Benzo(g,h,i)perylene12ndndnd0.01Benzo(k)fluoranthene12ndndnd0.01Chrysene1.2ndndnd0.02Dibenzo(a,h)anthracene40ndndnd0.005Fluoranthene

350ndndnd0.005Fluorene12ndndnd0.02Indeno(1,2,3-cd)pyrene

280ndndnd0.0051-Methylnaphthalene280ndndnd0.0052-Methylnaphthalene40ndndnd0.005Naphthalene40ndndnd0.005Phenanthrene

250ndndnd0.005Pyrene***7.477.237.96-pH

Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.

07126 BARENCO INC.

Table 5

GROUND WATER CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario

Page 1 of 1MOEMonitorMonitorMonitorMonitorMonitorMonitor

Table 3TH106TH105TH104TH103TH102TH101SampleGround Water1/24/20081/24/20081/24/20081/24/20081/24/20081/24/2008RDL*Sample DateStandards**W93620W93619W93618W93617W93616W93615Maxxam I.D.

1900ndndndndndnd0.2Benzene



5600ndndndndnd1.00.4Xylenes

No valuendndndndndnd100F1 (C6 to C10 - BTEX)No valuendndndndndnd0.01Aliphatic >C6 to C8No valuendndnd0.01nd0.010.01Aliphatic >C8 to C10No valuendndndndndnd0.01Aromatics >C8 to C10

No valuend120ndndnd130100F2 (C10 to C16)No value0.03ndnd0.07nd0.450.01Aliphatic >C10 to C12No value0.03nd0.010.01nd0.150.01Aromatic >C10 to C12No value0.30ndnd0.15nd1.20.05Aliphatic >C12 to C16No value0.33ndnd0.05nd0.500.05Aromatic >C12 to C16

No valuend310ndndnd130100F3 (C16 to C34)No value0.36ndnd0.18nd1.20.05Aliphatic >C16 to C21No value0.33nd0.170.140.060.640.05Aromatic >C16 to C21No value0.1ndndndnd0.20.1Aliphatic >C21 to C32No value0.1nd0.1ndnd0.30.1Aromatic >C21 to C32

No valuendndndndndnd100F4 (C34 to C50)

Analysis by Maxxam Analytics Inc. All results in ppb (ug/L); nd means "not detected" at reporting detection limit (RDL). na means "not analysed". n/a means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. Exceedances of Table 3 Standards are shown in bold.

07126 BARENCO INC.

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/05DANIELS GRP0:1}10/2008 11:58 4169790415

4January 7, 2008Proposal - Phase II Environmental A~~~ssmentThirteen Pr Ontario

attachment: Terms and Cqnditions

Barenco U}c. to proceed with the work.

"tOocg"j'A,.j \0Date

Terms and Conditions

1. SERVICES TO BE PROVIDED AND STANDARD OF CARE. Barenco Inc. ("Barenco") agrees to provide Client for its sole benefitand exclusive use, services set forth in Barenco's Proposal. Barenco's offer to perform shall be terminated if not accepted within sixty(60) days of the date of the Proposal. Barenco's services shall be performed in accordance with the standard of care of its professionwhich means generally accepted professional practices, related to the nature of the work accomplished, at the time and place theservices are performed. Subject to this standard of care, Barenco makes no express or implied warranties regarding its services exceptas otherwise expressly stated herein and all other representations and warranties, express or implied, are hereby expressly excluded.Both parties agree that no third-party beneficiaries are intended by this Agreement. 2. PAYMENT. Invoices will be submitted once a month for services performed during the prior month, or upon completion of the work,whichever is earlier. Payment terms are due upon receipt. Interest will be added to accounts thirty (30) days in arrears at the rate oftwo per cent (2%) of the arrears for each month of delinquency, not to exceed the maximum percentage rate allowed by law. In addition,Barenco may, after giving seven (7) days written notice, suspend services under this or any other Agreement with Client without liabilityuntil all past due accounts (including fees and accrued interest) have been paid. Timely payment is an essential requirement of Client'sperformance of any Agreement between Barenco and Client. All expenses incurred by Barenco for liening or collecting any delinquentamount including, without limitation, legal and other third-party fees and filing fees, shall be paid to Barenco by Client.3. RIGHT OF ENTRY AND PROPERTY RESPONSIBILITY. Client has responsibility for obtaining a right of entry to the property whichis the subject of the services. The right of entry shall allow Barenco, its agents, subcontractors and employees to enter the property,including buildings if required to complete the services as proposed, from time to time, as necessary to perform the agreed services.Barenco has responsibility for its own activities on the property including the safety of its employees; it does not assume control of norresponsibility for the property, the person in charge of the property, nor the safety of persons not in Barenco's employ. 4. INSURANCE. Barenco maintains Workers' Compensation insurance for its employees as required by provincial law. In addition,Barenco maintains the following insurance policies: Commercial General Liability, Pollution Liability and Professional Liability($1,000,000) each occurrence, $1,000,000 Policy Aggregate) and Automobile Third Party Liability ($2,000,000).5. DOCUMENTS. Barenco will furnish Client the agreed upon number of written reports and supporting documents. All such reportsand documents are furnished for Client's exclusive internal use and reliance, use of Client's counsel, and for regulatory submission asexpressly contemplated in connection with the services provided for in the Agreement, but not for advertising or other type of distribution,and are subject to the following: All documents generated by Barenco under this Agreement shall remain the sole property of Barenco.Any unauthorized use or distribution of Barenco's work shall be at Client's and recipient's sole risk and without liability to Barenco.Barenco retains a confidential file copy of its work product and related documents. If Client desires to release, or for Barenco to provide,its report to a third party, which is not entitled to receive or use the reports and documents as set out above, for that third party'sreliance, Barenco will agree to such release provided it receives written acceptance from such third party to be bound by acceptableterms and conditions similar to this Agreement, and provided payment by such third party of Barenco's standard fee. Reports providedfor disclosure of information only will not require separate agreement. Client acknowledges and agrees to inform such third party thatBarenco's report reflects conditions only at the time of the report and may not reflect conditions at a later time. Client furtheracknowledges that such request for release creates a potential conflict of interest for Barenco and by making any such request Clientwaives any such claim if Barenco complies with the request. Client agrees that all documents furnished to Client or Client's agent ordesignees, if not paid for, will be returned upon demand and will not be used by Client or any other person or entity for any purposewhatsoever. Client further agrees that documents produced by Barenco pursuant to this Agreement will not be used for any purposenot expressly provided for in this Agreement without Barenco's prior written approval. Client shall furnish documents or other informationreasonably within Client's control and deemed necessary by Barenco for proper performance of its services. Barenco may rely, withoutindependent investigation or enquiry, upon Client-provided documents in performing the services required under this Agreement;however, Barenco assumes no responsibility or liability for their accuracy. Client-provided documents will remain the property of Clientbut Barenco may retain one confidential file copy as needed to support its report. 6. CONFIDENTIALITY. Barenco will maintain as confidential any documents or information provided by Client and will not release,distribute or publish same to any third party without prior permission from Client, unless compelled by law or by order of a court orregulatory authority of competent jurisdiction. 7. INTELLECTUAL PROPERTY. All concepts, products, processes, inventions, trade-marks, works, designs and improvements to,and derivatives of, the foregoing, resulting from the services rendered by Barenco in connection with the project, or which are invented,authored, developed or first used or reduced to practise by Barenco in the performance of the services shall be and remain the propertyof Barenco. Client shall have a personal non-exclusive, royalty-free, non-assignable, non-sublicensable licence to use the IntellectualProperty in connection with the project, for the life of the project, and for no other purpose or project. Barenco does not make anyrepresentation or warranty that such Intellectual Property does not violate the rights of any other person. 8. WASTE. Client warrants that, if it knows or suspects that "waste" (within the meaning of the Ontario Environmental Protection Act)may exist on the property, it has so informed Barenco. Client also agrees that Barenco accepts no ownership of any waste and has noresponsibility as a generator of any waste found or identified at the project property. 9. LIMITATION OF LIABILITY. CLIENT EXPRESSLY AGREES THAT, TO THE FULLEST EXTENT PERMIT TED BY LAW, ITSMAXIMUM AGGREGATE RECOVERY AGAINST BARENCO, ITS DIRECTORS, EMPLOYEES, SUB-CONTRACTORS ANDREPRESENTATIVES, FOR ANY AND ALL CLAIMS BY CLIENT FOR ALL CAUSES INCLUDING, BUT NOT LIMITED TO, CLAIMSOF BREACH OF CONTRACT, BREACH OF WARRANTY AND/OR NEGLIGENCE, SHALL BE THE AMOUNT OF THE FEE PAID TOBARENCO FOR ITS PROFESSIONAL SERVICES RENDERED UNDER THE AGREEMENT WITH RESPECT TO THE PARTICULARSITE WHICH IS THE SUBJECT OF THE CLAIM BY CLIENT. PROVIDED THAT, IF THERE IS AN EVENTUAL FINALDETERMINATION BY A COURT OF COMPETENT JURISDICTION OF GROSS NEGLIGENCE OR WILLFUL MISCONDUCT BYBARENCO, THEN THE MAXIMUM AGGREGATE RECOVERY SHALL BE LIMITED AS FOLLOWS: THE GREATER OF (A) THE FEEOR (B) THE LESSER OF TWO TIMES (2x) THE FEE AND $25,000.

Terms and Conditions (cont.)

10. INDEMNIFICATION. To the fullest extent permitted by law, Client agrees to defend, indemnify, and hold Barenco, its agents,subcontractors, and employees harmless from and against any and all claims, defence costs, including legal fees, damages and otherliabilities arising out of or in any way related to Barenco's reports or recommendations concerning this Agreement, Barenco’s presenceon the project property, or the presence, release or threatened release of contaminants on or from the project property provided thatClient shall not indemnify Barenco against liability for damages caused by or resulting from the sole negligence of Barenco, its agents,subcontractors or employees or against penalties or fines resulting from violations by Barenco of its own Certificates of Approval; andprovided further that Client shall indemnify Barenco against liability for damages caused by or resulting from the concurrent orcontributory negligence of (a) Client, its agents, or employees and (b) Barenco, its agents, subcontractors, or employees, only to theextent of Client's negligence or the negligence of Client's agents or subcontractors. Provided further that Barenco's obligation hereundershall not extend to indemnification or holding harmless for any claims of loss of profits or any other indirect, special, incidental, orconsequential damages of any nature whatsoever. 11. UNFORESEEN OCCURRENCES. If any unforeseen conditions or occurrences are encountered which, in Barenco's judgement,significantly affect or may affect the original services as proposed, then Barenco will promptly notify Client. After such notification, theparties agree that Barenco has the unilateral right to complete the original services as proposed, if appropriate, or agree with Client tomodify the Agreement, or terminate the Agreement. 12. TERMINATION AND RESTART. In the event that Client requests termination of work prior to completion or Barenco terminateswork under Paragraph 11, a final invoice will be rendered. Where the method of payment is based on time and materials, Barenco willbe paid for all work performed up to notice of termination and for all expenses incurred or committed to that cannot be cancelled. Wherethe method of payment is based on a fixed price, the final invoice will be based on the percentage of work completed by the date oftermination. Barenco also has the right to complete at client's expense the analyses and records Barenco considers necessary to protectits professional reputation. 13. WELL ABANDONMENT. Any monitoring wells installed as part of Barenco's work may later need to be abandoned in accordancewith applicable law. Unless expressly provided for in the proposal, well abandonment is not included in the work. 14. DISPOSAL OF SAMPLES. Samples not submitted for analysis will be discarded 90 days after sampling unless differentarrangements are agreed to in writing. 15. SUBSURFACE RISKS AND SITE DAMAGE. Client recognizes that special risks occur and guarantees cannot be expectedwhenever professional consulting services are applied to determine the composition of a site's subsurface or the existence or non-existence of waste materials. Barenco cannot eliminate these risks altogether, but Barenco can apply professional techniques to reducethe risks to a level deemed tolerable and Client agrees to accept that level of risk. Whenever Barenco is providing field services, Clientrecognizes that the use of exploration and test equipment may unavoidably damage or alter the property surface or subsurface. Barencowill not be responsible for personal and property damages due to its interference with subterranean structures, such as pipes, tanks,and utility lines that are not called to Barenco's attention in writing or correctly shown on plans provided by Client, or for which clearancescannot be obtained from utility owners or their agents, or which are incorrectly cleared by utility owners or their agents. 16. SEVERABILITY AND SURVIVAL. Any element of this Agreement later held to violate a law shall be deemed void, and all remainingprovisions shall continue in force. However, Client and Barenco will in good faith attempt to replace any invalid or unenforceableprovision with one that is valid and enforceable, and which comes as close as possible to expressing the intent of the original provision.All terms and conditions of this Agreement allocating liability between Client and Barenco shall survive the completion of the serviceshereunder and the termination of the Agreement. 17. DISPUTES RESOLUTION. All matters in dispute howsoever caused may with the consent of both parties be referred to arbitration.The award of the arbitrator shall be final and binding upon the parties. The provisions of the Ontario Arbitrations Act, 1991, shall apply.Alternatively, if the dispute requires litigation, (a) Client assents to exclusive jurisdiction of the courts of the Province of Ontario (b) theclaim will be brought and tried in the judicial jurisdiction where Barenco's principal place of business is located and Client waives theright to move the action to any other judicial jurisdiction and (c) the prevailing party will be entitled to recovery of all reasonable costsincurred, including staff time, court costs, legal fees and other claim-related expenses. 18. PRECEDENCE. These terms and conditions shall take precedence over any inconsistent or contradictory provisions contained inany proposal, contract, purchase order, requisition, or like document concerning Barenco's services. 19. GOVERNING LAW. This Agreement shall be governed in all respects by the laws of the Province of Ontario. 20. ENTIRE AGREEMENT. This Agreement, together with Barenco's Proposal, constitutes the entire agreement between Client andBarenco pertaining to the subject matter of this Agreement and supersedes all other agreements, understandings, negotiations anddiscussions, whether oral or written. There are no conditions, warranties, representations or other agreements between the parties inconnection with the subject matter of this Agreement (whether oral or written, express or implied, statutory or otherwise) except asspecifically set out in this Agreement. Barenco shall not be bound or deemed to be bound by any other document or instrument issuedby the Client, including without limitation, purchase orders, requisitions, or contracts unless a duly authorized officer of Barenco expressly agrees in writing to be bound by the terms of such documents or instruments, notwithstanding that documents or instruments maystate otherwise. 21. PREPARATION OF AGREEMENT. Notwithstanding any rule or maxim of law or construction to the contrary, the parties agree thatany ambiguity or uncertainty contained in this Agreement shall not be construed against Barenco merely because this Agreement wasdrafted or prepared by or on behalf of Barenco.

FORM TC1 -JANUARY 2007

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PROJECT #

TECHNICIAN

07126

D.Doherty

TEST HOLE LOG TH101DRILL DATE: January 16, 2008

SHEET#

WEATHER:

ONE of TWO

EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:

Overcast, -7C

GROUND WATER DEPTH: 15.59m. (24/01/2008)

SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON

UTM: 483 45 39Northing Easting 62 39 81

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ANALYSISREQUESTED

DESCRIPTION OFSTRATIGRAPHY MONITOR

TOP OF MONITOR ELEVATION: NANA

(Blo

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per

ft)

1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 01/02/03/02 ND 65%

0.6

2 SS 01/02/03/04 ND 75%

1.4

0.8

3 SS 10/13/13/16 25 85%PPM

2.1

1.5

4 SS 10/09/11/12 ND 90%

3.7

3.0

5 SS 10/14/20/21 ND 100%

5.2

4.6

6 SS 07/22/25/22 25 75%PPM

6.7

6.1

7 SS 08/16/20/28 ND 100%

8.2

7.6

8 SS 10/30/39/40 25 100%PPM

9.8

9.1

TOPSOIL : Dark brown, soft, TOPSOIL, moist. 0.1SILTY SAND : Light brown, loose to very dense,SAND, fine grained, becomes coarse grained at13.2m, silty, damp, wet at 15.2m, petroleum odourbetween 13.7m and 14.3m and between 15.2mand 15.9m.

BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume

PROJECT #

TECHNICIAN

07126

D.Doherty


SHEET#

WEATHER:

TWO of TWO


Overcast, -7C




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ANALYSISREQUESTED



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14

15

16

17

18

19 19

18

17

16

15

14

13

12

11

16.76 m - END OF TEST HOLE

9 SS 11/29/24/29 25 20%PPM

11.3

10.7

10 SS 10/22/34/32 ND 100%

12.0

11.4

11 SS 09/27/41/42 25 90%PPM

12.8

12.2

12 SS 08/32/37/50 ND 90%13.6

13.3

13 SS 07/16/29/24 175 90% BTEX-F1toF4-pHPPM

14.3

13.7

14 SS 05/10/17/19 ND 90%

15.1

14.5

15 SS 03/10/13/15 150 90% BTEX-F1toF4-PAHs-pHPPM

15.8

15.2

16 SS 04/15/27/32 50 100%PPM

16.6

16.0

SILTY SAND : Light brown, loose to very dense,SAND, fine grained, becomes coarse grained at13.2m, silty, damp, wet at 15.2m, petroleum odourbetween 13.7m and 14.3m and between 15.2mand 15.9m.

16.6


PROJECT #

TECHNICIAN

07126

D.Doherty


SHEET#

WEATHER:

ONE of TWO


Overcast, -1C




SA

MP

LE

#

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ANALYSISREQUESTED



(Blo

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per

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1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 01/02/02/02 ND 85%

0.6

2 SS 01/02/02/01 ND 85%

1.4

0.8

3 SS 02/06/07/08 25 85%PPM

2.1

1.5

4 SS 03/08/11/11 25 90%PPM

3.7

3.0

5 SS 06/11/17/12 50 90%PPM

5.2

4.6

6 SS 05/10/12/15 50 85%PPM

6.7

6.1

7 SS 07/20/27/35 ND 90%

8.2

7.6

8 SS 10/31/45/40 25 100%PPM

9.8

9.1

TOPSOIL : Dark Brown, very soft, TOPSOIL, damp.0.2

SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, damp, wet at15.2m, petroleum odour between 14.5m and15.1m.


PROJECT #

TECHNICIAN

07126

D.Doherty


SHEET#

WEATHER:

TWO of TWO


Overcast, -1C




SA

MP

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#

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ANALYSISREQUESTED



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12

13

14

15

16

17

18

19 19

18

17

16

15

14

13

12

11


9 SS 08/21/41/40 ND 100%

11.3

10.7

10 SS 08/21/28/30 25 100%PPM

12.0

11.4

11 SS 08/13/36/47 25 100%PPM

12.8

12.2

12 SS 06/12/15/17 25 90%PPM

13.6

13.0

13 SS 05/17/21/23 25 90%PPM

14.3

13.7


15.1

14.5


15.8

15.2

16 SS 12/05/12/10 25 85%PPM

16.6

16.0

SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, damp, wet at15.2m, petroleum odour between 14.5m and15.1m.

16.6


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

ONE of TWO


Overcast, -1C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 06/18/21/22 ND 100%

4.3

3.7

2 SS 08/12/15/14 25 90%PPM

5.0

4.4

3 SS 08/11/18/24 150 85%PPM

5.8

5.2

4 SS 11/24/34/32 100 85%PPM

6.6

5.9

5 SS 05/07/11/17 125 100%PPM

7.3

6.7

6 SS 05/14/38/56 200 100%PPM

8.1

7.5

7 SS 10/39/38/50 275 100%PPM

8.8

8.2


9.6

9.0

9 SS 11/40/50/50 150 85%9.8

FILL : Light brown, dense, SAND (FILL), damp.

4.3SILTY SAND : Light Brown, compact to verydense, SAND, medium/fine grained, silty, damp,wet at 15.1m, petroleum odour and stainingbetween 5.2m and 15.7m.


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

TWO of TWO


Overcast, -1C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

11

12

13

14

15

16

17

18

19 19

18

17

16

15

14

13

12

11


9 SS 11/40/50/50 150 85%PPM

10.4

10 SS 04/23/25/40 125 85%PPM

11.1

10.5

11 SS 10/24/25/50 300 85%PPM

11.9

11.3

12 SS 10/21/30/45 250 85%PPM

12.6

12.0

13 SS 08/28/37/41 250 85%PPM

13.4

12.8

14 SS 06/23/36/50 250 100%PPM

14.2

13.6

15 SS 20/27/29/32 250 100%PPM

14.9

14.3

16 SS 05/14/35/27 275 100%PPM

15.7

15.1


16.5

15.8

SILTY SAND : Light Brown, compact to verydense, SAND, medium/fine grained, silty, damp,wet at 15.1m, petroleum odour and stainingbetween 5.2m and 15.7m.

16.6


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

ONE of TWO

EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:

Overcast, -5C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 01/01/01/01 ND 100%

0.6

2 SS 02/02/02/02 25 65% PAHs-pHPPM

1.4

0.8

3 SS 03/06/12/11 ND 100%

2.1

1.5

4 SS 07/14/14/19 25 85%PPM

3.7

3.0

5 SS 07/16/18/24 25 90%PPM

5.2

4.6

6 SS 07/10/17/22 25 85%PPM

6.7

6.1

7 SS 10/20/25/31 25 100%PPM

8.2

7.6

8 SS 06/16/13/13 25 100%PPM

9.8

9.1

TOPSOIL : Dark Brown, very soft, TOPSOIL, damp. 0.1SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 15.2m, petroleum odour between 13.7mand 14.3m.


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

TWO of TWO


Overcast, -5C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

11

12

13

14

15

16

17

18

19 19

18

17

16

15

14

13

12

11


9 SS 10/20/24/32 50 100%PPM

11.3

10.7

10 SS 05/23/30/33 50 90%PPM

12.8

12.2

11 SS 07/20/26/30 25 85%PPM

13.6

13.0


14.3

13.7

13 SS 05/11/14/15 50 85%PPM

15.1

14.5


15.8

15.2

15 SS 04/15/18/25 25 85%PPM

16.6

16.0

SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 15.2m, petroleum odour between 13.7mand 14.3m.

16.8


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

ONE of TWO


Clear, -15C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 01/01/01/01 ND 60%

0.6

2 SS 02/02/03/02 ND 60% PAHs-pH

1.4

0.8

3 SS 02/03/04/07 ND 75%

2.1

1.5

4 SS 07/10/14/20 ND 90%

3.7

3.0

5 SS 06/10/15/25 25 85%PPM

5.2

4.6

6 SS 05/19/21/30 25 90%PPM

6.7

6.1

7 SS 10/20/22/26 25 100%PPM

8.2

7.6

8 SS 08/21/24/30 25 75%PPM

9.8

9.1

TOPSOIL : Dark Brown, very soft, TOPSOIL, damp. 0.1SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 16.0m, petroleum odour between 13.7mand 16.6m.


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

TWO of TWO


Clear, -15C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

11

12

13

14

15

16

17

18

19 19

18

17

16

15

14

13

12

11


9 SS 08/21/26/32 50 90%PPM

11.3

10.7

10 SS 06/24/29/50 50 90%PPM

12.8

12.2

11 SS 11/21/35/50 50 90%PPM

13.6

13.0

12 SS 08/12/21/31 25 65%PPM

14.3

13.7

13 SS 06/18/29/40 50 90%PPM

15.1

14.5


15.8

15.2


16.6

16.0

SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 16.0m, petroleum odour between 13.7mand 16.6m.

16.8


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

ONE of TWO


Clear, -15C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

1

2

3

4

5

6

7

8

9 9

8

7

6

5

4

3

2

1

Continued...

1 SS 06/02/02/03 ND 40%

0.6

2 SS 02/05/03/01 ND 50%

1.4

0.8

3 SS 02/03/05/06 25 60%PPM

2.1

1.5

4 SS 07/12/10/21 ND 85%

3.7

3.0

5 SS 05/16/18/31 ND 90%

5.2

4.6

6 SS 08/21/23/28 ND 75%

6.7

6.1

7 SS 05/21/24/29 25 90%PPM

8.2

7.6

8 SS 10/20/23/29 50 90%PPM

9.8

9.1

TOPSOIL : Dark Brown, soft, TOPSOIL, damp.0.2

SILTY SAND : Light Brown, loose to very dense,SAND, medium/fine grained, silty, damp, wet at15.2m.


PROJECT #

TECHNICIAN

07126

D. Doherty


SHEET#

WEATHER:

TWO of TWO


Clear, -15C




SA

MP

LE

#

CO

UN

T

BL

OW

TY

PE

RE

AD

ING

VA

PO

UR

RE

CO

VE

RY

%

ST

RA

TA

PL

OT

DE

PT

H (

M)

DE

PT

H (

M)

ANALYSISREQUESTED



(Blo

ws

per

ft)

11

12

13

14

15

16

17

18

19 19

18

17

16

15

14

13

12

11


9 SS 12/21/24/34 25 85%PPM

11.3

10.7

10 SS 12/24/37/42 25 90%PPM

12.8

12.2

11 SS 10/20/26/30 25 85%PPM

13.6

13.0

12 SS 10/20/34/36 25 90%PPM

14.3

13.7

13 SS 10/21/30/38 50 85%PPM

15.1

14.5


15.8

15.2


16.6

16.0

SILTY SAND : Light Brown, loose to very dense,SAND, medium/fine grained, silty, damp, wet at15.2m.

16.8


��

��

Attached are copies of the original Certificates of Analysis provided by thelaboratory. The data contained in these analyses is to be read only inconjunction with the report to which it is attached. For interpretation ofthe chemical data, see the attached text.

All samples are submitted to and reported by the laboratory usingpurchase order numbers and sample location codes. These are onlydiscernable to persons familiar with the purchase order system and thelocation codes. For descriptions of the locations of the samples, see theattached text.

Not all data contained in the original laboratory certificate of analysis mayhave been referenced in the report. Samples may have been submitted astravel or field blanks or as duplicates. Some samples may be for controlpurposes and represent soil that is no longer on the site and is notrelevant to the report.

Since the laboratory data contains scientific terms and references, onlytrained persons familiar with sampling and laboratory methods shouldattempt to interpret the raw data.

Your P.O. #: 07126 Your Project #: 07126 Your C.O.C. #: 00553371

Attention: Bernard ChanBarenco Inc2561 Stouffville RdPO Box 295Gormley, ONL0H 1G0

Report Date: 2008/02/04

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: A805178Received: 2008/01/17, 14:24

Sample Matrix: Soil# Samples Received: 2

Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Soil (AA PIRI) ( 1 ) 2 N/A 2008/01/23 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Soil 2 2008/01/21 2008/01/22 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Soil 2 2008/01/21 2008/01/21 CAM SOP-00316 CCME CWS Moisture ( 1 ) 2 N/A 2008/01/21 ATL SOP 00001 R2 MOE Handbook 1983 MOISTURE 2 N/A 2008/01/19 Ont SOP-0114 MOE HANDBOOK(1983) PAH Compounds in Soil by GC/MS (SIM) 1 2008/01/18 2008/01/18 SOP - 00318 EPA 8270 pH CaCl2 EXTRACT 2 N/A 2008/01/23 Ont SOP-0067 4 5 0 0 - H + B VPH in Soil (PIRI2) ( 1 ) 2 N/A 2008/01/22 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Soil ( 1 ) 2 N/A 2008/01/24 n/a Based on Atl. PIRI

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed by Bedford

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

SARA SAROOP, Campobello Customer serviceEmail: [email protected]# (905) 817-5700 Ext:5819

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.

For Service Group specific validation please refer to the Validation Signature Page

Total cover pages: 1

Page 1 of 11

Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:

Your P.O. #: 07126Sampler Initials:

RESULTS OF ANALYSES OF SOIL

Maxxam ID W 8 0 9 9 7 W 8 0 9 9 8Sampling Date 2008/01/16 2008/01/16

12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 QC Batch TH101-15 R D L QC Batch

INORGANICS

Moisture % 8 1443911 16 1 1443911

Available (CaCl2) pH pH 7.80 1446001 7.96 1445535

RDL = Reportable Detection LimitQC Batch = Quality Control Batch

Page 2 of 11



ATLANTIC RBCA HYDROCARBONS (SOIL)


12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 R D L TH101-15 R D L QC Batch

TPH COMPOUNDS

Benzene mg/kg ND 0.3 ND 0.03 1444618

Toluene mg/kg ND 0.3 ND 0.03 1444618

Ethylbenzene mg/kg ND 0.3 ND 0.03 1444618

Xylene (Total) mg/kg 14 0.5 ND 0.05 1444618

Aliphatic >C6-C8 mg/kg 37 1 ND 0.1 1444618

Aliphatic >C8-C10 mg/kg 1400 4 ND 0.4 1444618

>C8-C10 Aromatics (-EX) mg/kg 200 2 ND 0.2 1444618

Aliphatic >C10-C12 mg/kg 3200 8.0 ND 8.0 1444005

Aliphatic >C12-C16 mg/kg 11000 15 ND 15 1444005

Aliphatic >C16-C21 mg/kg 4900 15 ND 15 1444005

Aliphatic >C21-<C32 mg/kg 520 15 ND 15 1444005

Aromatic >C10-C12 mg/kg 850 4.0 ND 4.0 1444005

Aromatic >C12-C16 mg/kg 3500 15 ND 15 1444005

Aromatic >C16-C21 mg/kg 2100 15 ND 15 1444005

Aromatic >C21-<C32 mg/kg 620 15 ND 15 1444005

Modified TPH (Tier 2) mg/kg 28000 20 ND 20 1443083

Surrogate Recovery (%)

Isobutylbenzene - Extractable % 57 92 1444005

Isobutylbenzene - Volatile % 81 ( 1 ) 111 1444618

n-Dotriacontane - Extractable % 82 ( 2 ) 80 1444005

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Elevated VPH RDL(s) due to sample dilution.( 2 ) Fuel oil fraction. TEH surrogate(s) not within acceptance limits. Analysis was repeated withsimilar results.

Page 3 of 11



SEMI-VOLATILE ORGANICS BY GC-MS (SOIL)

Maxxam ID W 8 0 9 9 8Sampling Date 2008/01/16

12:15COC Number 00553371 U n i t s TH101-15 R D L QC Batch

PAHs

Acenaphthene ug/g ND 0.01 1443550

Acenaphthylene ug/g ND 0.005 1443550

Anthracene ug/g ND 0.005 1443550

Benzo(a)anthracene ug/g ND 0.01 1443550

Benzo(a)pyrene ug/g ND 0.005 1443550

Benzo(b/j)fluoranthene ug/g ND 0.005 1443550

Benzo(g,h,i)perylene ug/g ND 0.02 1443550

Benzo(k)fluoranthene ug/g ND 0.01 1443550

Chrysene ug/g ND 0.01 1443550

Dibenz(a,h)anthracene ug/g ND 0.02 1443550

Fluoranthene ug/g ND 0.005 1443550

Fluorene ug/g ND 0.005 1443550

Indeno(1,2,3-cd)pyrene ug/g ND 0.02 1443550

1-Methylnaphthalene ug/g ND 0.005 1443550


Naphthalene ug/g ND 0.005 1443550

Phenanthrene ug/g ND 0.005 1443550

Pyrene ug/g ND 0.005 1443550


D10-Anthracene % 113 1443550

D14-Terphenyl (FS) % 109 1443550

D7-Quinoline % 75 1443550

D8-Acenaphthylene % 71 1443550

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch

Page 4 of 11



PETROLEUM HYDROCARBONS (CCME)


12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 TH101-15 R D L QC Batch

F1 PHC and BTEX

Benzene ug/g ND ND 0.02 1443986

Toluene ug/g ND ND 0.02 1443986

Ethylbenzene ug/g ND ND 0.02 1443986

o-Xylene ug/g 0.40 ND 0.02 1443986

p+m-Xylene ug/g 0.22 ND 0.04 1443986

Total Xylenes ug/g 0.62 ND 0.04 1443986

F1 (C6-C10) ug/g 92 ND 10 1443986

F1 (C6-C10) - BTEX ug/g 92 ND 10 1443986

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/g 2900 ND 10 1443839

F3 (C16-C34 Hydrocarbons) ug/g 2200 ND 10 1443839

F4 (C34-C50 Hydrocarbons) ug/g ND ND 10 1443839

Reached Baseline at C50 ug/g Yes Yes 1443839


1,4-Difluorobenzene % 103 106 1443986

4-Bromofluorobenzene % 96 94 1443986

D10-Ethylbenzene % 111 112 1443986

D4-1,2-Dichloroethane % 101 98 1443986

o-Terphenyl % 117 96 1443839


Page 5 of 11



GENERAL COMMENTS

Results relate only to the items tested.

Page 6 of 11

Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:

Quality Assurance ReportMaxxam Job Number: MA805178

QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits

1443550 MWG MATRIX SPIKE[W80998-01] D10-Anthracene 2008/01/18 104 % 30 - 130

D14-Terphenyl (FS) 2008/01/18 105 % 30 - 130D7-Quinoline 2008/01/18 86 % 30 - 130D8-Acenaphthylene 2008/01/18 82 % 30 - 130Acenaphthene 2008/01/18 121 % 30 - 130Acenaphthylene 2008/01/18 90 % 30 - 130Anthracene 2008/01/18 102 % 30 - 130Benzo(a)anthracene 2008/01/18 108 % 30 - 130Benzo(a)pyrene 2008/01/18 112 % 30 - 130Benzo(b/j)fluoranthene 2008/01/18 108 % 30 - 130Benzo(g,h,i)perylene 2008/01/18 93 % 30 - 130Benzo(k)fluoranthene 2008/01/18 109 % 30 - 130Chrysene 2008/01/18 104 % 30 - 130Dibenz(a,h)anthracene 2008/01/18 87 % 30 - 130Fluoranthene 2008/01/18 110 % 30 - 130Fluorene 2008/01/18 109 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/18 83 % 30 - 1301-Methylnaphthalene 2008/01/18 97 % 30 - 1302-Methylnaphthalene 2008/01/18 95 % 30 - 130Naphthalene 2008/01/18 96 % 30 - 130Phenanthrene 2008/01/18 100 % 30 - 130Pyrene 2008/01/18 106 % 30 - 130

Spiked Blank D10-Anthracene 2008/01/18 112 % 30 - 130D14-Terphenyl (FS) 2008/01/18 107 % 30 - 130D7-Quinoline 2008/01/18 96 % 30 - 130D8-Acenaphthylene 2008/01/18 88 % 30 - 130Acenaphthene 2008/01/18 125 % 30 - 130Acenaphthylene 2008/01/18 98 % 30 - 130Anthracene 2008/01/18 112 % 30 - 130Benzo(a)anthracene 2008/01/18 109 % 30 - 130Benzo(a)pyrene 2008/01/18 112 % 30 - 130Benzo(b/j)fluoranthene 2008/01/18 109 % 30 - 130Benzo(g,h,i)perylene 2008/01/18 95 % 30 - 130Benzo(k)fluoranthene 2008/01/18 110 % 30 - 130Chrysene 2008/01/18 105 % 30 - 130Dibenz(a,h)anthracene 2008/01/18 92 % 30 - 130Fluoranthene 2008/01/18 116 % 30 - 130Fluorene 2008/01/18 114 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/18 87 % 30 - 1301-Methylnaphthalene 2008/01/18 104 % 30 - 1302-Methylnaphthalene 2008/01/18 102 % 30 - 130Naphthalene 2008/01/18 101 % 30 - 130Phenanthrene 2008/01/18 112 % 30 - 130Pyrene 2008/01/18 109 % 30 - 130

Method Blank D10-Anthracene 2008/01/18 105 % 30 - 130D14-Terphenyl (FS) 2008/01/18 99 % 30 - 130D7-Quinoline 2008/01/18 81 % 30 - 130D8-Acenaphthylene 2008/01/18 78 % 30 - 130Acenaphthene 2008/01/18 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/18 ND, RDL=0.005 ug/gAnthracene 2008/01/18 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/18 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/18 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/18 ND, RDL=0.005 ug/g

Page 7 of 11


Quality Assurance Report (Continued)Maxxam Job Number: MA805178


1443550 MWG Method Blank Benzo(g,h,i)perylene 2008/01/18 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/18 ND, RDL=0.01 ug/gChrysene 2008/01/18 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/18 ND, RDL=0.02 ug/gFluoranthene 2008/01/18 ND, RDL=0.005 ug/gFluorene 2008/01/18 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/18 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/18 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/18 ND, RDL=0.005 ug/gNaphthalene 2008/01/18 ND, RDL=0.005 ug/gPhenanthrene 2008/01/18 ND, RDL=0.005 ug/gPyrene 2008/01/18 ND, RDL=0.005 ug/g

RPD [ W 8 0 9 9 8 - 0 1 ] Acenaphthene 2008/01/18 NC % 50Acenaphthylene 2008/01/18 NC % 50Anthracene 2008/01/18 NC % 50Benzo(a)anthracene 2008/01/18 NC % 50Benzo(a)pyrene 2008/01/18 NC % 50Benzo(b/j)fluoranthene 2008/01/18 NC % 50Benzo(g,h,i)perylene 2008/01/18 NC % 50Benzo(k)fluoranthene 2008/01/18 NC % 50Chrysene 2008/01/18 NC % 50Dibenz(a,h)anthracene 2008/01/18 NC % 50Fluoranthene 2008/01/18 NC % 50Fluorene 2008/01/18 NC % 50Indeno(1,2,3-cd)pyrene 2008/01/18 NC % 501-Methylnaphthalene 2008/01/18 NC % 502-Methylnaphthalene 2008/01/18 NC % 50Naphthalene 2008/01/18 NC % 50Phenanthrene 2008/01/18 NC % 50Pyrene 2008/01/18 NC % 50

1443806 MYG RPD Moisture 2008/01/19 0.8 % 501443823 MYG RPD Moisture 2008/01/19 0.9 % 501443839 JKA MATRIX SPIKE

[W80997-01] o-Terphenyl 2008/01/21 NC ( 1 ) % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 NC ( 2 ) % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/21 NC % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/21 NC % 60 - 130

Spiked Blank o-Terphenyl 2008/01/21 86 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 77 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/21 77 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/21 77 % 60 - 130

Method Blank o-Terphenyl 2008/01/21 87 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/gF3 (C16-C34 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/gF4 (C34-C50 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/g

RPD [ W 8 0 9 9 7 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/21 22.1 % 50F3 (C16-C34 Hydrocarbons) 2008/01/21 28.0 % 50F4 (C34-C50 Hydrocarbons) 2008/01/21 NC % 50

1443986 AGA MATRIX SPIKE[W80997-01] 1,4-Difluorobenzene 2008/01/22 101 % 60 - 140

4-Bromofluorobenzene 2008/01/22 97 % 60 - 140D10-Ethylbenzene 2008/01/22 123 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 99 % 60 - 140Benzene 2008/01/22 110 % 60 - 140Toluene 2008/01/22 116 % 60 - 140

Page 8 of 11




1443986 AGA MATRIX SPIKE[W80997-01] Ethylbenzene 2008/01/22 116 % 60 - 140

o-Xylene 2008/01/22 116 % 60 - 140p+m-Xylene 2008/01/22 121 % 60 - 140F1 (C6-C10) 2008/01/22 NC ( 3 ) % 60 - 140

Spiked Blank 1,4-Difluorobenzene 2008/01/22 105 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 107 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 98 % 60 - 140Benzene 2008/01/22 99 % 60 - 140Toluene 2008/01/22 105 % 60 - 140Ethylbenzene 2008/01/22 104 % 60 - 140o-Xylene 2008/01/22 106 % 60 - 140p+m-Xylene 2008/01/22 109 % 60 - 140F1 (C6-C10) 2008/01/22 93 % 60 - 140

Method Blank 1,4-Difluorobenzene 2008/01/22 103 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 99 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 101 % 60 - 140Benzene 2008/01/22 ND, RDL=0.02 ug/gToluene 2008/01/22 ND, RDL=0.02 ug/gEthylbenzene 2008/01/22 ND, RDL=0.02 ug/go-Xylene 2008/01/22 ND, RDL=0.02 ug/gp+m-Xylene 2008/01/22 ND, RDL=0.04 ug/gTotal Xylenes 2008/01/22 ND, RDL=0.04 ug/gF1 (C6-C10) 2008/01/22 ND, RDL=10 ug/gF1 (C6-C10) - BTEX 2008/01/22 ND, RDL=10 ug/g

RPD [ W 8 0 9 9 7 - 0 1 ] Benzene 2008/01/22 NC % 50Toluene 2008/01/22 NC % 50Ethylbenzene 2008/01/22 NC % 50o-Xylene 2008/01/22 25.6 % 50p+m-Xylene 2008/01/22 27.6 % 50Total Xylenes 2008/01/22 26.3 % 50F1 (C6-C10) 2008/01/22 38.4 % 50F1 (C6-C10) - BTEX 2008/01/22 38.5 % 50

1444005 KKE Spiked Blank Aliphatic >C10-C12 2008/01/23 87 % 30 - 130Aliphatic >C12-C16 2008/01/23 87 % 30 - 130Aliphatic >C16-C21 2008/01/23 87 % 30 - 130Aliphatic >C21-<C32 2008/01/23 87 % 30 - 130Aromatic >C10-C12 2008/01/23 122 % 30 - 130Aromatic >C12-C16 2008/01/23 111 % 30 - 130Aromatic >C16-C21 2008/01/23 105 % 30 - 130Aromatic >C21-<C32 2008/01/23 98 % 30 - 130

Method Blank Isobutylbenzene - Extractable 2008/01/23 92 % 30 - 130n-Dotriacontane - Extractable 2008/01/23 86 % 30 - 130Aliphatic >C10-C12 2008/01/23 ND, RDL=8 mg/kgAliphatic >C12-C16 2008/01/23 ND, RDL=15 mg/kgAliphatic >C16-C21 2008/01/23 ND, RDL=15 mg/kgAliphatic >C21-<C32 2008/01/23 ND, RDL=15 mg/kgAromatic >C10-C12 2008/01/23 ND, RDL=4 mg/kgAromatic >C12-C16 2008/01/23 ND, RDL=15 mg/kgAromatic >C16-C21 2008/01/23 ND, RDL=15 mg/kgAromatic >C21-<C32 2008/01/23 ND, RDL=15 mg/kg

RPD [ W 8 0 9 9 7 - 0 3 ] Aliphatic >C10-C12 2008/01/23 15.0 % 50Aliphatic >C12-C16 2008/01/23 16.9 % 50

Page 9 of 11




1444005 KKE RPD [ W 8 0 9 9 7 - 0 3 ] Aliphatic >C16-C21 2008/01/23 14.0 % 50Aliphatic >C21-<C32 2008/01/23 13.8 % 50Aromatic >C10-C12 2008/01/23 8.0 % 50Aromatic >C12-C16 2008/01/23 7.3 % 50Aromatic >C16-C21 2008/01/23 9.0 % 50Aromatic >C21-<C32 2008/01/23 15.3 % 50

1444618 LMU Spiked Blank Isobutylbenzene - Volatile 2008/01/22 102 % 60 - 140Benzene 2008/01/22 94 % 60 - 140Toluene 2008/01/22 92 % 60 - 140Ethylbenzene 2008/01/22 92 % 60 - 140Xylene (Total) 2008/01/22 90 % 60 - 140

Method Blank Isobutylbenzene - Volatile 2008/01/22 97 % 60 - 140Benzene 2008/01/22 ND, RDL=0.03 mg/kgToluene 2008/01/22 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/22 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/22 ND, RDL=0.05 mg/kgAliphatic >C6-C8 2008/01/22 ND, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/22 ND, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/22 0.2, RDL=0.1 mg/kg

ND = Not detectedNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample( 1 ) The extraction surrogate recovery is not calculated due to Matrix interferences.( 2 ) Matrix spike recoveries were not calculated (NC) because of high concentration of target compounds in the parent sample.( 3 ) The recovery in the matrix spiked is not calculated (NC) due to high concentration of this compound in the parent sample.

Page 10 of 11

Validation Signature Page

Maxxam Job #: A805178

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

BRAD NEWMAN, Scientific Specialist

JAMES MACDONALD, Organics Manager

MEDHAT RISKALLAH, Manager, Hydrocarbon Department

MICHAEL WANG,

SUZANA POPOVIC, Supervisor, Hydrocarbons

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.

Page 11 of 11

Your Project #: MA805178 Site: 07126

Attention: SUB CONTRACTORMAXXAM ANALYTICS INC.CAMPOBELLO6740 CAMPOBELLO ROADMISSISSAUGA, ONCANADA L5N 2L8





Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 2 2008/01/22 2008/01/22 CAL SOP-00086 CCME PHC-CWS Aliphatic and Aromatic Fractions C10-C50 1 2008/01/22 2008/01/30 CAL SOP-00184 CCME PHC-CWS Moisture 2 N/A 2008/01/22 CAL SOP-00023 McKeague MSSMA 2.411


Encryption Key


HEATHER ECCLES,Email: [email protected]# (403) 291-3077




Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468

Page 1 of 7

MAXXAM ANALYTICS INC.Maxxam Job #: A802778 Client Project #: MA805178Report Date: 2008/02/01 Site Reference: 07126

Sampler Initials:

RESULTS OF CHEMICAL ANALYSES OF SOIL

Maxxam ID I 6 2 4 7 8 I 6 2 4 8 2Sampling Date 2008/01/16 2008/01/16 U n i t s TH101-13 TH101-15 R D L QC Batch

(W80997-02R) (W80998-02R)

Physical Properties

Moisture % 9.2 15.9 0.3 2079421

RDL = Reportable Detection Limit

Page 2 of 7


Sampler Initials:


Maxxam ID I 6 2 4 7 8 I 6 2 4 8 2Sampling Date 2008/01/16 2008/01/16 U n i t s TH101-13 QC Batch TH101-15 R D L QC Batch

(W80997-02R) (W80998-02R)

Ext. Pet. Hydrocarbon

F2 (C10-C16 Hydrocarbons) mg/kg 12000 2082057 <10 10 2082057



Reached Baseline at C50 mg/kg Yes 2082057 Yes N/A 2082057

Hydrocarbons

>C10 - C12 Aliphatic mg/kg 2460 2079711 N/A 5 2079711

>C10 - C12 Aromatic mg/kg 92 2079711 N/A 5 2079711





>C21 - C34 Aliphatic mg/kg <10 2079711 N/A 10 2079711


>C34 Aliphatic (up to C50) mg/kg <10 2079711 N/A 10 2079711

>C34 Aromatic (up to C50) mg/kg 41 2079711 N/A 10 2079711


O-TERPHENYL (sur.) % 112 2079711 100 N/A 2082057

N/A = Not ApplicableRDL = Reportable Detection Limit

Page 3 of 7


Sampler Initials:

PETROLEUM HYDROCARBONS (CCME) Comments

Sample I62478-01 CCME Hydrocarbons (F2-F4 in soil): Matrix spike recovery non calculable, due to high concentration of original analyte.

Sample I62482-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are <DL.

Sample I62478-01 Aliphatic and Aromatic Fractions C10-C50: Matrix spike recovery non calculable, due to high concentration of original analyte.


Page 4 of 7

MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA805178P.O. #: Site Reference: 07126

Quality Assurance ReportMaxxam Job Number: CA802778


2079421 RM2 RPD Moisture 2008/01/22 7.0 % 202079711 LSH Calibration Check >C10 - C12 Aliphatic 2008/01/30 94 % 80 - 120

>C10 - C12 Aromatic 2008/01/30 97 % 80 - 120>C12 - C16 Aliphatic 2008/01/30 95 % 80 - 120>C12 - C16 Aromatic 2008/01/30 97 % 80 - 120>C16 - C21 Aliphatic 2008/01/30 94 % 80 - 120>C16 - C21 Aromatic 2008/01/30 98 % 80 - 120>C21 - C34 Aliphatic 2008/01/30 92 % 80 - 120>C21 - C34 Aromatic 2008/01/30 95 % 80 - 120>C34 Aliphatic (up to C50) 2008/01/30 93 % 80 - 120>C34 Aromatic (up to C50) 2008/01/30 90 % 80 - 120

MATRIX SPIKE[I62478-01] O-TERPHENYL (sur.) 2008/01/30 88 % 30 - 130

>C21 - C34 Aliphatic 2008/01/30 93 % 50 - 130>C34 Aliphatic (up to C50) 2008/01/30 108 % 50 - 130

QC STANDARD >C10 - C12 Aliphatic 2008/01/30 77 % 70 - 130>C10 - C12 Aromatic 2008/01/30 95 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 84 % 70 - 130>C12 - C16 Aromatic 2008/01/30 96 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 87 % 70 - 130>C16 - C21 Aromatic 2008/01/30 94 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 96 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 88 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 129 % 70 - 130

SPIKE O-TERPHENYL (sur.) 2008/01/30 79 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 71 % 70 - 130>C10 - C12 Aromatic 2008/01/30 121 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 83 % 70 - 130>C12 - C16 Aromatic 2008/01/30 117 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 78 % 70 - 130>C16 - C21 Aromatic 2008/01/30 72 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 89 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 125 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 73 % 70 - 130

BLANK O-TERPHENYL (sur.) 2008/01/30 100 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 <5 mg/kg>C10 - C12 Aromatic 2008/01/30 <5 mg/kg>C12 - C16 Aliphatic 2008/01/30 <10 mg/kg>C12 - C16 Aromatic 2008/01/30 <10 mg/kg>C16 - C21 Aliphatic 2008/01/30 <10 mg/kg>C16 - C21 Aromatic 2008/01/30 <10 mg/kg>C21 - C34 Aliphatic 2008/01/30 <10 mg/kg>C21 - C34 Aromatic 2008/01/30 <10 mg/kg>C34 Aliphatic (up to C50) 2008/01/30 <10 mg/kg>C34 Aromatic (up to C50) 2008/01/30 <10 mg/kg

RPD >C10 - C12 Aliphatic 2008/01/30 33.1 % 40>C10 - C12 Aromatic 2008/01/30 23.9 % 40>C12 - C16 Aliphatic 2008/01/30 33.1 % 40>C12 - C16 Aromatic 2008/01/30 13.3 % 40>C16 - C21 Aliphatic 2008/01/30 30.5 % 40>C16 - C21 Aromatic 2008/01/30 5.0 % 40>C21 - C34 Aliphatic 2008/01/30 25.3 % 40>C21 - C34 Aromatic 2008/01/30 3.7 % 40


Page 5 of 7


Quality Assurance Report (Continued)Maxxam Job Number: CA802778


2079711 LSH RPD >C34 Aliphatic (up to C50) 2008/01/30 NC % 40>C34 Aromatic (up to C50) 2008/01/30 15.7 % 40

2082057 LSH Calibration Check F2 (C10-C16 Hydrocarbons) 2008/01/22 105 % 80 - 120F3 (C16-C34 Hydrocarbons) 2008/01/22 104 % 80 - 120F4 (C34-C50 Hydrocarbons) 2008/01/22 104 % 80 - 120


F2 (C10-C16 Hydrocarbons) 2008/01/22 NA % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 NA % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 NA % 50 - 130

QC STANDARD F2 (C10-C16 Hydrocarbons) 2008/01/22 103 % 85 - 115F3 (C16-C34 Hydrocarbons) 2008/01/22 110 % 85 - 115F4 (C34-C50 Hydrocarbons) 2008/01/22 106 % 85 - 115

SPIKE O-TERPHENYL (sur.) 2008/01/22 85 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 100 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 98 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 113 % 50 - 130

BLANK O-TERPHENYL (sur.) 2008/01/22 99 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 <10 mg/kgF3 (C16-C34 Hydrocarbons) 2008/01/22 <10 mg/kgF4 (C34-C50 Hydrocarbons) 2008/01/22 <10 mg/kgReached Baseline at C50 2008/01/22 YES mg/kg

RPD [ I 6 2 4 7 8 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/22 3.7 % 50F3 (C16-C34 Hydrocarbons) 2008/01/22 0.3 % 50F4 (C34-C50 Hydrocarbons) 2008/01/22 NC % 50Reached Baseline at C50 2008/01/22 NC % 50

NC = Non-calculableRPD = Relative Percent Difference


Page 6 of 7




LUBA SHYMUSHOVSKA,

VERONICA FALK,


Page 7 of 7










Encryption Key






Page 1 of 13




Maxxam ID W 8 5 4 8 3 W 8 5 4 8 4 W 8 5 4 8 5 W 8 5 4 8 6Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17

12:00 12:30 14:00 14:30COC Number 00553374 00553374 00553374 00553374 U n i t s TH102-14 TH102-15 TH103-8 TH103-17 R D L QC Batch

INORGANICS

Moisture % 11 20 17 16 1 1445659

Available (CaCl2) pH pH 7.96 7.78 7.89 7.91 1447134



10:00 13:00COC Number 00553374 00553374 U n i t s TH104-2 R D L QC Batch TH104-12 R D L QC Batch

INORGANICS

Moisture % 20 0.2 1445548 17 1 1445659





INORGANICS

Moisture % 16 1 1445659

Available (CaCl2) pH pH 7.95 1447134


Page 2 of 13




Maxxam ID W 8 5 4 8 3 W 8 5 4 8 4 W 8 5 4 8 5Sampling Date 2008/01/17 2008/01/17 2008/01/17

12:00 12:30 14:00COC Number 00553374 00553374 00553374 U n i t s TH102-14 TH102-15 TH103-8 R D L QC Batch

TPH COMPOUNDS

Benzene mg/kg ND ND ND 0.03 1446082

Toluene mg/kg ND ND ND 0.03 1446082

Ethylbenzene mg/kg ND ND 0.05 0.03 1446082

Xylene (Total) mg/kg ND ND 2.0 0.05 1446082

Aliphatic >C6-C8 mg/kg ND ND 6.7 0.2 1446082

Aliphatic >C8-C10 mg/kg ND ND 170 0.7 1446082

>C8-C10 Aromatics (-EX) mg/kg ND ND 16 0.1 1446082

Aliphatic >C10-C12 mg/kg ND ND 370 8.0 1445718

Aliphatic >C12-C16 mg/kg ND ND 920 15 1445718

Aliphatic >C16-C21 mg/kg ND ND 880 15 1445718

Aliphatic >C21-<C32 mg/kg ND ND 76 15 1445718

Aromatic >C10-C12 mg/kg ND ND 120 4.0 1445718

Aromatic >C12-C16 mg/kg ND ND 440 15 1445718

Aromatic >C16-C21 mg/kg ND ND 390 15 1445718

Aromatic >C21-<C32 mg/kg ND ND 88 15 1445718

Modified TPH (Tier 2) mg/kg ND ND 3500 20 1444752


Isobutylbenzene - Extractable % 82 76 73 1445718

Isobutylbenzene - Volatile % 102 110 77 1446082

n-Dotriacontane - Extractable % 78 91 90 ( 1 ) 1445718

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Fuel oil fraction.

Page 3 of 13






TPH COMPOUNDS



Ethylbenzene mg/kg ND ND ND 0.03 1446082

Xylene (Total) mg/kg ND ND ND 0.05 1446082

Aliphatic >C6-C8 mg/kg ND ND ND 0.2 1446082


>C8-C10 Aromatics (-EX) mg/kg ND ND ND 0.1 1446082


Aliphatic >C12-C16 mg/kg ND ND ND 15 1445718


Aliphatic >C21-<C32 mg/kg ND ND ND 15 1445718

Aromatic >C10-C12 mg/kg ND ND ND 4.0 1445718

Aromatic >C12-C16 mg/kg ND ND ND 15 1445718


Aromatic >C21-<C32 mg/kg ND ND ND 15 1445718

Modified TPH (Tier 2) mg/kg ND ND ND 20 1444752




n-Dotriacontane - Extractable % 93 86 91 1445718


Page 4 of 13






PAHs


















Pyrene ug/g ND 0.005 1445735


D10-Anthracene % 84 1445735

D14-Terphenyl (FS) % 100 1445735




Page 5 of 13






F1 PHC and BTEX

Benzene ug/g ND ND ND 0.02 1445289

Toluene ug/g ND ND ND 0.02 1445289

Ethylbenzene ug/g ND ND ND 0.02 1445289

o-Xylene ug/g ND ND 1.1 0.02 1445289

p+m-Xylene ug/g ND ND 0.38 0.04 1445289

Total Xylenes ug/g ND ND 1.5 0.04 1445289

F1 (C6-C10) ug/g ND ND 220 10 1445289

F1 (C6-C10) - BTEX ug/g ND ND 220 10 1445289

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/g ND ND 1900 10 1445221

F3 (C16-C34 Hydrocarbons) ug/g ND ND 1400 10 1445221

F4 (C34-C50 Hydrocarbons) ug/g ND ND ND 10 1445221

Reached Baseline at C50 ug/g Yes Yes Yes 1445221


1,4-Difluorobenzene % 103 107 101 1445289

4-Bromofluorobenzene % 94 100 97 1445289

D10-Ethylbenzene % 94 100 111 1445289

D4-1,2-Dichloroethane % 120 124 116 1445289

o-Terphenyl % 110 111 129 1445221


Page 6 of 13






F1 PHC and BTEX




o-Xylene ug/g ND ND ND 0.02 1445289

p+m-Xylene ug/g ND ND ND 0.04 1445289

Total Xylenes ug/g ND ND ND 0.04 1445289

F1 (C6-C10) ug/g ND ND ND 10 1445289

F1 (C6-C10) - BTEX ug/g ND ND ND 10 1445289

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/g 16 12 ND 10 1445221

F3 (C16-C34 Hydrocarbons) ug/g 16 12 ND 10 1445221






D10-Ethylbenzene % 87 93 93 1445289


o-Terphenyl % 109 111 110 1445221


Page 7 of 13



GENERAL COMMENTS

Note: F1BTEX - all soils were Methanol extracted on 2008/01/22


VPH in Soil (PIRI2): Elevated VPH RDL(s) due to detected levels in the method blank.


Page 8 of 13




1445221 BLZ MATRIX SPIKE o-Terphenyl 2008/01/22 97 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 87 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 87 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 87 % 60 - 130



RPD F2 (C10-C16 Hydrocarbons) 2008/01/22 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/22 24.5 % 50F4 (C34-C50 Hydrocarbons) 2008/01/22 11.0 % 50

1445289 DTI MATRIX SPIKE 1,4-Difluorobenzene 2008/01/22 101 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 98 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 101 % 60 - 140Benzene 2008/01/22 89 % 60 - 140Toluene 2008/01/22 89 % 60 - 140Ethylbenzene 2008/01/22 92 % 60 - 140o-Xylene 2008/01/22 97 % 60 - 140p+m-Xylene 2008/01/22 96 % 60 - 140F1 (C6-C10) 2008/01/22 99 % 60 - 140



RPD F1 (C6-C10) 2008/01/22 NC % 50F1 (C6-C10) - BTEX 2008/01/22 NC % 50

1445548 AC RPD [ W 8 5 4 8 7 - 0 1 ] Moisture 2008/01/23 1.0 % 501445718 KKE Spiked Blank Aliphatic >C10-C12 2008/01/25 78 % 30 - 130

Aliphatic >C12-C16 2008/01/25 78 % 30 - 130Aliphatic >C16-C21 2008/01/25 86 % 30 - 130Aliphatic >C21-<C32 2008/01/25 85 % 30 - 130Aromatic >C10-C12 2008/01/25 100 % 30 - 130

Page 9 of 13




1445718 KKE Spiked Blank Aromatic >C12-C16 2008/01/25 93 % 30 - 130Aromatic >C16-C21 2008/01/25 92 % 30 - 130Aromatic >C21-<C32 2008/01/25 89 % 30 - 130


RPD [ W 8 5 4 8 3 - 0 2 ] Aliphatic >C10-C12 2008/01/25 NC % 50Aliphatic >C12-C16 2008/01/25 NC % 50Aliphatic >C16-C21 2008/01/25 NC % 50Aliphatic >C21-<C32 2008/01/25 NC % 50Aromatic >C10-C12 2008/01/25 NC % 50Aromatic >C12-C16 2008/01/25 NC % 50Aromatic >C16-C21 2008/01/25 NC % 50Aromatic >C21-<C32 2008/01/25 NC % 50

1445719 SPU RPD [ W 8 5 4 8 9 - 0 1 ] Moisture 2008/01/23 0.6 % 501445735 PMO MATRIX SPIKE D10-Anthracene 2008/01/23 102 % 30 - 130

D14-Terphenyl (FS) 2008/01/23 99 % 30 - 130D7-Quinoline 2008/01/23 62 % 30 - 130D8-Acenaphthylene 2008/01/23 73 % 30 - 130Acenaphthene 2008/01/23 NC % 30 - 130Acenaphthylene 2008/01/23 NC % 30 - 130Anthracene 2008/01/23 NC ( 1 ) % 30 - 130Benzo(a)anthracene 2008/01/23 NC % 30 - 130Benzo(a)pyrene 2008/01/23 NC % 30 - 130Benzo(b/j)fluoranthene 2008/01/23 NC % 30 - 130Benzo(g,h,i)perylene 2008/01/23 NC % 30 - 130Benzo(k)fluoranthene 2008/01/23 NC % 30 - 130Chrysene 2008/01/23 NC % 30 - 130Dibenz(a,h)anthracene 2008/01/23 NC % 30 - 130Fluoranthene 2008/01/23 NC % 30 - 130Fluorene 2008/01/23 NC % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/23 NC % 30 - 1301-Methylnaphthalene 2008/01/23 NC % 30 - 1302-Methylnaphthalene 2008/01/23 NC % 30 - 130Naphthalene 2008/01/23 NC % 30 - 130Phenanthrene 2008/01/23 NC % 30 - 130Pyrene 2008/01/23 NC % 30 - 130

Spiked Blank D10-Anthracene 2008/01/23 114 % 30 - 130D14-Terphenyl (FS) 2008/01/23 111 % 30 - 130D7-Quinoline 2008/01/23 87 % 30 - 130D8-Acenaphthylene 2008/01/23 86 % 30 - 130Acenaphthene 2008/01/23 117 % 30 - 130Acenaphthylene 2008/01/23 91 % 30 - 130Anthracene 2008/01/23 111 % 30 - 130Benzo(a)anthracene 2008/01/23 102 % 30 - 130Benzo(a)pyrene 2008/01/23 111 % 30 - 130Benzo(b/j)fluoranthene 2008/01/23 111 % 30 - 130Benzo(g,h,i)perylene 2008/01/23 86 % 30 - 130

Page 10 of 13




1445735 PMO Spiked Blank Benzo(k)fluoranthene 2008/01/23 114 % 30 - 130Chrysene 2008/01/23 102 % 30 - 130Dibenz(a,h)anthracene 2008/01/23 77 % 30 - 130Fluoranthene 2008/01/23 109 % 30 - 130Fluorene 2008/01/23 108 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/23 77 % 30 - 1301-Methylnaphthalene 2008/01/23 97 % 30 - 1302-Methylnaphthalene 2008/01/23 101 % 30 - 130Naphthalene 2008/01/23 95 % 30 - 130Phenanthrene 2008/01/23 107 % 30 - 130Pyrene 2008/01/23 103 % 30 - 130

Method Blank D10-Anthracene 2008/01/23 107 % 30 - 130D14-Terphenyl (FS) 2008/01/23 95 % 30 - 130D7-Quinoline 2008/01/23 79 % 30 - 130D8-Acenaphthylene 2008/01/23 78 % 30 - 130Acenaphthene 2008/01/23 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/23 ND, RDL=0.005 ug/gAnthracene 2008/01/23 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/23 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/23 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/23 ND, RDL=0.005 ug/gBenzo(g,h,i)perylene 2008/01/23 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/23 ND, RDL=0.01 ug/gChrysene 2008/01/23 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/23 ND, RDL=0.02 ug/gFluoranthene 2008/01/23 ND, RDL=0.005 ug/gFluorene 2008/01/23 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/23 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/23 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/23 ND, RDL=0.005 ug/gNaphthalene 2008/01/23 ND, RDL=0.005 ug/gPhenanthrene 2008/01/23 ND, RDL=0.005 ug/gPyrene 2008/01/23 ND, RDL=0.005 ug/g

RPD D14-Terphenyl (FS) 2008/01/23 14.8 % N/AAcenaphthene 2008/01/23 1 3 6 ( 2 ) % 50Acenaphthylene 2008/01/23 6 9 . 8 ( 2 ) % 50Anthracene 2008/01/23 1 4 5 ( 2 ) % 50Benzo(a)anthracene 2008/01/23 1 3 7 ( 2 ) % 50Benzo(a)pyrene 2008/01/23 1 3 6 ( 2 ) % 50Benzo(b/j)fluoranthene 2008/01/23 1 3 3 ( 2 ) % 50Benzo(g,h,i)perylene 2008/01/23 1 4 6 ( 2 ) % 50Benzo(k)fluoranthene 2008/01/23 1 3 2 ( 2 ) % 50Chrysene 2008/01/23 1 2 4 ( 2 ) % 50Dibenz(a,h)anthracene 2008/01/23 1 3 8 ( 2 ) % 50Fluoranthene 2008/01/23 1 3 5 ( 2 ) % 50Fluorene 2008/01/23 1 1 8 ( 2 ) % 50Indeno(1,2,3-cd)pyrene 2008/01/23 1 3 7 ( 2 ) % 501-Methylnaphthalene 2008/01/23 7 7 . 1 ( 2 ) % 502-Methylnaphthalene 2008/01/23 8 1 . 6 ( 2 ) % 50Naphthalene 2008/01/23 5 5 . 5 ( 2 ) % 50Phenanthrene 2008/01/23 1 3 0 ( 2 ) % 50Pyrene 2008/01/23 1 4 0 ( 2 ) % 50

1445905 SPU RPD Moisture 2008/01/23 1.9 % 501446082 LMU MATRIX SPIKE

[W85483-02] Isobutylbenzene - Volatile 2008/01/25 90 % 60 - 140

Page 11 of 13




1446082 LMU MATRIX SPIKE[W85483-02] Benzene 2008/01/25 71 % 60 - 140

Toluene 2008/01/25 88 % 60 - 140Ethylbenzene 2008/01/25 71 % 60 - 140Xylene (Total) 2008/01/25 87 % 60 - 140

Spiked Blank Isobutylbenzene - Volatile 2008/01/25 93 % 60 - 140Benzene 2008/01/25 83 % 60 - 140Toluene 2008/01/25 83 % 60 - 140Ethylbenzene 2008/01/25 84 % 60 - 140Xylene (Total) 2008/01/25 83 % 60 - 140

Method Blank Isobutylbenzene - Volatile 2008/01/25 97 % 60 - 140Benzene 2008/01/25 ND, RDL=0.03 mg/kgToluene 2008/01/25 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/25 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/25 ND, RDL=0.05 mg/kgAliphatic >C6-C8 2008/01/25 0.1, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/25 0.6, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/25 ND, RDL=0.1 mg/kg

RPD [ W 8 5 4 8 3 - 0 2 ] Benzene 2008/01/25 NC % 50Toluene 2008/01/25 NC % 50Ethylbenzene 2008/01/25 NC % 50Xylene (Total) 2008/01/25 NC % 50Aliphatic >C6-C8 2008/01/25 NC % 50Aliphatic >C8-C10 2008/01/25 NC % 50>C8-C10 Aromatics (-EX) 2008/01/25 NC % 50

ND = Not detectedN/A = Not ApplicableNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample( 1 ) The recovery in the matrix spike was not calculated (NC). Because of the high concentration of this analyte in the parent sample, therelative difference between the spiked and unspiked concentrations is not sufficiently significant to permit a reliable recovery calculation.( 2 ) Duplicate results exceeded RPD acceptance criteria due to sample heterogeneity.

Page 12 of 13




EWA PRANJIC, M.Sc., C.Chem, Scientific Specialist

GREG GILBERT, Scientific Specialist


ALINA SEGAL, Manager Main Lab - Organics



Page 13 of 13







Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 6 2008/01/24 2008/01/24 CAL SOP-00086 CCME PHC-CWS Aliphatic and Aromatic Fractions C10-C50 1 2008/01/22 2008/01/30 CAL SOP-00184 CCME PHC-CWS Moisture 6 N/A 2008/01/24 CAL SOP-00023 McKeague MSSMA 2.411


Encryption Key







Page 1 of 8


Sampler Initials:

CCME F2-F4 (SOIL)

Maxxam ID I 6 4 4 2 2 I 6 4 4 4 7 I 6 4 4 4 8 I 6 4 4 4 9Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17 U n i t s TH102-15 THIO2-14 TH103-17 TH103-8 R D L QC Batch

(W85484-03R) (W85483-03R) (W85486-03R) (W85485-03R)


F2 (C10-C16 Hydrocarbons) mg/kg <10 <10 <10 2800 10 2083622

F3 (C16-C34 Hydrocarbons) mg/kg <10 <10 <10 1500 10 2083622

F4 (C34-C50 Hydrocarbons) mg/kg <10 <10 <10 <10 10 2083622

Reached Baseline at C50 mg/kg Yes Yes Yes Yes N/A 2083622


O-TERPHENYL (sur.) % 99 99 99 98 N/A 2083622



(W85488-02R) (W85489-02R)


F2 (C10-C16 Hydrocarbons) mg/kg <10 <10 10 2083622



Reached Baseline at C50 mg/kg Yes Yes N/A 2083622


O-TERPHENYL (sur.) % 91 89 N/A 2083622


Page 2 of 8


Sampler Initials:


Maxxam ID I 6 4 4 2 2 I 6 4 4 4 7 I 6 4 4 4 8 I 6 4 4 4 9Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17 U n i t s TH102-15 THIO2-14 TH103-17 TH103-8 R D L QC Batch

(W85484-03R) (W85483-03R) (W85486-03R) (W85485-03R)

Physical Properties

Moisture % 19.5 15.6 17.1 4.5 0.3 2085878



(W85488-02R) (W85489-02R)

Physical Properties

Moisture % 17.0 16.2 0.3 2085878


Page 3 of 8


Sampler Initials:


Maxxam ID I 6 4 4 4 9Sampling Date 2008/01/17 U n i t s TH103-8 R D L QC Batch

(W85485-03R)

Hydrocarbons

>C10 - C12 Aliphatic mg/kg 563 5 2079711

>C10 - C12 Aromatic mg/kg 54 5 2079711


>C12 - C16 Aromatic mg/kg 208 10 2079711


>C16 - C21 Aromatic mg/kg 252 10 2079711


>C21 - C34 Aromatic mg/kg 161 10 2079711

>C34 Aliphatic (up to C50) mg/kg <10 10 2079711

>C34 Aromatic (up to C50) mg/kg 58 10 2079711


O-TERPHENYL (sur.) % 101 N/A 2079711


Page 4 of 8


Sampler Initials:

CCME F2-F4 (SOIL) Comments

Sample I64422-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.






Page 5 of 8




2079711 LSH Calibration Check >C10 - C12 Aliphatic 2008/01/30 94 % 80 - 120>C10 - C12 Aromatic 2008/01/30 97 % 80 - 120>C12 - C16 Aliphatic 2008/01/30 95 % 80 - 120>C12 - C16 Aromatic 2008/01/30 97 % 80 - 120>C16 - C21 Aliphatic 2008/01/30 94 % 80 - 120>C16 - C21 Aromatic 2008/01/30 98 % 80 - 120>C21 - C34 Aliphatic 2008/01/30 92 % 80 - 120>C21 - C34 Aromatic 2008/01/30 95 % 80 - 120>C34 Aliphatic (up to C50) 2008/01/30 93 % 80 - 120>C34 Aromatic (up to C50) 2008/01/30 90 % 80 - 120

MATRIX SPIKE O-TERPHENYL (sur.) 2008/01/30 88 % 30 - 130>C21 - C34 Aliphatic 2008/01/30 93 % 50 - 130>C34 Aliphatic (up to C50) 2008/01/30 108 % 50 - 130

QC STANDARD >C10 - C12 Aliphatic 2008/01/30 77 % 70 - 130>C10 - C12 Aromatic 2008/01/30 95 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 84 % 70 - 130>C12 - C16 Aromatic 2008/01/30 96 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 87 % 70 - 130>C16 - C21 Aromatic 2008/01/30 94 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 96 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 88 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 129 % 70 - 130

SPIKE O-TERPHENYL (sur.) 2008/01/30 79 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 71 % 70 - 130>C10 - C12 Aromatic 2008/01/30 121 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 83 % 70 - 130>C12 - C16 Aromatic 2008/01/30 117 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 78 % 70 - 130>C16 - C21 Aromatic 2008/01/30 72 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 89 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 125 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 73 % 70 - 130

BLANK O-TERPHENYL (sur.) 2008/01/30 100 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 <5 mg/kg>C10 - C12 Aromatic 2008/01/30 <5 mg/kg>C12 - C16 Aliphatic 2008/01/30 <10 mg/kg>C12 - C16 Aromatic 2008/01/30 <10 mg/kg>C16 - C21 Aliphatic 2008/01/30 <10 mg/kg>C16 - C21 Aromatic 2008/01/30 <10 mg/kg>C21 - C34 Aliphatic 2008/01/30 <10 mg/kg>C21 - C34 Aromatic 2008/01/30 <10 mg/kg>C34 Aliphatic (up to C50) 2008/01/30 <10 mg/kg>C34 Aromatic (up to C50) 2008/01/30 <10 mg/kg

RPD [ I 6 4 4 4 9 - 0 1 ] >C10 - C12 Aliphatic 2008/01/30 33.1 % 40>C10 - C12 Aromatic 2008/01/30 23.9 % 40>C12 - C16 Aliphatic 2008/01/30 33.1 % 40>C12 - C16 Aromatic 2008/01/30 13.3 % 40>C16 - C21 Aliphatic 2008/01/30 30.5 % 40>C16 - C21 Aromatic 2008/01/30 5.0 % 40>C21 - C34 Aliphatic 2008/01/30 25.3 % 40>C21 - C34 Aromatic 2008/01/30 3.7 % 40>C34 Aliphatic (up to C50) 2008/01/30 NC % 40>C34 Aromatic (up to C50) 2008/01/30 15.7 % 40


Page 6 of 8


Quality Assurance Report (Continued)Maxxam Job Number: CA803092




F2 (C10-C16 Hydrocarbons) 2008/01/24 87 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/24 78 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/24 86 % 50 - 130




RPD [ I 6 4 4 4 9 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/24 22.0 % 50F3 (C16-C34 Hydrocarbons) 2008/01/24 29.4 % 50F4 (C34-C50 Hydrocarbons) 2008/01/24 NC % 50Reached Baseline at C50 2008/01/24 NC % 50

2085878 RM2 RPD Moisture 2008/01/24 5.3 % 20



Page 7 of 8




LUBA SHYMUSHOVSKA,

VERONICA FALK,


Page 8 of 8










Encryption Key






Page 1 of 13





09:00 10:00COC Number 00553375 00553375 U n i t s TH105-2 R D L QC Batch TH105-14 R D L QC Batch

INORGANICS

Moisture % 13 0.2 1447106 12 1 1446268





INORGANICS

Moisture % 17 17 20 1 1446268

Available (CaCl2) pH pH 8.02 8.02 7.95 1448098


Page 2 of 13






TPH COMPOUNDS



Ethylbenzene mg/kg ND ND ND 0.03 1446082

Xylene (Total) mg/kg ND ND ND 0.05 1446082



>C8-C10 Aromatics (-EX) mg/kg ND ND ND 0.1 1446082




Aliphatic >C21-<C32 mg/kg ND ND ND 15 1446440

Aromatic >C10-C12 mg/kg ND ND ND 4.0 1446440



Aromatic >C21-<C32 mg/kg ND ND ND 15 1446440

Modified TPH (Tier 2) mg/kg ND ND ND 20 1444752




n-Dotriacontane - Extractable % 78 85 90 1446440


Page 3 of 13






TPH COMPOUNDS

Benzene mg/kg ND 0.03 1446082

Toluene mg/kg ND 0.03 1446082

Ethylbenzene mg/kg ND 0.03 1446082

Xylene (Total) mg/kg ND 0.05 1446082

Aliphatic >C6-C8 mg/kg ND 0.2 1446082


>C8-C10 Aromatics (-EX) mg/kg ND 0.1 1446082


Aliphatic >C12-C16 mg/kg ND 15 1446440

Aliphatic >C16-C21 mg/kg ND 15 1446440

Aliphatic >C21-<C32 mg/kg ND 15 1446440

Aromatic >C10-C12 mg/kg ND 4.0 1446440

Aromatic >C12-C16 mg/kg ND 15 1446440

Aromatic >C16-C21 mg/kg ND 15 1446440

Aromatic >C21-<C32 mg/kg ND 15 1446440

Modified TPH (Tier 2) mg/kg ND 20 1444752


Isobutylbenzene - Extractable % 84 1446440

Isobutylbenzene - Volatile % 127 1446082

n-Dotriacontane - Extractable % 91 1446440


Page 4 of 13






PAHs


















Pyrene ug/g ND 0.005 1446489


D10-Anthracene % 87 1446489

D14-Terphenyl (FS) % 87 1446489




Page 5 of 13






F1 PHC and BTEX




o-Xylene ug/g ND ND ND 0.02 1446054

p+m-Xylene ug/g ND ND ND 0.04 1446054

Total Xylenes ug/g ND ND ND 0.04 1446054

F1 (C6-C10) ug/g ND ND ND 10 1446054

F1 (C6-C10) - BTEX ug/g ND ND ND 10 1446054

F2-F4 PHC








D10-Ethylbenzene % 88 89 85 1446054


o-Terphenyl % 112 106 103 1447307


Page 6 of 13






F1 PHC and BTEX

Benzene ug/g ND 0.02 1446054

Toluene ug/g ND 0.02 1446054

Ethylbenzene ug/g ND 0.02 1446054

o-Xylene ug/g ND 0.02 1446054

p+m-Xylene ug/g ND 0.04 1446054

Total Xylenes ug/g ND 0.04 1446054

F1 (C6-C10) ug/g ND 10 1446054

F1 (C6-C10) - BTEX ug/g ND 10 1446054

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/g ND 10 1447307



Reached Baseline at C50 ug/g Yes 1447307


1,4-Difluorobenzene % 103 1446054

4-Bromofluorobenzene % 101 1446054

D10-Ethylbenzene % 92 1446054

D4-1,2-Dichloroethane % 94 1446054

o-Terphenyl % 111 1447307


Page 7 of 13



GENERAL COMMENTS

Note: F1BTEX - all soils were Methanol extracted on 2008/01/23


VPH in Soil (PIRI2): Elevated VPH RDL(s) due to detected levels in the method blank.


Page 8 of 13




1446054 GBA MATRIX SPIKE 1,4-Difluorobenzene 2008/01/24 96 % 60 - 1404-Bromofluorobenzene 2008/01/24 106 % 60 - 140D10-Ethylbenzene 2008/01/24 96 % 30 - 130D4-1,2-Dichloroethane 2008/01/24 94 % 60 - 140Benzene 2008/01/24 85 % 60 - 140Toluene 2008/01/24 98 % 60 - 140Ethylbenzene 2008/01/24 94 % 60 - 140o-Xylene 2008/01/24 90 % 60 - 140p+m-Xylene 2008/01/24 97 % 60 - 140F1 (C6-C10) 2008/01/24 96 % 60 - 140



RPD Benzene 2008/01/24 NC % 50Toluene 2008/01/24 NC % 50Ethylbenzene 2008/01/24 NC % 50o-Xylene 2008/01/24 NC % 50p+m-Xylene 2008/01/24 NC % 50Total Xylenes 2008/01/24 NC % 50F1 (C6-C10) 2008/01/24 NC % 50F1 (C6-C10) - BTEX 2008/01/24 NC % 50

1446082 LMU MATRIX SPIKE Isobutylbenzene - Volatile 2008/01/25 90 % 60 - 140Benzene 2008/01/25 71 % 60 - 140Toluene 2008/01/25 88 % 60 - 140Ethylbenzene 2008/01/25 71 % 60 - 140Xylene (Total) 2008/01/25 87 % 60 - 140

Spiked Blank Isobutylbenzene - Volatile 2008/01/25 93 % 60 - 140Benzene 2008/01/25 83 % 60 - 140Toluene 2008/01/25 83 % 60 - 140Ethylbenzene 2008/01/25 84 % 60 - 140Xylene (Total) 2008/01/25 83 % 60 - 140

Method Blank Isobutylbenzene - Volatile 2008/01/25 97 % 60 - 140Benzene 2008/01/25 ND, RDL=0.03 mg/kgToluene 2008/01/25 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/25 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/25 ND, RDL=0.05 mg/kg

Page 9 of 13




1446082 LMU Method Blank Aliphatic >C6-C8 2008/01/25 0.1, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/25 0.6, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/25 ND, RDL=0.1 mg/kg

RPD Benzene 2008/01/25 NC % 50Toluene 2008/01/25 NC % 50Ethylbenzene 2008/01/25 NC % 50Xylene (Total) 2008/01/25 NC % 50Aliphatic >C6-C8 2008/01/25 NC % 50Aliphatic >C8-C10 2008/01/25 NC % 50>C8-C10 Aromatics (-EX) 2008/01/25 NC % 50



RPD Aliphatic >C10-C12 2008/01/29 NC % 50Aliphatic >C12-C16 2008/01/29 NC % 50Aliphatic >C16-C21 2008/01/29 NC % 50Aliphatic >C21-<C32 2008/01/29 NC % 50Aromatic >C10-C12 2008/01/29 4.6 % 50Aromatic >C12-C16 2008/01/29 NC % 50Aromatic >C16-C21 2008/01/29 NC % 50Aromatic >C21-<C32 2008/01/29 NC % 50

1446489 PMO MATRIX SPIKE D10-Anthracene 2008/01/24 84 % 30 - 130D14-Terphenyl (FS) 2008/01/24 87 % 30 - 130D7-Quinoline 2008/01/24 69 % 30 - 130D8-Acenaphthylene 2008/01/24 79 % 30 - 130Acenaphthene 2008/01/24 86 % 30 - 130Acenaphthylene 2008/01/24 88 % 30 - 130Anthracene 2008/01/24 86 % 30 - 130Benzo(a)anthracene 2008/01/24 88 % 30 - 130Benzo(a)pyrene 2008/01/24 86 % 30 - 130Benzo(b/j)fluoranthene 2008/01/24 84 % 30 - 130Benzo(g,h,i)perylene 2008/01/24 87 % 30 - 130Benzo(k)fluoranthene 2008/01/24 92 % 30 - 130Chrysene 2008/01/24 85 % 30 - 130Dibenz(a,h)anthracene 2008/01/24 86 % 30 - 130Fluoranthene 2008/01/24 93 % 30 - 130Fluorene 2008/01/24 83 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/24 77 % 30 - 1301-Methylnaphthalene 2008/01/24 83 % 30 - 1302-Methylnaphthalene 2008/01/24 88 % 30 - 130

Page 10 of 13




1446489 PMO MATRIX SPIKE Naphthalene 2008/01/24 80 % 30 - 130Phenanthrene 2008/01/24 88 % 30 - 130Pyrene 2008/01/24 82 % 30 - 130

Spiked Blank D10-Anthracene 2008/01/24 102 % 30 - 130D14-Terphenyl (FS) 2008/01/24 109 % 30 - 130D7-Quinoline 2008/01/24 90 % 30 - 130D8-Acenaphthylene 2008/01/24 94 % 30 - 130Acenaphthene 2008/01/24 98 % 30 - 130Acenaphthylene 2008/01/24 105 % 30 - 130Anthracene 2008/01/24 111 % 30 - 130Benzo(a)anthracene 2008/01/24 99 % 30 - 130Benzo(a)pyrene 2008/01/24 118 % 30 - 130Benzo(b/j)fluoranthene 2008/01/24 108 % 30 - 130Benzo(g,h,i)perylene 2008/01/24 113 % 30 - 130Benzo(k)fluoranthene 2008/01/24 116 % 30 - 130Chrysene 2008/01/24 104 % 30 - 130Dibenz(a,h)anthracene 2008/01/24 114 % 30 - 130Fluoranthene 2008/01/24 113 % 30 - 130Fluorene 2008/01/24 99 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/24 104 % 30 - 1301-Methylnaphthalene 2008/01/24 97 % 30 - 1302-Methylnaphthalene 2008/01/24 100 % 30 - 130Naphthalene 2008/01/24 99 % 30 - 130Phenanthrene 2008/01/24 106 % 30 - 130Pyrene 2008/01/24 105 % 30 - 130

Method Blank D10-Anthracene 2008/01/24 101 % 30 - 130D14-Terphenyl (FS) 2008/01/24 102 % 30 - 130D7-Quinoline 2008/01/24 90 % 30 - 130D8-Acenaphthylene 2008/01/24 92 % 30 - 130Acenaphthene 2008/01/24 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/24 ND, RDL=0.005 ug/gAnthracene 2008/01/24 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/24 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/24 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/24 ND, RDL=0.005 ug/gBenzo(g,h,i)perylene 2008/01/24 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/24 ND, RDL=0.01 ug/gChrysene 2008/01/24 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/24 ND, RDL=0.02 ug/gFluoranthene 2008/01/24 ND, RDL=0.005 ug/gFluorene 2008/01/24 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/24 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/24 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/24 ND, RDL=0.005 ug/gNaphthalene 2008/01/24 ND, RDL=0.005 ug/gPhenanthrene 2008/01/24 ND, RDL=0.005 ug/gPyrene 2008/01/24 ND, RDL=0.005 ug/g

RPD D14-Terphenyl (FS) 2008/01/24 5.5 % N/AAcenaphthene 2008/01/24 NC % 50Acenaphthylene 2008/01/24 NC % 50Anthracene 2008/01/24 NC % 50Benzo(a)anthracene 2008/01/24 NC % 50Benzo(a)pyrene 2008/01/24 NC % 50Benzo(b/j)fluoranthene 2008/01/24 NC % 50Benzo(g,h,i)perylene 2008/01/24 NC % 50

Page 11 of 13




1446489 PMO RPD Benzo(k)fluoranthene 2008/01/24 NC % 50Chrysene 2008/01/24 NC % 50Dibenz(a,h)anthracene 2008/01/24 NC % 50Fluoranthene 2008/01/24 NC % 50Fluorene 2008/01/24 NC % 50Indeno(1,2,3-cd)pyrene 2008/01/24 NC % 501-Methylnaphthalene 2008/01/24 NC % 502-Methylnaphthalene 2008/01/24 NC % 50Naphthalene 2008/01/24 NC % 50Phenanthrene 2008/01/24 NC % 50Pyrene 2008/01/24 NC % 50

1447106 MYG RPD Moisture 2008/01/25 5.9 % 501447307 BWW MATRIX SPIKE o-Terphenyl 2008/01/25 106 % 30 - 130




RPD F2 (C10-C16 Hydrocarbons) 2008/01/25 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/25 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/25 NC % 50

ND = Not detectedN/A = Not ApplicableNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample

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BRAD NEWMAN, Scientific Specialist




TIM MUNSHAW, Lab Manager


Page 13 of 13







Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 4 2008/01/24 2008/01/24 CAL SOP-00086 CCME PHC-CWS Moisture 4 N/A 2008/01/25 CAL SOP-00023 McKeague MSSMA 2.411


Encryption Key







Page 1 of 6


Sampler Initials:

CCME F2-F4 (SOIL)

Maxxam ID I 6 5 5 0 6 I 6 5 5 1 2 I 6 5 5 1 3 I 6 5 5 1 4Sampling Date 2008/01/21 2008/01/21 2008/01/21 2008/01/21 U n i t s TH106-14 TH105-15 TH105-14 TH106-15 R D L QC Batch

(W87393-01R) (W87392-01R) (W87391-01R) (W87394-01R)





Reached Baseline at C50 mg/kg Yes Yes Yes Yes N/A 2086431


O-TERPHENYL (sur.) % 94 92 91 93 N/A 2086431


Page 2 of 6


Sampler Initials:


Maxxam ID I 6 5 5 0 6 I 6 5 5 1 2 I 6 5 5 1 3 I 6 5 5 1 4Sampling Date 2008/01/21 2008/01/21 2008/01/21 2008/01/21 U n i t s TH106-14 TH105-15 TH105-14 TH106-15 R D L QC Batch

(W87393-01R) (W87392-01R) (W87391-01R) (W87394-01R)

Physical Properties

Moisture % 16.1 15.7 8.4 16.1 0.3 2088155


Page 3 of 6


Sampler Initials:

CCME F2-F4 (SOIL) Comments






Page 4 of 6










RPD [ I 6 5 5 0 6 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/24 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/24 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/24 NC % 50Reached Baseline at C50 2008/01/24 NC % 50

2088155 RM2 RPD Moisture 2008/01/25 2.3 % 20



Page 5 of 6




LUBA SHYMUSHOVSKA,


Page 6 of 6






Sample Matrix: Water# Samples Received: 6

Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Water (AA PIRI) ( 1 ) 6 N/A 2008/02/07 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Water 6 N/A 2008/01/29 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Water 6 2008/01/29 2008/01/29 CAM SOP-00316 CCME Hydrocarbons VPH in Water (PIRI2) ( 1 ) 6 N/A 2008/02/04 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Water ( 1 ) 6 N/A 2008/02/07 Based on Atl. PIRI



Encryption Key






Page 1 of 10



ATLANTIC RBCA HYDROCARBONS (WATER)


11:00 11:30 12:00COC Number 00553384 00553384 00553384 U n i t s TH 101 TH 102 TH 103 R D L QC Batch

TPH COMPOUNDS

Benzene mg/L ND ND ND 0.001 1451710

Toluene mg/L ND ND ND 0.001 1451710

Ethylbenzene mg/L ND ND ND 0.001 1451710

Xylene (Total) mg/L ND ND ND 0.002 1451710

Aliphatic >C6-C8 mg/L ND ND ND 0.01 1451710

Aliphatic >C8-C10 mg/L 0.01 ND 0.01 0.01 1451710

>C8-C10 Aromatics (-EX) mg/L ND ND ND 0.01 1451710




Aliphatic >C21-<C32 mg/L 0.2 ND ND 0.1 1449839

Aromatic >C10-C12 mg/L 0.15 ND 0.01 0.01 1449839

Aromatic >C12-C16 mg/L 0.50 ND 0.05 0.05 1449839

Aromatic >C16-C21 mg/L 0.64 0.06 0.14 0.05 1449839

Aromatic >C21-<C32 mg/L 0.3 ND ND 0.1 1449839

Modified TPH (Tier 2) mg/L 4.6 ND 0.6 0.1 1449033




n-Dotriacontane - Extractable % 58 ( 1 ) 85 ( 2 ) 83 ( 3 ) 1449839

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Fuel oil fraction. TEH sample contained sediment. TEH surrogate(s) not within acceptance limits.Insufficient sample to repeat.( 2 ) TEH sample contained sediment.( 3 ) Weathered fuel oil fraction. One product in the fuel/lube oil range. TEH sample contained sediment. TEHsurrogate(s) not within acceptance limits. Insufficient sample to repeat.

Page 2 of 10





12:30 13:00COC Number 00553384 00553384 U n i t s TH 104 TH 105 R D L QC Batch

TPH COMPOUNDS

Benzene mg/L ND ND 0.001 1451710

Toluene mg/L ND ND 0.001 1451710

Ethylbenzene mg/L ND ND 0.001 1451710

Xylene (Total) mg/L ND ND 0.002 1451710

Aliphatic >C6-C8 mg/L ND ND 0.01 1451710


>C8-C10 Aromatics (-EX) mg/L ND ND 0.01 1451710




Aliphatic >C21-<C32 mg/L ND ND 0.1 1449839

Aromatic >C10-C12 mg/L 0.01 ND 0.01 1449839

Aromatic >C12-C16 mg/L ND ND 0.05 1449839

Aromatic >C16-C21 mg/L 0.17 ND 0.05 1449839

Aromatic >C21-<C32 mg/L 0.1 ND 0.1 1449839

Modified TPH (Tier 2) mg/L 0.3 ND 0.1 1449033


Isobutylbenzene - Extractable % 66 54 1449839

Isobutylbenzene - Volatile % 116 116 ( 1 ) 1451710

n-Dotriacontane - Extractable % 92 ( 2 ) 79 ( 3 ) 1449839

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) VPH analysis performed on previously opened vial.( 2 ) One product in the fuel/lube oil range. TEH sample contained sediment.( 3 ) TEH sample decanted due to sediment. TEH surrogate(s) not within acceptance limits.Insufficient sample to repeat.

Page 3 of 10





13:30COC Number 00553384 U n i t s TH 106 R D L QC Batch

TPH COMPOUNDS

Benzene mg/L ND 0.001 1451710

Toluene mg/L ND 0.001 1451710

Ethylbenzene mg/L ND 0.001 1451710

Xylene (Total) mg/L ND 0.002 1451710

Aliphatic >C6-C8 mg/L ND 0.01 1451710

Aliphatic >C8-C10 mg/L ND 0.01 1451710

>C8-C10 Aromatics (-EX) mg/L ND 0.01 1451710

Aliphatic >C10-C12 mg/L 0.03 0.01 1449839

Aliphatic >C12-C16 mg/L 0.30 0.06 1449839

Aliphatic >C16-C21 mg/L 0.36 0.06 1449839

Aliphatic >C21-<C32 mg/L 0.1 0.1 1449839

Aromatic >C10-C12 mg/L 0.03 0.01 1449839

Aromatic >C12-C16 mg/L 0.33 0.06 1449839

Aromatic >C16-C21 mg/L 0.33 0.06 1449839

Aromatic >C21-<C32 mg/L 0.1 0.1 1449839

Modified TPH (Tier 2) mg/L 1.5 0.1 1449033


Isobutylbenzene - Extractable % 77 1449839

Isobutylbenzene - Volatile % 121 ( 1 ) 1451710

n-Dotriacontane - Extractable % 76 ( 2 ) 1449839

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) VPH analysis performed on previously opened vial.( 2 ) One product in the fuel/lube oil range. TEH sample containedsediment.

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F1 PHC and BTEX

Benzene ug/L ND ND ND 0.2 1449242

Toluene ug/L ND ND ND 0.2 1449242

Ethylbenzene ug/L ND ND ND 0.2 1449242

o-Xylene ug/L 1.0 ND ND 0.2 1449242

p+m-Xylene ug/L ND ND ND 0.4 1449242

Total Xylenes ug/L 1.0 ND ND 0.4 1449242

F1 (C6-C10) ug/L ND ND ND 100 1449242

F1 (C6-C10) - BTEX ug/L ND ND ND 100 1449242

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/L 130 ND ND 100 1449135

F3 (C16-C34 Hydrocarbons) ug/L 130 ND ND 100 1449135

F4 (C34-C50 Hydrocarbons) ug/L ND ND ND 100 1449135

Reached Baseline at C50 ug/L Yes Yes Yes 1449135




D10-Ethylbenzene % 105 96 99 1449242


o-Terphenyl % 106 106 106 1449135


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F1 PHC and BTEX

Benzene ug/L ND ND ND 0.2 1449242

Toluene ug/L ND ND ND 0.2 1449242

Ethylbenzene ug/L ND ND ND 0.2 1449242

o-Xylene ug/L ND ND ND 0.2 1449242

p+m-Xylene ug/L ND ND ND 0.4 1449242

Total Xylenes ug/L ND ND ND 0.4 1449242

F1 (C6-C10) ug/L ND ND ND 100 1449242

F1 (C6-C10) - BTEX ug/L ND ND ND 100 1449242

F2-F4 PHC

F2 (C10-C16 Hydrocarbons) ug/L ND 120 ND 100 1449135

F3 (C16-C34 Hydrocarbons) ug/L ND 310 ND 100 1449135

F4 (C34-C50 Hydrocarbons) ug/L ND ND ND 100 1449135

Reached Baseline at C50 ug/L Yes Yes Yes 1449135




D10-Ethylbenzene % 98 94 95 1449242


o-Terphenyl % 105 103 103 1449135


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GENERAL COMMENTS


Page 7 of 10




1449135 ZZ MATRIX SPIKE o-Terphenyl 2008/01/29 116 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/29 111 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/29 111 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/29 111 % 60 - 130


Method Blank o-Terphenyl 2008/01/29 103 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/LF3 (C16-C34 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/LF4 (C34-C50 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/L

RPD F2 (C10-C16 Hydrocarbons) 2008/01/29 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/29 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/29 NC % 50

1449242 GRU MATRIX SPIKE 1,4-Difluorobenzene 2008/01/29 102 % 70 - 1304-Bromofluorobenzene 2008/01/29 110 % 70 - 130D10-Ethylbenzene 2008/01/29 105 % 70 - 130D4-1,2-Dichloroethane 2008/01/29 113 % 70 - 130Benzene 2008/01/29 99 % 70 - 130Toluene 2008/01/29 100 % 70 - 130Ethylbenzene 2008/01/29 102 % 70 - 130o-Xylene 2008/01/29 100 % 70 - 130p+m-Xylene 2008/01/29 106 % 70 - 130F1 (C6-C10) 2008/01/29 83 % 70 - 130


Method Blank 1,4-Difluorobenzene 2008/01/29 109 % 70 - 1304-Bromofluorobenzene 2008/01/29 96 % 70 - 130D10-Ethylbenzene 2008/01/29 102 % 70 - 130D4-1,2-Dichloroethane 2008/01/29 105 % 70 - 130Benzene 2008/01/29 ND, RDL=0.2 ug/LToluene 2008/01/29 ND, RDL=0.2 ug/LEthylbenzene 2008/01/29 ND, RDL=0.2 ug/Lo-Xylene 2008/01/29 ND, RDL=0.2 ug/Lp+m-Xylene 2008/01/29 ND, RDL=0.4 ug/LTotal Xylenes 2008/01/29 ND, RDL=0.4 ug/LF1 (C6-C10) 2008/01/29 ND, RDL=100 ug/LF1 (C6-C10) - BTEX 2008/01/29 ND, RDL=100 ug/L

RPD Benzene 2008/01/29 NC % 40Toluene 2008/01/29 NC % 40Ethylbenzene 2008/01/29 NC % 40o-Xylene 2008/01/29 NC % 40p+m-Xylene 2008/01/29 NC % 40Total Xylenes 2008/01/29 NC % 40F1 (C6-C10) 2008/01/29 NC % 40F1 (C6-C10) - BTEX 2008/01/29 NC % 40

Page 8 of 10





Method Blank Isobutylbenzene - Extractable 2008/02/07 62 % 30 - 130n-Dotriacontane - Extractable 2008/02/07 82 % 30 - 130Aliphatic >C10-C12 2008/02/07 ND, RDL=0.01 mg/LAliphatic >C12-C16 2008/02/07 ND, RDL=0.05 mg/LAliphatic >C16-C21 2008/02/07 ND, RDL=0.05 mg/LAliphatic >C21-<C32 2008/02/07 ND, RDL=0.1 mg/LAromatic >C10-C12 2008/02/07 ND, RDL=0.01 mg/LAromatic >C12-C16 2008/02/07 ND, RDL=0.05 mg/LAromatic >C16-C21 2008/02/07 ND, RDL=0.05 mg/LAromatic >C21-<C32 2008/02/07 ND, RDL=0.1 mg/L

1451710 GTH Spiked Blank Isobutylbenzene - Volatile 2008/02/04 112 % 70 - 130Benzene 2008/02/04 109 % 70 - 130Toluene 2008/02/04 109 % 70 - 130Ethylbenzene 2008/02/04 113 % 70 - 130Xylene (Total) 2008/02/04 116 % 70 - 130

Method Blank Isobutylbenzene - Volatile 2008/02/04 114 % 70 - 130Benzene 2008/02/04 ND, RDL=0.001 mg/LToluene 2008/02/04 ND, RDL=0.001 mg/LEthylbenzene 2008/02/04 ND, RDL=0.001 mg/LXylene (Total) 2008/02/04 ND, RDL=0.002 mg/LAliphatic >C6-C8 2008/02/04 ND, RDL=0.01 mg/LAliphatic >C8-C10 2008/02/04 ND, RDL=0.01 mg/L>C8-C10 Aromatics (-EX) 2008/02/04 ND, RDL=0.01 mg/L

ND = Not detectedNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample

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phase ii environmental assessment

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