predicting replication and planarity of a co2 gas sensor ... · • the curvature change is the...

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Planarity study Procedure Flat plates injection moulded to investigate how processing settings affects curvature The curvature on both sides measured with 3D DIC Surface topography fitted to a polynomial on the form z = ½ c xx x 2 +½c yy y 2 + d, x 2 + y 2 < (25 mm) 2 Three experimental parallels for each setting Injection moulding simulated using Moldflow midplane model Results Simulations show that the main cause of warpage is the slow cooling of the sprue Asymmetric mould temperature makes the part curve towards the warmer side • The curvature change is the same in the x and y directions: Δc xx = Δc yy • The shape of the curvature is affected by processing The curvature was slightly reduced by applying a longer cooling time. Previous work has shown that lower mould temperature and higher holding pressure reduces the curvature. The effects of these changes were not statistically significant in this work. Terje Tofteberg and Erik Andreassen SINTEF Materials and Chemistry, Oslo, Norway Contact: [email protected] Predicting replication and planarity of a CO 2 gas sensor www.sintef.no/mpc Replication of optical grating Good replication achieved • High mould temperature • High injection speed Simulations are performed in two steps • Filling of main geometry in Moldflow • Microscale simulation using Ansys CFX • One way pressure / temperature coupling • Simulations show complete replication Introduction CO 2 concentration, an important indicator for indoor air quality, can be accurately measured using IR spectroscopy. This is implemented in a robust and cost-effective way with the sensor in this study, based on a diffractive optical element (DOE). The sensor, for ventilation-on-demand applications, is developed and commercialised by the Norwegian company OptoSense (www.optosense.com ). The reflective DOE oscillates at 2 Hz with 2° deflections, scanning three selected IR absorption bands per cycle. The oscillation is driven in the same way as a loudspeaker. c xx < 0, c yy < 0 c xx < 0, c yy = 0 c xx < 0, c yy > 0 c xx = 0, c yy > 0 c xx > 0, c yy > 0 The ideal shapes described by the polynomial with given coefficients. Measuring curvature using digital image correlation (DIC) Two cameras shoot the sample from different angles Sample prepared with speckle pattern (white spray paint + dash of black) Software (Vic-3D from LIMESS) calculates the surface topography Resolution (x,y,z) ~ 5 μm + DIC measurements correlates well with white light interferometry (collage of ~100 images). DIC Cross section on shim and moulded parts measured with AFM. 2 μm 5 μm Topography of moulded DOE measured with AFM. Experimental Mould insert made using e-beam lithography followed by nickel electroplating Injection moulding on a Battenfeld EM 50/120 Main material: Lexan OQ 1026, a DVD grade polycarbonate Surface characterisation: AFM, white light interferometry, 3D digital image correlation Fatigue testing Experimental Simulations DIC: Two images from different angles are combined to give a 3D topography image Microscale filling simulations, performed using pressure from a macroscopic simulation. Fatigue life of hinge Structural analysis (FEM) to reduce stress concentration at hinge Constraints: Maintaining a planar DOE surface during bending, and having a good design in terms of processability Fatigue bending testing of the part in the actual application Frequencies: 2 Hz and 20 Hz, temperatures: 23 °C and 50 °C Polycarbonate materials have performed well so far (1.5 · 10 8 cycles) This applies to DVD grades (rather low molecular weight) as well as regular grades Other materials have fractured or are too stiff for the application Residual stresses in PC parts assessed by solvent exposure method No crack formation; indicating no detrimental residual stresses Simulated von Mises stresses at the hinge Maximum stress: 6 MPa, 10% of yield stress ACKNOWLEDGEMENTS Thanks to OptoSense for bringing this interesting case into our project. These activities were funded by the Research Council of Norway and OptoSense. Main objectives Good replication of the diffractive grating High planarity of surface with diffractive grating No fatigue in the hinge throughout product lifetime WLI T nozzle T ejector [K] T nozzle T ejector [K]

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Page 1: Predicting replication and planarity of a CO2 gas sensor ... · • The curvature change is the same in the x and y directions: Δc xx = Δc yy • The shape of the curvature is affected

Planarity studyProcedure

Flat plates injection moulded to investigate how processing settings affects curvatureThe curvature on both sides measured with 3D DICSurface topography fitted to a polynomial on the form

z = ½ cxx x2 + ½ cyy y2 + d, x2 + y2 < (25 mm)2

Three experimental parallels for each setting Injection moulding simulated using Moldflow midplane model

ResultsSimulations show that the main cause of warpage is the slow cooling of the sprueAsymmetric mould temperature makes the part curve towards the warmer side• The curvature change is the same in the x and y directions: Δcxx = Δcyy• The shape of the curvature is affected by processing

The curvature was slightly reduced by applying a longer cooling time. Previous work has shown that lower mould temperature and higher holding pressure reduces the curvature. The effects of these changes were not statistically significant in this work.

Planarity studyProcedure

Flat plates injection moulded to investigate how processing settings affects curvatureThe curvature on both sides measured with 3D DICSurface topography fitted to a polynomial on the form

z = ½ cxx x2 + ½ cyy y2 + d, x2 + y2 < (25 mm)2

Three experimental parallels for each setting Injection moulding simulated using Moldflow midplane model

ResultsSimulations show that the main cause of warpage is the slow cooling of the sprueAsymmetric mould temperature makes the part curve towards the warmer side• The curvature change is the same in the x and y directions: Δcxx = Δcyy• The shape of the curvature is affected by processing

The curvature was slightly reduced by applying a longer cooling time. Previous work has shown that lower mould temperature and higher holding pressure reduces the curvature. The effects of these changes were not statistically significant in this work.

Terje Tofteberg and Erik AndreassenSINTEF Materials and Chemistry, Oslo, NorwayContact: [email protected]

Predicting replication and planarity of a CO2 gas sensor

www.sintef.no/mpc

Replication of optical gratingGood replication achieved • High mould temperature • High injection speedSimulations are performed in two steps• Filling of main geometry in Moldflow• Microscale simulation using Ansys CFX• One way pressure / temperature coupling• Simulations show complete replication

Replication of optical gratingGood replication achieved • High mould temperature • High injection speedSimulations are performed in two steps• Filling of main geometry in Moldflow• Microscale simulation using Ansys CFX• One way pressure / temperature coupling• Simulations show complete replication

IntroductionCO2 concentration, an important indicator for indoor air quality, can be accurately measured using IR spectroscopy. This is implemented in a robust and cost-effective way with the sensor in this study, based on a diffractive optical element (DOE).

The sensor, for ventilation-on-demand applications, is developed and commercialised by the Norwegian company OptoSense (www.optosense.com).

The reflective DOE oscillates at 2 Hz with 2° deflections, scanning three selected IR absorption bands per cycle. The oscillation is driven in the same way as a loudspeaker.

cxx < 0, cyy < 0cxx < 0, cyy = 0cxx < 0, cyy > 0cxx = 0, cyy > 0cxx > 0, cyy > 0

The ideal shapes described by the polynomial with given coefficients.

Measuring curvature using digital image correlation (DIC) Two cameras shoot the sample from different angles Sample prepared with speckle pattern (white spray paint + dash of black)Software (Vic-3D from LIMESS) calculates the surface topographyResolution (x,y,z) ~ 5 µm

Measuring curvature using digital image correlation (DIC) Two cameras shoot the sample from different angles Sample prepared with speckle pattern (white spray paint + dash of black)Software (Vic-3D from LIMESS) calculates the surface topographyResolution (x,y,z) ~ 5 µm

+

DIC measurements correlates well with white light interferometry (collage of ~100 images).

DIC

Cross section on shim and moulded parts measured with AFM.

2 µm

5 µm

Topography of moulded DOE measured with AFM.

ExperimentalMould insert made using e-beam lithography followed by nickel electroplatingInjection moulding on a Battenfeld EM 50/120Main material: Lexan OQ 1026, a DVD grade polycarbonateSurface characterisation: AFM, white light interferometry, 3D digital image correlation Fatigue testing

Experimental Simulations

DIC: Two images from different angles are combined to give a 3D topography image

Microscale filling simulations, performed using pressure from a macroscopic simulation.

Fatigue life of hingeStructural analysis (FEM) to reduce stress concentration at hinge• Constraints: Maintaining a planar DOE surface during bending,

and having a good design in terms of processability

Fatigue bending testing of the part in the actual application• Frequencies: 2 Hz and 20 Hz, temperatures: 23 °C and 50 °C• Polycarbonate materials have performed well so far (1.5 · 108 cycles)• This applies to DVD grades (rather low molecular weight)

as well as regular grades• Other materials have fractured or are too stiff for the application

Residual stresses in PC parts assessed by solvent exposure method• No crack formation; indicating no detrimental residual stresses

Fatigue life of hingeStructural analysis (FEM) to reduce stress concentration at hinge• Constraints: Maintaining a planar DOE surface during bending,

and having a good design in terms of processability

Fatigue bending testing of the part in the actual application• Frequencies: 2 Hz and 20 Hz, temperatures: 23 °C and 50 °C• Polycarbonate materials have performed well so far (1.5 · 108 cycles)• This applies to DVD grades (rather low molecular weight)

as well as regular grades• Other materials have fractured or are too stiff for the application

Residual stresses in PC parts assessed by solvent exposure method• No crack formation; indicating no detrimental residual stresses

Simulated von Mises stresses at the hingeMaximum stress: 6 MPa, 10% of yield stress

ACKNOWLEDGEMENTSThanks to OptoSense for bringing this interesting case into our project.These activities were funded by the Research Council of Norway and OptoSense.

Main objectivesGood replication of the diffractive gratingHigh planarity of surface with diffractive gratingNo fatigue in the hinge throughout product lifetime

WLI

Tnozzle – Tejector [K] Tnozzle – Tejector [K]