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PHASE II ENVIRONMENTAL SITE ASSESSMENT HOWARD UNIVERSITY EAST CAMPUS (DIVINITY SCHOOL) 1400 SHEPHERD STREET, NE WASHINGTON, DC ECS PROJECT NO. 47:6230-A FOR ZOM MID-ATLANTIC, INC AUGUST 24, 2018

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PHASE II ENVIRONMENTAL SITE ASSESSMENT HOWARD UNIVERSITY EAST CAMPUS (DIVINITY SCHOOL)

1400 SHEPHERD STREET, NE WASHINGTON, DC

ECS PROJECT NO. 47:6230-A

FOR

ZOM MID-ATLANTIC, INC

AUGUST 24, 2018

 

   

August 24, 2018 Mr. Christopher Love ZOM Mid-Atlantic, Inc. 1054 31st Street, NW Washington, DC 20007

ECS Project No. 47:6230-A

Reference: Phase II Environmental Site Assessment Report, Howard University East Campus (Divinity School), 1400 Shepherd Street, NE, Washington, DC

Dear Mr. Love: ECS Mid-Atlantic, LLC (ECS) is pleased to present the following Phase II Environmental Site Assessment (ESA) report for the above-referenced site in Washington, DC.

PROJECT BACKGROUND The property consists of an approximately 22.51-acre parcel of land improved with the Howard University Divinity School including the Divinity Library, a vacant four-story historic building consisting of a library, offices, dormitories, a kitchen and cafeteria, a chapel, and a central courtyard. Additional improvements at the subject property include a two-story single family residence and a maintenance shed. Based on provided information, the property is being considered for redevelopment. ECS completed a Phase I ESA of the subject property in July 2018 (ECS Project Number 47:6230, dated July 2, 2018). The Phase I ESA identified the following Recognized Environmental Conditions (RECs) for the subject property:

The subject property was identified on the DC underground storage tank (UST) database as "HU - School of Divinity" addressed 1400 Shepherd Street, NE 14th & Shepherd Street, NE. The subject property was listed with three "Permanently Out of Use" USTs including one 1,000-gallon gasoline, one 4,000-gallon heating oil, and one 2,000-gallon heating oil UST. Additionally, one 550-gallon diesel UST with a "Currently In Use" status was listed at the subject property. ECS reviewed the DC Property Information Verification System (PIVS) for building department records. The PIVS included three construction/miscellaneous permits including permits for the removal of two 4,000-gallon underground storage tanks. The tank removal permit was dated March 7, 2005; however, no additional information related to the tank removal was available for review. Further, the Veeder Root tank monitoring system located in a mechanical room of the Divinity Library building did not appear to be operating during the site reconnaissance. Based on the potential for a petroleum release, the UST listing was considered a REC for the subject property.

ZOM Mid-Atlantic, Inc. ECS Project No. 47:6230-A August 24, 2018 Page 2  

Staining was observed on the dirt floor of the maintenance shed located on the central-eastern portion of the subject property. The staining was suspected to be related to vehicle and/or equipment repairs conducted in the maintenance shed. Containers of mechanical oils and degreasers were observed in the maintenance shed. The stained soil and suspected use of the maintenance shed for vehicle or equipment repairs was considered a recognized environmental condition (REC) for the subject property.

Additionally, the following Historical Recognized Environmental Condition (HREC) was identified:

The subject property was listed on the DC Leaking Underground Storage Tank (LUST) database as "Dr. Lynn Hamerling" addressed 1421 Taylor Street, NE. The subject property was listed with one closed LUST case which was opened in 1999 related to reports of heating oil in the sub-surface soil. The closed on-site LUST case was considered a HREC for the property.

The objective of this investigation was to collect soil and groundwater samples to assess whether the subsurface had been adversely impacted by previous on-site activities.

SCOPE OF WORK Utility Clearance ECS contracted a private utility locator to identify and mark the underground utilities in the work area (see boring location diagram included as Appendix I) on the property. The utilities were located on August 7, 2018. The proposed location of boring B-6 (according to the work plan) was not accessible due to dense vegetation. Therefore, boring B-6 was moved to the north in a more accessible area. Soil Borings On August 8, 2018, ECS employed a track-mounted Geoprobe to advance a total of six (6) soil borings across the site. The soil borings were drilled to depths ranging from approximately 17 to 27 feet below ground surface (bgs), at which point Geoprobe refusal was encountered. The Geoprobe used a hydraulic hammer to push a 2.5” diameter steel rod with a clear PVC sleeve into the ground in five-foot increments. The macrocore was then withdrawn from the ground and the sleeve removed, containing a relatively undisturbed soil core. The sleeve was cut open allowing examination of the entire soil core, and sampling of soil from the core. Soil was screened in 5-foot intervals throughout the depth of each boring. The soil was screened in the field with a Photoionization Detector (PID), which measures total volatile organic compounds (VOCs) emanating from the soil. While drilling the soil boring B-6, white to light gray sandy clay was encountered at a depth of 15 to 20 feet bgs, which was

ZOM Mid-Atlantic, Inc. ECS Project No. 47:6230-A August 24, 2018 Page 3  

saturated with free liquid petroleum product. Petroleum odors were noted in some of the other borings. However, free liquid petroleum product was only observed in the boring B-6. Temporary PVC wells were installed in borings B-5, B-6 and B-2 in order to collect groundwater samples. The wells consisted of ten feet of machine-slotted well screen topped with a solid PVC riser pipe to the surface.

SAMPLING METHODOLOGY Soil Sampling Based on field screening results, three soil samples from each boring were selected for laboratory analysis. During drilling activities, the PID malfunctioned and was not able to detect VOCs in the soil. Therefore, the soil samples were selected on the basis of visual and olfactory observations, such as staining and petroleum odors. When no evidence of petroleum impact was apparent in the soil cores, the soil samples were collected from (1) the top five feet of the borings, (2) immediately above the water table, and (3) the base of the boring. All selected soil samples were placed in laboratory grade glassware, packed on ice and submitted under chain-of-custody protocol to an independent laboratory for analysis of total petroleum hydrocarbons diesel-range and gasoline-range organics (TPH-DRO and TPH-GRO), polycyclic aromatic hydrocarbons (PAHs), volatile organic compounds (VOCs), and Resource Conservation and Recovery Act (RCRA) metals. Groundwater Sampling Saturated soil conditions indicative of groundwater were encountered in each of the six borings prior to termination of the borings at depths ranging from 10 feet to 15 feet bgs. ECS collected groundwater samples from three of the six borings (B-2, B-5 and B-6). The groundwater samples were collected with a peristaltic pump with dedicated tubing. The groundwater samples were placed into laboratory-grade bottles with appropriate preservative, packed on ice and submitted to an independent laboratory for analysis of TPH-DRO, TPH-GRO, PAHs, and VOCs. Temporary wells were removed after sampling. The borings were filled with bentonite clay according to the District Department of Energy and Environment (DOEE) guidelines.

RESULTS A total of six borings were advanced across the property. Obvious evidence of impact (i.e. PID readings, odors, staining, etc.) was observed in three of the six soil borings and free liquid petroleum product was observed in boring B-6. Detected soil contaminant concentrations were compared to the DC Risk Based Corrective Action (RBCA) Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Levels (RBSLs) for a Resident Adult, in Sub-Surface Soil, for Indoor Inhalation. Additionally, detected concentrations of TPH GRO, TPH DRO, benzene, ethylbenzene, toluene, and xylenes were compared to the DC RBCA

ZOM Mid-Atlantic, Inc. ECS Project No. 47:6230-A August 24, 2018 Page 4  

Tier 0 screening level. Where the DC RBSLs were not established for certain compounds, the detected concentrations were compared with their respective EPA Regional Screening Level (RSL) for Resident Soil. The groundwater contaminant concentrations were compared to the DC RBCA Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Levels (RBSLs) for a Resident Adult, in Groundwater, for Indoor Inhalation. Where the DC RBSLs were not established for certain compounds, the detected concentrations were compared with their respective EPA RSL for Maximum Contaminant Level (MCL). If the MCL was not established for certain compounds, the detected concentrations were compared with their respective EPA RSL for tapwater. The results are summarized below. The boring logs are included as Appendix II. The laboratory results are summarized in tables provided in Appendix III. A full laboratory report is provided in Appendix IV. Soil Sampling Results VOCs Thirteen VOCs were detected in one or more of the eighteen analyzed soil samples. Three samples had detectable concentrations above the Tier 1 screening levels. Most of the VOCs detected are typically associated with petroleum products. Benzene was detected in three of the eighteen analyzed soil samples. In borings B-1 and B-6, the detected benzene concentrations were 2.8 micrograms per kilogram (µg/kg) and 2.3 µg/kg, respectively. These concentrations were below the respective DC Tier 0 screening level of 5 µg/kg. Benzene was detected at a concentration of 7.2 ug/kg in boring B-5 at the depth of 27 feet bgs and exceeded its respective DC Tier 0 screening level. The benzene concentration in B-5 also exceeded the DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 5.06 µg/kg. n-Butylbenzene was detected at an estimated concentration of 4 µg/kg in boring B-6 at a depth of 5 feet bgs, and at a concentration of 17,600 µg/kg in B-6 at a depth of 20 feet bgs. The concentrations of n-butylbenzene were below the EPA RSL for resident soil of 3,900,000 ug/kg. sec-Butylbenzene was detected at a concentration of 3,860 µg/kg in boring B-6 at a depth of 20 feet bgs, which was below its EPA RSL for resident soil of 7,800,000 µg/kg. Carbon disulfide was detected in boring B-6 at the depth of 10 feet bgs, at an estimated concentration of 2.6 µg/kg, which was below its EPA RSL for resident soil of 770,000 µg/kg. Ethylbenzene was detected in eight of the eighteen soil samples at concentrations ranging from 3 µg/kg to 27,300 µg/kg. In boring B-6, the detected concentrations of ethylbenzene were 118 µg/kg at 5 feet bgs and 27,300 µg/kg at 20 feet bgs, which both exceeded the DC

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Tier 0 screening level of 40 µg/kg and the DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 40.8 µg/kg. Isopropylbenzene (Cumene) was detected in two of the eighteen soil samples at concentrations of 3.4 µg/kg in boring B-5 at a depth of 5 feet bgs and 6,960 µg/kg in boring B-6 at a depth of 20 feet bgs. The concentrations of isopropylbenzene did not exceed the EPA RSL for resident soil of 1,900,000 ug/kg. 4-Isopropyltoluene was detected at a concentration of 7,760 µg/kg in boring B-6 at the depth of 20 feet bgs. There is no established screening level for isopropyltoluene. Naphthalene was detected in six of the eighteen analyzed soil samples at concentrations ranging from 3.6 µg/kg to 31,200 µg/kg. The concentration of 31,200 µg/kg detected in boring B-6 at 20 feet bgs exceeded its DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 188 µg/kg. The remaining detected concentrations of naphthalene were below the DC Tier 1 screening level. n-Propylbenzene was detected in four of the eighteen analyzed soil samples at concentrations ranging from 3.7 µg/kg to 26,500 µg/kg. The concentrations of n-propylbenzene did not exceed its EPA RSL for resident soil of 3,800,000 ug/kg. Toluene was detected in fourteen of the eighteen analyzed soil samples at concentrations ranging from 2.6 µg/kg to 14,300 µg/kg. The concentration of 14,300 µg/kg detected in boring B-6 at 20 feet bgs exceeded its DC Tier 0 screening level of 9,600 ug/kg and DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 10,000 µg/kg. The remaining detected concentrations of toluene were below the DC Tier 0 screening level. 1,2,4-Trimethylbenzene was detected in ten of the eighteen analyzed soil samples at concentrations ranging from 2.5 µg/kg to 175,000 µg/kg. The concentrations of 1,2,4-trimethylbenzene did not exceed the EPA RSL for resident soil of 300,000 ug/kg. 1,3,5-Trimethylbenzene was detected in five of the eighteen analyzed soil samples at concentrations ranging from 9.5 µg/kg to 50,300 µg/kg. The concentrations of 1,3,5-trimethylbenzene did not exceed the EPA RSL for resident soil of 270,000 µg/kg. Xylenes (total) were detected in fourteen of the eighteen analyzed soil samples at concentrations ranging from 3.2 µg/kg to 173,800 µg/kg. The concentration of 173,800 µg/kg detected in boring B-6 at 20 feet bgs exceeded its DC Tier 0 screening level and DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 3,860 µg/kg. The remaining detected concentrations of xylenes were below the DC Tier 0 screening level. PAHs PAHs were detected in three of the eighteen analyzed soil samples from borings B-2, B-5, and B-6.

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Benzo[b]fluoranthene was detected in one of the analyzed soil samples at a concentration of 516 µg/kg in B-6 at a depth of 5 feet bgs. The detected concentration of benzo[b]fluoranthene was below the DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 3,460,000 ug/kg. 2-Methylnaphthalene was detected in one of the analyzed soil samples at a concentration of 9,690 µg/kg in B-6 at a depth of 20 feet bgs. The detected concentration was below its EPA RSL for resident soil of 240,000 µg/kg. Naphthalene was detected in one of the analyzed soil samples at a concentration of 8,650 µg/kg in B-6 to a depth of 20 feet bgs. The detected naphthalene concentration exceeded its DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 188 ug/kg. Pyrene was detected in one of the analyzed soil samples at a concentration of 491 µg/kg in B-6 at 5 feet bgs. The detected concentration was below its EPA RSL for resident soil of 1,800,000 µg/kg. TPH DRO and TPH GRO Detectable concentrations of TPH-DRO and TPH-GRO were identified in seven of the eighteen analyzed soil samples. TPH-DRO was detected in boring B-5 at a depth of 23 feet bgs at a concentration of 85 milligrams per kilogram (mg/kg), and in boring B-6 at a depth of 5 feet bgs at a concentration of 95.8 mg/kg and at a depth of 20 feet bgs at 106 mg/kg. The detected TPH-DRO concentration of 106 mg/kg exceeded the DC Tier 0 screening level of 100 mg/kg. However, the detected TPH-DRO concentration was below the DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 2,120 mg/kg. TPH-GRO was detected in seven of the eighteen soil samples at concentrations ranging from 0.29 mg/kg to 819 mg/kg. The highest concentration of TPH-GRO (819 mg/kg) was detected in boring B-6 at the depth of 20 feet bgs, and exceeded the DC Tier 0 screening level of 100 mg/kg and DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult of 54.4 mg/kg. RCRA Metals Five metals were detected in one or more of the eighteen analyzed soil samples. Arsenic was detected in two of the eighteen samples at a concentration of 289 mg/kg in B-1 at a depth of 5 feet bgs and 19.7 mg/kg in B-4 at a depth of 10 feet bgs. Both concentrations exceeded the EPA RSL for resident soil of 0.68 mg/kg. Barium was detected in twelve of the eighteen samples at concentrations ranging from 7.66 mg/kg to 329 mg/kg. None of the concentrations exceeded the EPA RSL for resident soil of 15,000 mg/kg. Total Chromium was detected in twelve of the eighteen samples at concentrations ranging from 7.54 mg/kg to 23.90 mg/kg. There is no established screening level for total chromium.

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Lead was detected in seventeen of the eighteen samples at concentrations ranging from 2.69 mg/kg to 109 mg/kg. None of the concentrations exceeded the EPA RSL for resident soil of 400 mg/kg. Mercury was detected in seven of the eighteen samples at concentrations ranging from 0.08 mg/kg to 1.01 mg/kg. None of the concentrations exceeded the EPA RSL for resident soil of 11 mg/kg. Groundwater Sampling Results Groundwater samples were collected from boring B-2, B-5, and B-6. All three groundwater samples collected had detected concentrations of VOCs. VOCs A total of twelve VOCs were detected. The compounds which exceeded their respective screening levels are discussed below. tert-Amyl Alcohol (TAA) was detected at a concentration of 270 micrograms per liter (µg/L) in B-5 which exceeded the EPA RSL of 6.3 µg/L for tapwater. Benzene was detected at a concentration of 9.8 µg/L in B-2, 1,400 µg/L in B-5, and 927 µg/L in B-6, each of which exceeded the DC Tier 0 screening level of 5 ug/L. Additionally, the concentrations detected in B-5 and B-6 exceeded the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 67.6 µg/L. Ethylbenzene was detected a concentration of 44.9 µg/L in B-2, 104 µg/L in B-5, and 3,540 µg/L in B-6. The detected concentrations in B-5 and B-6 exceeded the DC Tier 0 screening level of 70 ug/L. Additionally, the ethylbenzene concentration in B-6 exceeded the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 206 µg/L. Naphthalene was detected at a concentration of 12.7 µg/L in B-2 and 614 µg/L in B-6. The detected naphthalene concentration in B-6 exceeded the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 191 µg/L. Toluene was detected at a concentration of 188 µg/L in B-2, 1,580 µg/L in B-5, and 11,600 µg/L in B-6, each of which exceeded the DC Tier 0 screening level of 100 ug/L. However, none of the toluene concentrations exceeded the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 90,000 µg/L. 1,2,4-Trimethylbenzene was detected at a concentration of 19.0 µg/L in B-2, 1,200 µg/L in B-5 and 2,770 µg/L in B-6. The detected concentrations in B-5 and B-6 exceeded its EPA RSL of 56 µg/L for tapwater.

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1,3,5-Trimethylbenzene was detected at a concentration of 4.5 µg/L in B-2, 585 µg/L in B-5 and 716 µg/L in B-6. The detected concentrations in B-5 and B-6 exceeded its EPA RSL of 60 ug/L for tapwater. PAHs 2-Methylnaphthalene was detected at a concentration of 8.52 µg/L in B-2, 100 µg/L in B-5 and 464 µg/L in B-6. The detected concentrations in B-5 and B-6 exceeded its EPA RSL of 36 ug/L for tapwater. Naphthalene was detected at a concentration of 22.7 µg/L in B-2, 6.05 µg/L in B-5 and 880 ug/L in B-6. The detected concentration B-6 exceeded its DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 191 µg/L. TPH DRO and TPH GRO TPH-DRO was detected in the groundwater samples from B-5 and B-6 at concentrations of 7.04 milligrams per liter (mg/L) and 87.7 mg/L, respectively. The TPH-DRO concentrations were below the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 245 mg/L. TPH-GRO was detected in each of the three groundwater samples at a concentration of 1.35 mg/L in B-2, 39.8 mg/L in B-5 and 52.0 mg/L in B-6. The detected concentrations in B-5 and B-6 exceeded the DC Tier 1 RBSL for groundwater to indoor inhalation for a resident adult of 38.8 mg/L.

SUMMARY AND CONCLUSIONS In order to assess subsurface environmental conditions at the site, ECS advanced six borings across the site with a track-mounted Geoprobe to depths ranging between 17 to 27 feet bgs at which point refusal was encountered. Saturated conditions were observed in each of the six borings at depths ranging from 10 to 15 feet bgs. Three groundwater samples were collected from temporary wells. While drilling the soil boring B-6, white to light gray sandy clay was encountered and was saturated with free liquid petroleum product between a depth of 15 and 20 feet bgs. Petroleum odors were noted in some of the other borings. However, free liquid petroleum product was only observed in boring B-6. A total of 18 soil samples were submitted to an independent laboratory for analysis of TPH DRO, TPH GRO, VOCs, PAHs, and RCRA 8 Metals. Concentrations of VOCs including benzene, ethylbenzene, toluene, xylenes, and/or naphthalene exceeded their respective screening levels in three of the six samples collected from borings B-5 and B-6. Detected concentrations of PAHs were below their respective DC RBSLs or EPA RSLs; except for naphthalene which exceeded its DC Tier 1 RBSL for subsurface soil to indoor inhalation for a resident adult in the sample from boring B-6 collected at 20 feet bgs. TPH-DRO and TPH-GRO were detected in one of the soil samples exceeding its DC Tier 0 screening level and/or DC Tier 1 RBSL for subsurface soil to indoor

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inhalation for a resident adult. None of the metals detected exceeded their respective EPA RSL for a resident adult, with the exception of arsenic. Both detected arsenic concentrations exceeded the EPA RSL for resident soil and were above typical background concentrations for this geologic area. In the event that petroleum-impacted material is excavated, it will need to be disposed of appropriately at a landfill or treatment/disposal facility permitted to accept such wastes. Disposal criteria for contaminated soil will depend on the jurisdiction in which it is to be disposed. In the District of Columbia, soils may be re-used on site if TPH-DRO and TPH-GRO concentrations are no greater than their applicable Tier 0 and/or Tier 1 screening levels, and individual constituent concentrations of BTEX are no greater than: 0.005 part per million (ppm) for benzene; 9.6 ppm for toluene; 0.04 ppm for ethylbenzene; and, 3.86 ppm for total xylenes. Soils that are excavated containing petroleum concentrations above these thresholds or below these thresholds that cannot be reused onsite, cannot be disposed of within the District limits and must be disposed of at an appropriate disposal or treatment facility. In Maryland, based on the Land Materials Administration Fact Sheet dated August 2017, soil containing petroleum (TPH DRO or TPH GRO) concentrations less than 230 mg/kg may be used as Category 1 fill materials at both residential and non-residential sites. Soil containing petroleum (TPH DRO or TPH GRO) concentrations less than 620 mg/kg may be used as Category 2 fill materials on non-residential sites only. Soils containing petroleum concentrations greater than 620 mg/kg will need to be disposed at a licensed disposal/treatment facility capable of accepting the material. However, each of the other detected contaminants will also need to be below their respective residential or commercial screening level for use as Category 1 or 2 fill material. In Virginia, solid waste management regulations divide petroleum-impacted soils into various classes depending on concentration. Soils containing petroleum concentrations less than 50 mg/kg and total BTEX less than 10 mg/kg may be disposed with certain restrictions (see 9VAC20-81-660-D.2.d). Soils containing less than 500 mg/kg petroleum may be disposed of in a lined landfill permitted to receive such wastes. Soils containing petroleum concentrations greater than 500 mg/kg may not be disposed of in Virginia landfills, unless the permit expressly allows for such disposal. In practice, it is often difficult for developers and contractors to find a suitable disposal location for the “marginally-impacted” petroleum contaminated soils- i.e. soils containing detectable petroleum concentrations below the regulatory thresholds. This is due to the paucity of net fill construction sites in the area, and the relative abundance of legitimately clean fill materials with no petroleum contamination. Given the option, the developers of most fill sites will prefer clean fill materials over marginally-impacted materials. Consequently, it is common practice in this region to dispose of even low-level contaminated soils at petroleum-impacted soil facilities such as Clean Earth, Inc. of Greater Washington (Upper Marlboro, Maryland) or Soil Safe, Inc. (Brandywine, Maryland).

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Detected groundwater concentrations of VOCs including benzene, ethylbenzene, naphthalene, toluene, xylenes, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene and TAA, PAHs including 2-methylnaphthalene and naphthalene, TPH-DRO, and TPH-GRO exceeded their respective DC RBSLs or EPA RSLs. The property and surrounding areas are supplied with public water. Therefore, the primary risk pathway for exposure is from volatilization of subsurface contamination to indoor air. In the event contamination exceeding risk-based thresholds is left in place, ECS recommends that a vapor barrier be constructed beneath future buildings constructed. If the existing building will remain, ECS recommends soil vapor sampling to determine if the subsurface contamination poses an unacceptable vapor risk for the current building. If future redevelopment will result in groundwater dewatering during construction activities, A National Pollutant Discharge Elimination System (NPDES) permit from EPA and approval from DOEE will need to be obtained prior to discharge of the groundwater to the municipal separate storm sewer system (MS4). Additional groundwater characterization would be necessary in order to obtain DOEE approval to discharge. Based on the sampling results, it is possible that treatment of the groundwater would be necessary prior to discharge to the MS4. Based on the soil and groundwater analytical results, it is ECS’s opinion that the detected contaminant concentrations in soil and groundwater could pose an unacceptable risk to the environment and human health. The presence of free petroleum product in boring B-6 is a condition that ECS is obligated to report to the DOEE, as are the exceedances of the Tier 0 and Tier 1 Screening Levels identified for certain soil and groundwater samples. DOEE will likely open a Leaking Underground Storage Tank (LUST) case for the property as a result of the findings. Based on our experience with similar projects in the District of Columbia, additional investigation and remediation will be required before the case will be closed. While we do not know exactly what DOEE will require, it is ECS’s opinion that the additional work required for the site will include the installation of additional soil borings to assess the horizontal extent of the soil contamination, the removal of USTs and contaminated soil in the area of SB-5 and SB-6 (the maintenance shed area as discussed in the Phase I ESA), and the installation of down-gradient monitoring wells to assess the potential for off-site migration of contaminants. Additional remedial activities may be required by DOEE.

QUALIFICATIONS The conclusions presented within this report are based upon a reasonable level of investigation within normal bounds and standards of professional practice for a site in this particular geographic and geologic setting, and the areas of the site accessible for drilling. The results of this study are limited to the specific areas and elevations tested. Boring locations were chosen based on accessible areas of the site, located to avoid surface and subsurface obstructions.

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The findings of this study are not intended to serve as an audit of health and safety or compliance issues pertaining to improvements or occupant activities on-site. All observations, conclusions, and recommendations pertaining to environmental conditions at the subject site are limited to conditions observed, and or materials reviewed at the time this study was undertaken. No other warranty, expressed or implied, is made with regard to the conclusions and recommendations presented within this report. This report is provided for the exclusive use of ZOM Mid-Atlantic, Inc., and their prospective partners. This report is not intended to be used or relied upon in connection with other projects or by other unidentified third parties. The use of this letter by any undesignated third party or parties would be at such party's sole risk and ECS disclaims liability for any such third party use or reliance. ECS has not completed or used any form of predetermined language to report the conclusions of this work and it is our understanding that we will not be required to do so. Compensation for this investigation is not contingent upon results, and ECS has conducted this Phase II ESA objectively without reference to any particular outcome desired by the client. If you have any questions about this report or other aspects of this project, please contact us at (703) 471-8400. Respectfully submitted, ECS MID-ATLANTIC, LLC Swardhuni Pethe Environmental Scientist Pamela Furst, LEED AP David J. Bookbinder, C.P.G. Environmental Senior Project Manager Environmental Senior Project Manager Appendix I Boring Location Diagram Appendix II Boring Logs Appendix III Summary of Analytical Results Appendix IV Final Laboratory Results I:\_e-projects\6200-6299\6230- A HU East Campus Phase II ESA\Report\6230-A_Phase II Report_FINAL.docx

 

   

APPENDIX I

BORING LOCATION DIAGRAM

Boring Location Diagram 

Howard University ‐ East Campus 1400 Shepherd Street NE  

Washington, DC  

    ECS Project No.:   47:6230‐A 

           Scale: Not to Scale 

            Date:  8/15/2018 

 

B‐1 

B‐2 

B‐3 

B‐4 

B‐5 B‐6 

Boring Loca on 

 

APPENDIX II

BORING LOGS

0

5

10

15

20

25

30

35

28-----60

40-----60

52-----60

24-----24

Topsoil

GC-SC Fill

CL-ML

SW/SP

SM/MH

3" topsoilSandy Clay with 2" stone (GC-SC Fill), brown

Silty Clay (CL-ML), brown, med fine, moist

Sand (SW/SP), brown, loose, moist

Silty Sand (SM/MH), orange-brown, loose, wet

Refusal at 17'

PROJECT: MONITORING WELL NO. B-1

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

12

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

0

5

10

15

20

25

30

35

45-----60

48-----60

36-----60

12-----12

Topsoil

SM/MH

2" topsoilSilty Sand (SM/MH), orange-brown, loose, moist

loose, dry

color change to light brown

color change to light brown/gray, moist

Refusal at 16'

PROJECT: MONITORING WELL NO. B-2

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

15

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

0

5

10

15

20

25

30

35

22-----60

40-----60

45-----60

55-----60

36-----36

Topsoil

CH-MH

MH/SM

MH

CH

3" topsoilSilty Clay (CH-MH), brown, soft

Silty sand (MH/SM), brown to red, soft, loose

silty sand (MH/SM), red, coarse, loose, slightly moist

silty sand (MH/SM), orange/brown, coarse, loose, wet

silt (MH), red, med fine, moist

color change to orange/brown

clay (CH), brown muttling, med firm,

refusal at 23'

PROJECT: MONITORING WELL NO. B-3

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

15

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

0

5

10

15

20

25

30

35

36-----60

40-----60

40-----60

40-----60

36-----36

Topsoil

CH-MH

MH/SM

MH/CH

CH/SC

2" roots and grassclayey silt (CH-MH), brown, med coarse, med loose,moist

Silty sand (MH/SM), orange brown, coarse, moist

wet

Silty clay (MH/CH), white, trace sand, moist

Clayey Sand (CH/SC), white, med coarse, med loose,odor

refusal at 23'

PROJECT: MONITORING WELL NO. B-4

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

15

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

0

5

10

15

20

25

30

35

0.4

0.2

0.4

4.8

0.8

24-----60

24-----60

48-----60

58-----60

36-----60

24-----24

Gravel

GP-SP Fill

MH/SM

ML/SM

ML-CL

ML/SM

CH

6" gravelSandy Fill and Gravel (GP-SP Fill), brown, coarse, loose

Sandy Silt (MH/SM), brown, soft, moist

silty sand, orange/brown, coarse, wet, Sulfur odor

Silty Clay (ML-CL), white, coarse, wet

Silty sand (ML/SM), white/gray, coarse, med loose, moist

color change to gray

refusal at 23'

Clay (CH), brown/red, firm, fine, dense

refusal at 27'

PROJECT: MONITORING WELL NO. B-5

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

10

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

0

5

10

15

20

25

30

35

20-----60

20-----60

36-----60

54-----60

Asphalt

GM Fill

SW/SP

SP-SC

4" asphaltsilty gravel (GM Fill), brown

Sand (SW/SP), brown, coarse, loose, moist

black staining, odorodor continues

Sandy Clay (SP-SC), white/light gray, odor, and freeproduct

Refusal at 20'

PROJECT: MONITORING WELL NO. B-6

CLIENT: PROJECT NO.

LOCATION:

HU East Campus

ELEVATION:

N/A DRILLER:

JETCO Inc.

DATE DRILLED:

8/9/2018

LOGGED BY:

MMH, SPDRILL RIG:

GeoProbe

DEPTH TO WATER:

10

Elevation/

Depth (Ft)

PID

Readin

g

Sam

ple

Num

ber

Sam

ple

Recovery

(in/in)

Blo

w C

ount

Gra

phic

Log

Soil

Cla

ssific

ation

SOIL DESCRIPTION

This information pertains only to

this boring and should not be in

terpreted as being indicative of

the site.

Page 1 of 1

 

APPENDIX III

SUMMARY OF ANALYTICAL RESULTS

Table 1

Summary of Soil VOCs Results

1400 Shepherd Street NE

Washington, DC

Sample ID B1-5 B1-15 B1-17 B2-5 B2-15 B2-17 B3-5 B3-15 B3-23 B4-5 B4-10 B4-23 B5-5 B5-15 B5-27 B6-5 B6-10 B6-20

Sample Date 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018

Screening Level

VOCs ug/kg * ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Ethylbenzene 40 0 6.3 nd nd nd nd nd 5.3 nd nd nd nd 3.0 25.7 nd 4.9 118.0 7.6 27300

Toluene 9,600 0 27.8 17.1 nd nd nd nd 6.5 2.6 12.8 3.0 4.7 15.3 18.5 2.7 30.6 223.0 18.1 14300

Xylenes (total) 3,860 1 35.2 10.7 nd nd nd nd 64.1 3.2 12.0 6.8 10.8 18.8 168.5 4.4 26.2 696.0 52.7 173800

Benzene 5 0 nd 2.8 nd nd nd nd nd nd nd nd nd nd nd nd 7.2 2.3 nd nd

Naphthalene 188 1 nd nd nd nd nd nd 6.5 nd nd nd 9.8 3.6 nd nd nd 18.3 18.2 31200

n-Propylbenzene 3,800,000 2 nd nd nd nd nd nd 3.7 nd nd nd nd nd nd nd nd 26.4 3.8 26500.0

1,2,4-Trimethylbenzene 300,000 2 5.5 nd nd nd nd nd 46.7 nd 2.5 nd 8.0 6.0 86.1 nd 4.3 187.0 43.1 175000.0

1,3,5-Trimethylbenzene 270,000 2 nd nd nd nd nd nd 10.6 nd nd nd nd nd 21.2 nd nd 45.5 9.5 50300.0

Isopropylbenzene (Cumene) 1,900,000 2 nd nd nd nd nd nd nd nd nd nd nd nd 3.4 nd nd 8.6 nd 6960.0

n-Butylbenzene 3,900,000 2 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 4.0 nd 17600.0

Carbon disulfide 770,000 2 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 2.6 nd

sec-Butylbenzene 7,800,000 2 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 3860.0

4-Isopropyltoluene ne nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 7760.0

Notes:

Only compounds present at concentrations above the laboratory detection limit are included

*0 - DC RBCA Tier 0 Risk-Based Screening Levels (June 2011)

*1 - DC RBCA Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Level for a Resident Adult, Sub-Surface Soil, Indoor Inhalation, Updated June 2011

ug/kg = micrograms per kilogram

ne - not established

nd - not detected above laboratory method detection limit

Exceeds Screening Level

Analyte

*2 - If no DC RBCA screening level was established then the EPA Regional Screening Level (RSL) was utilized for comparison (May 2018)

Table 2

Summary of Soil PAHs Results

1400 Shepherd Street NE

Washington, DC

Sample ID B1-5 B1-15 B1-17 B2-5 B2-15 B2-17 B3-5 B3-15 B3-23 B4-5 B4-10 B4-23 B5-5 B5-15 B5-27 B6-5 B6-10 B6-20

Sample Date 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018

Screening Level*

Soil PAHs ug/kg * ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Benzo[b]fluoranthene 3,460,000 1 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 516 nd nd

Pyrene 1,800,000 2 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 491 nd nd

2-Methylnaphthalene 240,000 2 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 9,690

Naphthalene 188 1 nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd nd 8,650

Notes:

Only compounds present at concentrations above the laboratory detection limit are included

*1 - DC RBCA Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Level for a Resident Adult, Sub-Surface Soil, Indoor Inhalation, Updated June 2011

mg/kg = milligrams per kilogram

ug/kg = micrograms per kilogram

ne - not established

nd - not detected above laboratory method detection limit

Exceeds Screening Level

Analyte

*2 - If no DC RBCA screening level was established then the EPA Regional Screening Level (RSL) was utilized for comparison (May 2018)

Table 3

Summary of Soil TPH Results

1400 Shepherd Street NE

Washington, DC

Sample ID B1-5 B1-15 B1-17 B2-5 B2-15 B2-17 B3-5 B3-15 B3-23 B4-5 B4-10 B4-23 B5-5 B5-15 B5-27 B6-5 B6-10 B6-20

Sample Date 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018

Screening Level

TPH mg/kg * mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Gasoline-Range Organics 54 1 nd nd nd nd nd nd 0.29 nd nd nd 0.71 0.16 0.86 nd nd 4.24 0.27 819

Diesel-Range Organics 100 0 nd nd nd nd nd nd nd nd nd nd nd nd 85 nd nd 95.8 nd 106

Notes:

Only compounds present at concentrations above the laboratory detection limit are included

*0 - DC RBCA Tier 0 Risk-Based Screening Levels (June 2011)

*1 - DC RBCA Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Level for a Resident Adult, Sub-Surface Soil, Indoor Inhalation, Updated June 2011

mg/kg = milligrams per kilogram

ug/kg = micrograms per kilogram

ne - not established

nd - not detected above laboratory method detection limit

Exceeds Screening Level

Analyte

*2 - If no DC RBCA screening level was established then the EPA Regional Screening Level (RSL) was utilized for comparison (May 2018)

Table 4

Summary of Soil Metals Results

1400 Shepherd Street NE

Washington, DC

Sample ID B1-5 B1-15 B1-17 B2-5 B2-15 B2-17 B3-5 B3-15 B3-23 B4-5 B4-10 B4-23 B5-5 B5-15 B5-27 B6-5 B6-10 B6-20

Sample Date 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018 8/9/2018

Screening Level

RCRA 8 Metals mg/kg * mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Arsenic 0.68 2 289.0 nd nd nd nd nd nd nd nd nd 19.7 nd nd nd nd nd nd nd

Barium 15,000.00 2 22.1 11.2 nd 17.0 nd 7.66 31.00 nd nd 21.60 9.07 nd 35.10 nd 329.00 21.50 25.00 nd

Total Chromium ne 22.5 9.19 7.54 8.61 nd 6.90 14.40 nd nd 12.00 11.30 nd 12.10 23.30 23.90 19.00 19.90 nd

Lead 400.00 2 23.4 7.03 7.28 11.6 4.35 2.69 13.80 4.48 nd 10.00 4.37 5.75 109.00 2.71 68.20 22.60 29.80 9.82

Mercury (elemental) 11.00 2 0.08 nd nd nd nd 0.12 nd nd nd 0.10 0.10 nd 0.10 nd nd 0.70 1.01 nd

Notes:

Only compounds present at concentrations above the laboratory detection limit are included

*1 - DC RBCA Technical Guidance Tier 1, Table 5-9 Risk-Based Screening Level for a Resident Adult, Sub-Surface Soil, Indoor Inhalation, Updated June 2011

mg/kg = milligrams per kilogram

ug/kg = micrograms per kilogram

ne - not established

nd - not detected above laboratory method detection limit

Exceeds Screening Level

Analyte

*2 - If no DC RBCA screening level was established then the EPA Regional Screening Level (RSL) was utilized for comparison (May 2018)

Table 5

Summary of Groundwater Analytical Results

1400 Shepherd Street NE

Washington, DC

Sample ID B2 B5 B6

Sample Date 8/9/2018 8/9/2018 8/9/2018

Screening Level

GW VOCs ug/L * ug/L ug/L ug/L

Benzene 5 2 9.8 1,400 927

Ethylbenzene 70 2 44.9 104 3,540

Naphthalene 191 1 12.7 nd 614

Toluene 100 2 188 1,580 11,600

1,2,4-Trimethylbenzene 56 3 19.0 1,200 2,770

1,3,5-Trimethylbenzene 60 3 4.5 585 716

tert-Amyl alcohol (TAA) 6.3 3 nd 270 nd

sec-Butylbenzene 2,000 3 nd 61.3 nd

Isopropylbenzene (Cumene) 450 3 nd 76.6 nd

4-Isopropyltoluene ne nd 122 nd

n-Propylbenzene 660 6.7 450 489

Xylenes (total) 1,000 2 162 365 14,010

GW PAHs ug/L ug/L ug/L ug/L

2-Methylnaphthalene 36 3 8.52 100 464

Naphthalene 191 1 22.7 6.05 880

GW TPH mg/L mg/L mg/L mg/L

Gasoline-Range Organics 38.8 1 1.35 39.8 52

Diesel-Range Organics 245 1 nd 7.04 87.7

Notes:

ne - not established

nd - not detected above laboratory method detection limit

Exceeds Screening Level

Analyte

*1 - DC Risk-Based Corrective Action (RBCA) Technical Guidance, Table 5-9 Risk-Based Screening Level for

a Resident Adult, Groundwater, Indoor Inhalation, Updated June 2011

*2 - If no DC RBCA screening level was established then the EPA Region 3 Regional Screening Level (RSL)

Summary Table May 2018 Maximum Contaminant level (MCL) was utilized for comparison.

*3 - IF EPA MCL is not available then the EPA Region 3 Regional Screening Level (RSL) Summary Table

May 2018 Screening Level for Tapwater was utilized for comparison

 

APPENDIX IV

FINAL LABORATORY REPORTS

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

VELAP ID 460040

ECS-Chantilly

RE: HOWARD UNIVERSITY

Chantilly, VA 20151

14026 Thunderbolt Place, Suite 100

Pam Furst

Will Brewington

President

Enclosed are the results of analyses for samples received by the laboratory on 08/10/18 14:45.

A more detailed report format is available upon request, which lists the accreditation status for all analytical

methods performed.

Please visit our website at www.mdspectral.com for a complete listing of our accreditations.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

21 August 2018

Page 1 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

Client Sample ID Laboratory ID Matrix Date Sampled Date ReceivedAlternate Sample ID

B1-5' 8081012-01 08/09/18 00:00 08/10/18 14:45Soil

B1-15' 8081012-02 08/09/18 00:00 08/10/18 14:45Soil

B1-17' 8081012-03 08/09/18 00:00 08/10/18 14:45Soil

B2-5' 8081012-04 08/09/18 00:00 08/10/18 14:45Soil

B2-15' 8081012-05 08/09/18 00:00 08/10/18 14:45Soil

B2-17' 8081012-06 08/09/18 00:00 08/10/18 14:45Soil

B3-5' 8081012-07 08/09/18 00:00 08/10/18 14:45Soil

B3-15' 8081012-08 08/09/18 00:00 08/10/18 14:45Soil

B3-23' 8081012-09 08/09/18 00:00 08/10/18 14:45Soil

B4-5' 8081012-10 08/09/18 00:00 08/10/18 14:45Soil

B4-10' 8081012-11 08/09/18 00:00 08/10/18 14:45Soil

B4-23' 8081012-12 08/09/18 00:00 08/10/18 14:45Soil

B5-5' 8081012-13 08/09/18 00:00 08/10/18 14:45Soil

B5-15' 8081012-14 08/09/18 00:00 08/10/18 14:45Soil

B5-27' 8081012-15 08/09/18 00:00 08/10/18 14:45Soil

B6-5' 8081012-16 08/09/18 00:00 08/10/18 14:45Soil

B6-10' 8081012-17 08/09/18 00:00 08/10/18 14:45Soil

B6-20' 8081012-18 08/09/18 00:00 08/10/18 14:45Soil

B2 8081012-19 08/09/18 00:00 08/10/18 14:45Nonpotable Water

B5 8081012-20 08/09/18 00:00 08/10/18 14:45Nonpotable Water

B6 8081012-21 08/09/18 00:00 08/10/18 14:45Nonpotable Water

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 2 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-5'

8081012-01 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 13:57Acetone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 13:57tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 13:57tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Benzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 13:57tert-Butanol (TBA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 13:572-Butanone (MEK) 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 13:57n-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 13:57Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 13:572-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:574-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 3 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-5'

8081012-01 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 13:57trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:572,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

6.3 08/13/18 08/13/18 13:57Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:572-Hexanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 13:57Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:574-Isopropyltoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:574-Methyl-2-pentanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 13:57Methylene chloride 22.7ug/kg dry 1 GM22.7

ND 08/13/18 08/13/18 13:57Naphthalene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Tetrachloroethene 5.7ug/kg dry 1 GM2.3

27.8 08/13/18 08/13/18 13:57Toluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:57Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

5.5 08/13/18 08/13/18 13:571,2,4-Trimethylbenzene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 13:571,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 4 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-5'

8081012-01 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 13:57Vinyl chloride 5.7ug/kg dry 1 GM2.3

10.6 08/13/18 08/13/18 13:57o-Xylene 5.7ug/kg dry 1 GM2.3

24.6 08/13/18 08/13/18 13:57m- & p-Xylenes 5.7ug/kg dry 1 GM2.3

08/13/18 08/13/18 13:5770-130 105 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 13:5775-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 13:5765-120 97 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 12:23Acenaphthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Acenaphthylene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Benzo[a]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Benzo[b]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Benzo[k]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Benzo[ghi]perylene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Benzo[a]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Chrysene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Dibenzo[a,h]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Fluorene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Indeno[1,2,3-cd]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:232-Methylnaphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Naphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Phenanthrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 12:23Pyrene 284ug/kg dry 1 WB114

08/13/18 08/15/18 12:2321-110 84 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 12:2310-110 85 %Surrogate: Phenol-d5

08/13/18 08/15/18 12:2335-114 78 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 12:2310-123 86 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 12:2343-116 80 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 12:2333-141 107 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 5 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-5'

8081012-01 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 13:39Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/15/18 22:30Diesel-Range Organics 9.1mg/kg dry 1 SJA9.1

08/14/18 08/15/18 22:3070-130 90 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

88 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

87.6 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

289 08/13/18 08/20/18 10:39Arsenic 18.7mg/kg dry 2 RAS18.7

22.1 08/13/18 08/20/18 10:39Barium 7.49mg/kg dry 2 RAS7.49

ND 08/13/18 08/20/18 10:39Cadmium 1.87mg/kg dry 2 RAS1.87

22.5 08/13/18 08/20/18 16:17Chromium 5.61mg/kg dry 2 RAS5.61

23.4 08/13/18 08/20/18 10:39Lead 0.0187mg/kg dry 2 RAS0.0187

ND 08/13/18 08/21/18 09:49Selenium 9.36mg/kg dry 2 RAS9.36

ND 08/13/18 08/20/18 16:17Silver 3.74mg/kg dry 2 RAS3.74

Metals EPA 6020 Performed at Enviro-Chem

0.0778 08/13/18 08/20/18 14:03Mercury 0.0749mg/kg dry 2 MAP0.0749

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 6 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-15'

8081012-02 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 14:22Acetone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 14:22tert-Amyl alcohol (TAA) 58.8ug/kg dry 1 GM58.8

ND 08/13/18 08/13/18 14:22tert-Amyl methyl ether (TAME) 5.9ug/kg dry 1 GM2.4

2.8 08/13/18 08/13/18 14:22Benzene 5.9J ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Bromobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Bromochloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Bromodichloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Bromoform 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Bromomethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 14:22tert-Butanol (TBA) 58.8ug/kg dry 1 GM58.8

ND 08/13/18 08/13/18 14:222-Butanone (MEK) 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 14:22n-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22sec-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22tert-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Carbon disulfide 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Carbon tetrachloride 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Chlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Chloroethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 14:22Chloroform 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Chloromethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 14:222-Chlorotoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:224-Chlorotoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2-Dibromo-3-chloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Dibromochloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2-Dibromoethane (EDB) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Dibromomethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,3-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,4-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Dichlorodifluoromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1-Dichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2-Dichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1-Dichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22cis-1,2-Dichloroethene 5.9ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 7 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-15'

8081012-02 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 14:22trans-1,2-Dichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Dichlorofluoromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,3-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:222,2-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22cis-1,3-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22trans-1,3-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Diisopropyl ether (DIPE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Ethyl tert-butyl ether (ETBE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Ethylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Hexachlorobutadiene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:222-Hexanone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 14:22Isopropylbenzene (Cumene) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:224-Isopropyltoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Methyl tert-butyl ether (MTBE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:224-Methyl-2-pentanone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 14:22Methylene chloride 23.5ug/kg dry 1 GM23.5

ND 08/13/18 08/13/18 14:22Naphthalene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22n-Propylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Styrene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1,1,2-Tetrachloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1,2,2-Tetrachloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Tetrachloroethene 5.9ug/kg dry 1 GM2.4

17.1 08/13/18 08/13/18 14:22Toluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2,3-Trichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2,4-Trichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1,1-Trichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,1,2-Trichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Trichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:22Trichlorofluoromethane (Freon 11) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2,3-Trichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,2,4-Trimethylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 14:221,3,5-Trimethylbenzene 5.9ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 8 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-15'

8081012-02 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 14:22Vinyl chloride 5.9ug/kg dry 1 GM2.4

3.8 08/13/18 08/13/18 14:22o-Xylene 5.9J ug/kg dry 1 GM2.4

6.9 08/13/18 08/13/18 14:22m- & p-Xylenes 5.9ug/kg dry 1 GM2.4

08/13/18 08/13/18 14:2270-130 105 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 14:2275-120 92 %Surrogate: Toluene-d8

08/13/18 08/13/18 14:2265-120 94 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 13:07Acenaphthene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Acenaphthylene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Benzo[a]anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Benzo[b]fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Benzo[k]fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Benzo[ghi]perylene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Benzo[a]pyrene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Chrysene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Dibenzo[a,h]anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Fluorene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Indeno[1,2,3-cd]pyrene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:072-Methylnaphthalene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Naphthalene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Phenanthrene 294ug/kg dry 1 WB118

ND 08/13/18 08/15/18 13:07Pyrene 294ug/kg dry 1 WB118

08/13/18 08/15/18 13:0721-110 83 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 13:0710-110 84 %Surrogate: Phenol-d5

08/13/18 08/15/18 13:0735-114 78 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 13:0710-123 88 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 13:0743-116 79 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 13:0733-141 102 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 9 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-15'

8081012-02 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 14:12Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/15/18 22:56Diesel-Range Organics 9.4mg/kg dry 1 SJA9.4

08/14/18 08/15/18 22:5670-130 89 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

85 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

83.7 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 10:56Arsenic 23.0mg/kg dry 2 RAS23.0

11.2 08/13/18 08/20/18 10:56Barium 9.19mg/kg dry 2 RAS9.19

ND 08/13/18 08/20/18 10:56Cadmium 2.30mg/kg dry 2 RAS2.30

9.19 08/13/18 08/20/18 16:29Chromium 6.89mg/kg dry 2 RAS6.89

7.03 08/13/18 08/20/18 10:56Lead 0.0230mg/kg dry 2 RAS0.0230

ND 08/13/18 08/21/18 10:05Selenium 11.5mg/kg dry 2 RAS11.5

ND 08/13/18 08/20/18 16:29Silver 4.59mg/kg dry 2 RAS4.59

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:18Mercury 0.0919mg/kg dry 2 MAP0.0919

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 10 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-17'

8081012-03 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 14:46Acetone 11.5ug/kg dry 1 GM11.5

ND 08/13/18 08/13/18 14:46tert-Amyl alcohol (TAA) 57.5ug/kg dry 1 GM57.5

ND 08/13/18 08/13/18 14:46tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Benzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 14:46tert-Butanol (TBA) 57.5ug/kg dry 1 GM57.5

ND 08/13/18 08/13/18 14:462-Butanone (MEK) 11.5ug/kg dry 1 GM11.5

ND 08/13/18 08/13/18 14:46n-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 14:46Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 14:462-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:464-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 11 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-17'

8081012-03 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 14:46trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:462,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:462-Hexanone 11.5ug/kg dry 1 GM11.5

ND 08/13/18 08/13/18 14:46Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:464-Isopropyltoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:464-Methyl-2-pentanone 11.5ug/kg dry 1 GM11.5

ND 08/13/18 08/13/18 14:46Methylene chloride 23.0ug/kg dry 1 GM23.0

ND 08/13/18 08/13/18 14:46Naphthalene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Tetrachloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Toluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,2,4-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:461,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 12 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-17'

8081012-03 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 14:46Vinyl chloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46o-Xylene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 14:46m- & p-Xylenes 5.7ug/kg dry 1 GM2.3

08/13/18 08/13/18 14:4670-130 106 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 14:4675-120 90 %Surrogate: Toluene-d8

08/13/18 08/13/18 14:4665-120 91 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 15:23Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/15/18 23:22Diesel-Range Organics 9.2mg/kg dry 1 SJA9.2

08/14/18 08/15/18 23:2270-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

87 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

86.9 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 10:58Arsenic 18.9mg/kg dry 2 RAS18.9

ND 08/13/18 08/20/18 10:58Barium 7.54mg/kg dry 2 RAS7.54

ND 08/13/18 08/20/18 10:58Cadmium 1.89mg/kg dry 2 RAS1.89

7.54 08/13/18 08/20/18 16:31Chromium 5.66mg/kg dry 2 RAS5.66

7.28 08/13/18 08/20/18 10:58Lead 0.0189mg/kg dry 2 RAS0.0189

ND 08/13/18 08/21/18 10:07Selenium 9.43mg/kg dry 2 RAS9.43

ND 08/13/18 08/20/18 16:31Silver 3.77mg/kg dry 2 RAS3.77

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 13 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-17'

8081012-03 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:21Mercury 0.0754mg/kg dry 2 MAP0.0754

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 14 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B1-17'

8081012-03RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 13:35Acenaphthene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Acenaphthylene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Anthracene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Benzo[a]anthracene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Benzo[b]fluoranthene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Benzo[k]fluoranthene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Benzo[ghi]perylene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Benzo[a]pyrene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Chrysene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Dibenzo[a,h]anthracene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Fluoranthene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Fluorene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Indeno[1,2,3-cd]pyrene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:352-Methylnaphthalene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Naphthalene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Phenanthrene 287ug/kg dry 1 WB115

ND 08/13/18 08/17/18 13:35Pyrene 287ug/kg dry 1 WB115

08/13/18 08/17/18 13:3521-110 76 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 13:3510-110 78 %Surrogate: Phenol-d5

08/13/18 08/17/18 13:3535-114 69 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 13:3510-123 84 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 13:3543-116 81 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 13:3533-141 110 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 15 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-5'

8081012-04 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 15:11Acetone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 15:11tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 15:11tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Benzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 15:11tert-Butanol (TBA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 15:112-Butanone (MEK) 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 15:11n-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 15:11Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 15:112-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:114-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 16 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-5'

8081012-04 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 15:11trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:112,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:112-Hexanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 15:11Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:114-Isopropyltoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:114-Methyl-2-pentanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 15:11Methylene chloride 22.7ug/kg dry 1 GM22.7

ND 08/13/18 08/13/18 15:11Naphthalene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Tetrachloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Toluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,2,4-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:111,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 17 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-5'

8081012-04 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 15:11Vinyl chloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11o-Xylene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 15:11m- & p-Xylenes 5.7ug/kg dry 1 GM2.3

08/13/18 08/13/18 15:1170-130 108 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 15:1175-120 90 %Surrogate: Toluene-d8

08/13/18 08/13/18 15:1165-120 92 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 14:35Acenaphthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Acenaphthylene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Benzo[a]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Benzo[b]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Benzo[k]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Benzo[ghi]perylene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Benzo[a]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Chrysene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Dibenzo[a,h]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Fluorene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Indeno[1,2,3-cd]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:352-Methylnaphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Naphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Phenanthrene 284ug/kg dry 1 WB114

ND 08/13/18 08/15/18 14:35Pyrene 284ug/kg dry 1 WB114

08/13/18 08/15/18 14:3521-110 78 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 14:3510-110 80 %Surrogate: Phenol-d5

08/13/18 08/15/18 14:3535-114 76 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 14:3510-123 76 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 14:3543-116 79 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 14:3533-141 95 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 18 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-5'

8081012-04 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 15:56Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/15/18 23:49Diesel-Range Organics 9.1mg/kg dry 1 SJA9.1

08/14/18 08/15/18 23:4970-130 92 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

88 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

86.0 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:04Arsenic 21.5mg/kg dry 2 RAS21.5

17.0 08/13/18 08/20/18 11:04Barium 8.61mg/kg dry 2 RAS8.61

ND 08/13/18 08/20/18 11:04Cadmium 2.15mg/kg dry 2 RAS2.15

8.61 08/13/18 08/20/18 16:40Chromium 6.46mg/kg dry 2 RAS6.46

11.6 08/13/18 08/20/18 11:04Lead 0.0215mg/kg dry 2 RAS0.0215

ND 08/13/18 08/21/18 10:20Selenium 10.8mg/kg dry 2 RAS10.8

ND 08/13/18 08/20/18 16:40Silver 4.30mg/kg dry 2 RAS4.30

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:30Mercury 0.0861mg/kg dry 2 MAP0.0861

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 19 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-15'

8081012-05 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 15:36Acetone 11.0ug/kg dry 1 GM11.0

ND 08/13/18 08/13/18 15:36tert-Amyl alcohol (TAA) 54.9ug/kg dry 1 GM54.9

ND 08/13/18 08/13/18 15:36tert-Amyl methyl ether (TAME) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Benzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Bromobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Bromochloromethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Bromodichloromethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Bromoform 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Bromomethane 5.5ug/kg dry 1 GM5.5

ND 08/13/18 08/13/18 15:36tert-Butanol (TBA) 54.9ug/kg dry 1 GM54.9

ND 08/13/18 08/13/18 15:362-Butanone (MEK) 11.0ug/kg dry 1 GM11.0

ND 08/13/18 08/13/18 15:36n-Butylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36sec-Butylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36tert-Butylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Carbon disulfide 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Carbon tetrachloride 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Chlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Chloroethane 5.5ug/kg dry 1 GM5.5

ND 08/13/18 08/13/18 15:36Chloroform 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Chloromethane 5.5ug/kg dry 1 GM5.5

ND 08/13/18 08/13/18 15:362-Chlorotoluene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:364-Chlorotoluene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2-Dibromo-3-chloropropane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Dibromochloromethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2-Dibromoethane (EDB) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Dibromomethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2-Dichlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,3-Dichlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,4-Dichlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Dichlorodifluoromethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1-Dichloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2-Dichloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1-Dichloroethene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36cis-1,2-Dichloroethene 5.5ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 20 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-15'

8081012-05 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 15:36trans-1,2-Dichloroethene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Dichlorofluoromethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2-Dichloropropane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,3-Dichloropropane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:362,2-Dichloropropane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1-Dichloropropene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36cis-1,3-Dichloropropene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36trans-1,3-Dichloropropene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Diisopropyl ether (DIPE) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Ethyl tert-butyl ether (ETBE) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Ethylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Hexachlorobutadiene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:362-Hexanone 11.0ug/kg dry 1 GM11.0

ND 08/13/18 08/13/18 15:36Isopropylbenzene (Cumene) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:364-Isopropyltoluene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Methyl tert-butyl ether (MTBE) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:364-Methyl-2-pentanone 11.0ug/kg dry 1 GM11.0

ND 08/13/18 08/13/18 15:36Methylene chloride 22.0ug/kg dry 1 GM22.0

ND 08/13/18 08/13/18 15:36Naphthalene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36n-Propylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Styrene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1,1,2-Tetrachloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1,2,2-Tetrachloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Tetrachloroethene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Toluene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2,3-Trichlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2,4-Trichlorobenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1,1-Trichloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,1,2-Trichloroethane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Trichloroethene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36Trichlorofluoromethane (Freon 11) 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2,3-Trichloropropane 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,2,4-Trimethylbenzene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:361,3,5-Trimethylbenzene 5.5ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 21 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-15'

8081012-05 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 15:36Vinyl chloride 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36o-Xylene 5.5ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 15:36m- & p-Xylenes 5.5ug/kg dry 1 GM2.2

08/13/18 08/13/18 15:3670-130 109 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 15:3675-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 15:3665-120 91 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 22:11Acenaphthene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Acenaphthylene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Anthracene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Benzo[a]anthracene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Benzo[b]fluoranthene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Benzo[k]fluoranthene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Benzo[ghi]perylene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Benzo[a]pyrene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Chrysene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Dibenzo[a,h]anthracene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Fluoranthene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Fluorene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Indeno[1,2,3-cd]pyrene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:112-Methylnaphthalene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Naphthalene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Phenanthrene 275ug/kg dry 1 WB110

ND 08/13/18 08/15/18 22:11Pyrene 275ug/kg dry 1 WB110

08/13/18 08/15/18 22:1121-110 85 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 22:1110-110 84 %Surrogate: Phenol-d5

08/13/18 08/15/18 22:1135-114 75 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 22:1110-123 91 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 22:1143-116 81 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 22:1133-141 98 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 22 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-15'

8081012-05 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 16:29Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 00:15Diesel-Range Organics 8.8mg/kg dry 1 SJA8.8

08/14/18 08/16/18 00:1570-130 105 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

91 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

90.1 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:06Arsenic 21.8mg/kg dry 2 RAS21.8

ND 08/13/18 08/20/18 11:06Barium 8.70mg/kg dry 2 RAS8.70

ND 08/13/18 08/20/18 11:06Cadmium 2.18mg/kg dry 2 RAS2.18

ND 08/13/18 08/20/18 16:42Chromium 6.53mg/kg dry 2 RAS6.53

4.35 08/13/18 08/20/18 11:06Lead 0.0218mg/kg dry 2 RAS0.0218

ND 08/13/18 08/21/18 10:22Selenium 10.9mg/kg dry 2 RAS10.9

ND 08/13/18 08/20/18 16:42Silver 4.35mg/kg dry 2 RAS4.35

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:33Mercury 0.0870mg/kg dry 2 MAP0.0870

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 23 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-17'

8081012-06 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 16:00Acetone 11.2ug/kg dry 1 GM11.2

ND 08/13/18 08/13/18 16:00tert-Amyl alcohol (TAA) 56.2ug/kg dry 1 GM56.2

ND 08/13/18 08/13/18 16:00tert-Amyl methyl ether (TAME) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Benzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Bromobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Bromochloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Bromodichloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Bromoform 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Bromomethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 16:00tert-Butanol (TBA) 56.2ug/kg dry 1 GM56.2

ND 08/13/18 08/13/18 16:002-Butanone (MEK) 11.2ug/kg dry 1 GM11.2

ND 08/13/18 08/13/18 16:00n-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00sec-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00tert-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Carbon disulfide 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Carbon tetrachloride 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Chlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Chloroethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 16:00Chloroform 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Chloromethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 16:002-Chlorotoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:004-Chlorotoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2-Dibromo-3-chloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Dibromochloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2-Dibromoethane (EDB) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Dibromomethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,3-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,4-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Dichlorodifluoromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1-Dichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2-Dichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1-Dichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00cis-1,2-Dichloroethene 5.6ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 24 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-17'

8081012-06 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:00trans-1,2-Dichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Dichlorofluoromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,3-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:002,2-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00cis-1,3-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00trans-1,3-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Diisopropyl ether (DIPE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Ethyl tert-butyl ether (ETBE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Ethylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Hexachlorobutadiene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:002-Hexanone 11.2ug/kg dry 1 GM11.2

ND 08/13/18 08/13/18 16:00Isopropylbenzene (Cumene) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:004-Isopropyltoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Methyl tert-butyl ether (MTBE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:004-Methyl-2-pentanone 11.2ug/kg dry 1 GM11.2

ND 08/13/18 08/13/18 16:00Methylene chloride 22.5ug/kg dry 1 GM22.5

ND 08/13/18 08/13/18 16:00Naphthalene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00n-Propylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Styrene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1,1,2-Tetrachloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1,2,2-Tetrachloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Tetrachloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Toluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2,3-Trichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2,4-Trichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1,1-Trichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,1,2-Trichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Trichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00Trichlorofluoromethane (Freon 11) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2,3-Trichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,2,4-Trimethylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:001,3,5-Trimethylbenzene 5.6ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 25 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-17'

8081012-06 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:00Vinyl chloride 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00o-Xylene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 16:00m- & p-Xylenes 5.6ug/kg dry 1 GM2.2

08/13/18 08/13/18 16:0070-130 109 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 16:0075-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 16:0065-120 92 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 22:55Acenaphthene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Acenaphthylene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Anthracene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Benzo[a]anthracene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Benzo[b]fluoranthene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Benzo[k]fluoranthene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Benzo[ghi]perylene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Benzo[a]pyrene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Chrysene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Dibenzo[a,h]anthracene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Fluoranthene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Fluorene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Indeno[1,2,3-cd]pyrene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:552-Methylnaphthalene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Naphthalene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Phenanthrene 281ug/kg dry 1 WB112

ND 08/13/18 08/15/18 22:55Pyrene 281ug/kg dry 1 WB112

08/13/18 08/15/18 22:5521-110 63 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 22:5510-110 63 %Surrogate: Phenol-d5

08/13/18 08/15/18 22:5535-114 59 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 22:5510-123 73 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 22:5543-116 63 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 22:5533-141 104 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 26 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2-17'

8081012-06 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 17:03Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 00:41Diesel-Range Organics 9.0mg/kg dry 1 SJA9.0

08/14/18 08/16/18 00:4170-130 92 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

89 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

82.8 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:08Arsenic 17.3mg/kg dry 2 RAS17.3

7.66 08/13/18 08/20/18 11:08Barium 6.90mg/kg dry 2 RAS6.90

ND 08/13/18 08/20/18 11:08Cadmium 1.73mg/kg dry 2 RAS1.73

6.90 08/13/18 08/20/18 16:49Chromium 5.18mg/kg dry 2 RAS5.18

2.69 08/13/18 08/20/18 11:08Lead 0.0173mg/kg dry 2 RAS0.0173

ND 08/13/18 08/21/18 10:24Selenium 8.63mg/kg dry 2 RAS8.63

ND 08/13/18 08/20/18 16:49Silver 3.45mg/kg dry 2 RAS3.45

Metals EPA 6020 Performed at Enviro-Chem

0.116 08/13/18 08/20/18 14:36Mercury 0.0690mg/kg dry 2 MAP0.0690

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 27 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-5'

8081012-07 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 16:25Acetone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 16:25tert-Amyl alcohol (TAA) 58.1ug/kg dry 1 GM58.1

ND 08/13/18 08/13/18 16:25tert-Amyl methyl ether (TAME) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Benzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Bromobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Bromochloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Bromodichloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Bromoform 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Bromomethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 16:25tert-Butanol (TBA) 58.1ug/kg dry 1 GM58.1

ND 08/13/18 08/13/18 16:252-Butanone (MEK) 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 16:25n-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25sec-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25tert-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Carbon disulfide 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Carbon tetrachloride 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Chlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Chloroethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 16:25Chloroform 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Chloromethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 16:252-Chlorotoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:254-Chlorotoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2-Dibromo-3-chloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Dibromochloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2-Dibromoethane (EDB) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Dibromomethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,3-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,4-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Dichlorodifluoromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1-Dichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2-Dichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1-Dichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25cis-1,2-Dichloroethene 5.8ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 28 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-5'

8081012-07 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:25trans-1,2-Dichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Dichlorofluoromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,3-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:252,2-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25cis-1,3-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25trans-1,3-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Diisopropyl ether (DIPE) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Ethyl tert-butyl ether (ETBE) 5.8ug/kg dry 1 GM2.3

5.3 08/13/18 08/13/18 16:25Ethylbenzene 5.8J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Hexachlorobutadiene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:252-Hexanone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 16:25Isopropylbenzene (Cumene) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:254-Isopropyltoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Methyl tert-butyl ether (MTBE) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:254-Methyl-2-pentanone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 16:25Methylene chloride 23.3ug/kg dry 1 GM23.3

6.5 08/13/18 08/13/18 16:25Naphthalene 5.8ug/kg dry 1 GM2.3

3.7 08/13/18 08/13/18 16:25n-Propylbenzene 5.8J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Styrene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1,1,2-Tetrachloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1,2,2-Tetrachloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Tetrachloroethene 5.8ug/kg dry 1 GM2.3

6.5 08/13/18 08/13/18 16:25Toluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2,3-Trichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2,4-Trichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1,1-Trichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,1,2-Trichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Trichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:25Trichlorofluoromethane (Freon 11) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:251,2,3-Trichloropropane 5.8ug/kg dry 1 GM2.3

46.7 08/13/18 08/13/18 16:251,2,4-Trimethylbenzene 5.8ug/kg dry 1 GM2.3

10.6 08/13/18 08/13/18 16:251,3,5-Trimethylbenzene 5.8ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 29 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-5'

8081012-07 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:25Vinyl chloride 5.8ug/kg dry 1 GM2.3

27.6 08/13/18 08/13/18 16:25o-Xylene 5.8ug/kg dry 1 GM2.3

36.5 08/13/18 08/13/18 16:25m- & p-Xylenes 5.8ug/kg dry 1 GM2.3

08/13/18 08/13/18 16:2570-130 111 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 16:2575-120 90 %Surrogate: Toluene-d8

08/13/18 08/13/18 16:2565-120 99 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/15/18 23:38Acenaphthene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Acenaphthylene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Anthracene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Benzo[a]anthracene 291ug/kg dry 1 WB116

122 08/13/18 08/15/18 23:38Benzo[b]fluoranthene 291J ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Benzo[k]fluoranthene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Benzo[ghi]perylene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Benzo[a]pyrene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Chrysene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Dibenzo[a,h]anthracene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Fluoranthene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Fluorene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Indeno[1,2,3-cd]pyrene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:382-Methylnaphthalene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Naphthalene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Phenanthrene 291ug/kg dry 1 WB116

ND 08/13/18 08/15/18 23:38Pyrene 291ug/kg dry 1 WB116

08/13/18 08/15/18 23:3821-110 58 %Surrogate: 2-Fluorophenol

08/13/18 08/15/18 23:3810-110 62 %Surrogate: Phenol-d5

08/13/18 08/15/18 23:3835-114 58 %Surrogate: Nitrobenzene-d5

08/13/18 08/15/18 23:3810-123 80 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/15/18 23:3843-116 60 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/15/18 23:3833-141 97 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 30 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-5'

8081012-07 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

0.29 08/14/18 08/14/18 17:36Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 01:07Diesel-Range Organics 9.3mg/kg dry 1 SJA9.3

08/14/18 08/16/18 01:0770-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

86 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

83.5 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:09Arsenic 24.0mg/kg dry 2 RAS24.0

31.0 08/13/18 08/20/18 11:09Barium 9.59mg/kg dry 2 RAS9.59

ND 08/13/18 08/20/18 11:09Cadmium 2.40mg/kg dry 2 RAS2.40

14.4 08/13/18 08/20/18 16:51Chromium 7.19mg/kg dry 2 RAS7.19

13.8 08/13/18 08/20/18 11:09Lead 0.0240mg/kg dry 2 RAS0.0240

ND 08/13/18 08/21/18 10:25Selenium 12.0mg/kg dry 2 RAS12.0

ND 08/13/18 08/20/18 16:51Silver 4.79mg/kg dry 2 RAS4.79

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:39Mercury 0.0959mg/kg dry 2 MAP0.0959

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 31 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-15'

8081012-08 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 16:51Acetone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 16:51tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 16:51tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Benzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 16:51tert-Butanol (TBA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 16:512-Butanone (MEK) 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 16:51n-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 16:51Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 16:512-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:514-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 32 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-15'

8081012-08 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:51trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:512,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:512-Hexanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 16:51Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:514-Isopropyltoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:514-Methyl-2-pentanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 16:51Methylene chloride 22.7ug/kg dry 1 GM22.7

ND 08/13/18 08/13/18 16:51Naphthalene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Tetrachloroethene 5.7ug/kg dry 1 GM2.3

2.6 08/13/18 08/13/18 16:51Toluene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,2,4-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:511,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 33 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-15'

8081012-08 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 16:51Vinyl chloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 16:51o-Xylene 5.7ug/kg dry 1 GM2.3

3.2 08/13/18 08/13/18 16:51m- & p-Xylenes 5.7J ug/kg dry 1 GM2.3

08/13/18 08/13/18 16:5170-130 109 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 16:5175-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 16:5165-120 93 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/16/18 00:23Acenaphthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Acenaphthylene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Benzo[a]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Benzo[b]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Benzo[k]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Benzo[ghi]perylene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Benzo[a]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Chrysene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Dibenzo[a,h]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Fluorene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Indeno[1,2,3-cd]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:232-Methylnaphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Naphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Phenanthrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 00:23Pyrene 284ug/kg dry 1 WB114

08/13/18 08/16/18 00:2321-110 82 %Surrogate: 2-Fluorophenol

08/13/18 08/16/18 00:2310-110 82 %Surrogate: Phenol-d5

08/13/18 08/16/18 00:2335-114 75 %Surrogate: Nitrobenzene-d5

08/13/18 08/16/18 00:2310-123 86 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/16/18 00:2343-116 78 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/16/18 00:2333-141 95 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 34 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-15'

8081012-08 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 18:10Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 01:33Diesel-Range Organics 9.1mg/kg dry 1 SJA9.1

08/14/18 08/16/18 01:3370-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

88 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

87.3 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:11Arsenic 16.8mg/kg dry 2 RAS16.8

ND 08/13/18 08/20/18 11:11Barium 6.74mg/kg dry 2 RAS6.74

ND 08/13/18 08/20/18 11:11Cadmium 1.68mg/kg dry 2 RAS1.68

ND 08/13/18 08/20/18 16:53Chromium 5.05mg/kg dry 2 RAS5.05

4.48 08/13/18 08/20/18 11:11Lead 0.0168mg/kg dry 2 RAS0.0168

ND 08/13/18 08/21/18 10:27Selenium 8.42mg/kg dry 2 RAS8.42

ND 08/13/18 08/20/18 16:53Silver 3.37mg/kg dry 2 RAS3.37

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:41Mercury 0.0674mg/kg dry 2 MAP0.0674

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 35 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-23'

8081012-09 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 17:16Acetone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 17:16tert-Amyl alcohol (TAA) 58.8ug/kg dry 1 GM58.8

ND 08/13/18 08/13/18 17:16tert-Amyl methyl ether (TAME) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Benzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Bromobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Bromochloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Bromodichloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Bromoform 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Bromomethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 17:16tert-Butanol (TBA) 58.8ug/kg dry 1 GM58.8

ND 08/13/18 08/13/18 17:162-Butanone (MEK) 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 17:16n-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16sec-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16tert-Butylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Carbon disulfide 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Carbon tetrachloride 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Chlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Chloroethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 17:16Chloroform 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Chloromethane 5.9ug/kg dry 1 GM5.9

ND 08/13/18 08/13/18 17:162-Chlorotoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:164-Chlorotoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2-Dibromo-3-chloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Dibromochloromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2-Dibromoethane (EDB) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Dibromomethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,3-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,4-Dichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Dichlorodifluoromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1-Dichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2-Dichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1-Dichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16cis-1,2-Dichloroethene 5.9ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 36 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-23'

8081012-09 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 17:16trans-1,2-Dichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Dichlorofluoromethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,3-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:162,2-Dichloropropane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16cis-1,3-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16trans-1,3-Dichloropropene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Diisopropyl ether (DIPE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Ethyl tert-butyl ether (ETBE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Ethylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Hexachlorobutadiene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:162-Hexanone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 17:16Isopropylbenzene (Cumene) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:164-Isopropyltoluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Methyl tert-butyl ether (MTBE) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:164-Methyl-2-pentanone 11.8ug/kg dry 1 GM11.8

ND 08/13/18 08/13/18 17:16Methylene chloride 23.5ug/kg dry 1 GM23.5

ND 08/13/18 08/13/18 17:16Naphthalene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16n-Propylbenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Styrene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1,1,2-Tetrachloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1,2,2-Tetrachloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Tetrachloroethene 5.9ug/kg dry 1 GM2.4

12.8 08/13/18 08/13/18 17:16Toluene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2,3-Trichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2,4-Trichlorobenzene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1,1-Trichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,1,2-Trichloroethane 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Trichloroethene 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:16Trichlorofluoromethane (Freon 11) 5.9ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,2,3-Trichloropropane 5.9ug/kg dry 1 GM2.4

2.5 08/13/18 08/13/18 17:161,2,4-Trimethylbenzene 5.9J ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 17:161,3,5-Trimethylbenzene 5.9ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 37 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-23'

8081012-09 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 17:16Vinyl chloride 5.9ug/kg dry 1 GM2.4

4.2 08/13/18 08/13/18 17:16o-Xylene 5.9J ug/kg dry 1 GM2.4

7.8 08/13/18 08/13/18 17:16m- & p-Xylenes 5.9ug/kg dry 1 GM2.4

08/13/18 08/13/18 17:1670-130 112 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 17:1675-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 17:1665-120 93 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/16/18 01:07Acenaphthene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Acenaphthylene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Benzo[a]anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Benzo[b]fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Benzo[k]fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Benzo[ghi]perylene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Benzo[a]pyrene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Chrysene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Dibenzo[a,h]anthracene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Fluoranthene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Fluorene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Indeno[1,2,3-cd]pyrene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:072-Methylnaphthalene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Naphthalene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Phenanthrene 294ug/kg dry 1 WB118

ND 08/13/18 08/16/18 01:07Pyrene 294ug/kg dry 1 WB118

08/13/18 08/16/18 01:0721-110 76 %Surrogate: 2-Fluorophenol

08/13/18 08/16/18 01:0710-110 82 %Surrogate: Phenol-d5

08/13/18 08/16/18 01:0735-114 74 %Surrogate: Nitrobenzene-d5

08/13/18 08/16/18 01:0710-123 82 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/16/18 01:0743-116 73 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/16/18 01:0733-141 93 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 38 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B3-23'

8081012-09 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 18:43Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 02:00Diesel-Range Organics 9.4mg/kg dry 1 SJA9.4

08/14/18 08/16/18 02:0070-130 96 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

85 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

84.6 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:13Arsenic 21.1mg/kg dry 2 RAS21.1

ND 08/13/18 08/20/18 11:13Barium 8.44mg/kg dry 2 RAS8.44

ND 08/13/18 08/20/18 11:13Cadmium 2.11mg/kg dry 2 RAS2.11

ND 08/13/18 08/20/18 16:56Chromium 6.33mg/kg dry 2 RAS6.33

ND 08/13/18 08/20/18 11:13Lead 0.0211mg/kg dry 2 RAS0.0211

ND 08/13/18 08/21/18 10:29Selenium 10.6mg/kg dry 2 RAS10.6

ND 08/13/18 08/20/18 16:56Silver 4.22mg/kg dry 2 RAS4.22

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:44Mercury 0.0844mg/kg dry 2 MAP0.0844

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 39 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-5'

8081012-10 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 17:40Acetone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 17:40tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 17:40tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Benzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 17:40tert-Butanol (TBA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 17:402-Butanone (MEK) 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 17:40n-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 17:40Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 17:402-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:404-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 40 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-5'

8081012-10 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 17:40trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:402,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:402-Hexanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 17:40Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:404-Isopropyltoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:404-Methyl-2-pentanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 17:40Methylene chloride 22.7ug/kg dry 1 GM22.7

ND 08/13/18 08/13/18 17:40Naphthalene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Tetrachloroethene 5.7ug/kg dry 1 GM2.3

3.0 08/13/18 08/13/18 17:40Toluene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:40Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,2,4-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 17:401,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 41 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-5'

8081012-10 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 17:40Vinyl chloride 5.7ug/kg dry 1 GM2.3

2.4 08/13/18 08/13/18 17:40o-Xylene 5.7J ug/kg dry 1 GM2.3

4.4 08/13/18 08/13/18 17:40m- & p-Xylenes 5.7J ug/kg dry 1 GM2.3

08/13/18 08/13/18 17:4070-130 114 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 17:4075-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 17:4065-120 94 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/16/18 01:51Acenaphthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Acenaphthylene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Benzo[a]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Benzo[b]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Benzo[k]fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Benzo[ghi]perylene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Benzo[a]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Chrysene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Dibenzo[a,h]anthracene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Fluoranthene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Fluorene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Indeno[1,2,3-cd]pyrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:512-Methylnaphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Naphthalene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Phenanthrene 284ug/kg dry 1 WB114

ND 08/13/18 08/16/18 01:51Pyrene 284ug/kg dry 1 WB114

08/13/18 08/16/18 01:5121-110 81 %Surrogate: 2-Fluorophenol

08/13/18 08/16/18 01:5110-110 82 %Surrogate: Phenol-d5

08/13/18 08/16/18 01:5135-114 74 %Surrogate: Nitrobenzene-d5

08/13/18 08/16/18 01:5110-123 84 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/16/18 01:5143-116 79 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/16/18 01:5133-141 98 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 42 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-5'

8081012-10 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 19:17Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 03:18Diesel-Range Organics 9.1mg/kg dry 1 SJA9.1

08/14/18 08/16/18 03:1870-130 90 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

88 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

86.5 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:14Arsenic 19.9mg/kg dry 2 RAS19.9

21.6 08/13/18 08/20/18 11:14Barium 7.97mg/kg dry 2 RAS7.97

ND 08/13/18 08/20/18 11:14Cadmium 1.99mg/kg dry 2 RAS1.99

12.0 08/13/18 08/20/18 16:58Chromium 5.98mg/kg dry 2 RAS5.98

10.0 08/13/18 08/20/18 11:14Lead 0.0199mg/kg dry 2 RAS0.0199

ND 08/13/18 08/21/18 10:30Selenium 9.96mg/kg dry 2 RAS9.96

ND 08/13/18 08/20/18 16:58Silver 3.99mg/kg dry 2 RAS3.99

Metals EPA 6020 Performed at Enviro-Chem

0.0974 08/13/18 08/20/18 14:47Mercury 0.0797mg/kg dry 2 MAP0.0797

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 43 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-10'

8081012-11 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 18:05Acetone 11.1ug/kg dry 1 GM11.1

ND 08/13/18 08/13/18 18:05tert-Amyl alcohol (TAA) 55.6ug/kg dry 1 GM55.6

ND 08/13/18 08/13/18 18:05tert-Amyl methyl ether (TAME) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Benzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Bromobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Bromochloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Bromodichloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Bromoform 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Bromomethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 18:05tert-Butanol (TBA) 55.6ug/kg dry 1 GM55.6

ND 08/13/18 08/13/18 18:052-Butanone (MEK) 11.1ug/kg dry 1 GM11.1

ND 08/13/18 08/13/18 18:05n-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05sec-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05tert-Butylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Carbon disulfide 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Carbon tetrachloride 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Chlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Chloroethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 18:05Chloroform 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Chloromethane 5.6ug/kg dry 1 GM5.6

ND 08/13/18 08/13/18 18:052-Chlorotoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:054-Chlorotoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2-Dibromo-3-chloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Dibromochloromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2-Dibromoethane (EDB) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Dibromomethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,3-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,4-Dichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Dichlorodifluoromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1-Dichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2-Dichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1-Dichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05cis-1,2-Dichloroethene 5.6ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 44 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-10'

8081012-11 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:05trans-1,2-Dichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Dichlorofluoromethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,3-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:052,2-Dichloropropane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05cis-1,3-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05trans-1,3-Dichloropropene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Diisopropyl ether (DIPE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Ethyl tert-butyl ether (ETBE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Ethylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Hexachlorobutadiene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:052-Hexanone 11.1ug/kg dry 1 GM11.1

ND 08/13/18 08/13/18 18:05Isopropylbenzene (Cumene) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:054-Isopropyltoluene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Methyl tert-butyl ether (MTBE) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:054-Methyl-2-pentanone 11.1ug/kg dry 1 GM11.1

ND 08/13/18 08/13/18 18:05Methylene chloride 22.2ug/kg dry 1 GM22.2

9.8 08/13/18 08/13/18 18:05Naphthalene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05n-Propylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Styrene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1,1,2-Tetrachloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1,2,2-Tetrachloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Tetrachloroethene 5.6ug/kg dry 1 GM2.2

4.7 08/13/18 08/13/18 18:05Toluene 5.6J ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2,3-Trichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2,4-Trichlorobenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1,1-Trichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,1,2-Trichloroethane 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Trichloroethene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:05Trichlorofluoromethane (Freon 11) 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,2,3-Trichloropropane 5.6ug/kg dry 1 GM2.2

8.0 08/13/18 08/13/18 18:051,2,4-Trimethylbenzene 5.6ug/kg dry 1 GM2.2

ND 08/13/18 08/13/18 18:051,3,5-Trimethylbenzene 5.6ug/kg dry 1 GM2.2

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 45 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-10'

8081012-11 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:05Vinyl chloride 5.6ug/kg dry 1 GM2.2

4.6 08/13/18 08/13/18 18:05o-Xylene 5.6J ug/kg dry 1 GM2.2

6.2 08/13/18 08/13/18 18:05m- & p-Xylenes 5.6ug/kg dry 1 GM2.2

08/13/18 08/13/18 18:0570-130 108 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 18:0575-120 90 %Surrogate: Toluene-d8

08/13/18 08/13/18 18:0565-120 94 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/16/18 02:34Acenaphthene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Acenaphthylene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Anthracene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Benzo[a]anthracene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Benzo[b]fluoranthene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Benzo[k]fluoranthene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Benzo[ghi]perylene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Benzo[a]pyrene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Chrysene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Dibenzo[a,h]anthracene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Fluoranthene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Fluorene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Indeno[1,2,3-cd]pyrene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:342-Methylnaphthalene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Naphthalene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Phenanthrene 278ug/kg dry 1 WB111

ND 08/13/18 08/16/18 02:34Pyrene 278ug/kg dry 1 WB111

08/13/18 08/16/18 02:3421-110 83 %Surrogate: 2-Fluorophenol

08/13/18 08/16/18 02:3410-110 84 %Surrogate: Phenol-d5

08/13/18 08/16/18 02:3435-114 76 %Surrogate: Nitrobenzene-d5

08/13/18 08/16/18 02:3410-123 89 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/16/18 02:3443-116 80 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/16/18 02:3433-141 96 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 46 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-10'

8081012-11 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

0.71 08/14/18 08/14/18 19:50Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 03:44Diesel-Range Organics 8.9mg/kg dry 1 SJA8.9

08/14/18 08/16/18 03:4470-130 87 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

90 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

88.5 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

19.7 08/13/18 08/20/18 11:16Arsenic 18.8mg/kg dry 2 RAS18.8

9.07 08/13/18 08/20/18 11:16Barium 7.53mg/kg dry 2 RAS7.53

ND 08/13/18 08/20/18 11:16Cadmium 1.88mg/kg dry 2 RAS1.88

11.3 08/13/18 08/20/18 17:00Chromium 5.65mg/kg dry 2 RAS5.65

4.37 08/13/18 08/20/18 11:16Lead 0.0188mg/kg dry 2 RAS0.0188

ND 08/13/18 08/21/18 10:32Selenium 9.41mg/kg dry 2 RAS9.41

ND 08/13/18 08/20/18 17:00Silver 3.77mg/kg dry 2 RAS3.77

Metals EPA 6020 Performed at Enviro-Chem

0.0962 08/13/18 08/20/18 14:50Mercury 0.0753mg/kg dry 2 MAP0.0753

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 47 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-23'

8081012-12 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 18:30Acetone 12.0ug/kg dry 1 GM12.0

ND 08/13/18 08/13/18 18:30tert-Amyl alcohol (TAA) 60.2ug/kg dry 1 GM60.2

ND 08/13/18 08/13/18 18:30tert-Amyl methyl ether (TAME) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Benzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Bromobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Bromochloromethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Bromodichloromethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Bromoform 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Bromomethane 6.0ug/kg dry 1 GM6.0

ND 08/13/18 08/13/18 18:30tert-Butanol (TBA) 60.2ug/kg dry 1 GM60.2

ND 08/13/18 08/13/18 18:302-Butanone (MEK) 12.0ug/kg dry 1 GM12.0

ND 08/13/18 08/13/18 18:30n-Butylbenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30sec-Butylbenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30tert-Butylbenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Carbon disulfide 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Carbon tetrachloride 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Chlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Chloroethane 6.0ug/kg dry 1 GM6.0

ND 08/13/18 08/13/18 18:30Chloroform 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Chloromethane 6.0ug/kg dry 1 GM6.0

ND 08/13/18 08/13/18 18:302-Chlorotoluene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:304-Chlorotoluene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2-Dibromo-3-chloropropane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Dibromochloromethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2-Dibromoethane (EDB) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Dibromomethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2-Dichlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,3-Dichlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,4-Dichlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Dichlorodifluoromethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1-Dichloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2-Dichloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1-Dichloroethene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30cis-1,2-Dichloroethene 6.0ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 48 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-23'

8081012-12 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:30trans-1,2-Dichloroethene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Dichlorofluoromethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2-Dichloropropane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,3-Dichloropropane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:302,2-Dichloropropane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1-Dichloropropene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30cis-1,3-Dichloropropene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30trans-1,3-Dichloropropene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Diisopropyl ether (DIPE) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Ethyl tert-butyl ether (ETBE) 6.0ug/kg dry 1 GM2.4

3.0 08/13/18 08/13/18 18:30Ethylbenzene 6.0J ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Hexachlorobutadiene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:302-Hexanone 12.0ug/kg dry 1 GM12.0

ND 08/13/18 08/13/18 18:30Isopropylbenzene (Cumene) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:304-Isopropyltoluene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Methyl tert-butyl ether (MTBE) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:304-Methyl-2-pentanone 12.0ug/kg dry 1 GM12.0

ND 08/13/18 08/13/18 18:30Methylene chloride 24.1ug/kg dry 1 GM24.1

3.6 08/13/18 08/13/18 18:30Naphthalene 6.0J ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30n-Propylbenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Styrene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1,1,2-Tetrachloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1,2,2-Tetrachloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Tetrachloroethene 6.0ug/kg dry 1 GM2.4

15.3 08/13/18 08/13/18 18:30Toluene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2,3-Trichlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2,4-Trichlorobenzene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1,1-Trichloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,1,2-Trichloroethane 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Trichloroethene 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:30Trichlorofluoromethane (Freon 11) 6.0ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,2,3-Trichloropropane 6.0ug/kg dry 1 GM2.4

6.0 08/13/18 08/13/18 18:301,2,4-Trimethylbenzene 6.0J ug/kg dry 1 GM2.4

ND 08/13/18 08/13/18 18:301,3,5-Trimethylbenzene 6.0ug/kg dry 1 GM2.4

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 49 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-23'

8081012-12 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:30Vinyl chloride 6.0ug/kg dry 1 GM2.4

7.7 08/13/18 08/13/18 18:30o-Xylene 6.0ug/kg dry 1 GM2.4

11.1 08/13/18 08/13/18 18:30m- & p-Xylenes 6.0ug/kg dry 1 GM2.4

08/13/18 08/13/18 18:3070-130 107 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 18:3075-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 18:3065-120 94 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 01:28Acenaphthene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Acenaphthylene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Anthracene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Benzo[a]anthracene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Benzo[b]fluoranthene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Benzo[k]fluoranthene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Benzo[ghi]perylene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Benzo[a]pyrene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Chrysene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Dibenzo[a,h]anthracene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Fluoranthene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Fluorene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Indeno[1,2,3-cd]pyrene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:282-Methylnaphthalene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Naphthalene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Phenanthrene 301ug/kg dry 1 WB120

ND 08/13/18 08/17/18 01:28Pyrene 301ug/kg dry 1 WB120

08/13/18 08/17/18 01:2821-110 77 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 01:2810-110 77 %Surrogate: Phenol-d5

08/13/18 08/17/18 01:2835-114 67 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 01:2810-123 81 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 01:2843-116 76 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 01:2833-141 89 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 50 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B4-23'

8081012-12 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

0.16 08/14/18 08/14/18 20:23Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 04:11Diesel-Range Organics 9.6mg/kg dry 1 SJA9.6

08/14/18 08/16/18 04:1170-130 89 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

83 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

83.5 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:18Arsenic 16.0mg/kg dry 2 RAS16.0

ND 08/13/18 08/20/18 11:18Barium 6.39mg/kg dry 2 RAS6.39

ND 08/13/18 08/20/18 11:18Cadmium 1.60mg/kg dry 2 RAS1.60

ND 08/13/18 08/20/18 17:03Chromium 4.79mg/kg dry 2 RAS4.79

5.75 08/13/18 08/20/18 11:18Lead 0.0160mg/kg dry 2 RAS0.0160

ND 08/13/18 08/21/18 10:34Selenium 7.99mg/kg dry 2 RAS7.99

ND 08/13/18 08/20/18 17:03Silver 3.19mg/kg dry 2 RAS3.19

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 14:53Mercury 0.0639mg/kg dry 2 MAP0.0639

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 51 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-5'

8081012-13 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 18:54Acetone 10.5ug/kg dry 1 GM10.5

ND 08/13/18 08/13/18 18:54tert-Amyl alcohol (TAA) 52.6ug/kg dry 1 GM52.6

ND 08/13/18 08/13/18 18:54tert-Amyl methyl ether (TAME) 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Benzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Bromobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Bromochloromethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Bromodichloromethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Bromoform 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Bromomethane 5.3ug/kg dry 1 GM5.3

ND 08/13/18 08/13/18 18:54tert-Butanol (TBA) 52.6ug/kg dry 1 GM52.6

ND 08/13/18 08/13/18 18:542-Butanone (MEK) 10.5ug/kg dry 1 GM10.5

ND 08/13/18 08/13/18 18:54n-Butylbenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54sec-Butylbenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54tert-Butylbenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Carbon disulfide 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Carbon tetrachloride 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Chlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Chloroethane 5.3ug/kg dry 1 GM5.3

ND 08/13/18 08/13/18 18:54Chloroform 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Chloromethane 5.3ug/kg dry 1 GM5.3

ND 08/13/18 08/13/18 18:542-Chlorotoluene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:544-Chlorotoluene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2-Dibromo-3-chloropropane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Dibromochloromethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2-Dibromoethane (EDB) 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Dibromomethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2-Dichlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,3-Dichlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,4-Dichlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Dichlorodifluoromethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1-Dichloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2-Dichloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1-Dichloroethene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54cis-1,2-Dichloroethene 5.3ug/kg dry 1 GM2.1

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 52 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-5'

8081012-13 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:54trans-1,2-Dichloroethene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Dichlorofluoromethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2-Dichloropropane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,3-Dichloropropane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:542,2-Dichloropropane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1-Dichloropropene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54cis-1,3-Dichloropropene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54trans-1,3-Dichloropropene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Diisopropyl ether (DIPE) 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Ethyl tert-butyl ether (ETBE) 5.3ug/kg dry 1 GM2.1

25.7 08/13/18 08/13/18 18:54Ethylbenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Hexachlorobutadiene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:542-Hexanone 10.5ug/kg dry 1 GM10.5

3.4 08/13/18 08/13/18 18:54Isopropylbenzene (Cumene) 5.3J ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:544-Isopropyltoluene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Methyl tert-butyl ether (MTBE) 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:544-Methyl-2-pentanone 10.5ug/kg dry 1 GM10.5

ND 08/13/18 08/13/18 18:54Methylene chloride 21.1ug/kg dry 1 GM21.1

13.6 08/13/18 08/13/18 18:54Naphthalene 5.3ug/kg dry 1 GM2.1

12.1 08/13/18 08/13/18 18:54n-Propylbenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Styrene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1,1,2-Tetrachloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1,2,2-Tetrachloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Tetrachloroethene 5.3ug/kg dry 1 GM2.1

18.5 08/13/18 08/13/18 18:54Toluene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2,3-Trichlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2,4-Trichlorobenzene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1,1-Trichloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,1,2-Trichloroethane 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Trichloroethene 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:54Trichlorofluoromethane (Freon 11) 5.3ug/kg dry 1 GM2.1

ND 08/13/18 08/13/18 18:541,2,3-Trichloropropane 5.3ug/kg dry 1 GM2.1

86.1 08/13/18 08/13/18 18:541,2,4-Trimethylbenzene 5.3ug/kg dry 1 GM2.1

21.2 08/13/18 08/13/18 18:541,3,5-Trimethylbenzene 5.3ug/kg dry 1 GM2.1

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 53 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-5'

8081012-13 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:54Vinyl chloride 5.3ug/kg dry 1 GM2.1

49.5 08/13/18 08/13/18 18:54o-Xylene 5.3ug/kg dry 1 GM2.1

119 08/13/18 08/13/18 18:54m- & p-Xylenes 5.3ug/kg dry 1 GM2.1

08/13/18 08/13/18 18:5470-130 108 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 18:5475-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 18:5465-120 101 %Surrogate: 4-Bromofluorobenzene

IS-FAILSEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 02:12Acenaphthene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Acenaphthylene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Anthracene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Benzo[a]anthracene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Benzo[b]fluoranthene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Benzo[k]fluoranthene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Benzo[ghi]perylene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Benzo[a]pyrene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Chrysene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Dibenzo[a,h]anthracene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Fluoranthene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Fluorene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Indeno[1,2,3-cd]pyrene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:122-Methylnaphthalene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Naphthalene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Phenanthrene 1050ug/kg dry 2 WB421

ND 08/13/18 08/17/18 02:12Pyrene 1050ug/kg dry 2 WB421

08/13/18 08/17/18 02:1221-110 60 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 02:1210-110 76 %Surrogate: Phenol-d5

08/13/18 08/17/18 02:1235-114 67 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 02:1210-123 19 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 02:1243-116 79 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 02:1233-141 100 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 54 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-5'

8081012-13 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

0.86 08/14/18 08/14/18 20:57Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

85.0 08/14/18 08/16/18 04:37Diesel-Range Organics 16.8mg/kg dry 1 SJA16.8

08/14/18 08/16/18 04:3770-130 111 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

95 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

92.0 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:25Arsenic 20.1mg/kg dry 2 RAS20.1

35.1 08/13/18 08/20/18 11:25Barium 8.05mg/kg dry 2 RAS8.05

ND 08/13/18 08/20/18 11:25Cadmium 2.01mg/kg dry 2 RAS2.01

12.1 08/13/18 08/20/18 17:05Chromium 6.04mg/kg dry 2 RAS6.04

109 08/13/18 08/20/18 11:25Lead 0.0201mg/kg dry 2 RAS0.0201

ND 08/13/18 08/21/18 10:39Selenium 10.1mg/kg dry 2 RAS10.1

ND 08/13/18 08/20/18 17:05Silver 4.03mg/kg dry 2 RAS4.03

Metals EPA 6020 Performed at Enviro-Chem

0.103 08/13/18 08/20/18 14:56Mercury 0.0805mg/kg dry 2 MAP0.0805

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 55 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-15'

8081012-14 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 19:19Acetone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 19:19tert-Amyl alcohol (TAA) 58.1ug/kg dry 1 GM58.1

ND 08/13/18 08/13/18 19:19tert-Amyl methyl ether (TAME) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Benzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Bromobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Bromochloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Bromodichloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Bromoform 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Bromomethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 19:19tert-Butanol (TBA) 58.1ug/kg dry 1 GM58.1

ND 08/13/18 08/13/18 19:192-Butanone (MEK) 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 19:19n-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19sec-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19tert-Butylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Carbon disulfide 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Carbon tetrachloride 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Chlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Chloroethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 19:19Chloroform 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Chloromethane 5.8ug/kg dry 1 GM5.8

ND 08/13/18 08/13/18 19:192-Chlorotoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:194-Chlorotoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2-Dibromo-3-chloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Dibromochloromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2-Dibromoethane (EDB) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Dibromomethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,3-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,4-Dichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Dichlorodifluoromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1-Dichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2-Dichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1-Dichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19cis-1,2-Dichloroethene 5.8ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 56 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-15'

8081012-14 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 19:19trans-1,2-Dichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Dichlorofluoromethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,3-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:192,2-Dichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19cis-1,3-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19trans-1,3-Dichloropropene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Diisopropyl ether (DIPE) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Ethyl tert-butyl ether (ETBE) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Ethylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Hexachlorobutadiene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:192-Hexanone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 19:19Isopropylbenzene (Cumene) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:194-Isopropyltoluene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Methyl tert-butyl ether (MTBE) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:194-Methyl-2-pentanone 11.6ug/kg dry 1 GM11.6

ND 08/13/18 08/13/18 19:19Methylene chloride 23.3ug/kg dry 1 GM23.3

ND 08/13/18 08/13/18 19:19Naphthalene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19n-Propylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Styrene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1,1,2-Tetrachloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1,2,2-Tetrachloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Tetrachloroethene 5.8ug/kg dry 1 GM2.3

2.7 08/13/18 08/13/18 19:19Toluene 5.8J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2,3-Trichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2,4-Trichlorobenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1,1-Trichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,1,2-Trichloroethane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Trichloroethene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19Trichlorofluoromethane (Freon 11) 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2,3-Trichloropropane 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,2,4-Trimethylbenzene 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:191,3,5-Trimethylbenzene 5.8ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 57 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-15'

8081012-14 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 19:19Vinyl chloride 5.8ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 19:19o-Xylene 5.8ug/kg dry 1 GM2.3

4.4 08/13/18 08/13/18 19:19m- & p-Xylenes 5.8J ug/kg dry 1 GM2.3

08/13/18 08/13/18 19:1970-130 108 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 19:1975-120 92 %Surrogate: Toluene-d8

08/13/18 08/13/18 19:1965-120 95 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 21:30Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 05:03Diesel-Range Organics 9.3mg/kg dry 1 SJA9.3

08/14/18 08/16/18 05:0370-130 91 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

86 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

84.0 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:31Arsenic 23.3mg/kg dry 2 RAS23.3

ND 08/13/18 08/20/18 11:31Barium 9.34mg/kg dry 2 RAS9.34

ND 08/13/18 08/20/18 11:31Cadmium 2.33mg/kg dry 2 RAS2.33

23.3 08/13/18 08/20/18 17:07Chromium 7.00mg/kg dry 2 RAS7.00

2.71 08/13/18 08/20/18 11:31Lead 0.0233mg/kg dry 2 RAS0.0233

ND 08/13/18 08/21/18 10:44Selenium 11.7mg/kg dry 2 RAS11.7

ND 08/13/18 08/20/18 17:07Silver 4.67mg/kg dry 2 RAS4.67

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 58 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-15'

8081012-14 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 15:05Mercury 0.0934mg/kg dry 2 MAP0.0934

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 59 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-15'

8081012-14RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 14:19Acenaphthene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Acenaphthylene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Anthracene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Benzo[a]anthracene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Benzo[b]fluoranthene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Benzo[k]fluoranthene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Benzo[ghi]perylene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Benzo[a]pyrene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Chrysene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Dibenzo[a,h]anthracene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Fluoranthene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Fluorene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Indeno[1,2,3-cd]pyrene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:192-Methylnaphthalene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Naphthalene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Phenanthrene 291ug/kg dry 1 WB116

ND 08/13/18 08/17/18 14:19Pyrene 291ug/kg dry 1 WB116

08/13/18 08/17/18 14:1921-110 81 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 14:1910-110 82 %Surrogate: Phenol-d5

08/13/18 08/17/18 14:1935-114 69 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 14:1910-123 85 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 14:1943-116 69 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 14:1933-141 94 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 60 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-27'

8081012-15 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 19:44Acetone 12.7ug/kg dry 1 GM12.7

ND 08/13/18 08/13/18 19:44tert-Amyl alcohol (TAA) 63.3ug/kg dry 1 GM63.3

ND 08/13/18 08/13/18 19:44tert-Amyl methyl ether (TAME) 6.3ug/kg dry 1 GM2.5

7.2 08/13/18 08/13/18 19:44Benzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Bromobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Bromochloromethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Bromodichloromethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Bromoform 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Bromomethane 6.3ug/kg dry 1 GM6.3

ND 08/13/18 08/13/18 19:44tert-Butanol (TBA) 63.3ug/kg dry 1 GM63.3

ND 08/13/18 08/13/18 19:442-Butanone (MEK) 12.7ug/kg dry 1 GM12.7

ND 08/13/18 08/13/18 19:44n-Butylbenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44sec-Butylbenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44tert-Butylbenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Carbon disulfide 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Carbon tetrachloride 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Chlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Chloroethane 6.3ug/kg dry 1 GM6.3

ND 08/13/18 08/13/18 19:44Chloroform 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Chloromethane 6.3ug/kg dry 1 GM6.3

ND 08/13/18 08/13/18 19:442-Chlorotoluene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:444-Chlorotoluene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2-Dibromo-3-chloropropane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Dibromochloromethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2-Dibromoethane (EDB) 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Dibromomethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2-Dichlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,3-Dichlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,4-Dichlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Dichlorodifluoromethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1-Dichloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2-Dichloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1-Dichloroethene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44cis-1,2-Dichloroethene 6.3ug/kg dry 1 GM2.5

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 61 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-27'

8081012-15 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 19:44trans-1,2-Dichloroethene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Dichlorofluoromethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2-Dichloropropane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,3-Dichloropropane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:442,2-Dichloropropane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1-Dichloropropene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44cis-1,3-Dichloropropene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44trans-1,3-Dichloropropene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Diisopropyl ether (DIPE) 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Ethyl tert-butyl ether (ETBE) 6.3ug/kg dry 1 GM2.5

4.9 08/13/18 08/13/18 19:44Ethylbenzene 6.3J ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Hexachlorobutadiene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:442-Hexanone 12.7ug/kg dry 1 GM12.7

ND 08/13/18 08/13/18 19:44Isopropylbenzene (Cumene) 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:444-Isopropyltoluene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Methyl tert-butyl ether (MTBE) 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:444-Methyl-2-pentanone 12.7ug/kg dry 1 GM12.7

ND 08/13/18 08/13/18 19:44Methylene chloride 25.3ug/kg dry 1 GM25.3

ND 08/13/18 08/13/18 19:44Naphthalene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44n-Propylbenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Styrene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1,1,2-Tetrachloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1,2,2-Tetrachloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Tetrachloroethene 6.3ug/kg dry 1 GM2.5

30.6 08/13/18 08/13/18 19:44Toluene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2,3-Trichlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2,4-Trichlorobenzene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1,1-Trichloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,1,2-Trichloroethane 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Trichloroethene 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:44Trichlorofluoromethane (Freon 11) 6.3ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,2,3-Trichloropropane 6.3ug/kg dry 1 GM2.5

4.3 08/13/18 08/13/18 19:441,2,4-Trimethylbenzene 6.3J ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 19:441,3,5-Trimethylbenzene 6.3ug/kg dry 1 GM2.5

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 62 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-27'

8081012-15 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 19:44Vinyl chloride 6.3ug/kg dry 1 GM2.5

8.7 08/13/18 08/13/18 19:44o-Xylene 6.3ug/kg dry 1 GM2.5

17.5 08/13/18 08/13/18 19:44m- & p-Xylenes 6.3ug/kg dry 1 GM2.5

08/13/18 08/13/18 19:4470-130 107 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 19:4475-120 92 %Surrogate: Toluene-d8

08/13/18 08/13/18 19:4465-120 95 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

ND 08/14/18 08/14/18 22:03Gasoline-Range Organics 0.13mg/kg dry 1 GM0.13

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 05:29Diesel-Range Organics 10.1mg/kg dry 1 SJA10.1

08/14/18 08/16/18 05:2970-130 90 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

79 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

78.4 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:33Arsenic 19.9mg/kg dry 2 RAS19.9

329 08/13/18 08/20/18 11:33Barium 7.97mg/kg dry 2 RAS7.97

ND 08/13/18 08/20/18 11:33Cadmium 1.99mg/kg dry 2 RAS1.99

23.9 08/13/18 08/20/18 17:09Chromium 5.98mg/kg dry 2 RAS5.98

68.2 08/13/18 08/20/18 11:33Lead 0.0199mg/kg dry 2 RAS0.0199

ND 08/13/18 08/21/18 10:45Selenium 9.97mg/kg dry 2 RAS9.97

ND 08/13/18 08/20/18 17:09Silver 3.99mg/kg dry 2 RAS3.99

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 63 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-27'

8081012-15 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 15:08Mercury 0.0797mg/kg dry 2 MAP0.0797

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 64 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5-27'

8081012-15RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 15:03Acenaphthene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Acenaphthylene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Anthracene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Benzo[a]anthracene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Benzo[b]fluoranthene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Benzo[k]fluoranthene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Benzo[ghi]perylene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Benzo[a]pyrene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Chrysene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Dibenzo[a,h]anthracene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Fluoranthene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Fluorene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Indeno[1,2,3-cd]pyrene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:032-Methylnaphthalene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Naphthalene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Phenanthrene 316ug/kg dry 1 WB127

ND 08/13/18 08/17/18 15:03Pyrene 316ug/kg dry 1 WB127

08/13/18 08/17/18 15:0321-110 75 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 15:0310-110 75 %Surrogate: Phenol-d5

08/13/18 08/17/18 15:0335-114 64 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 15:0310-123 71 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 15:0343-116 69 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 15:0333-141 95 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 65 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-5'

8081012-16 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 20:09Acetone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 20:09tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 20:09tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 GM2.3

2.3 08/13/18 08/13/18 20:09Benzene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Bromobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Bromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Bromodichloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Bromoform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Bromomethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 20:09tert-Butanol (TBA) 56.8ug/kg dry 1 GM56.8

ND 08/13/18 08/13/18 20:092-Butanone (MEK) 11.4ug/kg dry 1 GM11.4

4.0 08/13/18 08/13/18 20:09n-Butylbenzene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09sec-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09tert-Butylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Carbon disulfide 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Carbon tetrachloride 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Chlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Chloroethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 20:09Chloroform 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Chloromethane 5.7ug/kg dry 1 GM5.7

ND 08/13/18 08/13/18 20:092-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:094-Chlorotoluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Dibromochloromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2-Dibromoethane (EDB) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Dibromomethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,3-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,4-Dichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Dichlorodifluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2-Dichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09cis-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 66 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-5'

8081012-16 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 20:09trans-1,2-Dichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Dichlorofluoromethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,3-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:092,2-Dichloropropane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09cis-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09trans-1,3-Dichloropropene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Diisopropyl ether (DIPE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 GM2.3

118 08/13/18 08/13/18 20:09Ethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Hexachlorobutadiene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:092-Hexanone 11.4ug/kg dry 1 GM11.4

8.6 08/13/18 08/13/18 20:09Isopropylbenzene (Cumene) 5.7ug/kg dry 1 GM2.3

3.7 08/13/18 08/13/18 20:094-Isopropyltoluene 5.7J ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:094-Methyl-2-pentanone 11.4ug/kg dry 1 GM11.4

ND 08/13/18 08/13/18 20:09Methylene chloride 22.7ug/kg dry 1 GM22.7

18.3 08/13/18 08/13/18 20:09Naphthalene 5.7ug/kg dry 1 GM2.3

26.4 08/13/18 08/13/18 20:09n-Propylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Styrene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Tetrachloroethene 5.7ug/kg dry 1 GM2.3

223 08/13/18 08/13/18 20:09Toluene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2,3-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2,4-Trichlorobenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1,1-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,1,2-Trichloroethane 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Trichloroethene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:091,2,3-Trichloropropane 5.7ug/kg dry 1 GM2.3

187 08/13/18 08/13/18 20:091,2,4-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

45.5 08/13/18 08/13/18 20:091,3,5-Trimethylbenzene 5.7ug/kg dry 1 GM2.3

ND 08/13/18 08/13/18 20:09Vinyl chloride 5.7ug/kg dry 1 GM2.3

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 67 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-5'

8081012-16 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

222 08/13/18 08/13/18 20:09o-Xylene 5.7ug/kg dry 1 GM2.3

474 08/13/18 08/13/18 20:09m- & p-Xylenes 5.7E ug/kg dry 1 GM2.3

08/13/18 08/13/18 20:0970-130 108 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 20:0975-120 92 %Surrogate: Toluene-d8

08/13/18 08/13/18 20:0965-120 102 %Surrogate: 4-Bromofluorobenzene

IS-FAILSEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 04:24Acenaphthene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Acenaphthylene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Anthracene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Benzo[a]anthracene 1140ug/kg dry 2 WB455

516 08/13/18 08/17/18 04:24Benzo[b]fluoranthene 1140J ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Benzo[k]fluoranthene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Benzo[ghi]perylene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Benzo[a]pyrene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Chrysene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Dibenzo[a,h]anthracene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Fluoranthene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Fluorene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Indeno[1,2,3-cd]pyrene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:242-Methylnaphthalene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Naphthalene 1140ug/kg dry 2 WB455

ND 08/13/18 08/17/18 04:24Phenanthrene 1140ug/kg dry 2 WB455

491 08/13/18 08/17/18 04:24Pyrene 1140J ug/kg dry 2 WB455

08/13/18 08/17/18 04:2421-110 87 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 04:2410-110 89 %Surrogate: Phenol-d5

08/13/18 08/17/18 04:2435-114 78 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 04:2410-123 80 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 04:2443-116 90 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 04:2433-141 108 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 68 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-5'

8081012-16 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

4.24 08/14/18 08/14/18 22:37Gasoline-Range Organics 0.11mg/kg dry 1 GM0.11

DIESEL RANGE ORGANICS BY EPA 3540/8015C

95.8 08/14/18 08/16/18 05:55Diesel-Range Organics 18.2mg/kg dry 1 SJA18.2

08/14/18 08/16/18 05:5570-130 95 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

88 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

87.8 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:35Arsenic 19.0mg/kg dry 2 RAS19.0

21.5 08/13/18 08/20/18 11:35Barium 7.60mg/kg dry 2 RAS7.60

ND 08/13/18 08/20/18 11:35Cadmium 1.90mg/kg dry 2 RAS1.90

19.0 08/13/18 08/20/18 17:16Chromium 5.70mg/kg dry 2 RAS5.70

22.6 08/13/18 08/20/18 11:35Lead 0.0190mg/kg dry 2 RAS0.0190

ND 08/13/18 08/21/18 10:47Selenium 9.49mg/kg dry 2 RAS9.49

ND 08/13/18 08/20/18 17:16Silver 3.80mg/kg dry 2 RAS3.80

Metals EPA 6020 Performed at Enviro-Chem

0.703 08/13/18 08/20/18 15:11Mercury 0.0760mg/kg dry 2 MAP0.0760

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 69 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-10'

8081012-17 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 20:33Acetone 12.3ug/kg dry 1 GM12.3

ND 08/13/18 08/13/18 20:33tert-Amyl alcohol (TAA) 61.7ug/kg dry 1 GM61.7

ND 08/13/18 08/13/18 20:33tert-Amyl methyl ether (TAME) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Benzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Bromobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Bromochloromethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Bromodichloromethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Bromoform 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Bromomethane 6.2ug/kg dry 1 GM6.2

ND 08/13/18 08/13/18 20:33tert-Butanol (TBA) 61.7ug/kg dry 1 GM61.7

ND 08/13/18 08/13/18 20:332-Butanone (MEK) 12.3ug/kg dry 1 GM12.3

ND 08/13/18 08/13/18 20:33n-Butylbenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33sec-Butylbenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33tert-Butylbenzene 6.2ug/kg dry 1 GM2.5

2.6 08/13/18 08/13/18 20:33Carbon disulfide 6.2J ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Carbon tetrachloride 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Chlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Chloroethane 6.2ug/kg dry 1 GM6.2

ND 08/13/18 08/13/18 20:33Chloroform 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Chloromethane 6.2ug/kg dry 1 GM6.2

ND 08/13/18 08/13/18 20:332-Chlorotoluene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:334-Chlorotoluene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2-Dibromo-3-chloropropane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Dibromochloromethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2-Dibromoethane (EDB) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Dibromomethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2-Dichlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,3-Dichlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,4-Dichlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Dichlorodifluoromethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1-Dichloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2-Dichloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1-Dichloroethene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33cis-1,2-Dichloroethene 6.2ug/kg dry 1 GM2.5

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 70 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-10'

8081012-17 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 20:33trans-1,2-Dichloroethene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Dichlorofluoromethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2-Dichloropropane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,3-Dichloropropane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:332,2-Dichloropropane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1-Dichloropropene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33cis-1,3-Dichloropropene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33trans-1,3-Dichloropropene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Diisopropyl ether (DIPE) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Ethyl tert-butyl ether (ETBE) 6.2ug/kg dry 1 GM2.5

7.6 08/13/18 08/13/18 20:33Ethylbenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Hexachlorobutadiene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:332-Hexanone 12.3ug/kg dry 1 GM12.3

ND 08/13/18 08/13/18 20:33Isopropylbenzene (Cumene) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:334-Isopropyltoluene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Methyl tert-butyl ether (MTBE) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:334-Methyl-2-pentanone 12.3ug/kg dry 1 GM12.3

ND 08/13/18 08/13/18 20:33Methylene chloride 24.7ug/kg dry 1 GM24.7

18.2 08/13/18 08/13/18 20:33Naphthalene 6.2ug/kg dry 1 GM2.5

3.8 08/13/18 08/13/18 20:33n-Propylbenzene 6.2J ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Styrene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1,1,2-Tetrachloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1,2,2-Tetrachloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Tetrachloroethene 6.2ug/kg dry 1 GM2.5

18.1 08/13/18 08/13/18 20:33Toluene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2,3-Trichlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2,4-Trichlorobenzene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1,1-Trichloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,1,2-Trichloroethane 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Trichloroethene 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:33Trichlorofluoromethane (Freon 11) 6.2ug/kg dry 1 GM2.5

ND 08/13/18 08/13/18 20:331,2,3-Trichloropropane 6.2ug/kg dry 1 GM2.5

43.1 08/13/18 08/13/18 20:331,2,4-Trimethylbenzene 6.2ug/kg dry 1 GM2.5

9.5 08/13/18 08/13/18 20:331,3,5-Trimethylbenzene 6.2ug/kg dry 1 GM2.5

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 71 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-10'

8081012-17 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 20:33Vinyl chloride 6.2ug/kg dry 1 GM2.5

20.1 08/13/18 08/13/18 20:33o-Xylene 6.2ug/kg dry 1 GM2.5

32.6 08/13/18 08/13/18 20:33m- & p-Xylenes 6.2ug/kg dry 1 GM2.5

08/13/18 08/13/18 20:3370-130 106 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 20:3375-120 91 %Surrogate: Toluene-d8

08/13/18 08/13/18 20:3365-120 98 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 09:10Acenaphthene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Acenaphthylene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Anthracene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Benzo[a]anthracene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Benzo[b]fluoranthene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Benzo[k]fluoranthene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Benzo[ghi]perylene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Benzo[a]pyrene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Chrysene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Dibenzo[a,h]anthracene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Fluoranthene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Fluorene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Indeno[1,2,3-cd]pyrene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:102-Methylnaphthalene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Naphthalene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Phenanthrene 309ug/kg dry 1 WB123

ND 08/13/18 08/17/18 09:10Pyrene 309ug/kg dry 1 WB123

08/13/18 08/17/18 09:1021-110 68 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 09:1010-110 71 %Surrogate: Phenol-d5

08/13/18 08/17/18 09:1035-114 64 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 09:1010-123 72 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 09:1043-116 72 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 09:1033-141 97 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 72 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-10'

8081012-17 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

0.27 08/14/18 08/14/18 23:10Gasoline-Range Organics 0.12mg/kg dry 1 GM0.12

DIESEL RANGE ORGANICS BY EPA 3540/8015C

ND 08/14/18 08/16/18 06:21Diesel-Range Organics 9.9mg/kg dry 1 SJA9.9

08/14/18 08/16/18 06:2170-130 102 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

81 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

88.2 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:36Arsenic 19.9mg/kg dry 2 RAS19.9

25.0 08/13/18 08/20/18 11:36Barium 7.96mg/kg dry 2 RAS7.96

ND 08/13/18 08/20/18 11:36Cadmium 1.99mg/kg dry 2 RAS1.99

19.9 08/13/18 08/20/18 17:18Chromium 5.97mg/kg dry 2 RAS5.97

29.8 08/13/18 08/20/18 11:36Lead 0.0199mg/kg dry 2 RAS0.0199

ND 08/13/18 08/21/18 10:49Selenium 9.94mg/kg dry 2 RAS9.94

ND 08/13/18 08/20/18 17:18Silver 3.98mg/kg dry 2 RAS3.98

Metals EPA 6020 Performed at Enviro-Chem

1.01 08/13/18 08/20/18 15:14Mercury 0.0796mg/kg dry 2 MAP0.0796

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 73 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-20'

8081012-18 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 5030/8015C

819 08/14/18 08/14/18 18:18Gasoline-Range Organics 15.2mg/kg dry 125 GM15.2

DIESEL RANGE ORGANICS BY EPA 3540/8015C

106 08/14/18 08/16/18 06:47Diesel-Range Organics 9.8mg/kg dry 1 SJA9.8

08/14/18 08/16/18 06:4770-130 98 %Surrogate: o-Terphenyl

PERCENT SOLIDS BY ASTM D2216-05

82 08/14/18 08/15/18 09:57Percent Solids % 1 KD

Wet Chemistry Performed at Enviro-Chem

79.7 08/13/18 08/13/18 13:14% Solids 1.00% 1 FRD1.00

Metals by EPA 6010C Performed at Enviro-Chem

ND 08/13/18 08/20/18 11:38Arsenic 18.5mg/kg dry 2 RAS18.5

ND 08/13/18 08/20/18 11:38Barium 7.38mg/kg dry 2 RAS7.38

ND 08/13/18 08/20/18 11:38Cadmium 1.85mg/kg dry 2 RAS1.85

ND 08/13/18 08/20/18 17:21Chromium 5.54mg/kg dry 2 RAS5.54

9.82 08/13/18 08/20/18 11:38Lead 0.0185mg/kg dry 2 RAS0.0185

ND 08/13/18 08/21/18 10:50Selenium 9.23mg/kg dry 2 RAS9.23

ND 08/13/18 08/20/18 17:21Silver 3.69mg/kg dry 2 RAS3.69

Metals EPA 6020 Performed at Enviro-Chem

ND 08/13/18 08/20/18 15:17Mercury 0.0738mg/kg dry 2 MAP0.0738

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 74 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-20'

8081012-18RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/14/18 08/14/18 22:21Acetone 3050ug/kg dry 250 GM3050

ND 08/14/18 08/14/18 22:21tert-Amyl alcohol (TAA) 15200ug/kg dry 250 GM15200

ND 08/14/18 08/14/18 22:21tert-Amyl methyl ether (TAME) 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Benzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Bromobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Bromochloromethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Bromodichloromethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Bromoform 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Bromomethane 1520ug/kg dry 250 GM1520

ND 08/14/18 08/14/18 22:21tert-Butanol (TBA) 15200ug/kg dry 250 GM15200

ND 08/14/18 08/14/18 22:212-Butanone (MEK) 3050ug/kg dry 250 GM3050

17600 08/14/18 08/14/18 22:21n-Butylbenzene 1520ug/kg dry 250 GM610

3860 08/14/18 08/14/18 22:21sec-Butylbenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21tert-Butylbenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Carbon disulfide 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Carbon tetrachloride 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Chlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Chloroethane 1520ug/kg dry 250 GM1520

ND 08/14/18 08/14/18 22:21Chloroform 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Chloromethane 1520ug/kg dry 250 GM1520

ND 08/14/18 08/14/18 22:212-Chlorotoluene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:214-Chlorotoluene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2-Dibromo-3-chloropropane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Dibromochloromethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2-Dibromoethane (EDB) 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Dibromomethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2-Dichlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,3-Dichlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,4-Dichlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Dichlorodifluoromethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1-Dichloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2-Dichloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1-Dichloroethene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21cis-1,2-Dichloroethene 1520ug/kg dry 250 GM610

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 75 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-20'

8081012-18RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/14/18 08/14/18 22:21trans-1,2-Dichloroethene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Dichlorofluoromethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2-Dichloropropane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,3-Dichloropropane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:212,2-Dichloropropane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1-Dichloropropene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21cis-1,3-Dichloropropene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21trans-1,3-Dichloropropene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Diisopropyl ether (DIPE) 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Ethyl tert-butyl ether (ETBE) 1520ug/kg dry 250 GM610

27300 08/14/18 08/14/18 22:21Ethylbenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Hexachlorobutadiene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:212-Hexanone 3050ug/kg dry 250 GM3050

6960 08/14/18 08/14/18 22:21Isopropylbenzene (Cumene) 1520ug/kg dry 250 GM610

7760 08/14/18 08/14/18 22:214-Isopropyltoluene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Methyl tert-butyl ether (MTBE) 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:214-Methyl-2-pentanone 3050ug/kg dry 250 GM3050

ND 08/14/18 08/14/18 22:21Methylene chloride 6100ug/kg dry 250 GM6100

31200 08/14/18 08/14/18 22:21Naphthalene 1520ug/kg dry 250 GM610

26500 08/14/18 08/14/18 22:21n-Propylbenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Styrene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1,1,2-Tetrachloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1,2,2-Tetrachloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Tetrachloroethene 1520ug/kg dry 250 GM610

14300 08/14/18 08/14/18 22:21Toluene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2,3-Trichlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2,4-Trichlorobenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1,1-Trichloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,1,2-Trichloroethane 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Trichloroethene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Trichlorofluoromethane (Freon 11) 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:211,2,3-Trichloropropane 1520ug/kg dry 250 GM610

175000 08/14/18 08/14/18 22:211,2,4-Trimethylbenzene 1520E ug/kg dry 250 GM610

50300 08/14/18 08/14/18 22:211,3,5-Trimethylbenzene 1520ug/kg dry 250 GM610

ND 08/14/18 08/14/18 22:21Vinyl chloride 1520ug/kg dry 250 GM610

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 76 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6-20'

8081012-18RE1 (Soil)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

54800 08/14/18 08/14/18 22:21o-Xylene 1520ug/kg dry 250 GM610

119000 08/14/18 08/14/18 22:21m- & p-Xylenes 1520ug/kg dry 250 GM610

08/14/18 08/14/18 22:2170-130 87 %Surrogate: 1,2-Dichloroethane-d4

08/14/18 08/14/18 22:2175-120 95 %Surrogate: Toluene-d8

08/14/18 08/14/18 22:2165-120 104 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/13/18 08/17/18 15:47Acenaphthene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Acenaphthylene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Anthracene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Benzo[a]anthracene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Benzo[b]fluoranthene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Benzo[k]fluoranthene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Benzo[ghi]perylene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Benzo[a]pyrene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Chrysene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Dibenzo[a,h]anthracene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Fluoranthene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Fluorene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Indeno[1,2,3-cd]pyrene 1220ug/kg dry 4 WB488

9690 08/13/18 08/17/18 15:472-Methylnaphthalene 1220ug/kg dry 4 WB488

8650 08/13/18 08/17/18 15:47Naphthalene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Phenanthrene 1220ug/kg dry 4 WB488

ND 08/13/18 08/17/18 15:47Pyrene 1220ug/kg dry 4 WB488

08/13/18 08/17/18 15:4721-110 74 %Surrogate: 2-Fluorophenol

08/13/18 08/17/18 15:4710-110 76 %Surrogate: Phenol-d5

08/13/18 08/17/18 15:4735-114 67 %Surrogate: Nitrobenzene-d5

08/13/18 08/17/18 15:4710-123 59 %Surrogate: 2,4,6-Tribromophenol

08/13/18 08/17/18 15:4743-116 78 %Surrogate: 2-Fluorobiphenyl

08/13/18 08/17/18 15:4733-141 104 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 77 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2

8081012-19 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 18:02Acetone 20.0ug/L 2 GM20.0

ND 08/13/18 08/13/18 18:02tert-Amyl alcohol (TAA) 40.0ug/L 2 GM40.0

ND 08/13/18 08/13/18 18:02tert-Amyl methyl ether (TAME) 10.0ug/L 2 GM4.0

9.8 08/13/18 08/13/18 18:02Benzene 10.0J ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Bromobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Bromochloromethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Bromodichloromethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Bromoform 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Bromomethane 10.0ug/L 2 GM10.0

ND 08/13/18 08/13/18 18:02tert-Butanol (TBA) 30.0ug/L 2 GM30.0

ND 08/13/18 08/13/18 18:022-Butanone (MEK) 20.0ug/L 2 GM20.0

ND 08/13/18 08/13/18 18:02n-Butylbenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02sec-Butylbenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02tert-Butylbenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Carbon disulfide 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Carbon tetrachloride 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Chlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Chloroethane 10.0ug/L 2 GM10.0

ND 08/13/18 08/13/18 18:02Chloroform 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Chloromethane 10.0ug/L 2 GM10.0

ND 08/13/18 08/13/18 18:022-Chlorotoluene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:024-Chlorotoluene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Dibromochloromethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2-Dibromo-3-chloropropane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2-Dibromoethane (EDB) 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Dibromomethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2-Dichlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,3-Dichlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,4-Dichlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Dichlorodifluoromethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1-Dichloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2-Dichloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1-Dichloroethene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02cis-1,2-Dichloroethene 10.0ug/L 2 GM4.0

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 78 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2

8081012-19 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:02trans-1,2-Dichloroethene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Dichlorofluoromethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2-Dichloropropane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,3-Dichloropropane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:022,2-Dichloropropane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1-Dichloropropene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02cis-1,3-Dichloropropene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02trans-1,3-Dichloropropene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Diisopropyl ether (DIPE) 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Ethyl tert-butyl ether (ETBE) 10.0ug/L 2 GM4.0

44.9 08/13/18 08/13/18 18:02Ethylbenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Hexachlorobutadiene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:022-Hexanone 20.0ug/L 2 GM20.0

ND 08/13/18 08/13/18 18:02Isopropylbenzene (Cumene) 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:024-Isopropyltoluene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Methyl tert-butyl ether (MTBE) 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:024-Methyl-2-pentanone 20.0ug/L 2 GM20.0

ND 08/13/18 08/13/18 18:02Methylene chloride 20.0ug/L 2 GM20.0

12.7 08/13/18 08/13/18 18:02Naphthalene 10.0ug/L 2 GM4.0

6.7 08/13/18 08/13/18 18:02n-Propylbenzene 10.0J ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Styrene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1,1,2-Tetrachloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1,2,2-Tetrachloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Tetrachloroethene 10.0ug/L 2 GM4.0

188 08/13/18 08/13/18 18:02Toluene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2,3-Trichlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2,4-Trichlorobenzene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1,1-Trichloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,1,2-Trichloroethane 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Trichloroethene 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:02Trichlorofluoromethane (Freon 11) 10.0ug/L 2 GM4.0

ND 08/13/18 08/13/18 18:021,2,3-Trichloropropane 10.0ug/L 2 GM4.0

19.0 08/13/18 08/13/18 18:021,2,4-Trimethylbenzene 10.0ug/L 2 GM4.0

4.5 08/13/18 08/13/18 18:021,3,5-Trimethylbenzene 10.0J ug/L 2 GM4.0

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 79 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2

8081012-19 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:02Vinyl chloride 10.0ug/L 2 GM4.0

54.0 08/13/18 08/13/18 18:02o-Xylene 10.0ug/L 2 GM4.0

108 08/13/18 08/13/18 18:02m- & p-Xylenes 10.0ug/L 2 GM4.0

08/13/18 08/13/18 18:0275-120 96 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 18:0284-110 96 %Surrogate: Toluene-d8

08/13/18 08/13/18 18:0278-110 93 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/15/18 08/17/18 17:58Acenaphthene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Acenaphthylene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Anthracene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Benzo[a]anthracene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Benzo[b]fluoranthene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Benzo[k]fluoranthene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Benzo[ghi]perylene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Benzo[a]pyrene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Chrysene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Dibenzo[a,h]anthracene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Fluoranthene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Fluorene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Indeno[1,2,3-cd]pyrene 6.80ug/L 1 WB2.72

8.52 08/15/18 08/17/18 17:582-Methylnaphthalene 6.80ug/L 1 WB2.72

22.7 08/15/18 08/17/18 17:58Naphthalene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Phenanthrene 6.80ug/L 1 WB2.72

ND 08/15/18 08/17/18 17:58Pyrene 6.80ug/L 1 WB2.72

08/15/18 08/17/18 17:5821-110 57 %Surrogate: 2-Fluorophenol

08/15/18 08/17/18 17:5810-110 37 %Surrogate: Phenol-d5

08/15/18 08/17/18 17:5835-114 66 %Surrogate: Nitrobenzene-d5

08/15/18 08/17/18 17:5810-123 82 %Surrogate: 2,4,6-Tribromophenol

08/15/18 08/17/18 17:5843-116 77 %Surrogate: 2-Fluorobiphenyl

08/15/18 08/17/18 17:5833-141 94 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 80 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B2

8081012-19 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 8015C

1350 08/13/18 08/13/18 16:50Gasoline-Range Organics 100ug/L 1 GM100

DIESEL RANGE ORGANICS BY EPA 3510/8015C

ND 08/13/18 08/14/18 14:20Diesel-Range Organics 0.63mg/L 1 SJA0.63

08/13/18 08/14/18 14:2060-120 72 %Surrogate: o-Terphenyl

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 81 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5

8081012-20 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/13/18 08/13/18 18:25Acetone 100ug/L 10 GM100

270 08/13/18 08/13/18 18:25tert-Amyl alcohol (TAA) 200ug/L 10 GM200

ND 08/13/18 08/13/18 18:25tert-Amyl methyl ether (TAME) 50.0ug/L 10 GM20.0

1400 08/13/18 08/13/18 18:25Benzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Bromobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Bromochloromethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Bromodichloromethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Bromoform 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Bromomethane 50.0ug/L 10 GM50.0

ND 08/13/18 08/13/18 18:25tert-Butanol (TBA) 150ug/L 10 GM150

ND 08/13/18 08/13/18 18:252-Butanone (MEK) 100ug/L 10 GM100

ND 08/13/18 08/13/18 18:25n-Butylbenzene 50.0ug/L 10 GM20.0

61.3 08/13/18 08/13/18 18:25sec-Butylbenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25tert-Butylbenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Carbon disulfide 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Carbon tetrachloride 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Chlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Chloroethane 50.0ug/L 10 GM50.0

ND 08/13/18 08/13/18 18:25Chloroform 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Chloromethane 50.0ug/L 10 GM50.0

ND 08/13/18 08/13/18 18:252-Chlorotoluene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:254-Chlorotoluene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Dibromochloromethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2-Dibromo-3-chloropropane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2-Dibromoethane (EDB) 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Dibromomethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2-Dichlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,3-Dichlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,4-Dichlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Dichlorodifluoromethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1-Dichloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2-Dichloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1-Dichloroethene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25cis-1,2-Dichloroethene 50.0ug/L 10 GM20.0

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 82 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5

8081012-20 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:25trans-1,2-Dichloroethene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Dichlorofluoromethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2-Dichloropropane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,3-Dichloropropane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:252,2-Dichloropropane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1-Dichloropropene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25cis-1,3-Dichloropropene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25trans-1,3-Dichloropropene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Diisopropyl ether (DIPE) 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Ethyl tert-butyl ether (ETBE) 50.0ug/L 10 GM20.0

104 08/13/18 08/13/18 18:25Ethylbenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Hexachlorobutadiene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:252-Hexanone 100ug/L 10 GM100

76.6 08/13/18 08/13/18 18:25Isopropylbenzene (Cumene) 50.0ug/L 10 GM20.0

122 08/13/18 08/13/18 18:254-Isopropyltoluene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Methyl tert-butyl ether (MTBE) 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:254-Methyl-2-pentanone 100ug/L 10 GM100

ND 08/13/18 08/13/18 18:25Methylene chloride 100ug/L 10 GM100

ND 08/13/18 08/13/18 18:25Naphthalene 50.0ug/L 10 GM20.0

450 08/13/18 08/13/18 18:25n-Propylbenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Styrene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1,1,2-Tetrachloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1,2,2-Tetrachloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Tetrachloroethene 50.0ug/L 10 GM20.0

1580 08/13/18 08/13/18 18:25Toluene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2,3-Trichlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2,4-Trichlorobenzene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1,1-Trichloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,1,2-Trichloroethane 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Trichloroethene 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:25Trichlorofluoromethane (Freon 11) 50.0ug/L 10 GM20.0

ND 08/13/18 08/13/18 18:251,2,3-Trichloropropane 50.0ug/L 10 GM20.0

1200 08/13/18 08/13/18 18:251,2,4-Trimethylbenzene 50.0ug/L 10 GM20.0

585 08/13/18 08/13/18 18:251,3,5-Trimethylbenzene 50.0ug/L 10 GM20.0

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 83 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5

8081012-20 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/13/18 08/13/18 18:25Vinyl chloride 50.0ug/L 10 GM20.0

118 08/13/18 08/13/18 18:25o-Xylene 50.0ug/L 10 GM20.0

247 08/13/18 08/13/18 18:25m- & p-Xylenes 50.0ug/L 10 GM20.0

08/13/18 08/13/18 18:2575-120 101 %Surrogate: 1,2-Dichloroethane-d4

08/13/18 08/13/18 18:2584-110 98 %Surrogate: Toluene-d8

08/13/18 08/13/18 18:2578-110 96 %Surrogate: 4-Bromofluorobenzene

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/15/18 08/17/18 18:42Acenaphthene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Acenaphthylene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Anthracene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Benzo[a]anthracene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Benzo[b]fluoranthene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Benzo[k]fluoranthene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Benzo[ghi]perylene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Benzo[a]pyrene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Chrysene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Dibenzo[a,h]anthracene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Fluoranthene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Fluorene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Indeno[1,2,3-cd]pyrene 4.69ug/L 1 WB1.88

100 08/15/18 08/17/18 18:422-Methylnaphthalene 4.69ug/L 1 WB1.88

6.05 08/15/18 08/17/18 18:42Naphthalene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Phenanthrene 4.69ug/L 1 WB1.88

ND 08/15/18 08/17/18 18:42Pyrene 4.69ug/L 1 WB1.88

08/15/18 08/17/18 18:4221-110 27 %Surrogate: 2-Fluorophenol

08/15/18 08/17/18 18:4210-110 17 %Surrogate: Phenol-d5

08/15/18 08/17/18 18:4235-114 43 %Surrogate: Nitrobenzene-d5

08/15/18 08/17/18 18:4210-123 72 %Surrogate: 2,4,6-Tribromophenol

08/15/18 08/17/18 18:4243-116 57 %Surrogate: 2-Fluorobiphenyl

08/15/18 08/17/18 18:4233-141 86 %Surrogate: Terphenyl-d14

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 84 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5

8081012-20 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

DIESEL RANGE ORGANICS BY EPA 3510/8015C

7.04 08/13/18 08/14/18 15:04Diesel-Range Organics 0.19mg/L 1 SJA0.19

08/13/18 08/14/18 15:0460-120 77 %Surrogate: o-Terphenyl

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 85 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B5

8081012-20RE1 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

GASOLINE RANGE ORGANICS BY EPA 8015C

39800 08/15/18 08/15/18 16:42Gasoline-Range Organics 1000ug/L 10 GM1000

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 86 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6

8081012-21 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

SEMIVOLATILE ORGANICS BY EPA METHOD 8270D (GC/MS)

ND 08/15/18 08/20/18 12:37Acenaphthene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Acenaphthylene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Anthracene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Benzo[a]anthracene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Benzo[b]fluoranthene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Benzo[k]fluoranthene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Benzo[ghi]perylene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Benzo[a]pyrene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Chrysene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Dibenzo[a,h]anthracene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Fluoranthene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Fluorene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Indeno[1,2,3-cd]pyrene 47.6ug/L 10 WB19.0

464 08/15/18 08/20/18 12:372-Methylnaphthalene 47.6ug/L 10 WB19.0

880 08/15/18 08/20/18 12:37Naphthalene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Phenanthrene 47.6ug/L 10 WB19.0

ND 08/15/18 08/20/18 12:37Pyrene 47.6ug/L 10 WB19.0

08/15/18 08/20/18 12:3721-110 37 %Surrogate: 2-Fluorophenol

08/15/18 08/20/18 12:3710-110 29 %Surrogate: Phenol-d5

08/15/18 08/20/18 12:3735-114 72 %Surrogate: Nitrobenzene-d5

08/15/18 08/20/18 12:3710-123 78 %Surrogate: 2,4,6-Tribromophenol

08/15/18 08/20/18 12:3743-116 83 %Surrogate: 2-Fluorobiphenyl

08/15/18 08/20/18 12:3733-141 92 %Surrogate: Terphenyl-d14

DIESEL RANGE ORGANICS BY EPA 3510/8015C

87.7 08/13/18 08/14/18 15:31Diesel-Range Organics 0.93mg/L 5 SJA0.93

08/13/18 08/14/18 15:3160-120 74 %Surrogate: o-Terphenyl

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 87 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6

8081012-21RE1 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 08/14/18 08/14/18 13:59Acetone 1000ug/L 100 GM1000

ND 08/14/18 08/14/18 13:59tert-Amyl alcohol (TAA) 2000ug/L 100 GM2000

ND 08/14/18 08/14/18 13:59tert-Amyl methyl ether (TAME) 500ug/L 100 GM200

927 08/14/18 08/14/18 13:59Benzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Bromobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Bromochloromethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Bromodichloromethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Bromoform 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Bromomethane 500ug/L 100 GM500

ND 08/14/18 08/14/18 13:59tert-Butanol (TBA) 1500ug/L 100 GM1500

ND 08/14/18 08/14/18 13:592-Butanone (MEK) 1000ug/L 100 GM1000

ND 08/14/18 08/14/18 13:59n-Butylbenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59sec-Butylbenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59tert-Butylbenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Carbon disulfide 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Carbon tetrachloride 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Chlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Chloroethane 500ug/L 100 GM500

ND 08/14/18 08/14/18 13:59Chloroform 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Chloromethane 500ug/L 100 GM500

ND 08/14/18 08/14/18 13:592-Chlorotoluene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:594-Chlorotoluene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Dibromochloromethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2-Dibromo-3-chloropropane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2-Dibromoethane (EDB) 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Dibromomethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2-Dichlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,3-Dichlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,4-Dichlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Dichlorodifluoromethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1-Dichloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2-Dichloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1-Dichloroethene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59cis-1,2-Dichloroethene 500ug/L 100 GM200

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 88 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6

8081012-21RE1 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/14/18 08/14/18 13:59trans-1,2-Dichloroethene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Dichlorofluoromethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2-Dichloropropane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,3-Dichloropropane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:592,2-Dichloropropane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1-Dichloropropene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59cis-1,3-Dichloropropene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59trans-1,3-Dichloropropene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Diisopropyl ether (DIPE) 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Ethyl tert-butyl ether (ETBE) 500ug/L 100 GM200

3540 08/14/18 08/14/18 13:59Ethylbenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Hexachlorobutadiene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:592-Hexanone 1000ug/L 100 GM1000

ND 08/14/18 08/14/18 13:59Isopropylbenzene (Cumene) 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:594-Isopropyltoluene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Methyl tert-butyl ether (MTBE) 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:594-Methyl-2-pentanone 1000ug/L 100 GM1000

ND 08/14/18 08/14/18 13:59Methylene chloride 1000ug/L 100 GM1000

614 08/14/18 08/14/18 13:59Naphthalene 500ug/L 100 GM200

489 08/14/18 08/14/18 13:59n-Propylbenzene 500J ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Styrene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1,1,2-Tetrachloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1,2,2-Tetrachloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Tetrachloroethene 500ug/L 100 GM200

11600 08/14/18 08/14/18 13:59Toluene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2,3-Trichlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2,4-Trichlorobenzene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1,1-Trichloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,1,2-Trichloroethane 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Trichloroethene 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:59Trichlorofluoromethane (Freon 11) 500ug/L 100 GM200

ND 08/14/18 08/14/18 13:591,2,3-Trichloropropane 500ug/L 100 GM200

2770 08/14/18 08/14/18 13:591,2,4-Trimethylbenzene 500ug/L 100 GM200

716 08/14/18 08/14/18 13:591,3,5-Trimethylbenzene 500ug/L 100 GM200

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 89 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

B6

8081012-21RE1 (Nonpotable Water)

Sample Date: 08/09/18

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 08/14/18 08/14/18 13:59Vinyl chloride 500ug/L 100 GM200

3510 08/14/18 08/14/18 13:59o-Xylene 500ug/L 100 GM200

10500 08/14/18 08/14/18 13:59m- & p-Xylenes 500ug/L 100 GM200

08/14/18 08/14/18 13:5975-120 96 %Surrogate: 1,2-Dichloroethane-d4

08/14/18 08/14/18 13:5984-110 99 %Surrogate: Toluene-d8

08/14/18 08/14/18 13:5978-110 94 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 8015C

52000 08/14/18 08/14/18 14:28Gasoline-Range Organics 5000ug/L 50 GM5000

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 90 of 98

Project:

Project Number:

Project Manager:

Reported:47:6230-A

Pam Furst

HOWARD UNIVERSITY

08/21/18 16:50

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

Notes and Definitions

S-07 Surrogate recovery outside control limits due to sample matrix effect.

J Detected but below the reporting limit; therefore, result is an estimated concentration (CLP J-Flag).

IS-FAIL Internal standard area outside control limits.

E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered

an estimate (CLP E-flag).

Sample results reported on a dry weight basis

Relative Percent DifferenceRPD

dry

Not ReportedNR

Analyte NOT DETECTED at or above the reporting limitND

Analyte DETECTEDDET

Will Brewington, President

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS can provide a certification list upon request. Page 91 of 98

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