field/lab analytical procedures and equipment detail · field/lab analytical procedures and...
TRANSCRIPT
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 1 of 1174
0800257
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Clear Creek Superfund
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
TitrationApparatus
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
TemperatureStabilizedGraphite FurnaceAASpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
IonChromatograph
0800257
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
UNKNOWN
2340
200.7(S)
200.7(W)
200.8(W)
200.9
245.1
300(A)
Unknown
Hardness in Water by EDTATitration
Metals in Soil by ICP-AES
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Metals by TemperatureStabilized GFAA
Mercury in Water by CVAA
Inorganic Anions by IonChromatography
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 2 of 1174
0800257
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Clear Creek Superfund
Status
USEPA, 1993, EPA Contract Laboratory ProgramWater Quality Parameters in Multi-ConcentrationWater, USEPA, CLP_WQP
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1986, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition., USEPA, EPA 530/SW-846
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
IonChromatograph
TitrationApparatus
InductivelyCoupled PlasmaSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Capillary GasChromatographwith MassSpectrophotometer
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
300_M
310.1
6020
7060A
7740
8260A
Determination of Anions byIC
Alkalinity by Titration
Inductively Coupled Plasma- Mass Spec.
Arsenic by GFAA
Selenium in VariousMatrices by GFAA
Volatile Organics in Wasteby CGC/MS
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 3 of 1174
0800597
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Ogden Railyard (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Society for Testing of Materials, 1994,ASTM Standards. Water and EnvironmentalTechnology (II), American Society for Testing andMaterials, Vol 11.02
Hach Chemical Company, 1992, Hach WaterAnalysis Handbook., HACH Chemical Company,2nd Edition
National Institute for Occupational Safety andHealth, 1994, NIOSH Manual of AnalyticalMethods, 4th Edition,, National Institute forOccupational Safety and Health, 4th Edition
USEPA, 1983, Methods for Chemical Analysis of
LaboratoryBalance
Total OrganicCarbon -Coulometry
Spectrophotometer
GasChromatograph
Titration
0800597
0800597
0800597
0800597
0800597
0800597
0800597
APHA
ASTM
HACH
NIOSH
USEPA
1668
OLM04.2 -BNA SI
OLM04.2 -PEST
OLM04.2 -SVOA
TO-14
TO-14 SIM
UNKNOWN
2540-G
D4129
8021
1005
130.2
1668
OLM04.2-BNA SIM
OLM04.2-PEST/PCB
OLM04.2-SVOA
TO-14
TO-14 SIM
UNKNOWN
Total, Fixed and VolatileSolids
Total Carbon and OrganicCarbon in Water
Free Chlorine in Water byDPD
Methylene Chloride byGC/FID
Total Hardness
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 4 of 1174
0800597
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Ogden Railyard (US EPA Region 8)
Status
Water and Wastes, USEPA, EPA 600/4-79-020
USEPA, 19--, CLP SOW for Inorganics Analysis-IHC01_3, USEPA, IHC01_3
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1992, Methods for the Determination ofOrganic Compounds in Drinking Water,Supplement II, USEPA, EPA 600/R-92-129
Apparatus
pH meter
LaboratoryBalance
LaboratoryBalance
LaboratoryBalance
InductivelyCoupled PlasmaCombined withMassSpectrophotome
IonChromatograph
TitrationApparatus
Colorimeter
Spectrophotometer
Total OrganicCarbon - Infra-Red Detector
Capillary GasChromatographwith Mass
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
150.2_M
160.1
160.2
160.3
200.7(W)
300(A)
310.1
353.2
354.1
415.1
524.2
pH in Industrial WasteMaterials
Filterable Residue - TDS
Non-Filterable Residue -TSS
Total Residue
Metals in Water by ICP-AES
Inorganic Anions by IonChromatography
Alkalinity by Titration
Nitrate-Nitrite Nitrogen byColorimetry
Nitrite Nitrogen bySpectophotometry
Total Organic Carbon byCombustion
Purgeable Organics inWater by CGC/MS
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 5 of 1174
0800597
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Ogden Railyard (US EPA Region 8)
Status
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 19--, Guidelines Establishing TestProcedures for the Analysis of Pollutants.,USEPA, 40 CFR Part 136
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
Spectrophotometer
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaCombined withMassSpectrophotome
GC withPhotoionizationDetector
InductivelyCoupled PlasmaSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
6010A
6010B
602
6020
7000A(FLAA)
7000A(GFAA)
7470A
ICP Spectroscopy
Inductively Coupled PlasmaAES
Purgeable Aromatics inWastewater by GC
Inductively Coupled Plasma- Mass Spec.
Atomic Absorption - FLAA
Atomic Absorption - GFAA
Mercury in Liquid Wastes byCVAA
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 6 of 1174
0800597
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Ogden Railyard (US EPA Region 8)
Status
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
Cold VaporAtomicAbsorptionSpectrophotometer
No equipment
GC with FlameIonizationDetector
GC withElectrolyticConductivityDetector
Capillary GCElectron CaptureDetector
Capillary GasChromatographwith MassSpectrophotometer
Capillary GasChromatographwith MassSpectrophotometer
Capillary GasChromatographwith MassSpectrophotometer
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
7471A
8000B
8015B
8080A
8082(W)
8260B
8270C(S)
8270C(W)
Mercury in Solid orSemisolid Waste
Organic Compounds by GasChromatography
Non-Halogenated OrganicsUsing GC/FID
Pesticides and PCBs
PCBs as Aroclors byCapillary Column GC
Volatile Organics byCGC/MS
Semivolatile OrganicCompounds by CGC/MS
Semivolatile OrganicCompounds by CGC/MS
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 7 of 1174
0800597
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Ogden Railyard (US EPA Region 8)
Status
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1986, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition., USEPA, EPA 530/SW-846
USEPA, 1986, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition., USEPA, EPA 530/SW-846
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
No equipment
pH meter
pH meter
Total OrganicCarbon - Infra-Red Detector
LaboratoryBalance
LaboratoryBalance
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
9012A
9040A
9045B
9060
9070
9071A
Total and AmenableCyanide (Auto UV)
pH in Water by ElectrometricMeasurement
Soil and Waste pH
Total Organic Carbon inWater and Waste
Total Recoverable Oil andGrease
Oil and Grease in Sludgeand Sediment
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 8 of 1174
0800650
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
International Smelter (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
LaboratoryBalance
LaboratoryBalance
IonChromatograph
pH meter
TitrationApparatus
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
0800650
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
UNKNOWN
160.1
160.2
300(A)
305.1
310.1
6010B
6020
7470A
7471A
Unknown
Filterable Residue - TDS
Non-Filterable Residue -TSS
Inorganic Anions by IonChromatography
Acidity by Titration with a pHMeter
Alkalinity by Titration
Inductively Coupled PlasmaAES
Inductively Coupled Plasma- Mass Spec.
Mercury in Liquid Wastes byCVAA
Mercury in Solid orSemisolid Waste
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 9 of 1174
0800650
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
International Smelter (US EPA Region 8)
Status
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
pH meter
pH meter
USEPA
USEPA
9040A
9045B
pH in Water by ElectrometricMeasurement
Soil and Waste pH
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 10 of 1174
0800852
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Mystery Bridge Road - US Highway 20
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
Capillary GC withPhotoionizationDetector
Capillary GasChromatographwith MassSpectrophotometer
0800852
USEPA
USEPA
UNKNOWN
8021A(PID)
8260B
Unknown
Halo and Aromatic Volatiles- CGC/PID
Volatile Organics byCGC/MS
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 11 of 1174
0801194
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Summitville Superfund site (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
TitrationApparatus
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
TemperatureStabilizedGraphite FurnaceAASpectrophotometer
0801194
APHA
USEPA
USEPA
USEPA
UNKNOWN
2340
200.7(W)
200.8(W)
200.9
Unknown
Hardness in Water by EDTATitration
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Metals by TemperatureStabilized GFAA
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 12 of 1174
0801417
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Red Mountain Pass Zinc (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801417 UNKNOWN
UnknownActive
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 13 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,
TitrationApparatus
TitrationApparatus
LaboratoryBalance
Flame AtomicAbsorptionSpectrophotometer
No equipment
No equipment
0801478
0801478
0801478
0801478
0801478
APHA
APHA
APHA
APHA
APHA
APHA
200.2
ILM05
ILM05.3
SOLIDCALC
UNKNOWN
2320
2340
2540-G
3500-AG(B)
3500-AL(B)
3500-AS(B)
Cal Gulch Procedure
ILM05
ILM05.3
Cal Gulch Procedure
Unknown
Alkalinity in Water byTitration
Hardness in Water by EDTATitration
Total, Fixed and VolatileSolids
Silver in Water by FLAA orGFAA
Aluminum in Water by FLAAor GFAA
Arsenic in Water by GFAA
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 14 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Water
Flame AtomicAbsorptionSpectrophotometer
No equipment
Flame AtomicAbsorptionSpectrophotometer
No equipment
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Hydride AtomicAbsorptionSpectrophotometer
Spectrophotometer
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
3500-CA(B)
3500-CD(B)
3500-CU(B)
3500-FE(B)
3500-MN(B)
3500-PB(B)
3500-SE(C)
3500-ZN(D)
or HYDAA
Calcium in Water by FLAA
Cadmium in Water byFLAA/GFAA
Copper in Water by FLAA orGFAA
Iron in Water by FLAA orGFAA
Manganese in Water byFLAA or GFAA
Lead in Water by FLAA orGFAA
Selenium in Water byHYDAA
Zinc in Water bySpectrophotometry
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 15 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USDOI, USGS, 19--, Methods for Determinationof Inorganic Substances in Water and FluvialSediments, Book 5, Chapter A1., USDOI, USGS,Book 5, Chapter A1
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
TitrationApparatus
No equipment
LaboratoryBalance
AutoAnalyzer
ConductivityBridge
pH meter
LaboratoryBalance
LaboratoryBalance
InductivelyCoupled PlasmaCombined withMassSpectrophotome
APHA
APHA
APHA
USDOI/USGS
USEPA
USEPA
USEPA
USEPA
USEPA
4500-CL-(B)
4500-CN(C)
4500-SO4(D)
I2700
120.1
150.1
160.1
160.2
200.7(S)
Chloride in Water byTitration- ArgentometricMethod
Cyanide in Water afterDistillation
Sulfate in Water byGravimetric Analysis
Silica in Water byColorimetry
Conductance
pH
Filterable Residue - TDS
Non-Filterable Residue -TSS
Metals in Soil by ICP-AES
Active
Active
Active
Active
Active
Active
Active
Active
Active
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 16 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
InductivelyCoupled PlasmaSpectrophotometer
TemperatureStabilizedGraphite FurnaceAASpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomic
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
200.7(W)
200.8(S)
200.8(W)
200.9
202.1
206.2
213.1
213.2
Metals in Water by ICP-AES
Metals in Wastes by ICP/MS
Metals in Waters by ICP/MS
Metals by TemperatureStabilized GFAA
Aluminum by FLAA
Arsenic by GFAA
Cadmium by FLAA
Cadmium by GFAA
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 17 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
AbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
220.1
220.2
236.1
239.1
239.2
242.1
245.1
Copper by FLAA
Copper by GFAA
Iron by FLAA
Lead by FLAA
Lead by GFAA
Magnesium by FLAA
Mercury in Water by CVAA
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 18 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
IonChromatograph
IonChromatograph
TitrationApparatus
AutoAnalyzer
Colorimeter
Colorimeter
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
272.1
272.2
273.1
289.2
300(A)
300(B)
310.1
325.2
335.4
353.2
Silver by FLAA
Silver by GFAA
Sodium by FLAA
Zinc by GFAA
Inorganic Anions by IonChromatography
Inorganic Anions by IonChromatography
Alkalinity by Titration
Chloride by ColorimetricAnalysis II
Cyanide by Semi-AutomatedColorimetry
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 19 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rd
Colorimeter
Colorimeter
LaboratoryBalance
Turbidimeter
Total OrganicCarbon - Infra-Red Detector
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Graphite FurnaceAtomic
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
365.1
375.2
375.3
375.4
415.1
6010A
6010B
6020
7060A
Nitrate-Nitrite Nitrogen byColorimetry
Phosphorus by Colorimetry
Sulfate in Water byColorimetry
Sulfate by GravimetricDetermination
Sulfate by TurbidimetricDetermination
Total Organic Carbon byCombustion
ICP Spectroscopy
Inductively Coupled PlasmaAES
Inductively Coupled Plasma- Mass Spec.
Arsenic by GFAA
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 20 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
Edition, Final Update II., USEPA, SW-846_II
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1986, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition., USEPA, EPA 530/SW-846
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1992, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update I., USEPA, SW-846_I
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1986, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition., USEPA, EPA 530/SW-846
AbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
pH meter
ConductivityBridge
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
7131A
7211
7421
7471A
7761
9040A
9050
Cadmium by GFAA
Copper by GFAA
Lead by GFAA
Mercury in Solid orSemisolid Waste
Silver by GFAA
pH in Water by ElectrometricMeasurement
Specific Conductance
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 21 of 1174
0801478
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
California Gulch (US EPA Region 8)
Status
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 22 of 1174
0801505
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
French Gulch Superfund site (US EPA Region 8)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
TitrationApparatus
TitrationApparatus
Hydride AtomicAbsorptionSpectrophotometer
ConductivityBridge
pH meter
LaboratoryBalance
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Graphite FurnaceAtomicAbsorption
0801505
APHA
APHA
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
UNKNOWN
2320
2340
3500-SE(C)
120.1
150.1
160.1
200.7(W)
200.8(W)
204.2
Unknown
Alkalinity in Water byTitration
Hardness in Water by EDTATitration
Selenium in Water byHYDAA
Conductance
pH
Filterable Residue - TDS
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Antimony by GFAA
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 23 of 1174
0801505
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
French Gulch Superfund site (US EPA Region 8)
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
Spectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
IonChromatograph
TitrationApparatus
AutoAnalyzer
Colorimeter
Colorimeter
LaboratoryBalance
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
206.2
279.2
300(A)
310.1
325.2
353.2
365.1
375.3
Arsenic by GFAA
Thallium by GFAA
Inorganic Anions by IonChromatography
Alkalinity by Titration
Chloride by ColorimetricAnalysis II
Nitrate-Nitrite Nitrogen byColorimetry
Phosphorus by Colorimetry
Sulfate by GravimetricDetermination
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 24 of 1174
0801600
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Captain Jack Mine (Colorado)
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
TitrationApparatus
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
IonChromatograph
TitrationApparatus
0801600
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
ILM05
2340
200.7(W)
200.8(W)
245.1
300(A)
310.1
ILM05
Hardness in Water by EDTATitration
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Mercury in Water by CVAA
Inorganic Anions by IonChromatography
Alkalinity by Titration
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 25 of 1174
0801695
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: Delta 400 West Plume
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801695 OLM04
OLM04Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 26 of 1174
0801698
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: 3700-3800 West 2100 South Solvent Plume
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801698
0801698
ILM05
OLM04
ILM05
OLM04
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 27 of 1174
0801800
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: Colorado and Evans PCE
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801800 OLC03
OLC03Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 28 of 1174
0801801
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: Fillmore and Cascade PCE Plume
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801801 OLC03
OLC03Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 29 of 1174
0801812
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: Murray Laundry 4200 S State Plume
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801812
0801812
ILM05
OLM04
ILM05
OLM04
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 30 of 1174
0801845
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: 5400 South 3600 West Plume
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801845
0801845
ILM05
OLM04
ILM05
OLM04
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 31 of 1174
0801966
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Region 8 Superfund: Upper Uncompahgre River
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0801966
0801966
ILM05
ILM05.3
ILM05
ILM05.3
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 32 of 1174
081575
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Slide Mine Boulder County Colorado
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
TitrationApparatus
LaboratoryBalance
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
081575
APHA
APHA
USEPA
USEPA
USEPA
USEPA
UNKNOWN
2340
2540-G
200.7(S)
200.7(W)
200.8(W)
7471A
Unknown
Hardness in Water by EDTATitration
Total, Fixed and VolatileSolids
Metals in Soil by ICP-AES
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Mercury in Solid orSemisolid Waste
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 33 of 1174
081577
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Vasquez Blvd and I-70
Status
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
TitrationApparatus
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
Cold VaporAtomicAbsorptionSpectrophotometer
APHA
USEPA
USEPA
USEPA
2340
200.7(W)
200.8(W)
7471A
Hardness in Water by EDTATitration
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Mercury in Solid orSemisolid Waste
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 34 of 1174
081700
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Gilt Edge Mine
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
TitrationApparatus
LaboratoryBalance
LaboratoryBalance
LaboratoryBalance
InductivelyCoupled PlasmaCombined withMassSpectrophotome
IonChromatograph
TitrationApparatus
Colorimeter
Spectrophotometer
081700
081700
APHA
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
ILM05
UNKNOWN
2320
2540-C
160.1
160.2
200.7(W)
300(B)
310.1
353.2
353.3
ILM05
Unknown
Alkalinity in Water byTitration
Total Dissolved Solids inWater
Filterable Residue - TDS
Non-Filterable Residue -TSS
Metals in Water by ICP-AES
Inorganic Anions by IonChromatography
Alkalinity by Titration
Nitrate-Nitrite Nitrogen byColorimetry
Nitrate-Nitrite Nitrogen byCd Reduction
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 35 of 1174
081700
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Gilt Edge Mine
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1994, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, SW-846, 3rdEdition, Final Update II., USEPA, SW-846_II
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating SolidWaste, Physical/Chemical Methods, 3rd Edition,Final Update III., USEPA, SW-846_III
USEPA, 19--, CLP SOW for Inorganics Analysis-LC_INORGANICS, USEPA, LC_INORGANICS
Total OrganicCarbon - Infra-Red Detector
Cold VaporAtomicAbsorptionSpectrophotometer
GC with FlameIonizationDetector
Capillary GasChromatographwith MassSpectrophotometer
Capillary GasChromatographwith MassSpectrophotometer
InductivelyCoupled PlasmaCombined withMassSpectrophotome
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
415.1
7470A
8015B
8260B
8270C(W)
ICP-AES
Total Organic Carbon byCombustion
Mercury in Liquid Wastes byCVAA
Non-Halogenated OrganicsUsing GC/FID
Volatile Organics byCGC/MS
Semivolatile OrganicCompounds by CGC/MS
Inductively Coupled Plasma
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 36 of 1174
0834QB00
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
Cheyenne River
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
0834QB00 UNKNOWN
UnknownActive
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 37 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
US EPA Research and Development, Cincinnati,Ohio, 1991, Test Methods for Escherichia Coli inDrinking Water, US EPA - Federal Register, TestMethod 1104
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
US EPA, 2003, Guidelines Establishing TestProcedures for the Analysis of Pollutants;Analytical Methods for Biological Pollutants inAmbient Water; Final Rule, US EPA FederalRegistry, 40 CFR Part 136
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Hach Chemical Company, 1992, Hach WaterAnalysis Handbook., HACH Chemical Company,2nd Edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Bovee, K.D., and R. Milhous, 1978, HydraulicSimulation in instream flow studies: Theory andTechniques, US Fish and Wildlife Service,Instream Flow Pap #5
Olem, H. and G. Flock, 1990, Lake and Reservoir
11113300
11113300
11113300
11113300
11113300
11113300
11113300
11113300
11113300
11113300
10-510-00-1-A
1104
353(VAR)
ENTEROLERT
HACH10029
HACH 8025
LIMNO QAMANUAL
LLMP-SECCHI
RIVERFLOW
SECCHI
Potassium LACHATMETHOD
Test Methods for E. Coli indrinking Water
NITRATE/NITRITEVARIATION OF EPA 353
ENTEROLERT FORAMBIENT WATERTESTING
m-ColiBlue24
Apparent Color bySpectrophotometer at455nm
Chlorophyll a (PROBE)
LLMP Secchi DiskTransparency
VRAP and RASP method fordetermining river flow
Determining water
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Description
Description
This Broth allows for the simultaneous detection of total coliform bacteria and E. coli within 24 hrs. An enzymatic indicator in the medium causes non-fecaltotal coliform colonies grown on the m-coliBlue24 medium to be red, while the E. coli (fecal coliform) colonies are blue.EPA Approved Method 10029
SCUFA
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 38 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
Restoration Guidance Manual, EPA, 2nd edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1995,Standard Methods for the Examination of Waterand Wastewater, APHA, 19th edition
American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Water
11113300
11113300
11113300
11113300
11113300
11113300
11113300
SECCHI-LLMP
SM 199213.D.3
SM 2320 B
SM 4500-NH3-H
SM 4500-P-F
SM9213.D.3
SM9230.C.2
transparency by Secchi Disk
LLMP Secchi DiskTransparency
E. Coli Counts
Low Alkalinity Titration to pH4.5
NITROGEN, AMMONIUM(NH4) AS NH4
PHOSPHORUS,ORTHOPHOSPHATE AS P
E. Coli Counts
Enterococci
Active
Active
Active
Active
Active
Active
Active
Description 1- The ecoregional character of NH lakes makes using a more dilute acid result in the higher sensitivity required to obtain adequate results. Thus, a titrantof .002N H2SO4 is used instead of the .02N acid of standard method.
2- While lab analysis typically uses a pH meter, for the field we use a pH indicator solution for efficiency unless the water has high organic color. A mixedbromocresol green-methyl red indicator allows for a sharper equivalence point at the lower pH that the test requires. It is greenish-blue at pH 5.2, light blueat pH 5.0, light gray at pH 4.8, and light pink at pH 4.5.Upon special request the protocol can be followed using the Hanna Model HI-9025 pH meter instead of indicator solution. Follow the protocols outlinedbelow but skip step C.2. and substitute pH 4.8 for gray endpoint and pH 4.5 for pink endpoint.
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 39 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Spectrophotometer
Human Eye
Spectrophotometer
Nephelometer
ConductivityBridge
Thermometer
pH meter
11113300
APHA
APHA
APHA
APHA
APHA
APHA
APHA
UNKNOWN
10200-H
2120-B
2120-C
2130
2510
2550
4500-H
Exact field or lab method isunkown
Chlorophyll a-b-cDetermination
Color in Water by VisualComparison
Color in Water bySpectrophotometry
Turbidity in Water
Conductivity in Water
Temperature of Water byThermometer
pH in Water
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 40 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Ion SelectiveElectrode
Colorimeter
AutoAnalyzer
Genericinspection-relatedequipment(egcolor charts)
Genericinspection-relatedequipment(egcolor charts)
Spectrophotometer
Colorimeter
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
4500-NH3(H)
4500-O-G
4500-P-E
4500-P-F
5210-B
5210-C
5910-B
9221-B
Ammonia in Water - FlowInjection Analysis
Total Dissolved Oxygen byMembrane ElectrodeMethod
Phosphorus in Water byColorimetry- Ascorbic AcidMethod
Phosphorus in Water byColorimetry- AutomatedAscorbic Acid Metho
5-Day Biochemical OxygenDemand
Ultimate BiochemicalOxygen Test
UV - Absorbing OrganicCompounds
Standard Total ColiformFermentation Technique,Multi-tube FermentationTechnique
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 41 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1985, Test Method for E. Coli andEnterococci in Water by the Membr. FilterProcedure, Methods 1103.1 and 1106.1, USEPA,EPA 600/4-85-076
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 2002, Method 1600: Enterococci in
Colorimeter
OpticalMicroscope
OpticalMicroscope
FiltrationApparatus
ConductivityBridge
TitrationApparatus
pH meter
LaboratoryBalance
LaboratoryBalance
APHA
APHA
APHA
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
9221-E
9222-B
9222-D
9230-B
1103_1
120.1
130.2
150.1
160.2
160.3
1600
Estimation of Fecal ColiformGroup Density, Multi-tubeFermentation Technique
Standard Total ColiformMembrane Filter Procedure
Fecal Coliform MembraneFilter Procedure
Fecal Streptococcus andEnterococcus, Multi-tubeFermentation Technique
E. coli in Water byMembrane Filtration
Conductance
Total Hardness
pH
Non-Filterable Residue -TSS
Total Residue
Enterococci in Water by
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 42 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)(September 2002), USEPA, EPA 821-R-02-022
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, Supplement I,USEPA, EPA 600-R-94-111
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
Nephelometer
InductivelyCoupled PlasmaCombined withMassSpectrophotome
InductivelyCoupled PlasmaSpectrophotometer
TemperatureStabilizedGraphite FurnaceAASpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomic
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
180.1
200.7(W)
200.8(W)
200.9
202.2
206.2
213.2
Membrane Filtration Usingmembrane-EnterococcusIndoxyl-B-D-Glucoside Agar(mEl)
Turbidity by Nephelometry
Metals in Water by ICP-AES
Metals in Waters by ICP/MS
Metals by TemperatureStabilized GFAA
Aluminum by GFAA
Arsenic by GFAA
Cadmium by GFAA
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 43 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of
AbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite FurnaceAtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
Graphite Furnace
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
215.1
218.1
220.1
236.1
239.2
243.1
249.1
270.2
Calcium by FLAA
Chromium by FLAA
Copper by FLAA
Iron by FLAA
Lead by GFAA
Manganese by FLAA
Nickel by FLAA
Selenium by GFAA
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 44 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
Water and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
AtomicAbsorptionSpectrophotometer
Flame AtomicAbsorptionSpectrophotometer
IonChromatograph
IonChromatograph
TitrationApparatus
AutoAnalyzer
Colorimeter
Ion SelectiveElectrode
Colorimeter
Colorimeter
Spectrophotometer
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
289.1
300(A)
300(B)
310.1
325.2
350.1
350.3
351.2
353.2
365.2
Zinc by FLAA
Inorganic Anions by IonChromatography
Inorganic Anions by IonChromatography
Alkalinity by Titration
Chloride by ColorimetricAnalysis II
Ammonia Nitrogen byColorimetry
Ammonia Nitrogen Using anISE
Total Kjeldahl Nitrogen byColorimetry
Nitrate-Nitrite Nitrogen byColorimetry
Phosphorus by SingleReagent Colorimetry
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 45 of 1174
11113300
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
New Hampshire Dept. of Environmental Services
Status
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis ofWater and Wastes, USEPA, EPA 600/4-79-020
USEPA, 1993, Methods for the Determination ofInorganic Substances in Environmental Samples,USEPA, EPA 600/R-93-100
USEPA, 1992, Methods for the Determination ofOrganic Compounds in Drinking Water,Supplement II, USEPA, EPA 600/R-92-129
Spectrophotometer
Genericinspection-relatedequipment(egcolor charts)
Colorimeter
Capillary GasChromatographwith MassSpectrophotometer
USEPA
USEPA
USEPA
USEPA
365.3
405.1
410.4
524.2
Phosphorus by TwoReagent Colorimetry
5 Day Biochemical OxygenDemand
Chemical Oxygen Demandby Colorimetry
Purgeable Organics inWater by CGC/MS
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 46 of 1174
1111REG1
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
USEPA, Region I
Status
Jack Paar, III, 1998, Fecal Coliform Analysis, U.S.EPA Office of Environmental Measurement andEvaluation, OEME SOP A102
1111REG1 BIOLOGY001
Fecal Coliform AnalysisActive
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 47 of 1174
1117MBR
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
US EPA Region 7
Status
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
R7 AMM - US EPA Region 7 Laboratory, UpdatedAnnually, US EPA Region 7 Laboratory AnalyticalMethods Manual, US EPA Region 7 Laboratory, .
R7 AMM - US EPA Region 7 Laboratory, UpdatedAnnually, US EPA Region 7 Laboratory AnalyticalMethods Manual, US EPA Region 7 Laboratory, .
R7 AMM - US EPA Region 7 Laboratory, UpdatedAnnually, US EPA Region 7 Laboratory AnalyticalMethods Manual, US EPA Region 7 Laboratory, .
R7 AMM - US EPA Region 7 Laboratory, UpdatedAnnually, US EPA Region 7 Laboratory AnalyticalMethods Manual, US EPA Region 7 Laboratory, .
Capillary GC withHigh ResolutionMassSpectrophotometer
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
FM-PH
M1613 REVB
RAFT FISHPARAM
REMAPFIELD PAR
RLABM3230.2
RLABM3121.14D
RLABM3122.3A
RLABM3210.3C
RLABM3240.2E NP
pH of Water by FieldMeasurement
PCDD/PCDF in soil byGC/HRMS
RAFT Fish Field Parameters
REMAP Field Parameters
Extraction and Analysis ofWater, Solids andHazardous Wast forSemivolatile OrganicCompounds
Mercury by AA-SemiAutomated for All Matrices
Analysis of Metals by PEOptima 3000 ICAP
Preparation of Fish Samplesfor Pesticide/PCB Analysis
Organochlorine Pesticidesand PCBs
Active
Active
Active
Active
Active
Active
Active
Active
Active
Description
Description
Description
Analysis of samples for mercury by RLAB Method 3121.14D
Analysis of samples by RLAB Method 3122.3A.
Fish samples are prepared by RLAB Method 3210.3C for analysis by RLAB Method 3240.2E (GC/EC).
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 48 of 1174
1117MBR
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
US EPA Region 7
Status
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS AND
pH meter1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
SOP2336.10
SOP2336.6
SOP2336.7
SOP2336.8
SOP3121.14
SOP3121.21
SOP3122.3
SOP3124.2
SOP3124.3
SOP3132.1
pH Determination Using theFisher Accumet Model 925pH Meter
Conductivity Using a YSIModel 32 Meter
Dissolved OxygenDetermination Using the YSIModel 58 Meter
Determination of WaterHardness: EDTA TitrimetricMethod
Mercury by AA-SemiAutomated for All Matrices
Determination of TraceElements by StabilizedTemperature GraphiteFurnace Atomic Absorption
Analysis of Metals by PEOptima 3000 ICAP
Spectrophotometric Methodfor Hexavalent Chromium inWater
Determination of HexavalentChromium in Soil UsingCapillary Electrophoresis
Automatic Operation forTitration Alkalinity
Active
Active
Active
Active
Active
Active
Active
Active
Active
Active
Description Analysis of samples by RLAB Method 3240.2E, except that a nitrogen phosphorus detector (NPD) is used instead of an electron capture detector (ECD).
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March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 49 of 1174
1117MBR
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
US EPA Region 7
Status
QUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
1117MBR
SOP3133.1
SOP3133.2
SOP3133.5
SOP3135.1
SOP3135.2
SOP3135.4
SOP3135.5
SOP3135.6
SOP3135.7
Nitrogen, Ammonia inAqueous Samples,Colorimetric, AutomatedPhenate
Nitrogen, Nitrate-Nitrite inAqueous SamplesColorimetric, Automated CdReduction
Phosphorous-Ortho inAqueous SamplesColorimetric, Automated,Ascorbic Acid
Automatic Operation forTitrating Chlorine inWater/Sediment
Cyanide, Total andAmenable in AqueousSamples ColorimetricAutomated uv.
pH, Soil
pH Lab, Water
Fluoride
Cyanide, Total & Amenablein Soil SamplesColorimetric, Automated,
Active
Active
Active
Active
Active
Active
Active
Active
Active
-
March 20, 2006 13:58:01Field/Lab Analytical Procedures and Equipment Detail
Page 50 of 1174
1117MBR
ProcedureSource
ProcedureID
ProcedureName Citation Equipment
ComparableNationalProcedure ID
US EPA Region 7
Status
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONS ANDQUALITY ASSURANCE MANUAL, EPA, R7, .
USEPA, REGION 7, ENVIRONMENTALSERVICE