hygieneering inc - phase ii environmental soil

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II208113

Phase II Environmental Soil Investigation Report1840 South 54th Avenue in Cicero, Illinois

Cicero, Illinois

Prepared for:J. Sterling Morton High School District 201

Prepared by:Hygieneering, Inc.7575 Plaza Court September 28, 2001Willowbrook, Illinois 60521 Project No. 200 i -3628

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Table of Contents

Executive Summary 1Discussion 2

Background .-.-. 2Methodology 2Results 3

Conclusion 9Appendices 10

Appendices

Appendix A: Soil Boring LocationsAppendix B: Soil Boring LogsAppendix C: Laboratory Analytical Results

Phase II InvestigationSchool District 2012/28/2001-3628

PHASE II ENVIRONMENTAL SOIL INVESTIGATION1840 SOUTH 54TH AVENUE

CICERO, ILLINOISOCTOBER 19,2000

Executive Summary

J. Sterling Morton High School District 201 (School District 201) retained Hygieneering, Inc.(Hygieneering) to perform a Phase II Environmental Soil Investigation of the property located at1840 South 54th Avenue in Cicero, Illinois (the Property). This project was conducted to attemptto determine the presence of contaminated soil potentially caused from the historical use of theProperty.

Hygieneering and its subcontractor, Rock & Soil Drilling Corporation of St. Charles, Illinois,performed the following tasks as a part of this project:

• Advanced 37 soil borings (in three separate phases) to variable depths inside thesouthern portion of the building and outside the building on the Property.

• Conducted continuous sampling on each boring and screened samples for organicvapors in the field with a photo-ionization detector (PID).

• Submitted the one sample from each boring that displayed the highest organicvapor reading for analysis of VOCs (volatile organic compounds), BTEX(benzene, toluene, ethyl benzene, and xylenes), PNAs (polynuclear aromaticcompounds), and RCRA (Resource Conservation and Recovery Act) metals. Theparameters listed were not all analyzed for each sample, rather for selectedparameters from this list based on historical uses of different areas of theProperty and adjoining properties.

• Interpreted the results and compared the contaminant concentration levels to themost stringent cleanup objectives listed in the Tiered Approach to CorrectiveAction Objectives (TACO): IL Adm. Code Part 742.

Hygieneering did not advance soil borings in the central and northern portions of the building dueto access issues and the presence of active operations being performed by Economail.

The results of our investigation indicate the presence of high concentrations of variouschlorinated solvents under and adjacent to the southwestern portion of the building on theProperty. Trichloroethylene, perchloroethylene, cis-l,2-dichloroethylene, and vinyl chloridewere the main contaminants of concern that were present in soil and groundwater above the moststringent cleanup objectives listed in TACO. The affected area appeared to be approximately 100feet by 150 feet, with contamination detected at depths of up to 30 feet below the ground surface(bgs).

1840 South 54Ih Ave Soil InvestigationSchool District 201Project Number 2001-3628

Discussion

Background

Hygieneering conducted a Phase I Environmental Site Assessment of the Property anddetermined the Property and the adjoining properties have been used for industrial purposes sincethe early 1900s. These uses include the use of the Property as for manufacturing electricalconnectors and components.

Hygieneering observed the presence of three underground storage tanks under the southwesternportion of the building during our Phase I Environmental Site Assessment. In addition, SanbornFire Insurance Maps indicated that a plating room was located on the southwest corner of thebuilding.

Hygieneering performed a Phase II Environmental Soil Investigation in an attempt to determinethe presence of VOCs, BTEX, PNAs, and RCRA metals, on different areas of the Property.VOCs were analyzed for in areas where a broad range of possible contaminants was suspected,including solvents, degreasers, and fuels. BTEX and PNAs were analyzed for in areas that weremost likely to be locations of fuel oil USTs (near the former boiler room). Hygieneeringcollected samples that were analyzed for metals near the plating area on the Property. A drawingshowing the sample locations is included in Appendix A.

Methodology

Hygieneering and its subcontractor, Rock & Soil Drilling, advanced thirty-seven soil borings witha Bobcat mounted Geoprobe rig on the Property to a depths of twelve feet to thirty feet on May25, 31, June 3, July 9 and 13, 2001. In addition, six monitoring wells were installed, three insideand three outside the building during this project.

Hygieneering performed continuous sampling on each boring using a PID to screen for organicvapors. Samples were collected at two-foot intervals and the screening sample with the highestPID reading was submitted to the laboratory. In addition, Hygieneering collected a secondsample from selected borings inside the building in the main contaminated area in an attempt todefine the vertical extent of contamination. Copies of the soil boring logs are included inAppendix B. \ *, > f?

•/ y f /•\ % •< .*Boring locations B4, B18, B21, B26, and B37 were converted into monitoring wells. B4 was atemporary well that was removed on the same day it was installed.

Hygieneering collected VOC samples using the SW-846 method with field preservation included.Samples were stored in a cooler on ice until they reached the laboratory at the end of the day.

Great Lakes Analytical analyzed the VOC, BTEX, and PNA samples using the EPA Method5035/8260B, and RCRA metals samples by EPA 6000/7000 Series Methods. Copies of theanalytical reports are included in Appendix C.


Results

Hygieneering interpreted the results and compared the contaminant concentrations to those listedin Illinois Administrative Code Part 742 (TACO). Hygieneering used the most stringent cleanupobjectives: Tier 1 Soil Remediation Objectives for Residential Properties, Soil Component of theClass I Groundwater Ingestion Exposure Route, except for RCRA metals. Hygieneeringattempted to compare these results to pH specific cleanup objectives, however, the pH of the soilwas greater than 8.0, which prevents this comparison from being made. Therefore, Hygieneeringcompared these levels to the concentrations of inorganic chemicals in background soils listed inAppendix A Table G of TACO.

The following table summarizes the results of the VOC, BTEX, RCRA metals (whereapplicable), and PNA (where applicable) laboratory analysis performed on the soil samplescollected.

BoringNo.

Bl

B4

B5

B7BIO

Bl l

Depth

6'

7'

8'

6'9'

ir

Contaminant

C ^!

Benzene 2 i.1 , 1 -Dichloroethane ' 1 ,2-Dichloroethane , °fi1,1-DCE ^Cis 1,2-DCE '-^Trans- 1,2-DCE 3" Ethyl benzene :; ':•Methylene ChlorideTolueneVinyl Chloride .' /Xylenes r 1 0No VOCs detectedPNAs:FluoranthenePhenanthrene1,1 Dichloroethane1,2-Dichloroethane1,1-DCEcis- 1,2-DCE1,1,1-TrichloroethaneTCE ' i-Vinyl ChlorideNo VOCs detectedCarbon Disulfide1,2-Dichlorore thanecis- 1,2-DCEPERCTCEVinyl ChlorideLeadBenzene(Only BTEX and PNAsanalyzed)

Concentration(mg/kg)

0.04271.1100.008250.0190.9020.2560.01510.0376130 ^0.8610.0441NA

1.0401.600230.07250.04625.5300.2478.1600.261NA0.008580.2050.01120.01710.005021.0600.0271 mg/L0.0406

Soil Comp ofGW Ingestion

Objective0.03230.020.060.40.7130.02120.01150NA

4,300NA230.020.060.420.060.01NA320.020.40.060.060.010.0075 mg/L0.03

Inhalation /Ingestion*Objective

0.813000.47007801600400136500.03410

3100NA13000.4700780120050.03NA7200.47801150.03400 mg/kg0.8

-


BoringNo.

B12

B13

B14

B15

B16

B17

B18B18

B19

B19

B20

B20B21

B22

B22

B23

Depth

10'

11'

3'

10'

2'

9'

8'32'

5'

9'

4'

14'15'

3'

15'

9'

Contaminant

FluoranthenePhenanthrenePyrene(Only BTEX and PNAsanalyzed)PERC -2SrTCE ~-^LeadCis- 1,2-DCETCE ^LeadCis- 1,2-DCE ''-&TCECis- 1,2-DCETCELeadBenzene(Only BTEX and PNAsanalyzed)AcetoneAcetoneMethylene ChlorideAcetone2-ButanoneMethylene ChlorideChloroethane1,1 -Dichloroethanecis- 1,2-DCEVinyl ChlorideAcetoneChloroethaneAnthracenePhenanthreneNo VOCs detectedCis- 1,2-DCEMethylene ChloridePERCTCEVinyl ChlorideCis- 1,2-DCETCEVinyl ChlorideCis- 1,2-DCEMethylene ChlorideTCECis- 1,2-DCETrans- 1,2-DCEMethylene ChlorideTCEVinyl Chloride


0.3530.4200.221

1020 ^42200.020 mg/L34.674.80.0104 mg/L43.924.834.33.690.0385 mg/L0.0292

0.03420.03210.005230.1030.01990.005150.01220.007150.005680.005410.04340.01070.1640.205NA3.6500.8450.9715911.3300.4114.7500.5110.009450.005980.14921.300.3970.4310.3422.530


Objective4,300No objective4,200

0.060.060.0075 mg/L0.40.060.0075 mg/L0.40.060.40.060.0075 mg/L0.03

16160.0216No objective0.02No objective230.40.0116No objective12,000No objectiveNA0.40.020.060.060.010.40.060.010.40.020.060.40.70.020.060.01

Inhalation /Ingestion*Objective

3100NA2300

115400 mg/kg7805400 mg/kg78057805400 mg/kg0.8

78007800137800NA13NA13007800.037800NA23,000NANA780131150.0378050.0378013578016001350.03

1840 South 54'h Ave Soil InvestigationSchool District 201Project Number 2001-3628

BoringNo.

B24

B25

B26

B27B28B28B29

B30

B30

B31

B32

B32

B34

B34

B35

B35

Depth

12'

7'

7'

13'4'13'10'

11'

25'

4'

3'

15'

5'

15'

6'

15'

Contaminant

Cis- 1,2-DCETrans- 1,2-DCEMethylene ChlorideTCEVinyl ChlorideCis- 1,2-DCEMethylene ChlorideTCEVinyl Chloride1,1 -Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCEMethylene ChlorideTCEVinyl ChlorideTfi^*'TCENo VOCs detectedCis- 1,2-DCETCECis- 1,2-DCEMethylene ChloridePERCTCEVinyl ChlorideMethylene ChlorideTCEAcetoneMethylene ChlorideTCEAcetone15 PNAs detected, noneabove cleanup objectives.(PNA analysis only)AcetoneMethylene ChlorideAcetone2-Butanone13 PNAs detected, noneabove cleanup objectives.(PNA analysis only)AcetoneMethylene ChlorideNo PNAs detectedAcetoneMethylene ChlorideAcetoneMethylene Chloride


5.5900.4380.8391560.000.4600.0370.006320.0840.1460.02330.0082711.800.5240.01150.006652.2300.007080.0115NA0.005990.036721.900.9384.8301160.001.2400.8359.9502.5200.8311.2100.0891See lab report

0.05270.005270.1020.0128See lab report

0.0790.00560NA0.07060.00560.05240.00525


Objective0.40.70.020.060.010.40.020.060.01230.060.40.70.020.060.010.060.06NA0.40.060.40.020.060.060.010.020.06160.020.0616NA

160.0216No objectiveNA

160.02NA160.02160.02

Inhalation/Ingestion*

>'• Objective78016001350.037801350.03130070078016001350.0355NA7805780131150.0313578001357800NA

7800137800NANA

780013NA780013780013

1840 South 54th Ave Soil InvestigationSchool District 201Project Number 2001-3628

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BoringNo.

B36

B36

B37

B37

Depth

3'

15'

6'

19'

Contaminant

Acetone2-ButanoneMethylene ChlorideAcetoneMethylene ChlorideChloroform1 , 1 -Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCEMethylene ChloridePERC1,1,1 -TrichloroethaneTCEVinyl ChlorideAcetoneChloroformCis- 1,2-DCETrans- 1,2-DCEMethylene chlorideTCEVinyl Chloride


0.1720.01730.007080.06020.005170.8800.2080.06482.3300.2030.006840.01720.01118.2300.5230.08260.03070.1980.009060.019771.1000.00602


Objective16No objective0.02160.020.6230.060.40.70.020.0620.060.01160.60.40.70.020.060.01

Inhalation /Jngestioii*

"" Objective7800NA137800130.3130070078016001311120050.0378000.378016001350.03

Bold value indicates an exceedance of the TACO Tier 1 Soil Component of the Groundwater Ingestions ExposureRoute Remediation Objective1,1-DCE: 1,1-dichloroethylene *More stringent value listedCis-1,2-DCE: cis-1,2-dichloroethyleneTrans-1,2-DCE trans-1,2-dichloroethylenePERC: TetrachloroethyleneTCE: Trichloroethylene

These results indicate the presence of chlorinated solvent impacted soil under the southwesternportion of the building and the area immediately adjacent to the southwest corner of the building.Several samples contained concentrations of PERC, TCE, cis-1,2-DCE, and vinyl chloride thatexceeded the soil component of the groundwater ingestion exposure route values (most stringent)and the ingestion and inhalation exposure route values listed in the TACO soil remediationobjectives for residential properties. In addition, the concentrations for lead in all of the boringsanalyzed for TCLP RCRA metals exceeded the most stringent cleanup objective.

The following table summarizes laboratory analysis of water samples collected during thisinvestigation.

Monitoring Well No.

Temp- 1

Boring Location

B4

Contaminant

No VOCs detectedBenzo(a)pyreneBenzo(b)fluorantheneBenzo(k)fluorantheneChryseneFluoranthenelndeno( 1 ,2,3-cd)pyrenePhenanthrene

Concentration(rag/L)

0.003250.004160.001130.01000.04810.002010.0618 J

J ; CleanupObjective

NA0.00020.000180.000170.00150.280.00043No objective


Monitoring Well No.

MW1MW2

MW3

Boring Location

B18B14

B21

Contaminant

AcetoneBenzeneChloroethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCETCEVinyl Chloride1,1 -Dichloroethanecis- 1,2-DCEtrans- 1,2-DCETCEVinyl Chloride

Concentration(mg/L)

0.05460.002590.02962.5800.04240.0853242.0002.58047.10014.0000.63232.2000.954937.0006.560

CleanupObjective

0.70.005No objective0.70.0050.0070.070.10.0050.0020.70.070.10.0050.002

Bold value indicates an exceedance of the TACO Tier 1 Groundwater Remediation Objective

Tier 1 groundwater remediation objectives were exceeded for PNAs in temporary well 1, whichwas located in the parking lot approximately 50 feet south of the building. The presence of PNAssuggest the contamination is from heating oil, that may have been generated from the formerStrom Steel Ball Plant that was formerly located on the southern portion of the Property.

Tier 1 groundwater remediation objectives were exceeded for several chlorinated solvents inwells MW2 and MW3, which are located inside the southwestern portion of the building.

Future Land Use ConsiderationsIllinois has set up a voluntary cleanup program known as the Site Remediation Program, or SRP.The program allows the use of a risk-based approach to remediation (Tiered Approach toCorrective Action Objectives, or TACO), including creating site-specific cleanup objectives thatare based on the risk of individuals ingesting or inhaling contaminants. The remedial objectivesreferred to in the table above represent the most stringent objectives listed in TACO. Thosevalues may be changed through the use of risk-based equations or through the elimination of theexposure route (soil component of the groundwater ingestion exposure route). This program alsoallows property owners to leave contamination in place if they can demonstrate that all of therisks and potential exposure routes have been addressed. In order for contamination to be left inplace, the Illinois Environmental Protection Agency will sometimes place some conditions orrequirements on properties to allow this. These conditions may include deed restrictions,groundwater use ordinances, and installation of engineered barriers.

This investigation has confirmed the presence of chlorinated solvent impacted soil under andaround the southwest portion of the building. The contamination extends from the near surfacesoil to depths of at least 30 feet below the ground surface. The nature of the contaminationrequires that excavated soil be handled as hazardous waste. Due to the high cost of hazardouswaste disposal, the best future land use options for this site would be ones that involve the leastamount of excavation. However, the presence of the contaminants in the soil would require theinstallation of an engineered barrier to prevent exposure to potential future occupants of theproperty. An example of an engineered barrier is an asphalt parking lot.


Hygieneering believes that through the use of the risk-based approach outlined in TACO, most, ifnot all of the contamination on the property may be left in place. The only material that wouldhave to be removed and disposed of as hazardous waste would be those materials excavated tofacilitate construction activities. Therefore, Hygieneering would recommend the installation ofan asphalt parking lot over the contaminated area in a manner that would only require theminimum amount of soil to be excavated from the site.


Conclusion

The results of this Phase II Environmental Soil Investigation indicate the presence of significantchlorinated solvent contamination under and around the southwest portion of the building on theproperty. The contamination has impacted both soil and groundwater at concentrations thatexceed the most stringent cleanup objectives listed in TACO.

Recommendations

J. Sterling Morton High School District 201 intends on using this parcel as part of a futurecampus area. Hygieneering recommends the submission of this property into the Illinois SiteRemediation Program (SRP) so that site-specific cleanup objectives can be developed for theproperty and approved by the IEPA. Hygieneering also recommends that the contaminated areabe covered with an engineered barrier, specifically an asphalt parking lot, in order to minimizethe costs associated with disposing of soil that will be classified as hazardous waste from theproperty.

We appreciate the opportunity to assist you on this important project. If you have any questionsor require additional information, please do not hesitate to contact us.

Respectfully submitted,Hygieneering, Inc.

Garrick J. Milkeris, CHMMEnvironmental Assessments Manager

ohn Feller, CIH, CSPVice President

Progress/Gary M/Morton PII 00-2782/Morton PH.doc


II* Appendices

• APPendi*A: B°ri"g Location Drawings

Appendix B: Soil Boring Logs

| APpendix c: Laboratoly Analytica]

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1840 South 54th Ave Soil Investigation J OSchool District 201Project Number 2001-3628

ii

Appendix A:

Boring Location Drawings

B954th Avenue

B8

eB7

eB6 I

~e ~[HIP

e82

n a

LD

eB3

eB5

B4 CD

e

< RAILROAD EASEMENT >

SITE PLAN

(NOT DRAWN TO SCALE)

Hygieneering, Inc.7575 Plaza Court

Willowbrook, IL 60521

CLIENT:

J. Sterling MortonHigh School District#201

PROJECT:

First Round OutdoorBorings1840 South 54th AvenueCicero, Illinois

PROJECT NO.:

2001-3628-E

Appendix B:

Soil Boring Logs

1 i>^1 l

\ Project Name: EconoMail

R^> Project Number: 2001-3495

f^P Project Location: 1834 South 54th Avenue

Samples Taken By: CD

^^ Ambient Air Tem p: 60F

a. HYGIENEERING. INC. start/stop Time:8:0° am - 4:0°Pm

1

1

1

1

4I1111

Boring Number: 3495-B1Drilling Company: Rock & Soil

Drilling Method: Geoprobe

Type of Sampling: Soil

Boring Location: GPS Coord.

Date: 05/29/01

c-3O>_c

f "5.

«• iQ W

0 -j

-1 -

-2-

-3-

-4-

-5-**-o

-7-

-8-

-9-

-10-

-11-

-12-

-13-

-14-

If?

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— ' '

0

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c(0o

CO £

Q 2.^ S Lithology Data Q. &

CONCRETE:M \

CLAY: Grey, Soft, Tracegravel.Noodor/discolorat

M

A CLAY: Grey/Tan, Hard,Trace gravel, Noodor/discoloration

W

W

J^^^^ l/ ^^^^^H — -ion ^^^1 108 ~ f ~2

^^^^^H .4

^•^ - -5

^^^^Hs98 .. ^

^H ^--*^^^^^1 — - -9

^ 1 --1°^^^^^H — -11H^ ^ ^HH ' . _

95---13

---14

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COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".

§ Boring was backfilled with bentonite chips. Photo-kmizatton Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated

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1

_ ^\ Project Name: EconoMail

g K^^^C l Project Number: 2001-3495

^y^ Project Location: 1834 South

t Samples Taken By: CD

• ^ ^^ Ambient Air Temp: 70F

Boring Number: 3495-BIDrilling Company: Rock & Soil

54th AvenueDrilling Method: Geoprobe


Borinq Location: GPS Coord.^ HYGIENEERING, INC. start/St°P Time:8:00 am - 4:00pm• Date: 05/29/01

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I = 0 D£ 0 - 0 . «\ 1 E o2 t5 5 2

1 00 -. ,: cu-1 - - W ^0

|-2-LS" ~ sAj? •^~r8f A

I "4 -- : CL/"* ~ r fe> w 9rai

gt ^ r" . * "

1 -7 - - ~ j£*F f

-8 U-

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1--*••* ••

-^r-11-- ;

^_ HO—• -12: . w• -13:r

-14

1 .-"-1.

10o

CO ^Q a

Lithology Data Q. Q

kY: Grey, Gravel, Soft, No | ^ ^ lr/discoloration ^^^^^^1 -1

1:: ;Of: Grey, Hard, Trace ^^^^H/el.Noodor/discoloration ^^^^^^1 -5

^^^^Ho.o IT"6

^H ^-'i^^^^H ---9^^H -~-™^ • ^H — -11^^^^^^^^H ~~ . _

o.o - -12

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---14

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1Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 1 0.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist. M/W=very moist, W=wet, S=saturated.

1

1

1

1

1

1

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.

Project Name: EconoMail

Project Number: 2001-3495

Project Location: 1834 South 54th Avenue


Ambient Air Temp: 70F

Start/Stop Time:8:00 am - 4:00pm

Date: 05/29/01





0) «

o cMg> z g i

j= 's. ~ -2 co £f c E E 1 O S .Q w 5 2 Lithology Data (L g

—

-1 -

-2-

-3-

-4-

-5-

-6-

-7-

-8-n-y

-10-

-11-

-12-

-13-

-14-

nftipH

tfIPR

IIv'tT:

A

W

W

W

w

NO RECOVERY:

SAND AND CLAY: Yellowsand, Well sorted/graded,Tan clay, Trace gravel,

/ / / / /

/////_/^ ,/1.8

\ Loose.Noodor/discoloration/ ^^^^B\ /muBiCLAY AND SILT: Grey/Tan, ^^^^B °'°Firm, Trace gravel, No HBI Bl

. odor/discoloration >r ^^^^^^\ /

— v

--2

--3

--4

--5

- -6

--7

- -8

o-y

- -10

— 11— -12

--13

--14

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=sligritly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.

Project Name: Morton High Schools


Project Location: Economail

Samples Taken By: GP

Ambient Air Temp: 80 F

Start/Stop Time:7am-3:30pm

Date: 05/24/2001

i I

Boring Number: B-4Drilling Company: Rock & Soil



Boring Location:

I *CO CO

oLithology Data

oCOQEL

o-1-2-3-4-5-6-7-8-9-10---11

-1;

-i-18-+-

-20---2-2-23-+--2-25+--261-

-28—

-30-3-3:-33-+--3*-35

B4-7

D

D

M

M

W

W

W

GRAVEL:Asphaltoverlayingfill Gravel

CLAY AND SILT: Grey SiltyClay. Soft. Very strong odor

CLAY AND SAND: Very littlerecovery. Very soft Gry Claywith Gravel. Strong petrolodor

CLAY AND SAND: Very softGrey Clay with trace graveland sand. Visible oil andsheen on exposed surface.Very strong petrol odor

CLAY AND SILT: Tan andGrey softSilty Clay with tracesand and gravel. No odor

CLAY AND SAND: Very softGrey Clay with trace sandand gravel. No odor. Wellplaced at 13'depth. EOB

0-1-2-3-4-5•6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30

--31--32--33--34--35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-tonization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist, M/W=very moist, W=wet, S=saturated.

I VW^i _ HYGIENEE

1

1

1

1

1

1

1

1

1

\ ^ Project Name: EconoMail BoHng Number 3495-B(mr> Project Number 2001-3495 Drj||jng ^ Roc(< &

p W Project Location: 1 834 South 54th Avenue H T M H- r

^ Samples Taken By: CD T , . . . . , . .^ J Type of Sampling: Soil• Ambient Air Temp: 70F

^ Boring Location: GPS Coord.:RING INC Start/Stop Time:8:00 am -4:00pm

Date: 05/29/01

0)

o

t ECOCO

0 -

-1 -

-2-

-3-

.-5-

-6-

-7-

-9-

-10-

-11-

-12-

-13-

-14-

1C

- Iti >«

%— " -i— -

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0

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« «CO

W

W

A

W

W

z Lithology Data Q.

CLAY: Tan/Black, Trace ^^^^Hgravel, Soft, Loose, No ^^^^^^1odor/discoloration ^^^^^^1

^^^^^^^^HCLAY: Grey/Tan, Trace ^^^^^Hgravel, Firm, No ^^^^H 28 8

odor/discoloration ^^^^^^1

I334^^^^^^^BmpuppnCLAY AND SILT: Grey, Soft, ||tj|im|No odor/discoloration ^^^^^^B

•fl1'5^B^ HE IBfl1 5I

feQ

---1

---2

---3A-4

---5

---6

---7

-o

---9*e\

-\\j

---11._

---13

A f— — -15


•

Boring was backfilled with bentonite chips. Photcnonizatkxi Detector (P.I.O.) scan performed using a Mini Rae equipped with a 1 0.8 eV lamp.Moisture symbols: D= dry, D/M=sligritly moist, M=moist, M/W=very moist, W=wet, S=saturated.

1

1

1

1

1

1

IIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 05/29/01





I ?f i t0) TO «Q co co i Lithology Data

ucoQQ.

u —

-1 --2-

-3-J

-5-

-6-

-7-

-8-

-9-

-10-

-11-

1*>£T

-13-

•1C

„

~"

' '

1 1_

»

„

_

J-

A

D

D

M

M

CLAY: Grey, Gravel, Firm,No odor/discoloration

CLAY: Grey, Tracegravel/Silt, Noodor/discoloration

0

-1-2

-3

-4

-5

-6

-7

-8

-9

-10

-11

-12

-13

-14

-15

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 05/29/01





Ia.9co

3

»a.aco

<aoco

i Lithology Data

0

-1-2

-3

•4

-5

-6

-7

-8

-9

-10-+-

-11-

-12

-1*

-14-

M

M

CLAY: Grey, Trace gravel,Some Silt, Soft, Noodor/discoloration

CLAY: Grey, Some Si It, Firm,No odor/discoloration

NO RECOVERY:

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-kmization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.

Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 05/31/2001




Boring Location:

w

I

Ia«jco

JS3

0)a.a

CO

Iio

Lithology Data

(0uCOoQ.

B-10

D

D

W

W

W

CEMENT: Concrete floor

ASPHALT:ThinAsphattlayer

CLAY: Stiff Grey Clay. Noodor

CLAY: Very soft Grey Clay.Mild petrol odor

BLANK: Refusal at 10'depth.Thick concrete layer. EOB

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.


Project Number 2001-3495





Date: 06/04/2001




Boring Location:

aa

CO

«a.«to

(0(JCO

Lithology Data

0-1-2-3-4-5-6-7-8-9-11-1-1;

-1-1-1-1-1-2-2-2

-3-3-3

-[-_

—

—_

--o1

•H21

31

A4

S1

61

•h-

81

91

JO1

5-H521

53-1

J41

IS1

l^IT2

IB1

291

301

3-H

32-

33-

34-?c

B-11

D

M

M

W

W

W

W

CEMENT: Concrete and\ wood floor /

CLAY: Very soft Grey Claywith trace gravel. No odor.High plasticity

CLAY: Stiff Grey Clay. Noodor. High plasticity. EOB

-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35


IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 06/04/2001

o 5c £

* I

| I |

« I 2




Boring Location:

Lithology Data

3cooQ.

-10--

-26--

-33--

B-12

D

D

D

D

D

W

W

CEMENT: Concrete andwood floor

CLAY: Soft Tan Clay. Slightchemical odor. Highplasticity

CLAY: Black-stained Claywith trace silt. Very Soft.Slight chemical odor. Highplasticity

CLAY: Very soft Tan andBlack Clay. No odor. Highplasticity

CLAY: Very soft Grey Claywith gravel. No odor

CLAY: Very stiff Grey Clay.No odor. EOB

0-1-2-3-4-5-6-7-8

-9-10-11-12-13-14-15-16-17-18-19-20-21-22

-f--23

-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled (M O1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated

.HYGIENEERING, INC.







Date: 06/04/2001




Boring Location:

I

I

I

I

I

I

I

IIIIIIII

I *I I£1"o

co co Lithology Data

tooCOgQ.

B-13


BLANK: No Recovery

CLAY AND SILT: Very softTan/Grey Silty Clay withtrace gravel. Some blackdiscoloration. Strongchemical odor. Highplasticity

CLAY: Very soft Grey Clay.Very strong chemical odor.Very high plasticity. EOB /

3500>10,000

435

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled CMO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=sligntly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 06/04/2001




Boring Location:

Z i!•3 1f \ 1 8

£ o. 1 « w £$ E E | Q "S.Q to to s Lithology Data a. £

O ft

-1 --2--3--4--5-J-b --7--8--9 J

-1O1

-1-H-121

-131

-14--151

-16^•IT

-181

-19--201

-21-22^-23^-241

-251

-26-1

-27-1

-2&1

-29^-301

-3-H-321

-331

-34^-tlV-

-

B-14

W-14(water)

D

D

D

D

D

D

D

W

W

k CEMENT: Concrete floor ,\ /

CLAY: Very soft black-i stained Clay. StrongI chemical odor. High J\ plasticity j

I CLAY AND SILT: Soft Black II Silty Clay. Strong chemical II odor. High plasticity I

CLAY AND SILT: Soft jI Tan/Grey Silty Clay with |I trace gravel. No odor. Low i\ plasticity |

CLAY: Soft Grey Clay. Noodor. High plasticity. Wellplaced at 17'depth.Groundwaterencountered at

\ 13' depth. EOB /

IQQQCQQQEi

^^^H^^^H

0

>400>400

35

>100

>150

20

20

10

u

--1--2--3L-4~--5- -6--7

^-8— --10I- -11L-12L-13--14--15--16

r-174 ft-TO

--19--20--21

oo

--23^ -24--25--26--27--28--29^--30

O-f-0 1

--32L -33- -34

•JC


Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 06/04/2001




Boring Location:

Lithology Data

§COaE

B-15

W


BLANK: No Recovery

CLAY AND SILT: Soft BlackSilty Clay. Slight chemicalodor. High plasticity

CLAY: Soft Tan/G<ey Claywith trace silt and gravel.Mild chemical odor

CLAY AND SILT: Stiff BrownSilty Clay with trace gravel.No odor

CLAY: Grey Clay. Slightpetrol odor. High plasticity.EOB

0-1-2

• -3-4•6-6-7-8•9-10-11-12-13-14-15-16-17-18-19-20-21-22

-f--23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIII1IIIIII

HYGIENEERING, INC.







Date: 06/04/2001




Boring Location:

o

f,o> a

I f t<B (8 mQ CO (0

oLithology Data

oCOoQ.

0-1-2-3-4-5-6-7-8-9-1(-1'-1:-1:-1.-1!-11-r-11-1!

-21-2

-2-2-2-2-2-2-3-3-3-3

O1

21

*-51

fr

7-1

tV91

O1

I1

2^

s1

51

&1

7-8^91

0^1-2-3-(4->K

B-16

D

D

D

D

W

W

W

CEMENT: Concrete and jwood floor n

CLAY: Stiff Grey Clay withtrace gravel. Strong Ichemical odor /I

CLAY AND SILT: Black Silty IClay. Slight chemical odor. /High plasticity /

CLAY: Very Soft Grey Clay. INo odor. High plasticity /]

CLAY AND SILT: Stiff GreyClay. No odor. High ,plasticity. EOB /

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-1ff with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.6 eV lamp.Moisture symbols: D= dry, D/M=sligrrtly moist, M=moist, M/W=very moist, W=wet, S=saturated.

.HYGIENEERING, INC.






Start/Stop Time: 7am-3:30pm

Date: 06/04/2001




Boring Location:

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

«J5

I Eco co

•8"5

Lithology Data

sCOaQ.

0-1-2-3-4-5-6-7-8-9-11-1-1;-1:-1--11-11-r-11-1!-21-2

-3-3:-3-3-35

—

—

—

——n <

•H2^

41

5-j6--h-tV91

O1

-K2^

31

41

51

6-1

IV

&1

to1

CH\2^\^

M--»K

' *Xt

--,

^ .

B-17

D

M

M

W

W

Ww

CEMENT: Concrete and\ wood floor /

CLAY: Soft Brown Clay withtrace silt and gravel. No

.odor. High plasticity

CLAY: Soft Brown Clay withtrace silt and gravel. Strongpetrol odor odor. High

^plasticity i

CLAY: Soft Grey Clay. No\odor. High plasticity /

CLAY AND SILT: Stiff GreyClay. No odor, medium

\ plasticity. EOB /

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIiIiiiiIiiiiIIii

HYGIENEERING, INC.







Date: 07/09/2001




Boring Location:

IIfl) «O CO

*

I

•5Lithology Data

oCOQa

o —.1 _~ 1

-2--3-^-4 —e _•o

-6 —-7--8-^

4 A_-10--11—11

10J—

-154ft—-10

-17-

«A-20-

oo

-23^-241

-25--26^-27-1

-28--29--30--31--32--33--34—1C-

'

B18-8

B18-32

D

D

D

D

W

W

W

W

W

CLAY: Black silty Clay.Petroleum odor

CLAY: Green/Brown Claywith interbedded gravel.Petrol odor

,

CLAY: Brown Clay withinterbedded gravel. No odor

CLAY: Soft Grey Clay withtrace gravel. No odor

CLAY: Hard Grey Clay withtrace gravel. No odor. Wellplaced at 28* depth. EOB


IIII1IIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/09/2001




Boring Location:

a.E

a.E

S%o

Lithology Data

8COQ0.

-10--

-13--

-23--

-26--

B19-5

B19-9

BLANK: No Recovery

CLAY AND SILT: Brown andGrey Silty Soft Clay. Blackdiscoloration. Visible oil onexposed soil. Very strongpetrol odor

CLAY AND SILT: Brown andGrey Silty Soft Clay. Blackdiscoloration. Slight petrolodor

CLAY: Very soft Grey Claywith Brown Silt and tracegravel. No odor

CLAY: Soft Grey Clay withBrown Sift and trace gravel.No odor

CLAY: Stiff Grey Silty Claywith trace gravel. No odor

CLAY: Soft Grey Clay withtrace gravel. No odor. EOB

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35



III1IIIIIIiiIIilIii

HYGIENEERING, INC.


Project Number. 2001-3495





Date: 07/09/2001




Boring Location:

J!

«a

oN

I I

i i

fii"6

Lithology Data

§COQE

o-1-2-3-4-5-6-7-8

-1

-1;-1:-1.-1!-11-1:-11

-3-3;-3:-3-35

H

3-

frj

T2

(

Ih12^31

^

tW7^8^91

O1

•H2-3-1

4-1

K-

1

^J "*"

it,

TS&

~

B20-4

B20-14

D

D

M

M

M

M

M

M

CEMENT: Concrete surface/

CLAY AND SAND: Black iGravelly Clay. Strong petrol /odor /

BLANK: No Recovery f

CLAY AND SILT: Soft Brownand GreySilty Clay with tracegravel. Black discoloration. Jvisible oil on exposed |surfaces. Very strong petrolodor

BLANK: No Recovery

CLAY AND SILT: Brown SiltyClay. Soft. No odor

CLAY: Stiff Grey. Clay. No 1odor. EOB 1

•s.vo

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled a-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonfte chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

I

I

I

I

I

I

I

I

t

I

I

I

I

I

I

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

III

I

s ! tCO CO Lithology Data

§COQQ.


CLAY AND SILT: Black SiltyClay. Strong organic odor

CLAY AND SILT: Brown andGrey Silty Clay. Soft. Strongchemical odor

BLANK: No Recovery

CLAY: Brown Silty Clay.Soft. Strong chemical odor

BLANK: No Recovery

>10,000

>400

>10,000

>10,000

BLANK: Wet sludge. >80%liquid. Very strong chemicalodor

CLAY: Stiff Grey Clay.Strong chemical odor. Wellplaced at 21'depth. EOB

>10,000>10,000

0

-1

-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

I *N I c^ bJ? Z « (0•S 0) 3 AJ

1 I * I Q |Q 5 co s Lrthology Data a. £

0 * »

-

-3--4-

-5--6-7-^-8--9--10

-12—-13^-14^

•IP-TO

-17-18-19--201

1«i_-21--22^-231

-241

-251

-26^-27^-2&1

-291

-301

-3-H-32^-331

-34^•**-

B22-3

B22-15

D

D

W

CEMENT: Concrete and S88888888Iwood floor 1888888883

^ nHBHEila 150CLAY AND SILT: Black Silty ^^^^9 >150

, Clay. Soft. Strong chemical ^^^^^^^9\odor IjBHI

CLAY AND SILT: Brown and BKBP >30°i Grey Silty Clay. Soft. Strong iBBBB|\ chemical odor / ^^^ l >200

\ ' ^^^^^MCLAY AND SAND: Very soft BBBEw Brown Sircy/Sandy Clay with ^^^^H

\ trace gravel. Very strong / ^^^^H|W I \chemical odor /^^^ l80

w I CLAY: Stiff Grey Clay with ^^^^H1 tracegravel. Slightchemical I ^ ^H1 odor . HHHHM

W 11 «^ 11| CLAY: Watery Clay. No odor |

| CLAY: Stiff Grey Clay. No ||odor. EOB

30

W

— -1

— -2--3--4--5— -6

~- -7— -8— -9--10--11— -12— -13--14--15

r-16

— -17--18--19

r-20

O<i— -21--22--23L-24L-25L-26- -27--2B--29--30L-31L-32- -33

r-34— 7K


IIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

2 &•3 1O> Z 4) (0C M 3 0

f i t ! o fa co 5 s Lithology Data Q. &

0 »«

-1 --2--3--4-

-5~-6 —-7--8--9--101

-1-H-121

-13-141

-151

-16-1

-17--1ft1

-191

-2Q1

-2-H-2Z1

-23^-24^-251

-261

-27--2&1

-291

-301

-3V-321

-331

-34-•»«-

;V :

J'-

- i

B23-9

D

D

D

M

M

M

W

W

W

W


/CLAY AND SILT: Black SiltyClay. Soft. Strong chemicalodor ,

CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Soft. Slight chemical jodor /

CLAY AND SAND: Brownand Grey Silty Clay with jSand and trace gravel. Stiff. 1No odor i

ICLAY AND SAND: Very Soft jGrey Sandy Clay. No odor /i

fCLAY AND SAND: Brown jand Grey Silty Clay withSand and trace gravel. Stiff.No odor

CLAY: Soft Grey Clay withtrace sand and gravel. Noodor

CLAY: Stiff Grey Clay withtrace sand and gravel. Noodor. EOB

^SSSSSSSSL50

100

100

>300

300

100

40

3015

50

--1--2--3- -4]--5

-6--7--8

r-8

in

--11--12

r~13

— -14--15--16--17r-18

4A-13

r-20

-21i— -22L-23L-24--25L-26L-27--28L-29L-30L-31--32--337-34— 1C

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

tHYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

o cN 1 C

S 5 ! J_ •— mZ u CO <—

U E 1" - Q U0 to 5 ^ Lrthology Data E S

0 1— r

--2--3--4--5--6 —-7--8-

-8~•irk—-ii/

. -~ •*

-13--14^•llv—

-1«/

-1ft—

-171

-1ft1

-19--201

-2-H-22^

-23--24^-2B1

-2^-27--2ft1

-29--301

-3-H-32--331

-341

•»R-

*j ^

,

r

1

824-Pff"l

12

D

D

W

W

W

W

CEMENT: Concrete and |£88888888iwood floor (888888888

•MI HBMI 550CLAY AND SILT: Black Sitty ^^^^HClay. Soft. Strong chemical ^^^^^Hgenodor , ^ ^ ^1

/ ^^^^•sooCLAY AND SILT: Brown and ^^^HGrey Silty Clay with trace J^^^^^B 10°gravel. Soft. Slightchemical / ^^^^^H

odor ll ^H^SOCLAY AND SAND: Brown l ^^ l 16°Sandy Clay. Stiff. No odor /^^^^•600

/ ^^^^^^^^^^^^H QQflCLAY: Stiff Grey Clay with i ^^^B 50trace gravel. No odor / ^^^^^H

CLAY AND SAND: Stiff Grey HiJ^ B50

Clay with trace sand and igravel. No odor. EOB /

20

V

— -1— -2--3J--4

A— -6~--7- -8'- -9

in- IU

— -11— -121 A

--13

I"'14

4C— -TO

--17--18--19--20--21— -22--23--24- -25--26--27--28--29--30L-31L-32L-33

r-34

— IK


IIriiiiiiiiiiiiiiii

YGIENEERING, INC.







Date: 07/10/2001




Boring Location:

= «

! t5 CBco coo

Lithology Data

8COoQ.

0-1-2-3-4-5-6-7-a-9-1-1-1-1-1-1-1-1

-2

-2;-2

-3-3:-3

—

—

-—

——

o1

•H21

31

4-

5^0

7^8-9:

Vh'•H•21

!3I41

'51

'61

J71

5ft1

591

JO1

J1-1

J2-1

J31

J4^»«-!

•y

' >

B25-7

D

D

M

M

M

M

M

CEMENT: Concrete and Iwood floor n

\CLAY AND SILT: Black Silty 1Clay. Soft. Strong chemical 1

^odor I

CLAY: Soft Grey Clay. Slight j\odor /

CLAY AND SILT: Stiff 1Brown/Grey Sirty Clay. No

\odor /

BLANK: No Recovery

CLAY AND SILT: Brown andGrey Silty Clay with someblackdiscoloration. Stiff. No

I odor. EOB j

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".


IIIIIIII1IIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

^ 3 C

I « 1 st ™~ OB M — fc ^rf

E E o 9 9 -Q to to s Lithology Data Q. 3

0 «

-1--2--3--4--5--6 —

-8--9-

-1-K-12-1

-131

-14--151

-1ft1

-17-1

-1fr

-20--2-H-22--231

-241

-251

-261

-27-1

-28^-29^-301

-3-H-321

-33^-34-1

i -

'">; .

-

B26-7

D

D

D

D

W

W

W

W

W

CEMENT: Concrete andwood floor /

CLAY AND SILT: Black SiltyClay. Stiff. Slight chemicalodor

CLAY AND SILT: Brown andGrey Silty Clay with trace ,gravel. Soft. No odor /

CLAY AND SILT: Brown andGrey Silty Clay with trace ,sand and gravel. Soft. No Iodor |

CLAY AND SAND: BlackSandy Clay with Gravel.Hard. No odor

CLAY: Very soft Grey Clay.No odor

CLAY: Stiff Grey Clay. No 1odor /

CLAY: Hard Grey Clay. Noodor. Well placed at22'depth. EOB

•

I

--2

^-3

--5J--6

7

--6--9--10--11--12--13--14--15

r-16

— -17--18--19

r-20

— -22--23L-24— -25L-26--27L-28L-29--30--31--32L-33--34— IK


IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.




Samples Taken By: GPAmbient Air Temp: 80 F


Date: 07/10/2001

« q>c jo

N i! 1




Boring Location:

Lithology Data

oWaE

o-1-2-3-4-5-6-7-8-9-11-1-1:-13-i-1-i-1

-3-3;-3-3-35

H21

^^

7^ft1

a1

0^•H2^3^41

S1

ft1

71

Q2

Q2

O1

•H21

31

41

f?

B27-13

D

D

W

W

W

W

W

CEMENT: Concrete and Iwood floor n

CLAY AND SILT: Brown and JGrey Sirty Clay. Soft. Slight j\chemical odor fl

CLAY AND SILT: Black Silty IIClay. Stiff. Strong chemicalodor

CLAY AND SILT: Brown andGrey Silty Clay. Stiff. No \odor /

CLAY: Stiff Grey Clay. Noodor. EOB /

0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".

Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.

Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

|

f0)D

SI f! t(0 CBCO CO

2

"5Lithology Data

COoQ.

0-1-2-3-4-5-6-7-8-9-11-1-1:-1:-1.

-r-11-1!-21-2

-3-3:-3

—

—

—

—

—

Q1

-H

21

41

61

T1

ft1

91

O1

•H•2^

4-1

.51

•6-1

•71

5ft1

59^>o-J-HJ2-1

J3-1

J41

>C-

- B28-4

B28-13

D

M

M

W

CEMENT: Concrete and I\ wood floor j\

CLAY AND SILT: Black SiltyClay w'rth trace gravel. Soft, j

\ Slight chemical odor /]

CLAY: Soft Grey Clay. No

yodor ^CLAY AND SILT: Brown and IGrey Silty Clay with tracesnad and gravel. Soft. No j

\odor A-» I

CLAY: Stiff Grey Clay. No ,\odor. EOB /

0-1-2-3-4-5-6-7-ft-9-10-11-12-13-14-15-16-17-18-19-20-21-22

-+--23-24-25-26-27-28-29-30-31-32-33-34-35


IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001

2 1




Boring Location:

• 3 Cg, Z £ «

f i l l S ia 3) to s Lithology Data o. £

0 /\—

_

-2--3 J

-4-je

-O

_

-8--9--10

-11-

-12:•!*»-U

-14-1

-15:-16--171

-1ft1

-191

-201

-21-1

-22^-23^-241

-251

-261

-27—-2ft1

-29--301

-31--32--33--34-

* >

-

-'

B29-10

D

D

M

W

W

W

CEMENT: Concrete and VSSS&SSSSkwood floor /• H^HH\ /•BMICLAY AND SILT: Black Silty ^^^^BClay. Soft. No odor / ^^^^ l

CLAY: Brown and Grey Silty ^^^^HClay. Very soft. No odor. IIB BEOB /

\ /

— -2r-3— -4

e-O

-_ ~*--8— -9

r-10

- -11--12--13--14- -15--16--17--18--19--20--21--22--23--24--25--26~— -27

— -28L-29--30- -31L -32- -33- -34— _7K

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/10/2001




Boring Location:

Lithology Data

c18U

COoQ.

-10--

-20--

B30-M

M


CLAY AND SILT: Black SiltyClay. Soft. Very strongchemical odor

CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Stiff. Very strongchemical odor

CLAY AND SAND: BrownSandy Clay with tracegravel.Stiff. Strong chemical odor

CLAY: Stiff Grey Clay. Verystrong chemical odor. EOB

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

HYGIENEERING, INC.







Date: 07/13/01





No>

a

a«to

I

"oLithology Data

(0o

CO9a.

u —

-1 --2-

-3-

.-5-

-6-

-7-

-a--9-

-10-

1*»£.

-13-

-14-

•tK-

' »

. j

^ A

M

M

CONCRETE:

CLAY: Grey, Soft, Tracegravel, Noodor/discoloration

REFUSAL: Unable toadvance boring

o-1-2

-3

-5

-6-7

-9

-10

-11

-12

-13

-14

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled Of-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/13/2001




Boring Location:

• ^ 3 C0) 2 « (0

1 1 ! 1 z %Q co co S Lithology Data Q. £

O A

-1 --2--3--4--5--6-7 _

-8--9--101

-1-H

-12:

-14-1

-154 A—

-17^

-19--201

-2-H-221

-23^-24-1

-25--26-1

-27-1

-28^-291

-301

-3-H-321

-331

-341

-

B32-3

B32-15

D

D

D

D

D

W

W

W

CEMENT: Concrete andwood floor /

CLAY AND SILT: Black SiltyClay. Soft. Visible oil onexposedsurf ace. Very strongchemical odor /

CLAY AND SILT: Brown andGrey Silty CNy with tracegravel. Soft. Visible sheen Ion exposed surface. Very Istrong chemical odor I

CLAY AND SILT: Brown and IGrey Silty Clay with tracegravel. Soft. No odor I

CLAY AND SAND: Brownand Grey Silty Clay withgravel. Soft. No odor

CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Soft. No odor

CLAY: Soft Grey Clay. Noodor

CLAY: Soft Gravelly Clay.Well-sorted. Poorly-graded.Coarse. No odor

CLAY: Grey Clay with tracegravel. Soft. Slight petrolodor. EOB

s«1

1

5

--1--2--3--4--5--6— .7

--8--9--10--11--12--13

r-14•fC

--16--17--18--19--20

r-21— -22

--23--24--25--26L-27L-28--29

~ -30

tl

- -32L-33

r-34

— •*•;

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-lff with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".


III1IIIIIIIIIIIIIII

HYGIENEERING, INC

Project Name: Morton High Schools Boring Number: B-33

Project Number: 2001-3495 Drj|ljng Company; Roc|< &

Project Location: Economail ^.^ ^ ^

Samples Taken By : GP _ , _ . . _ . .Type of Sampling: SoilAmbient Air Temp: 80 F

Boring Location:Start/Stop Time:7am-3:30pm

Date: 07/1 3/2001

£ £•3 1W Z £ CO

t i l l a iS co co ^ Lrthology Data Q. Q

0 «~[

-1 --2--3--4--5--6--7--8--9 -

-10:-1-H-121

-13-j-14^-15^

-17--18--191

-201

-2-H-221

-231

-241

-251

Oft^

-27--2&1

-29^-301

-311

-321

-331

-341

.':*=-^it&-

i)•*"

%

«.

CEMENT: Concrete. Refusaly at 11 depth. EOB /

^KKfZKKGi --1

--2--3--4--5--6--7--8--9--10- -11- -12--13--14

r-15

--17--18--19--20

r-21

--23*)A-24

--2S--26--27--28--29--30L-31--32L-33L-34

•JC

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0"-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.

IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/13/2001




Boring Location:

1I s

- 1 t * " £o- E E "o Q Q.Q co w 2 Lithology Data £ Q

-2--3--4--5--6-7 _

-8--9--101

-1-H-121

-13--141

-15:

-17-

-19^-201

-2V-22^-231

-241

-251

-26-1

-27-1

-281

-291

-3Q1

-31--32--331

-34^j»^-

B34-5

B34-15

D

D

M

W

W

W

W

W

CEMENT: Concrete andAsphalt floor /

CLAY AND SILT: Brown andGrey Sitty Clay with tracegravel. Soft. Visible oil onexposedsurface.Verystrong jpetrol odor f

CLAY AND SILT: Black SittyClay with trace gravel. VerySoft. Visible thick oil and Isheen on exposed surface. IVery strong petrol odor I

CLAY AND SILT: Brown andGrey Silty Clay with tracesand and gravel. Soft. Slightpetrol odor

CLAY AND SAND: BrownClay with compact sand andtrace gravel. Stiff. Slightpetrol odor

CLAY AND SILT: Brown andGrey Sitty Clay with tracesand and gravel. Soft. Slightpetrol odor

CLAY: Grey Clay with tracegravel. Soft. No odor

CLAY: Grey Clay with tracesand and gravel. Soft. Slightpetrol odor. EOB

^^^^•30

15

2.5

5.0

V

--1--2--3--4~--5

--8--9--10--11--12--13--14

r-15

_ "1"— -17--18--19

r-20

— -22--23L-24— -25--26- -27--28--29'--30

-

-oo

'--34— «


IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/13/2001




Boring Location:

o>

"5.nV)

J!

Q.

CBCO

Iio

Lrthology Data

<Bo(0oQ.

CEMENT: Concrete floor

CLAY AND SILT: Black SittyClay with trace sand andgravel. Soft. Visible oil onexposedsurface.Verystrongpetrol odor

CLAY AND SILT: Brown andGrey Sitty Clay with tracegravel. Very Soft. Visiblethick oil and sheen onexposedsurface.Verystrongpetrol odor

CLAY AND SILT: Brown andGrey Sitty Clay with tracesand and gravel. Soft. Slightpetrol odor

BLANK: No Recovery


o>Q


IIIIIIIIIIIIIIIIIII

HYGIENEERING, INC.







Date: 07/13/2001




Boring Location:

g> Z £ «J

t i l l S fQ to co s Ltthology Data Q. Q

O A—

-1 --2--3--4--5--6-

TT-f

•8-

-9--101

-1-H-121

-131

-141

-15-j<4C_-16-

.-18--19--201

-2-H

-23^-24^-251

-2&1

-27--28^-291

-3rP0*-Oj

-32^-331

-341

7B-

B36-3

B36-15

D

D

W

W

W

W

CEMENT: Concrete floor ^SSSSSSKS^

CLAY AND SILT: Black Sitty ^^^HClay. Soft. Visible oil on HjHHj 120exposedsurface.Verystrong J ^H^ Bpetrol odor /j ^H|H|

CLAY AND SILT: Brown and j ^BHj60

Grey Sitty Clay wtth trace fffmgravel. Very Soft. Visible j ^^^Bthick oil and sheen on I ^ I H 15exposedsurface.Verystrong I ^^^^^Bpetrol odor f^^^^^H

CLAY AND SILT: Brown and j ^^ lGrey Sitty Clay with trace f^^^^Hsand and gravel. Soft. Slightpetrol odor

CLAY: Grey Soft Clay wtthtrace Gravel. No odor


mmmrnHHflHI15

— u

--2--3~--4

r-5

r -®-i-i- -8--9- -10--11--12--13--14

r-15A £-16

— 17- 1 1--18--19--20

r -21

— -22--23--24--25~ -26— -27--28

r ~29L-30

L-32- -33

QC


HYGIENEERING, INC.







Date: 07/13/2001




Boring Location:

O C

f fI ! t* w aa co «

£3

Lithology Data

(0o(0QQ.

f0)Q

u

-1 --2--3-j-4 —•5--6--7--8--9--101

-1-H-1-13-1

-14-1

-151

-161

-17-1

-181O-

-201

-2-H-22—

-231

-2*i2K..

-26^

-27-

-281

-291

-301

-3-H

-32^

-33-

-341

.as-

" r

"

B37-6

B37-19

D I

°D

D

D

D

D

D

D

D

SAND AND SILT: Brown fineSilt with Sand. Loose. Well- jsorted. Poorly-graded. No /I odor /I

, CLAY AND SILT: Black Sitty II Clay wtth trace sand and II gravel. Soft. No odor I

CLAY AND SILT: Brown andGrey Sitty Clay wtth trace Isand and gravel. Soft. No Iodor

CLAY: Soft Grey Clay. No Iodor I

CLAY: Stiff Grey Clay wtthtrace gravel. No odor i

SAND AND SILT: Verticallense of Sand and Silt in stiffGrey soil. No odor. EOB

I

••I— — — _

15

10

160

99

85

5

1.5

u

--1

--2

- -3— .4

— •5- -6

--7

- -8

--9--10

I" -11- -12

r-13

— -14

--15

--16

--17

r-18

•10-|!»

--20--21

--23'--24

-25L-26L-27L-28L-29

--3QL-31L-32

--33

- -34tc

II

COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".

Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slJghtly moist, M=moist, M/W=very moist, W=wet, S=saturated.

B37/MW5$

B38/MW6

BIO

B-


Willowbrook, IL 60521(630) 654-2550

Scale: 1 "=7-1/2'

KEY PLAN

CLIENT:

J. Sterling Morton HighSchool District #201

PROJECT:

Phase II Assessment1840 South 54th AvenueCicero, Illinois

PROJECT NO.:

2001-3628-EBORING LOCATION DRAWING:

1 OF2

Appendix C:

Laboratory Analytical Reports

GREAT

ANALYTICAL1380 Busch Parkway

Buffalo Grove, Illinois 60089Email: [email protected]

(847)808-7766 FAX (847) 808-7772

June 21, 2001

Chris DePaolaHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521

RE: 2001-3495

Dear Chris DePaola

Enclosed are the results of analyses for sample(s) received by the laboratory on June 13, 2001. If you have anyquestions concerning this report, please feel free to contact me.

Sincerely,

Andy JohnsonProject Manager

-A-J GREAT•ll| LAKES-"-^ANALYTICAL

1380 Busch ParkwayBuffalo Grove, Illinois 60089

Email: [email protected](847) 808-7766 FAX (847) 808-7772

Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521

Project: 2001-3495Project Number: N/'A

Project Manager: Chris DePaola

Sampled: 5/29/01Received: 6/13/01Reported: 6/21/01 14:00

ANALYTICAL REPORT FOR SAMPLES:

Sample Description Laboratory Sample Number Sample Matrix Date Sampled

3495-B4 B106231-01 Soil 5/29/01

Great Lakes Analytical

Andy'Jonnson, Project Manager

The results in this report appl\' to the samples anatvzed in accordance with the chain of custody documentThis analytical report must be reproduced in us entirely

Page 1 of

»». lli,. •viml±1

GREATLAKESANALYTICAL



I Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521

Project: 2001-3495Project Number: N/A


Sampled: 5-29/01Received: 6,13/01Reported: 6/21/01 14:00

Total Petroleum Hydrocarbons as Diesel by EPA 8015MGreat Lakes Analytical—Oak Creek

• Analyte

*3495-B4Diesel

BatchNumber

1060038

DatePrepared

6/18/01

DateAnalyzed

SurrogateLimits

B106231-016/18/01

ReportingLimit

255

Result

708

Units

Soilmg/kg

Notes*

G1.G12.G15T10J15J8

Great Lakes Analytical *Refer to end of report lor text of notes and definitions.

Andy Johnson, Project Manager Page 2 of 5




Hygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521



Sampled: 5/29,01Received: 6/13/01Reported: 6/21/01 14:00

Dry Weight DeterminationGreat Lakes Analytical

Sample Name

3495-B4

Lab ID

B106231-01

Matrix

Soil

Result Units

90.0 %


Andy Jonnson, Project Manager Page 3 of

. •GREATLAKESANALYTICAL




Project:Project Number:

Project Manager:

2001-3495N/AChris DePaola

Sampled: 5,29,01Received: 6.13/01Reported: 6,21/01 14:00

Total Petroleum Hydrocarbons as Diesel by EPA 8015M/Quality Control' Great Lakes Analytical—Oak Creek

I Analyte

'Batch: 1060038Blank| Diesel

LCS

1Diesel

Matrix SpikeDiesel

[ Matrix Spike PupDiesel

Date SpikeAnalyzed Level

Date Prepared: 6/18/011060038-BLK16/18/01

1060038-BS16/18/01 37.1

SampleResult

QCResult Units

ReportingRecov.

LimitLimits

Recov. RPD RPD% Limit % Notes*

Extraction Method: EPA 3550B

ND

30.8

nig/kg

mg/kg

5.00

36.0-120 83.0

1060038-MS1 B106231-016/18/01 35.4 708

1060038-MSD1 B106231-016/18/01 34.4 708

461

366

mg/kg

mg/kg

10.0-160

10.0-160

NR

NR 30.0 -35

GrealftLakes Analytical

Andy Johnson, Project Manager

'Refer lo end of report for text of notes anil definitions.

Page 4 of 5

GREATLAI\to 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

Hygieneering, Inc. Project: 2001-3495 Sampled: 5/29/017575 Plaza Court Project Number: N/A Received: 6,13/01Willowbrook, IL 60521 Project Manager: Chris DePaola Reported: 6.21/01 14:00

Notes and Definitions

Note

Gl The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.

Gl 2 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.

G15 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.

T10 Diesel Range

Tl 5 Late Elevated Baseline

T8 Diesel Pattern

DET Analyte DETECTED

ND Analyte NOT DETECTED at or above the reporting l imit

NR Not Reported

dry Sample results reported on a dry weight basis

Recov. Recovery

RPD Relative Percent Difference


Andy Johnson. Project Manager Page 5 of



Email: [email protected](847)808-7766 FAX (847) 808-7772

June 12, 2001

Chris DePaolaHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521

RE: 200 1-3495

Dear Chris DePaola

Enclosed are the results or analyses for sample(s) received by the laboratory on May 30, 2001 . If you have anyquestions concerning this report, please feel free to contact me.

Sincerely,



1380 Busch ParkwayBuffalo Grove, Illinois 60089jfjalo


Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521



Sampled: 5,29,01Received: 5/30/01Reported: 6/12/01 13:57



3495-B1

3495-B4

3495-B5

3495-B7

B105425-01

Bl05425-02

B105425-03

B105425-04

Soil

Soil

Soil

Soil

5,29,01

5/29/01

5,29/01

5,29/01

Great Ivikes Analytical

I\LAndy Johnson, Project Manager

The results in this report apply to the samples analyzed in accordance \\ith the chain of custody documentThis analytical report must be reproduced in its entirety

Page 1 of 2

-_±^t*it.'iAi>*. ^H

$1_;;«• GREAT

LAKES(ANALYTICAL 1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772



Project Manager: Gary Milkeris


TCLP Metals by EPA 1311/6000/7000 Series MethodsGreat Lakes Analytical

Analyte

B-10 Sign ShopArsenicBariumCadmiumChromiumSeleniumSilverLeadMercury

BatchNumber

DatePrepared

DateAnalyzed

SpecificMethod

ReportingLimit Result

B106039-021060130n

"tit >""1060137

6/8/0111

"""11

11

6/12/01

6/U/01"«""11

6/8/016/12/01

EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421EPA 7470A

0.1001.00

0.00500O.I 000.100

0.05000.00500

0.000200

ND.NDNDNDNDND

0.0271ND

Units

Soilmg/111

""""11

"

Notes

G15.G

I

I

I Great Lakes Analytical

And Johnson, Project Manager

*Refer to end of report for text of notes and definitions

Page 2 of 2




I1JHygieneering, Inc.

7575 Plaza CourtWillowbrook. IL 60521

Analvte

3495-B1Arsenic

1BariumCadmiumChromiumLead

1SeleniumSilverMercury

I3495-B4ArsenicBarium

1CadmiumChromiumLeadSelenium

•SilverMercury

^3495-65•Arsenic

BariumCadmium

1ChromiumLeadSeleniumSilver

•Mercury

3495-B7•ArseniciBarium

CadmiumChromium

iLead^Selenium

Silver•Mercury

I*Great Lafces Analytical

I/ i A/ l /U-



Total Metals by EPA 6000/7000 SeriesGreat Lakes Analytical

Batch Date Date SpecificNumber Prepared Analyzed Method

Bl 05425-011050635 5/31/01 5/31/01 EPA6010B

EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OB

1060077 6/6/01 6/6/01 EPA7471A

Bl 05425-021050635 5/31/01 5/31/01 EPA6010B


1060077 6/6/01 6/6/01 EPA7471A

B105425-031050635 5/31/01 5/31/01 EPA60IOB


1060077 6/6/01 6/6/01 E P A 7 4 7 1 A

Bl 05425-041050635 5 ,31 /01 5,31/01 EPA6010B

EPA 601 OBEPA 601 OBEPA 601 OBEPA 6(11 OBEPA 601 OBEPA 601 OB

1060077 6 /601 6,6,01 E P A 7 4 7 1 A

Methods

ReportingLimit

2.5025.0

0.5000.500

1.002.502.50

0.0400

2.5025.0

0.5000.500

1.002.502.50

0.0400

2.5025.0

0.5000.500

1 .002.502.50

0.0400

2.5025.0

0.5000.500

1.002.502.5(1

0.0400

Sampled: 5/29/01Received. 530/01Reported: 6/12/01 13:57

Result Units Notes*

SoilND mg/kgNDND

9.1912.0NDND " G2ND " G15

SoilND mg/kg

59.8ND

8.9879.6 - "NDND " G2

0.119 " G15

SoilND mg/kgNDND12.36.62NDND " G2ND " G15

SoilND mg/kgNDND

13.09.67NDND " G2ND " G15

*Refer to end of report for text of notes and definitions

"Andy Jonnson, Project Manager Page 2 of 21

I





Analvte

3495-B4AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole


Project Manager. Chris DePaola

Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical

Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit

B105425-021060031 6/4/01 6/5/01 1000

200010001000900

1000100010001000900

100010001000100010001000

29.0-132

Sampled: 5,29,01Received: 5/30/01Reported: 6,12.01 13:57

Result Units Note?

Soil G12ND ug/kgNDNDNDNDNDNDNDNDND

1040NDNDND

1600NDAT? % O5

Great Lafces Analytical


'Refer to end of report for text of notes and definino

Page 3 ol




11

I Hygieneering, Inc.J 75 75 Plaza Court•JWillowbrook. IL 60521

•

Analvte

3495-B1Acetone

1BenzeneBromodichloromethaneBromoformBromomethane

12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene

•ChlorodibromomethaneIchloroethane

Chloroform

IChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene

|cis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropane

Icis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

1Methylene chloride

4-Methyl-2-pentanoneStyrene1,1 ,2.2-Tetrachloroethane

jTetrachloroethene[Toluene

1,1,1-Trichloroethane

11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

fVinyl chloride[Total XylenesSurrogate: DibromofluoromellianeSurrogate: 1 . 2-Dichtoroethuiw-d4



Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical


Bl 05425-011060024 6/1/01 6/2/01 25.0

5.005.005.005.0010.05.005.005.005.002505.005.00250

5.005.002505.005.005.005.005.0010.05.0010.05.005.005.00

250005.005.005.0(15.0010.0250

5.0081.2-1*45U.X-I45

Sampled: 5,29,01Received: 530/01Reported: 6,12,01 13:57

Result Units Notes*

Soil45.7 ug/kg A42.7NDNDND

36.3 " 1NDNDNDND

4410 " G12NDND

1110 " G128.2519.1902 " G12256NDNDND15.1ND

37.6 " 2NDNDNDND

130000 " G1226.1 " G3NDNDNDND861 " G12

44.1114 "/:,

115

'Great Lakes^Airalvtical

And>'Johnson, Project Manager

"Refer to end of report for text of notes and definitions.

Page 4 of 21

£.-«w._ Hsv&mliil





Project: 2001-3495 Sampled: 5,29/01Project Number: N/A Received: 5/30/01

Project Manager: Chris DePaola Reported: 6 / 1 2 0 1 1 3 : 5 7


Analvte

3495-B1 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*

B105425-01 SoilJ 060024 6/1/01 6/2/01 82.0-121 101 %

76.8-113 73.4 " O4


And>'Johnson. Project Manager

"Refer to end of report for text of notes and definition:

Page 5 of!

I GREATLAKESANALYTICAL



11

Hygieneering, Inc.7575 Plaza Court| Willowbrook. IL 605211

Analvte

1 3495-B4Acetone

_ BenzeneM Bromodichloromethane• Bromoform

Bromomethane


I chlorodibromomethaneChloroethaneChloroform

IChloromethane1.1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethene

I cis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane

. cis-l,3-Dichloropropene| trans- 1 ,3-Dichloropropene1 Ethylbenzene

2-Hexanone• Methylene chloride

1 4-Methyl-2-pentanoneStyrenc1 , 1 ,2,2-Tetrachloroethane

i Tetrachloroethene[ Toluene

1,1.1 -Trich loroethane• 1,1 ,2-Trichloroethane1 Trichloroethene' Trichlorofluoromethane

Vinyl acetateVinyl chlorideTotal XylenusSurrogate: DibromofluoromethaneSurrogate: 1 .2-DicMoroelhane-d4

\ ,. .. .





Bl 05425-021060024 6/1/01 6/7/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-1*450.K-I4?

Sampled: 5,29/01Received: 5,30/01Reported: 6,12,01 13:57

Result Units Notes*

Soil36.7 ug/kg ANDNDNDND15.7 " 1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " G3NDNDNDNDNDND12(1 "/„

120

Great Lakes Analyticalrcat Lak

Andy Johnson. Project Manager

"Refer l<> end of report for text of notes and definitions.

Page 6 of 21

. H|l




Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL60521

Analyte

3495-B4 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Project: 2001-3495 Sampled: 5/29,01Project Number: N/A Received: 5,30/01

Project Manager: Chris DePaola Reported: 6 /120113 :57


Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes"

B105425-02 Soil1060024 6/1/01 6/7/01 82.0-121 105 %

76.8-113 93.5

Great Lakfls Analytical


Refer to end of report for text of notes and definition

Page 7 of :




iHygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521

11

lAnalvte

•3495-B5Acetone

1BenzeneBromodichloromethaneBromoformBromomethane

l2-Butanone(Carbon disulfide

Carbon tetrachloride-Chlorobenzene•Chlorodibromomethane•Chloroethane

Chloroform

IChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene

|cis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropane

|Cis-l,3-DichloropropeneItrans- 1 ,3-Dichloropropene*Ethylbenzene2-Hexanone

iMethylene chloride|4-Methyl-2-pentanoneStyrene1 ,1 ,2.2-Tetrachloroethane

[Tetrachloroethene•Toluene1,1,1-Trichloroethane11,1,2-TrichloroethaneJTrichloroetheneTrichlorofluoromethaneVinyl acetate[Vinyl chloride[Total XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroelhane-d4





B105425-031060024 6/1/01 6/2/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.002505.005.002505.005.005.005.005.0010.05.0010.05.005.005.005.005.005.002505.0010.05.005.00

81.2-1*450.8-145

Sampled: 5,29/01Received: 5/30/01Reported: 6.12/01 13:57

Result Units Notes*

SoilND ug/kgNDNDNDND

18.5 " INDNDNDNDNDNDND

2300 " G127.2546.25530 " G12230NDNDNDNDNDNDNDNDNDNDND247 " G3ND

8160 " G12NDND261ND112 "/„in

Great Lal/es Analytical

Andy JVnmson, Project Manager

"Refer to end <>/ report for text of notes and definitions.

Page 8 of 21




Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521



Sampled:Received:Reported:

5,29/015/30/016,' 12/01 13:57


Analvte

3495-B5 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene


B105425-03~~1060024 6/1/01 6/2/01 82.0-121

76.8-11*

Result

86.373.0

Units Notes*

Soil%

04

Great Uakes Analytical "Refer to end of report for text of notes and definnioi.

And\ l Johnson, Project Manager Page 9 of




I1

j Hygieneering, Inc.J 75 75 Plaza CourtBJWillowbrook, IL6052I

•

Analvte

3495-B7Acetone

_ Benzene• Bromodichloromethane• Bromoform

Bromomethane

12-ButanoneCarbon disulfldeCarbon tetrachlorideChlorobenzene

HChlorodibromomethane• Chloroethane

Chloroform

tChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene

Icis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane

Icis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

1Methylene chloride

4-Methyl-2-pentanoneStyrene1 .1 ,2,2-Tetrachloroethane

ITetrachloroetheneToluene1,1,1 -Trichloroethane

11,1.2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

(Vinyl chlorideTotal XylenesSurrogate: Dibromofluoroinelliane

-Surrogate: 1 .2-Dichloroethane-d4





B105425-041060024 6/1/01 6/2/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

X 1.2 -1*4

50. 8- 145

Sampled: 5,29,01Received: 5,30/01Reported: 6 12,01 13:57

Result Units Notes*

SoilND ug/kgNDNDNDND

12.8 " 1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " G3NDNDNDNDNDND112 "/„1/2

Great Stakes Analytical "Refer to end of report for text of notes and definition*.

Andy Johnson. Project Manager Page 10 of 21



.Email: [email protected](847)808-7766 FAX (847) 808-7772



Project Manaeer: Chris DePaola


5,29/015/30/016/12.01 13:57


Analvte

3495-B7 (continued)Surrogate: Toluene-d8Surrogate: 4-Broinofluorobenzene


B105425-041060024 6/1/01 6/2/01 82.0-121

76.8-113

Result

92. 189.2

Units Notes*

Soil%



"Refer to end of report for text of notes and definition

Page 1 1 of




iI Hygieneering, Inc.

•7575 Plaza CourtJWillowbrook. IL 60521



Sampled: 5,29/01Received: 530/01Reported: 6 12/01 13:57

IDry Weight Determination


lampleName Lab ID Matrix Result Units

I

I

I

I

I

I

I

I

I

B105425-01

Bl 05425-02

B105425-03

B105425-04

Soil

Soil

Soil

Soil

80.9

90.0

78.9

83.0


I //A-AnuV JoTinson, Project Manager

I

Pane 12 of 21







Sampled: 5,29,01Received: 5,30,01Reported: 6,12,01 13:57

Total Metals by EPA 6000/7000 Series Methods/Quality ControlGreat Lakes Analytical

Analvte

Batch: 1050635

DateAnalyzed

Date Prepa

SpikeLevel

red: 5/31/0

SampleResult

1

QCResult

Reporting Limit Recov.Units Recov. Limits %


RPDLimit

RPD% Notes*

BlankArsenicBariumCadmiumChromiumLeadSeleniumSilver

1050635-BLK15/31/01

ArsenicBariumCadmiumChromiumLeadSeleniumSilver

Matrix SpikeArsenicBariumCadmiumChromiumLeadSeleniumSilver

Matrix Spike PupArsenicBariumCadmiumChromiumLeadSeleniumSilver

1050635-BS15/31/01 106

20020020020156.0200

1050635-MS15/31/01 105

198198198199

55.4198

Bl 05382-01ND

36.1ND

9.465.66NDND

1050635-MSD15/31/01 106

200200200

20156.0200

B 105382-01

ND36.1ND

9.465.66NDND

NDNDNDNDNDNDND

10819820019720155.2147

77.9191146159156

41.618.7

84.3202155169167

44.1I 1.8

mg/kg

mg/kg

mg/kg

mg,kg

2.5025.0

0.5000.500

1.002.502.50

81.1-12172.9-12174.3-11872.2-12172.2-12173.1-12010.0-155

53.1-11754.3-11152.5-10843.3-11543.3-11547.3-11310.0-117

10299.0100

98.5100

98.673.5

74.278.273.775.575.575:1

9.44

53.1-54.3-52.5-43.3-43.3-47.3-10.0-

17110815151317

79.583.077.579.880.378.75.90

26.728.824.924.1

24.125.347.0

6.905.965.035.546.164.6846.2

Great LAkes Analytical "Refer to end of report for text of notes and definitions.

An/ly Johnson, Project Manager Page 13 of 21

I

I

aSL. ,«a-- •vAmH

SSlGREATLAKESANALYTICAL



I Hygieneering, Inc.J?575 Plaza Court•Willowbrook.lL 60521

•



Sampled: 5/29/01Received: 530/01Reported: 6,12/01 13:57

Total Metals by EPA 6000/7000 Series Methods/Quality Control

lAnalyte

•Batch: 1060077Blank

1Mercury

LCSMercury

Matrix SpikeMercury


Date Spike Sample QCAnalvzed Level Result Result

Date Prepared: 6/6/011060077-BLK16/6/01 ND

1060077-BS16/6/01 0.200 0.188

1060077-MS1 B105425-016/6/01 0.200 ND 0.274

Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*

Extraction Method: EPA 7471 A

mg/kg 0.0400

mg/kg 71.9-126 94.0

mg/kg 38.3-154 137

•M

I

I

I

I

I

I

I

Matrix Spike Pup

reat Latfes Analyt ical

1060077-MSD1 B105425-016/6/01 0.156 ND 0.173 mg/kg 38.3-154 111 9.52 21.0

IAndy Johnson. Project Manager

Refer to end of report for text of notes and definitions.

Page 14 of 21





Analvte

Batch: 1060031BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

t



Polynuclear Aromatic Compounds byGreat Lakes

Date Spike SampleAnalyzed Level Result


11

""ii"11

n11

11

n"n

11

"

' 17.1

1 06003 1-BS16/5/01 67.0

67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.7

EPA MethodAnalytical

QCResult

Sampled: 5,29,01Received: 5/3001Reported: 6,12,01 13:57

8310/Quality Control

Reporting LimitUnits Recov. Limits

Recov. RPD RPD% Limit % Notes'


NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

9.28

58.495.066.266.251.072.572.562.268.774.660.736.469.558.166.374.115.2

ug/kg 100200100100

90.0100100100100

90.0100100100100100100

29.0-132

ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132

54.3

87.2142

98.898.876.1108I OK

92.81031 1 1

90.654.3104

86.799.0

I I I91.0

GreatX-.akes Analytical

A»dy Johnson, Project Manager

"Refer to end of report for text of notes and definition*

Page 15 of 2




11


• Willowbrook, IL 60521

1*\

(Analvte

Matrix SpikeAcenaphthene

1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene

1Benzo (b) ttuorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChrysene

I Dibenz (a,h) anthracene• Fluoranthene

Fluorene

1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene

( Surrogate: Carbazole

Matrix Spike Pup

1AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene

1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene

• Chrysene• Dibenz (a,h) anthracene

Fluoranthene

1FluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrene

1PyreneSurrogate: Carbazole

1 <



Sampled: 5,29/01Received: 5,30/01Reported: 6 12/01 13:57

Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical


SampleResult

QC Reporting LimitResult Units Recov. Limits

Recov. RPDLimit

RPD% Notes*

1060031-MS1 B105439-016/5/01 64.6

64.664.664.664.664.664.664.664.664.664.664.664.664.664.664.616.2

1 06003 1-MSD16/5/01 67.6

67.667.667.667.667.667.667.667.667.667.667.667.667.667.667.616.9


B 105439-01NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

36.0 ug/kg84.841.136.635.243.437.640.348.042.640.342.534.040.444.836.511.5

49.8 ug/kg104

54.148.449.356.244.055.670.057.562.560.047.454.456.549.614.6

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

10.0-15410.0-17610.0-1 1410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

55.7131

63.656.754.567.258.262.474.365.962.465.852.662.569.356.571.0

73.7154

80.071.672.983.165.182.2104

85.192.588.870.180.583.673.4N6.4

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

27.816.122.823.228.921.211.227.433.325.438.929.828.525.218.726.0

'Great ,tibkes Analytical

\AAndy Johnson. Project Manager

"Refer to end of report for text of notes ami definitions.

Page 16 of 21







Sampled: 5/29/01Received: 5/30/01Reported: 6,12/01 13:57

Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical

Date Spike SampleAnalvte Analyzed Level Result

Batch: 1060024 Date Prepared: 6/1/01Blank 1060024-BLK1Acetone 6/1/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachlorideChlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethene "cis-l,2-Dichloroethene "trans- 1,2-Dichloroethene "1 ,2-Dichloropropane "cis-1 ,3-Dichloropropene "trans- 1,3-Dichloropropene "Ethylbenzene2-HexanoneMethylene chloride "4-Methyl-2-pentanone "Styrene "1,1,2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1,1,1-Trichloroethane "1 , 1 ,2-Trichloroethane "Trichloroethene "Trichlorottuoromethane "Vinyl acetate "Vinyl chlorideTotal XylenesSurrogate: Dibrotnofluoromethane " 50.0

QCResult

NDNDNDNDND

11.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

8.71NDNDNDNDNDNDNDNDNDNDNDND

52. 1

Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notc<

Extraction Method: EPA 5035B [P/T]

ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-1*4 104

Great Lakes Analytical Refer to end of report for text of notes and definition.

AndV Johnson, Project Manager Page 17 of!



Email. info@glalabs com(847) 808-7766 FAX (847) 808-7772

11

Hygieneering, Inc.7575 Plaza Court| Willowbrook. 1L 60521

•



Sampled: 5/29/01Received: 5,30/01Reported: 6,12/01 13:57

Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control

Analvte

1 Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4

1Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCS

1AcetoneBenzeneBromodichloromethaneBromoform

H BromomethaneH 2-Butanone

Carbon disultlde

1Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane

1ChloroformChloromethane1,1 -Dichloroethane

11 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene

11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene

• 2-Hexanone• Methylene chloride

4-Methyl-2-pentanone

ISryrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene

11,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroethenc

_ Trichlorofluoromethane

Great Lakes


1060024-BLK16/1/01 50.0

50.050.0

1060024-BS16/1/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

Analytical

QCResult

48.446.946.0

45.545.150.749.558.655.050.762.858.353.4115

55.036.650.360.454.555.361.246.647.650.051.217.752.934.655.443.155.748.264.248.X53.161.4


ug/kg 50.8-14582.0-12176.8-11*

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-142641-13460.0-13476.4-12561.8-132140-241


96.893.892.0

91.090.2101

99.01 1 7110101126117107NR110

73.210112110911 1122

93.295.2100102

35.4106

69.21 1 1

86.21 1 1

964128

97.6106123

1 Great Ldkes Analytical

IAndy Johnson, Project Manager

I

"Refer to end of report /or text of notes and definitions.

Page 18 of 21







Sampled: 5,29,01Received: 530,01Reported: 6 12.01 13:57


Analyte

LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1.1-Dichloroethenecis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 .1 ,2.2-TetrachloroethaneTetrachloroetheneToluene


1060024-BS16/1/01 50.0

50.0150

50.050.050.050.0

1060024-BSD16/2/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.05(1.0

QC Reporting LimitResult Units

29.3 ug/kg41.5168

'53.752.948.045.3

39.8 ug/kg49.355.052.158.454.157.868.460.857.5119

59.335.257.862.160.060.267.751.250.15 1 . 153.617.259.735.957.046.958.152.1

Recov. Limits

10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-1752X.4-14910.0-1X864.6-1366X.4-13757.6-14264.1-134

riecov.%

58.683.0112107106

96.090.6

79.698.6110104117108116137122115NR119

70.4l l t >124120120135102100102107

34.41 19

7 1 . X1 14

93.X1 1 6104

RPDLimit

34541.442.057.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7

I 2 X67.4

1 1 937.254.646.342. (i

RPD% Notes'

13.48.908.534.93

01.8313.88.374.187.213.427.863.9013.82.459.617.7910.19.024.921.984.782.X71 1 . 63.692.d78.444.417.5X

Great Lakes Analytical "Refer to end of report for text of notes and definitions.

_LAndy Johnson, Project Manager Page 19 of 2

GREAT^^ 1380 Busch Parkway Email: [email protected]

ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

I

I

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Sampled: 5,29/01Received: 5,30/01Reported: 6,12/01 13:57


•J Analyte

* LCS Pup (continued)1,1,1 -Tri Chloroethane

11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane

_ Vinyl acetate• Vinyl chlorideB Total Xylenes

Surrogate: DibromofluoromethaneISurrogi. 'e: 1 ,2-Dichloroethane-d4

Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1

1

1

1

1

1

1

1Great Lakts Analytical

1 /L—1 , __


1

Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes

1060024-BSD16/2/01 50.0 68.7 ug/kg 60.0-134 137 44.2 6.79

50.0 52.9 " 76.4-125 106 53.2 8.2550.0 57.3 " 61.8-132 115 43.5 8.1450.0 56.7 " 14.6-241 113 115 8.4750.0 31.2 " 10.0-161 62.4 92.1 6.2850.0 40.2 " 57.9-143 80.4 81.0 3.18150 174 " 60.0-141 116 40.1 3.51

50.0 54.4 " 81.2-1*4 10950.0 50.9 " 50.8-145 10250.0 48.1 " 82.0-121 96.250.0 45.8 " 76.8-113 91.6

"Refer to end of report for text of notes and definitions

Page 20 of 2







Sampled: 5,29/01Received: 530-01Reported: 6.1201 13:57


Note

A The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.

G12 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.


G2 The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.

G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'.'established acceptance criteria. Refer to the included QC reports for more detail.

04 The recovery for this analyte is below the laboratory's established acceptance criteria.

05 The recovery for this analyte is above the laboratory's established acceptance criteria.

1 The method blank associated with this sample contains 11.6ppb of this analyte.

2 The method blank associated with this sample contains 8.71ppb of this analyte.


ND Analyte NOT DETECTED at or above the reporting l imit

NR Not Reported


Recov. Recovery


Great LakeyAnalytical,

And^Johnson, Project Manager Page 21 of 21

GREATLHl\CO


Buffalo Grove, Illinois 60089Email: info@glalabs com

(847) 808-7766 FAX (847) 808-7772

June 13, 2001

Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521

—

•

•

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RE: 2001 -3495

Dear Gary Milkeris

Enclosed are the results of analyses for sample(s) received by the laboratory on June 1 , 2001 . If you have anyquestions concerning this report, please feel free to contact me.

Sincerely,


&.*L . i £v_ ^H

ivAviB

•§••




Hygieneering, Inc.7575 Plaza CourtWiliowbrook. IL 60521



Sampled: 5,31/01Received: 6.1/01Reported: 613-0107:44



B-4 Outside Parking Lot

B-10 Sign Shop

B106039-01

Bl 06039-02

Water

Soil

5,31/01

5/31/01

Greatf Lakes Analytical The results in this report apply to the samples analyzed in accordance \vilh the chain of custody document.This analytical report must be reproduced in us entirety.


LAKESANALYTICAL



11

1 Hygieneering, Inc.J 75 75 Plaza Court•Willowbrook. IL 60521

•

•

| Analyte

^B-4 Outside Parking LotAcetone

^Benzene•Bromodichloromethane•Bromoform

Bromomethane•2-ButanoneBCarbon disultlde

Carbon tetrachloride—Chlorobenzene•Chlorodibromomethane•Chloroethane

Chloroform

f hloromethane1 -Dichloroethane

i ,2-Dichloroethane1,1-Dichloroethene

§is- 1 ,2-Dichloroethene•ans-1 ,2-Dichloroethene

1 ,2-Dichloropropane^;is-l ,3-Dichloropropene«rans-l ,3-Dichloropropene^fethylbenzene

2-Hexanone

Fethylene chlorideMethyl-2-pentanone

Styrene1 , 1 ,2,2-Tetrachloroethane

•1 etrachloroethene•Toluene

1,1 ,1 -TrichloroethaneM! , 1 ,2-Trichloroethane•Trich 1 oroeth en c^^"rich lorofl uoromethane

Vinyl acetate

§inyl chlorideotal Xylenes

Surrogate: Dibromofluoromelhane^surrogate: l.2-Dichloroethane-d4



Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical


Bl 06039-011060128 6/7/01 6/8/01 10.0

2.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00

9 1 . / - / I I

X5.I-IM

Sampled: 5/31/01Received: 6. 1/01Reported: 6,13/01 07:44

Result Units Notes*

Water G15ND ug,INDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDitr %HI 5 " O5

rcat L; kes Analytical

iAndy Johnson, Project Manager


Page 3 of 2 1

I

femal







Sampled: 5,31,01Received: 61 /01Reported: 6.13,01 07:44


AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits

ReportingLimit Result Units Notes*

B-4 Outside Parking Lot (continued')Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060128 6/7/01B106039-01

6/8/01 95.1-10589.6-105

Water106

99.4

CIS05

Great/Lakes Analytical "Refer to end of report for text of notes and definitions.


1 K:,A<~| GREATfill LAKES

- •&•• ANALYTICAL•11

1 Hygieneering, Inc.J?575 Plaza Court•Willowbrook, IL 60521

•

Analvte

B-4 Outside Parking LotAcenaphthene

•Acenaphthylene•Anthracene*Benz (a) anthracene

Benzo (a) pyrene•Benzo (b) fluoranthenejBenzo (ghi) perylene

Benzo (k) fluoranthene^Chrysene•Dibenz (a,h) anthraceneBpluoranthene

Fluorene•Indeno (1,2,3-cd) pyrene•Naphthalene^rhenanthrene

Pyrene•Surrogate: Carbazole

1

1

1

1

1

••brapt Lakes Analytical

1380 Busch Parkway Email: [email protected] Grove, I l l inois 60089 (847) 808-7766 FAX (847) 808-7772

Project: 2001-3495 Sampled: 5 3 1 , 0 1Project Number: N/A Received: 6/1/01

Project Manager: Gary Milkeris Reported: 6/130107:44



B106039-01 Water G12.G31060075 6/6/01 6/7/01 25.0 ND ug,l

25.0 ND25.0 ND

0.500 ND0.500 3.250.500 4.16

25.0 ND0.500 1.13

5.00 10.00.500 ND

25.0 48.125.0 ND1.00 2.0125.0 ND25.0 61.825.0 ND

24.5-122 93.2 "A,



I





Analyte

B-10 Sign ShopAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1 , 1 ,2.2-TetrachloroethaneTetrach loroetheneToluene1.1,1 -Trichloroethane1 , 1 ,2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroelhane-d4

Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris



B106039-021060123 6/7/01 6/9/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.02505.00

81.2-1*450. N- 145

Sampled: 5/31.01Received: 6.1/01Reported: 6 /13 01 07:44

Result Units Notes*

Soil66.0 ug/kg ANDNDNDND14.0 " A8.58NDNDNDNDNDNDND205ND11.2NDNDNDNDNDNDNDNDNDND17.1NDNDND

5.02NDND

1060 " G12ND104 "/,,108




Page 6 of 2



Email [email protected](847) 808-7766 FAX (847) 808-7772

IHygieneering, Inc.

J7575 Plaza CourtWillowbrook. IL 60521



Sampled: 5,31-01Received: 6,1,01Reported: 6 13,01 07:44



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Sign Shop (continued')Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060123 6/7/01Bl 06039-02

6/9/01 82.0-12176.8-113

98.975.8

Soil%

O4

Great Makes Analytical

I/

I



Page 7 of 21







Sampled: 5,31/01Received: 6.1/01Reported: 6,13/01 07:44

TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality ControlGreat Lakes Analytical

Analvte

Batch: 1060130BlankArsenicBariumCadmiumChromiumSeleniumSilverLead



""""

6/8/01

QCResult

NDNDNDNDNDNDND


Extraction Method: EPA 3015

mg/1 0.1001.00

0.005000.1000.100

0.05000.00500

LCSArsenicBariumCadmiumChromiumSeleniumSilverLead

Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilverLead

Matrix Spike PupArsenicBariumCadmiumChromiumSeleniumSilverLead

1060130-BS16/11/01 2.00

2.001 .002.001 .001 .00

6/8/01 0.0240

1060130-MS16/11/01 2.00

2.001.002.001.001 .00

6/8/01 0.0240

1060130-MSD16/11/01 2.00

2.001.002.001 .001.00

6/8/01 0.0240

Bl 06023-01NDND

0.0528NDNDND

0.281

Bl 06023-01NDND

0.0528NDNDND

0.281

2.092.071.012.041.02

0.9720.0255

2.103.071.062.011.09

0.3600.253

2.083.021.031.971.07

0.4940.266

mg/

mg,' I

72.8-13981.6-12676.7-13179.3-13069.9-13583.2-13759.9-152

10410310110210297.2106

82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176

105

153

101

100

109

36.0NR

82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176

104151

97.798.5107

49.4NR

19.316.023.813.X21.835.835.3

0.9571.323.321.511.8531.4

Great

Andy ohnson. Project Manager


Page 8 of 21

' Rill LAKES. iSmm ANALYTICAL11

Hygieneering, Inc._ 7575 Plaza CourtI Willowbrook, IL 60521

1380 Busch ParkwayBuffalo Grove, I l l inois 60089



Email, [email protected](847) 808-7766 FAX (847) 808-7772

Sampled: 5,31/01Received: 6/1/01Reported: 6,13/01 07:44

TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality Control

Analvte

Im Batch: 1060137

Blank

1Mercury

LCSMercury

[ Matrix SpikeMercury

• Matrix Spike Pup


Date Spike Sample QCAnalyzed Level Result Result


1060137-BS16/12/01 0.00100 0.000853

1060137-MS1 B106039-026/12/01 0.00100 ND 0.000879

1060137-MSD1 B106039-02


Extraction Method: EPA 7470A

mg/1 0.000200

mg/1 73.9-123 85.3

mg/1 58.0-152 87.9

Mercury

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6/12/01 0.00100 ND 0.000875 mg/1 58.0-152 87.5 26.2 0.456

Great L ikes Analytical

Andy Jonnson, Project Manager


Page 9 of 2!



Email: info@glalabs com(847) 808-7766 FAX (847) 808-7772

Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL60521



Sampled: 5/31/01Received: 6,1/01Reported: 6/13/01 07:44

Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical

Date Spike SampleAnalyte Analyzed Level Result

Batch: 1060128 Date Prepared: 6/7/01Blank 1060128-BLK1Acetone 6/7/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfideCarbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethene "cis- ,2-Dichioroethene "trans- 1,2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-DichloropropeneEthylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene1 , 1 ,2,2-TetrachloroethaneTetrachloroethene "Toluene "1,1, -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate-Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromeihane " 50.0

QCResult

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

50.*


Extraction Method: EPA 5030B (P/T)

ug/ l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00

91.1-111 101

Gre at Lakes Analytical



Page I Oof 2




11JHygieneering, Inc.

7575 Plaza CourtWillowbrook, IL 60521



Volatile Organic Compounds by EPA Method

1*T

| Analyte

[| Blank (continued^Surrogate: 1 . 2-Dichloroethane-d4

_ Surrogate: Toluene-d8V Surrogate: 4-Bromofluorobenzene

LCS


IBromomethane2-ButanoneCarbon disulfide


1ChloroformChloromethane

,1 -Dichloroethane^ ,2-Dichloroethane• ,1-DichloroetheneV cis-1 ,2-Dichloroethene

rans-1 ,2-Dichloroethene

1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthyl benzene

12-HexanoneMethylene chloride4-Methyl-2-pentanone

IStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroetheneToluene

11,1 ,1-Trichloroethane1,1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethane

• f

Great Lakes


1060128-BLK16/7/01 50.0

50.050.0

10601 28-BS16/8/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0-50.0

Analytical

QCResult

53.052.049.9

58.350.053.357.047.854.155.850.855.257.151.951.146.945.750.048.555.747.852.753.955.156.350.150.052.660.338.65(5.1

55.552.956.9d().254.0


8260B/Quality Control


ug/I 85.1-10495.1-10589.6-105

ug/1 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.0-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-12086.3-12063.5-14684.5-12451.4-15310.0-586


106104

99.8

117100107114

95.6108112102110114104102

93.891.4100

97.0

I"95.6105108110113100100105121

77.21121 ) 1106114120108

I Great Lakes Analytical

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Page 1 I of 21








Volatile Organic Compounds by EPA Method 82606/Quality ControlGreat Lakes Analytical

Analyte

LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Matrix SpikeAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2.2-TetrachloroethaneTetrachloroetheneToluene


1060128-BS16/8/01 50.0

50.0150

50.050.050.050.0

SampleResult

QC Reporting Limit Recov. RPD RPDResult Units Recov. Limits % Limit °/o Notes*

37.8 ug/l47.7173

49.747.451.551.9

10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105

75.695.4115

99.494.8103104

1060128-MS1 B106020-066/8/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

54.9 ug/l44.250.556.543.751.442.839.950.154.962.346.337.240.149.538.250.240.648.746.848.647.849.745.852.754.758.844.749.0

10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20849.7-12620.6-22345.1-11371.3-1 18

11088.4101113

87.4103

85.679.8100110125

92.674.480.299.076.4100

81.297.493.697.295.699.491.6105109118

89.498.0

Great L <es Analytical



Page 12 of 2




JHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521


Project Manager:

2001-3495N/AGary Milkeris

Sampled: 5,31,01Received: 6/1/01Reported: 6,13/01 07:44

Volatile Organic Compounds by EPA Method 82606/Quality ControlIjt Great Lakes Analytical

1_jAnalyte

BlMatrix Spike (continued)1,1,1 -Trichloroethane

a»\ ,1 ,2-Trichloroethane•Trichloroethene^^"ri ch 1 orofl uorom ethan e

Vinyl acetate

f inyl chlorideotal Xylenes

Surrogate: Dibromofluoromethane^Surrogate: 1 . 2-Dichloroethane-d4^[Surrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene

•Matrix Spike PupBAcetone

BenzeneBromodichloromethane

tromoformromomethane

2-Butanone•Carbon disulfide•Carbon tetrachloride^Chlorobenzene

Chlorodibromomethane

f hloroethanehloroform

Chloromethane

— 1 , 1 -Dichloroethane• I ,2-Dichloroethane9\ , 1 -Dichloroethene

cis- 1 ,2-Dichloroethene

Krans- ,2-Dichloroethene,2-Dichloropropane

cis- 1 ,3-Dichloropropenetrans- ,3-Dichloropropene

Kthylbenzene-Hcxanone

Methylene chloride

|

4-Methvl-2-pentanone'

Great ,akes Analytical

Andv ohnson. Project Manager


SampleResult

QCResult


RPDLimit

RPD 1°/o Notcs*|

1060128-MS1 B106020-066/8/01 50.0

50.050.050.050.050.0150

50.050.050.050.0

NDND12.1NDNDNDND

41.855.649.244.650.235.8151

50.650.351.950.9

ug/l 42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-1119 1.1-1 II85.1-10495.1-10589.6-105

83.6111

74.289.2100

71.6101101101104102

1060128-MSD1 B106020-066/8/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

59.937.044.950.643.860.834.834.339.048.046.240.032.334.546.332.442.734.042.639.643.037.558.640.152.7

ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20S

"Refer to end of report

12074.089.8101

87.6122

69.668.678.096.092.480.064.669.092.664.885.468.085.279.286.075.0117

80.2105

for text

73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7

of notes

8.7017.711.711.2

0.22916.920.615.124.713.630.014.614.115.06.6816.41S.717.713.416.712.224.216.313.3

0

and definitions

Page 1 3 of 2 1

I







Sampled: 5/31/01Received: 6/1/01Reported: 6-13/0107:44


AnalvteDateAnalyzed

SpikeLevel

SampleResult

QCResult Units

ReportingRecov.

LimitLimits

Recov. RPDLimit

RPDNotes*

Matrix Spike Pup (continued)Styrene1,1,2,2-TetrachloroethaneTetrach I oroeth en eToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060128-MSD1 B106020-066/8/01 50.0

50.050.050.050.050.050.050.050.050.0150

50.050.050.050.0

NDNDNDNDNDND12.1NDNDNDND

42.255.336.939.435.650.741.339.642.430.5119

50.349.951.250.7

ug/: 49.7-12620.6-22345.1-11371.3-118

42.5-12870.1-139

53.5-10610.0-41710.0-239

37.4-11370.8-11191. 1-11185.1-104

95.1-10589.6-105

84.411173.878.871.210158.479.284.861.079.310199.8102101

18.650.317.619.418.432.520.929.234.523.512.4

25.46.1119.121.716.09.4323.811.916.516.024.1

Array Johnson, Project Manager


Page 14 of 2'





75 75 Plaza CourtWillowbrook. IL 60521

11

1 Analyte

• Batch: 1060075Blank

IAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene

1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene

— Benzo (k) fluoranthene• Chrysene• Dibenz (a,h) anthracene

Fluoranthene

tFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene


§LCSAcenaphtheneAcenaphthyleneAnthracene

IBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluoranthene

— Benzo (ghi) perylene• Benzo (k) fluoranthene^Chrysene

Dibenz (a,h) anthracene

1FluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalene

1PhenanthrenePyreneSurrogate: Carbazole

I"Great Laka^ Analytical

1 /






11

"ii

""••11

""»""»

0.500

1060075-BS16/6/01 2.00

2.002.002.002.002.002.002.002.002.002.002.002.002.002.002.00

0.50(1

Sampled: 5/31/01Received: 6/1/01Reported: 6.13/01 07:44

EPA Method 8310/Quality ControlAnalytical

QCResult


Recov. RPD RPD% Limit % Notes"

Extraction Method: EPA3510C


0.423

.69

.732.10

.75

.74

.91

.96

.63

.84

.89

.68

.69

.76

.58

.881 .9(i

0.474

ug/l 5.005.005.00

0.1000.1000.100

5.000.100

1.000.1005.005.00

0.2005.005.005.00

24.5-122

ug/ l 23.9-10721.6-10124.8-10732.9-10023.5-11334.5-12635.7-97.542.9-11339.9-11031.3-92.536.1-10536.6-99.641.5-95.722.0-99.825.8-1153 1 . 5 - 1 1 224.5-122

84.6

84.586.5105

87.587.095.598.081.592.094.584.084.588.079.094.098.094.8


Anay Johnson. Project Manager Page 15 of 2

I







Sampled: 5,31/01Received: 6,1/01Reported: 6/13/01 07:44

Polynuclear Aromatic Compounds by EPA Method 8310/Quality Control

Analvte

LCS PupAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) ttuorantheneChryseneDibenz (a,h) anthraceneFiuorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole



1060075-BSD16/6/01 2.00 1.68

2.00 1.712.00 2.042.002.002.002.002.002.002.002.002.002.002.002.00

.74

.71

.87

.88

.66

.88

.841.06.71.72.59.92

2.00 2.06• • - - r - - Q500 Q408


ug/l 23.9-10721.6-10124.8-10732.9-10023.5-11334.5-126

35.7-97.542.9-11339.9-110

31.3-92.536.1-105

36.6-99.641.5-95.722.0-99.825.8-11531.5-11224.5-122

Recov.%

84.085.5102

87.085.593.594.083.094.092.0103

85.586.079.596.0103

81.6

RPDLimit

62.560.747.447.445.252.445.449.651.753.258.852.545.857.255.950.0

RPD% Notes*

0.5931.162.90

0.5731.742.124.171.822.152.6820.31.182.30

0.63 12.114.98

Great La/es Analytical


Refer to end of report for text of notes and definitions.

Page 16 of 21




I

JHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521



Sampled: 5/31-01Received: 6/1/01Reported: 6 13/01 07:44


^ Date Spike SamplelAnalyte Analyzed Level Result

• Batch: 1060123 Date Prepared: 6/7/01Blank 1060123-BLK1

IAcetone 6/7/01Benzene "Bromodichloromethane "Bromoform "

IBromomethane "2-Butanone "Carbon disulfide

— Carbon tetrachloride "• Chlorobenzene "WChlorodibromomethane "

Chloroethane "

1Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "

11,1-Dichloroethene "cis-l,2-Dichloroethene "trans- 1,2-Dichloroethene "

11 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "

12-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "

• 1,1 ,2,2-Tetrachloroethane "BlTetrachloroethene "

Toluene "

11,1,1-Tri chloroethane "1,1 ,2-Trichloroethane "TrichloroetheneTrichlorofluoromethane "

1Vinyl acetateVinyl chloride "Total Xylenes

1Surrogate: Dibromofluoromethane " 50.0

/Great Lakes/Analytical

QCResult


50.5


Extraction Method: EPA 5035B [P/T1

ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

HI. 2- 134 101



I

Page I 7 of 21




Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521



Sampled: 5,31/01Received: 6/1/01Reported: 6/13,01 07:44


Analvte

Blank (continued)Surrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCSAcetoneBenzeneBromodichloromethane3romotbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1.1,1-Trichloroethane1 ,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane

Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes'

1060123-BLK16/7/01 50.0

50.050.0

1060123-BS16/7/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

48.3 ug/kg52.849.0

87.5 ug/kg55.657.254.257.759.564.358.956.353.688.055.457.154.656.655.756.855.657.257.660.555.860.048.761.855.752.059.360.25h.l57.957.561.8

50.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241

96.6106

98.0

1751 1 11141081151191291181131071761 1 11141091131 1 11141 1 1114115121112120

97.41241 1 11041 1 9120112116115124

Ajrfdy Johnson, Project Manager

"Refer to end of report for text of notes and definition:

Page 18 of 2




I1

1 Hygieneering, Inc.7575 Plaza Court

HWillowbrook, IL 60521



Sampled: 5/31,01Received: 6,1/01Reported: 6 1 3 - 0 1 07:44

• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control! Great Lakes Analytical

Analvte

LCS (continued)Vinyl acetate

IVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4

( Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCS Pup• Acetone• Benzene

Bromodichloromethane

tBromoformBromomethane2-ButanoneCarbon disulfide

1Carbon tetrachlorideChlorobenzeneChlorodibromomethane

1ChloroethaneChloroformChloromethane1 , 1 -Dichloroethane

11,2-Dichloroethane1 .1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene

• 1 ,2-DichloropropaneBcis-1 ,3-Dichloropropene

trans- 1,3-Dichloropropene

IEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone

ISrs'rene-1 ,1 ,2,2-TetrachloroethaneTetrach 1 oroeth en e

— Toluene

Date Spike Sample QC Reporting Limit Recov.Analyzed Level Result Result Units Recov. Limits %

1060123-BS16/7/01 50.0

50.0150

50.050.050.050.0

1060123-BSD16/8/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

58.5 ug/kg52.5166

49.951.853.248.3

51.5 ug/kg53.253.551.867.957.165.153.852.450.6106

53.967.452.552.255.058.055.454.552.954.252.458.148.260.552.354.953.656.1

10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-11*

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134

1171051 1 1

99.8104106

96.6

103106107104136114130108105101NR1081351051041101161 1 1109106108105116

96.41211051 1 01071 12

RPDLimi t

34541.442.057.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.4119

37.254.646.342. fi

RPD% Notes*

51.84.616.333.7716.74.29

0.7728.857.345.7718.62.7416.93.748.29

0.9051.74

04.488.141 1 . 46.453.391 .032.455.565.6110.66.90

nalytical

Anay Johnson, Project Manager

I


Page 19 of 21




Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL60521



Sampled: 5.31-01Received: 6-1 ,01Reported: 6-13, ( ) l 07:44


AnalvteDateAnalyzed

SpikeLevel

SampleResult

QCResult Units

ReportingRecov.

LimitLimits

Recov. RPDLimit

RPD/() Notes"

LCS Pup (continued)1,1,1 -Tri chloroethane1,1,2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060123-BSD16/8/01 50.0

50.050.050.050.050.0150

50.050.050.050.0

54.155.256.173.257.563.6156

51.951.054.249.9

ug/kg 60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-11*

10811011214611512710410410210899.8

44.253.243.511592.181.040.1

3.645.312.6416.31.7219.06.51

Great La/es Analytical

A'ridy Johnson. Project Manager


Page 20 of 2

1•

1

11

| GREAT

•MEH'-"^" 1380 Busch Parkway•BflP ANALYTICAL Buffalo Grove. Illinois 60089

Hygieneering, Inc. Project:7575 Plaza Court Project Number:Willowbrook. IL 6052 1 Project Manager:



Sampled: 5,31,01Received: 6 1 / 0 1Reported: 6/13/01 07:44


# Note

(A

G12

IGIS

I02

rO4

i«I

DET

ND

>NR

dry

f Recov.

RPD

IIII

The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.

The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.

The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.

The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.

The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory^established acceptance criteria. Refer to the included QC reports for more detail.

The recovery for this analyte is below the laboratory's established acceptance criteria.

The recovery for this analyte is above the laboratory's established acceptance criteria.

Analyte DETECTED

Analyte NOT DETECTED at or above the reporting limit

Not Reported

Sample results reported on a dry weight basis

Recovery'

Relative Percent Difference

"Great Lake's Analytical

1 /—Atfclv Johnson. Project Manager

1

Page 21 of 21

LAKttiANALYTICAL

(847) 808-7766FAX (847) 808-777

(414) 570-9460FAX (414) 570-9461

TAT: (SID. \ 4 DAY 3 DAY 2 DAY 1 DAY < 24 HRSO YES - TAT is critical

D NO - TAT is not critical

TEMPERATURE UPON RECEIPT: OH OC£LSfafe <SProgram:

Deliverable Package Needed:D SID D Other

Project: bG\- 349-5T # of Soff/esPreservative Used

PO/Quote #: JOI - J- LABORATORYID NUMBERHELD /D, LOCATION

RELINQUISHED




IIII1II

July 26, 2001


RE: 2001 -3495

Dear Gary Milkeris

Enclosed are the results of analyses for sampie(s) received by the laboratory on July 13, 2001 . If you have anyquestions concerning this report, please feel free to contact me.

Sincerely

/Andy JohnsonProject Manager

_,«• GREATLAKES

[ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772


Sample Description

B32-3

B32-15

B34-5

B34-15

B35-6

B35-15

B36-3

B36-15

B37-6

B37-19

Project: 2001-3495Project Number: 200 1 -3495


ANALYTICAL REPORT FOR

Laboratory Sample Number

B107171-01

B107171-02

B107171-03

B107171-04

B107171-05

B107171-06

B107171-07

B107171-08

B107171-09

B107171-IO

SAMPLES:

Sample Matrix

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil


Date Sampled

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

7/13/01

JGreat Lal#es Analytical

'?Andy Johnson, Project Manager

The results in tins report apply to the samples analyzed in accordance with the chain of custody docuniiThis analytical report must be reproduced in its enlir

Page 1 c

|

-^| GREAT•All LAKES•&•• ANALYTICAL•1

fHygieneering, Inc.7575 Plaza Court


*

Analyte

IMMAcenaphthene

«AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene

1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChrysene

• Dibenz (a,h) anthraceneV Fluoranthene

Fluorene

1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePvrene

t _ . _ . . _Surrogate: Carbazole

B34-5

t AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene


, Benzo (k) fluoranthene

f ChryseneDibenz (a,h) anthraceneFluoranthene

1FluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrene

( PyreneSurrogate: Carbazole

I

1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)





B107171-011070317 7/17/01 7/21/01 100

200100100

90.0100100100100

90.01000

100100100100

1000~~" "" """""" 29.0-132

B107171-031070364 7/19/01 7/21/01 100

10001000

10090.0100100100100

90.010001000

100100

10001000

,29.0-132

Email: [email protected] FAX (847) 808-7772


Result Units Notes"

Soil G_l1050 ug/kg831717

1430467767681299

1150623

3900 " G12682364ND737

9650 " G12165 % OS

SoilND ug/kg

1330 " G122000 " G121520

ND968929574

166011808600 " G I 21860 " G12

179ND

5320 " G1210500 " G12

78.2 %

' Great Lakes Analytical

Andy Johnson, Project Manager Page 2 of 3'

I





Analyte

B34-15AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

B35-6AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

\

Project: 2001-3495Project Number: 2001-3495

Project Manager. Gary Milkeris



B107171-041070364 7/19/01 7/21/01 100

200100100

90.0100100100100

90.0100100100100100100

29.0-132

B107171-051070364 7/19/01 7/23/01 100

200100100

90.0100100100100

90.0100100100100100500

29.0-132


Result Units Notes*

SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

" "68.3 %

SoilND ug/kg386355NDNDNDNDNDNDND

1050415NDND380

2760 " G1260.5 %

Greit Lakes Analytical

\



Page 3 of 2

|

«, | GREAT•ill LAKES

_ •&• ANALYTICAL•11

Hygieneering, Inc.— 7575 Plaza Court• Willowbrook, IL 60521

|Analvte

• B35-15Acenaphthene


1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene

_ Chrysene• Dibenz (a,h) anthraceneB» Fluoranthene

Fluorene» Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene

B Surrogate: Carbazole

B36-3


K Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene

-^ Benzo (k) fluoranthene• Chrysene9 Dibenz (a,h) anthracene

Fluoranthene^ Fluorene• Indeno (1,2,3-cd) pyrene

NaphthalenePhenanthrene

1 Pyrene| Surrogate: Carbazole

1






B107171-061070336 7/18/01 7/22/01 100

200100100

90.0100100100100

90.0100100100100100100

29.0-132

B107171-071070336 7/18/01 7/22/01 100

200100100

90.0100100100100

90.0100500100100100500

29.0-132



Result Units Notes*


83. 1 %

SoilND ug/kg

1590801NDNDNDNDNDNDNDND788 " G 1 2NDND

13702040 " G I 283.0 %

Grekt Lakes Analytical

I

I

Andy\JoTinson, Project Manager

"Refer to end oj report for text of notes and definitions.

Page 4 of" 3 7









Analyte

B36-15AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole


B107171-081070336 7/18/01 7/26/01 100

200100100

90.0100100100100

90.0100100100100100100

29.0-132

Result Units Notes*


78.0 %

Great Lakes Analytical "Refer to end oj report for text of notes and definition

Andy Johnson, Project Manager Page 5 of

1111

-.-•GREAT•|!| LAKES•Bll ANALYTICAL





Project Manager:

2001-34952001-3495Garv Milkeris


7/13/017/13/017/26/01 12:15

I


9 B32-3 B107171-01Acetone 1070359 7/17/01 7/19/01

fBenzene " " "Bromodichloromethane " " "Bromoform " " "Bromomethane " " "

f 2-Butanone " " "Carbon disultlde " " "Carbon tetrachloride " " "

» Chlorobenzene " " "Chlorodibromomethane " " "Chloroethane " " "Chloroform " " "

I Chloromethane " " "1,1 -Dichloroethane " " "1 ,2-Dichloroethane "1,1-Dichloroethene

M cis-l,2-Dichloroethene " " "^ trans- 1 ,2-Dichloroethene " " "

1,2-Dichloropropane " " "

§cis-l,3-Dichloropropene " " "trans- 1 ,3-Dichloropropene " " "Ethylbenzene " " "2-Hexanone " " "

f Methylene chloride " " "4-Methyl-2-pentanone " " "Styrene

^ 1,1,2,2-Tetrachloroethane " " "• Tetrachloroethene " " "V Toluene " " "

1,1,1-Trichloroethane " " "

t l,l,2-Trichloroethane " " "Trichloroethene " " "Trichlorofluoromethane " " "Vinyl acetate "

• Vinyl chloride " " "|| Total Xylenes

Surrogate: Dibromofluoromethane " " " 81.2-134

« Surrogate: 1.2-Dichloroelhane-d4 " " " 50.8-145

. Greit Lakes Analytical

25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

"Refer to end i

Soil G19.G3.G^89.1 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND108 %153 " 05

fjf report for text of notes and definitions.

Andj| Johnson. Project Manager Page 6 of 37

I








B32-3 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene


AnalyteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits

ReportingLimit Result Units Notes'

B107171-01 Soil G19.G3.C1070359 7/17/01 7/19/01 82.0-121

76.8-113~10385.2



"Refer to end of report for text of notes and dcfinitio,

Page 7 of




1I

Hygieneering, Inc.75 75 Plaza Court

1 Willowbrook, IL 60521

P

•

Analvte

E B32-1SAcetone

_ BenzeneB Bromodichloromethane™ Bromoform

Bromomethane

K 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene

|c.hlorodibromomethaneChloroethaneChloroform

I Chloromethane1,1 -Dichloroethane1 ,2 -Dichloroethane1,1-Dichloroethene

I cis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane

^ cis-1, 3-Dichloropropene• trans-1 ,3-Dichloropropene™ Ethylbenzene

2-Hexanone

I Methylene chloride

4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane

I Tetrachloroethenef Toluene

1,1,1 -Trichloroethane

» 1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

t Vinyl chloride•• Total Xylenes

Surrogate: Dibromofluoromethaneg Surrogate: 1.2-Dichloroethane-d4





B107171-021070359 7/17/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145


Result Units Notes*

Soil G19.G3.G452.7 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

5.27 " ANDNDNDNDNDNDNDNDNDNDNDND112 "/„140


IAndy JMinson, Project Manager Page8 of 3 7









AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


B32-15 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

6107171-02^1070359 7/17/01 " 7/79/07:" " " 82.0-121

76.8-113

Soil G19.G3.G-"99.3 %71.1 " O4

GreatiLakes Analytical

KAndy Johnson, Project Manager

"Refer to end of report for text of notes and definitioi

Page 9 ol




11

Hygieneering, Inc._ 7575 Plaza Court• Willowbrook. IL 60521f

|Analvte

1 834^5Acetone

1BenzeneBromodichloromethaneBromoformBromomethane» 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene

• Chlorodibromomethane™ Chloroethane

Chloroform

IChloromethane1,1 -Dichloroethane

- 1 ,2-Dichloroethane1,1-Dichloroethene

• cis-1 ,2-Dichloroethene| trans- 1 ,2-Dichloroethene

1 ,2-Dichloropropane

§cis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

f Methylene chloride4-M ethyl -2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

• TetrachloroetheneR Toluene

1,1,1 -Tri chloroethane

11 , 1 ,2-Tri ch 1 oroethaneTrichloroetheneTrichlorofluoromethane

. . V i n y l acetateB Vinyl chloride• Total Xylenes

Surrogate: Dibromofluoromethane— Surrogate: l.2-Dichloroelhane-d4

• 1

Project: 2001-3495Project Number: 2001-3495Project Manager: Gary Milkeris



B107171-031070359 7/17/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.00

" " " 10.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145


Result Units Notes*

Soil G19.G3.G4102 ug/kg ANDNDNDND

12.8 " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND107 %149 " OS

'Great Lpkes Analytical


"Refer to end of report lor text of notes and definitions

Page 10 of 37

I





Project: 2001-3495Project Number: 2001 -3495




AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


B34-5 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1070359 7/17/01Bl07171-03

"7/79/0; 82.0-12776.8-113

Soil105 %

76.3

G19.G3.G

O4

tlfeGreat Lpkes Analytical "Refer to end of report for text of notes and definitions

\

Andy Johnson, Project Manager Page 1 1 of 3

I "—- - H G R EATF|Sl LAKES•fill ANALYTICAL

•1

|Hygieneering, Inc.7575 Plaza Court

f willowbrook, IL 60521

mI

1| Analyte

JB34-15Acetone

_ Benzene• Bromodichloromethane^ Bromoform

Bromomethane

12-ButanoneCarbon disulfideCarbon tetrachloride

. Chlorobenzene

IchlorodibromomethaneChloroethaneChloroform

tChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene

1cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropene

• trans-1 ,3-Dichloropropene™Ethylbenzene

2-Hexanone

fMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

ITetrach 1 oroeth eneToluene1,1,1 -Trichloroethane

§1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

§Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane

^Surrogate: 1 . 2-Dichloroethane-d4






B107171-041070359 7/17/01 7/19/01 25.0

5.005.005.005.001 0.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145



Result Units Notes*


5.60 " ANDNDNDNDNDNDNDNDNDNDNDND115 %144

Grea Lakes Analytical

i\Andyl Johnson, Project Manager


Page 12 of 37

I






Project Manager: Gary Milkens



AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits



1070359 7/17/01B107171-04

'7/19/01 ~~~ 8'2.0-lYr76.8-113

Soil94.071.7

G19.G3.G

04

IGreat Likes Analytical

Andy Jdhnson, Project Manager

"Refer to end of report for text of notes and definition.

Page 13 of!

I ^.^B GREAT'KM LAKES•&• ANALYTICAL

1Hygieneering, Inc.

_ 7575 Plaza Court• Willowbrook, IL 60521P

. Analyte

• B35-6Acetone

1BenzeneBromodichloromethane

_ BromoformBromomethane

I 2-ButanoneCarbon disultldeCarbon tetrachloride

^ ChlorobenzeneH Chlorodibromomethane9 Chloroethane

Chloroform

IChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

• cis-1 ,2-Dichloroethenejj trans-1 ,2-Dichloroethene


§cis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

tMethylene chloride4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane

• Tetrachloroethene••Toluene



f Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane

— Surrogate: 1 .2-Dichloroethane-d4






B107171-051070359 7/17/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145



Result Units Notes*

Soil G19.G3.G470.6 ug/kg ' ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

5.06 " ANDNDNDNDNDNDNDNDNDNDNDND107 %148 " O5

Gredt Lakes Analytical

II

red

Andy Jonnson, Project Manager

"Refer to end of report for text of notes and definition.',.

Page 14 of 37









AnalyteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits

ReportingLimit Result Units Notes"


1070359 7/17/01_B107171-05

~~7/19/6T~ '82.0-12176.8-113

Soil G19.G3.G705 %

91.0

Great Lakes Analytical "Refer to end of report for text of notes and definition.

Andy Johnson, Project Manager Page 15 of.

|

~..,| GREATyam LAKES•&•• ANALYTICAL•1

1Hygieneering, Inc.

|7575 Plaza CourtBwillowbrook.IL 60521

'

Analyte

B35-15Acetone

— Benzene•Bromodichloromethane^Bromoform

Bromomethane

I2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene

IchlorodibromomethaneChloroethaneChloroform

fChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

>cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropene

• trans-1 ,3-Dichloropropene^Ethylbenzene

2-Hexanone

IMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

ITetrachloroetheneToluene1,1,1 -Tri chloroethane

11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate»Vinyl chlorideTotal Xylenes

• - -- - • - - . . . _ . . . . _ _ .

Surrogate: DibromofluoromelhaneSurrogate: 1 . 2-Dichloroelhane-d4

I 1



Project Manager: Garv Milkeris



B107171-061070359 7/18/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

" " " 81.2-13450.8-145



Result Units Notes*



Lakes Analytical

IAndyUohnson, Project Manager


Page 16 of 37

I

ilGREATLAKESANALYTICAL




Analvte


Project: 2001-3495Project Number: 2001-3495Project Manager: Gary Milkeris



B107171-06;070359 7/18/01 7/19/01 82.0-121

76.8-113


Result

96.975.7

7/13/017/13/017/26/01

Units

Soil%

12:15

Notes"

G19.G3.G



Page 17 of'.'

I ^.^B GREAT•ill LAKES

_ iSmm ANALYTICAL•1I



9

Analyte

B360Acetone

_ Benzene• Bromodichloromethane9 Bromoform

Bromomethane

t 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene

• Chlorodibromomethane• Chloroethane

Chloroform

IChloromethane1 , 1 -Dichloroethane

- 1 ,2-Dichloroethane1,1-Dichloroethene

1cis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane

_ cis-1 ,3-Dichloropropene•trans- 1 ,3-Dichloropropene9 Ethylbenzene

2-Hexanone

1Methylene chloride4-M ethyl-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane

ITetrachloroetheneToluene1,1,1 -Trichloroethane

11 , 1 .2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

§Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: l.2-Dichloroethane-d4

I






B107171-071070359 7/18/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.00

" ' " 5.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145



Result Units Notes*G19.G3.G4.

Soil O2.O3172 ug/kg ANDNDNDND17J " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

7.08 " ANDNDNDNDNDNDNDNDNDNDNDND121 %150 " O5

Great -akes Analytical

IAndyWohnson, Project Manager


Page 18 of 37

I









Analyte

B36-3 (continued)

BatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits

ReportingLimit

B107171-07

Result Units

SoilG19.G302.03

Notes*.G4.


1070359 7/18/01 7/19/01 82.0-12176.8-113

90.3 %37.9 " O4

Groat Lakes Analytical "Refer to end of report for text of notes, and definitions

Andy Sofmson, Project Manager Page 19 of 3

I »*£*M GREAT•All LAKES•Ell ANALYTICAL•1

11 Hygieneering, Inc.

J 7575 Plaza CourtMl Willowbrook. IL 60521i

M

1

H1 Analyte

PB36-15Acetone

»BenzeneBromodichloromethaneBromoformBromomethane



Chloroform

IChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

1cis- 1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropane

_ cis-l,3-DichloropropeneM trans- 1,3-Dichloropropene9 Ethylbenzene

2-Hexanone

1Methylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

I TetrachloroetheneToluene1,1,1-Trichloroethane


1Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane

^ Surrogate: 1.2-Dichloroethane-d4

I• GreatjLakes Analytical

1 1 _






B107171-081070359 7/18/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145



Result Units Notes*




Andy Vohrrson, Project Manager Page 20 of 3 7

I





Project: 2001-3495 Sampled: 7/13/01Project Number: 2001-3495 Received: 7/13/01

Project Manager: Gary Milkeris Reported: 7/26/01 12:15


Analvte

B36-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzet

Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes'

B107171-08 Soil G19.G3.G;070159 7/18/01 7/19/01 82.0-121 96.3 %

le " " " 76.8-113 74.7 " O4

Great Lakes Analytical "Refer to end of report for text of notes and definition.

A^ndy Johnson, Project Manager Page 21 of.'

LAKESANALYTICAL



1I



Analyte

•m^6Acetone

_ Benzene• Bromodichloromethane• Bromoform

Bromomethane



Chloroform

I Chloromethane1,1-Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene

1cis-1, 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane

— cis- 1 ,3-Dichloropropene• trans- 1 ,3-Dichloropropene9 Ethylbenzene

2-Hexanone

1Methylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane

§TetrachloroetheneToluene1,1,1-Trichloroethane

11 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetate

1Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4





B107171-091070359 7/18/01 7/19/01 25.0

5.005.005.005.00

7/21/01 10.07/19/01 5.00

5.005.005.005.005.005.005.005.005.00

7/21/01 2507/19/01 5.00

5.005.005.005.0010.05.0010.05.005.005.005.005.005.00

7/21/01 25007/19/01 5.00

10.07/21/01 5.007/19/01 5.00

81.2-13450.8-145


Result Units Notes*

Soil G19.G3.G82.6 ug/kg ANDNDNDNDNDNDNDNDNDND880 " END208ND

64.82330 " G12

203NDNDNDNDND

6.84 " ANDNDND

17.2ND11.1ND

8230 " G12NDND523 " END107 "/„151 " O5

I Grdat Lakes Analytical

And_y'Johnson, Project Manager

Refer to end of report for text of notes and definitions

Page 22 of 3

I







Sampled: 7/13/01Received: 7/13/01 ,Reported: 7/26/01 12:15 1



AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


1070359 7/18/01B107171-09

"7/7 9/07" 82.0-12176.8-113

Soil79.880.6

G19,G3.G4O4

Great Lakes Analytical "Refer to end of report for text of notes and definitions

Andy Johnson. Project Manager Page 23 of 3'

I ^.^B GREATf|5| LAKES

_ •&• ANALYTICAL•11

Hygieneering, Inc._ 7575 Plaza CourtBlWillowbrook, IL 60521

•

1i1 Analyte

• B37-19Acetone

•

BenzeneBromodichloromethaneBromoformBromomethane

12-ButanoneCarbon disulfideCarbon tetrachloride

_ ChlorobenzeneI Chlorodibromomethane9 Chloroethane

Chloroform

IChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethene»cis-1, 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane

|

Cis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-Hexanone

§Methylene chloride4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane

• Tetrachloroethene• Toluene


11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetate


_ Surrogate: 1.2-Dichloroethane-d4

1380 Busch ParkwayBuffalo Grove, Illinois 60089 (847)





B107171-101070359 7/18/01 7/19/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.00

7/23/01 5.007/19/01 5.00

10.05.0010.05.005.005.005.00

7/23/01 5.007/19/01 5.007/23/01 50007/19/01 5.00

10.05.005.00

81.2-13450.8-145



Result Units Notes*

Soil G19.G3.G454J ug/kg ANDNDNDNDNDNDNDNDNDND

30.7NDNDNDND198

9.06NDNDNDNDND

19.7 " ANDNDNDNDNDNDND

71100 " G12NDND

6.02ND115 %159 " 05

' Great Lakps Analytical

I

I



Page 24 of 3 7

I•III





Analyte




Volatile Organic Compounds by EPA MethodGreat Lakes Analytical

Batch Date Date SurrogateNumber Prepared Analyzed Limits

B107171-101070359 7/18/01 7/19/01 82.0-121

76.8-113


5035/8260B


Soil G19.G3.G496. 6 %74. 1 " O4

4-Great Lakes Analytical "Refer to end of report for text of notes and definitions


I ^.^B GREATSASII LAKES• •B 1380 Busch Parkwayk^H ANALYTICAL Buffalo Grove, I l l inois 60089

1Hygieneering, Inc. Project:

17575 Plaza Court Project Number:Willowbrook, IL 60521 Project Manager:

Dry

2001-34952001-3495Gary Milkeris

Weight Determination



1 Great Lakes Analytical

1Sample Name Lab ID

B32-3 B107171-01

• B32-15 B107171-02

B34-5 B 1071 71 -03

BB34-15 B107171-04

B35-6 B107171-05

JB35-15 B107171-06

B36-3 B107171-07

• B36-15 B107171-08

I B37-6 B1071 71-09

B37-19 B107171-10

1

1

1

1

Matrix

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Result Units

73.7 %

77.5 %

75.8 %

84.2 %

83.1 %

79.6 %

70.1 %

82.0 %

87.7 %

83.5 %

II

Great Lqkes Analytical

1 i\ _Andy Johnson, Project Manager

1

Page 26 of 3









Analyte

Batch: 1070317BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole


Date Prepared: 7/17/011070317-BLKl7/22/01II

"

M

"

11

ii

"

n

11

11

"

11

11

n

n

"" ~" " 16.5

QCResult


11.4

Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes


ug/kg 100200100100

90.0100100100100

90.0100100100100100100

29.0-132 69.1


1070317-BS17/22/01 67.7

67.767.767.767.767.767.767.767.767.767.7

67.767.767.767.767.716.9

65.899.352.657.847.757.361.160.260.755.758.559.857.453.359.865.215.8

ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132

97.2147

77.785.470.584.690.388.989.782.386.488.384.878.788.396.393.5

Grebt Lakes Analytical



Page 27 of'.'




IHygieneering, Inc.

_ 7575 Plaza Court| Willowbrook, IL 60521

•

Analyte




_ Chrysene• Dibenz (a,h) anthracene9 Fluoranthene

Fluorene

1Indeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyrene

H Surrogate: Carbazole

Matrix Spike DUD

1AcenaphtheneAcenaphthyleneAnthraceneBenz fa) anthracene


^ Benzo (k) fluoranthene• Chrysene• Dibenz (a,h) anthracene

Fluoranthene

1FluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrene


1






SampleResult

QC Reporting Limit Recov.Result Units Recov. Limits %

RPDLimit

RPD% Note

1070317-MS1 B107145-057/22/01 65.9

65.965.965.965.965.965.965.965.965.965.965.965.965.965.965.916.5

1070317-MSD17/22/01 68.4

68.468.468.468.468.468.468.468.468.468.468.468.468.468.468.417.1


B107145-05NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

76.3 ug/kg139

57.760.650.556.359.456.860.853.665.564.154.277.564.965.531.7

55.2 ug/kg83.743.644.335.442.843.743.346.741.247.949.842.955.449.448.012.4

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

116NR

87.692.076.685.490.186.292.381.399.497J82.2118

98.599.4192

80.7122

63.764.851.862.663.963J68.360.270.072.862.781.072.270.272.5

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

35.953.531.634.738.630.834.030.629.929.834.728.826.937.230.834.4

Gre^t Lakes Analytical

I

I

Johnson, Project Manager

Refer to end of report for text of notes and definitions

Page 28 of 3










Analyte




it"""11

11

n11

""it11

"n

16.6

QCResult


"15.8



ug/kg 100200100100

90.0100100100100

90.0100100100100100100

29.0-132 95.2

1070336-BS17/21/01 67.7

67.767.767.767.767.767.767.767.767.767.767.767.767.767.767.716.9

58.177.355.758.953.356.864.457.159.658.360.954.559.553.655.959.217.4

ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132

85.8114

82.387.078:7

83.995.184.388.086.190.080.587.979.282.687.4103

Great Lalfes Analytical "Refer to end of report for text of notes and definitions

Andy Johnkm^xProject Manager Page 29 of" '•




11

Hygieneering, Inc.7575 Plaza Court| Willowbrook, IL 60521

•

Analyte




_ Chrysene• Dibenz (a,h) anthracene• Fluoranthene

Fluorene

1Indeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyrene

• Surrogate: Carbazole

Matrix Spike DUD



I Chrysene9 Dibenz (a,h) anthracene

Fluoranthene

1FluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene

I PvreneSurrogate: Carbazole

1






SampleResult

QCResult


Recov.%

RPDLimit

RPD% Notes

1070336-MS1 B107171-067/21/01 66.4

66.466.466.466.466.466.466.466.466.466.466.466.466.466.466.416.6

1070336-MSD17/19/01 67.2

67.267.267.267.267.267.267.267.267.267.267.267.267.267.267.216.8



39.780.049.150.548.849.853.249.452.848.452.646.851.759.450.051.412.3

57.669.246.547.440.752.340.143.046.236.047.843.041.365.649.956.617.4

ug/kg 10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

ug/kg 10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

59.8120

73.976.173.575.080.174.479.572.979.270.577.989.575377.474.1

85.7103

69.270.560.677.859.764.068.853.671.164.061.597.674.384.2104

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

35.615.26.577.6419.23.6629.215.014.430.510.89.6723.58.661.348.42

II

Andy Johrrsfjn, Project Manager


Page 3 Oof 3 7










Analyte




NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

" 16.5 "13.6



ug/kg 100200100100

90.0 !100100100100

90.0100100100100100100

29.0-132 82.4 \

1070364-BS17/24/01 65.9

65.965.965.965.965.965.965.965.965.965.965.965.965.965.965.9

16.5

49.463.343.446.543.247.451.048.249.749.345.645.246.640.545.646.911.0

ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132

75.096.165.970.665.671.9

77.473.175.474.869.268.670.761.569.271.266.7


Andy Johnson, Project Manager Page 31 of 3'




11

Hygieneering, Inc._ 7575 Plaza Court| Willowbrook, IL 60521

•

|Analyte

| Matrix SpikeAcenaphthene



_ Chrysene• Dibenz (a,h) anthraceneB Fluoranthene

Fluorene

1 Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene


Matrix Spike DUD



• Chrysene• Dibenz (a,h) anthracene

Fluoranthene

1FluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene

1 PyreneSurrogate: Carbazole

1






SampleResult


RPDLimit

RPD% Notes"

1070364-MS1 B107171-047/24/01 67.0

67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.8

1070364-MSD17/24/01 67.6

67.667.667.667.667.667.667.667.667.667.667.667.667.667.667.616.9



44.2 ug/kg62.043.447.642.847.448.646.550.545.268.244.544.447.649.667.11 1.0

38.0 ug/kg76.444.446.343.046.952.043.553.246.966.144.344.548.548.769.310.1

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

66.092.564.871.063.970.772.569.475.467.5102

66.466371.074.0100

65.5

56.2113

65.768.563.669.476.964.378.769.497.865.565.871.772.0103

59.8

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

16.020.01.383.58

0.4711.865.897.634.282.784.201.36

0.7570.981

2.742.96



Page 3 2 of 3 7

I









Analyte

Batch: 1070359BlankAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis- 1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroethen eToluene1,1,1-Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane


Date Prepared: 7/18/011070359-BLK17/19/01 59.0

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

7.47NDNDNDNDNDNDNDNDNDNDNDND

50.0 54.0

Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes"

Extraction Method: EPA 5035B 1P/T1

ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-134 108

GreathLakes Analytical "Refer to end of report for text of notes and definitions.

\

Andy Johnson, Project Manager Page 3 3 of 3 7






Project Manager: Ganr Milkeris



V1 Analyte

H Blank (continued)Surrogate: 1 , 2-Dich/oroethane-d4


LCS


• Bromomethane• 2-Butanone

Carbon disulfide


1ChloroformChloromethane1,1 -Dichloroethane

11 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene

11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene


IStyrene1.1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene

11,1,1-Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroethene


Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes-

1070359-BLK17/19/01 50.0

50.050.0

1070359-BS17/18/01 50.0

50.050.0

. " 50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

68.9 ug/kg54.348.8

\ 1 0 ug/kg45.349.339.5171

55.638.840.639.641.858.945.832.743.851.242.943.940.049.150.656.440.964.345.660.741.153.137.242.944.748.144.1

191

50.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241

138109

97.6

NR90.698.679.0NR1 1 1

77.681.279.283.6118

91.665.487.6102

85.887.880.098.2101113

81.8129

91.2121

82.2106

74.485.889.496.288.2NR

Great Lakes Anjifytical

II



Page 34 of 3 7




*!




Sampled: Ii \ 3/0 1Received: 7/13/01Reported: 7/26/01 12:15


Analyte


LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene


1070359-BS17/18/01 50.0

50.0150

50.050.050.050.0

1070359-BSD17/19/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

QC Reporting LimitResult Units

5 1 .4 ug/kg56.8203

44.055.245.441.5

1 34 ug/kg47.748.539.269.453.351.437.039.041.144.450.624.351.851.650.349.443.751.248.354.940.464.355.461.442.650.334.442.9

Recov. Limits

10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134

Recov.%

103114135

88.0110

90.883.0

NR95.497.078.4139107103

74.078.082.288.8101

48.6104103101

98.887.4102

96.6110

80.81291 1 1123

85.2101

68.885.8

RPDLimit

34541.442.057.461.9•173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.4119

37.254.646.342.6

RPD% Notes*

19.75.161.64

0.76284.43.6728.19.281.531.6928.29.7629.517.1

0.97616.311.88.843.804.452.691.23

019.61.643.584.837.82

0

Great Lakes Analytical7


AndyjJohnson, Project Manager Page 35 of 3




IHygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521


Project Manager:

2001-34952001-3495Gary Milkeris


7/13/017/13/017/26/01 12:15

IVolatile Organic Compounds by EPA Method 5035/8260B/Quality Control


1Analyte

LCS Pup (continued)

DateAnalyzed

SpikeLevel

SampleResult

QCResult


RPDLimit

RPD% Notes

1070359-BSD1

I

I

I

I

I

I

I

I

I

I

II

I

I

1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: l,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

7/19/01 50.050.050.050.050.050.0_150_

~50.0~50.050.050.0

46.850.545.3197

41.647.9204

ug/kg

48.155.146.042.2

60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-141'81.2-13450.8-14582.0-12176.8-113

93.6101

90.6NR

83.295.8136

96.2110

92.084.4

44.253.243.5115

92.181.040.1

4.594.872.683.0921.317.3

0.738

Great LakaS Analytical

And/ Johnson, Project Manager


Page 36 of 3'

SL.fcS-HmGREAT

^ 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

Hygieneering, Inc. Project: 2001-3495 Sampled: 7/13/017575 Plaza Court Project Number: 2001-3495 Received: 7/13/01Willowbrook, IL 60521 Project Manager: Gary Milkeris Reported: 7/26/01 12:15


# Note


E This result is estimated. The analysis gave a final result that is above the calibration range



G19 The relative percent difference (RPD) of one or more analytes in the laboratory control QC (BS/BSD) associated with this sampleis above the laboratory's established acceptance limits. Refer to the included QC reports for more detail.

G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'sestablished acceptance criteria. Refer to the included QC reports for more detail.

G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory';established acceptance criteria. Refer to the included QC reports for more detail.

02 One or more internal standard recoveries were below the method specified acceptance criteria.

03 One or more internal standard recoveries were above the method specified acceptance criteria.




ND Analyte NOT DETECTED at or above the reporting limit

NR Not Reported


Recov. Recovery


Great Lakes^Analvtical

Andy'Johnson, Project Manager Page 37 of 3

SP LAKESANALYTICAL

CHAIN OF CUSTODY REPORT (847) 808-7766FAX (847) 808-7772

531M(414) 570-9460

FAX (414) 570-9461

Client: e/// TO.- 3 DAY 2 DAY 1 DAY < 24 HRS.

-T ±-, -Address: /h?7!P

D YES^fAT is Critical

n N<"i - TAT is

D/irE RESULTS NEEDED:

TFMPFRATI 1RF 1 IPON RFC.FIPT « C«-

Report to:Phone *:Fax #:

Sfafe &Program:

P/ione #: f J Deliverable Package Needed:D STD D Other

Air Bill No.

^roject: <:

Sampler:

PO/Quote #:

FIELD ID, LOCATION

# of Boff/esPreservative Used

LABORATORYID NUMBER

-.•..•GREATILAKES 1380 Busch Parkway Email: [email protected]


July 20, 2001


RE: 2001-3495

Dear Gary Milkeris

Enclosed are the results of analyses for sample(s) received by the laboratory on July 11, 2001. If you have anyquestions concerning this report, please feel free to contact me.

Sino


•

-.-•GREATMil LAKES•&•• ANALYTICAL

1


•7575 Plaza Court•Villowbrook, IL 60521

sample Description

ft 18-8

B 18-32

^19-5

J19-9

^20-4

«20-14

%21-15

^22-3

B22-15

K23-9

B24-12

^25-7

C26-7

27-13

128-4

28-13

•^29-10

B30-11

•30-25

B31

1Great/Lakes Analytical

1 \iu '

1380 Busch ParkwayBuffalo Grove, I l l inois 60089



(847)Email, [email protected] FAX (847) 808-7772

Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41


Laboratory Sample Number

B107129-01

B 107 129-02

B 107 129-03

B 107 129-04

B 107 129-05

B 107 129-06

B107129-07

B107129-08

B 107 129-09

B107129-10

B107129-11

B107129-12

B107129-I3

B107129-I4

B107129-15

B107129-16

B107129-17

B107129-18

BI07129-I9

B 107 129-20

The results in this report apply to the samples

Sample Matrix

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Soil

Date Sampled

7/9/01

7/9/01

7/9/01

7/9/01

7/9/01

7/9/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

7/10/01

analyzed in accordance with the chum of custody documentThis analvlicul report must he reproduced in its entirely.

Andy Johnson, Project Manager Page I of 70

I





Analvte

B31AcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2 -Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene1,1,1 -Tri chloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4





B107129-201070323 7/18/01 7/18/01 2500

500500500500

1000500500500500500500500500500500500500500500500500

1000500

1000500500500500500500500500

1000500500

" " " 8 1.2- 1 3450.8-145

Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41

Result Units Notes*

Soil G12.G3.G42520 ug/kg A

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND831 " ANDNDNDNDNDNDND

1210NDNDNDND130 %118



*Refer to end of report tor text oj notes and de/inittons.

Page 2 of 70

GREATLAKES

NALYTICAL1380 Busch Parkway

Buffalo Grove, Illinois 60089Email, [email protected]

(847) 808-7766 FAX (847) 808-7772

I Hygieneering, Inc.^575 Plaza Court•Villowbrook. IL 60521



Sampled: 7/9/01 to 7,10/01Received: 7/11/01Reported: 7/20/01 13:41


AnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*

t31 (continued)Surrogate: Toluene-d8

m£urrogale: 4-Bromofluorobenzene

I

I

I

I

I

I

I

I

I

JO 703 2 3 7/18/01B107129-20

"7/AS/07 82.0-121"76.8-113

Soil G12.G3.G4126 % 05129 " OS

^read Lakes Analyt ical

1 Andy Johnson, Project Manager

1

*Refer to end of report fur left of notes and definition*.

Page 3 of 70





Analyte

B19-5AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-ChloronaphthaIene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-Dinitrotoluene


lu' \ i \; \i •



Semivolatile Organic Compounds by EPA Method 8270CGreat Lakes Analytical


B107129-031070237 7/13/01 7/17/01 1000

1000100010005000100010001000100010001000100010001000330010001000100010001000100010001000100010001000100010005000100010001000100033005000500010001000


Result Units Notes*

Soil G12.G15.G2.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND


Andy'Johnson. Project Manager Page 4 of 7'

GREATLAKESANALYTICAL 1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772

11

1 Hygieneering, Inc.JJ5 75 Plaza Court•Villowbrook, IL 60521

•

|TlAnalyte

•19-5 (continued)Di-n-octyl phthalate

(luorantheneluoreneexachlorobenzene

Hexachlorobutadiene

Eexachlorocyclopentadieneexachloroethane

Indeno (1,2,3-cd) pyrene^ophoronel-Methylnaphthalene"-Cresolm,p-Cresols

!

aphthalene•Nitroaniline•Nitroaniline

4-Nitroaniline

t itrobenzene•Nitrophenol

4-Nitrophenol

(-Nitrosodi-n-propylamine-Nitrosodiphenylamine

. entachlorophenolPhenanthrene

Khenolyrene

1 ,2,4-Trichlorobenzene^,4,5-Trichlorophenol•,4,6-Trichlorophenolmurrogate: 2-FluorophenolSurrogate: Phenol-d6

^Surrogate: Nitrobenzene-d5Wiurrogale: 2-FluorobiphenylSurrogate: 2.4,6-TribromophenolSurrogate: p-Terphenyl-d!4

1



Semivolatile Organic Compounds by EPA Method 8270CGreat Lakes Analytical


B107129-031070237 7/13/01 7/17/01 1000

100010001000100010001000100010001000100010001000500050005000100010005000100010005000100010001000100050001000

10.0-10910.0-11510.0-114/ 0.0- 10619.3-88.710.0-126


Result Units Notes*

Soil G12.G15.G2.G4ND ug/kgNDNDNDNDNDNDNDND

3740NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND104 %

6.32 " O427.429.036.532.0

jrcat Lakes Analytical

Anthr Johnson, Project Manager

"Refer to end of report fur text of notes and definitions.

Page 5 of 70

I





Analyte

B20-4AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole



Polynuclear Aromatic Compounds by EPAGreat Lakes Analytical

Batch Date Date SurrogateNumber Prepared Analyzed Limits

B107129-OS1070277 7/16/01 7/17/01II II M

II II II

II II II

II II II

II II II

tl II II

II II II

II It M

II II II

II II II

II II II

II II II

II II II

II II II

II II II

_ _._. ._. . . „ (..._. . . . 29.0-132

Method 8310

ReportingLimit

JOO200100100

90.0100100100100

90.0100100100100100100


Result Units Notes*

Soil G1.G15.G4.O5ND ug/lcgND164NDNDNDNDNDNDNDNDNDNDND205NDAT? % 05

Lakes Analytical

, 1Andy Johnson, Project Manager


Page 6 of 70

1 -,,-«• GREATfill LAKES•BM ANALYTICAL•1


^75 75 Plaza Court•Willowbrook, IL 60521

•

|J_Analvte

1VI 8-8

Acetone•Benzenefcromodichloromethane^Jromoform

Bromomethane•i-ButanoneCarbon disulfide

Carbon tetrachloride^ThlorobenzenemThlorodibromomethaneBbhloroethane

ChloroformKhloromethane• , 1 -Dichloroethane

1,2-Dichloroethane1,1-Dichloroethene

B;is-l ,2-DichloroetheneBrans- 1 ,2-Dichloroethene

1 ,2-Dichloropropane•cis- 1 ,3-Dichloropropene•rans- 1 ,3-Dichloropropene^Ethylbenzene

2-Hexanone

tethylene chlorideMethyl-2-pentanone

Styrene^1,1 ,2,2-Tetrachloroethane•Tetrachloroethene•Toluene

1,1,1 -Trichloroethane•1 , 1 , 2 -Tri ch 1 oroeth an e•Trichloroethene^"richlorofluoromethane

Vinyl acetate•Vinyl chloride(Total Xylenes

Surrogate: DibromofluoromethanemSurrogate: 1 ,2-Dichloroethane-d4






B107129-011070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

HI. 2-13450.8-145



Result Units Notes*

Soil G3.G434.2 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND112 %122

I

jreat Lakes Analytical

AndyiJohnson, Project Manager


Page 7 of 70

I



(847) 808-7766 FAX (847) 808-7772





7/9/01 to 7/1 0/017/11/017/20/01 13:41


Analyte

•B18-8 (continued)Surrogate: Toluene-dSSurrogate: 4-Bromofluorobenzene


B107129-011070296 7/17/01 7/17/01 82.0-121

76.8-113

Result

99.297.4

Units

Soil%

Notes*

G3.G4



"Refer to end of report /or text of notes and definitions.

P a u e & o f 7<

i!-.-.B GREATLAKESANALYTICAL



1I

1 Hygieneering, Inc.A7575 Plaza CourtB^illowbrook, IL 605219

ITUnalyte

»18-32Acetone

^BenzeneBiromodichloromethane^Bromoform

Bromomethane

t-Butanonearbon disulfide

Carbon tetrachloride^ThlorobenzeneMThlorodibromomethane•Chloroethane

Chloroform•Chloromethane• ,1 -Dichloroethane

l ,2-Dichloroethane1,1-Dichloroethene

•is- 1 ,2-DichloroetheneBrans- 1 ,2-Dichloroethene

1 ,2-Dichloropropanejj£\s- 1 ,3-Dichloropropene•rans-1 ,3-Dichloropropene^tthylbenzene

2-Hexanone•blethylene chloride•p-Methyl-2-pentanone

Styrene_1 , 1 ,2,2-Tetrachloroethane•Tetrachloroethene^Toluene


t,l ,2-Trichloroethanerichloroethenerichlorottuoromethane

Vinyl acetate

t inyl chlorideotal Xylenes

Surrogate: Dibromofluoromethane

t arrogate: 1 ,2-Dichloroethane-d4

r4ai Lakes Analytical



Volatile Organic Compounds by EPA Method 503S/8260BGreat Lakes Analytical


B107129-021070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.00

" " " 5.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7/20/01 13:41

Result Units Notes*

Soil G3.G432.1 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

5.23 " ANDNDNDNDNDNDNDNDNDNDNDND/ / / %125


Artdy JohrisonT-Project Manager Page 9 of 70

I





Analyte






B107129-021070296 7/17/01 7/17/01 82.0-121

76.8-113


Result

98.396.1

7/9/01 to 7/10/017/11/017/20/01 13:41

Units

Soil%

Notes*

G3.G4

Great Liikes Analytical Refer to end of report for text of notes and definitions.

Andy Johnson, Project Manager uc 10 of 70




1I

1 Hygieneering, Inc.J7575 Plaza CourtB\Villowbrook, IL 60521

•

|f

lAnalvte

•319-5• - ...

Acetone^Benzene•3romodichloromethane^feromoform

BromomethaneBte-ButanoneBârbon disulfide

Carbon tetrachloride_Chlorobenzene•Chlorodibromomethane•Chloroethane

ChloroformHChloromethane•l , 1 -Dichloroethane

1 ,2-Dichloroethane1,1-Dichloroethene

tis- 1 ,2-Dichloroethene-ans-1 ,2-Dichloroethene

1 ,2-Dichloropropane^:is-l ,3-Dichloropropene•trans-1 ,3-DichloropropeneÊthylbenzene

2-Hexanone•Methylene chloride

•4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

•Tetrachloroethene•Toluene

1,1,1 -Trichloroethanem\ , 1 ,2-Trichloroethane•Trichloroethene^Trichlorofluoromethane

Vinyl acetateHVinyl chlorideJTotal Xylenes

Surrogate: Dibromofluoromethaneûrrogale: 1 ,2-Dichloroelhane-d4

1 !





B107129-031070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.00

" 5.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7,20/01 13:41

Result Units Notes*

Soil G3.G4.02103 ug/kg ANDNDNDND

19.9 " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND


I

jreaj Lakess Analytical


"Refer 10 end of report for text of notes and definition.'*.

Page 11 of 70

I





Analyte

B19-5 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei





B107129-031070296 7/17/01 7/17/01 82.0-121

le " " " 76.8-113


Result

94. 179.7

7/9/01 t7/11/017/20/01

Units

Soil%

07/10/01

13:41

Notes*

G3.G4.O2

Great Lakes Analytical "Refer to end of report for text of notes and definition

Andy Johnson, PToject Manager Page 12 of




11

1 Hygieneering, Inc.^7575 Plaza Court•Willowbrook, IL 605219

_JAnalyte

fcl9-9Acetone

^BenzeneBiromodichloromethane^Bromoform

Bromomethane

§-Butanonearbon disulfide

Carbon tetrachloride^Chlorobenzene•Chlorodibromomethane•Chloroethane

ChloroformfChloromethane•1,1-Dichloroethane


»:is-l, 2-Dichloroethene^rans-1 ,2-Dichloroethene

1 ,2-DichloropropaneMpis-1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene^Ethylbenzene

2-Hexanone•Methylene chloride•4-Methyl-2-pentanone


•Tetrach 1 oroeth en e•Toluene

1,1.1 -Trichloroethanemt\ ,1 ,2-Trichloroethane•Trichloroethene

1 richlorofluoromethaneVinyl acetate

t'inyl chlorideotal Xylenes


( arrogate: / ,2-Dichloroethane-d4

rett Lakes Analytical





B107129-041070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

"Refer to end of i


Result Units Notes*

Soil G3.G4ND ug/kgNDNDNDNDNDNDNDNDND

12.2NDND

7.15NDND

5.68NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

5.41ND104 %128

•eport for text of notes and definitions.

I \.Andy\Johnson, Project Manager Page 13 of 70

I





Analyte

B19-9 (continued)Surrogate: Toluene-dSSurrogate: 4-Bromofluorobenzene

Project: 2001-3495 Sampled: 7/9/01 to 7Project Number: N/A Received: 7,11/01

Project Manager: Gary Milkeris Reported: 7/20/01 13


Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units

B107129-04 Soil1070296 7/17/01 7/17/01 82.0-121 97.8 %

76.8-113 91.4

10/01

41

Notes*

G3,G4

Grew Lakes Analytical "Refer to end of report for text of notes and definitions.

Andy Johnson. Project Manager Pace 14 of 70




1I

1 Hygieneering, Inc.^7575 Plaza CourtBw-illowbrook. IL 60521V

•1T_iAnalyte

luAcetone

•Benzene•Sromodichloromethane^Sromoform

Bromomethane

t-Butanonearbon disultlde

Carbon tetrachloride^Chlorobenzene•Chlorodibromomethane^Chloroethane

Chloroform•Chloromethanell , 1 -Dichloroethane

1 ,2-Dichloroethane^J ,1 -Dichloroethene•;is-l ,2-DichloroetheneBrans- 1 ,2-Dichloroethene

1 ,2-Dichloropropane•pis- 1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene^Ethylbenzene

2-Hexanoner ethylene chlorideMethyl-2-pentanone

Styrene^1 ,1 ,2,2-Tetrachloroethane•Tetrach 1 oroethen e•Toluene

1,1,1 -Trichloroethane• 1 , 1 ,2-Trichloroethane•Trichloroethene^"richlorofluoromethane

Vinyl acetate•Vinyl chlorideIfTotal Xylenes


C irrogale: 1.2-Dich/oroelhane-d4

reat ^.akes Analytical


Proj ect M anager: Gary M i Ikeri s



B107129-051070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

"Refer to end of


Result

43.4NDNDNDNDNDNDNDNDND10.7NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND103123

7/9/01 to 7/1 0/017/11/017/20/01 13:41

Units Notes*

Soil G3.G4ug/kg A11

11

11

"

:M"„n••**""""„"..n"""••"..%

report for text of notes and definitions.

IAndy Jphnson, Project Manager Page 15 of 70

I

&s*£-£(^_^|JTZT _r!rr H

$1GREATLAKESANALYTICAL



Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 6052 1

Analvte






Bl 07 129-051070296 7/17/01 7/17/01 82.0-121

76.8-113


Result

99.592.1

7/9/01 to 77/11/017/20/01 13

Units

Soil%

10/01

41

Notes*

G3.G4

Great\Lakes Analytical "Refer to end of report for text of notes and definitions.

Andy lohrtson. Project Manager Page 16 of 70

GREATLAKES

(ANALYTICAL 1380 Busch ParkwayBuffalo Grove, Illinois 60089


11iHygieneenng, Inc.^575 Plaza Court•Villowbrook, IL 60521I

§1TlAnalyte

•20-14Acetone

BenzeneRromodichloromethaneTiromoformBromomethane


Carbon tetrachloride^hlorobenzeneKhlorodibromomethanefthloroethane

Chloroformrhloromethane1 -Dichloroethane

,2-Dichloroethane1,1-Dichloroethene

R- 1 ,2-Dichloroethenens-1 ,2-Dichloroethene

1 ,2-Dichloropropane^is- 1 ,3-Dichloropropenetans-1 ,3-Dichloropropeneftthylbenzene2-Hexanoner ethytene chloride

Methyl-2-pentanoneStyreneJ ,1 ,2,2-Tetrachloroethane•"etrach 1 oroeth ene•"oluene

1,1,1 -Trichloroethaney ,1 ,2-Trichloroethane•"richloroetheneTrichlorofluoromethaneVinyl acetate

f invl chloride-otal Xylenes

Surrogate: DibromofluoromethaneSurrogate: l,2-Dichloroelhane-d4

I 1^jreat Lakes Analytical





B107129-061070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

"Refer to end o


Result Units Notes*

Soil G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND112 %121

f report for text of notes and definitions.

iAndy JoHnscMi, Project Manager Page 17 of 70

I

-.-•GREAT•All LAKES•Sil ANALYTICAL




Analvte

B20-14 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzet





B107129-061070296 7/17/01 7/17/01 82.0-121

te " " " 76.8-113


Result

97.596. 1

7/9/01 to 7/1 0/017/11/017/20/01 13:41

Units

Soil%

Notes*

G3.G4

Great Lakes Analytical 'Refer to end of report for text of notes and definitions.

Andy Johnson. Project Manager Page I X of 70




11

1 Hygieneenng, Inc.^7575 Plaza CourtBWillowbrook, IL 605219

|

:

Acetone^Benzene•Bromodichloromethane^Bromoform

Bromomethaneto-Butanone•Carbon disulfide

Carbon tetrachloride^ Chlorobenzene•Chlorodibromomethane•Chloroethane

ChloroformMChloromethane•1 , 1 -Dichloroethane


f s-l,2-Dichloroethenean s-1 ,2-Dichloroethene

1 ,2-Dichloropropanegpis-l,3-DichloropropeneBrans- 1 ,3-Dichloropropene^thylbenzene

2-Hexanone

tlethvlene chloride-Methyl-2-pentanone



1,1,1 -Trichloroethane•1 , 1 ,2 -Trichloroethane•TrichloroetheneTYichlorofluoromethane

Vinyl acetatePt'inyl chloride[Total XylenesSurrogate: Dibromofluoromethane

^urrogate: 1 . 2-Dichloroelhane-d4

1 <





B107129-071070323 7/18/01 7/17/01 2500

500500500500

1000500500500500500500500500500500500500500500500500

1000500

1000500500500500500500

10000500

1000500500

81.2-13450.8-145

Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7.20/01 13:41

Result Units Notes*

Soil GI2.G19.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

3650NDNDNDNDNDND845 " ANDNDND971NDNDND

591000NDND

1330ND122 %1 10

jreat Lakes AnalyticalS



Page 19 of 70

mGREATLAKESANALYTICAL







7/9/01 to 7/1 0/017/11/017/20/01 13:41


Analyte

B2 1-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei


B107129-071070323 7/18/01 7/17/01 82.0-121

te " " " 76.8-113

Result

113118

Units

Soil%

Notes*

C12.G19.G3.G4

O5

Great Lakfcs Analytical Refer to end of report for text of notes and definitions.

Andy Johrrson. Project Manager Page 20 of 70




11

1 Hygieneering, Inc.1?5 75 Plaza CourtpVillowbrook, IL 60521I

•T^Analvte

|22.3

AcetoneBenzeneBjromodichloromethaneTiromoform

Bromomethane


Carbon tetrachloride^ThlorobenzenethlorodibromomethanePfchloroethane

ChloroformfeChloromethane• ,1 -Dichloroethane~i ,2-Dichloroethane

1,1-DichloroetheneKs-l,2-Dichloroethene^rans-l ,2-Dichloroethene


El ,3-Dichloropropenes-1 ,3-Dich)oropropeneylbenzene

2-Hexanone•Methylene chloride•-M ethyl-2-pentanone

StyreneJ,l,2,2-Tetrachloroethane•"etrach 1 oroeth en e•"oluene


(, 1 ,2-Trichloroethanerichloroethenerichlorotluoromethane

Vinyl acetate


Surrogate: Dibromofluoromethane^urrogate: 1 ,2-Dichloroethane-d4


Project Manager: Gary M ilkeris



Bl 07 129-081070323 7/18/01 7/18/01 1250

250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250

" " " 500250250

81.2-13450.8-145

Sampled: 7/9,01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41

Result Units Notes*

Soil G12.CI9.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND411NDNDNDNDNDNDNDNDNDNDNDNDNDND

4750NDND511ND110 %

97.7

K5tt Lakes Analytical

Andly Jbhhson, Project Manager


Page 21 of 70

I





Analvte

B22-3 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzer





B107129-081070323 7/18/01 7/18/01 82.0-121

le " " " 76.8-113


Result

98.597.9

7/9/01 t7/11/017,20/01

Units

Soil%

0 7 / 1 0 / 0 1

13:41

Notes*

G12.GI9.G3.G4

Great Lafces Analytical



Page 22 of 7(

> -,-• GREAT•All LAKES•&•• ANALYTICAL

IHygieneenng, Inc.l?575 Plaza Court

BVillowbrook, IL 60521

9

|

T1

lAnalyte

y22-15Acetone

^Jenzene•Jromodichloromethane^Bromotorm

Bromomethane|K-Butanone•Tarbon disulfide

Carbon tetrachlorideChlorobenzene

thlorodibromomethanehloroethane

ChloroformWThloromethane•i ,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene»is-l,2-Dichloroethene•ans- 1 ,2-Dichloroethene


E' -1,3-Dichloropropenens- 1 ,3-Dichloropropenenylbenzene

2-Hexanone

f lethylene chloride-Methyl-2-pentanonetyrene

1 , 1 ,2,2-Tetrachloroethane•Tetrach 1 oroeth ene^Toluene

1 , 1 ,1 -Trichloroethane

t, 1 ,2-Trichloroethanerichloroethenerichlorofluoromethane

Vinyl acetatefe/inyl chloride•Total Xylenes

Surrogate: Dibromofluoromethane^urrogate: 1 ,2-Dichloroethane-d4

1380 Busch ParkwayBuffalo Grove, Illinois 60089 (847)





B107129-091070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145



Result Units Notes*

Soil G3.G4.O243.5 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDND

9.45NDNDNDNDNDND

5.98 " ANDNDNDNDNDNDND149NDNDNDND/ 15 %124

Great Lakes AnalyticalI V

\Andy JihnVon, Project Manager


Page 23 of 7C

I

GREAT

1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772




Sampled: 7/9/01 to 7/10/01Received: 7/1 1/01Reported: 7/20/01 13:41


AnalyteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


B22-15 (continued) B107129-09 Soil G3.G4.O2Surrogate: Toluene-d8 1070296 7/77/07 7/77/01 82.0-121 "" 79.9 % O4Surrogate: 4-Bromofluorobenzene " " " 76.8-113 72.0 " O4

Great uftkes Analytical "Refer to end of report for text of notes and definitions.


I -.-B GREATf All LAKES

_ IBM ANALYTICAL•11

1 Hygieneering, Inc.^7575 Plaza CourtMvillowbrook, IL 60521V

1j

^Analvte

miM.Acetone

^Benzene•Jromodichloromethane^Jvomoform

Bromomethane


Carbon tetrachloride^Uhlorobenzene•ThlorodibromomethaneBfchloroethane

Chloroform•Chloromethane• ,1 -Dichloroethane^\ ,2-Dichloroethane

1 , 1 -Dichloroethene»is-l,2-Dichloroethenerans-l,2-Dichloroethene


E-l,3-Dichloropropenens- 1 ,3-Dichloropropenenylbenzene

2-Hexanone

f ethylene chlorideMethyl-2-pentanone

Styrene

f1 ,1,2,2-Tetrachloroethane

etrachloroetheneoluene


t,l,2-Trichloroethanerichloroethenerichlorofluoromethane

Vinyl acetate»inyl chlorideotal Xylenes

" Surrogate: Dibromofluoromethane^Surrogate: 1.2-Dichloroethane-d4

•^jreal Lakes Analytical






B107129-101070323 7/18/01 7/19/01 1250

7/17/01 250250250250500250250250250250250250250250250500250250250250250500250500250250250250250250250250500250250

81.2-13450.8-145

"Refer to end ofr



Result Units Notes*

Soil G12.G19.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

21300397NDNDNDND "ND431 " ANDNDNDNDNDNDND342NDND

2530ND159 % OS151 " 05

eport for text of notes and definitions.

IAndy Johnson, Project Manager Page 25 of 70

I

—,«• GREATtillLAKES

•&• ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772


Analvte






B107129-101070323 7/18/01 7/17/01 82.0-121

76.8-113


Result

138148

7/9/01 to 7/1 0/017/1 1/017/20/01 13:41

Units Notes*

Soil G1iGI9.GJ.G4% O5

05


Andy Jdbrtson, Project Manager Page 26 of 70

1 —^1 GREATi|S| LAKES•fill ANALYTICAL•1

Slygieneering, Inc.575 Plaza Court/illowbrook, IL 60521

|J.Analyte

»24-12Acetone

Benzene•Jromodichloromethane^Bromoform

Bromomethane

(•Butanonearbon disulfide

Carbon tetrachloride^Thlorobenzene•ThlorodibromomethaneHbhloroethane

Chloroform

(hloromethane,1 -Dichloroethane,2-DichIoroethane

1 , 1 -Dichloroethene•ris-l,2-Dichloroethene•rans-1, 2-Dichloroethene


Kis-1 ,3-Dichloropropeneans-1 ,3-Dichloropropenethylbenzene

2-Hexanone

Fethylene chlorideM ethy \-2-pentanone

StyreneJ ,1 ,2,2-Tetrachloroethane•TetrachloroetheneMfoluene

1,1,1 -TrichloroethaneM , 1 ,2-Trichloroethane•Trichloroethene^Trich lorofluoromethane

Vinyl acetate

t inyl chlorideotal Xylenes

Surrogate: Dibromofluoromethane^urro gale: 1 . 2-Dichloroethane-d4

1Wjreat Lakes Analytical






B107129-111070323 7/18/01 7/17/01 1250

250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250



Result


5590438NDNDNDNDND839NDNDNDNDNDNDND

7/9/01 to 7 /1 0/017/11/017/20/01 13:41

Units Notes*

Soil G12.G19.G3.C4ug/kg11

"""

"11

)(

"

it

»

11

11

:M""""

A-""••"""

7.20/01 25000 15600007/17/01 250

500250250

81.2-13450.8-145

NDND460ND103

94.6

""••%"


IAndy Jehnson, Project Manager Page 27 of 70

I








7/9/01 to 7/1 0,017/11/017/20/01 13:41


Analvte



B107129-111070323 7/18/01 7/17/01 82.0-121

76.8-113

Result

96.3102

Units

Soil G12.G19%

Notes*

.C3.G4

Great Lakes AnalyticalT!



Page 28 of 70

-;~1 GREATI LAKESI ANALYTICAL



IHygieneering, Inc.

^575 Plaza Court•Villowbrook, IL 60521




T Batch Date Date SurrogatejAnalyte Number Prepared Analyzed Limits

•bs-7 B107129-12Acetone 1070323 7/18/01 7/18/01

BenzeneBiromodichloromethane " " "^Bromoform " " "

Bromomethane " " "

§-Butanone " " "arbon disulfide " " "

Carbon tetrachloride " " "^Thlorobenzene " " "m?hlorodibromomethane " " "•Chloroethane " " "

Chloroform " " "•Chloromethane " " "• ,1 -Dichloroethane " " "

1 ,2-Dichloroethane " " "1,1-Dichloroethene " " "

•is-1, 2-Dichloroethene " " "•Vans- 1, 2-Dichloroethene " " "

1,2-Dichloropropane " " "îs-l,3-Dichloropropene " " "Brans- 1,3-Dichloropropene " " "

Lithylbenzene " " "2-Hexanone " " "

Ilethylene chloride " "-Methyl-2-pentanone " " "

Styrene " " "«,l,2,2-Tetrachloroethane " "etrachloroethene "oluene " " "

1 ,1 ,1 -Trichloroethane

K l,2-Trichloroethane " " "richloroethene " "richlorofluoromethane " "

Vinyl acetate " "

f inyl chlorideotal Xylenes " " "

Surrogate: Dibromofluoromethane " " " 81.2-134ûrrogale: 1.2-Dichloroethane-d4 " " " 50.8-145

îreat/Lakes Analytical

ReportingLimit

25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

"Refer to end oj

Result Units Notes*

Soil G19.G3.G481.7 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDND

37.0NDNDNDNDNDND

6.32 " ANDNDNDNDNDNDND

84.1NDND146ND137 % O5177 " 05

f report for text of notes and definitions.

Johnson, Project Manager Page 29 of 70

I

&3iWTIKUfi^ IB i

••• •••V i

^£l GREATLAKES

(ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772


Analyte






B107129-121070323 7/18/01 7/18/01 82.0-121

ie " " " 76.8-113


Result

123107

7/9/01 to 7,7/11/017/20/01 13:

Units

Soil%

10/01

Notes*

G19,G3,G4OS




Page 30 of 7C

-.-•GREAT1LAKES

[ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772

L_(Hygieneering, Inc.^575 Plaza Court

•Villowbrook, IL 60521





T Batch Date Date Surrogate^nalvte Number Prepared Analyzed Limits

^26-7 B107129-13Acetone 1070296 7/17/01 7/17/01

Benzene " " "•Jromodichloromethane " " "Hjromoform " " "

Bromomethane " " "•-Butanone " " "Karbon disulfide " " "

Carbon tetrachloride " " "_Chlorobenzene " " "

•Chlorodibromomethane " " "•Chloroethane " " "

Chloroform " " "

f^hloromethane,1-Dichloroethane " " ",2-Dichloroethane

1,1-Dichloroethene "•is-l,2-Dichloroethene " "^rans-1, 2-Dichloroethene " "

1,2-Dichloropropane " " "

E-l,3-Dichloropropene " " "ns-l,3-Dichloropropene " " "^ylbenzene " " "

2-Hexanone " " "

Klethylene chloride " " "-Methyl-2-pentanone " " "

btyrene " " "1 , 1 ,2,2-Tetrachloroethane "

Jetrachloroethene " " "oluene " " "

1,1,1 -Trichloroethane " " "

t, 1 ,2-Trichloroethane "richloroethene " " "richlorofluoromethane "

Vinyl acetate " " "

(inyl chloride " "otal Xylenes " "arrogate: Dibromofluoromethane " " " 81.2-134

^urrogate: 1.2-Dichloroethane-d4 " " " 50.8-145

ReportingLimit

25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005005005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.0500

5.00

Result Units Notes*

Soil G3.G4.O2125 ug/kg ANDNDNDNDNDNDNDNDNDNDNDND23.3ND

8.2711800 " G12

524 " G12NDNDNDNDND11.5 " ANDNDNDNDNDNDND

6.65NDND

2230 " G12ND134 %145

ireat Lakes Analytical

indy Johnson, Project Manager


Page 31 of 70

I




Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 6052 1




7/9/01 to 7/1 0/017/11/017/20/01 13:41


Analvte



B107129-131070296 7/17/01 7/17/01 82.0-121

ie " " " 76.8-1/3

Result

77.662.0

Units

Soil%

Notes*

G3.G4.O2O404

Great Uakes Analytical "Refer to end of report for text of notes and definitions.

Andy Joimson, Project Manager Page 32 of 7<




1I

[Hygieneering, Inc.^75 75 Plaza Court^Villowbrook, IL 60521

i

M

I

T1 Analyte

•327-13Acetone

^BenzeneBfromodichloromethane^feromoform

Bromomethane


Carbon tetrachloride.Chlorobenzene

•Thlorodibromomethane•Thloroethane

Chloroform••ThloromethaneB ,1 -Dichloroethane^ ,2-Dichloroethane

1 ,1 -DichloroethenejAis-1 ,2-DichloroetheneJpans-1 ,2-Dichloroethene


E-l,3-Dichloropropenens-1 ,3-Dichloropropenelylbenzene

2-Hexanone•dethylene chlorideBr-Methyl-2-pentanone

Styrene1 ,1 ,2,2-Tetrachloroethane

•TetrachloroetheneB^oluene


K,l ,2-Trichloroethanerichloroethenerich 1 orofluoromethane

Vinyl acetate»inyl chloride

otal Xylenes- - - • — -Surrogate: Dibromofluoromethane

^urrogate: !,2-Dichloroethane-d4





B107129-141070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145

Sampled: 7/9/01 to 7,10/01Received: 7,11/01Reported: 7/20/01 13:41

Result Units Notes*

Soil G3.G4.O238.8 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

7.08NDNDNDND101 %116

•eit Lakes Analytical



Page 33 of 70

I








B27-13 (continued)


AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits



B107129-141070296 7/17/01 " 7/17/01 82JJ-J~2T

76.8-113

Soil84.070.3

G3.G4.O2

O4



Page 34 of 70

|~^l GREAT•All LAKES•Sill ANALYTICAL•1

I| Hygieneering, Inc.

Jj5 75 Plaza Court•Viliowbrook, IL 60521m

tTJAnalyte

P28-4Acetone

BenzeneBromodichlorom ethane^Bromoform

BromomethaneV^Butanone•arbon disulfide

L'arbon tetrachlorideelorobenzenelorodibromomethaneloroethane

Chloroform•ChloromethaneV, 1 -Dichloroethane

n,2-Dichloroethane1,1-Dichloroethene

•is- 1 ,2-Dichloroethene(fans- 1 ,2-Dichloroethene


C-l,3-Dichloropropenens-1 ,3-Dichloropropenelylbenzene

2-Hexanone

Vethylene chlorideMethyl-2-pentanone

atyrene1 , 1 ,2,2-Tetrachloroethane

§etrachloroetheneoluene


t l,2-Trichloroethanerichloroethenerichlorotluoromethane

Vinyl acetate

K inyl chlorideotal Xylenes

Surrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4

I !**reaC:Lakes Analytical

M• i ^^ ~^~






B107129-151070262 7/13/01 7/13/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81. 2-13450.8-145


Sampled: 7/9/01 to 7, 10/01Received: 7 /11 /01Reported: 7/20/01 13:41

Result Units

Soil63.2 ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

11.5NDNDNDND113 %1 19

Notes* ''

G19.G4A


\ndy Johnson, Project Manager Page 3 5 of 70

I

—.—•GREAT•AllLAKES

•&• ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772






AnalvteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits



1070262 7/13/01^6107129-15

i/imi " 82.0-ni76.8-113

Soil G19.G4104

89.5

dy Johnson, Project Manager


Page 3 6 of 70

§ -.«• GREAT•All LAKES•fill ANALYTICAL

1Hygieneering, Inc.7575 Plaza Court

•Willowbrook, IL 60521

•

JAnalyte

JB28-13Acetone

—Benzene•Bromodichloromethane^Bromoform

BromomethaneM2-Butanone•Carbon disulfide


•Chlorodibromomethane•Chloroethane

Chloroform

(hloromethane,1 -Dichloroethane,2-Dichloroethane

1,1-Dichloroethene•:is-l ,2-DichloroetheneB^rans- 1 ,2-Dichloroetheme

1 ,2-Dichloropropane<pis- 1 ,3-Dichloropropene

Brans- 1 ,3-DichloropropeneBz thy (benzene

2-Hexanone•Methylene chloride^•t-Methyl-2-pentanone^ityrene

1 , 1 ,2,2-Tetrachloroethane

tetrachloroetheneoluene

1,1,1 -Trichloroethane1 , 1 ,2-Trichloroethane

•Trichloroethene"Trichlorofluoromethane

Vinyl acetate•Vinyl chloride•Total Xylenes

Surrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4

1 380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)



Volatile Organic Compounds by EPA Method 5035/8260B .Great Lakes Analytical


B107129-161070262 7/13/01 7/13/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.00

" " " 10.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

" " " 81.2-13450.8-145



Result Units Notes*

Soil G19.G429.6 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND119 %129

jreatlLakes Analytical



Page 3 7 of 70

I



(847) 808-7766 FAX (847) 808-7772





7/9/01 to7 /10 /7/11/017/20/01 13:41

01


Analvte



B107129-161070262 7/13/01 7/13/01 82.0-121

76.8-113

Result

83.066.3

Units

Soil%

Notes*

G19.G4

O4

Great Bakes Analytical! \



•—.—•GREAT•All LAKES

_ •&• ANALYTICAL11

1 Hygieneering, Inc.J7575 Plaza Court•vVillowbrook, IL 60521

•

|

lAnalvte

•329-10Acetone

•BenzeneBjromodichloromethane'^Bromoform

Bromomethane


Carbon tetrachloride_ChlorobenzeneB^hlorodibromomethane•Chloroethane

Chloroform•ChloromethaneB , 1 -Dichloroethane

1 ,2-Di chloroethane1,1-Dichloroethene

M:is-l, 2-DichloroetheneBrans- 1 ,2-Dichloroethene


K s-l ,3-Dichloropropeneans-1 ,3-Dichloropropenethylbenzene

2-Hexanone

f ethylene chlorideMethyl-2-pentanone


BretrachloroetheneBfoluene


t l ,2-Trichloroethanerichloroethene

i richlorofluoromethaneVinyl acetate

§inyl chlorideotal Xylenes

Surrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4

I >^jredt Lakes Analytical

f\

l\

1 iV~- —






B107129-171070296 7/17/01 7/17/01 25.0

5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-13450.8-145


Sampled: 7/9/01 to 7, 10,01Received: 7/11/01Reported: 7/20/01 13:41

Result Units

Soil41.7 ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

5.99NDNDNDNDNDNDNDNDNDNDNDNDNDND

36.7NDNDNDND113 %118

Notes*

G3.G4A



I

k«=**-*W;V BH

MGREATLArXLo 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772


Analvte






B107129-171070296 7/17/01 7/17/01 82.0-121

76.8-113


Result

93.880.3

7/9/01 to 7/1 0/017/11/017/20/01 13:41

Units

Soil

y°

Notes*

G3.G4



I ^.^H GREAT•All LAKES•Hii ANALYTICAL

1"THygieneering, Inc.

17575 Plaza Court•Willowbrook, IL 60521I

11

JAnalyte

BB30-11l B^ '"•

Acetone—BenzeneBjromodichloromethane•Bromotorm

Bromomethane•2-Butanone•Carbon disulfide


•Chlorodibromomethane•Chloroethane

ChloroformMjChloromethane•! , 1 -Dichloroethane™1 ,2-Dichloroethane

1,1-Dichloroethene•cis-1, 2-DichloroetheneBran s-1 ,2-Dichloroethene

1 ,2-Dichloropropane^f is- 1 ,3-Dichloropropene•rans-1 ,3-Dichloropropene•Ethylbenzene

2-Hexanone

f lethylene chloride-Methyl-2-pentanonetyrene

1 , 1 ,2,2-Tetrachloroethane•TetrachloroetheneBjoluene

1,1,1 -Trichloroethane•1 , 1 ,2-TrichloroethaneBrrichloroethene•Trichlorofluoromethane

Vinyl acetate


Surrogate: Dibromofluoromethane^urrogate: l.2-Dichloroelhane-d4

m- I•Jniit Lakes Analytical

• \

1 1 \i \/^

1380 Busch ParkwayBuffalo Grove, Il l inois 60089 (847)





B107129-181070323 7/18/01 7/17/01 2500

500500500500

1000500500500500500500500500500500

7/20/01 5007/17/01 500

500500500500

1000500

1000500500500500500500


Sampled: 7/9/01 to 7. 10/01 !

Received: 7/11/01Reported: 7/20/01 13:41

Result Units Notes*

Soil G12.GI9.G.1.G42580 ug/kg A


21900NDNDNDNDNDND938 " ANDNDND

4830NDNDND

25000 1160000500

1000500500

81.2-13450.8-145

NDND

1240ND139 % O5125



I

-.«• GREAT•All LAKES•Sll ANALYTICAL




Analvte






B107129-181070323 7/18/01 7/17/01 82.0-121

76.8-113


Result

129138

7/9/01 t7/11/017/20/01

Units

Soil%

o7/10/01

13:41

Notes*

G12.G19.G3.G4O5O5

Great llakes Analytical



Page 42 of 70




11Hygieneenng, Inc.75 75 Plaza Court[Willowbrook, IL 605211

|[Analyte

1830-25Acetone•BenzenebromodichloromethanewomoformBromomethane|2-ButanoneJGarbon disulfideCarbon tetrachlorideChlorobenzene

IChlorodibromomethaneChloroethaneChloroform

iChloromethanell , I -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

fcis-1 ,2-Dichloroethenefrans- 1 ,2-Dichloroethene

1 ,2-Dichloropropaneg:is-l ,3-Dichloropropene•rans-1 ,3-Dichloropropenetthylbenzene2-Hexanone

•Methylene chlorideR-M ethy 1-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane



( , 1 ,2-Trichloroethanefrichloroethenerrichlorofluoromethane

Vinyl acetate

§'inyl chloride'otal Xylenes

Surrogate: Dibromofluoromethane^urrogate: 1 . 2-Dichloroethane-d4





B107129-191070323 7/18/01 7/17/01 2500

500500500500

1000500500500500500500500500500500500500500500500500

1000500

1000500500500500500500500500

1000500500

81.2-13450.8-145


Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND835NDNDNDNDNDNDND

9950NDNDNDND165166

7/9/01 to 7, 10, 017/11/017/20/01 13:41

Units Notes*

Soil GI2.GI9.G3.C4ug/kg11

"""

»"»11

11

"n

••"""

n

11

A

11

"11

"""11

"

"% 05

O5

jjeat Lakes AnalyticalA



Page 43 of 7t

I






Proj ect M an ag er: Gary M i 1 k eri s



AnalyteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits



1070323 7/18/01B107129-19

"7/77/07 82.0-12176.8-113

Soil G12.GI9.G3.G4154 % O5161 " 05




Page 44 of 70




I Hygieneering, Inc.•7575 Plaza CourtJwillowbrook, IL 60521



Sampled: 7/9/01 to 7/10/01Received: 7,11/01Reported: 7/20/01 13:41

Dry Weight DeterminationGreat Lakes Analytical

gample Name Lab ID Matrix Result Units

J19-5

320-4

B31

B107129-03

B107129-05

Bl 07129-20

Soil

Soil

Soil

77.3

78.4

80.0

Great'jLaldes Analytical

Andy) Johnson, Project Manager Page 45 of 70

I









Date Spike SampleAnalyte Analyzed Level Result

Batch: 1070323 Date Prepared: 7/18/01Blank 1070323-BLK1Acetone 7/20/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "1,1-Dichloroethene "cis- 1 ,2-Dichloroethene "trans-1, 2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1,3-Dichloropropene "Ethylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "1,1,2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1,1,1 -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50.0

1Great Lkkek Analytical

QCResult


57..?


Extraction Method: EPA 5035B 1P/T1

ug/kg 1250250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250500250250

81.2-134 115


Andy Jdhnson, Project Manager Page 46 of 70




1iHygieneenng, Inc.JJ575 Plaza Court•Villowbrook, IL 60521

•



Volatile Organic Compounds by EPA Method 8260B/Qualiry ControlGreat Lakes Analytical

T1 Analyte

Hilank (continued)Surrogate: 1.2-Dichloroethane-d4

^urrogate: Toluene-dS^Surrogate: 4-Bromofluorobenzene

LCS»cctoneenzene

Bromodichloromethane^BromoformBjromomethaneB-Butanone

Carbon disulfide•parbon tetrachlorideBrhlorobenzene^Thlorodibromomethane

Chloroethane

§hloroformhloromethane

1,1 -Dichloroethane

t1 ,2-Dichloroethane, I -Dichloroetheneis- 1 ,2-Dichloroethene

trans- 1 ,2-Dichloroethene

1,2-Dichloropropaneis- 1 ,3-Dichloropropene

trans- 1 ,3-DichloropropeneEthylbenzene

B-HexanoneB^ethylene chloride


("tyrene,1 ,2,2-Tetrachloroethaneetrachloroethene

Toluene

1,1,1 -Trichloroethane, 1 ,2-Trichloroethane

TrichloroetheneJYichlorofluoromethane

1 I•jreat Laket AnalyticalA f \


1070323-BLK17/20/01 50.0

50.050.0

1070323-BS17/20/01 2500

2500250025GO25002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

QCResult

51.049.945.8

334030102590209032103930127023202200214033703500584

35902170200032002800311026503000232037902860333023202090218028002820281025402690

Reporting Limit Recov. RPD RPDUnits Recov. Limits

ug/kg 50.8-14582.0-12176.8-113

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241

% Limit % Notes*

70299.891.6

134120104

83.6128157

50.892.888.085.6135140

23.4144

86.880.0128112124106120

92.8152114133

92.883.687.2112113112102108


^ndy'Johnson, Project Manager Page 4 7 of 70







7/9/01 107/10/017/11/017/20/01 13:41


Analvte


LCS PUPAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-TetrachloroethaneTetrachloroetheneToluene

'Great Ldkas Analytical

u. \ j\


1070323-BS17/20/01 2500

2500750050.050.050.050.0

1070323-BSP17/20/01 2500

2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

QCResult

40301110728084.558.164.252.1

55903220303021902780430029002860233022702760396038803480275030603610329034102870315024503990309035702440220024203020


ug/kg 10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134

Recov.%

16144.497.1169116128104

NR129121

87.61 1 1172116114

93.290.8110158155139110122144132136115126

98.0160124143

97.688.096.8121

"Refer to end of report for text

RPDLimit

34541.442.057.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.4119

37.254.646.342.6

of notes

RPD% Notes*

50.37.2315.14.6714.29,1278.220.55.745.9020.412.1148

3.5323.641.611.816.49.238.144.885.455.138.407.255.045.1310.47.73

and definitions.

Page 4 8 of 70




I Hygieneering, Inc.JJS 75 Plaza CourtKvillowbrook. IL 60521





T DatelAnalyte Analyzed

Spike SampleLevel Result


RPDLimit

RPD% Notes*

B.CS DUD (continued) 1070323-BSD11,1,1 -Trichloroethane 7/20/01

t, 1 ,2 -Trichloroethane "richloroethene "richlorofluoromethane "

Vinyl acetate "Byinyl chloride "Bfotal Xylenes "

Surrogate: Dibromofluoromethane "^Surrogate: 1 ,2-Dichloroethane-d4 "•Surrogate; Toluene-d8 "^Surrogate: 4-Bromofluorobenzene "

250025002500250025002500750050.050.050.050.0

3430 ug/kg29602780265038304280762059.670.566.252.8

60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

1371181 1 1106153171102779141132106

44.253.243.5115

92.181.040.1

19.25.228.451.875.10118

4.92

IIIIIIIIireat Lakes Analytical



Page 49 of 70

I




Hygieneering, Inc.75 75 Plaza CourtWillowbrook. IL 60521




Semivolatile Organic Compounds by EPA Method 8270C/Qualiry ControlGreat Lakes Analytical

Analvte

Batch: 1070237BlankAcenaphtheneAcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-ChIoroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4.6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene






ug/kg 100100100100500100100100100100100100100100330100100100100100100100100100100100100100500100100100100330500500100


"Refer to end of report for text of notes and definitions .

Page 50 of 70




1THygieneering, Inc.

J7575 Plaza Court•Willowbrook, IL 60521

•


Project Manager:

2001-3495N/AGarv Milkeris


7/9/01 to7/10/7/11/017/20/01 13:41

01

Semivolatile Organic Compounds by EPA Method 8270C/Quality ControlGreat Lakes Analytical

| Date Spike Sample QC1 Analyte Analyzed Level Result Result

Blank (continued) 1070237-BLK12,6-Dinitrotoluene 7/17/01

J3i-n-octyl phthalate "•fluoranthene "^•'luorene "

Hexachlorobenzene "•hexachlorobutadiene "B-Iexachlorocyclopentadiene "

Hexachloroethane "Jndeno ( 1 ,2,3-cd) pyrene "Bsophorone "B2-Methylnaphthalene "

o-Cresol "•rn.p-Cresols "•Naphthalene "^^-Nitroaniline "

3-Nitroaniline "

K-Nitroaniline "itrobenzene "

2-Nitrophenol "^1-Nitrophenol "BvI-Nitrosodi-n-propylamine "^J-Nitrosodiphenylamine "

Pentachlorophenol "

(henanthrene "henolyrene "

1,2,4-Trichlorobenzene "•2, 4,5-TrichlorophenolB?,4,6-Trichlorophenol "

Surrogate: 2-Fluorophenol " 3400mSurrogate: Phenol-d6 " 3400USurrogate: Nitrobenzene-d5 " 1710^Surrogate: 2-Fluorobiphenyl " 1710

Surrogate: 2.4,6-Tribromophenol " 3400fKurrogate: p-Terphenvl-d 1 4 " 1710

LCS 1070237-BS1Acenaphthene 7/17/01 1690

^jreat Lakes Analytical

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

438109157179229312

611


ug/kg 100100100100100100100100100100100100100100500500500100100500100100500100100100100500100

10.0-109 12.910.0-1/5 3.2110.0-114 9.1810.0-106 10.519.3-88.7 6.7410.0-126 18.2

ug/kg 29.4-110 36.2



I

Page 51 of 70







Semivolatile Organic Compounds by EPA Method

Analvte

LCS (continued)AcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Ch!oro-3-methy!phenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a.h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 .4-Dichlorobenzene3,3'-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-ocryl phthalate

1—

Great Lakes


1070237-BS17/17/01 1690

1 69016901690169016901690169016901690169016901690169016901 690169016901690169016901 6901 6901 69016901 69016901690169016901 6901 69016901 6901 6901 69016901 690

Analytical

QCResult

605ND589212629750759774828613639636627

104063872918.9657665776657590796735671661662216695591624646475554526680691643

Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7.20/01 13:41

8270C7Quality Control


ug/kg 31.0-1105.00-11032.9-1105.00-11035.9-11040.3-11041.9-11015.0-11039.6-11029.1-11027.8-11010.8-11016.5-1105.00-13132.6-1105.00-1595.00-11033.5-11017.0-11030.6-11015.2-11036.1-11030.5-11015.3-11015.6-11016.2-11016.3-1105.00-11016.9-11015.8-11016.1-11015.3-11032.0-1106.14-1105.00-11032.1-11034.2-1105.00-124

Recov. RPD RPD% Limit °/o Notes*

35.8NR

34.912.537.244.444.945.849.036.337.837.637.161.537.843.11.1238.939.345.938.934.947.143.539.739.139.212.841.135.036.938.228.132.831.140.240.938.0

Great Lako^ Analytical

Andy/Johnson, Project Manager


Page 5 2 of 7(



(847) 808-7766 FAX (847) 808-7772

JHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521





JAnalyte

f r<* (continued)Fluoranthene

^Fluorene•Hexachlorobenzene^iexachlorobutadiene

Hexachlorocyclopentadiene•lexachloroethane•ndeno (1,2,3-cd) pyrene

Isophorone2-Methylnaphthalene

•s-CresolBn,p-Cresols

Naphthalene•p-Nitroaniline•3-Nitroaniline

4-NitroanilineNitrobenzene

tNitrophenolNitrophenol

N-Nitrosodi-n-propylamineJ'J-Nitrosodiphenylamine•"entaehlorophenol•"henanthrene

Phenol•PyreneB ,2,4-Trichlorobenzene

2,4,5-Trichlorophenol2,4,6-Trichlorophenol

mSurrogate: 2-FluorophenolIfurrogale: Phenol-d6

Surrogate: Nitrobenzene-d5mSurrogate: 2-FluorobiphenylmSurrogate: 2.4.6- Tribromophenol^Surrogate: p-Terphenyl-d 1 4

•Klatrix Spike(Acenaphthene

Acenaphthylene—Aniline

I•treat La/es Analytical


1070237-BS17/17/01 1690

16901 69016901690169016901690169016901690169016901690169016901 69016901 690169016901 6901 69016901 69016901 690

~"" 536033607690/69033601690

1070237-MS1 B1071 15-127/17/01 1700 ND

1700 ND1700 ND

QCResult

552631639635374679793513773653596613662360589623687561647494594606654

1170652632678

14001150640729

12701280

566561106


ug/kg 15.0-11030.1-11031.8-11011.1-1107.46-11010.6-11011.3-11828.0-11031.8-11020.3-1105.00-11027.0-11012.0-1105.00-1105.00-11027.3-11029.7-11010.4-11032.4-11031.2-1105.00-11035.4-11015.8-1105.00-16614.3-11014.3-11030.9-11010.0-10910.0-11510.0-11410.0-10619.3-88.710.0-126

ug/kg 5.00-1405.00-1315.00-110

"Refer to end ofrepor

32.737.337.837.622.140.246.930.445.738.635.336.339.221.334.936.940.733.2 '38.329.235.135.938.769.238.637.440.141.734.237.943.137.875.7

33.333.06.24

for text of notes and definitions.

Anuy Johnson, Project Manager Page 53 of 70

I






Project Manager:




Analvte

Matrix Spike (continued)AnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chloropheno!4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateFluorantheneFluorene


SampleResult

QC Reporting Limit Recov. RPD RPDResult Units Recov. Limits % Limit % Notes*

1070237-MS1 B107115-127/17/01 1700

1 7001 7001 7001 7001 70017001 7001 7001 70017001 7001 70017001 7001 7001 7001 7001 7001 7001 70017001 7001700170017001 7001 7001 7001 70017001 7001 7001 7001 70017001 7001 700

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

542 ug/kg442572665671696749619630609591997

588689275693610778604540732674627619622263734586655636498590583654661653504572

5.00-1465.00-1495.00-1495.00-1345.00-1275.00-2235.00-1208.91-11023.1-11016.6-11014.5-1105.00-1535.00-1525.00-2165.00-11017.8-1105.00-1175.03-1285.00-1105.00-1555.00-1645.00-1335.00-1175.00-1105.00-1105.00-11021.5-1105.00-1125.00-12214.4-1145.00-1175.00-1265.00-14016.2-1105.00-1355.00-1705.00-1105.00-130

31.926.033.639.139.540.944.136.437.135.834.858.634.640.516.240.835.945.835.531.843.139.636.936.436.615.543.234.538.537.429.334.734.338.538.938.429.633.6




Page 54 of 70



(847) 808-7766 FAX (847) 808-7772

11

1 Hygieneering, Inc.J75 75 Plaza CourtMvillowbrook, IL 60521



Sampled: 7/9/01 to 7/10/01Received: 7/1 1/01Reported: 7/20/01 13:41

• Semivolatile Organic Compounds by EPA Method 8270C7Quality Control! Great Lakes Analytical

.nalvte

latrix Spike (continued)Hexachlorobenzene

Kexachlorobutadieneexachlorocyclopentadieneexachloroethane

Indeno (1,2,3-cd) pyrene»sophorone-Methylnaphthalene

o-Cresol

f,p-Cresols>r

aphthalene•Nitroaniline

3-NitroanilineMt-NitroanilineBjitrobenzene^-Nitrophenol

4-NitrophenolBk•^•Nitrosodi-n-propylamine^J-Nitrosodiphenylamine

Pentachlorophenol^fhenanthreneVhenol^"yrene

1 ,2,4-Trichlorobenzene

1,4,5-Trichlorophenol,4,6-Trichlorophenol

Surrogate: 2-Fluorophenol^urrogate: Phenol-d6^Surrogate: Nilrobenzene-d5^Surrogate: 2-Fluorobiphenyl

Surrogate: 2.4.6- Tribromophenolmfurrogale: p-Terphenvl-d 1 4

I~1atrix Soike DUDAcenaphthene

tcenaphthyleneni l ine

Anthracene^Jenzoic acid



RPD RPDLimit % Notes*

1070237-MS1 B107115-127/17/01 1700

1 7001 70017001 7001 7001 7001 7001 7001 7001 70017001 7001 7001 7001 7001 7001 7001 7001 7001 7001 7001 70017001 700339033901 700170033901700

1070237-MSD1 B10717/17/01 1670

16701 67016701670


15-12NDNDNDNDND

582 ug/kg601321622709538714667624579633535625599717646622501661549679

1090627688697

14501280600574

12201120

218 ug/kg221

26.4208168

5.00-1175.00-1105.00-1105.00-1105.00-16923.1-1105.00-1375.00-1285.00-1315.00-12618.1-1105.00-11015.8-11014.4-1105.00-1205.00-12423.2-1105.00-1275.00-1145.00-13723.7-1105.00-4025.00-11011.6-11318.8-11010.0-10910.0-11510.0-11410.0-10619.3-88.710.0-126

5.00-1405.00-1315.00-1105.00-1465.00-149

34.235.418.936.641.731.642.039.236.734.137.231.536.835.242.238.036.629.538.932.339.964.136.940.541.042.837.835.333.836.065.9

13.113.21.5812.510.1

81.8 87.173.0 85.7116 119

98.1 87.478.8 88.1

Ijreat Lakerf Analytical

// 'i

Andy^Johnson, Project Manager


Page 5 5 of 70

I






Project Manager:




Analyte

Matrix Spike DUD (continued)Benz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-BromophenyI phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2.4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneH ex ach 1 oroben zeneHexachlorobutadiene


SampleResult


RPDLimit

RPD% Notes*

1070237-MSD1 B1071 15-127/17/01 1670

16701670167016701670167016701 670167016701670167016701670167016701670167016701670167016701670167016701 6701670167016701670167016701 6701 6701 67016701670

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

227 ug/kg243267229

324270262266265852222222

94.4294238281238208227267258254263220247174332237119260310273268349

200228219

220

5.00-1495.00-1345.00-1275.00-2235.00-1208.91-11023.1-11016.6-11014.5-1105.00-1535.00-1525.00-2165.00-11017.8-1105.00-1175.03-1285.00-1105.00-1555.00-1645.00-1335.00-1175.00-1105.00-1105.00-11021.5-1105.00-1125.00-12214.4-1145.00-1175.00-1265.00-14016.2-1105.00-1355.00-1705.00-1105.00-1305.00-1175.00-110

13.614.616.013.719.416.215.715.915.951.013.313.35.6517.614.316.814.312.513.616.015.415.215.713.214.810.419.914.27.1315.618.616.316.020.912.013.713.113.2

124124121121107103

86.083.480.8115

70.792.3196100

77.777.473.0122105

76.284.984.086.6146

81.075.8145

77.1107

97.425.685.789.676.1142

79.579.582.0

84.791.284.799.677.876.881.177.074.613.988.9101

96.679.586.192.785.187.1104

84.982.282.279.916.097.9107

63.789.9122

75.959.481.083.459.084.684.189.291.4


Andy JoKnson, Project Manager


Page 56 of 71

I tzssm GREAT•All LAKES•fill ANALYTICAL

1


^7575 Plaza Court•Villowbrook, IL 60521

1380 Busch ParkwayBuffalo Grove, Il l inois 60089


Project Manager:

2001-3495N/AGar,' Milkeris



BSemivolatile Organic Compounds by EPA Method 8270C/Quality Control

1 Great Lakes Analytical

.nalvte

latrix Spike Pup (continued)Hexachlorocyclopentadiene«exachloroethane

ideno (1,2,3-cd) pyreneophorone

2-Methylnaphthalene

tCresol,p-Cresols

Naphthalene^2-NitroanilineB-NitroanilineBl-Nitroaniline

Nitrobenzened£-NitrophenolB-Nitrophenol

r4-Nitrosodi-n-propylamineN-Nitrosodiphenylamine

f entachlorophenolhenanthrene

PhenolJyreneB ,2,4-Trichlorobenzene^1,4,5-Trichlorophenol

2,4,6-Trichlorophenol

f arrogate: 2-Fluorophenolurrogate: Phenol-d6urrogate: Nitrobenzene-dS

Surrogate: 2-Fluorobiphenyl^turrogate: 2,4.6- TribromophenolB-urrogafe: p-Terphenyl-d!4

1

1

I*Creat LakesAnalvtical

1 ///


SampleResult

QCResult


Recov.%

RPDLimit

RPD% Notes*

1070237-MSD1 B107115-127/17/01 1670

1670167016701670167016701670167016701670167016701670167016701670167016701670167016701670

334033401670167033401670

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

155259236142284190173237253218302257317264193127304

.220240438238270318677418250184507377

ug/kg 5.00-1105.00-1105.00-16923.1-1105.00-1375.00-1285.00-1315.00-12618.1-1105.00-11015.8-11014.4-1 105.00-1205.00-12423.2-1105.00-1275.00-1145.00-13723.7-1105.00-4025.00-11011.6-11318.8-11070.0-70910.0-11510.0-11410.0-106

19.3-88.710.0-126

9.2815.514.18.5017.011.410.414.215.113.118.115.419.015.811.67.6018.213.214.426.214J16.219.020. 112.515.011.015.222.6

71.290.3107

84.671.786.192.875.689.31 1 1

99.984.285.155.293.574.370.7141

88.0157

76.779.388.2

68.381.098.9115

84.7110112

82.484.582.568.178.375.882.5104118

72.584.093.983.988.385.773.3



I









Analvte

Batch: 1070277BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole




76.6 16.0



ug/kg 100200100100

90.0100100100100

90.0100100100100100100

29.0-132 96.4


1070277-BS17/17/01 67.2

67.267.267.267.267.267.267.267.267.267.267.267.267.267.267.216.8

16.7 ug/kg81.650.860.551.658.060.861.861.659.652.749.761.872.757. Q9.6914.2

30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132

24.9121

75.690.076.886.390.592.091.788.778.474.092.0108

86.214.4

84.5

Great Lake* Analyticalke» Anal;



Page 58 of 7(

LAKESANALYTICAL




^7575 Plaza Court•Willowbrook, IL 60521B


Project Manager:



7/9,01 to 7, 107/11/017/20/01 13:41

01


Unalyte

•Matrix SoikeAcenaphthene

^Acenaphthylene•Anthracene^feenz (a) anthracene

Benzo (a) pyrene

f enzo (b) fluorantheneenzo (ghi) perylene

Benzo (k) fluoranthene^Zhrysene•Dibenz (a,h) anthraceneB^luoranthene

Fluorene| ndeno (1 ,2,3-cd) pyrene

•Naphthalenei^henanthrenePyrene

VKurrogate: Carbazole

Matrix Spike DUD—Acenaphthene•Acenaphthylene"Anthracene

Benz (a) anthracene•Benzo (a) pyrene•Benzo (b) fluoranthene

Benzo (ghi) peryleneBenzo (k) fluoranthene

BrhryseneB)ibenz (a,h) anthracene

Fluoranthene•rluorene•ndeno (1,2,3-cd) pyrene^Japhthalene

Phenanthrene

§yreneurrogate: Carbazole


SampleResult


RPDLimit

RPD% Notes*

1070277-MS1 B1071 15-057/17/01 68.4

68.468.468.468.468.468.468.468.468.468.468.468.468.468.468.4

" ~ 77.7

1070277-1MSD17/17/01 64.9

64.964.964.964.964.964.964.964.964.964.964.964.964.964.964.916.2


Bl 07 11 5-05NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

45.3 ug/kg103

55.4119

54.957.647.357.967.049.678.351.460.180.358.176.4Tl.8

25.5 ug/kg39.443.256.347.747.043.446.269.346.570.345.959.781.253.381.49.33

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

66.2151

81.017480384.269.284.698.072.5114

75.187.9117

84.9112

69.0

39360.766.686.773.572.466.971.2107

71.6108

70.792.0125

82.1125

57.6

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

51.085.319.567.08.8415.13.3817.28.781.255.416.044.566.613.3511.0

jreat Lakes Anlajytical

IAnd/ Johnson, Project Manager

I


Page 59 of 70





Project: 2001-3495Project Number: N/AProject Manager: Garv Milkeris


Volatile Organic Compounds by EPA Method 503578260B/Qualiry ControlGreat Lakes Analytical

Date Spike SampleAnalvte Analyzed Level Result

Batch: 1070262 Date Prepared: 7/13/01Blank 1070262-BLK1Acetone 7/13/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethenecis-1, 2-Dichloroethene "trans- 1 ,2 -Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "1.1.2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1 ,1 ,1 -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50.0

QCResult


53.0


Extraction Method: EPA S035B IP/T1

ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-134 106

Great LakeyAnalytical

///



GREATLAKES



(847) 808-7766 FAX (847) 808-7772

1I

1 Hygieneering, Inc.J75 75 Plaza Court•Willowbrook, IL 60521



Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7,20/01 13:41

• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control• Great Lakes Analytical

^J Analyte

B3lank (continued)Surrogate: 1.2-Dichloroethane-d4

^^urrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene

LCS•Acetone^Benzene

Bromodichloromethane^romoform•BromomethaneB2-Butanone

Carbon disulfideg«Carbon tetrachlorideBrhlorobenzene^-hlorodibromomethane

ChloroethaneBChloroformBrhloromethane

1,1 -Dichloroethane

I1 ,2-Dichloroethane, 1 -Dichloroetheneis- 1 ,2-Dichloroethene

trans-1 . 2-Dichloroethene

§,2-Dichloropropaneis- 1 ,3-Dichloropropene

trans-1 ,3-DichloropropeneEthvlbenzene

B--HexanoneBviethylene chloride

4-Methyl-2-pentanoneMftyrene|l , 1 ,2,2-Tetrachloroethane

1 etrachloroetheneToluene

§,1 ,1 -Trichloroethane, 1 ,2-Trichloroethane

Trichloroethene^Trichlorofluoromethane

1 ,•breat La/es Analytical


1070262-BLK17/73/07 50.0

50.050.0

1070262-BS17/13/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

QCResult

54.052.357.3

57.953.057.857.826.164.447.754.056.659.440.049.121.843.956.150.248.744.454.358.566.152.860.045.358.953.356.458.051.851.455.552.7194


ug/kg 50.8-14582.0-12176.8-113

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241

"Refer to end of report


705705703

116106116116

52.2129

95.4108113119

80.098.243.687.8112100

97.488.8109117132106120

90.61181071131161041031 1 1105NR

r for text of notes and definitions./ 4//L

Antiy Johnson, Project Manager

I

Page 61 of 70






Project Manager:

2001-3495N/AGan.' Milkeris

Sampled: 7/9/01 to 7/1 0/01Received: 7/1 1/01Reported: 7/20/01 13:41


Analvte

LCS (continued)Vinyl acetateVinyl chlorideTotal XvlenesSurrogate: DibromofluoromethaneSurrogate: I,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTerrachloroetheneToluene

ti — _ — .


1070262-BS17/13/01 50.0

50.0150

50.050.050.050.0

1070262-BSDl7/17/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

Sample QC Reporting Limit Recov.Result Result Units

48.6 ug/kg53.5269

~' 47.3 "51.051.051.6

83.1 ug/kg49.849.355.563.450.946.734.452.455.434.946.918.443.647.950.650.545.950.849.755.149.955.554.755.750.155.451.X45.1

Recov. Limits

10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134

%

97.2107179

94.6102102103

16699.698.6

111127102

93.468.81051 1 1

69.893.836.887.295.8101101

91.8102

99.4110

99.81 1 11091 1 11001 1 1104

90.2

RPDLimit

34541.442.057.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.4119

37.254.646.342.6

RPD% Notes*

35.56.2316.24.4183.523.42.1244.37.346.9613.64.5816.9

0.68615.6

0.9953.633.326.6416.318.26.037.79

. 18.46 .116.761.7910.914.2


Andy Johnsort, Prdject Manager Page 62 of 7 C




1~J Hygieneering, Inc.J 75 75 Plaza Court•Willowbrook, IL 60521

•



Sampled: 7/9/01 to 7/1 0,01Received: 7/1 1/01Reported: 7,20/01 13:41


1•| Analyte

jpLCS DUD (continued')1,1,1 -Trichloroethane

f1 , 1 ,2-Trichloroethane

richloroethenerichlorofluoromethane

Vinyl acetate•Vinyl chloride•Total Xylenes

Surrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4

^Surrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene

•Batch: 1070296•Blank^Acetone

BenzeneBBromodichloromethaneBSromoform

Bromomethane^2-Butanone•Carbon disulfideBcarbon tetrachloride

Chlorobenzene•Chlorodibromomethane•Chloroethane

ChloroformChloromethane

11 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

^cis- 1 . 2-DichloroetheneBtrans-1 ,2-Dichloroethene™1 ,2-Dichloropropane

cis-1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene•Ethylbenzene

2-Hexanone_Methylene chloride

Great Lakes f


1070262-BSP17/17/01 50.0

50.050.050.050.050.0150

" "" " " "50.050.050.050.0

Date Prepared: 7/17/011070296-BLK17/17/01"""n

"

»

..11

"

„11

ii»"11

..11

Analytical

QCResult

42.251.047.9162

57.233.6205

50.257.749.349.7

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND


ug/kg 60.0-134 84.4 44.2 19.976.4-125 102 53.2 8.4561.8-132 95.8 43.5 9.1614.6-241 NR 115 18.010.0-161 114 92.1 15.957.9-143 67.2 81.0 45.760.0-141 137 40.1 26.681.2-134 10050.8-145 Iu382.0-121 98.676.8-113 99.4

Extraction Method: EPA 503SB tP/TI

ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.00

I

ircat Uakes Analytical

,' I/i/1



Page 63 of 70

I





Volatile

Analvte

Blank (continued)4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 , 1 ,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1 . 1 -Dichloroethenecis-1 . 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropene


Project Manager:



Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical

Date SpikeAnalvzed Level

1070296-BLK17/17/0111

"nn11

"""ii11

11

" 50.0~'50.050.050.0

1070296-BS17/17/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

Sample QC Reporting Limit Recov. RPD RPDResult Result Units

ND ug/kgNDNDNDNDNDNDNDNDNDNDND

' 55.0 "55.357.652.5

83.8 ug/kg51.251.753.247.966.346.247.351.152.033.847.434.044.649.249.650.446.951.854.5

Recov. Limits

10.05.005.005.005.005.005.005.005.0010.05.005.00

81.2-~13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-124

°/o Limit % Notes*

7/0/ / /703705

168102103106

95.8133

92.494.6102104

67.694.868.089.298.499.2

10193.8104109

Great Lakes/\nalytical "Refer to end of report for text of notes and definitions

Andy Johnson, Project Manager Paue64 of 7<

*-AKE5


Buffalo Grove. Illinois 60089Email: [email protected]

(847) 808-7766 FAX (847) 808-7772

1fHygieneering, Inc.

J7575 Plaza Court•Willowbrook, IL 60521



Sampled: 7Received: 7Reported: 7

\

/9/OI to 7. 10/01/1 1/01/20/01 13:41

• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control• Great Lakes Analytical

_[Analvte

I '•XS (continued)

trans-1 ,3-Dichloropropene^Ethylbenzene•2-Hexanone•vlethylene chloride


ttyrene, 1 ,2,2-Tetrachloroethane

TetrachloroetheneToluene

Bl ,1,1 -TrichloroethaneBl , 1 ,2-Trichloroethane

TrichloroetheneMjTrichlorofluoromethane•Vinyl acetate^^/inyl chloride

Total Xylenes

f urrogate: Dibromofluoromelhaneurrogate: 1 . 2-Dichloroethane-d4

Surrogate: Toluene-d8

C arrogate: 4-Bromofluorobenzene

CSDuDAcetone

•Benzene^promodichloromethane

Bromoform^Bromomethane•2-ButanoneBCarbon disulfide

Carbon tetrachlorideaChlorobenzeneBrhlorodibromomethane^3hloroethane

Chloroform

ff hloromethane,1 -Dichloroethane

1 ,2-Dichloroethane^1 , 1 -Dichloroethene

Date Spike Sample QC Reporting Limit Recov.Analyzed Level Result Result Units Recov. Limits %

1070296-BS17/17/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.0150

50.050.050.050.0

1070296-BSD17/17/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

62.6 ug/lcg48.459.947.558.049.753.252.348.247.454.649.2170

31.258.5253

50.257.657.552.4

82.1 ug/lcg52.252.560.667.557.746.338.056.460.344.949.118.745.151.749.8

63.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-129

12596.8120

95.0116

99.4106105

96.494.8109

98.4NR

62.4117169100103103105

164104105121135115

92.676.0113121

89.898.237.490.2103

99.6

RPDLimit

34541.442.057.461.9173126

43.539.041.690.343.571.84 1 . X68.647.5

RPD% Notes*

2.411.941.9213.234.014.5

0.21621.810.215.128.23.5258.11 . 1 !4.57

0.402



Page 65 of 70

I







7/9/01 to 7/1 0/017/11/017,20/01 13:41


Analyte

LCS Pup (continued)cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 ,1 ,1 -Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichiorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethdne-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Batch: 1070323BlankAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane


1070296-BSD17/17/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0150

50.050.050.050.0

Date Prepared: 7/18/011070323-BLK17/20/01"11

"11

""-""

QCResult

53.746.754.353.658.652.660.656.060.852.962.154.147.643.356.749.391.160.935.6269

50.357.649.049.3


ug/lcg 64.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

Recov.%

10793.4109107117105121112122106124108

95.286.6113

98.6182122

71.2179101103

98.098.6


NDNDNDNDNDNDNDNDNDNDND

ug/kg 1250250250250250500250250250250250

RPDLimit

39.343.038.141.557.242.7128

67.4119

37.254.646.342.644.253.243.5115

92.181.040.1

[P/T1

RPD% Notes*

5.770.427

4.691.856.618.13

0.83016.45.046.4315.72.821.259.043.60

0.20360.564.648.75.75

Great LakesAnalyticalesAnalytic

/i



Page 66 of 70




IJ Hygieneering, Inc.

^7575 Plaza CourtpVillowbrook, IL60521

•


Project Manager:



7/9/01 to 7/1 0/017/11/017,20/01 13:41

Volatile Organic Compounds by EPA Method 5035/8260B7Quality ControlGreat Lakes Analytical

T Date Spike Sample_|_Analyte Analyzed Level Result

Blank (continued) 1070323-BLK1Chloroform 7/20/01

jChloromethane "B , 1 -Dichloroethane "™ ,2-Dichloroethane "

1,1-Dichloroethene "

(is- 1, 2-Dichloroethene "-ans- 1 ,2-Dichloroethene "

1 ,2-Dichloropropane "^;is-l,3-Dichloropropene "Brans- 1 ,3-Dichloropropene "Btthylbenzene "

2-Hexanone "||vlethylene chloride "•l-Methyl-2-pentanone "^Styrene "

1 , 1 ,2,2-Tetrachloroethane "

tetrachloroethene "oluene "

1,1,1 -Trichloroethane "J , 1 ,2-Trich 1 oroethane "•Trichloroethene "^Trichlorofluoromethane "

Vinyl acetate "

f inyl chloride "otal Xylenes "

Surrogate: Dibromofluoromethane " 50.0^urrogate: 1.2-Dichloroethane-d4 " 50.0^Kurrogate: Toluene-d8 " 50.0Wfurrogate: 4-Bromofluorobenzene " 50.0

QCResult


57.351.049.945.8


ug/kg 250250250250250250250250250250250500250500250250250250250250250250500250250

81.2-134 11550.8-145 10282.0-121 99.876.8-113 91.6

•LCS•\cetone^Benzene

Bromodichloromethane»romoformromomethane

2-Butanone^Tarbon disulfide

1070323-BS17/20/01 2500

250025002500250025002500

3340301025902090321039301270

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-175

13412010483.612815750.8

jreat LaWs Analvtical



Page 67 of 70









Analvte

LCS (continued)Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroeth eneToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCS DimAcetoneBenzeneBromodichloromethane

Date Spike SampleAnalvzed Level Result

1070323-BS17/20/01 2500

250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500750050.050.050.050.0

1070323-BSD17/20/01 2500

25002500

QC Reporting Limit Recov. RPD RPDResult Units

2320 ug/kg2200214033703500

5843590217020003200280031102650300023203790286033302320209021802800282028102540269040301 1 1 0728084.558. 164.252. 1

5590 ug/kg32203030

Recov. Limits

51.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10.0-16662.1-13864.3-125

% Limit % Notes*

92.888.085.6135140

23.4144

86.880.0 .128112124106120

92.8152114133

92.883.687.2112113112102108161

44.497.1169116128104

NR 345 50.3129 41.4 7.23121 42.0 15 .1

Great LaJ/es Analytical



Page 68 of 70




1IHygieneering, Inc.17575 Plaza Court[Willowbrook, IL 60521



Sampled: 7/9/0 1 to 7, 1 0/0 1Received: 7 /11 /01Reported: 7,20/01 13:41


1

Cnalyte

CS Pup (continued)Bromoformbromomethanep-ButanoneCarbon disulfideCarbon tetrachloride[ChlorobenzenefchlorodibromomethaneChloroethane•ChloroformjChloromethane1 , 1 -Dichloroethane1 ,2-DichIoroethane

11 , 1 -Dichloroethene|eis-l ,2-Dichloroethenetrans-1 ,2-Dichloroethene|) ,2-Dichloropropanepis-1 ,3-DichloropropeneTrans-1 ,3-DichloropropeneEthylbenzene

fc-HexanoneIvlethylene chloride4-Methyl-2-pentanone

^tyrene

1 , 1 ,2,2-Tetrachloroethaneiretrach 1 oroeth en eToluene

•1,1,1 -Trichloroethane•1 , 1 ,2-TrichloroethaneTrichloroethene

TrichlorofluoromethanePv'inyl acetatetyinyl chlorideTotal Xylenes

^urrogate: Dibromofluoromethane^Surrogate: 1.2-Dichloroethane-d4^Surrogate: Toluene-d8Surro gate: 4-Bromofluorobenzene

1Great Lake/ Analytical



1070323-BSD17/20/01 2500

2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

250025002500250025002500250025002500750050.050.050.050.0

QCResult

21902780430029002860233022702760396038803480275030603610329034102870315024503990309035702440220024203020343029602780265038304280762089.670.566.252.8


ug/kg 47.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

Recov.%

87.61 1 1172116114

93.290.8110158155139110122144132136115126

98.0160124143

97.6

88.096.8121137118111106153171102179141132106

"Refer to end of report for text

RPDLimit

57.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.4119

37.254.646.342.644.253.243.5

11592.181.040.1

of notes

RPD% Notes*

4.6714.29.1278.220.55.745.9020.412.1148

3.5323.641.611.816.49.238.144.885.455.138.407.255.045.1310.47.7319.25.228.451.875.10118

4.92

and definitions


I

GREAT

1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

Hygieneering, Inc. Project: 2001-3495 Sampled: 7/9,01 to 7 10.017575 Plaza Court Project Number: N/A Received: 7/11/01Willowbrook, IL 60521 Project Manager: Gary Milkeris Reported: 7,20/01 13:41


_# Note




Gl 5 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.

G19 The relative percent difference (RPD) of one or more anaiytes in the laboratory control QC (BS/BSD) associated with this sampleis above the laboratory's established acceptance limits. Refer to the included QC reports for more detail.



G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory';established acceptance criteria. Refer to the included QC reports for more detail.

O2 One or more internal standard recoveries were below the method specified acceptance criteria.

04 The recovery for this analyle is below the laboratory's established acceptance criteria.




NR Not Reported


Recov. Recovery


Great La^es AnalyticalT /


ESI LAKESANALYTICAL

(847) 808-7766FAX (847) 808-7772

(414) 570-9460FAX (414) 570-9461

LAKhS

ANALYTICAL(847) 808-7766

FAX (847) 808-7772(414) 570-9460

FAX (414) 570-9461

Client: H£lflVff/n* B/// To: TAT: (STO/ 4 DAY 3 DAY 2 DAY 1 DAY 4 HRS

Address: 7^7 Address:D YES - TAT is critical


DATE RESULTS NEEDED:

I L - i ;pnw RFC.FIPT

Report to: QPhone »:Fa**:

State &Program:

Phone #: f JFax #: ? )

Deliverable Package Needed:D STD D Oilier

Air Bill No.

Project: 2cc4> - . 34 -5"

Sampler:

not BottlesPreservative Used

PO/Quote #:

JJF/ELD /D, LOCATION

LABOnATORYID NUMBER

^L

-^LPID-(fOP

7-10-0)

PID: 2-CO

3

X-~7

p/0-'7^IT - 13

P/D:

5J

P/D: 3XIT

P/D: XU -b

P/D:

UPID: ^10,000

X'U ftTcr- 2:5

PfD-g>.OOQ-7

10J

P/D: .f?a//A/QV*SH£

PL /

RECEIVED RECEIVED

COMMENTS:

RAGE " 2- OF

I

I

I

I

I

I

I

I

i

GREATLAI\CO 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

July 31, 2001

I


RE: 2001-3495

Dear Gary Milkeris

Enclosed ars the results of analyses for sample(s) received by the laboratory on July 19, 2001. If you have anyquestions concerning this report, please feel free to contact me.

Sincerely,

7,Andy JohnsonProject Manager

»,„• GREAT1LAKES



(847) 808-7766 FAX (847) 808-7772







B18

B21

B107244-01

B107244-02

Water

Water

7/13/01

7/13/01

GreatA-aKes Analytical


The results in this report apply to the samples analyzed in accordance with the chain of custody document.Tins analytical report must be reproduced in its entirety.

Page 1 of 1




1i

Hygieneering, Inc.

— 7575 Pla2a Court• Willowbrook, IL 60521f

1*T

1 Analyte

IBISAcetone

»BenzeneBromodichloromethaneBromoformBromomethane



Chloroform

IChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene

Icis- 1 ,2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane

— cis- 1 ,3-Dichloropropene• trans-1 ,3-DichloropropeneW Ethylbenzene

2-Hexanone

1Methylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane

• TetrachloroetheneQ Toluene


§1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate

§Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane

« Surrogate: \.2-Dichloroethane-d4

I





B107244-011070436 7/23/01 7/30/01 10.0

2.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00

91.1 '-11185.1-104


Result Units Notes*

Water G1S.G2.G20.G?54.6 ug/l ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " 'NDNDNDNDNDNDNDNDNDNDNDNDNDND

91.2 %IDS " O5

• Great Likes Analytical

IAndy lohnson, Project Manager


Page 2 of 11

I









Analvte-BatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


B18 (continuedSurrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1070436 7/23/01B107244-01

7/30/01 ~95.1-10589.6-105

Water G15.G2.G20.G3"108 % OS105

Greht Lakes Analytical



Page 3 of 1




111



Project Manager:

2001-34952001-3495Garv Milkeris


7/13/017/19/017,31/01 11:52


gB21 Bl 07244-02Acetone 1070436 7/23/01 7/24/01

_ BenzeneH Bromodichloromethane " " "9 Bromoform " " "

Bromomethane " " "

12-Butanone " " "Carbon disulfide " " "Carbon tetrachloride " " "Chlorobenzene " " "

1Chlorodibromomethane " " "Chloroethane " " "Chloroform " " "

I Chloromethane " " "1,1-Dichloroethane1 ,2-Dichloroethane " "1,1-Dichloroethene

t cis-l,2-Dichloroethenetrans-1, 2-Dichloroethene " " "1 ,2-Dichloropropane " " "cis-l,3-Dichloropropene " " "

H trans- 1 ,3-Dichloropropene " " "1 Ethylbenzene " " "

2-Hexanone " " "

1Methylene chloride "4-Methyl-2-pentanone " " "Styrene1,1,2,2-Tetrachloroethane " " "

1Tetrachloroethene " " "Toluene " " "1,1,1 -Trichloroethane " " "

t l,l,2-Trichloroethane " "Trichloroethene "Trichlorofluoromethane " " "Vinyl acetate " " "

§Vinyl chloride " "Total XylenesSurrogate: Dibromofluoromethane " " " 9 I.I - I I I

-Surrogate: 1 .2-Dichloroethane-d4 " " " 85.I-HI4

I /

2000400400400400

2000400400400400400400400400400400400400400400400400

2000400

2000400400400400400400

10000400400400400

NDNDNDNDNDNDNDNDNDNDNDNDND632NDND

32200954NDNDNDNDNDNDNDNDNDNDNDNDND

937000NDND

6560ND

98.897.4

Water G12.G15.G2.G3ug/l11

..11

"""

11

:"""I!

"

G17G17

""

»11

"i,

"11

G17""

G16"

11

G17

%

'Great Lfikes/Analytical

^ 'l-i

"Refer to end of report for text (if notes and dc'finilu

AndyiJorrhson, Project Manager Page 4 of

I








Volatile Organic Compounds by EPA Method S260BGreat Lakes Analytical

AnalyteBatchNumber

DatePrepared

DateAnalyzed

SurrogateLimits


B21 (continued^ Bl 07244-02Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1070436 7/23/01 7/24/01 95.1-10589.6-105

10996.2

Water C12.C15.G2.G3% O5

Great L^kes Analytical

Andy JoVnson, Project Manager


Page 5 of 1

1111

—.—•GREAT•All LAKES•&• ANALYTICAL




Project Manager:

2001-34952001-3495Gary Milkeris



7/13/017/19/017/31/01 11:52


^ Date Spike SampleAnalvte Analyzed Level Result

• Batch: 1070436 Date Prepared: 7/23/01Blank 1070436-BLK1

_ Acetone 7/23/01B Benzene "™ Bromodichloromethane "

Bromotbrm "

1Bromomethane . "2-Butanone "Carbon disulfide "Carbon tetrachloride "

• Chlorobenzene "• Chlorodibromomethane "

Chloroethane "

1Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "

11,1-Dichloroethene "cis- 1 ,2-Dichloroethene "trans- 1 ,2-Dichloroethene "

_ 1,2-Dichloropropane "• cis-1 ,3-Dichloropropene "™ trans- 1 ,3-Dichloropropene "

Ethylbenzene "to 2-Hexanone "• Methylene chloride "

4-Methyl-2-pentanoneStyrene "

• 1,1,2,2-Tetrachloroethane "P Tetrachloroethene "

Toluene

11, 1,1 -Trichloroethane "1 ,1 ,2-TrichloroethaneTrichloroethene "Trichlorofluoromethane "

• Vinyl acetate "• Vinyl chloride "

Total Xylenes "^Surrogate: Dibromofluoromethane " 50.0

1 f

QCResult


46.8


Extraction Method: EPA S030B (P/T)

ug/l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00

91. 1-1 II 93.6

i Great Lakes Analytical

I

I

Anay Johnson, Project Manager Page 6 of 1 1




I

1Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521




Analvte

Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 .1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1.1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane

Great Lakes


1070436-BLK17/23/01 50.0

50.050.0

1070436-BS17/23/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

Analytical

QCResult

45.653.948.9

89.658.054.847.641.553.599.645.348.046.742.354.640.960.650.075.455.159.864.159.565.851.870.071.760.350.545.543.053.846.152.753.362.3




ug/l 85.1-10495.1-10589.6-105

ug/l 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.9-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-12086.3-12063.5-14684.5-12451.4-15310.0-586

i


i

91.2108

97.8

179116110

95.283.0107199

90.696.093.484.6109

81.8'121100151110120128119132104140143121101

91.086.0108

92.2105107125

Great Lak^ Analytical



Page 7 of 1 1




I1

Hygieneering, Inc._ 7575 Plaza Court• Willowbrook, IL 60521

•


Project Manager:

2001-34952001-3495Gary Milkeris


Volatile Organic Compounds by EPA Method 8260B/Quality Control

1^_ Analvte

1 '• LCS (continued)

Vinyl acetate

§Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4


_ Matrix Spike• Acetone• Benzene


t BromoformBromomethane2-ButanoneCarbon disulfide

• Carbon tetrachloride• Chlorobenzene


IChloroethaneChloroformChloromethane1 , 1 -Dichloroethane

t l ,2-Dichloroethane1 ,1 -Dichloroethenecis-1 ,2-Dichloroethene

^ trans-1, 2-Dichloroethene• 1,2-DichloropropaneB cis-l,3-Dichloropropene

trans-1 ,3-Dichloropropene

I Ethylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone

• Styrene• 1 . 1 ,2,2-Tetrachloroethane

Tetrach 1 oroethene^ Toluene

Great Lakes


1070436-BS17/23/01 50.0

50.0150

50.050.050.050.0

SampleResult

Analytical

QCResult

39.443.7153

44.744.846.345.0


ug/l 10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105


78.887.4102

89.489.692.690.0

1070436-MS1 B107220-017/26/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

52.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

66.448.448.941.014.140.151.137.049.345.768.149.327.944.849.015.451.442.549.944.936.949.849.344.750.049.352.148.449.4

ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20849.7-12620.6-22345.1-11371.3-118

27.696.897.882.028.280.2102

74.098.691.4136

98.655.889.698.030.8103

85.099.889.873.899.698.689.4100

98.6104

96.898.8

kes Analytical



Page 8 of 11

I




Hygieneering, Inc.75 75 Plaza CourtWillowbrook. IL 60521


Project Manager:

2001-34952001-3495Gary Milkeris


Volatile Organic Compounds by EPA Method 8260B/QuaIity ControlGreat Lakes Analytical

Analvte

Matrix Spike (continued)1,1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Matrix Spike DUDAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanone


SampleResult


Recov.%

RPDLimit

RPD% Notes'

1070436-MS1 B107220-017/26/01 50.0

50.050.050.050.050.0150

50.050.050.050.0

NDNDNDNDNDNDND

48.7 ug/l51.941.649.840.129.4156

44.944.544.845.6

42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-11191.1-11185.1-10495.1-10589.6-105

97.4104

83.299.680.258.8104

89.889.089.691.2

1070436-MSD1 B107220-017/26/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

52.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

59.1 ug/l48.348.741.814.239.651.237.848.845.757.047.727.443.448.420.050.742.249.444.438.050.046.244.347.1

10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-208

13.096.697.483.628.479.2102

75.697.691.4114

95.454.886.896.840.0101

84.498.888.876.0100

92.488.694.2

73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7

71.90.2070.410

1.930.707

1.250

2.141.02

017.63.301.813.171.2326.01.96

0.7081.011.122.94

0.4016.49

0.8995.97

Great Lakp Analytical



Page 9 of 1

LAKESANALYTICAL



I1

Hygieneering, Inc.

17575 Plaza CourtWillowbrook, IL 60521

1

«Analyte

Matrix Spike Pup (continued)Styrene

11 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane

M 1,1,2-Trichloroethane• Trichloroethene

Trichlorofluoromethane

1Vinyl acetateVinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane

1Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1

1

1

1

1

1

|Great L«(kes Analytical

1 ,/_-_Andy Johnson, Project Manager

1



Volatile Organic Compounds by EPA MethodGreat Lakes Analytical


1070436-MSD1 B107220-017/26/01 50.0 ND 49.1

50.0 ND 50.550.0 ND 48.350.0 ND 49.550.0 ND 47.850.0 ND 51.050.0 ND 39.350.0 ND 50.550.0 ND 38.550.0 ND 30.8150 ND 155

50.0 43.350.0 44.150.0 44.350.0 45.3



Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes1

ug/l 49.7-126 98.2 18.6 0.40720.6-223 101 50.3 2.9345.1-113 96.6 17.6 0.20771.3-118 99.0 19.4 0.20242.5-128 95.6 18.4 1.8770.1-139 102 32.5 1.9453.5-106 78.6 20.9 5.6910.0-417 101 29.2 1.4010.0-239 77.0 34.5 4.0737.4-113 61.6 23.5 4.6570.8-111 103 12.4 0.96691.1-111 86.685.1-104 88.295.1-105 88.689.6-105 90.6

"Refer to end of report for tc.rl of notes and definitions

Page 1 0 of 1 1

mLAKF9fnrvt'J 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847) 808-7766 FAX (847) 808-7772

Hygieneering, Inc. Project: 2001-3495 Sampled: 7/13/017575 Plaza Court Project Number: 2001-3495 Received: 7/19/01Willowbrook. IL 60521 Project Manager: Gary Milkeris Reported: 7/31/01 11:52


# Note




Gl 6 The percent recovery of the internal standard used to quantitate this analyte is below the method specified limits.

Gl 7 The percent recovery of the internal standard used to quantitate this analyte is above the method specified limits.


G20 This analyte was initially analyzed within holdtime; however, reanalysis at a dilution was performed outside the method specifiedholdtime.

G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory's-established acceptance criteria. Refer to the included QC reports for more detail.

OS The recovery for this analyte is above the laboratory's established acceptance criteria.



NR Not Reported


Recov. Recovery


Great Lakas Analytical

A/dy Johnson, Project Manager Page I I of 1

mM LAKESANALYTICAL FAX (84?) 808-7772 FAX (414) 570-9461

Client: Bill To: 4 DAY 3 DAY 2 DAY 1 DAY < 24 HRS

Address: /Address:D YEST^TAT is critical

n NO . TAT is nn( cnli


U \i-kuufcfiuot IL TFMPERATURF IPON RFCEIPT

Report to: Q .Phone #: State &

Program:Phone #: fFa**: (.

Deliverable Package Needed:D STD D Other

Air Bill No.

Project: 2c& \ - ^

Sampler:

» of BottlesPreservative Used

PO/Quote #:

JTF/ELD /D, LOCATION

SAMPLE/CONTROL

LABORATORY'^NUMBER

Li -02,PID:

ITP/D:

5J

P/D:

P/D:

UP/D:

8J

P/D:

UP/D:

P/D:1-2D'0\

^2^sffn- vx£e-^LINQUISHEDRELINQUISHED RELINQUIS

COMMENTS:

R4GE OF




June 18, 2001


RE: 2001-3495

Dear Gary Milkeris

Enclosed are the results of analyses for sample(s) received by the laboratory on June 5, 2001. If you i.gve anyquestions concerning this report, please feel free to contact me.

Sincerely,


siau, • i'iuis* ^HurAwl

•§51GREATLAKESANALYTICAL



I Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521





[Sample Description Laboratory Sample Number Sample Matrix Date Sampled

IV

I

I!i;iiiiiiii

lB-14Central-3'

W-14 Central-17'

|B-15

.B-16

IB-17

IB-11

B-12

IB-13

B106065-01

B106065-02

B106065-03

B106065-04

B106065-05

B106065-06

B106065-07

B106065-08

Soil

Water

Soil

Soil

Soil

Soil

Soil

Soil

6/4/01

6/4/01

6/4/01

6/4/01

6/4/01

6/4/01

6/4/01

6/4/01

Great

I

Lakes Analytical

Andy'Johnson, Project Manager

Tltt' result!: in this report apply to ill? samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in us entirely.

Page 1 ot"34





Project: 200)-3495Project Number: N/A


Sampled: 6/4/01Received: 6/5/01Reported: 6'18/01 16:18

Total Metals by EPA 6000/7000 Series MethodsGreat Lakes Analytical

Analvte

W-14 Central-lTArsenicBariumCadmiumChromiumSeleniumSilverLeadMercury

Batch Date DateNumber Prepared Analyzed

SpecificMethod

ReportingLimit

B106065-021060181 6/12/01 6/12/01.i n M,in., ., nnn .i i i

1060196 6/13/01 6/13/01

EPA 601 OBE P A 6 0 I O BEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421EPA 7470A

0.05000.500

0.005000.01000.05000.0500

0.005000.000200

Result Units Note

WaterND mg/1NDNDNDNDNDNDND

Grt^it Lakes Analytical *Refer to end of report for text oj notes and dcfmuioi

Andy Johnson. Project Manager Page 2 of





75 75 Plaza CourtWillowbrook. IL 60521

Analyte

B-14 Central-3'Arsenic

1BariumCadmiumChromiumSelenium

•

SilverLeadMercury

ArsenicBarium

1CadmiumChromiumSeleniumSilver

•LeadMercury

— B-16• Arsenic^ Barium

Cadmium

1ChromiumSeleniumSilverLead

• Mercury

B-13

1ArsenicBariumCadmiumChromium

1SeleniumSilverLead

— MercuryI '

"Great Lakes Analytical\ \

1 '-K-



TCLP Metals by EPA 1311/6000/7000 SeriesGreat Lakes Analytical

Batch Date Date SpecificNumber Prepared Analyzed Method

B 106065-011060182 6/12/01 6/12/01 EPA6010B

EPA 601 OBEPA 601 OBEPA 601 OBEPA6010BEPA 601 OBEPA 7421

1060137 " " EPA7470A

B106065-031060182 6/12/01 6/12/01 EPA6010B" , " " EPA 601 OB

EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421

1060137 " " EPA7470A

Bl 06065-041060182 6/12/01 6/12/01 EPA60IOB

EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421

1060137 " " EPA7470A

Bl 06065-081060182 6,12,01 6,12/01 EPA6010B

EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421

1 OWI1 37 " " EPA 7470A

Methods

ReportingLimit

0.1001.00

0.005000.1000.100

0.05000.00500

0.000200

0.1001.00

0.005000.1000.100

0.05000.00500

0.000200

0.1001.00

0.005000.1000.100

0.05000.00500

0.000200

0.1001.00

0.005000.1000 100

0.05000.00500

0.000200


Result Units Notes*

SoilND mg/1NDNDNDNDND

0.0104ND


0.0385ND


0.0278ND


0.0200ND

*Re/er to end of report /or le.rl of notes uiul definitions.


I





Analvte

W-14Central-lTAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 .1 ,1 -Trichloroethane1 . 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroetliane-d4


Project Manaeer: Garv Milkeris


Batch Date Date Surrogate ReportingNumber Prepared Analvzed Limits Limit

B106065-021060148 6/8/01 6/9/01 10.0

2.002.002.002.0010.02.002.002.002.002.002.002.00

20002.002.00200020002.002.002.002.0010.02.0010.02.002.002.002.002.002.0020002.002.0020002.00

Vl.l-lll85.1-104

Sampled: 6/4/01Received: 6/5/01Reported: 6 18/01 16:18

Result Units Notes"

Water G15.G2.G3.O'ND ug/l

2.59NDNDNDNDNDNDNDND

29.6NDND

2580 " G1242.485.3

242000 " G122580 " G12

NDNDNDNDNDNDNDNDNDNDNDNDND

47100 " GI2NDND

14000 " G12ND

91.2 %111) " O5

Grca| Lakes Analytical

^ \,'< \ \

"Refer lo end of report lor text of notes and definition:

Andy (Johnson. Project Manager Page 4 of '•




I Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521





JAnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*

iw-14Central-17' (continued)Surrogate: Toluene-d8

• Surrogate: 4-Bromofluorobenzene1060148 6/8/01

B106065-026/9/01 95.1-105

89.6-105

Water G15,G2,G3.O9100 %102

I

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IGreat Lpkes Analytical

IAndy Jo+mson, Project Manager

*Rc/cr to end of report for text of notes and definition!,

Page 5 of" 34

I





Analyte

B-17AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

B-llAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole





B106065-051060134 6/8/01 6/12/01 100

200100100

90.0100100100100

90.0100100100100100100

29.0-132

Bl 06065-061060134 6/8/01 6,11/01 100

200100100

90.0100100100100

90.0100100100100100100

29.0-132


Result Units Notes:


44.8 %


84.9 %

Great bakes Analytical *Refer to end of report for text of notes and definition.

Andy Johnson, Project Manager Page 6 of '.

I ^^B GREATI All LAKES

. •&•• ANALYTICAL•11

1 Hygieneering, Inc.J 75 75 Plaza Court• Willowbrook, IL 60521

•

Analyte

B-,2Acenaphthene



— Chrysene1 Dibenz (a,h) anthracene• Fluoranthene

Fluorene

1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene


1

1

1

1

1

1— Grefct Lakes Analytical

i W/-

1380 Busch Parkway Email: [email protected] Grove, I l l ino is 60089 (847) 808-7766 FAX (847) 808-7772

Project: 2001-3495 Sampled: 6/4/01Project Number: N/A Received: 6/5/01

Project Manager: Garv Milkeris Reported: 618/01 16:


Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units

Bl 06065-07 Soil1060134 6/8/01 6/11/01 100 ND ug/kg

200 ND100 ND100 ND

90.0 ND100 ND100 ND100 ND100 ND

90.0 ND100 353100 ND100 ND100 ND100 420100 221

29.0-132 AT? %

•18

Notes

05

'Refer to end of report for text of notes and definition

AndyVIohnson, Project Manager Page 7 of:

I





Analyte

B-14 Central-3'AcetoneBenzeneBromodichloromethaneBromotbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 . 1 ,2.2-TetrachloroethaneTetrachloroetheneToluene1,1.1 -Trichloroethane1 . 1 .2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroethane-d4





B 106065-011060197 6/12/01 6/13/01 25000

5000500050005000

100005000500050005000500050005000500050005000500050005000500050005000

100005000

1000050005000500050005000500050005000

1000050005000

81.2-1345(1.8-145

Sampled: 6/4/0 iReceived: 6/5/01Reported: 6/18/01 16:18

Result Units Notes*

Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

34600 " G 1 2NDNDNDNDNDNDNDNDNDNDNDNDNDND

74800 " I . G 1 2NDNDNDND

96.6 "/:,

12-

Gruat Lakes Analytical *Refer to end of report for lext of notes uiul definitions

An<Jy Johnson. Project Manager Page X of 3

I

I£\




1 Hygieneering, Inc.7575 Plaza Court

BJWillowbrook, IL 60521

•

11 Analyte

[JB-14Central-3' (continued)Surrogate: Toluene-d8

_ Surrogate: 4-Bromofluorobenzene

1

1

1

1

1

1

1

1

1

IHi Great Lakes Analytical


1

Project: 2001-3495 Sampled: 6,4-01Project Number: N/A Received: 6,5/01

Project Manager: Gary Milkeris Reported: 618/01 lb :18



B 106065-01 Soil G41060197 6/12/01 6/13/01 82.0-121 100 %

76.8-113 108

"Refer 10 end of report for text of notes and definitions.

Page 9 of 34





-

Analvte

MSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 . 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane1 ,1 ,2 -TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4





B106065-031060197 6/12/01 6/13/01 25000

5000500050005000

100005000500050005000500050005000500050005000500050005000500050005000

100005000

1000050005000500050005000500050005000

1000050005000

8 1.2- 13450.8-145


Result Units Notes"


43900 " G\2NDNDNDNDNDNDNDNDNDNDNDNDNDND

24800 " 1.GI2NDNDNDND

93. 7 %127

Great Lpkes Analytical "Refer to end of report for text of notes and de/iniltons

Andy Johnson. Project Manager Page 10 of 3

III

ISal

GREAT1380 Busch Parkway Email: [email protected]


IHygieneering, Inc. Project: 2001-3495 Sampled: 6/4/017575 Plaza Court Project Number: N/A Received: 6/5/01Willowbrook. IL 60521 Project Manager: Gary Milkeris Reported: 6/18/01 16:18


Batch Date Date Surrogate ReportingI Analyte Number Prepared Analyzed Limits Limit Result Units Notes*

I B-15 (continued^ B106065-03 Soil G4Surrogate: Toluene-d8 ~ 1060197 6/12/01 6/13/01 82.0-121 101 %

• Surrogate: 4-Bromofluorobenzene " " " 76.8-113 109

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IGreat Lakes Analytical "Refer to end of report for text of notes and definitions.\

\\Andy J\>hnson, Project Manager Page 1 1 of 34

I









Analvte

B-16AcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene1,1 ,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroelhane-d4


Bl 06065-041060197 6/12/01 6/13/01 12500

25002500250025005000250025002500250025002500250025002500250025002500250025002500250050002500500025002500250025002500250025002500500025002500

81.2-13450.8-145

Result Units Notes*


34300 " G12NDNDNDNDNDNDNDNDNDNDNDNDNDND

3690 " G 1 2NDNDNDND

97.2 %127

GreatJLakes Analytical "Refer 10 end of report for text of notes and definitions

Andj' Johnson, Project Manager Page 12 of 3'

II

„-..••A* ISSl




I Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521



Sampled: 6,4/01Received: 6/5/01Reported: 6/18/01 16:18


lAnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*

I

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B-16 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060197 6/12/01B106065-04

6/13/01 82.0-12176.8-113

99.7108

Soil%

G4

Gre|it Lakes Analytical

II JAndy Johnson, Project Manager


Pane 13 of 3-

I





Analvte

BdlAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1,1.2,2-TetrachloroethaneTetrach loroeth en eToluene1,1 ,1 -Trichloroethane1 . 1 .2-TrichloroethaneTrichloroetheneTri ch 1 orott uoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromelhaneSurrogate: 1.2-Dichloroeiliane-d4





B106065-081060197 6/12/01 6/13/01 1250000

250000250000250000250000500000250000250000250000250000250000250000250000250000250000250000250000250000250000250000250000250000500000250000500000250000250000250000250000250000250000250000250000500000250000250000

81.2-13450.8-145


Result Units Notes*

Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1020000 " G12NDNDND

4220000 " 2.G12NDNDNDND

93.4 "/„142

Great Ltikes Analytical "Refer to end of report lor texl of notes and definitions

Andy Johnson, Project Manager Page 14 of 3-




I Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521



Sampled: 6,4/01Received: 6,5/01Reported: 6 18/01 16:18

JAnalyte



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B-13 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060197 6/12/01B106065-08

6/13/01 82.0-12176.8-113

Soil G4

98.5111

Great Lajces Analytical

Antly Johnson, Project Manager


Page 15 of

I

I GREATurAwBi Aifcc••••UMrvco 1380 Busch Parkway Email: [email protected]•fill ANALYTICAL Buffalo Grove, I l l inois 60089 (847) 808-7766 FAX (847) 808-7772


Analvte

B-17BenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB

B-llBenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB

B-12BenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB



BTEX by EPA Method 5035/802 IBGreat Lakes Analytical


B 106065-051060153 6/8/01 6/11/01 25.0

250250250

" ~ " " 35.1-140

B 106065-061060153 6/8/01 6/11/01 25.0

250250250

35.1-140

B106065-071060153 6/8/01 6/11/01 25.0

250250250

35.1-140


Result

29.2NDNDND

23.8

40.6NDNDND

34. 1

NDNDNDND

21.8

6,4,016/5/016,18/01 16:18

Units Notes*

Soil G4.O3ug/kg11

11

"

% O4

Soil G4.O3ug/kg"

11

"

% O4

Soil G4.O3ug/kg"""

% O4


"Refer lo end of report for text of notes and definitions.

Page 16 of 34

1 g*slGREAT

•All LAKto 1380 Buscri Parkway_ •fifll ANALYTICAL Buffalo Grove, Il l inois 60089•1

11 Hygieneering, Inc. Project: 2001-3495

• 7575 Plaza Court Project Number: N/A•Willowbrook, IL 60521 Project Manager: Gary Milkeris

Dry Weight DeterminationI Great Lakes Analytical

BJSampleName Lab ID Matrix1^B-14Central-3- B106065-01 Soil

• B-15 B106065-03 Soil

B-16 B106065-04 Soil

• B-17 B106065-05 Soil

B- l l B 106065-06 Soil

|B-12 B106065-07 Soil

,_B-13 Bl 06065-08 Soil

1

1

1

1

1

1

1

1Great Lakes Analytical

1 /1A^


Sampled: 6/4,01Received: 6/5/01Reported: 6,18/01 16:18

Result Units

75.5 %

72.9 %

81.0 %

81.2 %

81.1 %

76.3 %

75.3 %

I





iHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521

Project: 2001-3495Project Number: N,A

Project Manager: Gar,- Milkeris

Sampled: 6,4/01Received: 6.5/01Reported: 6 18/01 16:18


Analvte



Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilverLead




""""11

1060181-BS16/12/01 2.00

2.001.002.001 .001.00

0.0240

1060181-MS1 B106070-016/12/01 2.00 ND

2.00 ND1 .00 ND2.00 0.03471.00 ND1.00 ND

0.0240 0.0249

1060181-MSD1 B106070-016/12/01 2.00 ND

2.00 ND1.00 ND2.00 0.03471.00 ND1.00 ND

0.0240 0.0249

QCResult

NDNDNDNDNDNDND

2.082.081.012.061.001.10

0.0309

2.062.15

0.9972.061.03

0.6880.0505

2.022.13

0.9732.021.02

0.4970.0502


Extraction Method: EPA

mg/1 0.05000.500

0.005000.01000.05000.0500

0.00500

mg/1 78.6-12677.1-11878.2-11679.1-11676.2-12425.7-16964.1-149

mg/1 74.0-12372.0-12673.7-12055.6-13431..5-15710.0-14142.0-184

mg/1 74.0-12372.0-12673.7-12055.6-13431.5-15710.0-14142.0-184

3015

104104101103100110129

103108

99.7101103

68.8107

101107

97.399.3102

49.7105

i

RPD RPDLimit % Notes*

20.5 1.961 7.0 0.93014.2 2.4414. S 1.7036.2 0.97677.9 32.232. S 1.89

Great Likes Analytical

An0y Johnson. Project Manager

"Refer to end of report for text of notes and definition.'*.

Page I K of 3'

I ^^.BGREATfill LAKES

B WSmm ANALYTICAL1380 Busch Parkway


(847) 808-7766 FAX (847) 808-7772

Hygieneering, Inc.J7575 Plaza CourtIwillowbrook, IL60521



Sampled: 6,4/01Received: 6/5/01Reported: 6.18/01 16:18

I Batch: 1060196Blank

i Mercury

'LCSMercury

[Matrix SpikeMercury

I Matrix Spike PupMercury

I

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Date Spike Sample QC Reporting Limit Recov. RPD RPDlAnalvte Analyzed Level Result Result Units Recov. Limits % Limit % Notes*

Pate Prepared: 6/13/011060196-BLK16/13/01

1060196-BS16/13/01 0.0200

1060196-MS1 Bl 06070-016/13/01 0.0200 ND

1060196-MSP1 Bl 06070-016/13/01 0.0200 ND

NP

Extraction Method: EPA 7470A

mg/1 0.000200

0.0218 mg/I

0.0200 mg/1

0.0196 mg/1

73.4-125 109

42.2-148 100

42.2-148 98.0 27.5 2.02

Great Lqkes Analytical

AndyjJohnson. Project Manager

"Refer in end of report for text of notes and definitions

Page 19 of 34







Sampled: 6,4/01Received: 6,5/01Reported: 6.18/01 16:18


Analvte

Batch: 1060137BlankMercury

LCSMercury

Matrix SpikeMercury

Matrix Spike PupMercury



Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilver ,


Date Prepared:1060137-BLK16/12/01

1060137-BS1

6/12/01

6/12/01 0.00100

1060137-MS1 B 10603 9-026/12/01 0.00100 ND

1060137-MSP1 Bl 06039-026/12/01 0.00100 ND

Pate Prepared:1060182-BLK16/12/01""11

"11

11

1060182-BS16/12/01"""11

n

6/12/01

2.002.001.002.001.001.00

0.0240

1060182-MS16/12/0111

"""

B106062-012.00 ND2.00 ND1.00 ND2.00 ND1.00 ND1.00 ND

QCResult

NP

0.000853

0.000879

0.000875

NRNPNPNPNPNPNP

2.012.02

0.9901.99

0.97S0.986

0.0297

1.952.71

0.9671.911.01

O.S93



mg/1 0.000200

mg/1 73.9-123

mg/1 58.0-152

mg/1 58.0-152


mg/1 0.1001.00

0.005000.1000.100

0.05000.00500

mg.l 72.8-13981.6-12676.7-13179.3-13069.9-13583.2-13759.9-152

mg/1 82.8-13567.1-15466.3-15367.1-14966.1-15019.6-176

7470A

85.3

87.9

87.5 26.2 0.456

3015

100101

99.099.597.898.6124

97.5136

96.795.5101

89.3

Great Liakt$ Analytical "Refer to end of report for text of notes and definition

AndyUohnson, Project Manager Page 20 of

111

;n-~»\e.w.B

ti&Aml

•III(GREAT(LAKES(ANALYTICAL

1380 Busch Parkway Email: [email protected] Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

IHygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521


Pro j ect Manager: Gary Milkeris



[AnalyteDate Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit u/o Notes

I

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[Matrix Spike (continued)Lead


1060182-MS1 Bl 06062-016/12/01 0.0240 ND 0.0303

6/12/01 2.002.001.002.001.001 .00

0.0240

NDNDNDNDNDNDND

1.972.72

0.9661.911.01

0.9990.0310

mg/1

mg/1

35.2-176 126

82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176

98.5136

96.695.5101

99.9129

19.316.023.813.821.835.835.3

1.020

0.10300

11.22.35

Great Lakds Analytical



Page 21 of 3'






Project Manager:



6/4/016/5/016/18/01 16:18


Date Spike Sample QCAnalyte Analyzed Level Result Result

Batch: 1060148 Pate Prepared: 6/8/01Blank 1060148-BLK1Acetone 6/8/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1 , 1 -Dichloroethane "1 ,2-Dichloroethane "1,1-Dichloroethene "cis-1, 2-Dichloroethene "trans-1, 2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "2-HexanoneMethylene chloride "4-Methyl-2-pentanone "Styrene "1 . 1 ,2,2-Tetrachloroethane "Tetrachloroethene "Toluene1,1,1 -Trichloroethane "1 , 1 ,2-Trichloroethane "Trichloroethene "Trichlorotluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50 .1)

— i

NPNPNPNPNPNPNPNDNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNDNPNP

46.1

Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit "/o Notes*

Extraction Method: EPA 5030B (P/T)

ug/l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00

91.1-111 92.2

Great t\akes Analytical

\iArrdy Johnson, Project Manager

"Refer lo end of report for text of notes and definitions

Page 22 of 3^




IwHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521


Project Manager:



6/6/6,

4/015/0118/01 16 18


•1Analvte

H Blank (continued)Surrogate: 1 .2-Dichloroethane-d4

_ Surrogate: Toluene-d8• Surrogate: 4-Bromofluorobenzene

LCS


H Bromomethane• 2-Butanone

Carbon disulfide


1ChloroformChloromethane1 , 1 -Dichloroethane

11 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene

11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene


IStyrene1 , 1 .2,2-TetrachloroethaneTetrachloroetheneToluene

11, 1.1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroethene



1060148-BLK1"~6/87oi" 50.0

50.050.0

1060148-BS16/8/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

- 50.0

QCResult

39 J50.749.6

38.849.755.058.663.446.354.755.657.258.954.549.850.644.251.250.653.147.850.654.857.658.142.446.445.961.057.461.455.953.254.550.263.1


ug/l 85.1-10495.1-10589.6-105

ug/l 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.9-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-120X6.3-12063.5-14684.5-12451.4-15310.0-586

Recov. RPD RPD% Limit % Notes'

78.2101

99.2

77.699.4110117127

92.61091 1 1114118109

99.6101

88.4102101106

95.61011 10115116

84.892.891.81221151231 1 210610910012(3


1Andy Johnson, Project Manager

I


Page 23 of 34








Analvte

LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

Matrix SpikeAcetoneBenzeneBromodichloromethaneBromofbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 .1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis- 1 ,2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropanecis- 1 .3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene

Great Lakes


1060148-BS16/8/01 50.0

50.0150

-- - „ 500

50.050.050.0

1060148-MS1 B106046-016/9/01 50.0 ND

50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 12.450.0 ND50.0 ND50.0 29550.0 6.4150.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND

Analytical

QCResult

12154.1179

48.849.650.650.1

50.045.252.457.546.962.241.039.751.356.240.946.231.551.049.834.3280

43.449.448.251.549.450.045.353.155.759. S46.249.5

Sampled: 6,4/01Received: 6/5/01Reported: 6/18/01 16:18



ug/l 10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105

ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-1501 0.0-20849.7-12620.6-22345 .1-11371.3-118

Recov. RPD RPD% Limit % Note;

NR108119

97.699.2101100

10090.4105115

93.8124

82.079.4103112

81.892.463.077.299.668.6NR

74.098.896.4103

98.8100

90.6106111120

92.499.0

Griit Lakes Anaivtical "Refer to end of report for text of notes and definition.'

\

Anj\ly Johnson, Project Manager Page 24 of 3




11

1 Hygieneering, Inc.J7575 Plaza Court• Willowbrook, IL 60521


Project Manager:


Sampled: 6/4/01Received: 65/01Reported: 6,18/01 16:18

• Volatile Organic Compounds by EPA Method 8260B/Quality Controlm Great Lakes Analytical

T~[Analvte

1^ Matrix Spike (continued)


11 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate


^ Surrogate: 1.2-Dichloroethane-d4H Surrogate: Toluene-d8• Surrogate: 4-Bromofluorobenzene

1Matrix Spike PupAcetoneBenzeneBromodichloromethane

IBromofbrmBromomethane2-Butanone

1Carbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethane

1ChloroethaneChloroformChloromethane

_ 1,1 -Dichloroethane• 1 ,2-DichloroethaneU 1 , 1 -Dichloroethene

cis-1, 2-Dichloroethene

1trans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-Dichloropropene

I Ethylbenzene2-HexanoneMethylene chloride

|

4-Methyl-2-pentanone1 '


SampleResult


RPDLimit

RPD% Notes

1060148-MS1 B 106046-016/9/01 50.0

50.050.050.050.050.0150

" "~"~ " 50.050.050.050.0

NDND

3.36NDND

35.2ND

41.4 ug/l57.550.842.180.646.1154

'50.549.951.751.4

42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-11191.1-11185.1-10495.1-10589.6-105

82.8115

94.984.2161

21.8103101

99.8103103

1060148-MSP1 B 106046-016/9/01 50.0

50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0

NDNDNDNDNDNDNDNDNDNDNDNDND12.4NDND295

6.41NDNDNDNDNDNDND

45.0 ug/l44.251.655.951.644.841.539.851.255.444.745.635.647.748.934.4274

44.247.247.149.949.044.344.746.1

10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-1 1 110.0-22545.6-15010.0-208

90.088.4103112103

89.683.079.6102111

89.491.271.270.697.868.8NR

75.694.494.299.898.088.689.492.2

73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7

10.52.241.922.649.3532.21.21

0.2520.9760.897

8.881.3112.28.931.82

0.291

2.144.552.313.16

0.81312.11.3313.9

' Great. Lakes Analytical

I

I

Andy Johnson, Project Manager Page 25 of 3-









AnalvteDateAnalyzed

SpikeLevel

SampleResult

QCResult Units

ReportingRecov.

LimitLimits

Recov. RPDLimit

RPDu/o Notes

Matrix Spike Pup (continued)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060148-MSD1 B106046-016/9/01 50.0

50.050.050.050.050.050.050.050.050.0150

50.050.050.050.0

NDNDNDNDNDND

3.36NDND

35.2ND

55.756.646.648.341.954.845.543.7.'3.753.3153

49.750.050.650.8

ug/l 49.7-12620.6-22345.1-11371.3-11842.5-12870.1-139

53.5-10610.0-41710.0-239

37.4-11370.8-11191.1-1/1

85.1-10495.1-10589.6-105

11111393.296.683.811084387.414736.2102

99.4.100101102

18.650.317.619.418.432.520.929.234.523.512.4

06.010.862

2.451.204.4411.83.739.0949.70.976

Great\Lakes Analytical• \

\"Refer to end of report for text of notes and definitions




Email. info@glalabs com(847)808-7766 FAX (847) 808-7772

1I"iHygieneering, Inc.J?575 Plaza Court

•Willowbrook, IL 60521I

nalvte

atch: 1060134Blank

—Acenaphthene•Acenaphthylene•Anthracene

Benz (a) anthracene•Benzo (a) pyrene•Benzo (b) fluoranthene

Benzo (ghi) peryleneBenzo (k) fluoranthene

•Chrysene•Dibenz (a,h) anthracene

Fluoranthene••Fluorene•Indeno ( 1 ,2,3-cd) pyrene^Naphthalene

Phenanthrene•PyreneJfSurrogate: Carbazole

^LCS•Acenaphthene"Acenaphthylene

Anthracene

Eenz( a) anthraceneenzo (a) pyrene

" Benzo (b) fluoranthene^Benzo (ghi) peryleneVBenzo (k) fluoranthene•Chrysene

Dibenz (a,h) anthracene

f luorantheneluoreneideno ( 1 ,2,3-cd) pyrene

NaphthaleneIBPhenanthreneJP'yrene

Surrogate: Carbazole

1




Date Spike SampleAnalvzed Level Result

Pate Prepared: 6/8/011060134-BLK16/11/01

""11

nn

it"M

»

76.7

1060134-BS16/11/01 64.9

64.964.964.964.964.964.964.964.964.964.964.964.964.964.964.916.2

EPA MethodAnalytical

QCResult


8310/Quality Control


Recov. RPD RPD% Limit % Note>


NPNPNPNPNRNPNPNPNPNPNPNPNPNPNPNP

15.4

49.680.747.352.143.259.948.855.255.248.454.149.148.643.453.164.212.6

ug/kg 100200100100

90.0100100100100

90.0100100100100100100

29.0-132

ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.11-132

92.2

76.4124

72.980.366.692.375.285.185.174.683.475.774.966.981.898977.8

jreal Lakes Analytical

IAndyVlohnson, Project Manager

I


Page 27 of 3'







Sampled: 6/4/01Received: 6,5/01Reported: 6,18,01 16:18


Analvte

Matrix SpikeAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

Matrix Spike PupAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2.3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole

\


SampleResult


^ecov.%

RPDLimit

RPD% Notes

1060134-MS1 B106061-076/12/01 67.0

67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.8

1060134-MSP16/12/01 68.5

68.568.568.568.568.568.568.568.568.568.568.56S.568.568.568.517.1



48.9 ug/kg66.751.637.238.043.929.033.253.021.265.337.130.837.349.275.610. 7

44.9 ug/kg68.958.036.038.044.431.336.566.827.052.539.332.235.536.263. S12.7

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145

29.0-132

73.099.677.055.556.765.543.349.679.131.697.555.446.055.773.4113

63. 7

65.5101

84.752.655.564.845.753.397.539.476.657.447.051.852.893.174.3

66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6

10.81.409.525.372.141.075.397.1920.822.024.03.552.157.2632.619.3

Great \Lakes Analytical


"Refer to end of report for text of notes and definition

Page 28 of




II Hygieneering, Inc.

_7575 Plaza Court• Willowbrook. IL 6052 1

•



Sampled. 6/4/01Received: 6/5/01Reported: 6/18/01 16:18

VolatUe Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical

| Date Spike SamplejAnalyte Analyzed Level Result

M Batch: 1060197 Pate Prepared: 6/12/01Blank 1060197-BLK1

1Acetone 6/14/01Benzene "Bromodichloromethane "Bromoform "

1Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "

• Chlorobenzene "•Chlorodibromomethane "

Chloroethane "

1ChloroformChloromethane "1,1 -Dichloroethane1 ,2-Dichloroethane "

• l,l-Dichloroethene "B'-is-l, 2-Dichloroethene "

trans-1, 2-Dichloroethene "

K1. ,2-Dichloropropane "ois-l,3-Dichloropropene "irans- 1 ,3-Dichloropropene "Ethylbenzene "

|

.'-Hexanone "Methylene chloride "4-Methyl-2-pentanone "

^Styrene "• 1 ,1 ,2,2-Tetrachloroethane•-Tetrachloroethene

Toluene "

I', 1,1 -Trichloroethane "1,1 ,2-Trichloroethane "frichloroethene "Trichlorotluoromethane "

KVinyl acetate "Vinyl chloride "Total Xylenes "

•

^urrogate: Dibromofluoromelhane " 50.0

^ortsot Lakes Analytical

QCResult

NPNPNDNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNDNPNPNPNPNPNPNPNPNPNPNRNP

46. 8


Extraction Method: EPA 5035B fP/Tl

ug/kg 1250250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250500250250

81.2-134 93.6

"Refer lo end of report for text of notes and def inn ions.

\Andy Jbimson, Project Manager

I

Page 29 of 34









Analyte

Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChioroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 , 1 , 1 -Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane

1


1060197-BLK16/14/01 50.0

50.050.0

1060197-BS16/14/01 2500

25002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

QC Reporting Limit Recov. RPD RPDResult Units

69.9 ug/kg46.348.0

3320 ug/kg18202580262025602200139030402330268031602140

9371560269018301 9601710168020702360241012201 550852

23901380292022402630208024501130

Recov. Limits

50.8-14582.0-12176.8-113

10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-125h i . 8-13214.6-241

% Limit % Notes

14092.696.0

13372.8103105102

88.055.6122

93.2107126

85.637.562.4108

73.278.468.467.282.894.496.448.862.034.195.655.21 1 7

89.6105

83.298.045.2

Gnjat Lakes Analytical "Refer to end of report for text of notes and de/initioi,

Andy Johnson, Project Manager Page 30 of




11

1 Hygieneering, Inc.J 75 75 Plaza CourtI Willowbrook, IL 60521



Sampled: 6-4,01Received: 6 .501Reported: 61801 16:18

1Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control


Analvte

LCS (continued)Vinyl acetate

1Vinyl chlorideTotal Xylenes

-. - . .

Surrogate: DibromofluoromethaneSurrogate: / , 2-Dichloroethane-d4


LCS PUDB AcetoneB Benzene


IBromoformBromomethane2-ButanoneCarbon disulfide

B Carbon tetrachlorideBCh lorobenzene


1ChloroethaneChloroformChloromethane1 .1 -Dichloroethane

11,2-Dichloroethane1 .1 -Dichloroethenecis- 1 ,2-Dichloroethene

-trans-1, 2-DichloroetheneB 1 .2-Dichloropropane• cis-1 ,3-Dichloropropene

trans-1 ,3-Dichloropropene

IEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone

J stvrene•1 , 1 ,2,2-TetrachloroethaneTetrachloroethene

1Toluene


1 :l,~


1060197-BS16/14/01 2500

25007500

" 50.050.050.050.0

1060197-BSP16/14/01 2500

2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

QCResult

10101640725050.071.748.649.6

338019002860274027402200146033302390281030002260

7961600305017801940178018102210255024701750159099S

2480141029502390

Reporting LimitUnits Reeov. Limits

ug/kg 10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-1366S.4-13757.6-14264.1-134

"Refer 10 end of report

Recov.%

40.465.696.7100143

97.299.2

13576.0114110110

88.058.4133

95.6112120

90.431.864.0

12271.277.671.272.488.4102

98.870.063 639.999.256.4I I S

95.6

for text

RPDLimit

34541.442.057.461.9173126

43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128

67.41 1 9

37.254646.342.6

of notes

RPD% Notes*

1.494.3010.14.657.55

04.918.632.544.574.885.4516.52.5312.22.771.034.017.456.547.742.4635.72.5515.73.702.15

O.X516.4S

and definitions.


I







Sampled: 6/4,01Received: 6/5/01Reported: 6/18/01 16:18


AnalvteDateAnalyzed

SpikeLevel

SampleResult

QCResult Units

ReportingRecov.

LimitLimits

Recov. RPDLimit

RPDNote;

LCS Pup (continued)1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene

1060197-BSP16/14/01 2500

25002500250025002500750050.050.050.050.0

272022402700109010901370737051.376.750.451.7

ug/kg 60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113

10989.610843.643.6' 54.898.3103153101103

44.253.243.511592.181.040.1

3.747.419.713.607.6217.91.64

Grcat/Lakes Analytical Refer to end of report for text of notes and definition'

Andy Johnson. Project Manager Page 32 of:

1 i**|GREATBMBH*-""^^ 1380 Busch Parkway Email: [email protected]^BjBJ ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772

1

1iHygieneering, Inc.

• 75 75 Plaza Court• Willowbrook, IL 60521

1J Analyte

1 '•Batch: 1060153

Blank

1BenzeneTolueneEthylbenzeneTotal Xylenes

• Surrogate: 4-BFB

I CSLt*~ <J


•Surrogate: 4-BFB

LCS Pup


•Surrogate: 4-BFB

1

1

1

1

GreatlLakes Analytical

i XAndv Johnson. Project Manaeer

1

Project: 2001-3495 Sampled: 64,01Project Number: N/A Received: 65/01

Project Manager: Gary Milkeris Reported: 6 1 8 0 1 16:18

BTEX by EPA Method 5035/802 IB/Quality ControlGreat Lakes Analytical

Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes

Pate Prepared: 6/8/01 Extraction Method: EPA 5035B [P/T11060153-BLK16/11/01 NP ug/kg 25.0

NP " 250NP " 250NP " 250

1000 829 " 35.1-140 82.9

1060153-BS16/11/01 1000 610 ug/kg 77.6-105 61.0

1000 842 " 65.0-131 84.21000 960 " 82.7-115 96.03000 2780 " 86.7-115 92.71000 1000 " 35.1-140 100

1060153-BSP16/11/01 1000 665 ug/kg 77.6-105 66.5 15.4 8.63

1000 858 " 65.0-131 85.8 18.9 1.881000 950 " 82.7-115 95.0 19.8 1.053000 2740 " 86.7-115 91.3 19.8 1.521000 933 " 35.1-140 93.3

"Refer to end of report (or text of notes find definitions.

Page 33 of 34







Sampled: 6/4/01Received: 6,5/01Reported: 6/18/01 16:18


Note

Gl 2 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.

Gl 5 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.



G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory'.'established acceptance criteria. Refer to the included QC reports for more detail.

03 One or more internal standard recoveries were above the method specified acceptance criteria.



O9 The pH of this volatile sample was checked prior to analysis and was found to be above the method specified pH of 2.

1 The method blank associated with this sample contains 7800 ug/L of this analyte

2 The method blank associated with this sample contains 200,500 ug/ L of this analyte.



NR Not Reported


Recov. Recovery


Great Lakes Analytical\vAndyJonnson, Project Manager Page 34 of 3-

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