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Page 1: Hot Disk TPS Absolute measurement of thermal conductivity, thermal diffusivity, and ... · 2020-02-11 · The Hot Disk TPS is widely used for the accurate measurement of absolute

Hot Disk TPS Absolute measurement of thermal conductivity, thermal diffusivity,and specific heat.

Page 2: Hot Disk TPS Absolute measurement of thermal conductivity, thermal diffusivity, and ... · 2020-02-11 · The Hot Disk TPS is widely used for the accurate measurement of absolute

Thermal Conductivity [ W/(m•K)]0.001 0.01 0.1 1.0 10.0 100.0 1000.0 10000.0

Hot Disk TPS

HFM

THW

TLS

-160 to 1000°C

-20 to 70°C

-40 to 100°C

-50 to 400°C

LABORATORY INSTRUMENTS

Thermtest has been advancing the measurement of thermal conductivity, thermal diffusivity, and specific heat for more than a

decade. With more than 1500 satisfied customers, our unique combination of advanced thermal conductivity instrumentation

for the laboratory, portable meters for the field, and accessories, enables us to provide ideal solutions to fit any material testing

application and budget. Our proud commitment to being a leader in thermal conductivity has fueled our success through rigorous

development and key partnerships, creating a lineup of industry leading testing solutions for the laboratory, field, and production-line.

PORTABLE METERS

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The Hot Disk TPS is widely used for the accurate measurement of absolute thermal conductivity,

thermal diffusivity, and specific heat of solids, liquids, pastes, and powders. This non-destructive

method has a thermal conductivity testing range of 0.005 to 1800 W/mK and can be used to measure

bulk properties of homogeneous and heterogeneous materials, as well as directional properties

for anisotropic materials. This versatility is greatly appreciated by academic and commercial users

alike, which has led to more than 1000 publications on a wide variety of applications.

Hot Disk Transient Plane Source

SOLIDS

LIQUIDS

PASTES

POWDERS

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INTRODUCTION

2

ResistanceRecording

Pure NickelDouble Spiral

Electrical Insulation:Kapton (400°C) orMica (800/1000°C)

Backing Insulation may beadded for single-sided testing

Power Supply

High SensitivityWheatstone Bridge

Multi-channelCommunications

SensorConnections

Hot Disk Transient Plane Source

SENSOR OPTIONS

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Featured Hot Disk TPS Capabilities

3

Electrical Insulation:Kapton (400°C) orMica (800/1000°C)

Backing Insulation may beadded for single-sided testing

The TPS sensor is comprised of a flat, double-spiral of Nickel, encapsulated between layers

of dielectric insulation. The sensor is electrically connected to a separated power supply and

electrical resistance sensing circuit. An auto-balancing Wheatstone bridge is used to maximize

electrical resistance sensitivity at the sensor spiral, which is critical for measuring a wide range of

thermal conductivity. During a measurement, a current passes through the spiral and creates an

increase in temperature, which is recorded over time. Heat generated, dissipates into the sample

at a rate dependent on the thermal transport characteristics of the material. A unique feature of

the Hot Disk TPS, is the ability to remove the effects of contact resistance from a measurement

without the use of a contact agent. Contact resistance presents itself as a non-linear region

at the start of the calculated results for the transient measurement. This is easily identified and

removed, manually or automatically, leaving a linear slope free of contact resistance. From this

slope, high accuracy thermal conductivity (W/mK) and thermal diffusivity (mm2/s) is calculated,

without the need of complex calibration. Additional properties including volumetric heat

capacity (MJ/m3K) and thermal effusivity (Ws½/m2K) are automatically calculated and displayed.

• Thermal conductivity, thermal diffusivity, & specific heat

• Solids, liquids, pastes, & powders

• ISO & ASTM Standards

• No calibration

• No contact agent

• Control of penetration depth with variable test times

• Two-sided & single-sided sensors

• Bulk & directional properties

• Proven method with 1000+ publications

k = thermal conductivity P = power a = sensor radius m = slope

Tem

pera

ture

Ris

e

Time Constant

Contact ResistanceTime Constant

Tem

pera

ture

Ris

e

k = P/(π3/2•a•m)

21

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SPECIFICATIONS

4

Models TPS 3500 TPS 2500 S

Solids, Liquids, Pastes, and Powders

Thermal Conductivity & Thermal Diffusivity

Bulk or Average

Through-thickness

Through-plane

Two-sided & Single-sided Sensors

Minimum Sample Size (diameter or square) 2 mm 2 mm

Maximum Sample Size 1 Unlimited Unlimited

Thermal Conductivity Range 0.005 to 1800 W/mK 0.005 to 1000+ W/mK

Temperature Range -160 to 1000°C -160 to 1000°C

1 Although there is no maximum sample size, there are limits on depths of heat penetration. This depth of penetration is determined by available test times and thermal diffusivity (mm2/sec) of the material.

TLS Specifications: ASTM D5334, ASTM D5930, & IEEE 442-1981

Thermal Conductivity Range: 0.1 to 5 W/mK

Materials: Soil, Concrete, Rocks, and Plastics

TPS Specifications: ASTM D7984

One Dimensional Thermal Effusivity Range: up to 60,000 Ws½/m2K

Materials: Textiles

TPS EFFUSIVITY MODULE: ALL MODELS

TPS MODELS: STANDARD ISO 22007-2.2

TLS MODULE: ALL MODELSiTPS iTPS

D = Penetration Depthk = Thermal Conductivity a = Thermal Diffusivity t = Time

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5

TPS 2200 TPS 1500 TPS 500 / 500S

6 mm 13 mm 13 mm / 6 mm

Unlimited Unlimited Unlimited

0.01 to 500 W/mK 0.01 to 20+ W/mK 0.03 to 100 / 200 W/mK

-160 to 750°C -160 to 750°C -160 to 300°C

THW Specifications: ASTM D7896

Thermal Conductivity Range: 0.01 to 2 W/mK

Materials: Liquids and Pastes

THW MODULE: ALL MODELS

Dilatometer Specifications: ASTM E228

Measures: Coefficient of Thermal Expansion (CTE)

Materials: Solids

DILATOMETER MODULE: ALL MODELSiTPS iTPS

D = Penetration Depthk = Thermal Conductivity a = Thermal Diffusivity t = Time

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HOT DISK TPS HIGHLIGHTSVERSATILITY

PENETRATION DEPTH TPS SENSORS iTPS PLUGIN

TPS Automation

ABSOLUTE - QUANTITATIVE NO CONTACT AGENT

Solids, Liquids, Pastes, & Powders

Variable Two -sided & Single -sided Expanded Use

No Calibration Effects of ContactResistance Removed

56

HIGHLIGHTS

iTPS+

A S TM D79 8 4A S TM D5 3 3 4A S TM D593 0A S TM D78 9 6A S TM E 2 2 8

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7

VERSATILITY

ABSOLUTE - QUANTITATIVE

The Hot Disk TPS is able to measure solids, liquids, pastes,

and powders for thermal conductivity, thermal diffusivity,

and specific heat. These properties can be measured on a

broad range of samples sizes; samples as small as 2 x 2 mm,

to an unlimited maximum size. For liquids, the sample volume

can be as small as 3 ml. A unique feature of the Hot Disk TPS

- its ability to measure powders of various particle sizes.

Measured results of thermal conductivity, thermal diffusivity, and specific heat are absolute

and quantitative, without the requirement of factory, or user calibrations. The Hot Disk

transient plane source (TPS) technology was developed by Dr. Silas Gustavsson, from his

award-winning research in thermal conductivity measurements, dating back to the 1960’s.

The Hot Disk TPS technology has been widely recognized as one of the most accurate

testing methods commercially available, having undergone multiple independent published

theory investigations. This acceptance has led to more than 1000 systems sold world-

wide and more than 1000+ publications and growing across countless testing applications.

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78

HIGHLIGHTS

PENETRATION DEPTH

NO CONTACT AGENT

The Hot Disk TPS measures thermal conductivity and thermal diffusivity with different intervals

of test times (0.1 to 1280 sec) and sensor diameters (1 to 60 mm). Control of test times are critical

when using a transient measurement, as it ensures the true thermal conductivity is representative

of the sample dimension and is not just a surface measurement, common to methods using only

short test times. The penetration depth of the heat from the sensor is based on three sample

qualities: dimensions, thermal diffusivity (mm2/s), and test time. As the Hot Disk measures thermal

diffusivity, the results are displayed with representative penetration depth, based on the dimensions

of the sample. Test times can be manually selected, or with the iTPS Plugin, automatically selected.

An important testing capability of the Hot Disk TPS is the ability to remove the

effects of contact resistance, without the need of a contact agent, between the

sensor and sample. The early portion of a test represents contact resistance

and is non-linear, when compared to the remainder of the test, representing

the heat from the sensor as it dissipates into the sample in a linear fashion. The

non-linear portion of the test, representing contact resistance, can be removed

automatically or manually after the measurement is made. As the contact

resistance does not require normalizing with a contact agent, measurements on

materials from insulations to conductive metals are possible, without calibration.

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9

TWO-SIDED & SINGLE-SIDED

iTPS PLUGIN

Hot Disk TPS sensors can be used in both two-sided and single-sided configurations.

Highly accurate lab testing can be performed by surrounding the flat sensor with a

sample piece, on either side. If two pieces of a sample are not available, the unique

single-sided sensor, first invented by Dr. Silas Gustavsson in 1983*, can be used. There

are two versions of the single-sided sensor available; a standard two-sided sensor

can be configured for single-sided testing by placing an insulation material of known

properties on one side of the sensor, the second option is a permanently configured

spring-loaded single-sided sensor, for convenient testing of large, hard to handle samples.

With the introduction of the iTPS Plugin, full automation of TPS parameters and calculations

is possible. While maintaining the ability to manually select parameters, the iTPS provides

full automation of all aspects of TPS measurement. In addition, the already versatile Hot

Disk TPS is expanded for testing according to multiple international testing standards;

TPS - Thermal Effusivity for Textiles (ASTM D7984), TLS - Thermal Conductivity for Soil,

Concrete, and Polymers (ASTM D5334, ASTM D5930, & IEEE 442-1981), THW - Thermal

Conductivity for Liquids (ASTM D7896), and coefficient of thermal expansion (ASTM E228).

TPS AutomationiTPS

+A S TM D798 4A S TM D53 3 4A S TM D593 0A S TM D789 6A S TM E 2 28

*Gustafsson, Karawacki. July 1983. Transient hot-strip probe for measuring thermal properties ofinsulating solids and liquids. Review of Scientific Instruments, 54(6):744 – 747.

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12

10

SAMPLE MEASUREMENTMEASUREMENT

1 min.

2 min.

Power and test time parameters may be selected manually or automatically

with the included iTPS Plugin. Only requiring input of sample dimensions,

the iTPS automatically selects test times to maximize penetration depth

for measurement of thermal conductivity. Advanced software features are

available for automation of multiple tests or control of temperature.

When testing in the laboratory, two sample pieces may be clamped on either

side of the TPS sensor. If two sample pieces are not available, the TPS single-

sided sensor may be used. For compressible materials, a compression stand

may be used to record force applied and thickness of the sample.

SAMPLE SET-UP

TPS SOFTWARE

iTPS

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43

1 min.

11

SAMPLE MEASUREMENT ACCURACY WITH EASE

< 2 min.

As the Hot Disk TPS method is absolute, the results are calculated from

the temperature rise vs. time graph, after a measurement is complete. At

this point, the effects of contact resistance at the early portion of the

measurement can be removed manually or automatically with the iTPS

Plugin. Results can then be exported to Excel or Notepad.

Once start measurement is selected, the Hot Disk TPS will first auto-balance

an internal Wheatstone bridge for maximum sensitivity. A temperature drift

log of 40 seconds is then recorded. Once complete, the test automatically

begins, and the temperature rise with time raw data is displayed.

MEASUREMENT

RESULT CALCULATIONS

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12

HOT DISK APPLICATIONSAPPLICATIONS

TWO-SIDED AND SINGLE-SIDED BULK MEASUREMENTSFor standard testing, the Hot Disk measures absolute bulk thermal conductivity, thermal

diffusivity, and auto-calculates volumetric specific heat and thermal effusivity for solids, liquids,

pastes, and powders.

There are two convenient ways to measure thermal properties; lab scale testing, which involves

positioning the two-sided TPS sensor between two pieces of the same sample, and single-sided

testing of one sample piece using the single-sided TPS sensor. In addition to room temperature,

measurements can be made over a wide temperature range. Using the Hot Disk TPS software

and a compatible furnace, the furnace is conveniently controlled through setting an automated

testing schedule that includes the temperatures of interest.

Multiple measurements were made on Pyrex Glass, Pyroceram, and 316 Stainless Steel from 20°C

to 400°C and results show excellent agreement with literature values. The same samples were

measured with both the two-sided and single-sided TPS sensors and results are compared below.

Ther

mal

Con

duct

ivit

y (W

/mK

)

Temperature (˚C)

Pyrex GlassPyroceram316 Stainless Steel

Literature MeasuredPyrex GlassPyroceram316 Stainless Steel

Sample

Two-Sided TPS Single-Sided TPSThermal

Conductivity(W/mK)

ThermalDiffusivity (mm²/s)

VolumetricSpecific Heat

(MJ/m³K)

ThermalEffusivity

(Ws½/m²K)

ThermalConductivity

(W/mK)

ThermalDiffusivity(mm²/s)

VolumetricSpecific Heat

(MJ/m³K)

ThermalEffusivity

(Ws½/m²K)

Pyrex Glass 1.14 0.69 1.71 1416 1.14 0.67 1.71 1396

Pyroceram 3.99 1.92 1.98 2739 3.96 1.93 2.06 2851

316 Stainless Steel 13.72 3.51 3.73 6985 13.46 3.48 3.83 7133

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ANISOTROPIC POLYMER COMPOSITES

Polymer composites, with conductive fillers, are the perfect example of anisotropic materials. These materials experience directional

dependent thermal properties, meaning the in-plane properties differ from through-plane properties. The TPS Anisotropic

Module has the ability to accurately and simultaneously measure the thermal properties of both planes. To create the composites,

synthetic graphite particles were added to a liquid crystal polymer, in varying weight contents. Results indicate a higher in-plane

thermal conductivity, as well as an increasing trend in thermal conductivity, as the weight percentage of graphite increased.

Through-plane results from the TPS testing correlates well with results from the steady-state guarded heat flow meter (ASTM E1536).

Miller, M.G., Keith, J.M., King, J.A., Edwards, B.J., Klinkenberg, N., Schiraldi, D.A. 2006. Measuring the Thermal Conductivities of Anisotropic Synthetic Graphite-Liquid Crystal Polymer Composites. Polymer Composites, 27(4): 388-394.

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APPLICATIONS

14

Convection is the dominant force of heat transfer in fluids and must be minimized to

accurately measure thermal conductivity. The TPS method is able to minimize the effects

of convection by lowering the heating power and time settings for each measurement.

With the small volume test cell, only 3 ml of liquid is required. Varying volume fractions

of aluminum nitride particles, 20 nm in diameter, were dispersed into ethanol. Using

the TPS technique, thermal properties were measured at 273.15 K and 297.15 K.

NANOFLUIDS

Hu, P., Shan, W-L., Yu, F., Chen, Z-S. 2008. Thermal Conductivity of AlN-Ethanol Nanofluids. International Journal of Thermophysics, 29: 1968-1973.

Thin sheets are a common geometric shape of conductive materials.

The TPS Slab Module can measure the thermal properties of

such materials, by insulating the lateral surfaces of the sample

with an insulative backing, to minimize heat loss and mimic an

infinite medium in-plane. With the use of Thermtest’s Temperature

Platform, thermal property measurements are possible from 10 to

300˚C. All results showed good agreement with literature values.

HIGH CONDUCTING SLABS

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15

SampleHeat

Capacity(J/K)

SpecificHeat

Capacity(J/kgK)

VolumetricHeat

Capacity(MJ/m3K)

Macor 2.53 807 1.97

Stainless Steel 304 2.91 487 3.79

Copper 110 2.49 381 3.38

SPECIFIC HEAT OF MATERIALSThe TPS Specific Heat Module is a convenient method for directly measuring

high accuracy heat capacity of materials. Each cell is fabricated from a

highly conductive material, fastened to a Hot Disk sensor and surrounded

by a thermally insulative backing. With the input of mass and density,

Specific Heat Capacity (J/kgK), and Volumetric Heat Capacity (MJ/m3K), are

also determined. The Specific Heat Capacity (J/kgK) results, show good

agreement with literature values for various materials that were measured,

and the mean results had an excellent reproducibility of less than 0.75%.

Yuan, M. Thermal Conductivity Measurements of Polyamide Powder. Master’s Thesis, The University of Texas at Austin, December 2011. https://repositories.lib.utexas.edu/handle/2152/ETD-UT-2011-12-4476.

Using the TPS method and a standard powder cell, the relationship between

density and thermal conductivity of laser-sintered fresh polyamide 12 powder

was determined. As the contact resistance between sensor and powders of

different particle size is removed, accurate thermal properties can be measured.

3D PRINTER POWDERS

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TESTING MODULES

16

For measurement of bulk or average thermal conductivity (W/mK), thermal diffusivity

(mm2/s), and volumetric heat capacity (MJ/m3K) of homogeneous and heterogeneous

solids, liquids, pastes, and powders. Standard measurements can be made with TPS

two-sided and TPS single-sided sensors for highest accuracy and maximum flexibility.

Available on: All TPS Models.

STANDARD

Directional (axial and radial) thermal conductivity and thermal diffusivity for anisotropic

materials. This testing module requires the input of volumetric heat capacity; if not

known, it can be easily measured with the TPS specific heat testing module. Anisotropic

measurements may be made with TPS two-sided and TPS single-sided sensors.

Available on: TPS 3500, TPS 2500 S, TPS 2200, TPS 1500

ANISOTROPIC

Thermal conductivity, thermal diffusivity, and volumetric heat capacity of sheets or

slabs. Ideal for thin conductive materials like steel, aluminum, copper, and graphite.

Measurements of samples from 0.04 to 10 mm thick, and as high as 1800 W/mK are possible.

Available on: TPS 3500, TPS 2500 S, TPS 2200, TPS 500 S

SLAB

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Designed for measuring along the length of elongated materials, like rods or core samples.

This module is particularly powerful for testing complex materials, such as heterogeneous

or anisotropic materials, which are difficult to test with standard testing techniques.

This testing can be done with the standard two-sided or single-sided sensor formats.

Available on: TPS 3500, TPS 2500 S, TPS 1500, TPS 500 S

ONE-DIMENSIONAL

Designed for the measurement of thermal conductivity on free standing thin-films

or coatings (> 0.01 mm). The thin-film testing module is most widely used in the

measurement of polymer films, however additional testing of coatings is also possible.

Available on: TPS 3500, TPS 2500 S, TPS 2200

THIN-FILM

In addition to calculated volumetric heat capacity from the measurement of thermal

conductivity and thermal diffusivity, the Hot Disk TPS is able to directly measure, with high

accuracy, specific heat. With various sizes of specific heat cells available (7 to 300 mm),

unique testing of complex structures and heterogeneous materials is possible.

Available on: TPS 3500, TPS 2500 S, TPS 2200, TPS 1500, TPS 500 S

SPECIFIC HEAT

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iTPS EXPANDED

Using the thermal property of effusivity, the human feeling of comfort (coolness or warmth) can be measured for textiles and

automotive interiors. In addition to the initial feeling of comfort, covered by the ASTM, this feeling of comfort can also be measured with

longer touch times, providing design engineers with a full understanding of how effusivity changes with touch time.

TPS – EFFUSIVITY(ASTM D7984)

The transient line source (TLS) method is commonly used for testing the thermal conductivity and thermal resistivity of soils, rocks,

concretes, and plastics. The standard 100 mm probe is ideal for soft, or easy to drill samples, while the shorter 50 mm needle is best

suited for harder to drill, rigid samples like rock and concrete.

TLS - THERMAL CONDUCTIVITY - THERMAL RESISTIVITY(ASTM D5334, ASTM D5930, and IEEE 442-1981)

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19

The transient hot wire (THW) method, for thermal conductivity testing of liquids. The THW features unique characteristics to limit the

effects of convection; short test times, thin diameter (0.1 mm) wire, and the wire is held in a vertical orientation, when testing liquids.

With this control of convection, testing of a wide range of viscosities is possible.

THW- THERMAL CONDUCTIVITY(ASTM D7896)

A compact, digital, horizontal, single-sample, benchtop system for measuring dimensional changes of solid materials, such as ceramics,

glass, metals, carbon composites, cements, minerals, and polymers, from RT to 1000°C. The dilatometer records reversible and

irreversible changes in length (expansion and contraction) during heating and cooling.

DILATOMETER – THERMAL EXPANSION(ASTM E228)

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ACCESSORIES

20

COMPRESSION STAND+ TEMPERATURE

FAN FURNACE

MUFFLE FURNACETUBE FURNACE

TEMPERATURE PLATFORM

• Affordable, compact, rapid testing • -150°C, -50°C or 5 to 300°C

• Size up to: 40 mm diameter x 20 mm • Two channel TPS switch & Gas purge

• Affordable, versatile, expandable• Up to 4 samples

• 300°C, 400°C, & 500°C options• Optional gas purge

• Option 1: 40 x 40 x 13 mm• Option 2: 75 x 75 x 25 mm

• 1000°C in backfilled environment

• Large sample or multiple samples• Size up to: 150 x 150 x 50 mm

• 750°C in backfilled environment

• For compressible materials• Force gauge: 10 to 100 N

• Distance gauge• Room temp or -40 to 200°C

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STANDARD TPS SENSORS

TESTING CELLSEXTENDED TPS SENSORS TPS SWITCH

21

• One sensor for any sample, 20 mm or larger• Two-sided sensor for accurate lab testing

• Single-sided, spring-loaded sensor for testing of large samples

• Liquid cell: 3 ml• Powder cell

• Paste cell

• Small sensors for samples as small as 2 mm• Large sensors for heterogeneous samples or

large particle powders.

• Automate multi-sensor testing• Channels: x 2, x 4, or x 8

• Can be combined with furnace

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22

METHODS

Methods Comparison TPS HFM THW TLS Methods Comparison LFA GHP GHFM MTPS

Accuracy ± 5% ± 3% ± 5% ± 5% Accuracy ± 5 to 7% ± 2% ± 5% ± 5 to 15%

Measured Property Thermal Conductivity, Thermal Diffusivity, Specific Heat 1

Thermal Resistance,Thermal Conductivity 1

Thermal Conductivity, Thermal Diffusivity, Specific Heat 1

Thermal Conductivity, Thermal Resistivity 1 Measured Property Thermal Diffusivity, Specific

Heat 1, Thermal Conductivity 1Thermal Resistance,

Thermal Conductivity 1Thermal Resistance,

Thermal Conductivity 1Thermal Effusivity,

Thermal Conductivity 1

Temperature Range -160 to 1000°C -20 to 70°C -50 to 400°C -40 to 100°C Temperature Range -253 to 2800°C -160 to 600°C -20 to 300°C -50 to 200°C

Materials Solids, Liquids, Pastes, &Powders Solids – Insulation Liquids and Pastes Soils, Rocks, & Plastics Materials Solids Solids – Insulation Solids Solids, Liquids, & Paste

Calibration None – Absolute Measurement Single – Offset Single – Offset Multiple – Offset Calibration None – Absolute Measurement None – Absolute Measurement Single – Offset Multiple – Secondary

Contact Resistance Removed After Measurement Removed Through Calibration N/A Contact Paste Contact Resistance Graphite Spray Contact Paste Contact Paste Water & Contact Paste

Penetration Depth Up to 180 mm Entire Sample < 1 mm < 50 mm Penetration Depth Entire Sample Entire Sample Entire Sample 0.1 to 3 mm

Heterogenous Samples < 10 mm scale < 20 mm scale < 1 mm scale < 10 mm scale Heterogenous Samples < 0.1 mm scale < 20 mm scale < 5 mm scale < 0.05 mm scale

Theory ScientificallyReviewed Several Published Papers Several Published Papers Several Published Papers Several Published Papers Theory Scientifically

Reviewed Several Published Papers Several Published Papers Several Published Papers One Published Paper

Specifications sourced from user manuals and available literature.

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Methods Comparison TPS HFM THW TLS Methods Comparison LFA GHP GHFM MTPS

Accuracy ± 5% ± 3% ± 5% ± 5% Accuracy ± 5 to 7% ± 2% ± 5% ± 5 to 15%

Measured Property Thermal Conductivity, Thermal Diffusivity, Specific Heat 1

Thermal Resistance,Thermal Conductivity 1

Thermal Conductivity, Thermal Diffusivity, Specific Heat 1

Thermal Conductivity, Thermal Resistivity 1 Measured Property Thermal Diffusivity, Specific

Heat 1, Thermal Conductivity 1Thermal Resistance,

Thermal Conductivity 1Thermal Resistance,

Thermal Conductivity 1Thermal Effusivity,

Thermal Conductivity 1

Temperature Range -160 to 1000°C -20 to 70°C -50 to 400°C -40 to 100°C Temperature Range -253 to 2800°C -160 to 600°C -20 to 300°C -50 to 200°C

Materials Solids, Liquids, Pastes, &Powders Solids – Insulation Liquids and Pastes Soils, Rocks, & Plastics Materials Solids Solids – Insulation Solids Solids, Liquids, & Paste

Calibration None – Absolute Measurement Single – Offset Single – Offset Multiple – Offset Calibration None – Absolute Measurement None – Absolute Measurement Single – Offset Multiple – Secondary

Contact Resistance Removed After Measurement Removed Through Calibration N/A Contact Paste Contact Resistance Graphite Spray Contact Paste Contact Paste Water & Contact Paste

Penetration Depth Up to 180 mm Entire Sample < 1 mm < 50 mm Penetration Depth Entire Sample Entire Sample Entire Sample 0.1 to 3 mm

Heterogenous Samples < 10 mm scale < 20 mm scale < 1 mm scale < 10 mm scale Heterogenous Samples < 0.1 mm scale < 20 mm scale < 5 mm scale < 0.05 mm scale

Theory ScientificallyReviewed Several Published Papers Several Published Papers Several Published Papers Several Published Papers Theory Scientifically

Reviewed Several Published Papers Several Published Papers Several Published Papers One Published Paper

1 Italicized property delineates calculated properties.

Page 26: Hot Disk TPS Absolute measurement of thermal conductivity, thermal diffusivity, and ... · 2020-02-11 · The Hot Disk TPS is widely used for the accurate measurement of absolute

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