trc project number: 310725 environmental protection agency ... · massdep massachusetts contingency...

L2019-051

TRC Project Number: 310725 March 7, 2019 Ms. Shauna Little Environmental Protection Agency Office of Environmental Stewardship (OES) Water Technical Unit 5 Post Office Square, Suite 100 (OES4-SMR) Boston, MA 02109-3912

Re: Eagle Mill Basement Dewatering Project 73 West Center Street, Lee Massachusetts Notice of Intent (NOI) for Coverage under the Remediation General Permit (RGP) for Massachusetts Discharge of Treated Water to the Housatonic River, Lee, Massachusetts

Dear Ms. Little: On behalf of Eagle Mill Enterprises, Inc. and DEW Properties, LLC, TRC Environmental Corporation has prepared the attached National Pollutant Discharge Elimination System (NPDES) Notice of Intent (NOI) (Attachment A) for coverage under the Remediation General Permit (RGP). Project Background The Housatonic River has damaged the Eagle Mill building and flooded the basement with water from the river. The project involves the dewatering of the basement level of the Eagle Mill building at 73 West Center Street in Lee, Massachusetts. Since asbestos containing material is known to be present in the basement it is assumed that an EPA Dewatering General Permit is not viable and pumped water will need to be treated via physical filtration to remove asbestos fibers and discharged under an Environmental Protection Agency (EPA) Remediation General Permit (RGP). Between 1 million and 2.5 million gallons of water is anticipated to require removal from the basement. A Site Plan and a Massachusetts Department of Environmental Protection (MassDEP) Priority Resources Map are provided as Figures 1 and 2 in Attachment B, respectively. Dewatering, treatment, and discharge of treated water from the basement is expected to begin upon issuance of a permit.

MassDEP Massachusetts Contingency Plan (MCP) Disposal Site Release Tracking Number (RTN) 1-20494 has been assigned to the parcel in March 2018 for the detection of volatile petroleum hydrocarbon fractions, lead, and 1,4-dichlorobenzene in soil. The source of the water in the basement is believed to be from the Housatonic River, and therefore, not considered an MCP Remediation Waste. As such, this RTN is not referenced in section A.5 of the Notice of Intent form.

March 7, 2019

L2019-051

Water Characterization To characterize water in the basement, a sample of water was collected on February 14, 2019. The water sample was submitted to Alpha Analytical of Westborough, Massachusetts for laboratory analysis of EPA RGP parameters. A summary of water sampling results and the supporting laboratory analytical reports are provided as Table 1 in Attachment C and Attachment D, respectively. Laboratory analytical results were compared to the RGP Technology Based Effluent Limitations (TBELs) and Water Quality Based Effluent Limitations (WQBELs). The WQBELs were calculated in accordance with Appendix V of the RGP, for sites in Massachusetts discharging to freshwater surface water bodies. The water was characterized for pH and temperature on February 28, 2019 using a hand-held water-quality meter. In addition to the typical water analysis for RGP characterization, one sample (BSMT-F5) was filtered through a 5-micron filter in the field and another sample (BSMT-F 0.45) was filtered through a 0.45-micron filter. The purpose of this sampling and analysis is to evaluate the treatment performance of 5 micron and 1-micron bag filters. Constituents of concern identified in the water samples is asbestos. Receiving Water Classification The Housatonic River is listed on the Massachusetts 303(d) list as an impaired water body for the following constituents:

• PCB in Fish Tissue; • Zebra Mussel (Dreissena polymorph); • Excess Algal Growth; • PCBs; and, • Phosphorus (Total).

On February 14, 2019, TRC personnel collected a surface water sample in the Housatonic River from the approximate location of the proposed discharge point and submitted it for laboratory analysis of RGP metals, ammonia, and hardness. Surface water sampling results are summarized in Table 2 in Attachment C and the supporting laboratory analytical report is included in Attachment D. The surface water was characterized for pH and temperature on February 28, 2019 using a hand-held water-quality meter. Discharge of treated effluent from the dewatering treatment system will be in compliance with the effluent limitations contained in the RGP. A dilution factor of 17.9 was utilized based on a 7Q10 low flow rate of 22.6 cubic feet per second (cfs) [i.e., 14.6 million gallons per day (MGD)] for Housatonic River (as determined by a US Geological Survey StreamStats Database – see Attachment E) and the proposed discharge rate of 275 gpm (0.396 GPM). The dilution factor has been verified by MassDEP (a copy of the MassDEP confirmation is included in Attachment E). The 7Q10 value was calculated using the United States Geologic Survey’s StreamStats online application, and the dilution factor was calculated as instructed by the Dilution Factor and Effluent Limitation Calculations for Massachusetts, Appendix V of the RGP. Treatment Systems The water removed from the basement will be treated via physical filtration (e.g. bag filters) before being discharged directly to the Housatonic River. Given the simplicity of the treatment system it is assumed a process and instrumentation diagram is not necessary. A Design Flow treatment system discharge rate of 275 GPM (i.e. 0.396 MGD) was used to evaluate the applicable RGP discharge standards. Five-micron bag filters have been determined practical for removal of asbestos fibers from water based on previous experience.

March 7, 2019

L2019-501

A Best Management Practices Plan (BMPP) for the water extraction and treatment systems satisfying the requirements of Section 2.5 of the RGP will be available at the Site prior to initiating dewatering activities. Owner and Operator

Owner Operator Eagle Mill Enterprises, Inc. Fabino & Libardi Construction Services Eagle Mill Redevelopment 49 Holmes Road Street PO Box 777 Lennox, MA 01240 South Egremont, MA 01258

Notice of Intent Preparation of this NOI has included a review of the literature pertaining to Areas of Critical Environmental Concern (ACECs), the Endangered Species Act (ESA), and the National Historic Preservation Act (NHPA), as documented below: • Review of a Massachusetts Geographic Information Systems MassDEP Priority Resources Map,

Figure 3 in Attachment B, shows the Site is not within an ACEC.

• The Northern Long-eared Bat (Myotis septentrionalis) is listed as a Threatened Species in the vicinity of the Project by the US Fish and Wildlife Service (USFWS); however, treatment and discharge of water is not anticipated to cause a disruption to this species. A letter from USFWS is included as Attachment F. Sensitive receptors in the vicinity of the Project are shown on Figure 2 in Attachment B.

• According to the USFWS Information, Planning and Conservation (IPaC) tool, there are no critical habitats at the Site. USFWS confirmed there are no critical habitats in the area and confirmed permit eligibility meets “Criterion A” (Attachment F).

• Additionally, according to the MassDEP Priority Resources Map, no Natural Heritage & Endangered Species Program (NHESP) Priority Habitats for Rare Species or Estimated Habitats for Rare Wildlife were present within half a mile downstream of the discharge location. Therefore, permit eligibility meets “Criterion A.”

• This work will not affect historical properties that are listed by the US Park Service or Massachusetts Cultural Resources. The Eagle Mill is listed in the Macris database; however, discharge will be directly to the Housatonic River, so no structures will be modified or negatively affected by this work. Cultural resources in the vicinity of the Site are listed in Attachment G.

The proposed treatment systems have been designed to reduce contaminants of concern to below the applicable effluent limits. Effluent compliance monitoring will be conducted in compliance with the RGP. Additionally, the flow rate, pH and temperature levels will be monitored in the field and recorded.

March 7, 2019

L2019-501

Your assistance in processing this application is greatly appreciated. If you have any questions or would like additional information, please feel free to contact me at (603) 325-5480 or via email at [email protected]. Sincerely, TRC Environmental Corporation

Jamie Stapleton, PG N. Scott Buchanan Senior Geologist Project Manager cc: Cathy Vakalopoulos, MassDEP Leigh Davis, Eagle Mill Enterprises

Matthew Wheaton, DEW Properties Tom Biolsi, TRC

Attachments: Attachment A – RGP NOI Form and Calculation Spreadsheet Attachment B – Figures

Figure 1 - Site Location Plan Figure 2 - Site Plan Figure 3 - MassDEP Priority Resources Map

Attachment C – Tables Table 1 - Summary of Water Analytical Results – February 2019 Table 2 - Summary of Surface Water Analytical Results – February 2019

Attachment D – Laboratory Analytical Reports Attachment E – StreamStats Database Export for Housatonic River / MassDEP Dilution Factor

Confirmation Documentation Attachment F – Letter from US Fish and Wildlife Service Attachment G – Massachusetts Cultural Resources Database Search Results

mailto:[email protected]

L2019-051

ATTACHMENT A

NOI FORM AND CALCULATION SPREADSHEET

MAG910000 Appendix IV – Part 1 – NOI NHG910000 Page 14 of 24

II. Suggested Format for the Remediation General Permit Notice of Intent (NOI) A. General site information:

1. Name of site:

Site address: Street: City:

State:

Zip:

2. Site owner Owner is (check one): □ Federal □ State/Tribal □ Private □ Other; if so, specify:

Contact Person:

Telephone: Email:

Mailing address: Street: City:

State:

Zip:

3. Site operator, if different than owner

Contact Person:

Telephone: Email:

Mailing address: Street: City:

State:

Zip:

4. NPDES permit number assigned by EPA:

NPDES permit is (check all that apply: □ RGP □ DGP □ CGP □ MSGP □ Individual NPDES permit □ Other; if so, specify:

5. Other regulatory program(s) that apply to the site (check all that apply):

□ MA Chapter 21e; list RTN(s): □ NH Groundwater Management Permit or

Groundwater Release Detection Permit:

□ CERCLA □ UIC Program □ POTW Pretreatment □ CWA Section 404

Eagle Mill Redevelopment Project73 West Center Street

Lee MA 01238

Leigh Davis

413.429.4850 [email protected]

PO Box 777

■

South Egremont MA 01258

Fabino & Libardi Construction Services

Christopher Fabino

617-335-9820 [email protected]

49 Holmes Road Street

Lenox MA 01240

Eagle Mill Enterprises, Inc.


B. Receiving water information: 1. Name of receiving water(s):

Waterbody identification of receiving water(s):

Classification of receiving water(s):

Receiving water is (check any that apply): □ Outstanding Resource Water □ Ocean Sanctuary □ territorial sea □ Wild and Scenic River

2. Has the operator attached a location map in accordance with the instructions in B, above? (check one): □ Yes □ No Are sensitive receptors present near the site? (check one): □ Yes □ No If yes, specify:

3. Indicate if the receiving water(s) is listed in the State’s Integrated List of Waters (i.e., CWA Section 303(d)). Include which designated uses are impaired, and any pollutants indicated. Also, indicate if a final TMDL is available for any of the indicated pollutants. For more information, contact the appropriate State as noted in Part 4.6 of the RGP.

4. Indicate the seven day-ten-year low flow (7Q10) of the receiving water determined in accordance with the instructions in Appendix V for sites located in Massachusetts and Appendix VI for sites located in New Hampshire.

5. Indicate the requested dilution factor for the calculation of water quality-based effluent limitations (WQBELs) determined in accordance with the instructions in Appendix V for sites in Massachusetts and Appendix VI for sites in New Hampshire.

6. Has the operator received confirmation from the appropriate State for the 7Q10and dilution factor indicated? (check one): □ Yes □ No If yes, indicate date confirmation received: 7. Has the operator attached a summary of receiving water sampling results as required in Part 4.2 of the RGP in accordance with the instruction in Appendix VIII? (check one): □ Yes □ No C. Source water information: 1. Source water(s) is (check any that apply):

□ Contaminated groundwater Has the operator attached a summary of influent sampling results as required in Part 4.2 of the RGP in accordance with the instruction in Appendix VIII? (check one): □ Yes □ No

□ Contaminated surface water Has the operator attached a summary of influent sampling results as required in Part 4.2 of the RGP in accordance with the instruction in Appendix VIII? (check one): □ Yes □ No

□ The receiving water

□ Potable water; if so, indicate municipality or origin: □ A surface water other

than the receiving water; if so, indicate waterbody: □ Other; if so, specify:

Housatonic River MA21-19 B

22.6 cubic feet per second

37.9

March 5, 2019

PCB in Fish Tissue, PCBs, Zebra Mussel, excess algal growth, and total phosphorus


2. Source water contaminants:

a. For source waters that are contaminated groundwater or contaminated surface water, indicate are any contaminants present that are not included in the RGP? (check one): □ Yes □ No If yes, indicate the contaminant(s) and the maximum concentration present in accordance with the instructions in Appendix VIII.

b. For a source water that is a surface water other than the receiving water, potable water or other, indicate any contaminants present at the maximum concentration in accordance with the instructions in Appendix VIII? (check one): □ Yes □ No

3. Has the source water been previously chlorinated or otherwise contains residual chlorine? (check one): □ Yes □ No

D. Discharge information 1.The discharge(s) is a(n) (check any that apply): □ Existing discharge □ New discharge □ New source

Outfall(s): Outfall location(s): (Latitude, Longitude)

Discharges enter the receiving water(s) via (check any that apply): □ Direct discharge to the receiving water □ Indirect discharge, if so, specify: □ A private storm sewer system □ A municipal storm sewer system If the discharge enters the receiving water via a private or municipal storm sewer system: Has notification been provided to the owner of this system? (check one): □ Yes □ No Has the operator has received permission from the owner to use such system for discharges? (check one): □ Yes □ No, if so, explain, with an estimated timeframe for obtaining permission: Has the operator attached a summary of any additional requirements the owner of this system has specified? (check one): □ Yes □ No Provide the expected start and end dates of discharge(s) (month/year): Indicate if the discharge is expected to occur over a duration of: □ less than 12 months □ 12 months or more □ is an emergency discharge

Has the operator attached a site plan in accordance with the instructions in D, above? (check one): □ Yes □ No

Housatonic River 42.31182 / -73.25156

■

■

April 1, 2019 to April 30, 2019


2. Activity Category: (check all that apply) 3. Contamination Type Category: (check all that apply)

□ I – Petroleum-Related Site Remediation □ II – Non-Petroleum-Related Site Remediation □ III – Contaminated Site Dewatering □ IV – Dewatering of Pipelines and Tanks □ V – Aquifer Pump Testing □ VI – Well Development/Rehabilitation □ VII – Collection Structure Dewatering/Remediation □ VIII – Dredge-Related Dewatering

a. If Activity Category I or II: (check all that apply)

□ A. Inorganics □ B. Non-Halogenated Volatile Organic Compounds □ C. Halogenated Volatile Organic Compounds □ D. Non-Halogenated Semi-Volatile Organic Compounds □ E. Halogenated Semi-Volatile Organic Compounds □ F. Fuels Parameters

b. If Activity Category III, IV, V, VI, VII or VIII: (check either G or H)

□ G. Sites with Known Contamination

□ H. Sites with Unknown Contamination c. If Category III-G, IV-G, V-G, VI-G, VII-G or VIII-G: (check all that apply) □ A. Inorganics □ B. Non-Halogenated Volatile Organic Compounds □ C. Halogenated Volatile Organic Compounds □ D. Non-Halogenated Semi-Volatile Organic Compounds □ E. Halogenated Semi-Volatile Organic Compounds □ F. Fuels Parameters

d. If Category III-H, IV-H, V-H, VI-H, VII-H or VIII-H Contamination Type Categories A through F apply

MAG910000 Appendix IV – Part 1 – NOINHG910000 Page 18 of 24

4. Influent and Effluent Characteristics

Parameter

Known or

believed absent

Known or

believed present

# of samples

Test method

(#)

Detection limit (μg/l)

Influent Effluent LimitationsDaily

maximum (μg/l)

Daily average

(μg/l)TBEL WQBEL

A. Inorganics

Ammonia Report mg/L ---Chloride Report μg/l ---Total Residual Chlorine 0.2 mg/LTotal Suspended Solids 30 mg/LAntimony 206 μg/LArsenic 104 μg/LCadmium 10.2 μg/LChromium III 323 μg/LChromium VI 323 μg/LCopper 242 μg/LIron 5,000 μg/LLead 160 μg/LMercury 0.739 μg/LNickel 1,450 μg/LSelenium 235.8 μg/LSilver 35.1 μg/LZinc 420 μg/LCyanide 178 mg/L

B. Non-Halogenated VOCs

Total BTEX 100 μg/L ---Benzene 5.0 μg/L ---1,4 Dioxane 200 μg/L ---Acetone 7.97 mg/L ---Phenol 1,080 μg/L

---

1

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✔

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✔

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✔

✔

✔

✔

14500NH3- 0.075 0.078 0.078300.0

1111111111111111

4500CL-D2540D200.8200.8200.8107200.8200.8200.7200.8245.1200.8200.8200.8200.84500CN-C

5.00.025.00.004000.001000.00020100.001000.001000.0500.001000.000200.002000.005000.000400.010000.005

82.2013000.3201.4648.2242312.6400

038.070

82.2013000.3201.4648.2242312.64000038.070

0.197

1145517910.8953779204.740614502229.2716.2123.5689.5444.75419.393.1

11111

624.1624.1624.1624.1420.1

21.050100.030

0

000

00000 5369

0

0


Parameter

Known or

believed absent

Known or

believed present

# of samples

Test method

(#)



maximum (μg/l)

Daily average

(μg/l)TBEL WQBEL

C. Halogenated VOCsCarbon Tetrachloride 4.4 μg/L1,2 Dichlorobenzene 600 μg/L ---1,3 Dichlorobenzene 320 μg/L ---1,4 Dichlorobenzene 5.0 μg/L ---Total dichlorobenzene 763 μg/L in NH ---1,1 Dichloroethane 70 μg/L ---1,2 Dichloroethane 5.0 μg/L ---1,1 Dichloroethylene 3.2 μg/L ---Ethylene Dibromide 0.05 μg/L ---Methylene Chloride 4.6 μg/L ---1,1,1 Trichloroethane 200 μg/L ---1,1,2 Trichloroethane 5.0 μg/L ---Trichloroethylene 5.0 μg/L ---Tetrachloroethylene 5.0 μg/Lcis-1,2 Dichloroethylene 70 μg/L ---Vinyl Chloride 2.0 μg/L ---

D. Non-Halogenated SVOCsTotal Phthalates 190 μg/LDiethylhexyl phthalate 101 μg/LTotal Group I PAHs 1.0 μg/L ---Benzo(a)anthracene

As Total PAHs

Benzo(a)pyrene Benzo(b)fluorantheneBenzo(k)fluoranthene ChryseneDibenzo(a,h)anthraceneIndeno(1,2,3-cd)pyrene

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111111111

624.1624.1624.1624.1624.1624.1624.1624.1504.1

1.05.05.05.05.01.51.51.50.010

00000

000

000000000

0

1111111

624.1624.1624.1624.1624.1624.1624.1

1.02.01.51.01.01.01.0

00000

0

0000000

0

28.6

59.1

11111

625.1625.1625.1625.1625.1

550.100.100.10

000.34

0

000.340.100

0.10

11111

625.1625.1625.1625.1625.1

0.100.100.100.100.10

0.1400.10

0

0.1400.1000

0

-39.1

0.06800.06800.06800.06800.06800.06800.0680


Parameter

Known or

believed absent

Known or

believed present

# of samples

Test method

(#)



maximum (μg/l)

Daily average

(μg/l)TBEL WQBEL

Total Group II PAHs 100 μg/L ---Naphthalene 20 μg/L ---

E. Halogenated SVOCsTotal PCBs 0.000064 μg/L ---Pentachlorophenol 1.0 μg/L ---

F. Fuels ParametersTotal Petroleum Hydrocarbons 5.0 mg/L ---

Ethanol Report mg/L ---Methyl-tert-Butyl Ether 70 μg/L

tert-Butyl Alcohol 120 μg/L in MA40 μg/L in NH ---

tert-Amyl Methyl Ether 90 μg/L in MA140 μg/L in NH ---

Other (i.e., pH, temperature, hardness, salinity, LC50, additional pollutants present); if so, specify:

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pH (Surface water)pH (water)Temperature (Surface Water)Temperature (Water)

11

625.1625.1

0.100.10

0.310

0.310

11

608.3625.1

0.2501.0

00

00

11

1671A624.1

210

00

00 358

1

1

624.1

624.1

100

20

0

0

0

0

1 1664A 4.0 0 0

1111

FieldFieldFieldField

0.010.010.10.1

8.357.501.2 Deg C

8.357.501.2 Deg C3.1 Deg C3.1 Deg C


E. Treatment system information 1. Indicate the type(s) of treatment that will be applied to effluent prior to discharge: (check all that apply) □ Adsorption/Absorption □ Advanced Oxidation Processes □ Air Stripping □ Granulated Activated Carbon (“GAC”)/Liquid Phase Carbon Adsorption □ Ion Exchange □ Precipitation/Coagulation/Flocculation □ Separation/Filtration □ Other; if so, specify:

2. Provide a written description of all treatment system(s) or processes that will be applied to the effluent prior to discharge.

Identify each major treatment component (check any that apply): □ Fractionation tanks□ Equalization tank □ Oil/water separator □ Mechanical filter □ Media filter □ Chemical feed tank □ Air stripping unit □ Bag filter □ Other; if so, specify:

Indicate if either of the following will occur (check any that apply): □ Chlorination □ De-chlorination

3. Provide the design flow capacity in gallons per minute (gpm) of the most limiting component.

Indicate the most limiting component:

Is use of a flow meter feasible? (check one): □ Yes □ No, if so, provide justification:

Provide the proposed maximum effluent flow in gpm.

Provide the average effluent flow in gpm.

If Activity Category IV applies, indicate the estimated total volume of water that will be discharged:

4. Has the operator attached a schematic of flow in accordance with the instructions in E, above? (check one): □ Yes □ No

275275275

Bag Filtration

Transfer pumps to bag filtration to discharge

Bag Filtration


F. Chemical and additive information

1. Indicate the type(s) of chemical or additive that will be applied to effluent prior to discharge or that may otherwise be present in the discharge(s): (check all that apply) □ Algaecides/biocides □ Antifoams □ Coagulants □ Corrosion/scale inhibitors □ Disinfectants □ Flocculants □ Neutralizing agents □ Oxidants □ Oxygen □ scavengers □ pH conditioners □ Bioremedial agents, including microbes □ Chlorine or chemicals containing chlorine □ Other; if so, specify: 2. Provide the following information for each chemical/additive, using attachments, if necessary:

a. Product name, chemical formula, and manufacturer of the chemical/additive; b. Purpose or use of the chemical/additive or remedial agent; c. Material Safety Data Sheet (MSDS) and Chemical Abstracts Service (CAS) Registry number for each chemical/additive; d. The frequency (hourly, daily, etc.), duration (hours, days), quantity (maximum and average), and method of application for the chemical/additive; e. Any material compatibility risks for storage and/or use including the control measures used to minimize such risks; and f. If available, the vendor's reported aquatic toxicity (NOAEL and/or LC50 in percent for aquatic organism(s)).

3. Has the operator attached an explanation which demonstrates that the addition of such chemicals/additives may be authorized under this general permit in accordance

with the instructions in F, above? (check one): □ Yes □ No; if no, has the operator attached data that demonstrates each of the 126 priority pollutants in CWA Section 307(a) and 40 CFR Part 423.15(j)(1) are non-detect in discharges with the addition of the proposed chemical/additive? (check one): □ Yes □ No

G. Endangered Species Act eligibility determination

1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit:

□ FWS Criterion A: No endangered or threatened species or critical habitat are in proximity to the discharges or related activities or come in contact with the “action area”.

□ FWS Criterion B: Formal or informal consultation with the FWS under section 7 of the ESA resulted in either a no jeopardy opinion (formal consultation) or a written concurrence by FWS on a finding that the discharges and related activities are “not likely to adversely affect” listed species or critical habitat (informal consultation). Has the operator completed consultation with FWS? (check one): □ Yes □ No; if no, is consultation underway? (check one): □ Yes □ No

□ FWS Criterion C: Using the best scientific and commercial data available, the effect of the discharges and related activities on listed species and critical habitat have been evaluated. Based on those evaluations, a determination is made by EPA, or by the operator and affirmed by EPA, that the discharges and related activities will have “no effect” on any federally threatened or endangered listed species or designated critical habitat under the jurisdiction of the FWS. This determination was made by: (check one) □ the operator □ EPA □ Other; if so, specify:


□ NMFS Criterion: A determination made by EPA is affirmed by the operator that the discharges and related activities will have “no effect” or are “not likely

to adversely affect” any federally threatened or endangered listed species or critical habitat under the jurisdiction of NMFS and will not result in any take of listed species. Has the operator previously completed consultation with NMFS? (check one): □ Yes □ No

2. Has the operator attached supporting documentation of ESA eligibility in accordance with the instructions in Appendix I, and G, above? (check one): □ Yes □ No Does the supporting documentation include any written concurrence or finding provided by the Services? (check one): □ Yes □ No; if yes, attach.

H. National Historic Preservation Act eligibility determination

1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit: □ Criterion A: No historic properties are present. The discharges and discharge-related activities (e.g., BMPs) do not have the potential to cause effects on

historic properties. □ Criterion B: Historic properties are present. Discharges and discharge related activities do not have the potential to cause effects on historic properties. □ Criterion C: Historic properties are present. The discharges and discharge-related activities have the potential to have an effect or will have an adverse

effect on historic properties. 2. Has the operator attached supporting documentation of NHPA eligibility in accordance with the instructions in H, above? (check one): □ Yes □ No Does the supporting documentation include any written agreement with the State Historic Preservation Officer (SHPO), Tribal Historic Preservation Officer (TPHO), or other tribal representative that outlines measures the operator will carry out to mitigate or prevent any adverse effects on historic properties? (check one): □ Yes □ No

I. Supplemental information

Describe any supplemental information being provided with the NOI. Include attachments if required or otherwise necessary.

Has the operator attached data, including any laboratory case narrative and chain of custody used to support the application? (check one): □ Yes □ No

Has the operator attached the certification requirement for the Best Management Practices Plan (BMPP)? (check one): □ Yes □ No


J. Certification requirement

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I have no personal knowledge that the information submitted is other than true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

BMPP certification statement:

Notification provided to the appropriate State, including a copy of this NOI, if required. Check one: Yes □ No □

Notification provided to the municipality in which the discharge is located, including a copy of this NOI, if requested. Check one: Yes □ No □

Notification provided to the owner of a private or municipal storm sewer system, if such system is used for site discharges, including a copy of this NOI, if requested. Permission obtained from the owner of a private or municipal storm sewer system, if such system is used for site discharges. If yes, attach additional conditions. If no, attach explanation and timeframe for obtaining permission.

Check one: Yes □ No □ NA □ Check one: Yes □ No □ NA □

Notification provided to the owner/operator of the area associated with activities covered by an additional discharge permit(s). Additional discharge permit is (check one): □ RGP □ DGP □ CGP □ MSGP □ Individual NPDES permit □ Other; if so, specify:

Check one: Yes □ No □ NA □

Signature: Date:

Print Name and Title:

A BMPP meeting the requirements of this general permit will be developed and implemented uponinitiation of discharge.


□ NMFS Criterion: A determination made by EPA is affirmed by the operator that the discharges and related activities will have “no effect” or are “not likely

to adversely affect” any federally threatened or endangered listed species or critical habitat under the jurisdiction of NMFS and will not result in any take of listed species. Has the operator previously completed consultation with NMFS? (check one): □ Yes □ No

2. Has the operator attached supporting documentation of ESA eligibility in accordance with the instructions in Appendix I, and G, above? (check one): □ Yes □ No Does the supporting documentation include any written concurrence or finding provided by the Services? (check one): □ Yes □ No; if yes, attach.

H. National Historic Preservation Act eligibility determination

1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit: □ Criterion A: No historic properties are present. The discharges and discharge-related activities (e.g., BMPs) do not have the potential to cause effects on

historic properties. □ Criterion B: Historic properties are present. Discharges and discharge related activities do not have the potential to cause effects on historic properties. □ Criterion C: Historic properties are present. The discharges and discharge-related activities have the potential to have an effect or will have an adverse

effect on historic properties. 2. Has the operator attached supporting documentation of NHPA eligibility in accordance with the instructions in H, above? (check one): □ Yes □ No Does the supporting documentation include any written agreement with the State Historic Preservation Officer (SHPO), Tribal Historic Preservation Officer (TPHO), or other tribal representative that outlines measures the operator will carry out to mitigate or prevent any adverse effects on historic properties? (check one): □ Yes □ No

I. Supplemental information

Describe any supplemental information being provided with the NOI. Include attachments if required or otherwise necessary.

Has the operator attached data, including any laboratory case narrative and chain of custody used to support the application? (check one): □ Yes □ No

Has the operator attached the certification requirement for the Best Management Practices Plan (BMPP)? (check one): □ Yes □ No

L2019-501

ATTACHMENT B

FIGURES

0 1,000 2,000Feet$

Massachusetts

MapLocation

Wannalancit Mills650 Suffolk StreetLowell, MA 01854978-970-5600

FIGURE 1 OctoberR:\Projects\GIS_2017\272533_EagleMill\mxd\FIG_C-1_SiteLocus_EagleMill_20170822.mxd

2018

SITE LOCATION MAP

EAGLE MILL73 WEST CENTER ST

LEE, MA

Approximate Site Boundary

Base Map: Copyright:© 2013 National Geographic Society, i-cubed

Site Location

NOTE: SITE CONSISTS OF 2 PARCELS.

#*

Housatonic River

Offices

No. 5, No. 6,

& Wiper Machine Room

Shipping/Storage

Finishing Room

No. 9 Machine Room

BeaterRoom

FinishedProduct Storage

Auto Shop/Carpenter's Shop

Stock Prep

& Willwright

Shop

Main Mill Building

SecondaryCarpenter Shop

Surface Water Sample Location

Proposed Discharge Location

MAINSTREET

UNIONSTREET

DUBLIN

HILL STREET

CANA

L STR

EET

HIGH STREET

CENTER STREET

0 100 200Feet$ Massachusetts

MapLocation

Wannalancit Mills650 Suffolk StreetLowell, MA 01854978-970-5600

FIGURE 2R:\Projects\GIS_2017\272533_EagleMill\mxd\FIG C-2_Site_Layout_EagleMill_2019_02_28.mxd

FEB 2019

SITE PLAN

EAGLE MILL73 WEST CENTER ST

LEE, MABase Map: Source: Esri, DigitalGlobe, GeoEye,Earthstar Geographics, CNES/Airbus DS, USDA,USGS, AeroGRID, IGN, and the GIS User Community

LegendApproximate Site Boundary Neighboring Parcels

#* Surface Water Sample

Note: 1) Due to the presence of ACM on the floors in the main Mill Building, soil borings SB-9, SB-10 and SB-12 were not conducted. 2) All locations are approximate.

D

PARK STREET

CENTER STREET

MAIN STREET

HOUSATONIC STREET

LAUREL STREET

COLUMBIA STR

EET

73 WEST CENETER STREETLEE, MASSACHUSETTS

Source: MassGIS/EOEA

FIGURE 3

±0 1,250

FeetPublic Water Supplies: Ground, Surface, Non-Community (NTNC, TNC) &% &( &(&%

Approved Zone II, IWPA, Surface Water Supply Zone AProtected Open Space, ACEC

EPA Sole Source Aquifer, FEMA 100 Yr. Floodplain, DEP Solid Waste FacilityNon-Potential Drinking Water Source Area: Medium, High YieldPotentially Productive Aquifers: Medium, High Yield

Boundaries: County and Town

Roads: Limited Access, Multi-Lane, Major/Minor, Track, TrailRailroad, Pipline, Powerline \\\ !! ! ! !!

Wetland, Salt Wetland, Submerged Wetland, Open Water, Reservoir, Tidal Flat/Shoal

Major Basin, Sub Basin, Perennial Stream, Intermittent Stream, Shoreline, Man made Shore, Dam, Aqueduct

Priority Habitat, Certified Vernal Pool [́ FEB.2019

S:\1-PROJECTS\EagleMill\mxd\Fig3_73west_center.mxd

500 FOOT & 0.5 MILE RADIIWannalancit Mills650 Suffolk StreetLowell, MA 01854978-970-5600

Legend

MassGIS Priority Resources Map

L2019-501

ATTACHMENT C

TABLES

Table 1Summary of Analytical Results for Groundwater Samples -- February 2019

Eagle MillsLee, Massachusetts

Sample Location:Sample Name:Sample Date:

Analysis Analyte Unit TBEL WQBELCompliance

Level(2)

Volatile OrganicsBenzene ug/L 5 N/A N/A 5 NA NA 1.0 UToluene ug/L N/A N/A N/A N/A NA NA 1.0 UEthylbenzene ug/L N/A N/A N/A N/A NA NA 1.0 Um,p-Xylene ug/L N/A N/A N/A N/A NA NA 2.0 Uo-Xylene ug/L N/A N/A N/A N/A NA NA 1.0 UXylenes, total ug/L N/A N/A N/A N/A NA NA 1.0 UTotal BTEX ug/L 100 N/A N/A 100 NA NA NDMethylene chloride ug/L 4.6 N/A N/A 4.6 NA NA 1.0 U1,1-Dichloroethane ug/L 70 N/A N/A 70 NA NA 1.5 UCarbon tetrachloride ug/L 4.4 28.6 N/A 1.6 NA NA 1.0 U1,1,2-Trichloroethane ug/L 5 N/A N/A 5 NA NA 1.5 UTetrachloroethene ug/L 5 59.1 N/A 3.3 NA NA 1.0 U1,2-Dichloroethane ug/L 5 N/A N/A 5 NA NA 1.5 U1,1,1-Trichloroethane ug/L 200 N/A N/A 200 NA NA 2.0 UVinyl chloride ug/L 2 N/A N/A 2 NA NA 1.0 U1,1-Dichloroethene ug/L 3.2 N/A N/A 3.2 NA NA 1.0 UTrichloroethene ug/L 5 59.1 N/A 5 NA NA 1.0 U1,2-Dichlorobenzene ug/L 600 N/A N/A 600 NA NA 5.0 U1,3-Dichlorobenzene ug/L 320 N/A N/A 320 NA NA 5.0 U1,4-Dichlorobenzene ug/L 5 N/A N/A 5 NA NA 5.0 UMethyl tert-butyl ether ug/L 70 358 N/A 20 NA NA 10 Ucis-1,2-Dichloroethene ug/L 70 N/A N/A 70 NA NA 1.0 UAcetone ug/L 7,970 N/A N/A 7,970 NA NA 10 U1,2-Dibromo-3-chloropropane ug/L N/A N/A N/A N/A NA NA 0.010 Utert-Butyl alcohol ug/L 120 N/A N/A 120 NA NA 100 Utert-Amyl methyl ether ug/L 90 N/A N/A 90 NA NA 20 U1,2-Dibromoethane (Ethylene dibromide) ug/L 0.05 N/A N/A 0.05 NA NA 0.010 U1,4-Dioxane ug/L 200 N/A N/A 50 NA NA 50 U

Semivolatile Organics by GC/MSBis(2-ethylhexyl)phthalate ug/L 101 39.4 N/A 2.2 NA NA 2.2 UButylbenzylphthalate ug/L N/A N/A N/A N/A NA NA 5.0 UDi-n-butylphthalate ug/L N/A N/A N/A N/A NA NA 5.0 UDiethyl phthalate ug/L N/A N/A N/A N/A NA NA 5.0 UDimethylphthalate ug/L N/A N/A N/A N/A NA NA 5.0 UDi-n-octylphthalate ug/L N/A N/A N/A N/A NA NA 5.0 UTotal Phthalates ug/L 190 N/A N/A 190 NA NA ND

Semivolatile Organics by GC/MS-SIMBenzo(a)anthracene ug/L 1 0.068 0.1 0.1 NA NA 0.10Benzo(a)pyrene ug/L 1 0.068 N/A 0.1 NA NA 0.10 UBenzo(b)fluoranthene ug/L 1 0.068 0.1 0.1 NA NA 0.14Benzo(k)fluoranthene ug/L 1 0.068 N/A 0.1 NA NA 0.10 UChrysene ug/L 1 0.068 0.1 0.1 NA NA 0.10Dibenz(a,h)anthracene ug/L 1 0.068 N/A 0.1 NA NA 0.10 UIndeno(1,2,3-cd)pyrene ug/L 1 0.068 N/A 0.1 NA NA 0.10 UTotal Group I PAHs ug/L 1 N/A N/A 1 NA NA 0.34Acenaphthene ug/L N/A N/A N/A N/A NA NA 0.10 UFluoranthene ug/L N/A N/A N/A N/A NA NA 0.16Naphthalene ug/L 20 N/A N/A 20 NA NA 0.10 UAcenaphthylene ug/L N/A N/A N/A N/A NA NA 0.10 UAnthracene ug/L N/A N/A N/A N/A NA NA 0.10 UBenzo(g,h,i)perylene ug/L N/A N/A N/A N/A NA NA 0.10 UFluorene ug/L N/A N/A N/A N/A NA NA 0.10 UPhenanthrene ug/L N/A N/A N/A N/A NA NA 0.10 UPyrene ug/L N/A N/A N/A N/A NA NA 0.15Total Group II PAHs ug/L 100 N/A N/A 100 NA NA 0.31Pentachlorophenol ug/L 1 N/A N/A 1 NA NA 1.0 U

PCB AroclorsAroclor-1016 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1221 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1232 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1242 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1248 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1254 ug/L N/A N/A N/A N/A NA NA 0.250 UAroclor-1260 ug/L N/A N/A N/A N/A NA NA 0.200 UPCBs, Total ug/L 0.000064 N/A 0.5 0.5 NA NA 0.250 U

Total MetalsAntimony ug/L 206 11,455 N/A 206 NA NA 4 UArsenic ug/L 104 179 N/A 10 NA NA 1 UCadmium ug/L 10.2 10.895 N/A 0.25 NA NA 0.32Chromium ug/L N/A N/A N/A N/A NA NA 1.46Copper ug/L 242 406 N/A 9 NA NA 48.22Iron ug/L 5,000 14,502 N/A 1,000 NA NA 423Lead ug/L 160 229.27 N/A 2.5 NA NA 12.64Mercury ug/L 0.739 16.21 N/A 0.77 NA NA 0.2 UNickel ug/L 1,450 2,356 N/A 52 NA NA 2 USelenium ug/L 235.8 89.5 N/A 5 NA NA 5 USilver ug/L 35.1 444.7 N/A 3.2 NA NA 0.4 UZinc ug/L 420 5,419.30 N/A 120 NA NA 38.07

Dissolved MetalsAntimony ug/L 206 11,455 N/A 206 4 U 4 U NAArsenic ug/L 104 179 N/A 10 1 U 1 U NACadmium ug/L 10.2 10.895 N/A 0.25 0.2 U 0.2 U NAChromium ug/L N/A N/A N/A N/A 1 U 1 U NACopper ug/L 242 406 N/A 9 5.9 4.3 NAIron ug/L 5,000 14,502 N/A 1,000 50 U 50 U NALead ug/L 160 229.27 N/A 2.5 1 U 1 U NAMercury ug/L 0.739 16.21 N/A 0.77 0.2 U 0.2 U NANickel ug/L 1,450 2356 N/A 52 2 U 2 U NASelenium ug/L 235.8 89.5 N/A 5 5 U 5 U NASilver ug/L 35.1 444.7 N/A 3.2 0.4 U 0.4 U NAZinc ug/L 420 5,419.30 N/A 120 10.2 10 U NA

General ChemistrypH su 6.5-8.3 N/A N/A N/A NA NA 7.5Temperature deg. C N/A N/A N/A N/A NA NA 3.1Chloride mg/L N/A N/A N/A 230 NA NA 82.2Hardness as CaCO3 mg/L N/A N/A N/A N/A NA NA 310Total Suspended Solids (TSS) mg/L 30 N/A N/A 30 NA NA 13Cyanide, total mg/L 178 0.0931 N/A 0.0052 NA NA 0.005 UChlorine, Total Residual mg/L 0.2 0.197 N/A 0.05 NA NA 0.02 UAmmonia as Nitrogen mg/L N/A N/A N/A 0.1 NA NA 0.078TPH, SGT-HEM mg/L 5 N/A N/A 5 NA NA 4.00 UPhenolics, Total mg/L 1.08 5.369 N/A 0.3 NA NA 0.030 UChromium (III) (Filtered) mg/L 0.323 3.779 N/A 0.074 0.010 U 0.010 U NAChromium (III) (Unfiltered) mg/L 0.323 3.779 N/A 0.074 NA NA 0.010 UChromium, Hexavalent (Filtered) mg/L 0.323 0.2047 N/A 0.011 0.010 U 0.010 U NAChromium, Hexavalent (Unfiltered) mg/L 0.323 0.2047 N/A 0.011 NA NA 0.010 UEthanol ug/L N/A N/A N/A 400 NA NA 2,000 U^

RGP for Freshwater(1) RGP Required Minimum

Level(3)

BSMT-F5(4) BSMT-FO.45(5) BSMT-NF*BSMT-F5 BSMT-FO.45 BSMT-NF02/14/2019 02/14/2019 02/14/2019

Version: 3/1/2019 Page 1 of 2

Table 1Summary of Analytical Results for Groundwater Samples -- February 2019



Analysis Analyte Unit TBEL WQBELCompliance

Level(2)

RGP for Freshwater(1) RGP Required Minimum

Level(3)

BSMT-F5(4) BSMT-FO.45(5) BSMT-NF*BSMT-F5 BSMT-FO.45 BSMT-NF02/14/2019 02/14/2019 02/14/2019

Notes:mg/L - milligrams per liter.ug/L - micrograms per liter.su - Standard unit.NA - Sample not analyzed for the listed analyte.N/A - Not applicable.ND - Not detected.NS - No MassDEP standards exist for this analyte.U - Analyte was not detected at specified quantitation limit.Values in bold indicate the analyte was detected.^ - Quantitation limit value exceeds the RGP Required Minimum Level.Values shown in bold and shaded black exceed the applicable bolded and underlined RGP Effluent Limits.GC - Gas Chromatography.HEM - Hexane extracted material.MS - Mass Spectrometry.SVOCs - Semivolatile Organic Compounds.SGT - Silica gel treated.PAHs - Polycyclic Aromatic Hydrocarbons.PCBs - Polychlorinated Biphenyls.TPH - Total Petroleum Hydrocarbons.RGP - EPA Remediation General Permit, Effluent Limits, 2016.SIM - Selected Ion Monitoring. TBEL - Technology-Based Effluent Limitation.WQBEL - Water Quality-Based Effluent Limitation.* - The sample was collected on February 28, 2019 for pH and temperature.The above standards apply to discharge to freshwater receiving waters. The RGP contains separate discharge standards for discharges to saltwater receiving waters.(1) RGP for Freshwater standards are an average monthly discharge limitation in Massachusetts only. (2) The compliance level is a discharge standard for analytes with detection limits above the RGP discharge standard.(3) Additional Resource for Selecting Sufficiently Sensitive Test Methods for RGP Notice of Intent (NOI) Sampling Requirements, Table 1. (4) The sample was filtered through a 5-micron filter.(5) The sample was filtered through a 0.45-micron filter.


Table 2Summary of Analytical Results for Surface Water Sample -- February 2019



Analysis Analyte UnitMetals, total

Antimony ug/L 4 UArsenic ug/L 1 UCadmium ug/L 0.2 UChromium ug/L 1 UChromium (III) ug/L 10 UChromium (IV) ug/L 10 UCopper ug/L 1.14Iron ug/L 201Lead ug/L 1 UMercury ug/L 0.2 UNickel ug/L 2 USelenium ug/L 5 USilver ug/L 0.4 UZinc ug/L 10 U

General ChemistryTotal Hardness as CaCO3 mg/L 107Ammonia as Nitrogen mg/L 0.075 UpH su 8.36Temperature Deg. C 1.2

Notes:deg. C - degree Celsius.mg/L - milligrams per liter.ug/L - micrograms per liter.su - Standard unit.U - Analyte was not detected at specified quantitation limit.Values in bold indicate the analyte was detected.

* The sample was collected for pH and temperature on February 28, 2019.

RW*RW

02/14/2019


L2019-501

ATTACHMENT D

LABORATORY ANALYTICAL REPORTS

L1906007

TRC Environmental Consultants

310725

EAGLE MILLS

Client:

Project Name:

Project Number:

02/25/19

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

Wannalancit Mills

650 Suffolk Street

Scott BuchananATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NJ (MA935), NY (11148), NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-17-00196).

Lowell, MA 01854

(978) 656-3518Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:02251914:47

Page 1 of 76

L1906007-01

L1906007-02

L1906007-03

L1906007-04

Alpha Sample ID

BSMT-NF

BSMT-F5

BSMT-FO.45

RW

Client ID

LEE, MA

LEE, MA

LEE, MA

LEE, MA

Sample Location

EAGLE MILLS

310725

Project Name:Project Number:

Lab Number: Report Date:

L190600702/25/19

02/14/19 12:00

02/14/19 13:00

02/14/19 13:15

02/14/19 13:30

Collection Date/TimeMatrix Receive Date

WATER

WATER

WATER

WATER

02/14/19

02/14/19

02/14/19

02/14/19

Serial_No:02251914:47

Page 2 of 76

EAGLE MILLS

310725

Project Name:

Project Number:

Lab Number:

Report Date:L1906007

02/25/19

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all

NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter

(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list

for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified

Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target

Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality

control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R"

or "RE", respectively.

When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in

the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed

Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria

for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the

specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC

information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in

conjunction with the sample result, associated regulatory criteria and any associated data usability implications.

Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms

used in this report are provided in the Glossary located at the back of the report.

HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21

calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put

on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air

canisters will be disposed after 3 business days from the date the project is completed.

Please contact Project Management at 800-624-9220 with any questions.

Serial_No:02251914:47

Page 3 of 76

Case Narrative (continued)

EAGLE MILLS

310725

Project Name:

Project Number:

Lab Number:

Report Date:L1906007

02/25/19

Report Submission

The analysis of Ethanol was subcontracted. A copy of the laboratory report is included as an addendum.

Please note: This data is only available in PDF format and is not available on Data Merger.

Sample Receipt

The samples were field filtered for Dissolved Metals.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 02/25/19

Serial_No:02251914:47

Page 4 of 76

ORGANICS

Serial_No:02251914:47

Page 5 of 76

VOLATILES

Serial_No:02251914:47

Page 6 of 76

FF

Methylene chloride

1,1-Dichloroethane

Carbon tetrachloride

1,1,2-Trichloroethane

Tetrachloroethene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene

cis-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p/m-Xylene

o-xylene

Xylenes, Total

Acetone

Methyl tert butyl ether

Tert-Butyl Alcohol

Tertiary-Amyl Methyl Ether

Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

1.0

1.5

1.0

1.5

1.0

1.5

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

5.0

5.0

2.0

1.0

1.0

10

10

100

20

02/25/19

BSMT-NFClient ID:02/14/19 12:00Date Collected:02/14/19Date Received:

LEE, MASample Location:

L1906007-01Lab ID:

Field Prep: Not Specified

Matrix: WaterAnalytical Method:Analytical Date:Analyst:

128,624.102/15/19 20:17MKS

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 7 of 76

Parameter Result Dilution FactorQualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Pentafluorobenzene

Fluorobenzene

4-Bromofluorobenzene

95

89

102

60-140

60-140

60-140

Acceptance CriteriaSurrogate % Recovery Qualifier

02/25/19



L1906007-01Lab ID:


MDL

Sample Depth:

Serial_No:02251914:47

Page 8 of 76

1,4-Dioxane


ND ug/l 1

Qualifier Units RL

Volatile Organics by GC/MS-SIM - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

50

Fluorobenzene


104

73

60-140

60-140


02/25/19



L1906007-01Lab ID:


Matrix: WaterAnalytical Method:Analytical Date:Analyst:

128,624.1-SIM02/15/19 20:17MKS

MDL

--

Sample Depth:

Serial_No:02251914:47

Page 9 of 76

1,2-Dibromoethane

1,2-Dibromo-3-chloropropane


ND

ND

ug/l

ug/l

1

1

Qualifier Units RL

Microextractables by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

0.010

0.010

02/25/19



L1906007-01Lab ID:


Matrix: Water Extraction Method:

Analytical Method:Analytical Date:Analyst:

14,504.102/20/19 13:21AWS

EPA 504.1Extraction Date: 02/20/19 11:42

MDL

--

--

A

A

Column

Sample Depth:

Serial_No:02251914:47

Page 10 of 76

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/15/19 09:06128,624.1Analytical Method:

Analytical Date:

02/25/19

Analyst: NLK

Methylene chloride

1,1-Dichloroethane



Tetrachloroethene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p/m-Xylene

o-xylene

Xylenes, Total

Acetone


Tert-Butyl Alcohol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.0

1.5

1.0

1.5

1.0

1.5

2.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

5.0

5.0

2.0

1.0

1.0

10

10

100

20

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1207153-4

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:02251914:47

Page 11 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007


Analytical Date:

02/25/19

Analyst: NLK

Parameter Result RLUnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1207153-4

Pentafluorobenzene

Fluorobenzene


94

100

99

60-140

60-140

60-140

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

Serial_No:02251914:47

Page 12 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/15/19 09:06128,624.1-SIMAnalytical Method:

Analytical Date:

02/25/19

Analyst: NLK

1,4-Dioxane

Parameter Result

ND

RL

50ug/l

UnitsQualifier

Volatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 01 Batch: WG1207154-4

Fluorobenzene


117

76

60-140

60-140


Criteria

MDL

--

Serial_No:02251914:47

Page 13 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007


Analytical Date:Extraction Method: EPA 504.1Extraction Date: 02/20/19 11:42

02/25/19

Analyst: AWS

1,2-Dibromoethane


Parameter Result

ND

ND

RL

0.010

0.010

ug/l

ug/l

UnitsQualifier

Microextractables by GC - Westborough Lab for sample(s): 01 Batch: WG1208482-1

MDL

--

--

A

A

Serial_No:02251914:47

Page 14 of 76

Methylene chloride

1,1-Dichloroethane



Tetrachloroethene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

p/m-Xylene

o-xylene

Acetone


Tert-Butyl Alcohol


90

85

85

90

90

90

90

90

95

95

95

85

80

85

100

90

95

92

90

96

90

99

85

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

60-140

50-150

70-130

70-130

70-130

70-130

70-130

65-135

70-130

60-140

5-195

50-150

60-140

65-135

65-135

70-130

65-135

60-140

60-140

40-160

60-140

60-140

60-140

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

28

49

41

45

39

49

36

61

41

63

66

32

30

48

57

43

57

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1207153-3

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual

Serial_No:02251914:47

Page 15 of 76

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1207153-3


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

PentafluorobenzeneFluorobenzene4-Bromofluorobenzene

959999

60-14060-14060-140

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

02/25/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:02251914:47

Page 16 of 76

1,4-Dioxane 100 - 60-140 - 20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 01 Batch: WG1207154-3


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Fluorobenzene4-Bromofluorobenzene

11773

60-14060-140


02/25/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:02251914:47

Page 17 of 76

1,2-Dibromoethane


95

84

-

-

80-120

80-120

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Microextractables by GC - Westborough Lab Associated sample(s): 01 Batch: WG1208482-2


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual Column

A

A

Serial_No:02251914:47

Page 18 of 76

1,2-Dibromoethane


ND

ND

0.247

0.241

99

96

-

-

-

-

80-120

80-120

-

-

20

20

ParameterNative Sample

MS Found

MS%Recovery

MSD Found

MSD %Recovery RPD

RPD Limits

Microextractables by GC - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1208482-3 QC Sample: L1905877-04 Client ID: MS Sample

0.25

0.25

MS Added

Matrix Spike AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

RecoveryLimitsQual Qual Qual Column

A

A

Serial_No:02251914:47

Page 19 of 76

SEMIVOLATILES

Serial_No:02251914:47

Page 20 of 76

FF

Bis(2-ethylhexyl)phthalate

Butyl benzyl phthalate

Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate


ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

2.2

5.0

5.0

5.0

5.0

5.0

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

56

55

57

42-122

46-121

47-138


02/25/19



L1906007-01Lab ID:




129,625.102/19/19 11:42SZ


MDL

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 21 of 76

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Pentachlorophenol


ND

0.16

ND

0.10

ND

0.14

ND

0.10

ND

ND

ND

ND

ND

ND

ND

0.15

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS-SIM - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

1.0

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

38

26

73

60

67

57

25-87

16-65

42-122

46-121

45-128

47-138


02/25/19



L1906007-01Lab ID:




129,625.1-SIM02/20/19 17:24DV


MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 22 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007



02/25/19

Analyst: SZ



Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Parameter Result

ND

ND

ND

ND

ND

ND

RL

2.2

5.0

5.0

5.0

5.0

5.0

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1207584-1

Nitrobenzene-d5

2-Fluorobiphenyl

4-Terphenyl-d14

69

67

71

42-122

46-121

47-138


Criteria

MDL

--

--

--

--

--

--

Serial_No:02251914:47

Page 23 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/19/19 12:46129,625.1-SIMAnalytical Method:


02/25/19

Analyst: DV

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Pentachlorophenol

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.10

1.0

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Semivolatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 01 Batch: WG1207585-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

49

34

92

68

79

74

25-87

16-65

42-122

46-121

45-128

47-138


Criteria

MDL

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:02251914:47

Page 24 of 76



Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

94

106

96

107

82

89

-

-

-

-

-

-

29-137

1-140

8-120

19-132

1-120

1-120

-

-

-

-

-

-

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1207584-3


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Nitrobenzene-d52-Fluorobiphenyl4-Terphenyl-d14

818586

42-12246-12147-138


02/25/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:02251914:47

Page 25 of 76

Acenaphthene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Pentachlorophenol

74

73

66

77

79

80

79

76

73

72

61

78

68

67

68

72

66

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

60-132

43-121

36-120

42-133

32-148

42-140

25-146

44-140

54-126

43-120

1-195

70-120

65-120

1-200

1-151

70-120

38-152

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 01 Batch: WG1207585-2


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual

Serial_No:02251914:47

Page 26 of 76

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 01 Batch: WG1207585-2


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

2-FluorophenolPhenol-d6Nitrobenzene-d52-Fluorobiphenyl2,4,6-Tribromophenol4-Terphenyl-d14

453180617066

25-8716-6542-12246-12145-12847-138


02/25/19

AcceptanceCriteria

Qual Qual Qual

Serial_No:02251914:47

Page 27 of 76

PCBS

Serial_No:02251914:47

Page 28 of 76

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL

Polychlorinated Biphenyls by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

0.250

0.250

0.250

0.250

0.250

0.250

0.200

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl


Decachlorobiphenyl

94

93

94

81

37-123

38-114

37-123

38-114

Acceptance Criteria

B

B

A

A

Surrogate % Recovery Qualifier Column

02/25/19



L1906007-01Lab ID:



Cleanup Method:Analytical Method:Analytical Date:Analyst:

127,608.302/19/19 18:19WR

EPA 608.3

EPA 3665AExtraction Date: 02/18/19 08:02

Cleanup Date: 02/18/19Cleanup Method: EPA 3660BCleanup Date: 02/18/19

MDL

--

--

--

--

--

--

--

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:02251914:47

Page 29 of 76


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007


Analytical Date:Extraction Method:

Cleanup Method:

EPA 608.3

EPA 3665AExtraction Date: 02/18/19 08:02

02/25/19

Cleanup Method: EPA 3660B

Analyst: WR

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.250

0.250

0.250

0.250

0.250

0.250

0.200

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 01 Batch: WG1207681-1


Decachlorobiphenyl


Decachlorobiphenyl

102

95

101

79

37-123

38-114

37-123

38-114

Surrogate %Recovery Qualifier ColumnAcceptance

Criteria

Cleanup Date: 02/18/19

Cleanup Date: 02/18/19

MDL

--

--

--

--

--

--

--

Column

A

A

A

A

A

A

A

B

B

A

A

Serial_No:02251914:47

Page 30 of 76

Aroclor 1016

Aroclor 1260

79

77

-

-

50-140

8-140

-

-

36

38

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 01 Batch: WG1207681-2


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl

91849171

37-12338-11437-12338-114

BBAA

Surrogate Qual Column%Recovery Qual%RecoveryLCS LCSD

02/25/19

AcceptanceCriteria

Qual Qual Qual Column

A

A

Serial_No:02251914:47

Page 31 of 76

METALS

Serial_No:02251914:47

Page 32 of 76

FF

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

SAMPLE RESULTS


Matrix: Water


L1906007-01Lab ID:


Parameter ResultDilution FactorQualifier Units RL

DateAnalyzed

AnalyticalMethod Analyst

Date Prepared

Total Metals - Mansfield Lab

Total Hardness by SM 2340B - Mansfield Lab

General Chemistry - Mansfield Lab

Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Iron, Total

Lead, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Hardness

Chromium, Trivalent (Unfiltered)

ND

ND

0.00032

0.00146

0.04822

0.423

0.01264

ND

ND

ND

ND

0.03807

310

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00400

0.00100

0.00020

0.00100

0.00100

0.050

0.00100

0.00020

0.00200

0.00500

0.00040

0.01000

0.660

0.010

02/15/19 15:28

02/15/19 15:28

02/15/19 15:28

02/15/19 15:28

02/15/19 15:28

02/19/19 16:54

02/15/19 15:28

02/15/19 18:58

02/15/19 15:28

02/15/19 15:28

02/15/19 15:28

02/15/19 15:28

02/19/19 16:54

02/15/19 15:28

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

3,200.8

3,245.1

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

107,-

AM

AM

AM

AM

AM

LC

AM

EA

AM

AM

AM

AM

LC

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 10:50

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 245.1

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

NA

PrepMethodMDL

--

--

--

--

--

--

--

--

--

--

--

--

NA

--

Sample Depth:

Serial_No:02251914:47

Page 33 of 76

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

SAMPLE RESULTS

BSMT-F5Client ID:02/14/19 13:00Date Collected:02/14/19Date Received:

Matrix: Water


L1906007-02Lab ID:

Field Prep: Refer to COC


DateAnalyzed


Date Prepared


Dissolved Metals - Mansfield Lab

Chromium, Trivalent (Filtered)

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved

Mercury, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

ND

ND

ND

ND

ND

0.0059

ND

ND

ND

ND

ND

ND

0.0102

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

0.010

0.0040

0.0010

0.0002

0.0010

0.0010

0.050

0.0010

0.00020

0.0020

0.0050

0.0004

0.0100

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

02/19/19 23:47

02/19/19 20:29

02/18/19 15:11

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

02/19/19 20:29

107,-

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

3,200.8

3,245.1

3,200.8

3,200.8

3,200.8

3,200.8

AM

AM

AM

AM

AM

AB

AM

MG

AM

AM

AM

AM

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/18/19 10:44

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

NA

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 245.1

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 34 of 76

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

SAMPLE RESULTS

BSMT-FO.45Client ID:02/14/19 13:15Date Collected:02/14/19Date Received:

Matrix: Water


L1906007-03Lab ID:

Field Prep: Refer to COC


DateAnalyzed


Date Prepared


Dissolved Metals - Mansfield Lab

Chromium, Trivalent (Filtered)

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Iron, Dissolved

Lead, Dissolved

Mercury, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

ND

ND

ND

ND

ND

0.0043

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

0.010

0.0040

0.0010

0.0002

0.0010

0.0010

0.050

0.0010

0.00020

0.0020

0.0050

0.0004

0.0100

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

02/20/19 00:05

02/19/19 20:17

02/18/19 15:22

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

02/19/19 20:17

107,-

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

3,200.8

3,245.1

3,200.8

3,200.8

3,200.8

3,200.8

AM

AM

AM

AM

AM

AB

AM

MG

AM

AM

AM

AM

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/18/19 10:44

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

NA

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 245.1

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

PrepMethodMDL

--

--

--

--

--

--

--

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 35 of 76

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

SAMPLE RESULTS

RWClient ID:02/14/19 13:30Date Collected:02/14/19Date Received:

Matrix: Water


L1906007-04Lab ID:



DateAnalyzed


Date Prepared

Total Metals - Mansfield Lab

Total Hardness by SM 2340B - Mansfield Lab


Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Iron, Total

Lead, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Hardness

Chromium, Trivalent (Unfiltered)

ND

ND

ND

ND

0.00114

0.201

ND

ND

ND

ND

ND

ND

107

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.00400

0.00100

0.00020

0.00100

0.00100

0.050

0.00100

0.00020

0.00200

0.00500

0.00040

0.01000

0.660

0.010

02/15/19 15:32

02/15/19 15:32

02/15/19 15:32

02/15/19 15:32

02/15/19 15:32

02/19/19 17:33

02/15/19 15:32

02/15/19 19:00

02/15/19 15:32

02/15/19 15:32

02/15/19 15:32

02/15/19 15:32

02/19/19 17:33

02/15/19 15:32

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

3,200.8

3,245.1

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

107,-

AM

AM

AM

AM

AM

LC

AM

EA

AM

AM

AM

AM

LC

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 10:50

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 245.1

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

EPA 3005A

NA

PrepMethodMDL

--

--

--

--

--

--

--

--

--

--

--

--

NA

--

Sample Depth:

Serial_No:02251914:47

Page 36 of 76

FF

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

02/25/19

Iron, Total

Hardness

Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

0.050

0.660

0.00400

0.00100

0.00020

0.00100

0.00100

0.00100

0.00200

0.00500

0.00040

0.01000

02/19/19 15:22

02/19/19 15:22

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

02/15/19 13:59

19,200.7

19,200.7

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

LC

LC

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

02/15/19 08:52

Total Metals - Mansfield Lab for sample(s): 01,04 Batch: WG1207013-1

Total Hardness by SM 2340B - Mansfield Lab for sample(s): 01,04 Batch: WG1207013-1


EPA 3005A

EPA 3005A

EPA 3005A

Digestion Method:

Digestion Method:

Digestion Method:

Prep Information

Prep Information

Prep Information

MDL

MDL

MDL

--

NA

--

--

--

--

--

--

--

--

--

--

Serial_No:02251914:47

Page 37 of 76

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

02/25/19

Mercury, Total

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Lead, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

Iron, Dissolved

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

0.0002

0.0040

0.0010

0.0002

0.0010

0.0010

0.0010

0.0020

0.0050

0.0004

0.0100

0.050

02/15/19 18:08

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 20:09

02/19/19 21:50

3,245.1

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

3,200.8

19,200.7

EA

AM

AM

AM

AM

AM

AM

AM

AM

AM

AM

AB

02/15/19 10:50

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26

02/15/19 14:26


Dissolved Metals - Mansfield Lab for sample(s): 02-03 Batch: WG1207174-1


EPA 245.1

EPA 3005A

EPA 3005A

Digestion Method:

Digestion Method:

Digestion Method:

Prep Information

Prep Information

Prep Information

MDL

MDL

MDL

--

--

--

--

--

--

--

--

--

--

--

--

Serial_No:02251914:47

Page 38 of 76



Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

DateAnalyzed


Date Prepared

02/25/19

Mercury, Dissolved ND mg/l 10.00020 02/18/19 15:08 3,245.1 MG02/18/19 10:44


EPA 245.1Digestion Method:

Prep Information

MDL

--

Serial_No:02251914:47

Page 39 of 76

Iron, Total

Hardness

Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

92

106

94

102

102

98

98

105

101

100

96

104

102

-

-

-

-

-

-

-

-

-

-

-

-

-

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,04 Batch: WG1207013-2

Total Hardness by SM 2340B - Mansfield Lab Associated sample(s): 01,04 Batch: WG1207013-2




Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual

Serial_No:02251914:47

Page 40 of 76

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Lead, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

Iron, Dissolved

Mercury, Dissolved

88

102

99

98

96

107

98

111

96

107

100

96

-

-

-

-

-

-

-

-

-

-

-

-

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

85-115

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Dissolved Metals - Mansfield Lab Associated sample(s): 02-03 Batch: WG1207174-2




Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Serial_No:02251914:47

Page 41 of 76

Iron, Total

Hardness

Iron, Total

Hardness

Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

1.84

139

ND

112

ND

ND

ND

ND

ND

ND

0.00809

ND

ND

ND

ND

2.81

204

1.04

182

0.4154

0.1245

0.05724

0.1978

0.2508

0.5476

0.5228

0.1279

0.05050

0.5524

0.0050

97

98

104

106

83

104

112

99

100

107

103

106

101

110

100

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,04 QC Batch ID: WG1207013-3 QC Sample: L1905877-04 Client ID: MS Sample

Total Hardness by SM 2340B - Mansfield Lab Associated sample(s): 01,04 QC Batch ID: WG1207013-3 QC Sample: L1905877-04 Client ID: MS Sample


Total Hardness by SM 2340B - Mansfield Lab Associated sample(s): 01,04 QC Batch ID: WG1207013-7 QC Sample: L1905728-01 Client ID: MS Sample



1

66.2

1

66.2

0.5

0.12

0.051

0.2

0.25

0.51

0.5

0.12

0.05

0.5

0.005

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual

Serial_No:02251914:47

Page 42 of 76

Mercury, Total

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Lead, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

Iron, Dissolved

Mercury, Dissolved

ND

ND

ND

ND

ND

0.0059

ND

ND

ND

ND

0.0102

ND

ND

0.0048

0.4657

0.1235

0.0538

0.1926

0.2381

0.5478

0.4957

0.1311

0.0473

0.5281

1.05

0.00437

97

93

103

106

96

93

107

99

109

94

104

105

87

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


Dissolved Metals - Mansfield Lab Associated sample(s): 02-03 QC Batch ID: WG1207174-3 QC Sample: L1906007-02 Client ID: BSMT-F5



0.005

0.5

0.12

0.051

0.2

0.25

0.51

0.5

0.12

0.05

0.5

1

0.005

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Serial_No:02251914:47

Page 43 of 76

Iron, Total

Antimony, Total

Arsenic, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, Total

1.84

ND

ND

ND

ND

ND

ND

0.00809

ND

ND

ND

ND

ND

1.83

ND

ND

ND

ND

ND

ND

0.00819

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

NC

NC

NC

NC

NC

NC

1

NC

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20

20

20

20

20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,04 QC Batch ID: WG1207013-4 QC Sample: L1905877-04 Client ID: DUP Sample




EAGLE MILLS

310725

Project Name:

Project Number:

L1906007Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

02/25/19

Qual

Serial_No:02251914:47

Page 44 of 76

Antimony, Dissolved

Arsenic, Dissolved

Cadmium, Dissolved

Chromium, Dissolved

Copper, Dissolved

Lead, Dissolved

Nickel, Dissolved

Selenium, Dissolved

Silver, Dissolved

Zinc, Dissolved

Iron, Dissolved

Mercury, Dissolved

ND

ND

ND

ND

0.0059

ND

ND

ND

ND

0.0102

ND

ND

ND

ND

ND

ND

0.0053

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

NC

NC

NC

NC

10

NC

NC

NC

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20

20

20

20





EAGLE MILLS

310725

Project Name:

Project Number:

L1906007Lab Number:

Report Date:


02/25/19

Serial_No:02251914:47

Page 45 of 76

INORGANICS&

MISCELLANEOUS

Serial_No:02251914:47

Page 46 of 76

FF


Parameter ResultDilution Factor

Matrix: Water


L1906007-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough Lab

Anions by Ion Chromatography - Westborough Lab

Solids, Total Suspended

Cyanide, Total

Chlorine, Total Residual

Nitrogen, Ammonia

TPH, SGT-HEM

Phenolics, Total

Chromium, Hexavalent (Unfiltered)

Chloride

13.

ND

ND

0.078

ND

ND

ND

82.2

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

10

5.0

0.005

0.02

0.075

4.00

0.030

0.010

5.00

02/15/19 14:20

02/15/19 15:19

02/15/19 07:10

02/15/19 20:47

02/15/19 22:03

02/19/19 13:03

02/15/19 06:04

02/16/19 19:35

121,2540D

121,4500CN-CE

121,4500CL-D

121,4500NH3-BH

74,1664A

4,420.1

1,7196A

44,300.0

DR

LH

MA

AT

ML

BR

MA

JR

Date Prepared

-

02/15/19 12:10

-

02/15/19 16:13

02/15/19 16:30

02/15/19 06:00

02/15/19 04:40

-

02/25/19

MDL

NA

--

--

--

--

--

--

--

Sample Depth:

Serial_No:02251914:47

Page 47 of 76

FF

BSMT-F5Client ID:02/14/19 13:00Date Collected:02/14/19Date Received:


Matrix: Water


L1906007-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Field Prep:

DateAnalyzed


Refer to COC

General Chemistry - Westborough LabChromium, Hexavalent (Filtered) ND mg/l 10.010 02/15/19 05:54 1,7196A MA

Date Prepared

02/15/19 04:40

02/25/19

MDL

--

Sample Depth:

Serial_No:02251914:47

Page 48 of 76

FF

BSMT-FO.45Client ID:02/14/19 13:15Date Collected:02/14/19Date Received:


Matrix: Water


L1906007-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Field Prep:

DateAnalyzed


Refer to COC

General Chemistry - Westborough LabChromium, Hexavalent (Filtered) ND mg/l 10.010 02/15/19 05:55 1,7196A MA

Date Prepared

02/15/19 04:40

02/25/19

MDL

--

Sample Depth:

Serial_No:02251914:47

Page 49 of 76

FF

RWClient ID:02/14/19 13:30Date Collected:02/14/19Date Received:


Matrix: Water


L1906007-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabNitrogen, Ammonia


ND

ND

mg/l

mg/l

1

1

0.075

0.010

02/15/19 20:50

02/15/19 06:05

121,4500NH3-BH

1,7196A

AT

MA

Date Prepared

02/15/19 16:13

02/15/19 04:40

02/25/19

MDL

--

--

Sample Depth:

Serial_No:02251914:47

Page 50 of 76

FF



Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

DateAnalyzed


Date Prepared

02/25/19

Phenolics, Total

Chromium, Hexavalent




Nitrogen, Ammonia

Cyanide, Total

TPH, SGT-HEM

Chloride

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

0.030

0.010

0.010

5.0

0.02

0.075

0.005

4.00

0.500

02/19/19 12:57

02/15/19 05:49

02/15/19 05:49

02/15/19 14:20

02/15/19 07:10

02/15/19 20:43

02/15/19 14:53

02/15/19 22:03

02/16/19 15:47

4,420.1

1,7196A

1,7196A

121,2540D

121,4500CL-D

121,4500NH3-BH

121,4500CN-CE

74,1664A

44,300.0

BR

MA

MA

DR

MA

AT

LH

ML

JR

02/15/19 06:00

02/15/19 04:40

02/15/19 04:40

-

-

02/15/19 16:13

02/15/19 12:10

02/15/19 16:30

-

General Chemistry - Westborough Lab for sample(s): 01 Batch: WG1206962-1

General Chemistry - Westborough Lab for sample(s): 02-03 Batch: WG1206965-1

General Chemistry - Westborough Lab for sample(s): 01,04 Batch: WG1206968-1



General Chemistry - Westborough Lab for sample(s): 01,04 Batch: WG1207062-1



Anions by Ion Chromatography - Westborough Lab for sample(s): 01 Batch: WG1207903-1

MDL

--

--

--

NA

--

--

--

--

--

Serial_No:02251914:47

Page 51 of 76

Phenolics, Total




Nitrogen, Ammonia

Cyanide, Total

TPH

94

100

100

92

109

106

86

-

-

-

-

-

-

-

70-130

85-115

85-115

90-110

80-120

90-110

64-132

-

-

-

-

-

-

-

20

20

20

34

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 01 Batch: WG1206962-2

General Chemistry - Westborough Lab Associated sample(s): 02-03 Batch: WG1206965-2

General Chemistry - Westborough Lab Associated sample(s): 01,04 Batch: WG1206968-2


General Chemistry - Westborough Lab Associated sample(s): 01,04 Batch: WG1207062-2




Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual Qual Qual

Serial_No:02251914:47

Page 52 of 76

Chloride 97 - 90-110 -

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Anions by Ion Chromatography - Westborough Lab Associated sample(s): 01 Batch: WG1207903-2


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Serial_No:02251914:47

Page 53 of 76

Phenolics, Total




Nitrogen, Ammonia

Cyanide, Total

TPH

Chloride

ND

ND

ND

0.28

0.078

ND

ND

37.7

0.40

0.098

0.096

0.46

3.61

0.209

17.4

39.8

100

98

96

72

88

104

87

53

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

70-130

85-115

85-115

80-120

80-120

90-110

64-132

90-110

-

-

-

-

-

-

-

-

20

20

20

20

20

30

34

18


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1206962-4 QC Sample: L1906007-01 Client ID: BSMT-NF

General Chemistry - Westborough Lab Associated sample(s): 02-03 QC Batch ID: WG1206965-4 QC Sample: L1906007-03 Client ID: BSMT-FO.45

General Chemistry - Westborough Lab Associated sample(s): 01,04 QC Batch ID: WG1206968-4 QC Sample: L1906007-04 Client ID: RW

General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1207041-4 QC Sample: L1905997-02 Client ID: MS Sample

General Chemistry - Westborough Lab Associated sample(s): 01,04 QC Batch ID: WG1207062-4 QC Sample: L1906007-01 Client ID: BSMT-NF



Anions by Ion Chromatography - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1207903-3 QC Sample: L1906215-01 Client ID: MS Sample

0.4

0.1

0.1

0.25

4

0.2

20

4

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

EAGLE MILLS

310725

L1906007

02/25/19

Qual

Q

Q

Qual Qual

Serial_No:02251914:47

Page 54 of 76

Phenolics, Total





Nitrogen, Ammonia

Cyanide, Total

TPH

Chloride

ND

ND

ND

140

2.0

0.078

ND

ND

37.7

ND

ND

ND

120

1.9

ND

ND

ND

37.7

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

NC

NC

NC

15

5

NC

NC

NC

0

20

20

20

29

20

20

30

34

18


General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1206962-3 QC Sample: L1906007-01 Client ID: BSMT-NF

General Chemistry - Westborough Lab Associated sample(s): 02-03 QC Batch ID: WG1206965-3 QC Sample: L1906007-02 Client ID: BSMT-F5


General Chemistry - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1207016-2 QC Sample: L1905989-01 Client ID: DUP Sample





Anions by Ion Chromatography - Westborough Lab Associated sample(s): 01 QC Batch ID: WG1207903-4 QC Sample: L1906215-01 Client ID: DUP Sample

EAGLE MILLS

310725

Project Name:

Project Number:

L1906007Lab Number:

Report Date:


02/25/19

Qual

Serial_No:02251914:47

Page 55 of 76

*Values in parentheses indicate holding time in days

L1906007-01A

L1906007-01B

L1906007-01C

L1906007-01D

L1906007-01E

L1906007-01F

L1906007-01G

L1906007-01H

L1906007-01I

L1906007-01J

L1906007-01K

L1906007-01L

L1906007-01M

L1906007-01N

L1906007-01P

L1906007-01Q

L1906007-01R

L1906007-01S

L1906007-01T

L1906007-01U

Vial Na2S2O3 preserved








Amber 950ml H2SO4 preserved

Vial HCl preserved

Vial HCl preserved

Vial HCl preserved

Plastic 250ml unpreserved

Plastic 250ml NaOH preserved

Plastic 250ml HNO3 preserved


Plastic 500ml H2SO4 preserved


Amber 1000ml Na2S2O3


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

<2

NA

NA

NA

7

>12

<2

7

<2

7

7

7

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A

B

Absent

Absent

Cooler Custody SealCooler Information

EAGLE MILLS

310725

624.1-RGP(7),624.1-SIM-RGP(7)

624.1-RGP(7),624.1-SIM-RGP(7)

624.1-RGP(7),624.1-SIM-RGP(7)

624.1-RGP(7),624.1-SIM-RGP(7)

624.1-RGP(7),624.1-SIM-RGP(7)

624.1-RGP(7),624.1-SIM-RGP(7)

504(14)

504(14)

TPHENOL-420(28)

SUB-ETHANOL(14)

SUB-ETHANOL(14)

SUB-ETHANOL(14)

HEXCR-7196-UF(1)

TCN-4500(14)

CD-2008T(180),NI-2008T(180),ZN-2008T(180),CU-2008T(180),FE-UI(180),HARDU(180),AG-2008T(180),AS-2008T(180),HG-U(28),SE-2008T(180),CR-2008T(180),PB-2008T(180),SB-2008T(180)

CL-300(28),TRC-4500(1)

NH3-4500(28)

TSS-2540(7)

PCB-608.3(7)

PCB-608.3(7)

Project Name:

Project Number:

L1906007Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type CoolerTempdeg C Pres Seal

Container Information

Analysis(*)

02/25/19

Were project specific reporting limits specified? YES

<2

7

>12

<2

7

<2

7

7

7

FrozenDate/Time

FinalpH

Initial pH

Serial_No:02251914:47

Page 56 of 76

*Values in parentheses indicate holding time in days

L1906007-01V

L1906007-01W

L1906007-01X

L1906007-01Y

L1906007-01Z

L1906007-01Z1

L1906007-02A

L1906007-02B

L1906007-03A

L1906007-03B

L1906007-04A

L1906007-04B

L1906007-04C





Amber 1000ml HCl preserved

Amber 1000ml HCl preserved







Plastic 500ml H2SO4 preserved

A

A

A

A

A

A

B

B

B

B

B

B

B

7

7

7

7

NA

NA

<2

7

<2

7

<2

7

<2

3.2

3.2

3.2

3.2

3.2

3.2

3.6

3.6

3.6

3.6

3.6

3.6

3.6

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

EAGLE MILLS

310725

625.1-RGP(7)

625.1-RGP(7)

625.1-SIM-RGP(7)

625.1-SIM-RGP(7)

TPH-1664(28)

TPH-1664(28)

AG-2008S(180),CR-2008S(180),FE-RI(180),AS-2008S(180),PB-2008S(180),ZN-2008S(180),NI-2008S(180),SE-2008S(180),CD-2008S(180),CU-2008S(180),SB-2008S(180),HG-R(28)

HEXCR-7196(1)

AG-2008S(180),CR-2008S(180),FE-RI(180),AS-2008S(180),PB-2008S(180),ZN-2008S(180),NI-2008S(180),SE-2008S(180),CD-2008S(180),CU-2008S(180),SB-2008S(180),HG-R(28)

HEXCR-7196(1)

CD-2008T(180),NI-2008T(180),ZN-2008T(180),CU-2008T(180),FE-UI(180),HARDU(180),AG-2008T(180),AS-2008T(180),HG-U(28),SE-2008T(180),CR-2008T(180),PB-2008T(180),SB-2008T(180)

HEXCR-7196-UF(1)

NH3-4500(28)

Project Name:

Project Number:

L1906007Lab Number:

Report Date:

Container ID Container Type CoolerTempdeg C Pres Seal

Container Information

Analysis(*)

02/25/19

7

7

7

7

<2

7

<2

7

<2

7

<2

FrozenDate/Time

FinalpH

Initial pH

Serial_No:02251914:47

Page 57 of 76

Report Format: Data Usability Report

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1906007EAGLE MILLS

310725 02/25/19

Acronyms

EDL

EMPC

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TEF

TEQ

TIC

Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Estimated Maximum Possible Concentration: The concentration that results from the signal present at the retention time of an analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria. An EMPC is a worst-case estimate of the concentration.Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample forwhich an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.N-Nitrosodiphenylamine/Diphenylamine.

Not Ignitable.

Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.Semi-dynamic Tank Leaching Procedure per EPA Method 1315.

Toxic Equivalency Factors: The values assigned to each dioxin and furan to evaluate their toxicity relative to 2,3,7,8-TCDD.

Toxic Equivalent: The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF and then summing the resulting values.Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined uponreceipt, if applicable.PFAS Total: With respect to PFAS analyses, the 'PFAS, Total (5)' result is defined as the summation of results for: PFHpA, PFHxS, PFOA, PFNA and PFOS. If a 'Total' result is requested, the results of its individual components will also be reported.Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total'

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method.

-

Footnotes

Serial_No:02251914:47

Page 58 of 76

Report Format: Data Usability Report

Project Name:

Project Number:

Lab Number:

Report Date:

L1906007EAGLE MILLS

310725 02/25/19

result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082.

Data Qualifiers

A

B

C

D

E

G

H

I

J

M

ND

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone). Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The lower value for the two columns has been reported due to obvious interference.

Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs).

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Not detected at the reporting limit (RL) for the sample.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

Analytical results are from modified screening analysis.

Serial_No:02251914:47

Page 59 of 76

Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

3

4

14

19

44

74

107

121

127

128

129

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007.

Methods for the Determination of Metals in Environmental Samples, Supplement I. EPA/600/R-94/111. May 1994.

Methods for Chemical Analysis of Water and Wastes. EPA 600/4-79-020. Revised March 1983.

Methods for the Determination of Organic Compounds in Finished Drinking Water and Raw Source Water. EPA/600/4-88/039, Revised July 1991.

Inductively Coupled Plasma Atomic Emission Spectrometric Method for Trace Element Analysis of Water and Wastes. Appendix C, Part 136, 40 CFR (Code of Federal Regulations). July 1, 1999 edition.

Methods for the Determination of Inorganic Substances in Environmental Samples, EPA/600/R-93/100, August 1993.

Method 1664,Revision A: N-Hexane Extractable Material (HEM; Oil & Grease) and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) by Extraction and Gravimetry, EPA-821-R-98-002, February 1999.

Alpha Analytical - In-house calculation method.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF. Standard Methods Online.

Method 608.3: Organochlorine Pesticides and PCBs by GC/HSD, EPA 821-R-16-009, December 2016.

Method 624.1: Purgeables by GC/MS, EPA 821-R-16-008, December 2016.

Method 625.1: Base/Neutrals and Acids by GC/MS, EPA 821-R-16-007, December 2016.

Project Name:

Project Number:

Lab Number:

Report Date:

L1906007EAGLE MILLS

310725

REFERENCES

02/25/19

Serial_No:02251914:47

Page 60 of 76

Alpha Analytical, Inc. ID No.:17873 Facility: Company-wide Revision 12Department: Quality Assurance Published Date: 10/9/2018 4:58:19 PMTitle: Certificate/Approval Program Summary Page 1 of 1

Document Type: Form Pre-Qualtrax Document ID: 08-113

Certification Information

The following analytes are not included in our Primary NELAP Scope of Accreditation:

Westborough FacilityEPA 624/624.1: m/p-xylene, o-xyleneEPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), Methyl methacrylate, 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene.EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine.

EPA 6860: SCM: Perchlorate SM4500: NPW: Amenable Cyanide; SCM: Total Phosphorus, TKN, NO2, NO3.

Mansfield FacilitySM 2540D: TSSEPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187.EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. Biological Tissue Matrix: EPA 3050B

The following analytes are included in our Massachusetts DEP Scope of Accreditation

Westborough Facility:

Drinking WaterEPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-BEPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP.Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D.

Non-Potable WaterSM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500P-E, SM4500P-B, E, SM4500SO4-E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D, EPA 300: Chloride, Sulfate, Nitrate. EPA 624.1: Volatile Halocarbons & Aromatics, EPA 608.3: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBsEPA 625.1: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, EPA 1600, EPA 1603.

Mansfield Facility:

Drinking WaterEPA 200.7: Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg.EPA 522.

Non-Potable WaterEPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn. EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Fe, Pb, Mn, Ni, K, Se, Ag, Na, TL, Zn.EPA 245.1 Hg. SM2340B

For a complete listing of analytes and methods, please contact your Alpha Project Manager.

Serial_No:02251914:47

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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Nashville2960 Foster Creighton DriveNashville, TN 37204Tel: (615)726-0177

TestAmerica Job ID: 490-168679-1Client Project/Site: L1906007

For:Alpha Analytical Inc145 Flanders RoadWestborough, Massachusetts 01581-1019

Attn: Ashaley Kane

Authorized for release by:2/24/2019 6:00:33 PMRoxanne Cisneros, Senior Project Manager(615)[email protected]

Designee for

Ken Hayes, Project Manager II(615)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com



Table of Contents

Client: Alpha Analytical IncProject/Site: L1906007

TestAmerica Job ID: 490-168679-1

Page 2 of 13TestAmerica Nashville

2/24/2019

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

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Sample SummaryTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc

Project/Site: L1906007

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-168679-1 BSMT-NF Water 02/14/19 12:00 02/19/19 09:05

TestAmerica Nashville

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Case NarrativeClient: Alpha Analytical Inc TestAmerica Job ID: 490-168679-1Project/Site: L1906007

Job ID: 490-168679-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative490-168679-1

Comments

No additional comments.

Receipt

The sample was received on 2/19/2019 9:05 AM; the sample arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 1.3º C.

GC Semi VOA Method(s) 1671A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

analytical batch 490-576455.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

TestAmerica NashvillePage 4 of 13 2/24/2019

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Definitions/GlossaryTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc


Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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Client Sample ResultsTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc


Lab Sample ID: 490-168679-1Client Sample ID: BSMT-NFMatrix: WaterDate Collected: 02/14/19 12:00

Date Received: 02/19/19 09:05

Method: 1671A - Ethanol (GC/FID)RL MDL

Ethanol ND 2000 500 ug/L 02/20/19 11:26 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Isopropyl acetate (Surr) 76 70 - 130 02/20/19 11:26 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery


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QC Sample ResultsTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc


Method: 1671A - Ethanol (GC/FID)

Client Sample ID: Method BlankLab Sample ID: MB 490-576455/7Matrix: Water Prep Type: Total/NAAnalysis Batch: 576455

RL MDL

Ethanol ND 2000 500 ug/L 02/20/19 11:02 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Isopropyl acetate (Surr) 84 70 - 130 02/20/19 11:02 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-576455/8Matrix: Water Prep Type: Total/NAAnalysis Batch: 576455

Ethanol 50200 45450 ug/L 90 70 - 130

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Isopropyl acetate (Surr) 70 - 130

Surrogate

85

LCS LCS

Qualifier Limits%Recovery

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-576455/9Matrix: Water Prep Type: Total/NAAnalysis Batch: 576455

Ethanol 50200 46640 ug/L 93 70 - 130 3 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Isopropyl acetate (Surr) 70 - 130

Surrogate

88

LCSD LCSD

Qualifier Limits%Recovery


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QC Association SummaryTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc


GC VOA

Analysis Batch: 576455

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 1671A490-168679-1 BSMT-NF Total/NA

Water 1671AMB 490-576455/7 Method Blank Total/NA

Water 1671ALCS 490-576455/8 Lab Control Sample Total/NA

Water 1671ALCSD 490-576455/9 Lab Control Sample Dup Total/NA


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Lab ChronicleClient: Alpha Analytical Inc TestAmerica Job ID: 490-168679-1Project/Site: L1906007

Client Sample ID: BSMT-NF Lab Sample ID: 490-168679-1Matrix: WaterDate Collected: 02/14/19 12:00

Date Received: 02/19/19 09:05

Analysis 1671A ZXS02/20/19 11:261 TAL NSH576455

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177


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Method SummaryTestAmerica Job ID: 490-168679-1Client: Alpha Analytical Inc


Method Method Description LaboratoryProtocol

EPA1671A Ethanol (GC/FID) TAL NSH

Protocol References:

EPA = US Environmental Protection Agency

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177


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Accreditation/Certification SummaryClient: Alpha Analytical Inc TestAmerica Job ID: 490-168679-1Project/Site: L1906007

Laboratory: TestAmerica NashvilleUnless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.

Authority Program EPA Region Identification Number Expiration Date

California 29389State Program 06-30-19 *

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which

the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

1671A Water Ethanol

Maine State Program 1 TN00032 11-03-19

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which

the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

1671A Water Ethanol


* Accreditation/Certification renewal pending - accreditation/certification considered valid.

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L2019-501

ATTACHMENT E

STREAMSTATS DATABASE EXPORT HOUSATONIC RIVER / MASSDEP

DILUTION FACTOR CONFIRMATION DOCUMENTATION

StreamStats Report: Housatonic River

Basin Characteristics

Parameter Code Parameter Description Value Unit

DRNAREA Area that drains to a point on a stream

185 square miles

BSLDEM250 Mean basin slope computed from 1:250K DEM

6.996 percent

DRFTPERSTR Area of stratified drift per unit of stream length

0.0743 square mile per mile

Region ID: MAWorkspace ID: MA20190225203022365000Clicked Point (Latitude, Longitude): 42.31182, -73.25156Time: 2019-02-25 15:30:37 -0500

Page 2 of 4StreamStats

2/25/2019https://streamstats.usgs.gov/ss/

Parameter Code Parameter Description Value Unit

MAREGION Region of Massachusetts 0 for Eastern 1 for Western

1 dimensionless

Low-Flow Statistics Parameters [Statewide Low Flow WRIR00 4135]

Parameter Code Parameter Name Value Units

Min Limit

Max Limit

DRNAREA Drainage Area 185 square miles 1.61 149

BSLDEM250 Mean Basin Slope from 250K DEM

6.996 percent 0.32 24.6

DRFTPERSTR Stratified Drift per Stream Length

0.0743 square mile per mile

0 1.29

MAREGION Massachusetts Region 1 dimensionless 0 1

Low-Flow Statistics Disclaimers [Statewide Low Flow WRIR00 4135]

One or more of the parameters is outside the suggested range. Estimates were extrapolated with unknown errors

Low-Flow Statistics Flow Report [Statewide Low Flow WRIR00 4135]

Statistic Value Unit

7 Day 2 Year Low Flow 37.8 ft^3/s

7 Day 10 Year Low Flow 22.6 ft^3/s

Low-Flow Statistics Citations

Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S. Geological Survey Water Resources Investigations Report 00-4135, 81 p. (http://pubs.usgs.gov/wri/wri004135/)



USGS Data Disclaimer: Unless otherwise stated, all data, metadata and related materials are considered to

satisfy the quality standards relative to the purpose for which the data were collected. Although these data and

associated metadata have been reviewed for accuracy and completeness and approved for release by the U.S.

Geological Survey (USGS), no warranty expressed or implied is made regarding the display or utility of the data

for other purposes, nor on all computer systems, nor shall the act of distribution constitute any such warranty.

USGS Software Disclaimer: This software has been approved for release by the U.S. Geological Survey (USGS).

Although the software has been subjected to rigorous review, the USGS reserves the right to update the

software as needed pursuant to further analysis and review. No warranty, expressed or implied, is made by the

USGS or the U.S. Government as to the functionality of the software and related material nor shall the fact of

release constitute any such warranty. Furthermore, the software is released on condition that neither the USGS

nor the U.S. Government shall be held liable for any damages resulting from its authorized or unauthorized use.

USGS Product Names Disclaimer: Any use of trade, firm, or product names is for descriptive purposes only and

does not imply endorsement by the U.S. Government.

Application Version: 4.3.0



From: Ruan, Xiaodan (DEP)To: Stapleton, JamieCc: Vakalopoulos, Catherine (DEP)Subject: RE: Housatonic River DF Confirmation RequestDate: Tuesday, March 5, 2019 12:10:05 PM

I can confirm the dilution factor 37.9 is correct.Also we will get back to you on the application and the MCP site either today or tomorrow. Thanks,Xiaodan

From: Stapleton, Jamie [mailto:[email protected]] Sent: Tuesday, March 05, 2019 12:04 PMTo: Ruan, Xiaodan (DEP)Cc: Vakalopoulos, Catherine (DEP)Subject: RE: Housatonic River DF Confirmation Request Yes. I can confirm. Thank you.

From: Ruan, Xiaodan (DEP) <[email protected]> Sent: Tuesday, March 5, 2019 11:53 AMTo: Stapleton, Jamie <[email protected]>Cc: Vakalopoulos, Catherine (DEP) <[email protected]>Subject: RE: Housatonic River DF Confirmation Request Hi Jamie, Could you confirm if the 275 gpm is the maximum flow through the component with the lowest limiting capacity, which would be theworst scenario? Thanks,Xiaodan

From: Stapleton, Jamie [mailto:[email protected]] Sent: Friday, March 01, 2019 9:51 AMTo: Ruan, Xiaodan (DEP)Cc: Vakalopoulos, Catherine (DEP)Subject: RE: Housatonic River DF Confirmation Request Hi Xiaodan, We are proposing to reduce the Design Flow of the system. Could you please verify that at a 275 gpm discharge rate the DF would be37.9? Thank you. -Jamie

DewateringLocation

Receiving Waterbody Lat Long7Q10 (cfs) Treatment Discharge Rate

DilutionFactor

cfs gpm MGD cfs gpm MGD

Eagle Mill Housatonic River 42.311820 -73.251560 22.6 10143.6 14.6 0.61 275.0 0.396 37.9

From: Ruan, Xiaodan (DEP) <[email protected]> Sent: Tuesday, February 26, 2019 4:25 PMTo: Stapleton, Jamie <[email protected]>Cc: Vakalopoulos, Catherine (DEP) <[email protected]>Subject: RE: Housatonic River DF Confirmation Request Thanks for the reply, Jamie.I can confirm that the 7Q10 14.6 MGD and the DF 17.9 are correct.




https://nam01.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.mass.gov%2Ffiles%2Fdocuments%2F2016%2F08%2Fsa%2F14list2_0.pdf&data=02%7C01%7CJStapleton%40trcsolutions.com%7Cd2067841031d4785272708d69c30da22%7C543eaf7b7e0d4076a34d1fc8cc20e5bb%7C0%7C1%7C636868130973923347&sdata=QQ2dUbSk1uqARYY0OBzMIOWmz53b9HPM5DgGqHY5drs%3D&reserved=0

https://nam01.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.mass.gov%2Fhow-to%2Fwm-15-npdes-general-permit-notice-of-intent&data=02%7C01%7CJStapleton%40trcsolutions.com%7Cd2067841031d4785272708d69c30da22%7C543eaf7b7e0d4076a34d1fc8cc20e5bb%7C0%7C1%7C636868130973933355&sdata=rNXnmkFB0OzssG0Kp4%2FrIMDuSMRJsNrMpXkc7b%2BSe3M%3D&reserved=0

https://nam01.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.mass.gov%2Fhow-to%2Fwm-15-npdes-general-permit-notice-of-intent&data=02%7C01%7CJStapleton%40trcsolutions.com%7Cd2067841031d4785272708d69c30da22%7C543eaf7b7e0d4076a34d1fc8cc20e5bb%7C0%7C1%7C636868130973933355&sdata=rNXnmkFB0OzssG0Kp4%2FrIMDuSMRJsNrMpXkc7b%2BSe3M%3D&reserved=0

The Housatonic River is not Outstanding Resource Waters. There are no TMDLs for this river and to see the impairments, go to:https://www.mass.gov/files/documents/2016/08/sa/14list2_0.pdf and look up “MA21-19”. In addition to submitting the NOI to EPA, if this is not currently an MCP site, you will also have to apply with the state (submit same NOI toCathy Vakalopoulos, fill out a transmittal form, and submit a $500 fee unless exempt). Instructions are located here:https://www.mass.gov/how-to/wm-15-npdes-general-permit-notice-of-intent. Please let me know if you have any additional questions. Thanks,Xiaodan

From: Stapleton, Jamie [mailto:[email protected]] Sent: Tuesday, February 26, 2019 2:08 PMTo: Ruan, Xiaodan (DEP)Cc: Vakalopoulos, Catherine (DEP)Subject: RE: Housatonic River DF Confirmation Request HI Xiaodan, Yes. I think we will just need to filter the water through bag filters so we were thinking about having two separate bag filter units in paralleldischarging to a single location.

From: Ruan, Xiaodan (DEP) <[email protected]> Sent: Tuesday, February 26, 2019 2:00 PMTo: Stapleton, Jamie <[email protected]>Cc: Vakalopoulos, Catherine (DEP) <[email protected]>Subject: RE: Housatonic River DF Confirmation Request Hi Jamie, Is the 600 gpm or 0.864 MGD the design flow of the system?The design flow in the RGP is defined as flow though the component in the treatment system with the most restricted flow. Thanks,Xiaodan

From: Vakalopoulos, Catherine (DEP) Sent: Tuesday, February 26, 2019 10:13 AMTo: Ruan, Xiaodan (DEP)Cc: Stapleton, JamieSubject: FW: Housatonic River DF Confirmation Request Hi Xiaodan,Do you have time to look at this today?Thanks,Cathy

Cathy Vakalopoulos, Massachusetts Department of Environmental Protection1 Winter St., Boston, MA 02108, 617-348-4026P Please consider the environment before printing this e-mail

From: Stapleton, Jamie [mailto:[email protected]] Sent: Monday, February 25, 2019 4:50 PMTo: Vakalopoulos, Catherine (DEP)Subject: Housatonic River DF Confirmation Request Hi Cathy, I’m looking at a site where we will be dewatering a mill building basement which was inundated by a recent flood of river water. We wouldlike to have multiple filtration treatment systems discharging up to 600 gpm to return the water to the Housatonic River. Can you confirma 17.9 dilution factor is acceptable based on the attached information? Please let me know if you need additional information. Thank you. -


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L2019-501

ATTACHMENT F

LETTER FROM US FISH & WILDLIFE SERVICE

United States Department of the Interior

FISH AND WILDLIFE SERVICENew England Ecological Services Field Office

70 Commercial Street, Suite 300

Concord, NH 03301-5094

Phone: (603) 223-2541 Fax: (603) 223-0104

http://www.fws.gov/newengland

In Reply Refer To:

Consultation Code: 05E1NE00-2019-SLI-0978

Event Code: 05E1NE00-2019-E-02239

Project Name: Eagle Mills

Subject: List of threatened and endangered species that may occur in your proposed project

location, and/or may be affected by your proposed project

To Whom It May Concern:

The enclosed species list identifies threatened, endangered, proposed and candidate species, as

well as proposed and final designated critical habitat, that may occur within the boundary of your

proposed project and/or may be affected by your proposed project. The species list fulfills the

requirements of the U.S. Fish and Wildlife Service (Service) under section 7(c) of the

Endangered Species Act (Act) of 1973, as amended (16 U.S.C. 1531 et seq.).

New information based on updated surveys, changes in the abundance and distribution of

species, changed habitat conditions, or other factors could change this list. Please feel free to

contact us if you need more current information or assistance regarding the potential impacts to

federally proposed, listed, and candidate species and federally designated and proposed critical

habitat. Please note that under 50 CFR 402.12(e) of the regulations implementing section 7 of the

Act, the accuracy of this species list should be verified after 90 days. This verification can be

completed formally or informally as desired. The Service recommends that verification be

completed by visiting the ECOS-IPaC website at regular intervals during project planning and

implementation for updates to species lists and information. An updated list may be requested

through the ECOS-IPaC system by completing the same process used to receive the enclosed list.

The purpose of the Act is to provide a means whereby threatened and endangered species and the

ecosystems upon which they depend may be conserved. Under sections 7(a)(1) and 7(a)(2) of the

Act and its implementing regulations (50 CFR 402 et seq.), Federal agencies are required to

utilize their authorities to carry out programs for the conservation of threatened and endangered

species and to determine whether projects may affect threatened and endangered species and/or

designated critical habitat.

February 25, 2019

http://www.fws.gov/newengland

02/25/2019 Event Code: 05E1NE00-2019-E-02239 2

A Biological Assessment is required for construction projects (or other undertakings having

similar physical impacts) that are major Federal actions significantly affecting the quality of the

human environment as defined in the National Environmental Policy Act (42 U.S.C. 4332(2)

(c)). For projects other than major construction activities, the Service suggests that a biological

evaluation similar to a Biological Assessment be prepared to determine whether the project may

affect listed or proposed species and/or designated or proposed critical habitat. Recommended

contents of a Biological Assessment are described at 50 CFR 402.12.

If a Federal agency determines, based on the Biological Assessment or biological evaluation, that

listed species and/or designated critical habitat may be affected by the proposed project, the

agency is required to consult with the Service pursuant to 50 CFR 402. In addition, the Service

recommends that candidate species, proposed species and proposed critical habitat be addressed

within the consultation. More information on the regulations and procedures for section 7

consultation, including the role of permit or license applicants, can be found in the "Endangered

Species Consultation Handbook" at:

http://www.fws.gov/endangered/esa-library/pdf/TOC-GLOS.PDF

Please be aware that bald and golden eagles are protected under the Bald and Golden Eagle

Protection Act (16 U.S.C. 668 et seq.), and projects affecting these species may require

development of an eagle conservation plan (http://www.fws.gov/windenergy/

eagle_guidance.html). Additionally, wind energy projects should follow the wind energy

guidelines (http://www.fws.gov/windenergy/) for minimizing impacts to migratory birds and

bats.

Guidance for minimizing impacts to migratory birds for projects including communications

towers (e.g., cellular, digital television, radio, and emergency broadcast) can be found at: http://

www.fws.gov/migratorybirds/CurrentBirdIssues/Hazards/towers/towers.htm; http://

www.towerkill.com; and http://www.fws.gov/migratorybirds/CurrentBirdIssues/Hazards/towers/

comtow.html.

We appreciate your concern for threatened and endangered species. The Service encourages

Federal agencies to include conservation of threatened and endangered species into their project

planning to further the purposes of the Act. Please include the Consultation Tracking Number in

the header of this letter with any request for consultation or correspondence about your project

that you submit to our office.

Attachment(s):

▪ Official Species List

02/25/2019 Event Code: 05E1NE00-2019-E-02239 1

Official Species ListThis list is provided pursuant to Section 7 of the Endangered Species Act, and fulfills the

requirement for Federal agencies to "request of the Secretary of the Interior information whether

any species which is listed or proposed to be listed may be present in the area of a proposed

action".

This species list is provided by:

New England Ecological Services Field Office

70 Commercial Street, Suite 300

Concord, NH 03301-5094

(603) 223-2541

02/25/2019 Event Code: 05E1NE00-2019-E-02239 2

Project SummaryConsultation Code: 05E1NE00-2019-SLI-0978

Event Code: 05E1NE00-2019-E-02239

Project Name: Eagle Mills

Project Type: SPILL / RELEASE

Project Description: Discharge of municipal storm outfall to Housatonic River, Lee, MA

Project Location:

Approximate location of the project can be viewed in Google Maps: https://

www.google.com/maps/place/42.31103726194954N73.25358308851656W

Counties: Berkshire, MA

https://www.google.com/maps/place/42.31103726194954N73.25358308851656W

https://www.google.com/maps/place/42.31103726194954N73.25358308851656W

02/25/2019 Event Code: 05E1NE00-2019-E-02239 3

Endangered Species Act SpeciesThere is a total of 1 threatened, endangered, or candidate species on this species list.

Species on this list should be considered in an effects analysis for your project and could include

species that exist in another geographic area. For example, certain fish may appear on the species

list because a project could affect downstream species.

IPaC does not display listed species or critical habitats under the sole jurisdiction of NOAA

Fisheries , as USFWS does not have the authority to speak on behalf of NOAA and the

Department of Commerce.

See the "Critical habitats" section below for those critical habitats that lie wholly or partially

within your project area under this office's jurisdiction. Please contact the designated FWS office

if you have questions.

1. NOAA Fisheries, also known as the National Marine Fisheries Service (NMFS), is an

office of the National Oceanic and Atmospheric Administration within the Department of

Commerce.

MammalsNAME STATUS

Northern Long-eared Bat Myotis septentrionalisNo critical habitat has been designated for this species.

Species profile: https://ecos.fws.gov/ecp/species/9045

Threatened

Critical habitatsTHERE ARE NO CRITICAL HABITATS WITHIN YOUR PROJECT AREA UNDER THIS OFFICE'S JURISDICTION.

1

https://www.fisheries.noaa.gov/

https://ecos.fws.gov/ecp/species/9045

L2019-501

ATTACHMENT G

MASSACHUSETTS CULTURAL RESOURCES DATABASE SEARCH RESULTS

MACRIS Search ResultsTown(s): Lee; Street No: 73; Street Name: West Center St; Resource Type(s): Area, Building, Burial Ground, Object, Structure; Search Criteria:

LEE.188 Eagle Paper Mill - Smith Paper Company 73 West Center St Lee 1808

Inv. No. Property Name Street Town Year

Thursday, February 28, 2019 1 1Page of

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