1999 Table of Contents Product-Method List by Section

Section A: Vegetable Oil Source Materials ('ollonacc~l

S a ~ i i l ) l i ~ ~ g ................................................................................................................................................. A I -38 (07) I-orciyi M:I I I~~ ....................................................................................................................................... A;I 2 -38 (07) Moialurc illid Volatile M:IIIC~ .................................................................................................................. A 3 -38 (07) Oi l Con lc~ i l .............................................................................................................................................. A 4 -38 ( 0 0 ) Prolcin ..................................................................................................................................................... A 5 -38 (80) :I: Prolein ..................................................................................................................................................... A 5 -0 I (07) Conversion Table for Nitrogc~i-A~ii~i io~iia-Protcin ................................................................................ An 5 -0 I (07) Frcc Falty Acids ...................................................................................................................................... A 0 -38 ( 0 0 ) Kcsitlu:~l Lint ........................................................................................................................................... A 7 -55 (07) . . A f l o l ox i~~s ............................................................................................................................................... A X -83 ( 0 0 ) Allntoxins . Co~i l i r~ i in l ion by T L C .......................................................................................................... Aa 9 -80 ( 0 0 ) Al'la~oxins in Corn :und Pcanul by TLC: .................................................................................................. A;I ();I -07 ( 0 0 ) Allatoxin S~andards (preparation) .......................................................................................................... A:I 10 -88 ( 0 0 )

Sampling ................................................................................................................................................. A I -40 (07) Moisture 2nd Voli~t i lc Maltcr ................................................................................................................. Al) 2 -40 (07) Oi l Conten1 .............................................................................................................................................. /\I) . \ -40 (07) Prolcin ................................................................................................................................................... I -I -50 (80) 'I: Protein ..................................................................................................................................................... A 4 -0 1 (07 ) IYrcc Fatly Acids .................................................................................................................................... A 5 -40 (07)

............................................................................................................................................... A l I ; ~ l o x i ~ ~ s /\I) 0 -OX ( 0 0 ) ...

Al'latoxins (a l l ~n i l y colu~i in) ................................................................................................................... A 7 -0 I ( 0 0 )

........................................................................................................................................... Alsoscc 1 0 -X0(07) Also scc ........................................................................................................................................... Ail I 0 - X X (07)

Soy hcans ................................................................................................................................................. Snnipling Ac I -45 (07)

.................................................................................................................. Moia~urc and Volatile Mallcr A 7- -4 I (07 1 Oi l C o ~ i t c ~ i ~ .............................................................................................................................................. A 3 -44 (07)

..................................................................................................................................................... Protci~i A 4 -41 (NO) 'I'

IJrolci~i ..................................................................................................................................................... A 4 -0 I (97) Frcc Rltty Acids ...................................................................................................................................... A 5 -4 I (07)

l 'ung Fruit ................................................................................................................................................. Sampling A I -48 (07)

Mois1ul.c a~ i t l Volatilc Ma t~e r .................................................................................................................. d 2 -53 (07) ................................................................................................................ Oi l C o ~ i l c ~ i t (wliolc ti111g I'rui~) Ad 3 -52 (07)

Physical Analysis (kcrncl c o n ~ c n ~ ) ................................................................................................... A 4 -57 (07) Oil C o ~ i ~ c ~ i t (lung kcl-ncls) ...................................................................................................................... A 5 -52 (97)

................................................................................................................ Oil ('onccnl (Iiullcd lung I'ruit) Ad 0 -52 (07) Castor Beans

.................................................................................................................. Moisture and Vol:~tilc Matter A 7- -52 (07) Oi l Con~cnt .............................................................................................................................................. A 3 -52 (07) Frcc Fatly Acids ...................................................................................................................................... A 4 -52 (07)

I'laxsccd ................................................................................................................................................. Sanipling /\I' I -54 (03) 'b

Moisture and Volntilc Mutccr .................................................................................................................. A 2 -54 (07) 'I' Oi l Content .............................................................................................................................................. A 3 -54 (05) 'b

Sal'l'lowcr Sccd Oi l Co~ l t c~ i t ............................................................................................................................................. t\g I -05 (97)

col"';' A l la~oxins .............................................................................................................................................. A I -72 ( 0 0 )

Sunllowcr Seed

I'l<( )I )I I A l l I I I( )I I I\ I I I V \I ( I I( ) N 1 Method Latest

number issue

Moistt~rc illid Volalilc M i ~ ~ t e r .................................................................................................................. A 2 -75 (97) Oil Conten1 ......................................................................................................................................... A 3 -75 (95) * I'l.otcin ................................................................................................................................................... A 4 -75 (89) * 1'1.otcin Ai 4 -9 I (97) \ .....................................................................................................................................................

Corn ............... i\l'la~oxins ............................................................................................................................... : Aj 1 -86 (97)

Zcalalcnonc alid a-Zcarnlc~iol ................................................................................................................ A j 2 -80 (97) Allatoxins in Corn ............................................................................................................................... A 3 -87 (99)

Also see Atlatoxins (affinily column) ............................................................................................. A 7 -91 (97) Oil in Corn Germ .................................................................................................................................... A j 4 -89 (97) Fumonisins B, and B, in Corn by LC .................................................................................................. A 5 -93 (97) Fl~ino~iisins BI . B, . ancl B3 in Corn by LC ............................................................................................. A 5a -97 (97) Alliitoxins B,. B, ;~nd GI ill Corn . Cottonseed, Peanuts and Peanut Butter ........................................... A j 6 -95 (09) Allotoxins B I . B, . and GI in Corn by ELlSA ........................................................................................ A 6a -97 (99)

R;~pcsccd Glucosinolates ......................................................................................................................................... A 1 -92 (97) Chlorophyll ............................................................................................................................................. A 2 -92 (97) Oil Content by NMR (and other oilseeds) .............................................................................................. A 3 -94 (99)

Simultaneous Dctcrmination of Oil and Moisture Contents of Oilsectls Using Pulsed NMR Spectroscopy ........................................................................ A 4 -95 (99)

Near Inl'rarcd R ~ l l ~ c t i ~ ~ i c c .............................................................................................................................. A I -02 (99) Oil in Oilsccds (FOSFA Method) .................................................................................................................. A 2 -93 (07) Oil in Oilsccds: Supercritical Fluid Extraction Method ................................................................................ I 3 -96 (97)

Section B: Oilseed By-Products Cilkc . Meal. Meats and Pellets

Silml'lilig ................................................................................................................................................ 13i1 1 -38 (07) Moisture and Volatile Matter (breed draft ovcn) ................................................................................... I 2a -38 (97) Moisture and Volatile Matter (vacuum oven) ......................................................................................... a I b -82 (97) Oil Content ............................ ............................... ................................................................................ B 3 -38 (97) I'rotcin ..................................................................................................................................................... I 4a -38 (89) * - I'rotcin . Copper Sulkltc Ciltalyst ............................................................................................................. I 4b -87 (00) * I'rotcin . Kjcl-l:oss Automatic .............................................................................................................. Ba 4c -87 (80) * I'rotein . Tit:uiium Dioxide + Copper Sulfate Catalyst ............................................................................ Ba 4d -90 (99) PI-otcin Nitrogen by Combustion ............................................................................................................ a 4e -93 (99) Ash .......................................................................................................................................................... Ba 5a -49 (97) Acid-lnsolublc Ash ................................................................................................................................. Ba 5b -08 (97) ('nlclc Fibcr ............................................................................................................................................. Rn (3 -84 (07) Free Gossypol (cottonseed products) ...................................................................................................... I 7 -58 (99) Frcc Gossypol (rapid method) ......................................................................................................................... I 7b -96 (97) Total Gossypol (cottonseed products) .................................................................................................... I 8 -78 (97) Gossypol by HPLC ............................................................................................................................... Ba 8a -99 (99) Ureasc Activity (soybean meals, flours and mill feed) ........................................................................... Ba 9 -58 (97) I1l.otcin Dispcrsihility Index (PDI) (soybean products) .......................................................................... Bit I 0 -65 (90) Nitrogen Solubility Index (NSI) (soybean products) .............................................................................. a I 1 -65 (97) Trypsin Illhibitor Activity (soybean products) ....................................................................................... a 12 -75 (97) Free Hexane Content in Extracted Meals ............................................................................................... a 13 -87 (97) Total Hcxanc Content in Extracted Meals .............................................................................................. I 14 -87 (97)

Linters i u ~ d Hull Fiber Sampling .............................................................................................................................................. B 1 -38 (97)

.......................................................................................................... Oil Content (cottonseed hulls) B I -38 (97) ........................................................................................................................................ Ccllulosc Yield I 3 3 -47 (09)

Soya Flo11r ................................................................................................................................................. Sa111l)ling Bc 1 -50 (97)

Moisturc and Volatile Matter .................................................................................................................. Bc 2 -40 (97) Oil Content ........................................................................................................................................... Be 3 -49 (97) Protein ..................................................................................................................................................... Bc 4 -49 (89) * I'rotcin . Tita~iiuni Dioxide + Copper Sulfate Catalyst ............................................................................ B 4 -91 (97)

Section C: Commercial Fats and Oils S; l~ i i l> l i~ iy ........................................................................................................................................................ (' I' -47 (011) Moistu~.c

I > i s ~ i l l ; ~ t i o ~ ~ Mc\llocl ................................................................................................................................. (';I 21 -45 (07) ;111d Vol;ltilc M.ltlcr . Hot Plillc Mct l iod ................................................................................................ I I -3s ( 0 7 ) :111cl Vol;ltilc M~IIICI .. A i r O v c ~ i Method ................................................................................................... <';I 2c . -25 (07) i111d Volatile Mil t tcr . V;lcuu~l i Ovc l i Mctl iot l ........................................................................................... (';I 711 -75 ( 0 7 ) Moi l i l ' ict l Kar l l;isclicr Mct l iod ............................................................................................................... (';I 2c -S4 (07) . . . Mot l l l lcd M o i s ~ u r c ;ultl Vol:~lilcs ......................................................................................................... (';I 21' -03 (07)

I~ iso luh lc I~ i i l>~r r i t i cs ....................................................................................................................................... (';I 3;1 -40 (07 ) I lcs i~r lc I<csiilucs ill I .. ;11h ;111iI o i l s .................................................................................................................. (':I 311 -S7 ( 0 0 ) Soluble Mineral MLIII~~ i111d Fatty Acids Con ib i~ icd as M i ~ i c r a l Soap ........................................................... (';I J -25 (07) 14.1. cc I;atty Acirlh ............................................................................................................................................. (';I i;~ -40 (07) ('l.uilc. I;;ltly /\cit l\ (lot;ll I';~tty ;~citls ~ILIS u~ is ;~ l~o~~ i I ' i ;~h lcs ) ............................................................................ (';I 511 -7 I ( 0 7 ) 13uty1.ic A c i d ................................................................................................................................................... ( ':I 5c . -S7 ( 0 7 ) l i~is;~l>c~i i l ' ia l>lc Matter

I l x c c l ~ t M i l r i ~ i c Oi ls ............................................................................................................................... I (i;~ -J( J ( \ )7 J

I ~ i c lud i l l g Marine Oi ls ............................................................................................................................. (';I (111 -53 (07) ........................................................................................................ . I lyilroc . .lrho~is (III~I~CI.;I~ o i l ) ill 1;;1ls ('.I Oc Oi (071

l ) c t c c ~ t i o ~ ~ ol ' ( ' l i lovi~~;~tct l Solvc~i ts Bc i l s tc i~ i Tcsl .......................................................................................................................................... (';I 7 -35 (00)

I )c~cct io l i ol' Sul l'ur Coil1 I > > ( ............................................................................................................................................. I S;I -35 (00) ' I '

. . Silvcr I j c ~ ~ z o ; ~ l c Icst ............................................................................................................................... (';I SII -35 (00) !

. ................................................................................................................................................. .. I <c I ' i~ i i~ i y I oss ( ';I O;I i ? (07) ('rutlc Oi ls ............................................................................................................................................... (';I ');I -52 ( 0 7 ) I5xt1-;lctcil Soyl>c:~~i O i l .......................................................................................................................... (';I 0;1 -52 ( 0 7 ) I ) c g u ~ i i ~ i i c i l . I i y d r i ~ u l i c i l l id Estractcd Soybc;111 O i l ................................................................................ (';I 0;1 -52 (07) L>cgu~i i~i icr l . Esl>cllcv Soyhc;~ri O i l ......................................................................................................... I I -57 (07) I~~st ractc t l ;111tl KCC~IISI~~IIIC~ I'rc~rcsscd Cotto~iscci l Oi ls ................................................................... (';I O i l -57 (07 )

Neutral O i l ;11id 1~1ss ...................................................................................................................................... (':I 01' -57 ('10) Ijrcak 'Tc.51 (cl.utlc soyhcati o i l ) ...................................................................................................................... (..I 10 -40 (SOJ 'I' A311 ............................................................................................................................................................. I I I -55 (07) l ' l iosl~hor~rs ( c o l o r i ~ i i c ~ r i c ) .............................................................................................................................. I I 2 -55 (07) I ' l i os l> l~~~-us by A A S ....................................................................................................................................... (';I 1717 -02 ('17) Gossypol . Total (cl'udc cotto~isccd o i l iuid soap stock) .............................................................................. I 1 . 1 -50 (07) Cilyccrol: Total . Free and Combinct l .............................................................................................................. (';I I 4 -50 (07) Cilyccrol . Frcc . by IiPLCILI, S D ............................................................................................................................ I 1-11) -00 ('17) l'racc Meti l l .; by A A S ..................................................................................................................................... (';I 15 -75 (07)

........................................................................................................................ So i l i u~ i i ;111tl C;IIC'~LIIII by A A S I 151) -S7 (07) I'olyctliylc~ic ill Fats and Oi ls ........................................................................................................................ (';I I 0 -75 (07) . Trilcc Mc1.1ls . A A S wi th Graphite Furnace I IS -70 ( 0 7 ) l'~.acc Mct.11~. A A S with Grnpliitc Furnace .................................................................................................... (';I IS11 -0 I (07)

. I .cat I. A A S wi th Graphite Furnace ................................................................................................................. I 1 Sc -9 1 (07) I ' l~ospl~oli l>icls ill Vcgctablc O i l ................................................................................................................. (';I 10 -SO ('17 I'liosl3lio1.~1\ ill O i l by ICI'-01's ...................................................................................................................... (. .I 20 -0'1 ('10) I>ctcct io~i ol'Co\tonsccd O i l . H ; ~ l p l i e ~ ~ Test .............................................................................................. I I -25 ('17)

................................................................................... 1)ctcctiori ol'Scsi11nc O i l . Modi f ied Vil l;~vcccli ia Tcst I -40 (07) ......................................................................................................... I)c~cct iol i ol'Tc;~sccd O i l . Fitelso11 Tcst I 3 -30 (07)

................................................................................................ I t lc~~ti I ' ic. ;~t io~i ol' Oi ls . Motlil.ictl Crisnicr Test (-17 4 -3.5 (07) ...................................................................................................... I ) c~c~c l i c~n 01' I:c11.ciy11 I;;I~S ill I'orC, 1;;1t ( '11 5 -40 ( 0 3 ) 'I'

I 'KOI)LI( 'T-MI T I IOO LIST I1Y SL ( 'T I0N

Method Latest number issue

Allatoxins M I iuid M. in Dairy Products ....................................................................................................... C 6 -86 (97) Melting Point

Capillary Tuhc Method ............................................................................................................................ C I -25 (97) Wilcy Method C 2 -38 (9 I ) * b .........................................................................................................................................

........................................................................ Slip Mclting Point of Hard Fats ( lx~ ln i oil) . AOCS Standard C 3 -25 (97) Slip Melting Point . IS0 Standard .................................................................................................................. C 3h -92 (97) Slip Point (soft fats) ................................. : ..................................................................................................... C 4 -25 (89) * Flow Test ........................................................................................................................................................ C 5 -25 (89) * Cloud Point Test ............................................................................................................................................. Cc 6 -25 (97) Refractive Index ............................................................................................................................................. C 7 -25 (97) Blcacliing Tcst

......................................................................................................................... Cottonseed Oil (refined) C 8a -52 (97) Soyhcan and Sunflower Oil .................................................................................................................... Cc 8b -52 (97)

.................................................................. Refined and Bleached Color (tallow and greases for soaps) c 8d -55 (97) Modified Bleach Test for Soybcan Oil ................................................................................................... c 8c -63 (97) Evaluation of Bleaching Clays and Ahsorhcnts .................................................. ........................ C XI' -91 (97)

........................................................................ Smokc . Flash and 1-ire Points: Clcvcli~~id Open Cup Method Cc (>:I -48 (07) Flash Point . Closed Cup Method ................................................................................................................... C 91, -55 (97) Flashpoint hy Pcnsky-Martens Closed Cup Flash Tcstcr ............................................................................... C 9c -95 (97) Specilic Gravity of Oils and Liquid Fats ....................................................................................................... C IOa -25 (95) * Specitic Gr-avity of Solid Fats and Waxes ...................................................................................................... C IOh-25 (97)

....................................... Dctcrmination 01' Mass pcr Unit Volu~iic ("Liter Weight") in Air of Oils and Fats C I Oc -95 (97) Cold Test ........................................................................................................................................................ C I 1 -53 (07) Titer Tcst (for oils) ......................................................................................................................................... C 12 -59 (97) Color

FAC Method .............................. : ........................................................................................................... C 13:1 -43 (97) Wcsson Method (AOCS Lovihond) ....................................................................................................... Ce 13h-45 (97) Spcctrophotolnetric Method ................................................................................................................... c 13c -50 (97) Chlorophyll Pigments (refined and bleached oils) ................................................................................. Cc l3d-55 (99) Lovihond (British Standard) ................................................................................................................... Cc 13c -92 (97) Refined and Bleached Saponification Color ........................................................................................... C 13s -94 (97) High Quality Tallow and Coconut Oil Saponification Color ............................................................... C 13g-04 (97) Tallow and Coconut Oil Saponification Color ........................................................................................ c 1311 -94 (97) Chlorophyll Pigments (crude vegetable oils) .......................................................................................... Cc l3i -96 (97) Autoniated Method ................................................................................................................................. C 13j -97 (97)

Congeal Point ................................................................................................................................................. CC I4 -59 (97) Soap in Oil . Coilductivity Method ................................................................................................................. c 15 -60 (89) 'k

Consistency, Pcnetro~ncter Mcthod ................................................................................................................ c 16 -60 (97) Soap in Oil . Titri~netric Method .................................................................................................................... Cc I7 -95 (97) Droppilip Point ............................................................................................................................................... c I8 -80 (99)

........................................................................................................................................ lodine Value (Wijs) d 1 -25 (93) * lodi~ie Value. Cyclohexane Method ............................................................................................................... d I h -87 (97) lodinc Value (calculated from GLC) .............................................................................................................. d Ic -85 (97)

.......................................................................................... lodi~ic Value . Cyclohexane-Acctic Acid Mcthod Cd I d -92 (97) Thiocyanogen Value ....................................................................................................................................... d 2 -38 (73) * Saponification V ~ ~ l u c (oils and fats) ............................................................................................................... C 3 -25 (97)

.......................................................................................... Saponilication Value . Calculated (Oils and Fats) d 3n -94 (97) Saponilication Value (dcodol.izcl. distillates and sludges) ............................................................................. d 31, -76 (07)

............................................................................ Saponification Vi~lue . Modilictl Mcthod Using Mcth;~nol d Rc -01 (97) Acid Vi~luc of Fats and Oils ........................................................................................................................... d 3d -03 (99) Acetyl and Hydroxyl Values (by saponification) ......................................................................................... d 4 -40 (99) Reichcrt-Mcissl . Polenskc and Kirschner Values .......................................................................................... d 5 -40 (97)

......................................................................................................................... Liquitl and Solid Fatty Acitls C 6 -38 (89) * P~ l~~~nsa tu ra tcd Acids ................................................................................................................................... ( 1 7 -58 (97)

........................................................................................ . Pcroxidc Value Acetic Acid-Chloroform Method d 8 -53 (07) ........................................................................................... . Peroxidc Vi~luc Acetic Acid-lsooctane Method d 8h -90 (97)

Oxiranc Oxygen ............................................................................................................................................. C 9 -57 (97) ............................................................................................................................................... Solid Fat llldex d 10 -57 (97)

I'KODU(:l -ME 1 1 I( 11) L I S 1 UY S E C l ION

Method Lalesl

number issue a-Monoglyccriclcs ......................................................................................................................................... C I 1 -57 (09) Mono- and Diglyccridcs by Capillary GLC ................................................................................................... Cd I Ih-Ol (97)

/F Mono. . Di- and Triglyccridcs by Silica Gel Chromatography ..................................................................... C I lc-93 (07) Mono- and Diglyceridcs by HPLC-ELSD .......................................................................................................... Cd I I t l -06 (90) Fa1 Stability . Active Oxygc~ i Method ( A O M ) ................................................................................................ C(l I 2 -57 (03) 4:

\-'at Stability . Oi l Slnbility Index (OSI) .......................................................................................................... ('tl I ?I)-')? (07) Hydroxyl Valuc (direct titration) ................................................................................................................... d 13 -60 (07) /r.rrrr.r 1so111crs . Isolated (FTIR) ....................................................................................................................... d I 4 -95 (07) tr.~rrr.r Iso~llcrs in Partially Hydrogc~iatcd Oils by GLC-IR ............................................................................ I I4h-03 (95) :': tr.[or.s Isollicrs by Capillary CiLC .................................................................................................................... Cd 14c-94 (04) d:

Also scc ................................................................................................................................................... I ?;I -04 (07) t,urir.s Iso~iicrs ill Triglyccridcs by ATKIFTIIZ ............................................................................................................ Ccl l4tl -00 (00) cis. c.i.v Polyu~isaturnted Fatty Acids .............................................................................................................. C 15 -78 (97) Solid Far Content (SFC) by NMR ................................................................................................................. Ctl I 6 -81 (YO) Solid h t Content (SFC) by Low-Resolution NMR ..................................... I hb-00 (09) rr(r1r.v U~isaturation in Margarine .................................................................................................................... I 17 -85 (03) :" 1)-Anisidine Valuc ........................................................................................................................................... d I8 -00 (07) 2-Tliiobarhituric Acid ( T B A ) V:~luc ............................................................................................................... C:il I 0 -90 (07) Polar Co~i ipou~lds in Frying Fats ................................................................................................................... d 3-0 -91 (07) Benzo(a)pyrcne in Edible Oils and Fats ........................................................................................................ C 3-1 -01 (97) Polymerized Triglyccridcs by Gel-Permeation HPLC ................................................................................... CLI 22 -01 (07) Pesticides in Oils anil Fats ............................................................................................................................. 3 3 -03 (07) Dctcrminalion o f Di~ncthylpolysiloxa~ies in Fats and Oils ............................................................................ ['(I 24 -05 (07) DowthermTM (heat tra~isfcr fluid in I l l s and oils) by GLC .......................................................................... C 25 -Oh (97) Stigmnstadiencs in Vegetable Oils ................................................................................................................. I 26 -06 (07) Steroidal Hydrocarbons in Vegetable Oils .................................................................................................. d 77 -00 (07) Fatty Acid Composition by GLC ................................................................................................................... c I -02 (97) Marine Oi l Fatty Acid Composition by GLC ................................................................................................ C'c I I? -80 (09) Fatty Acid Composition by GLC, (.is. cis and r r~ r r~s Isorncrs ........................................................................ Cc Ic -80 (05) :I' n-3 and n-6 Fatty Acids by Capillary GLC .................................................................................................... C I d -0 I (03) 'I: Fatty Acids by Capillary GLC ....................................................................................................................... C Ic -0 I (97) c.i.v - :uid rruor.v- Fatty Acids in Oils and h t s by Capillary G L C .................................................................... c I I' -06 (07) 1,rrrr.s. Fatty Acids by Silver-Ion Exclinngc HPLC ........................................................................................ Cc l g -00 (97) Prcpnrution o f Methyl Esters o f Fatty Acids .................................................................................................. C 2 -66 (07) Tocopherols and Sterols in Soya Residues by GLC ...................................................................................... C 3 -74 (07) Erucic Acid in Oils and Fats .......................................................................................................................... c 4 -86 (95)

............ Erucic Acid in I-ligli Elucic Acitl Oils and F;~ts hy Packctl Co lu~nn G;Is-Licluid CIirorn;~togr;~l?lly Cc -t -05 (07) Triglycc~.idcs by Cius Chronlntography .......................................................................................................... Cc 5 -80 (07) Triglycerides by HPLC .................................................................................................................................. c 5b -89 (07) Individual Triglyccridcs by HPLC ................................................................................................................. Cc Sc -93 (97) Antioxidants by HPLC ................................................................................................................................... C'c h -86 (07) Tocopherols (total ) in Ilcodolizcr Distil lntc .................................................................................................. C 7 -87 (07)

.. 1i)col'Iicrols ;ulil 'rocotric~lols ill Vcgc~al>lc Oils ;11ic1 Ii;1ts by tIPI, C: ............................................................. Cc X 80 (07) 12cco1iin1cndctl Practices I '~)~.Tcst i~ ig Fccd-Gri~dc h t I'roducts ..................................................................... I I -68 (07) Corrclutio~l ol' O i l Volatilcs with Flavor Scores ol' Edible Oils ..................................................................... C 1 -83 (07) I;lavor Panel Evalu;~tion ol' Vcgc~ablc Oils .................................................................................................... C 3- -83 (07) licconlmcndcd Practices for Assessing Oi l Quol ity Stability ........................................................................ ('g 3 -0 I (07) Volatilcs (VOC) it1 Fats and Oils by G1.C .................... .. .......................................................................... g 4 -04 (07)

.................................................................................. Oven Storage Teat I'or Accclcratcd Aging ol' Oils ('y 5 -07 (07) Olive Oi l . Preparation of Mcthy l Esters of L.o~ig-Chain Fatty Acids .......................................................... I I -0 I (07) Olive O i l . Fatty Acids by Capillary G L C ............................................................................................... I 7- -0 I (07)

r~ur~r.s Unsaturated Fatty Acids by Capil l i~ry Co lum~i GC ....................................................................... cli ?a -04 ( 0 0 ) .............................................................................. Olive Oi l . Fatty Acids in the 3_-P~)sitio1i in Triglyccridcs 3 -01 (07)

Olivc Oi l . Chlorophyll Pigriicnts ................................................................................................................... I 4 -01 (97) Olive Oil. Specilic Extinction ........................................................................................................................ 5 -91 (07)

.................................................. ......................... Olive Oi l . Stcrol Fraction by TI, C and Capillary GLC ... I h -9 I (97) ....................................................................................................... Olivc Oi l . International Trc~dc Standards I 7 -04 (07)

................................................................ Jo-john Oil, Methods I'or thc Determination ol'Quolity and Pur.ity C I -01 (07)

. - . ~~~~~

Mclhod Lalcsl

nu~ii l~cr issuc

Jojoh;~ Oil . Dc~cction ol'Triglyccridc Adulteralion ...................................................................................... C 3 -01 (07) ................................................................................................................................... Jojoha Oil . Acid Vi~lue C 4 -0 I (07)

DSC Mclting Properties of Fals and Oils ...................................................................................................... Cj I -94 (97) X- l iny Diffraction Analysis of Fats C 2 -95 (97)

A ............................................................................................................... Calihriltion of Rhcologicnl Instruments ......................................................................................................... C 3 -90 (00 )

Section D: Soap and Synthetic Detergents Soap and Soap Products Conip~uison of AOCS & ASTM Methods ................................................................................................... D- 1 -99 (99)

................................................................................................................................................. Sampling I 1 -45 (97) Moisture and Volatile Matter . Air Oven Method .................................................................................... Da Za -48 (97) Moisture. Distillation Method ................................................................................................................ I 2h -42 (97) Alcohol-Soluhle and Alcohol-Insoluble Matter ..................................................................................... I 3 -48 (97) Free Acid or Free Alkali (soda soaps) .................................................................................................... a 4a -48 (97) Free Alkali and Potassium Carbonate (potash paste soaps) ................................................................... a 5 -44 (97)

Water-Insoluble Matter .................................................................................................................................. D 6 -48 (97) Total Alkalinity ot' Alcohol-Insoluble Matter ................................................................................................ a 7 -48 (97) Total Anhydrous Soap and Combined Alkali ................................................................................................ a 8 -48 (97)

..................................................................................................................................................... Chlorides a 9 -48 (97) Unsaponilied Plus Unsaponitiable Matter ..................................................................................................... a 10 -42 (97) Unsnponiliablc Matter ................................................................................................................................ Do 1 1 -42 (97) Rosin . McNicoll Method ............................................................................................................................... h~ 12 -48 (99) Titer Test ........................................................................................................................................................ a 13 -48 (97) Acid Value of Fatly Acids ............................................................................................................................ a 14 -48 (97) Iodine Value ................................................................................................................................................ I 15 -48 (97) Saponification V;~luc ..................................................................................................................................... I 16 -48 (97) Borax ........................................................................................................................................................... 1 17 -52 (97) Alkaline Silicates .......................................................................................................................................... I 18 -48 (97) Carbonates . Glavinietric Absorption Method ............................................................................................... Da 19a -42 (97) Carbonates . Volumetric Evolution Method .................................................................................................... a 19b-42 (97) Phosphates (gravimetric method) ................................................................................................................. D 20a -48 (97) F Phosphates (titri~iictric method) ................................................................................................................... D;I 20h-57 (97) Tetrnsodium Pyrophosphatc ........................................................................................................................... I 2 1 -48 (97) Sulfi~lcs ....................................................................................................................................................... I 22 -48 (97) Free Glycerol ................................................................................................................................................. a 23 -56 (97) Sugars ............................................................................................................................................................. a 24 -48 (99) Starch ........................................................................................................................................................ I 25 -48 (97) Volalilc I-l ydrocarhons ................................................................................................................................... Dn 26 -42 (97) Comhinccl Sodium and Potassium Oxides .................................................................................................. I 27 -48 (97) Screc~i Test ..................................................................................................................................................... a 28 -39 (97) Copper ............................................................................................................................................................ I 3 1 -58 (97) Soap Containing Synthetic Detergents

Moist~tre and Volatile Matter ................................................................................................................. D I -48 (97) Alcohol-Soluhlc and Alcohol-Insoluble Matter ..................................................................................... I 2 -48 (97) Free Acid or Free Alkali ......................................................................................................................... D 3 -48 (97) Water-l~isoluble Matter ........................................................................................................................... Dh 4 -48 (97) Total Alkalinity of Alcohol-lnsoluhlc Matter ...................................................................................... D 5 -48 (97) Total Anhydrous Soap ............................................................................................................................ D l 6 -48 (97) Chlorides (indicator method) ............................................................................................................... I 7 -48 (97) Chlorides . Potentiornetric Determination .............................................................................................. D 7h -5.5 (97) Snponilication Value ............................................................................................................................... D 8 -48 (97) Alkalinc Silicates .................................................................................................................................... D 9 -48 (97) Fatty Matter ............................................................................................................................................ D 10 -38 (97) Rosin . McNicoll Method ........................................................................................................................ D I I -48 (97)

Fatty Alkyl SulTales Sampling ................................................................................................................................................. D 1 -59 (97) Moisture by Distillation Method ............................................................................................................ D 2 -59 (97) Alcohol-Soluble Matter .......................................................................................................................... Dc 3i1 -59 (07)

I l'UOl)U( I-MI I1 1 0 1 1 1151 l % Y SIC ll( ) N 1 I

Mcthod Latest

number issue

Alcohol-lnsolut>lc Matter ....................................................................................................................... I)c 3h -50 (97) Eslcr SO. ............................................................................................................................................... Dc 4 -50 (97) Comhincd Alcohols ................................................................................................................................ Dc 5 -59 (97) Alkalinity ................................................................................................................................................ c 6 -50 (07) Sod~um Sulfiitc ........................................................................................................................................ D 7 -59 (07) Unsull'ated Material ................................................................................................................................ Dc S -59 (07)

Alkvlbcnzcnc Sulfonates Sanipling ................................................................................................................................................. D I -59 (07) Moisture by Distillation Method ............................................................................................................ D 2a -50 (07) Modified Karl Fischcr Reagent ............................................................................................................... d 2b -59 (80) * Sodium Alkylbcnzenc Sulfonatc by Ultraviolet Absorption .................................................................. Dtl 3 -00 (07) Neutral Oil (unsulfonated material) ........................................................................................................ D l 4 -60 (97) Color . Linear A l kylbenzenc Sulfonatcs .................................................................................................. D 5 -92 (97)

Section E: Glycerin S;lnlpling ........................................................................................................................................................ I I -38 (97) Ash ................................................................................................................................................................. i 2 -38 (73) * Alkalinity ....................................................................................................................................................... I 2 -38 (73) :k

Acidity ............................................................................................................................................................ I 2 -38 (73) * Sodiu~n Chloride ............................................................................................................................................ a 2 -38 (73) * Total and Organic Residue ............................................................................................................................. En 3 -58 (73) * (jlyccrol .......................................................................................................................................................... 13 0 -5 1 (07) * Crude Glycerin ............................................................................................................................................... I 0 -04 (07)

............................................................................................................................................. Spccific Gravity i 7 -95 (97) Moisture ......................................................................................................................................................... I 8 -58 (97) Color (APHA scale) ....................................................................................................................................... I 9 -65 (07)

Section F: Sulfonated and Sulfated Oils Moisture . Distillation Method ........................................................................................................................ F' la -44 (97) Moisture atld Volatile Matter. Hot Plate Method ........................................................................................... F Ib -44 (97) Orgiuiically Co~nbincd Sulfuric Anhydride

Titration Mcthod ..................................................................................................................................... F 23 -44 (07) Extraction Titr;ition Mctliod .................................................................................................................. I 2b -44 (07) Ash-Gravinietric Method ........................................................................................................................ I; 2c -44 (07)

' l i~t i i l Dcsull'iited Fatty Matter ........................................................................................................................ F 3 -44 (97) ................................................................................................................................. 'Totnl Active Inyrcdients 4 -44 (97)

Unsal>o~~iliablc Nonvolatile Matter ................................................................................................................ F 5 -44 (97) ............................................................................................................................................... Inorganic Salts F 0 -44 (97) .............................................................................................................................................. Total Alkalinity F 7 -44 (97)

Total Ammonia .............................................................................................................................................. F 8 -44 (97) Acidity (sulfonnted or sulfated oils . with exceptions) ................................................................................... F 9n -44 (97) Acidity (dark-colored oils, with exceptions) ................................................................................................. F Ob -44 (07)

. ............................................................. Acidity '(in the prcscnce of ammonium 01 triethanolaniine soaps) F 9c -44 (07) Water-lniniisciblc Organic Solvents .............................................................................................................. 1 I0 -44 (07)

Section G: Soap Stocks Sampling ........................................................................................................................................................ G I -40 (07)

.................................................................................................... ' l i~tal Fatty Acids . Wet Extraction Method 3 -53 (97) Oxidized Fatty Acids . Wet Extraction Method .............................................................................................. G 3 -53 (07)

............................................................................................................................................ Total Fatty Acids G 4 -40 (07) Neutral Oil ..................................................................................................................................................... G 5 -40 (07) Titcr Test ........................................................................................................................................................ G h -40 (07) 111 1 ................................................................................................................................................................... G 7 -50 (07)

Section H: Specifications for Reagents. Solvents and Apparatus I:orccd I)! . ~I'L O v c ~ ......................................................................................................................................... H I -30 (07) Pctrolcum Elher ............................................................................................................................................. t-l 2 -41 (07)

...................................................................................................................................................... A i l Ovcn I1 3 -45 (97)

I I

Method Latest

number issue Vacuum Ovcn ................................................................................................................................................. H 4 -45 (97) Thcrniomcter Specilications ......................................................................................................................... H 5 -40 (97) *rhermonieter Specifications (see H 5-40) ..................................................................................................... H 6 -40 (97) . / \

..................................................................................................... Thcrmomcter Specilications (see H 5-40) H 7 -45 (97)

..................................................................................................... Thcrmomctcr Spccilications (see H 5-40) H 8 -45 (97) Desiccants ...................................................................................................................................................... H 9 -87 (97) Ther~iionieter Specifications (see H 5-40) ..................................................................................................... H 10 -55 (97) Thermometer Specifications (see H 5-40) ..................................................................................................... H I 1 -58 (97) Sodiu~li Hydroxide . Standard Solution ......................................................................................................... H 12 -52 (97) Sulfuric Acid. Standard Solution ................................................................................................................... H 13 -52 (97) Hydrochloric Acid, Standard Solution ........................................................................................................... H 14 -52 (97) Alcoholic Potassium Hydroxide. Standard Solution ..................................................................................... H 15 -52 (97) Commercial Hexane ....................................................................................................................................... H I 6 -56 (97) Synthetic Mcthyl Alcohol .............................................................................................................................. H 17 -58 (97) lsopropyl Alcohol .......................................................................................................................................... H 18 -58 (97) Industrial Tolucnc .......................................................................................................................................... H I 9 -58 (97)

Section J: Lecithin Moisture ...................................................................................................................................................... a 2a Moisture . Karl Fischcr Reagent ..................................................................................................................... a 2h Hexanc-Insoluble Matter ............................................................................................................................... I 3

.............................................................................................................................. Acetone-lnsolublc Mattcr I 4 Phosphorus . Total ........................................................................................................................................... I 5 Acid Valuc ...................................................................................................................................................... I 6 Phospholipids in Lccithin Concentrates by TLC ........................................................................................... Ja 7a Phospholipids in Lecithin Concentrates by HPLC ........................................................................................ a 7b Pcroxidc Value ............................................................................................................................................... a 8

............................................................................................................................................... Gardncr Color J ~ L 9 Brooklicld Viscosity ...................................................................................................................................... a 10 Viscosity of Transparent Liquids by Bubble Time Method .......................................................................... a I I Analysis of Lecithin Co-Products .................................................................................................................. a 12 Deterniination of Tocophcrols in Lecithin by HPLC ..................................................................................... Ja 13 Determination of Iodine Value in Lecithin . Wijs Method ............................................................................. I I 4

Section M: Evaluation and Design of Test Methods Precision of Analytical Methods .................................................................................................................. M 1 -92 (97) Writing and Approval of Methods ................................................................................................................ M 2 -65 (97) Surplus Status of Mcthods ............................................................................................................................ M 3 -82 (97) Collabor;~tivc Study Proccdures ..................................................................................................................... M 4 -86 (97)

Section R: Official Listings Approved Chemists ............................ .: .......................................................................................................... R 1 -99 (99) Ccrtificd Laboratories .................................................................................................................................... R 2 -99 (99)

........................................................................................................................ AOCS Tcclinical Comniittecs R 3 -99 (99) Sninlley Statistical Data. 1985-1986 ............................................ .... ............................................................. R 4 -89 (97) International Trade Methods ......................................................................................................................... R 5 -93 (97) Surplus (obsolete) Methods Listing ............................................................................................................... See Index

Section S: Recommended Practices for Testing Industrial Oils and Derivatives Conimcrcii~l Fatty Acids ................................................................................................................................ S I Drying Oils ..................................................................................................................................................... S 2 Epoxidizcd Oils .............................................................................................................................................. S 3 Fatty Nitrogcn Products

F;~tty Amincs ............................ .... ........................................................................................................... S 4;1 p . itty Amidoamincs ................................................................................................................................. S 4b Fatty Quaternary Amnionium Chlorides ............................................................................................... S 4c Fatty Diamines ........................................................................................................................................ S 4d

Polymcrized Fatty Acids ................................................................................................................................ S 5

"'Surplus ~iicthod Page R of 1 0

I'h'OI7(l( T-hlL I l iOD LIST I I Y SL('Tl t IN

Method Latesl number issue

Cleveland Opcn Cup ( I i ~ ~ t y acids) ........................................................................................................... 'l'n la -64 (97) Cleveland Open Cup (drying oils) .......................................................................................................... T I l a -64 (97) Closcd Cup . Fatty Quaternary Ammoniuln Chlorides ........................................................................... Tn 2a -86 (97)

Specilic Gravity Commercial Fatty Acids ......................................................................................................................... To la -64 (97) Drying Oils ............................................................................................................................................. TI I h -04 (97)

Refractive lndcx Commercial Fatty Acids ......................................................................................................................... T la -64 (97) Drying Oils ............................................................................................................................................. Tp la -64 (97)

Viscosity Buhhlc Timc Method (drying oils) ......................................................................................................... T la -64 (97)

Titer Commercial Fatty Acids ......................................................................................................................... Tr la -64 (97)

Rosin Acids Corn~nercial Fatty Acids ........................................................................................................................ T la -64 (97)

Tolcra~lcc Tcst . Acctollc (drying oils) ............................................ ; , ............................................................................. T In -64 (97)

P H of Fatty Quaternary Ammonium Chlorides ............... ............................................................................ Tu In -64 (97)

Average Molecular Weight Fatty Quatcrnary Anilnoniu~n Chlorides .................. .............................................................................. Tv la -64 (97)

Nonamincs Fatty Amines and Fatty Diamines ........................................................................................................ Tw l a -64 (97)

Hydroxyl Value of Epoxidized Oils ............................................................................................................... Tx la -66 (97) ....................................................................... Dicarboxylic Acid Composition of Dimethyl Esters by fiLC Ty la -76 (97)

Activity o f Hydrogcnation Catalysts ............................ . . . ............................................................................. T l a -78 (97) Sclcctivity of Hydrogcna~ion Catalysts ........................... ., ............................................................................. T . I h -79 (97)

*Surplus method Page 1 0 of 10

1999 Table of Contents Alphabetical Index

Mrtl~ocl L,l lrsl

I numljcr issur Acc(one-lnsolublc Mntlcr ill Lecithin ............................................................................................................ .la 4 -40 (07)

. . Acetone Tolcr:~ncc o f Heat-Bodied Drying Oils ............................................................................................ '1'1 I ;I -04 (07) Acctyl and t lydroxyl V:~lucs (by sapol~ilication) ........................................................................................... ('(1 4 -40 ( 0 0 ) Acid-Insoluble Ash ill Oilsced Meal Products .......................................................................................... I ~ I 51) -08 (07) Acid Value

ol' Conlmcrcial Fatty Acids .................................................................................................................... TC I ;I -04 (07) ol' I>ihasic Acids .................................................................................................................................. 4 ; 1 -70 (07) ol' I l ry ing Oi l \ ......................................................................................................................................... I ';I -04 (07) o f Fats and Oils ....................................................................................................................................... Ccl 3~1 4.3 (00) o f F:ltty Acids ......................................................................................................................................... O ~ I I 4 -48 (07) ol' Fatty Quatcr~iary Anlmorlium Chlorides ......................................................................................... I 3 a -04 (07) . . . ol I . cc~t l l~n ................................................................................................................................................ I:\ 0 -55 (07)

Acidity ol'Glyccrin .............................................................................................................................................. I<;I 2 -3s (7.3) 'I: of Sulfonntctl :~nd SulL~tcd Oils . Dark Colored, with Exceptions ........................................................ F Oh -44 (07) o f Sull'onatcd arid SulL~tct l Oils. in the Presence o f Ani~nonium or

Triet\lanol;~mine Soaps .................................................................................................................... F 9c -44 (07) 01' Sull'on;~tcd ant1 Sulkltcd Oils . with Exceptions .................................................................................. 1; O;I -44 (07)

Active I~~grct l icnts in Sulfonatcil ant1 Sull';~tcd Oils ....................................................................................... l;4 -44 (07) Active Oxygen Method (AOM) for Fat Stability ........................................................................................... Ctl I 7 -57 (0.3) :I'

Activity of Hydrogenation Catalysts .............................................................................................................. T . I ;I -78 (07) Allatoxins

in Copra and Copra Meal ....................................................................................................................... A I -72 ( 0 0 ) .................................................................................................................................................... in Corn A. 1 I -SO (07)

... in C'orn (a l l~n i ty col i~r i ln) ........................................................................................................................ A1) 7 -0 I (00) in Corn by ELIS A ................................................................................................................................... A Oa -07 (00) in Corn (whole . clxcked. meal . germ) .................................................................................................... A; 3 -87 ( 0 0 ) in Corn and Peanut by T L C .................................................................................................................... A;! ();I -07 (00 ) in Corn . Zcaralcnonc and a-Zcaralcnol .................................................................................................. A 2 -80 (07) in Cottonseed. Sccd Meal . Meats . Fl:~kcs ............................................................................................... A S -83 (00) in Dniry Products . M I and M, ................................................................................................................ C'l) 0 -80 ( 0 7 ) in Peanut Butter (affinity colurnn) .......................................................................................................... A 7 -01 (00) in Pconuts (groundnuts), Raw (:~flinity column) ..................................................................................... A 7 -0 I (90) in Pcnnuts (groundnuts) . Raw, Roasted . Meal . Butter ............................................................................ A 0 -08 (00 )

Allatoxins B I . B, and G I in Corn, Cottonseed. Peanuts and Pe;~nut Butter ................................................ A 0 -05 (00 ) Allatoxins . Conlirmation by T L C .................................................................................................................. A 0 -SO (00) Allatoxin Standards (preparation) .................................................................................................................. A;I 10 -88 (00) Alcohol-Insoluble Matter in Fatty Alkyl Sulfates .......................................................................................... c ?I> -50 (07) Alcohol-Soluble and Alcohol-Insoluble Matter

in Soap and Soap Products ..................................................................................................................... I):\ 3 -4s (07) in Soap Containing Synthetic Detergents ....................................... t 7 -48 (07)

Alcohol-Soluble Mnttcr in Fatty Alkyl Sull'lltcs ............................................................................................ c 3a -59 (07) Alkaline Silic:~tcs

................................................................................................................... in So;~p and Soap Products I I S -48 (07) in Soap Cont;~ining Syrltllctic I)ctcrgc~lts ............................................................................................ 0 -4s (07)

Alkalinity ol' F:ltty Alkyl Sull~:~tcs ............................................................................................................................ I l c 0 - 5 0 (07) 01 ' Glyccrirl .............................................................................................................................................. E:I 2 -38 (7.3) 'I'

o f Sullhnatcd ant1 Sull':~tcd Oils .............................................................................................................. 1: 7 -44 (07) Alkalinity ol' Alcoliol-lnsoli~I,lc Matter

in Sotla Seal> ;lntI I '~.od~cts .................................................................................................................... I 7 -48 (07 ............................................................ ill Sotl:~ Soap and Prc~Iucts Coritaining Syrltllctic Dctcrgcrlts I 5 -48 (07)

Aniincs . Tests ........................................................................................... I'or Fatty Qu.~tcrna~.y Ammo~i ium Cliloridcs I 3i1 -64 (07)

lor Prinlary A~nincs . by Gas Chromatogr:~phy ....................................................................................... I 'I '4a -77 (07)

ALI'HAI1LTI('AI . INDEX 1 Method .. Latest

number issue

for Primary . Sccondi~ry and Tertiary Amincs . Percent in Fatty Acids .................................................. T 3n -04 (07) Aminc Value

Fatty Quaternary A~n~nonium Chlorides ................................................................................................ T 3n -64 (07) Primary . Secondary and Tertiary Indicator Fatty Amines ...................................................................... T 2h -04 (97) Pri~liary . Secondary and Terliary Polentiometric Fatty Atnines ............................................................ T I 2a -64 (97) Total Indicator Fatty Amines .................................................................................................................. T I h -04 (97) Totill Potentiometric Fatty Amines ...................................................................................................... T In -64 (97)

Ammonia (total) in Sulfonated nnd Sulfated Oils .......................................................................................... F 8 -44 (97) Anhydrous Soap (tolal) .................................................................................................................................. Dh 6 -48 (97) Anhydrous Soap and Cotnhined Alkali (total) ............................................................................................... D i 8 -48 (07) Anisidinc Value .............................................................................................................................................. Cd I8 -90 (97) Antioxidants in Oils hy HPLC ................................................................................................................ C h -86 (07) AOCS & ASTM Methods l i ~ r Soaps nnd Detergenl Analysis ..................................................................... D I -99 (99) Approved Chemists (AOCS) ................................................................................................................... R 1 -99 (99) Ash

in Dt.yinp Oils ......................................................................................................................................... Tm la -64 (97) in Fn~s and Oils .................................................................................................................................. Cir I 1 -55 (97) in Fatty Acids .......................................................................................................................................... Tm In -64 (07) in Fatty Quntcrnnry A~n~nonium Chlorides ............................................................................................ T I 2a -64 (97) in Glycerin .............................................................................................................................................. I 2 -38 (73) * in Oilsced Cilke and Me:~ls ..................................................................................................................... B;I 5;1 -49 (07) in Oilsccd Mcul. Acid-lnsoluhle ............................................................................................................. I ~ I 5l? -68 (07) in Soya Flours .......................................................................................................................................... B 5 -49 (97)

Beilsteit~ Test .................................................................................................................................................. I 7 -3.5 (90) :E

Benzo(a)pyrenc in Edihle Oils and Fats ........................................................................................................ C 2 1 -9 I (97) Bleaching Tcst

Ihr Cottonseed Oil (relined) .................................................................................................................... Cc 8i1 -52 (07) fi)r Evaluation of Clays and Ahsorhents ................................................................................................. C XI' -0 I (07) for Soyhean Oil (refined) ........................................................................................................................ Cc 8h -52 (97) l i ~ r Soyhci~n Oil (niodificd test) .............................................................................................................. Cc 8c -0.7 (97) for Sunllowcr Oil (refined) .................................................................................................................. c 8h -57, (97)

Boemcr Nutnhcr lor Delcction of Foreign Fats in Pork Fat .......................................................................... C 5 -40 (03) :I:

Borax in Soap and Soap Products .................................................................................................................. i 17 -52 (07) Brcak Test (crude soyhcun oil) ............................... .... .................................................................................... C ~ I 10 -40 (80) :k

Butyric Acid ................................................................................................................................................... C ~ I Sc -87 (97) .................................................................... Butyric Acid (Kirschner valuej in Butterht and Coconut Oils C 5 -40 (07)

Carhona~es hy Gravimetric Ahsorption Method ........................................................................................................ I l %I -42 (97) hy Volutnetric Evolution Method ........................................................................................................... I 1%-42 (07)

Cellulose Yield ............................................................................................................................................... B 3 -47 (90) Ccrtilicd 12ahoratorics (AOCS) ...................................................................................................................... R 2 -96 (97) Chlorides

in Glycerin (crudc) ............................................................................................................................. Ea 2 -38 (73) :I: in Soap and Soap Products ..................................................................................................................... Da 9 -48 (97) in Soap and Sonp Products Contilining Synthetic Detergents Indicntor Method .................................................................................................................................... D 7 -48 (07) Po~cntiomctric Method ......................................................................................................................... h 7h -55 (07)

Clilorinatctl Solvctlts (Bcilstcit~ Tcst) ............................................................................................................ C~I 7 -35 (00) 'I' ................................................................................................................... Chlorol~hyll Pigments (lapcsecd) A 3 -Y2 (07)

......................................................................................... Chlorophyll Pipmcnts (relined and hlcached oils) C 13tl-55 (09) ................................................................................................ Chlorophyll Pigtncnts (crude vegetable oils) c 13i -06 (97)

Chromiuni . Tri~ce Amounts by AAS ................................................................................................................................................... I 15 -75 (07)

.............................................................................................................. hy AAS will1 Graphite Furnace Ci1 I8 -70 (07) ........................................................................ (.is. c . i s i~nd ~ r ~ r r t s Isomers. Filtty Acid Composition by GLC c Ic -80 (05) #'

.............................................................................................................. c.i.c. c.i.r Polyunsaturated Fatty Acids C IS -78 (97) ............................................................................................................................................. Cloud Point Test C 6 -35 (97)

Cold Tcst ........................................................................................................................................................ Cc 1 1 -53 (07)

*'Surplus method Pap , 2 o f 12

,\I 1'1 l;\lil I I( ... IN1 11 A

Mrlliocl L a l c ~ l

nc l~ i~ l tcr i r sw

('ollal>ori~tivc Slutly P~.occdurcs ..................................................................................................................... M 4 -80 (07) Color M c ; ~ s ~ ~ r c ~ i i c ~ i t

by APHA Scale for Glycerin .................................................................................................................. I 0 -05 (07) Ily Color Stability I'or F;~tly Acids ( : ~ f ~ c r Iic;lti~lg) ................................................................................... I ?;I -04 (07) Ily ('omllilictl Alcoliols ill h l l y Alkyl Sull';~tcs ...................................................................................... l)c 5 -50 (07) by Co~ i i l l i ~ i cd Alkal i in Soap i111d Soup Producls .................................................................................... );I 8 -48 (07) by Co~i ih incd Sodium iuld Polassium Oxides in Soap and So:~p Products ............................................. I 27 -48 (07) by FAC Mctllod ..................................................................................................................................... c I3i1 -43 (07) hy Frilly Acids (commercial) .................................................................................................................. 7'tl ?:I -(14 (07) hy Gart l~icr lo r Indu>t~-ial Oils ................................................................................................................. I ' 1 i 1 -04 (07) Color (Aulom;~tctl Mclhocl) .................................................................................................................... ('c 13.1 -07 (07 hy Ga~-dllcr lor 1. ccilhin .......................................................................................................................... I 0 -S7 (07) by I..incor Alkylhcnzcnc Sulfona~cs (LAS) ............................................................................................. l)tl 5 -02 (07) I>y 1, ovihond (I3ritish Slondard) .............................................................................................................. ('c I ?c -02 (07) Ily I . ovihond ( Wcssoll ) ............................................................................................................................ (-c I 31) -45 (07 ) Ily I'~;I~~I~~IIII -('oIli111 Sc;~lc 1.01. 1,igll 1-CoIorctl I. i t l t~it ls ......... .. ................ -I'd 111 -04 (07) Ily S lwc l~~op l~o lo~ i i c t~~ i c Co lo~ ' Mclhotl I'or Oils ....................................................................................... ('c I Jc -50 (07) hy Wchson (1, ovi l>o~id) ............................................................................................................................ ('c 131) -45 (07)

('o~nnliltcc~s (AOCS 1ccIl11ic;ll) ..................................................................................................................... I< 3 -00 (00) C'om~x'siliion ol' I l ih i~sic Acid> hy G L C ......................................................................................................... ' I j la -70 (07) ('o~iiposilion o f Fi11ty Acitls by Gl, C ........................................................................................................... c I -02 (07) ( ' o ~ l i l ~ ) > i l i o ~ i 01' I'ri~nary Amincs by G LC ..................................................................................................... 'l'f 4;1 -77 (07) Congc;~l I'oinl ................................................................................................................................................. c I 4 -50 (07)

. . Conjugated Dicnoic Acid ill Cnslor O i l and Acids ........................................................................................ l i l a 414 (07) Consis~cncy . Pe~ic~l-ation Method ................................................................................................................... c I 0 -00 (07) Copper

ill Oils by AAS ........................................................................................................................................ I 15 -75 (07) in Oils hy AAS will1 Gr:~phitc Furnncc ................................................................................................... I IS -70 (07) in Soap illid Soap Products ..................................................................................................................... I)a 3 1 -5s (97)

Cotlonsccd Oi l . Dc~cct ion in Oils hy Halphen Test ....................................................................................... I I -25 (07) ................................................................................................................................................... Crismcr Tcsl I 4 -35 (07)

C r ~ ~ d c Fi l t~y Acids (total 1';11ty klcids plus unsaponilinhlcs) ............................................................................ (*;I 51) -7 I (07) ('rude Fihcr

in Grains . M c ~ ~ l s . F l o ~ ~ r s . Fccds and A l l Fihcr-Bearing Matcri;lls from Which Fat Can Be Extracted .................................................................................................. I (1 -84 (07)

in Soya Flours ......................................................................................................................................... 13c 0 -40 (07 ) I>c>icc.lnts. Spccilicntions .............................................................................................................................. I I 0 -87 ('17) I les~~ll 'atcd Fatly M i~ t t c r . Total ....................................................................................................................... I 3 -44 (07) Dicarhoxylic Acid . Composition by G L C ..................................................................................................... I l a -70 (07) I l icnc Value o f D1.yi11g Oils ............................................................................................................................ I I;I -64 (07) Dicnoic Acids in Dehydrated Caslor O i l and Acids ...................................................................................... 1 la -04 (07) I ) i la~omc~r ic blctliod for Solid Fat Index ....................................................................................................... ('(1 10 -57 (07) I> i~ i l c r Acitls . Co~l l l los i~ ion by HPLC ............................................................................................................ 5 -0 I (07) Di1~ic1I1ylpolysiloxi111cs ill Fals :~nd Oils ........................................................................................................ I 24 -05 (07) ~ n w t h c r ~ i ~ ' ~ (heat tnunsfcr l lu id in fats and oils) by GLC ............................................................................ I 25 -0(1 (07) Dropping Point ............................................................................................................................................... C I X -SO ( 0 0 ) I)SC M c l ~ i n g Prol>crtics ol' Fats and Oils ...................................................................................................... ('. i I -04 (07) lipoxitlizccl I-a~ry M;llcrials ............................................................................................................................ ('tl 0 -57 (07)

.............. Iirucic Acid in High Iirucic Acitl Oils and Fk11s I>y Pnckcd Colunin G:ls-L-itl~~icl Chromatogra~, liy ( ' c 4 -05 (07) Erucic Acid in Oils and Fats .......................................................................................................................... c 4 -80 (05) 'I' Essential F i~t ty Acids ...................................................................................................................................... I 15 -7s (07)

................................................................................................................... Ehlcr SO3 in Fatly Alkyl Sulliltcs l)c 4 -50 (07) ................................................................................................ IYal St.lhili~y . Aclivc Oxygc~ l M c ~ h o d (AC)M) ('tl 12 -57 (07)

.......................................................................................................... I.'.II Sl.~hili ly . O i l Sl ;~I l i l i~y l~ l t lcx (OSI) ( ' ( 1 l21'-'12 (07) I;;ltty Acids

Ily Cilpillary G1.C. ................................................................................................................................... ( 'c lc -0 I (07) . . c.i.\ .. a ~ i d r,.c/irs I>o~licrs by GI-C .......................................................................................................... (.I. I L -80 (05) '

....................................................................................................... < 'o~l i l l i~ ic t I ;IS M i~ l c r ;~ l SO;IO~ ill F;tts (';I 4 -3 (07)

$11 1'1 l:\l!l I[( A l lNl)l N

Method Latest

nulrrl~rr isslle

C'on~posilion by GI-C ol' Methyl Estcrs .................................................................................................. c I -07 (97) Co~iilx)sitio~i of Mnl-inc Oils ................................................................................................................... Cc I h -89 (09) Cruilc (total I;~tty acids plus unsaponiliahlcs) ......................................................................................... I 5h -71 (97) n-3 and n-0 hy Capillary GLC Cc Id -91 (03) :Ic

\ ................................................................................................................

Oxit l i~ci l in Soill) Slocks ......................................................................................................................... G 3 -53 (07) . . . Scpur;~tio~i ol I . ~c lu~ i l nil Soliil ............................................................................................................... ('(1 0 -38 (80) :I: ' l i )~al in Coconut and Sirnili~r Soap Stock ............................................................................................... C; 4 -40 (07) Toti11 in Fats or Hydrolyzed Fats ............................................................................................................. C 5h -71 (07) Total in Soap Stocks Other Than Coconut .............................................................................................. G 3 -53 (97) rr.(rrrs Co~ilpositio~i of Partially Hydrogcnatcd Oils hy GLC-IR ............................................................ Cd l4h-93 (05) *: I I .YIII.\ I:atty Acids in Oils and Fats hy Capillary GI, C ............................................................................. C I f -00 (07) I I ~ I I I . ~ Iialty Aciils (isolated) hy 14TIR ...................................................................................................... Cil I4 -05 (00) I I . I I I I . ~ \=ally Acids by Silver-Ion Excha~igc HPLC .................................................................................. Cc l g -00 (97)

Fatty M i ~ ~ t c r in Soaps ..................................................................................................................................... D 10 -48 (97) Fihcr (crude)

in Gr i~ i~ ls . Meals . Flours . Feeds ........................................................................................................... I 0 -84 (07) in Soya Flours ......................................................................................................................................... B 0 -49 (97)

Fitelson Tcsl for Teiisced Oil ....................................................................................................................... C 3 -39 (07) Flash Point

Clcvcland Open Cup Method for Fats and Oils .............................................................................................................................. c Yn -48 (97) Ibr Fatly Acids and Drying Oils ...................... ., ............................................................................. T la -64 (97)

Pensby-Martens Closed Cup Method for Fats and Oils ..................................................................................................................... C Yh -55 (97) for Fatty Quaternary Ammonium Chlorides ................................................................................... T I 2a -86 (97)

Flashpoint hy Pensky-Martcns Closed Cup Flash Tester ............................................................................... C Oc -95 (97) Flavor

Correlation of Volatiles with Flavor ....................................................................................................... C I -83 (97) Panel Evaluatio~i o f Vegetable Oils ......................................................................................................... Cp 2 -83 (97)

Flow Test ........................................................................................................................................................ C 5 -25 (89) :%

Forcig~i Fats in Pork Fat and Lard C 5 -40 (93) 'k - ................................................................................................................. Foreign Matter in Cottonseed ....................................................................................................................... A 7 -38 (07) Free Acid or Frce Alkali

in Soda Soap ........................................................................................................................................... D 4u -48 (97) in Soda Soap Containing Synthetic Dctcrgcnt ........................................................................................ D 3 -48 (97)

Frce Fatty Acids in Castor Bcnns ............................ ... ................................................................................................. A 4 -52 (07) in Cottonseed ......................................................................................................................................... ALI (3 -38 (c)O) in Crude and Retined Fats and Oils ........................................................................................................ C;I 5a -40 (97) in P~;IIILIIS (grou~~dnuts) ....................................................................................................................... Ab 5 -49 (97) in Soybeans ............................................................................................................................................. A 5 -4 1 (97)

Fumonisins B, and B, in Corn hy LC ........................................................................................................... A 5 -93 (07) in Corn by I, C ......................................................................................................................................... A i 5i1 -97 (07)

.............................................................................................................................. Glucosinolntcs (rapeseed) A k I -92 (97) Glycerin . Total itlid Organic Residue ...................................................................................................... a 3 -58 (73) : Glycerine . Free . by HPLCILLSD ................................................................................................................................. I I4h -96 (97) Glycerol by Periodate Method

in Fnts and Oils ....................................................................................................................................... I I4 -56 (97) in Glycerin ............................................................................................................................................ li:~ 0 -04 (07) in Soup and Soap Products (free) ............................................................................................................ I 23 -56 (97)

Gossy pol . Free in Cottonseed Products ........................................................................................................ Ba 7 -58 (99) Gossypol . Free . Rapid Method ............................................................................................................................... I 7h -96 (99) Gossypol hy HPLC ........................................................................................................................................ a Xa -99 (99) Gossy pol . Total

in Cottonseed Products ........................................................................................................................... Ba 8 -78 (97) .............................................................................................. in Crudc Cottonseed Oil and Soap Stocks I 13 -56 (97)

Hnlplicn Test li)r Dctccting Cottonseed Oil ................................................................................................... I 1 -75 (07) tlcxanc

. .................................................................................................................... ('o~il~ilcrcial Spcciliciltions I I I0 -50 (07) ....................................................................................................................... Frcc in Extructcd Meals I 3 -X7 (07)

i~isoluhlcs in Lecithin ............................................................................................................................. J i 3 -87 (07) Kcsiducs in Fats ;lnd Oils ........................................................................................................................ I 3h -87 ( 0 0 )

......................................................................................................................... Total in Extracted Mc;tls Hi1 I4 -37 (07) I lyil~.oc;~rl~ons

Mincr;il Oil in 'Triglyccridcs .............................................................................................................. I (lc -05 (07) ........................................................................................................ Volatile in Soap and Soap Products I lu 26 -42 (07)

.............................................................................................. Slcroidal Hydrocarbons in Vegetable Oils C 27 -00 (07)

I-lydrogc~i;~tion Catalyst . . Activity ................................................................................................................................................... I / . l a -7s (07) Sclcctivity ............................................................................................................................................... . I I) -70 (07)

tlydroxy l Vnluc of Epoxidized Oils .................................................................................................................................. Tx \;I -00 (07) of Fats and Oils (acctyl valuc) .............................................................................................................. C 4 -40 ( 0 0 ) ol' Fatty Oils and Alcohols ...................................................................................................................... I 13 -00 (07)

Inorgil~iic Salts ............................................................................................................................................... 0 -44 (07) I~isoluble Impurities

in Fats and Oils ....................................................................................................................................... I 3a -40 (07) in Lecithin (hcxanc insoluhlcs) ................................................................................................................ l a 3 -87 (07)

Intcrnationnl Trade Methods .......................................................................................................................... I 5 -03 (07) lodinc Vr~luc

Calculated fro111 GLC ............................................................................................................................. C Ic -85 (07) Cyclohcxnnc Method ............................................................................................................................. I 1 h -87 (07) Cyclohcxanc-Acetic Acid Mcthod ......................................................................................................... ('11 I tl -02 ( 0 7 ) ol' Drying Oils ......................................................................................................................................... g I -04 (07) ol' Fats and Oils ....................................................................................................................................... I I -75 (03 :I:

ol' f2;1tty Acids ......................................................................................................................................... T la -04 (07) 01' Fatty Amincs . Dial~lincs and Anlidoanlines ....................................................................................... I 'g ?:I -04 (07) ol' Fatty Quaternary Ammonium Chlorides ............................................................................................ TF 3;1 -04 (07) oI' I.ccitlii~i ............................................................................................................................................... l i ~ 1.4 -0 I (07) ol' Soap and Soi~p Products ..................................................................................................................... I I5 -4X (07)

Iron . l'rocc Anioi~~its in Oils I, y AAS ................................................................................................................................................... I 15 -75 (07) hy AAS with Graphite Furnace .............................................................................................................. I I X -70 (07)

Isopropyl Alcohol . Spccilications .................................................................................................................. I I I S -5X (07) lo. jol~il Oil

Aciil Valuc .............................................................................................................................................. i 4 -0 I (07) Detection ol' Triglyccridc Adulteration ................................................................................................... Ci 2 -0 I (07) Mctliods I'or Ilctcrminatio~i of Quality and Purity .................................................................................. Vi I -0 I (07)

Kcrncl Content of Tung Fruit ....................................................................................................................... A 4 -57 (07) Kirschncr V;lluc l i)r 13utyric Acid in Ruttcrl'itt anil Coconut Oils ................................................................. I 5 -40 (07) I.aril . I;orcign Fat Contclit .............................................................................................................................. I 5 -40 ( 0 3 ) 'I' L, cad ill Oils hy Grnpliitc Furn;~cc .................................................................................................................. Cii l8c -01 (07) I,cc.itliin Co-Products Analyses ...................................................................................................................... J i l I:! -SO (07) 1, int Rcsiduc in Cottonseed ............................................................................................................................ Aa 7 -55 (07)

............................................................................................................... l.icluid Fatty Acids in Fats and Oils I (J -38 (80) 'I' Mi~~igi~ncsc in Oils hy Graphite Furnace ........................................................................................................ C'n IS -70 (07) Mass per Unit Volume ("Lilcr Weight") in Air ol'Oils and Fats ................................................................... ('c IOc -05 (07) Melting Point

Capillary Tube Method ........................................................................................................................... Cc I -25 (07) Mcttlcr Dropping Point ........................................................................................................................... c IX -80 ( 0 0 ) Slip Melting Point . AOCS Stiindard ....................................................................................................... V 3 -2.5 (07) Slip Melting Point . IS0 Standard ........................................................................................................... Cc 311 -02 (07) Wilcy Method ......................................................................................................................................... C 2 -3s ( 0 I ) 'I'

Melting P~.opcrtics of Fats and Oils by DSC ................................................................................................. <...I I -04 (07) Metals . T ~ x c

AI I l IAI5I I I ( A l IN1 )I S

Mclliud Lalcsl

numl)rr issue

by A A S I'or ('I .. Cu . I-c . N i i n Oi ls .......................................................................................................... (';I I 5 -75 (07) by A A S wi th Graphite Furnace lo r C r . Cu . Fc . N i . M n in Oil5 .............................................................. (';I I 8 -70 (07) by S p c c ~ r o ~ ~ l i o ~ o ~ i i c t r y li)r Copper .......................................................................................................... I 3 I -58 (07)

Mct l iy l Alcohol . Spccilic;~tions ...................................................................................................................... I 17 -58 (97) w

Mcthyl Esters Preparation .............................................................................................................................. Cc 3 -00 (07) Mineral O i l i n Triglyccridcs .......................................................................................................................... I Oc -65 (07) M i sc i h i l i ~ y ol' Oils . Cr is~ i i c r Tcst ................................................................................................................... C 4 -35 (07) MO~SIUIP ;111d VoI;llilc M i ~ t t c r . by A i r Ovcn

i n Cns~or Beans ....................................................................................................................................... A 3, -52 (97) in Castor Pomace .................................................................................................................................... I 1 -52 (07) i n Cot~onsccd .......................................................................................................................................... A 3 -38 (07) i n Fats and Oi ls (except c o c o ~ i u ~ and drying oi ls) .................................................................................. I 2c -25 (07) i n Flaxseed .............................................................................................................................................. A 2 -54 (97) :I: i n Oilsccd Mc.11~ . Meal . Cakc and Pcllcts .............................................................................................. I 2h -82 (07) in Oilscctl Protein Conccntrn~cs .............................................................................................................. 13e 2;1 -38 (07) in I'c;lnuIs (groundnu~s) ........................................................................................................................ A 2 -40 (07) in Soap :lnd Soap Producls ..................................................................................................................... I);I 2i1 -4% (07) ill Soill' and Soap Produels Conlaining Synthetic Dclcrgcnts ................................................................ I I -48 (07)

......................................................................................................................................... in Soya Flours c 2 -40 (07) in Soy hc;111s ............................................................................................................................................. Ac 7- -4 I (07) ill Su~i l ' lowcr Scctl ................................................................................................................................... A 2 -75 (07) in T L I I ~ ~ t:ruil (hulls and I ' rui~ plus Iiulls) ................................................................................................. A 3- -52 (97)

Moislul-c and Volatile Mntlc I-. by Forccd Dral i Ovcl i i n Oilsccd Cnkc . Mcnl . Mc.11~ . Pcllcls ..................... i , ............................................................................. I 2a -38 (97)

Moislurc ;uid Volalilc M.111cr . by Hot Plalc Mc lhod Bul lcr . Fats . Mi~rgarincs . Oils ................................................................................................................ I 311 -38 (07) Ii;ltly Acitls ............................................................................................................................................. I I;I -04 (07) Mod i l i cd Moisture and Vola~i lcs ............................................................................................................ (';I 21' -03 (07)

Mo i s~u rc ;lnd Vo lo~ i l c Mal lcr . by V:~cuu~i i O v c ~ i in Fois and Oils (except coco~ iu t ) ........................................................................................................... I 2d -35 (07)

.................................................................................................... i n Oilsccd Cukc . Mcnl . Mc.11s. Pcllcts I 21) -83 (07) M o i s ~ i ~ ~ . c . hy I> is~i l l ;~ l ion M c ~ l i o d

....................................................................................................... ill A l ky l hc~ i zc~ i c Sull'o~i;~lc I'roducls l)tl 21 -50 (07 in Fats and Oils ....................................................................................................................................... I 2a -45 (07)

............................................................................................................... in Fatly A lky l S u l l i ~ ~ c Products c 3 -50 (97) in L c c i ~ l i i n ............................................................................................................................................... I 2a -40 (07) in So:lp and So;~p Products ..................................................................................................................... I 21' -42 (97) in Sull'onn~cd and Su l l i~ lcd Oils .............................................................................................................. I; l a -44 (07)

Mo i s~u rc . hy Kar l Fisclicr Method in Alky lhc~lzcnc Sul lhnu~c Produc~s ....................................................................................................... d 3h -50 (89) in F ; I ~ and Oils ....................................................................................................................................... I 2c -84 (07) ill F:III~ Nitrogcn Compounds ................................................................................................................ T b 21 -04 (81)) 'I'

i n Glyccrin .............................................................................................................................................. L~ X -58 (07) ill Indus~riul Oi ls olitl Dcriv;~livcs ........................................................................................................... T 2 -64 (05) 'I' i n Lcc i~ l i i n ............................................................................................................................................... Ja 2h -87 (07)

..................................................... Molcculnr Wcighl (average) ol' Fi111y Qualcrnary Ammon iu~ i i Chlorides T v I u -hJ (07) ................................................................................................... Mono- i111tl Diglyccridcs by Capill i iry G L C Ctl I l h - 0 I (07)

............................................................................................................. Mono- a~icl Diglyccridcs by HPLC-ELSD ('tl I It1 -00 ( 0 0 ) ...................................................................... Mono- . I l i - and Triglyccridcs by Silica Gel Chromntography ('tl I l c - 03 (07)

or-Monoglyccridcs .......................................................................................................................................... I I I -57 (00) .............................................................................................................................. Near I~i l ' r ;~rcd Kcl'lccloncc A I -02 ( 0 0 )

Ncucrnl O i l .............................................................................. in Alky lbcnzc~ic Sul(i)n;llcs (~~ns i r l l ' ona~cd material) I)(! 4 (07)

............................................................................................... ill Neutral O i l ;111d Loss I'or Fills i l l id Oi ls (':I 01' -57 ( 0 0 ) ill Soap Slack (uns;rpo~iilinhIc mn~cri;l l) ................................................................................................ G 5 -40 (07)

Nitrogc~i-Ani~i i~~~i i ;~-P~'olci~i ................................................................................................................................... Co~ i vc r s i o~ i Tilhlc A;I 5 -0 I (07)

......................................................................................................................... . ('oppc~ S11ll';llc Ca1;ll yst I 41) -87 (00) :'

Copper Sull'rl~c Plus T i ta~ l iu~ l l Dioxide C;~talys~ ..................................................................................... l3;1 Jtl -00 ( 0 0 ) i l l Cotto~lscccl .......................................................................................................................................... A 5 -38 (SO) :I:

i l l Cotro~lsccd ......................................................................................................................................... A 5 -0 l (07) i l l Oilsccds . Meats . Meal . Cake and Pcllcts .......................................................................................... 4 ; 1 -3X ( X O j

in Pc;~nuts (groi~nd~iuts) .......................................................................................................................... A 4 -50 ( X O ) :I:

in Pc;~liuts (groi~nd~iuts) .......................................................................................................................... A 4 -01 (07) in Soya Flours ......................................................................................................................................... I J -49 (80) in Soya Flours ......................................................................................................................................... c 4 -01 (07) in Soybeans ............................................................................................................................................. A 4 -41 ( X O ) in Soybcnns ............................................................................................................................................. A J -0 I (07) in Sunllowcr Sccds ................................................................................................................................ A 4 -75 ( X O ) 'I:

in Sunilowcr Sccds ................................................................................................................................. A J -0 I (07) .............................................................................................................................. Kjcl-Foss Automatic I 4c -X7 ( X O ) 'I:

........................................................................................ Nitrogen Solubility Index (soybean products) B ~ I I I -05 (07) ................................................................................................... Non;~niincs in FT;1tty A~ i i i~ i cs ;111d Di:~~iiincs ' 1;) -04 (07)

Nonvola~ilcs (solids) . by I4ot Pl;~tc Mc~l iot l 1.0 r Drying Oils (solutions) ...................................................................................................................... ' I l a -04 (07)

.................................................................................................... for Quaternary Amnioniu~ii Chlorides T ?a -04 (07) Oil Content

....................................................................................................................................... in Castor Beans A 3 -52 (07) .................................................................................................................................... in Castor Po~nncc I 3 -52 (07)

in Linters (cottonseed hulls) .................................................................................................................. I 7 -3X (07) i l l Oilsccd Mcnts . Cakc and Mcal ........................................................................................................... 3 -3X (07) ill Oilsccds (I;OSI:A Method) ................................................................................................................. A 3, -03 (07) in Oilsccds: Supcrcritic;~l Fluid Exlraction Mctliod .............................................................................. A 3 -00 (07) in Peanuts (groundnuts). Raw or Roasted ............................................................................................... Ah 3 -40 (07) in Ropcsccd ;uid otlicr oilsccds by NMR ................................................................................................ Ah3 -04(00) in Salllowcr Sccd ................................................................................................................................... A I -05 (07) inSoyaFloi~rs ......................................................................................................................................... I 3 3 -40(07) in Soybcans ............................................................................................................................................. Ac 3 -44 (07) in Sunllowcr Seed or Dehulled Kcr~iels .................................................................................................. A 3 -75 (05) 'I: in Tu~ ig Fruit . Hulled .............................................................................................................................. Ad 0 -52 (07 j in Tung Fruit . Kcrncls ............................................................................................................................. A 5 -52 (07) in Tulig Fruit . Whole .............................................................................................................................. A 3 -53- (07)

Olive Oil Chlorophyll Pigments ............................................................................................................................ I J -0 I (07) Fatty Acids by Capillary GLC ................................................................................................................ <'I1 7, -0 I (07) /t.rrtr.v Unsaturated Fatty Acids by C;~pillary Colunin GC ....................................................................... CIl 3-;I -04 ( 0 0 ) . . Fotry Acids in 2-Pos~t~on ........................................................................................................................ CII 3 -0 I (07) Preparation ol' Methyl Esters ................................................................................................................... I I -0 I (07) Spccilic Exliiiction .................................................................................................................................. I 5 -9 I (97) Stcrol Fraction by TLC and Capillary GLC .......................................................................................... I h -0 I (07) International Trade Standards ................................................................................................................. ('11 7 -04 (97)

Organic Residue in Glycerin .......................................................................................................................... 3 -5X ( 7 1 ) 'I: Ovcns

Air . Spccificalions ................................................................................................................................... I1 3 -45 (07) ................................................................................................................... Fo~.ccd Dri~I't . Spccilicntions I I I -30 (07)

........................................................................................................................... Vacuum. Specifications I l J -45 (07) ........ ......................................... Oxidizctl Farry Acids in Soap Stocks ...... ........................................ 3 -53 (07)

...................................................................................................... Oxiranc Oxygen ill El, oxitlizcd M.~tc~.ials ('(1 0 -57 (07) Peroxide Vi~luc

of Lecithin ................................................................................................................................................ l a X -87 (07) Using C1ilorofo1.m ................................................................................................................................... <'LI X -53 (07) Usilig Isooctonc ..................................................................................................................................... ('(1 Sl> -00 (07)

I'csticidcs in Oils and Fats ............................................................................................................................. ('(1 2.3 -03 (071

Al.1'1 l~\l$l I I( A1 ININ h

Method Lat rs l

~~un l l~ r r issur

Pctrolcum IJ~licr . Sl~ccil'ications ..................................................................................................................... I I 1 -4 I (07) pt l

ol' Acid~ll;~tcd Soapstocks ....................................................................................................................... G 7 -56 (97) ol' Farty Quatcr~i;~ry Aliinioniu~n Chlorides ............................................................................................ Tu la -64 (07) f'liosph;~tcs ill Soap and Soap Producls (gr;rviliictric nlctliod) ............................................................... I>;I ?();I-JX (07) Pliospl~nlcs ill Soap nnil Soap Producls (ti1rin1ctl.i~ ~nctliod) .................................................................. l>a 7Oh-57 (07)

Pliospliol ipids in I . ccitliin Conccntratca hy HPLC .......................................................................................................... .I .I 7h -0 I (07) ill L. ecitliin Concc~itratcs hy . 1-LC ........................................................................................................... I 7 1 -86 (97) ill Vcgctablc Oil ...................................................................................................................................... I 11) -86 (07)

Pliospliort~s . Atomic Al>sorption Spectroscopy ............................................................................................. I 121,- 97 (97) l'llos~>llo~lls

ill I, ccit l i i~i (total) .................................................................................................................................... I 5 -55 (80) :I:

i l l Oils ...................................................................................................................................................... I 12 -55 (97) in Oil hy ICP-OES .................................................................................................................................. I 20 -90 (09)

Photoliictric Inilcx (colol.) ol' Co~ii~iicrcial Fatty Acids ................................................................................. l‘tl 2a -04 (07) Physic;ll Allillysix

Polcllhkc V;1luc ........................................................................................................................................ Cd 5 -40 (97) Twig IYruit (kcr~icl content) ..................................................................................................................... Ad 4 -52 (97)

Polar Compounds in Frying Fats ................................................................................................................... C 70 -9 1 (97) Polyctliylc~ie in Fats and Oils ........................................................................................................................ Co 16 -75 (07) Polymc~.izcd Triglyccridcs hy Gel-Pcrnieation HPLC ................................................................................... Cd 22 -0 I (07) Polyunsaturntcd Acids

c.1.v. c i . v Essential Fatty Acids (enzymatic) .............................................................................................. d 1.5 -78 (97) Co~nmercial Fatty Acids . Spcctrophotometric Method .......................................................................... T la -64 (93) * in Fats and Oils ....................................................................................................................................... C 7 -58 (97)

Potassium Carho~ialc in Potash Soaps ........................................................................................................... f l u 5 -44 (97) Potassium Oxidc in So;~p and Soap Products ................................................................................................ I 27 -48 (97) Precision of Analytical Methods .................................................................................................................... M I -02 (07) Protein Contcnt

hy Co~nhuslion Ha 4c -93 (99) - ........................................................................................................................................ Conversion T;lhlc ................................................................................................................................... A 5 -0 I (07) in Cot~onsccd ......................................................................................................................................... A 5 -9 I (07) - in Oilsced Mcats . Meal . Cake and Pellets .............................................................................................. I Ja -38 (89) 'I' in Pea~~uts (groundnuls) ......................................................................................................................... A 4 -9 I (97) in soy:^ Flours .......................................................................................................................................... 13c 4 -01 (97) in Soyl>cans ............................................................................................................................................. Ac 4 -0 I (07) Protein Ilispcrsibility l~idcx (PDI) (soybean products) .......................................................................... I ~ I 10 -05 (09)

............................................................................................................................... in Sunllower Secds A 4 -0 I (07) Kjcl-Foss Auto~natic Method ................................................................................................................. I 4c -87 (80) with Copper Sulhtc Catalyst .................................................................................................................. I 4h -87 (90) 'I: with Copper Sull'atc Plus T i~n~i iun i Dioxide Cnt;ilyst ............................................................................. Ha 4d -00 (l)l))

l i c c o ~ ~ ~ ~ i ~ c n d c i l Pr;~cticcs Ibr l'csting ol' Co~ii~iicrcial Fatty Acids ..................................................................................................................... S I -04 (97) of Drying Oils ......................................................................................................................................... S 2 -04 (97) ol' Epoxidizcd Oils .................................................................................................................................. S 3 -04 (97) of Fatty Atnidoaniincs ............................................................................................................................ S 4b -64 (97) ol' I:;llty A~n i~ ics ...................................................................................................................................... S 4;1 -04 (07) 01' \:ally I) i;~~ii i~ics ................................................................................................................................... S 411 -04 (07) of I-atty Quaternary Ammonium Chlorides .......................................................................................... S 4c -64 (07) of Fced-Gradc Fat Produc~s .................................................................................................................... C I -08 (97) ol' Poly~iierized Fatty Acids .................................................................................................................... S 5 -64 (97)

......................................................................... Rcl'incd and Blcachcd Color (t:~llow and greases Ihrsoaps) Cc Xd -55 (07) licl'ini~ig 1, oss

Dcguninicd . Expeller Soyhcan Oil ......................................................................................................... Cn Oa -52 (07) ................................................................................ Dcgu~iinicd . Hydraulic and Exlractcd Soyhcan Oil I 9n -52 (97)

Ext~.actcd and Reconstituted Prepressed Co~tonsccd Oils .................................................................... I Oa -52 (07) Extrac~cd Soybean Oil ............................................................................................................................ C 9a -5-7 (97) Vcgct;~hlc Oils . Crildc ............................................................................................................................. C ~ I O;I -52 (07)

Kefrnctivc Index ............................................................................................................................................ Drying Oils T I I -04 (97)

r Fats and Oils ........................................................................................................................................... C 7 -25 (07) Fatty Acids . Commercial ........................................................................................................................ T la -64 (97)

liciclicrt-Mcissl V a l ~ ~ c .................................................................................................................................. I 5 -40 (07) I i cs id~~a l 1, int in Co~tonsccds ......................................................................................................................... A 7 -55 (07) Kcsiduc . Total and Organic . in Glycerin ........................................................................................................ I 3 -58 (73) :I: Kheologicnl Instrument Calibration ............................................................................................................... C j 3 -00 (90) Rosin

in Soap ;lnd Soap Products .................................................................................................................... I 1 7 - -48 (90) in Soap Containi~ig Synthetic Detergents ............................................................................................... I I I -48 (07)

. . liosin Acids in Fatty Acids ............................................................................................................................ I s I ;I -64 (07) Sa~iipling

ol' Alkylbcnzcnc Sulfonatcs .................................................................................................................... 1 1 -59 (07) ol' Cottonseed .......................................................................................................................................... A I -38 (07)

. . .................... ................................................................... 0 1 ( o~to~isc~c~t l I . i~ i tcr \ ;111(1 1 1 ~ 1 1 1 F ihc~ ... 131, I -3s (07) . . . . .

01 l ) ~ l ~ a \ ~ c /\citl\ ................................................................................................................................. I;I I' -70 (07) 01' I i l~oxi t l izcd Oils .................................................................................................................................. I I I, -64 (07) ol' Fats and Oils ....................................................................................................................................... C I -47 ( 0 0 ) ol' Fatty Acids. Co~iiniercial .................................................................................................................... TI In -64 (97) ol' Fatty Alky l Sull'ntcs ............................................................................................................................ I I -SO (07) 01' Fatty Nitrogen Products ...................................................................................................................... I Ic -64 (07) o f Flnxsccd .............................................................................................................................................. A I -54 (93) :"

.............................................................................................................................................. o f Glycerin I I -38 (07) o f Industrial Oils . Gcncml ...................................................................................................................... I I -04 (07)

. ..................................................................................................... ol' Oilsccd Slah . Cake, Pcllcts Meals I I -38 (07) . ............................................................................................... ol' I'canuts (grounrlnuts) . Wliolc Shcllcd A I -40 (07)

.................................................................................................................... ol' Po lymcr i~c t l E';ltty Acids 'I-;I I d -64 (07) ol' Soall ant1 Soap Products ..................................................................................................................... I I -45 (97) ol' Soall Stock .......................................................................................................................................... i I -40 (07) 01 . S0y:1 I:loul.h ........................................................................................................................................ I3c I -50 (07 1

............................................................................................................................................. 01' SOYI, ci111s I -1.5 (97) o f S~~nl ' lowcr Sccd ................................................................................................................................... t i I -SO (0.3) 'I' o fTung Fruit ........................................................................................................................................... Ad I -48 (07)

Saponil'ication Color Rclinctl :uid Bleached ............................................................................................................................. Cc 1.31' -04 (07) I~ l ig l i Qualily Tallow, (:oconut Oils ........................................................................................................ ( 13s-04 (07) 'r:lIlow . Coconut Oils ............................................................................................................................. .C'c 1.311-04 (07)

Snponil'ication Value ol' Dcodorizcr Llistillatcs and SIudgcs .................................................................................................... Ccl 311 -76 (07) ol' D r y i ~ i g Oils ......................................................................................................................................... I 1;1 -64 (07) oI'F;~ts ;~ntl Oils ....................................................................................................................................... I 3 -25 (07) OI'I:;II\ ; ~ m l Oi l \ ( ( ' .~ lc~r~l .~~c. t l ) .......................................................................................................... .(*(I . 3.1 -0.1 (0.1) ( 1 1 I;;IIS ; I I I ~ Oi l \ . hlo(liI ' ic~I l l \ ing Met l~ ;~~ io l ........................................................................................... . k. -0 I (0~1 1

.................................................................................................................... ol' F;ltty Acitls . Comnicrcinl TI I ;I -04 (07) o f Soap iuid Soup Products ..................................................................................................................... I I h -48 (07)

............................................................................................... of Soap Containing Synthetic Detergents I X -4% (07) Scrccll 7i.sl

.......................................................................................................................................... So;q) I'ow~lc~.s I):\ 28 -30 (07) ............................................................................................................................................. Soya Flours I 7 -5 I (07)

.......................................................................................................... Sclcctivity o f Hydrogenation Catalysts T i I b -70 (97) ....................................................................................... Scsamc Oi l Dctcction, Modified Villavecchia Tcst C 7- -40 (97)

Simultnncous Dctcrniinntion o f O i l and Moisture ................................ Contc~its 01' Oilhccds Using Pulsed Nuclear M;~gnctic I<cao~iancc Spectroscopy Ak 4 -05 ( 0 0 )

Slip Melting Point . ISO Sta11d;u.d .................................................................................................................. c 311 -03 (07) Slip Point

Hard Fats (palm oi l) ................................................................................................................................ c 3 -25 iY7) .................................................................................................................................................. Sol'tFats 4 -?5(80) 'I'

ALI'I l r l l i l 1 I( A l INI)I X

Method Latest

numl)er issue

Sm:~llcy Slatistical Kcsulls . 1085-1986 ......................................................................................................... li 4 -89 (07) Sniolic . Flash and F i x Poinl; Clcvcland Opcn Cup Mctliod ......................................................................... c Oa -48 (07) Soap in Oil -

by Conductivily Mcthod ......................................................................................................................... C 15 -60 (80) * Ily . rilri~iiclric Mclhod ............................................................................................................................. C 17 -05 (07)

Sodium Alliy lbcnzcnc Sullijna~e by Ullraviolc~ Absorption ......................................................................... l)d 3 -00 (97) Sodium and Cnlciurn by AAS ........................................................................................................................ I 15h-87 (97) Sodium Chloride in Glycerin ......................................................................................................................... I 2 -38 (73) * Sodium Oxide in Soap and Soap Products .................................................................................................... I 27 -48 (97) Sodium Sull':~lc in Folly Alkyl Sulfates .......................................................................................................... c 7 -59 (07) Soflcni~ig Point (slip poinl ol'hard fats) ......................................................................................................... C 3 -25 (97) Solid Fnl Conlenl (SFC) by Magnetic Resonance ......................................................................................... Cd IOh-99 (90) Solid Fat Conlcnl (SFC) by Nuclear Magnetic Resonance ........................................................................... C 16 -8 1 (99) Solid Fa1 Indcx (SF!) o f Fats and Oils ........................................................................................................... C 10 -57 (97) Solid Fatty Acids in Fats ;lnd Oils ................................................................................................................. 6 -38 (80) :k

Soluhlc Mintrill Mntlcr and Fn11y Acids Combincd as Mineral Soi11j ........................................................... I 4 -25 (07) Spccilications ................................................................................................................................................. S Scclion H Spccilic Gravity

Drying Oils ............................................................................................................................................. To I h -64 (97) Fatly Acids . Commercial .................................................................................................................... To I;\ -(A (97)

.................................................................................................................................................. Glyccrin 7 -95 (07) Liquid Oils and Fats .............................................................................................................................. Cc I(kt -25 (05) 'I' Solid Fats and Waxes ................................... ........................................................................................... Cc IOb-25 (97)

Stability and Quality of Fats and Oils (recommended pr+(ices) .................................................................. Cg 3 -91 (07) Ovcn Storage Test for Accelerated Aging of Oils .................................................................................. C 5 -97 (97)

Stability ol' Fats and Oils . Active Oxygen Method (AOM) ........................................................................... d 12 -57 (03) :I: Slandnrtl Solutions

............................................................................................................. Alcoholic Potassium Hydroxide I 15 -53 (07) Hydrochloric Acid .................................................................................................................................. H 14 -52 (97) Sodium Hydroxide .................................................................................................................................. H 12 -52 (97) Sulfuric Acid ......................................................................................................................................... H 13 -52 (07)

Starch in Soap and Soap Products ................................................................................................................. l la 25 -48 (97) Statistical Rcsults . Smalley . 1985-1986 ........................................................................................................ I 4 -80 (07) Sterols in Soya Residues hy GLC .................................................................................................................. C 3 -74 (97) Stigmastndicnes in Vegetable Oils ................................................................................................................. C 2(1 -96 (97) Sugars in Soap and Soap Products ................................................................................................................. Dn 24 -48 (99) Sulfates in Soap and Soap Products .............................................................................................................. I 22 -48 (97) Sulfur in Olive Oil

by Coin Test ......................................................................................................................................... I Xn -35 (00) :': by Silver Benzoate Test ......................................................................................................................... I 811 -35 (90) '"

Sulfuric Anhydride in Sulfonated and Sulfated Oils by Ash Gravimetric Method ................................................................................................................... F 7-c -44 (07) by Extraction Titration Mcthod .............................................................................................................. 2 h -44 (97) hy Titra~ion Method ................................................................................................................................ F 2a -44 (97)

Surplus Status of Methods ............................................................................................................................. M 3 -83 (97) Teasced Oil Detection . Fitelson Test .............................................................................................................. C 3 -39 (97) Tetrasodium Pyrophosphate ........................................................................................................................... Da 3 I -48 (07) Tlicnnomctcrs . Spccilications ....................................................................................................................... t 5 -40 (07) 2-Thiohnrbituric Acid (TBA) Value ............................................................................................................... Cd I9 -90 (07) Thiocynnogcn Valuc ....................................................................................................................................... C 2 -38 (73) :I: Titcr test

for Fats and Oil ...................................................................................................................................... C 12 -59 (07) I'or I'atly Acids. Commercial .................................................................................................................. Tr l e 414 (07)

.................................................................................................................... for Soap and Soap Products I 13 -4X (07) for So;~p Stocks ....................................................................................................................................... G h -40 (97)

Tocopherols in Deodorizer Distillates . Total ............................................................................................................... c 7 -87 (97) in I.cci11iin Conccnlrntcs by HPLC ......................................................................................................... I 13 -9 I (07)

M(.lliocl L.il~~*l ~~u~iil) 'r i>>u c.

in Soya Slurlgc and I<c\irlucs hy G I X .................................................................................................... (-c 3 -74 (07) ill Vcycl;1l3lc Oils ;111rl f i l s I3y HI'I ............................................................. ('1% S -SO (07)

~l i ) lucnc . Inrlusl~.i.~l. Spccilicatio~is .......... .......... ............................................................................................ I I I0 -58 (07) -1iIt;ll ly:llly !\~i<l\

ill ('oc.011~1l Oi l ;111tl 1';1I1ii Oi l So;ll) StocA .............................................................................................. ( ; 4 4) (07) ill I-'a~s 01 . I lycl~.oly/.crl I:ats ...................................................................................................................... (';I 51) -7 I (07) ill So:~p Stocks Otlicr l'lian Coconut Oi l and Palm Oi l .......................................................................... Ci 3 -5.3 (07)

Trace Metals in Oils hy AAS (Cr . Cu . Fe . N i ) ......................................................................................................................... I 15 -75 (07) by Cirapliitc Fu~.ni~cc AAS (Cr . Cu . Fc . N i . M n ) ..................................................................................... I I X -70 (07) hy Gr:~pl~itc I;urnacc AAS I1i1'cct (Cu . Fc . N i ) ....................................................................................... (';I 1 x 1 3 - O l (07) by Grapl i i~c 1;urnacc AAS (lead only) .................................................................................................... C';I I Sc -0 I (07 j

l~ . rr t r . r and c.i .v.c. i .v ison~crs by G L C ................................................................................................................ r e l c -80 (05) 4: lr(1tr.v Co~npos i t io~ i ol' k~ r t i u l l y Hydrogenated Oils by GLC-IR .................................................................... Crl l4b-03 (05) * 11.(11r.v Isonicrs (isolatcrl) by FTlK ................................................................................................................... (-(I I 4 -05 (09) 1111rr.v Isonic~.s hy Cill>illa~'y GI, C .................................................................................................................... ( ' ( 1 l4c -04 ( 0 . 4 ) I:

11.tr11.v I\orncrs by Cilpillary GLC .................................................................................................................... I ?a -04 ( 0 0 ) Ilzr1r.v Iso~iicrs in Triglyccrirlcs by ATRIFTIR ............................................................................................................ ('(1 l4d -90 ( 0 0 ) l'riglyccridcs by GLC .................................................................................................................................. c 5 -86 (07) Triglyccridcs by HPLC .................................................................................................................................. c 5h -SO (07) Triglyccridcs (Inrlividual) by I~l l 'LC .............................................................................................................. c 5c . -02 (07) 'l'rylxiili I ~ ~ l i i b i t o r Activity in Soybean anrl CottonlSoyhc:~~~ I11.y l'roduc~\ ........................... LI 13 -75 (07) Tulig Fruit . Pliysical Analysis (kernel content) ............................................................................................. d 4 -53 (07) U~~s;~po~i i l iab lc Mnttcr

in I l ry ing Oils ......................................................................................................................................... k la -h4 (07) in Fats and Oils . Except Marine Oils ...................................................................................................... I ha -40 (07) in Fnrs nntl Oils, Including Marine Oils .................................................................................................. I 011 -52 (07) in I;;lts or Hydrolyzed Fnrs ...................................................................................................................... (';I 51) -7 I (07) in Fatty Acids . Commercial .................................................................................................................... k l a -04 (07) ill Fntty Acids . Polymerized ................................................................................................................... k la -h4 (07) in Soap :uid Soap Products ..................................................................................................................... [>a I I -42 ( 0 0 )

lJ~~s;~pori i l i i~blc Nonvolatile Mo~rcr in Sull'arcd Oils ...................................................................................... 1: 5 -44 (07) lJ~is;~ponilicrl I'lus Unsaponilii~blc Matter in Soap ;mil Soap l'roducts ......................................................... I>;\ 10 -47 (07) Unsul l 'a~cdM;~tcr ia l i~ iFat tyAlky lSul la lcs .................................................................................................. l > c S -50(07) IJrcasc Activity (soybean mc.rls . llours and mi l l I'ecd) .................................................................................. I 0 -5s (07) Villavccclii;~ Test {'or Scsnmc Oil. Modified .................................................................................................. ('1, 3 -40 (07) Viscosity

L11.yi1ig Oils . Bul, blc Tinic Method ......................................................................................................... 1 I ;I -04 (07) ................................................................................................................................ Lcc i th i~ l . Hrookliclrl J;I I 0 -87 (07)

Lecithin . Bubhlc 'rime Method ............................................................................................................... J;I I I -87 (07) Tr;uisparcnt I.icluitl\. Bubble T i ~ i i c Method ............................................................................................. 1:1 I I -87 (07)

Vol;llilc I I y t l ~ ~ o c ; ~ ~ ~ l ~ o ~ i \ i l l SO;II) a~ir l Soill) Prorluc.t\ .................................................................................... 1h 7 0 42 i1)1l Volatile\ (VOC.') ill I;;I~\ ;111tl Oil5 by G1.C ..................................................................................................... C's -4 . 04 ( l ) - 7 ) Water-Immiscible O~.g.~riic Solvcnts in Sulfonotcd and Sulf'ntcd Oils ........................................................... 1.' I 0 -44 (07) Wntcr-l~~solublc M;~rler

in Soap and So i~p Products ..................................................................................................................... I : 6 -48 (07) ............................................................................................... in So;lp Containing Synthetic Detergents 1% 4 -4s (07)

Wilcy Melt ing Po in~ Mctliorl ......................................................................................................................... C'c 3 -3s (01) 'I' Writing and Approval ol' Methods ................................................................................................................. M 3 -05 (07) X-Kay Ilil'l'raction Analysis o f Fi~ts ............................................................................................................... C. i 3 -05 (01)

......................................................................................................... Zcaralcnonc arid a-%c;~ralc~iol in Col-11 1. 7 -St1 (07)

ALI'HABETI('AL INDEX

Surplus Methods The nicthods listed in this section have been declared surplus (i.e.. obsolete) by the AOCS Uniform Methods Cornrnittce. The surplus methods have been or wil l be removed from Officiul Methods in the year stated; however. they are available upon rcquest from AOCS headquarters at the prevailing photocopying rate. i

Method number Topic Year removcd fro111 book

Modified Kjeldahl Method (cottonseed) Modified Kjeldahl Method (peanuts) Modified Kjeldahl Method (soybeans) Sampling (flaxseed) Moisture and Volatile Matter (flaxseed) Oil Content (flaxseed) Sampling (sunflower seed) Oil Content (sunflower seed) Modified Kjeldahl Method (sunflower) Modified Kjeldahl Method (oilseed meals) Modified Kjeldahl Method (copper sulfate) Kjel-Foss Automatic Method Nitrogen and Protein (soya flour) Beilstein Test Coin Test Silver Benzoate Test Break Test (soybean oil) Bomer Value Wiley Melting Point Slip Point (soft fats) Flow Test Specific Gravity of Oils and Liquid Fats Soap in Oil (Conductivity) Soap in Oil by Titrimetric Method Wijs Method for Iodine Value Thiocyanogen Valuc Liquid and Solid Fatty Acids Monoglycerides (Section I ) AOM for Oil Stability rrtrrrs Fatty Acids by FI'1R trtrris Fatty Acids by GLC traris Isomers in Partially Hydrogenated Oils by GLC-IR traru Isomers by Capillary GLC Fatty Acid Composition by GLC, cis. cis and traris lsomers n-3 and n-6 Fatty Acids by Capillary GLC Erucic acid by TLC Moditicd Karl Fischer (alkylbenzene sulfonates) Acidity (glycerol) Alkalinity (glycerol) Ash (glycerol) Sodium Chloride (glycerol) Total and Organic Residue Specific Gravity: Glycerin Total Phosphorus in Lecithin Precision of Analytical Methods Modified Karl Fischer, General Modified Karl Fischer, Fatty Nitrogen Products Polyunsaturated Acids. Ultraviolet Spectrophotometric Method

*This method wil l be removed when Section A is revised. ** This method, which uses mercuric oxide, was retained in the book for historical and reference purposes only.

Page 12 of 12