field/lab analytical procedures and equipment summary · october 27, 2008 14:37:36 field/lab...

515
October 27, 2008 14:37:36 Field/Lab Analytical Procedures and Equipment Summary Page 1 of 515 Clear Creek Superfund 200.7(S) 200.7(W) 200.8(W) 200.9 2340 245.1 300(A) 300_M 310.1 6020 7060A 7740 8260A UNKNOWN Procedure Id USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 0800257 Procedure Source Metals in Soil by ICP-AES Metals in Water by ICP-AES Metals in Waters by ICP/MS Metals by Temperature Stabilized GFAA Hardness in Water by EDTA Titration Mercury in Water by CVAA Inorganic Anions by Ion Chromatography Determination of Anions by IC Alkalinity by Titration Inductively Coupled Plasma - Mass Spec. Arsenic by GFAA Selenium in Various Matrices by GFAA Volatile Organics in Waste by CGC/MS Unknown Procedure Name Active Active Active Active Active Active Active Active Active Active Active Active Active Active Status 0800257

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October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 1 of 515

Clear Creek Superfund

200.7(S) 200.7(W) 200.8(W) 200.9 2340 245.1 300(A) 300_M 310.1 6020 7060A 7740 8260A UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 0800257

Procedure Source

Metals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAHardness in Water by EDTA TitrationMercury in Water by CVAAInorganic Anions by Ion ChromatographyDetermination of Anions by ICAlkalinity by TitrationInductively Coupled Plasma - Mass Spec.Arsenic by GFAASelenium in Various Matrices by GFAAVolatile Organics in Waste by CGC/MSUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0800257

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 2 of 515

Ogden Railyard (US EPA Region 8)

1005 130.2 150.2_M 160.1 160.2 160.3 1668 200.7(W) 2540-G 300(A) 310.1 353.2 354.1 415.1 524.2 6010A 6010B 602 6020 7000A(FLAA) 7000A(GFAA) 7470A 7471A 8000B 8015B 8021 8080A 8082(W) 8260B 8270C(S) 8270C(W) 9012A 9040A 9045B 9060 9070 9071A D4129 OLM04.2 -BNA SIOLM04.2 -PEST OLM04.2 -SVOA TO-14 TO-14 SIM UNKNOWN

Procedure Id

NIOSH USEPA USEPA USEPA USEPA USEPA 0800597 USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA HACH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA ASTM 0800597 0800597 0800597 0800597 0800597 0800597

Procedure Source

Methylene Chloride by GC/FIDTotal HardnesspH in Industrial Waste MaterialsFilterable Residue - TDSNon-Filterable Residue - TSSTotal Residue1668Metals in Water by ICP-AESTotal, Fixed and Volatile SolidsInorganic Anions by Ion ChromatographyAlkalinity by TitrationNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryTotal Organic Carbon by CombustionPurgeable Organics in Water by CGC/MSICP SpectroscopyInductively Coupled Plasma AESPurgeable Aromatics in Wastewater by GCInductively Coupled Plasma - Mass Spec.Atomic Absorption - FLAAAtomic Absorption - GFAAMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteOrganic Compounds by Gas ChromatographyNon-Halogenated Organics Using GC/FIDFree Chlorine in Water by DPDPesticides and PCBsPCBs as Aroclors by Capillary Column GCVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSSemivolatile Organic Compounds by CGC/MSTotal and Amenable Cyanide (Auto UV)pH in Water by Electrometric MeasurementSoil and Waste pHTotal Organic Carbon in Water and WasteTotal Recoverable Oil and GreaseOil and Grease in Sludge and SedimentTotal Carbon and Organic Carbon in WaterOLM04.2-BNA SIMOLM04.2-PEST/PCBOLM04.2-SVOATO-14TO-14 SIMUNKNOWN

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0800597

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 3 of 515

International Smelter (US EPA Region 8)

160.1 160.2 300(A) 305.1 310.1 6010B 6020 7470A 7471A 9040A 9045B UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 0800650

Procedure Source

Filterable Residue - TDSNon-Filterable Residue - TSSInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAlkalinity by TitrationInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Mercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WastepH in Water by Electrometric MeasurementSoil and Waste pHUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0800650

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 4 of 515

Mystery Bridge Road - US Highway 20

8021A(PID) 8260B UNKNOWN

Procedure Id

USEPA USEPA 0800852

Procedure Source

Halo and Aromatic Volatiles - CGC/PIDVolatile Organics by CGC/MSUnknown

Procedure Name

ActiveActiveActive

Status0800852

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 5 of 515

Summitville Superfund site (US EPA Region 8)

200.7(W) 200.8(W) 200.9 2340 UNKNOWN

Procedure Id

USEPA USEPA USEPA APHA 0801194

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAHardness in Water by EDTA TitrationUnknown

Procedure Name

ActiveActiveActiveActiveActive

Status0801194

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 6 of 515

Red Mountain Pass Zinc (US EPA Region 8)

UNKNOWN

Procedure Id

0801417

Procedure Source

Unknown

Procedure Name

Active

Status0801417

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 7 of 515

California Gulch (US EPA Region 8)

120.1 150.1 160.1 160.2 200.2 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 202.1 206.2 213.1 213.2 220.1 220.2 2320 2340 236.1 239.1 239.2 242.1 245.1 2540-G 272.1 272.2 273.1 289.2 300(A) 300(B) 310.1 325.2 335.4 3500-AG(B) 3500-AL(B) 3500-AS(B) 3500-CA(B) 3500-CD(B) 3500-CU(B) 3500-FE(B) 3500-MN(B) 3500-PB(B) 3500-SE(C) 3500-ZN(D)

Procedure Id

USEPA USEPA USEPA USEPA 0801478 USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

ConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSCal Gulch ProcedureMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAArsenic by GFAACadmium by FLAACadmium by GFAACopper by FLAACopper by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationIron by FLAALead by FLAALead by GFAAMagnesium by FLAAMercury in Water by CVAATotal, Fixed and Volatile SolidsSilver by FLAASilver by GFAASodium by FLAAZinc by GFAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IICyanide by Semi-Automated ColorimetrySilver in Water by FLAA or GFAAAluminum in Water by FLAA or GFAAArsenic in Water by GFAA or HYDAACalcium in Water by FLAACadmium in Water by FLAA/GFAACopper in Water by FLAA or GFAAIron in Water by FLAA or GFAAManganese in Water by FLAA or GFAALead in Water by FLAA or GFAASelenium in Water by HYDAAZinc in Water by Spectrophotometry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0801478

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 8 of 515

California Gulch (US EPA Region 8)

353.2 365.1 375.2 375.3 375.4 415.1 4500-CL-(B) 4500-CN(C) 4500-SO4(D) 6010A 6010B 6020 7060A 7131A 7211 7421 7471A 7761 9040A 9050 I2700 ILM05 ILM05.3 SOLIDCALC UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USDOI/USGS 0801478 0801478 0801478 0801478

Procedure Source

Nitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetrySulfate in Water by ColorimetrySulfate by Gravimetric DeterminationSulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionChloride in Water by Titration- Argentometric MethodCyanide in Water after DistillationSulfate in Water by Gravimetric AnalysisICP SpectroscopyInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Arsenic by GFAACadmium by GFAACopper by GFAALead by GFAAMercury in Solid or Semisolid WasteSilver by GFAApH in Water by Electrometric MeasurementSpecific ConductanceSilica in Water by ColorimetryILM05ILM05.3Cal Gulch ProcedureUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0801478

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 9 of 515

French Gulch Superfund site (US EPA Region 8)

120.1 150.1 160.1 200.7(W) 200.8(W) 204.2 206.2 2320 2340 279.2 300(A) 310.1 325.2 3500-SE(C) 353.2 365.1 375.3 UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA 0801505

Procedure Source

ConductancepHFilterable Residue - TDSMetals in Water by ICP-AESMetals in Waters by ICP/MSAntimony by GFAAArsenic by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationThallium by GFAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IISelenium in Water by HYDAANitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetrySulfate by Gravimetric DeterminationUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status0801505

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 10 of 515

Captain Jack Mine (Colorado)

200.7(W) 200.8(W) 2340 245.1 300(A) 310.1 ILM05

Procedure Id

USEPA USEPA APHA USEPA USEPA USEPA 0801600

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Water by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationILM05

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status0801600

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 11 of 515

Region 8 Superfund: Delta 400 West Plume

OLM04

Procedure Id

0801695

Procedure Source

OLM04

Procedure Name

Active

Status0801695

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 12 of 515

Region 8 Superfund: 3700-3800 West 2100 South Solvent Plume

ILM05 OLM04

Procedure Id

0801698 0801698

Procedure Source

ILM05OLM04

Procedure Name

ActiveActive

Status0801698

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 13 of 515

Region 8 Superfund: Colorado and Evans PCE

OLC03

Procedure Id

0801800

Procedure Source

OLC03

Procedure Name

Active

Status0801800

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 14 of 515

Region 8 Superfund: Fillmore and Cascade PCE Plume

OLC03

Procedure Id

0801801

Procedure Source

OLC03

Procedure Name

Active

Status0801801

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 15 of 515

Region 8 Superfund: Murray Laundry 4200 S State Plume

ILM05 OLM04

Procedure Id

0801812 0801812

Procedure Source

ILM05OLM04

Procedure Name

ActiveActive

Status0801812

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 16 of 515

Region 8 Superfund: 5400 South 3600 West Plume

ILM05 OLM04

Procedure Id

0801845 0801845

Procedure Source

ILM05OLM04

Procedure Name

ActiveActive

Status0801845

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 17 of 515

Region 8 Superfund: Upper Uncompahgre River

ILM05 ILM05.3

Procedure Id

0801966 0801966

Procedure Source

ILM05ILM05.3

Procedure Name

ActiveActive

Status0801966

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 18 of 515

Slide Mine Boulder County Colorado

200.7(S) 200.7(W) 200.8(W) 2340 2540-G 7471A UNKNOWN

Procedure Id

USEPA USEPA USEPA APHA APHA USEPA 081575

Procedure Source

Metals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationTotal, Fixed and Volatile SolidsMercury in Solid or Semisolid WasteUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status081575

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 19 of 515

Vasquez Blvd and I-70

200.7(W) 200.8(W) 2340 7471A

Procedure Id

USEPA USEPA APHA USEPA

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Solid or Semisolid Waste

Procedure Name

ActiveActiveActiveActive

Status081577

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 20 of 515

Gilt Edge Mine

160.1 160.2 200.7(W) 2320 2540-C 300(B) 310.1 353.2 353.3 415.1 7470A 8015B 8260B 8270C(W) ICP-AES ILM05 UNKNOWN

Procedure Id

USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 081700 081700

Procedure Source

Filterable Residue - TDSNon-Filterable Residue - TSSMetals in Water by ICP-AESAlkalinity in Water by TitrationTotal Dissolved Solids in WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionTotal Organic Carbon by CombustionMercury in Liquid Wastes by CVAANon-Halogenated Organics Using GC/FIDVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSInductively Coupled PlasmaILM05Unknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status081700

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 21 of 515

Cheyenne River

UNKNOWN

Procedure Id

0834QB00

Procedure Source

Unknown

Procedure Name

Active

Status0834QB00

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 22 of 515

New Hampshire Dept. of Environmental Services

10-510-00-1-A 10029

10200-H 1103_1 1104 1104 120.1 130.2 150.1 160.2 160.3 1600

180.1 200 200.7(W) 200.8(W) 200.9 202.2 206.2 2120-B 2120-C 213.2 2130 215.1 218.1 220.1 2320 236.1 239.2 243.1 249.1 2510 2520-B 2540-B 2540-D 2550 270.2 289.1 300(A) 300(B) 310.1 3113-B

Procedure Id

11113300 HACH

APHA USEPA 11113300 USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA

Procedure Source

Potassium LACHAT METHODm-ColiBlue24 Method of the Determination of Total Coliforms and E.coliChlorophyll a-b-c DeterminationE. coli in Water by Membrane FiltrationTest Methods for E. Coli in drinking WaterE. coli in Drinking Water/EC Medium with Mug TubConductanceTotal HardnesspHNon-Filterable Residue - TSSTotal ResidueEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Turbidity by NephelometryMetals by Atomic AbsorptionMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by GFAAArsenic by GFAAColor in Water by Visual ComparisonColor in Water by SpectrophotometryCadmium by GFAATurbidity in WaterCalcium by FLAAChromium by FLAACopper by FLAAAlkalinity in Water by TitrationIron by FLAALead by GFAAManganese by FLAANickel by FLAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Solids Dried 103-105C in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerSelenium by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by GFAA

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11113300

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 23 of 515

New Hampshire Dept. of Environmental Services

325.2 350.1 350.2(C) 350.3 351.2 351.3(A) 351.3(B) 351.3(C) 353(VAR) 353.2 365.2 365.3 405.1 410.4 4110-B 4500-H 4500-NH3(H) 4500-NO3(D) 4500-O-G 4500-P-E 4500-P-F

5210-B 5210-C 524.2 5310-B 5910-B 8025 9056 9213-D 9221-B

9221-E

9222-B 9222-D 9223-B 9230-B

9230-C APHA 3.0 ASTM D6503-99(2DUFOUR MTEC ENTEROLERT HACH 10029

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 11113300 USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA

APHA APHA USEPA APHA APHA HACH USEPA APHA APHA

APHA

APHA APHA APHA APHA

APHA 11113300 11113300 11113300 IDEXX 11113300

Procedure Source

Chloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricNITRATE/NITRITE VARIATION OF EPA 353Nitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent Colorimetry5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryAnions in Water by Ion ChromatographypH in WaterAmmonia in Water - Flow Injection AnalysisNitrate in Water Using an ISETotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMetho5-Day Biochemical Oxygen DemandUltimate Biochemical Oxygen TestPurgeable Organics in Water by CGC/MSTotal Organic Carbon by Combustion-Infrared MethodUV - Absorbing Organic CompoundsColor, APHA Platinum-CobaltAnion Chromatography MethodE. coli methodStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter TechniqueTotal Fecal ColiformStandard Test Method for Enterococci in Water Using EnterolertMembrane filter method for enumerating Escherechia coliEnterolert Quanti-Tray; Multi Tube, Multi Well, for Enterococciim-ColiBlue24

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

Status11113300

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 24 of 515

New Hampshire Dept. of Environmental Services

HACH 8025 LIMNO QA MANUALRIVERFLOW SECCHI SHELLFISH FLOW SM 19 9213.D.3 SM 2320 B SM 4110 A SM 4500-NH3-H SM 4500-P-F SM 5310 A SM 9213.D.3 SM 9230.C.2 UNKNOWN ENTEROLERT

Procedure Id

11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300 11113300

Procedure Source

Apparent Color by Spectrophotometer at 455nmChlorophyll a (PROBE)VRAP and RASP method for determining river flowDetermining water transparency by Secchi DiskShellfish Flow MethodologyE. Coli CountsLow Alkalinity Titration to pH 4.5MetalsNITROGEN, AMMONIUM (NH4) AS NH4PHOSPHORUS, ORTHOPHOSPHATE AS POrganic CarbonE. Coli CountsEnterococciExact field or lab method is unknownENTEROLERT FOR AMBIENT WATER TESTING

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveSusp

Status11113300

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 25 of 515

USEPA, Region I

BIOLOGY001

Procedure Id

1111REG1

Procedure Source

Fecal Coliform Analysis

Procedure Name

Active

Status1111REG1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 26 of 515

US EPA Region 7

6010B 7470A FM-PH M1613 REV B RAFT FISH PARAMREMAP FIELD PARRLAB M3230.2

RLABM3121.14D RLABM3122.3A RLABM3210.3C RLABM3240.2E NPSOP2336.10 SOP2336.6 SOP2336.7 SOP2336.8 SOP3121.14 SOP3121.21

SOP3122.3 SOP3124.2 SOP3124.3

SOP3132.1 SOP3133.1

SOP3133.2

SOP3133.5

SOP3135.1 SOP3135.2

SOP3135.4 SOP3135.5 SOP3135.6 SOP3135.7

SOP3135.8

SOP3142.3 SOP3142.8 SOP3142.9 SOP3152.2 SOP3153.1

Procedure Id

USEPA USEPA 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR

1117MBR 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR 1117MBR

1117MBR 1117MBR 1117MBR

1117MBR 1117MBR

1117MBR

1117MBR

1117MBR 1117MBR

1117MBR 1117MBR 1117MBR 1117MBR

1117MBR

1117MBR 1117MBR 1117MBR 1117MBR 1117MBR

Procedure Source

Inductively Coupled Plasma AESMercury in Liquid Wastes by CVAApH of Water by Field MeasurementPCDD/PCDF in soil by GC/HRMSRAFT Fish Field ParametersREMAP Field ParametersExtraction and Analysis of Water, Solids and Hazardous Wast forSemivolatile Organic CompoundsMercury by AA-Semi Automated for All MatricesAnalysis of Metals by PE Optima 3000 ICAPPreparation of Fish Samples for Pesticide/PCB AnalysisOrganochlorine Pesticides and PCBspH Determination Using the Fisher Accumet Model 925 pH MeterConductivity Using a YSI Model 32 MeterDissolved Oxygen Determination Using the YSI Model 58 MeterDetermination of Water Hardness: EDTA Titrimetric MethodMercury by AA-Semi Automated for All MatricesDetermination of Trace Elements by Stabilized TemperatureGraphite Furnace Atomic AbsorptionAnalysis of Metals by PE Optima 3000 ICAPSpectrophotometric Method for Hexavalent Chromium in WaterDetermination of Hexavalent Chromium in Soil Using CapillaryElectrophoresisAutomatic Operation for Titration AlkalinityNitrogen, Ammonia in Aqueous Samples, Colorimetric, AutomatedPhenateNitrogen, Nitrate-Nitrite in Aqueous Samples Colorimetric,Automated Cd ReductionPhosphorous-Ortho in Aqueous Samples Colorimetric, Automated,Ascorbic AcidAutomatic Operation for Titrating Chlorine in Water/SedimentCyanide, Total and Amenable in Aqueous Samples ColorimetricAutomated uv.pH, SoilpH Lab, WaterFluorideCyanide, Total & Amenable in Soil Samples Colorimetric,Automated, with Manual DigestionSulfide in Aqueous Samples, Automated, Colorimetric, MethyleneBlueNFS - Non-Filterable SolidsTurbidityDetermination of Percent Solids in Soil and Sedimentreserved -------Oil & Grease in Water ?????????Biochemical Oxygen Demand (Total and Carbonaceous) forWastewater

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

ActiveActive

Active

Active

ActiveActive

ActiveActiveActiveActive

Active

ActiveActiveActiveActiveActive

Status1117MBR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 27 of 515

US EPA Region 7

SOP3153.2 SOP3154.1

SOP3161.1A SOP3210.3

SOP3230.1

SOP3230.2 SOP3240.2 SOP3240.4

SOP3240.5

SOP3260.3

SOP4201SO2

Procedure Id

1117MBR 1117MBR

1117MBR 1117MBR

1117MBR

1117MBR 1117MBR 1117MBR

1117MBR

1117MBR

1117MBR

Procedure Source

COD, Water Samples, Test Tube - Colorimetric MethodPhenolics, Total Recoverable Colorimetric, Automated 4-AAP withDistillationChlorophyll AnalysisExtraction of Fish Samples for Pesticide/PCB Analysis & % LipidDeterminationGC/MS Analysis of Volatile Organic Compounds in an AqueousMatrixExtraction and Analysis of Water and Solids for SemivolatileOrganochlorine Pesticides and PCBsDetermination of 1,2-Dibromoethane (EDB) and 1,2-Dibromo-3-Chloropropane (DBCP) by Electron Capture Gas ChromotographyDetermination of Chlorinated Acids in Water by GasChromatography with an Electronic Capture DetectorDetermination of Polycyclic Aromatic Hydrocarbons in DrinkingWater by Liquid-Solid Extraction and HPLCPhenolics, Total Recoverable in Soil??????

Procedure Name

ActiveActive

ActiveActive

Active

ActiveActiveActive

Active

Active

Active

Status1117MBR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 28 of 515

Bureau of Reclamation

10200-H 110.2 1103.1

1106.1

120.1 140.1 150.1 160.1 160.2 180.1 212.3 213.1 213.2 2130 215.1 218.2 220.2 236.1 239.2 242.1 243.1 245.1 2540-G 258.1 273.1 289.1 310.1 3114-B 3114-C 31627 325.2 340.2 350.3 351.2 352.1 353.2 365.2 365.3 375.4 405.1 410.2 415.1

Procedure Id

APHA USEPA USEPA

USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA APHA APHA 1119USBR USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)Enterococci in Water by Membrane Filtration Using membrane-Enterococcus-Esculin Iron Agar (mE-EIA)ConductanceOdor in Water Using a Consistent SeriespHFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryBoron by Colorimetric AnalysisCadmium by FLAACadmium by GFAATurbidity in WaterCalcium by FLAAChromium by GFAACopper by GFAAIron by FLAALead by GFAAMagnesium by FLAAManganese by FLAAMercury in Water by CVAATotal, Fixed and Volatile SolidsPotassium by FLAASodium by FLAAZinc by FLAAAlkalinity by TitrationMetals in Water by Manual HYDAAMetals in Water by Continuous HYDAAE. coli membrane filterChloride by Colorimetric Analysis IIFluoride in Water Using an ISEAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandLow Level Chemical Oxygen DemandTotal Organic Carbon by Combustion

Procedure Name

ActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status1119USBR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 29 of 515

Bureau of Reclamation

9132 9213-D 9222-B 9222-D 9230 C BIOMASS EC I1327 I2700 I3026 P31627 P680 P681 P70301 P80154 P82078 P931 P94 PH

Procedure Id

USEPA 1119USBR APHA APHA 1119USBR 1119USBR 1119USBR USDOI/USGS USDOI/USGS 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR 1119USBR

Procedure Source

Total Coliform by Membrane FilterE. coli membrane filterStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureStreptococcusbiomass dry weightField ECFluoride in Water Using an ISESilica in Water by ColorimetryArsenic, HYAAE coliTOTAL ORGANIC CARBON (TOC)Dissolved Organis CarbonTOTAL SUSPENDED SOLIDS (TSS)Suspended Sediment ConcentrationFIELD TURBIDITYSODIUM ABSORPTION RATIOField Specific ConductanceField pH

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status1119USBR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 30 of 515

Delaware River Basin Commission

10200-H 1106_1 120.1 130.1 130.2 150.1 160.1 160.1_M 160.2 160.2_M 170.1 180.1 2510 2550 300(A) 310.1 350.1 351.2 353.2 353.3 354.1 365.1 365.2 4500-H 4500-O-C 4500-O-G 9222-B 9222-D 9230-C DISCH-INCR GAGEHT

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA 11DELMOD 11DELMOD

Procedure Source

Chlorophyll a-b-c DeterminationEnterococci in Water by Membrane FilterConductanceTotal HardnessTotal HardnesspHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsTemperatureTurbidity by NephelometryConductivity in WaterTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetrypH in WaterTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Membrane Electrode MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueDischarge - Incremental Velocity Area MethodGage height - water surface elevation

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11DELMOD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 31 of 515

Florida Keys National Marine Sanctuary (Florida)

RYAN_RTM2000 SEABIRD_SBE39

Procedure Id

11FLKNMS 11FLKNMS

Procedure Source

Ryan Industries, Inc. RTM 2000 ThermographSea-Bird Electronics, Inc. SBE 39 Thermograph

Procedure Name

ActiveActive

Status11FLKNMS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 32 of 515

National Park Service

10200-H 120.1 150.1 160.1 160.2 160.3 1600

1664 170.1 180.1 200 200.15 200.7(W) 200.8(W) 206.2 208.1 208.2 210.2 2120-B 213.1 213.2 2130 2130-B 215.1 218.2 220.1 2310 2320 236.1 239.1 239.2 242.1 243.1 245.1 2510 2540-C 2540-D 2540-F 258.1 270.2 272.1 272.2 273.1

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Extractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals by Atomic AbsorptionMetals in Water by Nebulization and ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSArsenic by GFAABarium by FLAABarium by GFAABeryllium by GFAAColor in Water by Visual ComparisonCadmium by FLAACadmium by GFAATurbidity in WaterNephelometric MethodCalcium by FLAAChromium by GFAACopper by FLAAAcidity in Water by TitrationAlkalinity in Water by TitrationIron by FLAALead by FLAALead by GFAAMagnesium by FLAAManganese by FLAAMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSettleable Solids in WaterPotassium by FLAASelenium by GFAASilver by FLAASilver by GFAASodium by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 33 of 515

National Park Service

279.2 289.1 300(A) 310.1 3111-B 3111-D 3113-B 3120 325.1 325.2 325.3 340.2 350.1 350.3 351.2 351.3(A) 353.2 353.3 360.1 365.1 365.2 365.3 365.4 370.1 375.2 375.4 405.1 410.4 4110-B 4110-C 445 4500-NH3(F) 4500-NH3(H) 4500-NO2(B) 4500-NO3(D) 4500-NO3(F) 4500-O-C 4500-P-C

4500-P-E 4500-SO4(F) 5210-B 5310-B 5520-B

Procedure Id

USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA APHA APHA

Procedure Source

Thallium by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAMetals in Water by ICPChloride by Colorimetric Analysis IChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryAnions in Water by Ion ChromatographySingle Column Ion ChromatographyIn-Vitro Determination of ChlorophyllAmmonia in Water Using Phenate MethodAmmonia in Water - Flow Injection AnalysisNitrite in Water by ColorimetryNitrate in Water Using an ISENitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Titration- Azide ModificationPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSulfate in Water by Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodOil and Grease by Gravimetric Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 34 of 515

National Park Service

5540-C 6010B 7000A(FLAA) 7470A 8038 8048 8051 8080A 8221 900 9010A(A) 9050A 9060 9221-B

9221-E

9222-B 9222-D 9223-B 9230-B

9230-C ALPO_FE2 B0060 CABR_SBE13DO

CABR_SBE18PH CABR_SBE3TEMP

CABR_SBE4_C-S

CABR_SENSO_P-D

CABR_WET_FL-CHLCACO_10107041A CACO_10107043B CACO_10107061C CACO_10115011F CACO_10511001A CACO_31107041BCCACO_31115011G CACO_ALKPH_TITRCACO_CATIONS CACO_CHLORO_A CACO_DO_WINK_75

Procedure Id

APHA USEPA USEPA USEPA HACH HACH HACH USEPA HACH USEPA USEPA USEPA USEPA APHA

APHA

APHA APHA APHA APHA

APHA 11NPSWRD USDOI/USGS 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Anionic Surfactants in Water as MBASInductively Coupled Plasma AESAtomic Absorption - FLAAMercury in Liquid Wastes by CVAAAmmonia Nitrogen in WaterReactive Phosphorus in WaterSulfate in WaterPesticides and PCBsAlkalinity by Buret TitrationGross Alpha and Beta Activity in WaterTotal and Amenable Cyanides by ColorimetrySpecific ConductanceTotal Organic Carbon in Water and WasteStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter TechniqueFe(II) Modified from L. StookeyFecal Streptococcal Bacteria- Confirmation TestSeabird Model SBE-13 Dissolved Oxygen Sensor Field DissolvedOxygen MeasurementSeabird Model SBE-18 pH Sensor Field pH MeasurementSeabird Model SBE-3 Temperature Sensor Field TemperatureMeasurementSeabird Model SBE-4 Conductivity Sensor Salinity FieldMeasurementSensometrics Model SP91PFS-500A Pressure Sensor Field DensityMeasurementWet Star Fluorometer Chlorophyll Field MeasurementNitrate/Nitrite (Cadmium Reduction Method)Total Nitrogen Inline Persulfate DigestionAmmonium, Phenolate MethodTotal Phosphorus: Acid Persulfate DigestionIC ¿ Anions, Chloride, Sulfates, (rapid determination)Total Nitrogen Nitrates/Nitrites MethodOrthophosphatesKettle Pond Monitoring - pH and Alkalinity TitrationsCations, Atomic Absorption SpectrometrySpectrophotometric Determination of ChlorophyllDO by Winkler Titration in 1975

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActive

ActiveActiveActiveActive

ActiveActive

Active

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 35 of 515

National Park Service

CACO_DO_YSIWINKCACO_FE2+ CACO_LICOR CACO_LVLFROMMSLCACO_PHOTOMETERCACO_WINK_DO COLILERT/2000 CRLA_14C_PHYTO CRLA_AAS_CA CRLA_AAS_MG CRLA_ATITR_CL CRLA_BOF_PLNKTNCRLA_BOF_SVTEMPCRLA_BOTT_PPM CRLA_CCAL_303A

CRLA_CCAL_4034C

CRLA_CCAL_417F CRLA_CCAL_418F CRLA_CCAL_423 CRLA_CCAL_CL CRLA_CCAL_OP1

CRLA_CCAL_OP2

CRLA_CCAL_SIO2 CRLA_CCAL_SM205

CRLA_CCAL_SO4 CRLA_CCAL_TKN1 CRLA_CCAL_TKN2 CRLA_CCAL_TP1

CRLA_CCAL_TP2

CRLA_DETRITUS CRLA_DIL_EVAP CRLA_DIL_NZ CRLA_DIL_WLGAGECRLA_DIL_WT CRLA_DL_CHLRA CRLA_DOLE_FE CRLA_DOLE_SI CRLA_EMSTRIP_PHCRLA_FES_K

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD IDEXX 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

DO by YSI or Winkler TitrationFerrous Iron, Ferrozine MethodLight Transmittance in Water ColumnWell Water Level Measured From Mean Sea LevelProtomatic PhotometerDO by Winkler TitrationColilert Quanti-Tray/2000; MPN - Multi Tube, Multi Well for E.coliPhytoplankton Productivity In Situ with 14CCalcium by Atomic Absorption SpectroscopyMagnesium by Atomic Absorption SpectroscopyChloride by Automated AgNO3 TitrationU.S. BOF Plankton Enumeration at Crater LakeWater Temperature by Schmidt-Vossberg ThermometerBott Primary Production MethodSM 15th Ed Method 303A Flame Atomic Absorption with Perkins-Elmer 5000 SpectrophotometerAlkalinity by Standard Methods 15th Edition Method 403, Procedure4CAmmonia by Standard Methods 15th Edition Method 417FNitrate by Standard Methods 15th Edition Method 418FpH by Standard Method 15th Edition Method 423Chloride Technicon Industrial Method 99-70WOrthophosphate by Standard Methods 15th Edition Method 424FKlett Summerson ColorimeterOrthophosphate by Standard Methods 15th Edition Method 424FMilton Roy 601Silica by Technicon Industrial Method 105-71W/BSpecific Conductance by Standard Methods 15th Edition Method205 Wheatstone BridgeSulfate by Technicon Industrial Method 105-72WTotal Kjeldahl Nitrogen Fisher Electro Model 81 SpectrophotometerTotal Kjeldahl Nitrogen Milton-Roy 601Total Phosphorus by Standard Methods 15th Edition Methods 424Cand 424F Klett Summerson ColorimeterTotal Phosphorus by Standard Methods 15th Edition Methods 424Cand 424F Milton Roy 601Detritus in Sediment DeterminationPan Evaporation on Lake SurfaceWater Temperature by Negretti-Zambra ThermometerCrater Lake 1892-1901 Water Level GageWater Temperature by Thermometer with Thick Glass JacketChlorophyll a Procedure by D. Larson, 1968-69 StudyDole's Procedure for IronDole's Procedure for SilicapH by E.M. Colorphast pH StripsPotassium by Flame Emission Spectroscopy

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActive

Active

ActiveActive

ActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 36 of 515

National Park Service

CRLA_FES_LI CRLA_FES_NA CRLA_HCB_PH CRLA_HOFF_ZOO CRLA_ISE_FL CRLA_JS_PHYTOPLCRLA_JS_ZOOPLNKCRLA_KAHL268_LT

CRLA_LTMP_423 CRLA_MASON_PO4 CRLA_MBSPE_SIO2CRLA_MOSS_EXAM CRLA_PHYTOID CRLA_RRWT_TEMP CRLA_SECCHI_100CRLA_SECCHI_20 CRLA_SECCHI_30 CRLA_SECCHI_40 CRLA_TITR_HCO3 CRLA_TRI_CHLA CRLA_TROUT_ID CRLA_TURB_SO4 CRLA_UTT_PHYT CRLA_VW_CA CRLA_VW_CL CRLA_VW_HCO3 CRLA_VW_MG CRLA_VW_NO3 CRLA_VW_SO4 CRLA_VW_TDS CRLA_WESTON_LT CUPN_909C CUPN_ANC_FIELD CUPN_ATRAZINE CUPN_CHLORELLA CUPN_CHLOR_DNA CUPN_DISCHARGE CUPN_NH4 CUPN_OLDCATIONS

CUVA_AKRON_UNK CUVA_ALKALINITYCUVA_CHLORIDE

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Lithium by Flame Emission SpectroscopySodium by Flame Emission SpectroscopypH Hellige Comparator BlockHoffman Zooplankton Identification and EnumerationFluoride by Orion Ion Specific ElectrodePhytoplankton Identification and Enumeration by John SalinasZooplankton Identification and Enumeration by John SalinasLight Transmissivity Determined by Kahl Model 268-WA310Submarine PhotometerpH by Standard Method 14th Edition Method 423 Altex MeterPhosphate Colorimetric MethodSilica Molybdenum Blue Spectrophotometric ProcedureCrater Lake Deep-water Moss ExaminationPhytoplankton Identification and EnumerationWater Temperature by Reversing Richter-Wiesse ThermometerSecchi Disk-100 cmSecchi Disk-20 cmSecchi Disk-30 cmSecchi Disk-40 cmBicarbonate TitrametricallyChlorophyll a by Trichromatic MethodBul Trout Study Identification and Counting ProcedureSulfate by Turbidimetric ProcedurePhytoplankton EnumerationCalcium TitrationChloride PrecipitationBicarbonate, GravimetricallyMagnesium, GravimetricallyNitrate Phenol-Disulphonic MethodSulfate PrecipitationTotal Dissolved Solids, GravimetricallyLight Transmissivity by Weston Cell Submarine PhotometerCUPN Fecal Coliform Membrane Filter ProcedureCUPN ANC Field Procedure Using Colorimetric TitrationCUPN ImmunoassayCUPN Chlorella Cell DensityCUPN Chlorella DNACUPN Open Flow Determination with Electronic MeterCUPN Ion Chromatograph (non-approved)CUPN Cation analysis from 7-10-2002 through 9-30-2004 (notapproved)Unspecified Procedures for Historical Data by Akron LabAlkalinity Analytical ProcedureChloride Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 37 of 515

National Park Service

CUVA_ECOLI CUVA_FECAL_ODOHCUVA_FECAL_PARKCUVA_HACHHARD GLKN_BCHMK GLKN_HL_DS4X GLKN_MT132 GLKN_MT318 GLKN_MT_SDI12 GLKN_SECHI GLKN_THERM GLKN_TP/TN GLKN_TTUBE GLKN_YSI6820 GRBA_KESTREL GRBA_OAKTON_PH GRCA_CMC_200.15

GRCA_HORNCRFLOWGRPO_APHA_2320MGRPO_EPA300/340GRPO_LEV1_DISCHGRPO_LEV1_TCOLIGRSM_AAS GRSM_ANC GRSM_FLOW_STAGEGRSM_IC_METAL GRSM_LYSM_MEAS

GRSM_NH4 GRSM_PREC_WGHT GRSM_YSI2900 GRYN_150.2 GRYN_180.1 GRYN_2540-E GRYN_360.1 GRYN_FLOW HAFO_PHOSP

I1114 I1187 I1250 I1327 I1472 I1630(W)

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

E. Coli in Water by Membrane FiltrationFecal Coliform by Membrane Filtration by Ohio Dept. of HealthFecal Coliform by Membrane Filtration by Park StaffHardness by Hach Digital Titration CartridgeWater LevelMultiprobe Field Analysis with Hydrolab 4XMultiproe Field Analysis Eureka Manta M09050132Multiprobe Field Analysis with Eureka Manta M080600318Multiprobe Field Analysis with Eureka Manta SDI-12Secchi DiskThermometerAlkaline Persulfate Digestion for Total N and P in WaterTransparency TubeMultiprobe Field Analysis with YSI Model 6820Air Temperature Measured with KestrelPH Testing using either Oakton pH Testr2 and Testr3Metals and Trace Elements by Inductively Coupled Plasma AtomicEmission Spectroscopy-Colorado DOWDischarge Determined at Horn CreekAPHA Standard Method 2320 Modified for Carbonate AlkalinityFluoride by USEPA Method 300 or 340.2Grand Portage N.M. Level 1 DischargeGrand Portage N.M. Level 1 Total Coliform-Presence/AbsenceMetals by atomic absorption spectroscopyANC using Gran TitrationContinuous Insitu Measurement for Flow StageK, Na, Ca, Mg by ICUse Graduated Cylinder to Measure the Amount of Soil WaterCollected During Sampling PeriodIon Chromatograph (non-approved)Weight Collected Precipitation to Compute the Precipitation HeightInsitu Multi-parameter Data Collection Using YSI2900pH According to GranAcid Neutralizing Capacity (ANC) According to GranFixed and Volatile Solids by Greater Yellowstone NetworkOxygen, dissolved, membrane electrodeStream Discharge CalculationPhospate and Total P Determination According to Olsen andSommersBoron in Water by DC Plasma SpectrometryChloride in Water by ColorimetryColor in Water by Visual ComparisonFluoride in Water Using an ISEMetals in Water by ICPPotassium in Water by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 38 of 515

National Park Service

I1750 I1780 I2030 I2057 I2058 I2327 I2522 I2540 I2545(W) I2601 I2700 I3462 I3860 MULT_SSCR_DIC MULT_SSCR_FLOW NGPN_DISCHARGE NGPN_GPSCOMPASSNGPN_METRICTAPENGPN_VISUALEST NGPN_WADINGROD NGPN_WOODDEBRISNPS_A-11 NPS_AA_CATIONS NPS_ACCUAP84 NPS_ACCUPH NPS_AIRTEMP_ANLNPS_ALK_TITRATENPS_AS_504 NPS_BECKMAN_11 NPS_BECKRB4-250NPS_BELFORT_IR NPS_BEUK92_14C NPS_BIGEL52_2H NPS_BROM_TOTALK

NPS_CL97_12/13C

NPS_CLINOMETER NPS_COP93_2H/1HNPS_CORNING4 NPS_CORNING620 NPS_CORNING7_PHNPS_CORNINGCH90NPS_CORNINGCHII

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Residue by Evaporation and GravimetricSpecific ConductanceAlkalinity in Water by TitrationAnions in Water by Ion ChromatographyAnions in Water by Ion ChromatographyFluoride in Water Using an ISEAmmonia Nitrogen in Water by ColorimetryNitrite-Nitrogen in Water by ColorimetryNitrite- Plus Nitrate-Nitrogen in WaterOrthophosphate-Phosphorus by ColorimetrySilica in Water by ColorimetryMercury in Water by CVAANephelometric Turbidity in WaterMulti-Park Dissolved Inorganic Carbon CalculationMulti-Park Colorado River Spring Flow Measurement0.6x Depth Method for Stream DischargeGPS CompassMeter TapeVisual EstimationWading RodLarge Woody Debris TallyPerchlorate Method A-11Cations By Atomic Adsorption SpectroscopyAccumet Model AP84 DO MeterAccumet Model 640A Portable pH MeterAir Temperature Measured with Analog ThermometerAlkalinity by TitrationAmerican Scientific Model 504 Conductivity MeterBeckman Model 11 Temperature-Compensated pH MeterBeckman RB4-250 Conductivity MeterIncident Radiation by Belfort Recording PyrheliometerCarbon 14 Isotope Analysis by Accelerator Mass SpectrometryDeuterium by 1952 Bigeleisen MethodTotal Alkalinity-Colorimetrically, by Bromcresol Green-Methyl RedIndicatorCarbon Isotope Analysis by Isotopic Ratio Mass SpectrometricTechniqueClinometerHydrogen Isotope Ratio by Hydrogen Equilibration TechniqueCorning Model 4 Temperature/pH MeterCorning Model 620 pH MeterCorning Model 7 pH meterCorning Checkmate 90Corning Checkmate II Handheld Analysis System

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 39 of 515

National Park Service

NPS_DEN1921_SP NPS_DENBRD NPS_DENSIOMETERNPS_DUGAN85_18ONPS_DWV_FLOW

NPS_EPA79_URAN NPS_EPADWR76RAD

NPS_EPA_RBP2 NPS_EPS53_O18

NPS_EVAP180_TDSNPS_EXT341450P NPS_FIELD_WTEMPNPS_FISH152 NPS_FLOAT_FLOW NPS_FLOAT_VEL NPS_FLOWPROBE NPS_FLOW_USGS NPS_FLUME_FLOW NPS_GCA_87/86SRNPS_GENOC2030 NPS_GLOBALFLOW NPS_GS-2175FLOWNPS_GS2175-82FL

NPS_GS2175-82PYNPS_GS2175-82VLNPS_GS79-101_IC

NPS_GS93-638

NPS_GS94-358TRA

NPS_GS95-426A

NPS_GSTWRI79ALKNPS_GSTWRI83DOC

NPS_GSTWRI97AIRNPS_GSTWRI97ALK

NPS_GSTWRI97CO3NPS_GSTWRI97HCONPS_GSTWRI97SPC

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Soluble Phosphorus Method of DenigesTerrestrial Vegetation Density Measurement with Density BoardCanopy Coverage by Convex Spherical Densiometer MeasurementOxygen Isotopes-Guanidine Hydrochloride MethodFlow Calculated with Measurements of Depth, Width and Velocity ofStreamUranium Disequilibrium AnalysisGross Alpha and Gross Beta Radioactivity by Gas-ProportionalCounterEPA Rapid Bioassessment Protocol Second EditionOxygen Isotope Ratio by Carbon Dioxide Equilibration Technique,Epstein and Mayeda,1953Total Dissolved Solids By Evaporation At 180 Degrees CentigradeExtech 341450P Oyster pH/Temperature/Conductivity MeterField Measurement of Water Temperature by ThermometerFisher Model 152 Conductivity MeterDischarge Determined by Float MethodStream Velocity Approximated by Float MethodFlow Probe Hand-held FlowmeterInstantaneous Discharge from Nearby USGS Stream Flow GageDischarge Determined by FlumeStrontium Isotope Analysis by Solid Source Mass SpectrometryStream Velocity by General Oceanics Model 2030 Flow MeterDischarge Determined by Global Flow MeterUSGS/Rantz Method for Stream Discharge MeasurementDischarge Determined by Portable Flume, 1982 U.S. GeologicalSurvey Water-Supply Paper 2175Discharge Determined by Pygmy MeterDischarge Determined by VolumeSelected Anions in Water by Ion Chromatography-USGS WRI No.79-101.Automated Colorimetric Method for NO3+NO2, Nitrite, Ammonium,and Orthophosphate Ions, USGS Open-File Report 93¿638Trace Elements by Inductively Coupled Plasma-Mass Spectrometer,USGS Open-File Report No. 94-358Determination of Dissolved Chloride, Nitrate, and Sulfate by IonChromatography, USGS Open-File Report No. 95-426ATotal Alkalinity by Automated Gran Titration USGS TWRI 1979Dissolved Organic Carbon by Infrared AbsorptionSpectrophotometry USGS TWRI 1983Air Temperature by Thermometer USGS TWRI 1997Field Alkalinity Determined with pH meter and Alkalinity Kit USGSTWRI 1997Dissolved Carbonate Determined by Titrimetry USGS TWRI 1997Dissolved Bicarbonate Determined by Titrimetry USGS TWRI 1997Specific Conductance USGS TWRI 1997

Procedure Name

ActiveActiveActiveActiveActive

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Active

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Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 40 of 515

National Park Service

NPS_GSTWRI97_DONPS_GSTWRI97_PHNPS_GSTWRI97_WTNPS_GWFM-FP101 NPS_HACH150 NPS_HACH16046 NPS_HACH175 NPS_HACH2010DR NPS_HACH2100P NPS_HACH700IRONNPS_HACH8203 NPS_HACH8203ED3NPS_HACH8213 NPS_HACH8P NPS_HACHPOK_NO3NPS_HACHPOK_PO4NPS_HACH_16900 NPS_HACH_8171 NPS_HACH_AL36DTNPS_HACH_ALK NPS_HACH_EC10 NPS_HACH_ONEPH NPS_HACH_SPCTRO

NPS_HANNPHEP1 NPS_HAN_8314_PHNPS_HAN_DISTWPI

NPS_HI8733 NPS_HI991300 NPS_HNDHLD_TEMPNPS_HOBOUNKN NPS_HORIBA_U-10NPS_HYDRLAB4000NPS_HYDRLAB_DS4NPS_HYDRLAB_MS NPS_HYDRLAB_UNKNPS_HYDROLA_H2ONPS_HYDR_M&D_4ANPS_HYDSCOUT2 NPS_HYD_H2O_SC2NPS_ICP_METALS NPS_INS98_DD NPS_INSITU_TROL

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Dissolved Oxygen USGS TWRI 1997pH by pH Meter USGS TWRI 1997Water Temperature by Thermometer USGS TWRI 1997Global Water Flow Meter FP101Hach Model 150 Conductivity MeterHach Model 16046 Portable Dissolved Oxygen MeterHach Model 175 DO MeterHach DR2010 SpectrophotometerHach Model 2100P Portable TurbidimeterIron by Hach DR/700 Portable ColorimeterHach Alkalinity Method 8203 Water Analysis HandbookHach Alkalinity Method 8203, 3rd Edition,1997 WAHHach Total Hardness Method 8213Hach Model 8P Chloride Test KitNitrate by Hach Pocket ColorimeterPhosphate by Hach Pocket ColorimeterHach Digital Titrator Model 16900Nitrate-Hach Method 8171, Cadmium Reduction MethodHACH Model AL-36DT Water Chemistry KitUnspecified Hach Alkalinity KitHach Model EC10 pH MeterHach Model One pH MeterHach Kit with spectrophotometer, unknown model or instrumentnumberHanna Model pHep1 Pocket-Sized pH MeterHanna Instruments HI 8314 Membrane pH MeterHanna Instruments DiST Wpi Handheld Meter for Total DissolvedSolidsHanna Specific Conductance Meter Model # HI8733Hanna Multi-probe Meter Model # HI991300Hand-Held ThermometerOnset HOBO Temperature Data LoggerHoriba U-10 Water CheckerHydrolab Probe Model 4000Hydrolab DataSonde 4 Data Logger ProbesHydrolab MiniSonde Data Logger ProbesHydrolab Probe-Unknown ModelHydrolab H2OHydrolab MiniSonde 4a or Hydrolab DataSonde 4aHydrolab Scout 2 ProbeHydrolab H2O DataSonde and Scout 2 Display UnitMetals by Unknown ICP ProcedureINSTAAR Hydrogen Isotope AnalysisIn-Situ Inc Troll Multi-parameter Water Quality Instrument, UnknownModel Number

Procedure Name

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ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 41 of 515

National Park Service

NPS_INTROLL9000NPS_INVERTS NPS_KEND98_3H NPS_KENDALL85_DNPS_KESTREL4000NPS_KL1954_3H NPS_LACHAT

NPS_LACHAT_8000NPS_LAMOPH NPS_LAMOT4491DRNPS_LAMOT4503DRNPS_LAMOT4533DRNPS_LAMOT4824DR

NPS_LAMOT7297DR

NPS_LAMOTTE3119NPS_LAMOTTE4456NPS_LAMOTTE4463NPS_LAMOTTE4795NPS_LAMOTTE7414NPS_LAM_DHA3000NPS_LAM_SC26617NPS_LAM_SMARTC2NPS_LAWR130TUBE

NPS_LEGACY NPS_LICOR1800UWNPS_LORENZEN NPS_LSC_TRITIUMNPS_MARSHMCBIRNNPS_MAR_201_FLONPS_MAR_FLO2000NPS_METERUNKN NPS_MYRON532T2 NPS_NURE_LA1

NPS_NURE_LA2

NPS_NURE_LA3

NPS_NURE_LA4

NPS_NURE_LA5

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD

Procedure Source

In-Situ TROLL 9000 Multi-Parameter Water Quality MonitorInvertebrate Sample ProcessingTritium by Liquid Scintillation Counting TechniqueHydrogen Isotopes by Zinc Reducing AgentKestrel 4000 Pocket Weather TrackerAnalytical Procedure for TritiumLachat AutoAnalyzer for Colorimetric Determination of DissolvedInorganic NutrientsLachat Flow Injection Machine - QuickChem 8000LaMotte Colorimetric pHLaMotte Alkalinity Test Kit 4491-DRLaMotte Chloride Test Kit #4503-DR Model PSC-DRLaMotte Total Alkalinity Test Kit #4533-DR Model WT-MP-DRLaMotte Total Hardness/ Calcium Hardness/Magnesium HardnessKit # 4824-DR-LT Model PHT-CM-DR-LTLaMotte Carbon Dioxide Test Kit #7297-DR Model PCO-DR(Incremental Titration)LaMotte Phosphate/Nitrate Test Kit #3119 Model NPLLaMotte Sulfide Test Kit #4456 PSILaMotte Silica Test Kit #4463 Model PSILaMotte Ammonia Test Kit #4795 Model PAN (Colorimetric)LaMotte Dissolved Oxygen Test Kit #7414 Model EDOLaMotte DHA-3000 Digital pH MeterLaMotte Smart Colorimeter #26617LaMotte Smart 2 ColorimeterWater Clarity (transparency) by 130cm Lawrence EnterprisesTransparency TubeLEGACYLI-COR Scanning Radiometer Model LI-1800UWChlorophyll a Using an Acetone ExtractTritium with Liquid Scintillation CounterMarsh-McBirney Current MeterMarsh McBirney Model 201 Electromagnetic FlowmeterMarsh-McBirney Flo-Mate Model 2000 Portable FlowmeterPortable Meter or Probe (Unknown Model)Myron L Company Model 532T2 DS MeterLos Alamos Delayed-Neutron Counting Analysis of Sediments forUraniumLos Alamos Procedure LA2, Energy Dispersive X-Ray FluorescenceAnalysis of Sediments, Selected ParametersLos Alamos Procedure LA3, Energy Dispersive X-Ray FluorescenceAnalysis of Sediments, Selected ParametersLos Alamos Arc-Source Emission Spectrography Analysis ofSediments for Be and LiLos Alamos Neutron Activation Analysis of Sediments for Selectedparameters

Procedure Name

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ActiveActiveActiveActiveActiveActiveActiveActiveActive

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Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 42 of 515

National Park Service

NPS_NURE_LA6-DN

NPS_NURE_LA6-FLNPS_NURE_LA7

NPS_NURE_LAF NPS_NURE_LAPHF NPS_NURE_LASCS

NPS_NURE_LATEMPNPS_NURE_OR13

NPS_NURE_OR2

NPS_NURE_OR7

NPS_NURE_OR9-FL

NPS_NURE_OR9-MSNPS_NZ_TEMP NPS_OAKPHTESTR3NPS_OAKTON NPS_OAKTON_PH2 NPS_OMEGA_871

NPS_OPTIMA4300

NPS_ORION_105 NPS_ORION_122

NPS_ORION_126 NPS_ORION_210A NPS_ORION_250A NPS_ORION_710A NPS_ORION_PH NPS_PE3300DV

NPS_PER_MPP NPS_PRICETYPEAANPS_PYGMY_FLOW NPS_ROB1930_OP NPS_ROTH94_MERC

NPS_SBE19_C-T-D

NPS_SECCHI100CMNPS_SECCHI20CM

Procedure Id

11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD

Procedure Source

Los Alamos Delayed-Neutron Counting Analysis of Waters forUraniumLos Alamos Fluorometry Analysis of Waters for UraniumLos Alamos Plasma-Source Emission Spectrography Analysis ofWaters for Selected ParametersLos Alamos Field Meters for Alaska NURE MonitoringLos Alamos pH Field MeasurementsLos Alamos Procedure to Determine Specific Conductance Valuesin the Field from SamplesLos Alamos Temperature Field MeasurementsOak Ridge Emission Spectrochemical Analysis of Waters forSelected ParametersOak Ridge Neutron Activation Analysis - Neutron Counting ofSediments for UraniumOak Ridge Emission Spectrochemical Analysis of Sediments forSelected ParametersOak Ridge Fluorescence Spectroscopy Analysis of Waters forUraniumOak Ridge Mass Spectrometry Analysis of Waters for UraniumWater Temperature by Deep Sea Negretti-Zambra ThermometerOakton pHTestr3Portable Oakton Probe, unknown model or instrument numberOakton pHTestr 2Temperature by Omega Engineering Model 871 ThermocoupleThermometerInductively Coupled Plasma-Optical Emission Spectroscopy -Optima 4300 DVOrion Model 105Orion Model 122 Temperature-Compensated Specific ConductanceMeterOrion Model 126 Conductivity MeterOrion Model 210A pH MeterOrion Model 250A pH Meter and Orion pH TriodeOrion 710A pH/ISE MeterpH Determined by Unknown Model of Portable Orion pH MeterMajor Constituents by Inductively Coupled Plasma-Atomic EmissionSpectrometry, J.R. Garbarino, 1979Perstorp In-situ Multi-parameter ProbeDischarge Determined with Price Type AA Pygmy MeterDischarge Determined with Pygmy MeterOrganic Phosphorus Method of Robinson and KemmererMercury by Automated Cold-Vapor Atomic FluorescenceSpectrometrySea-Bird Model SBE19 Conductivity, Temperature, and DepthProfilerSecchi Disk Depth with a 100 cm Diameter DiskSecchi Disk Depth with a 20 cm Diameter Disk

Procedure Name

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Active

ActiveActiveActiveActiveActiveActive

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Active

ActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 43 of 515

National Park Service

NPS_SECCHIDISK NPS_SECCHI_12 NPS_SEY1894_CO2NPS_SHMAK_TRAN

NPS_SLTSPK_FLOWNPS_SM14_403_4A

NPS_SM14_WINKDONPS_SM15_303A NPS_SM403_ALK NPS_SM424F_PHOSNPS_SM703_AB NPS_SM705_RA226NPS_SPRINGFLOW NPS_STD_RAIN NPS_SUM_TDS NPS_SWOF_2100 NPS_SWOF_3000 NPS_TAPE_STRWDTNPS_TURN40-100 NPS_TYROSIN8193NPS_USGS-PYGMY NPS_VALDERRAMA

NPS_VEL_FLOW NPS_VISUAL_FLOWNPS_VNOTCH NPS_VOLUME_FLOWNPS_WHTM_CDM300

NPS_WINK1888_DONPS_YSI23200_SCNPS_YSI30_S-C-TNPS_YSI33S-C-T NPS_YSI3800 NPS_YSI43TD NPS_YSI50B NPS_YSI518 NPS_YSI51B NPS_YSI55 NPS_YSI556MPS NPS_YSI57 NPS_YSI58 NPS_YSI6820

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Secchi Disk Depth Readings-Unspecified DetailsSecchi Disk Depth 12 cm DiskCarbon Dioxide by Seyler MethodWater Clarity (Transparency) Measured with a SHMAK HorizontalClarity TubeDischarge Determined by NaCl Salt SpikingAlkalinity by Standard Methods 14th Edition Method 403, Procedure4ADissolved Oxygen Winkler Method-Standard Methods 14th EditionSM 15th Ed Method 303A Flame Atomic Absorption SpectroscopyStandard Methods 403 AlkalinityStandard Methods 424F PhosphateStandard Methods 703 Gross Alpha BetaStandard Methods 705 Radium 226Spring flow measurements using sample container and stopwatchPrecipitation by Standard Rain GaugeTotal Dissolved Solids By Summation Of ConstituentsSwoffer Instruments Model 2100 Series Current Velocity MeterSwoffer Model 3000 FlowmeterStream Width by Tape MeasurementTurner Model 40-100 NephelometerTyrosine Method 8193USGS Flow Measurement with Pygmy Current Meter #229262Simultaneous Analysis of Total Nitrogen and Total Phosphorus inNatural WatersDischarge Determined with Velocity MeasurementDischarge Visual DeterminationDischarge Determined by V-Notch Weir PlateDischarge Determined VolumetricallySpecific Conductance by Whatman CDM 300 Digital ConductivityMeterDissolved Oxygen (DO) by Winkler MethodSpecific Conductance YSI Model 23200-009 Conductivity BridgeYSI Model 30 Conductivity, Salinity and Temperature InstrumentYSI Model 33 Salinity-Conductivity-Temperature MeterYSI Model 3800 Multi-Parameter MeterYSI Model 43TD Tele-ThermistorYSI Portable Dissolved Oxygen MeterYSI Model 518YSI Model 51B DO MeterYSI Model 55 DO MeterYSI Model 556 Multiprobe SystemYSI Model 57 DO MeterYSI Model 58 DO MeterYSI 6820 Multi-parameter Water Quality Sonde

Procedure Name

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Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 44 of 515

National Park Service

NPS_YSI85 NPS_YSI95

NPS_YSIDOUNKNOWNPS_YSI_3403 NPS_YSI_50B NPS_YSI_550 NPS_YSI_TEMPUNKNPS_YSI_UNKN O3100 OZAR_CHLA OZAR_FS OZAR_HACH2100P OZAR_HACH44600 OZAR_HACHALK OZAR_ORION290A OZAR_TEMPAIR OZAR_TN OZAR_YSI550_DO OZAR_YSI55_DO OZAR_YSI63PROBEREDW_RCW_FLOW

REDW_RCW_PRECIP

REDW_RCW_SSD

REDW_RCW_STAGE

ROMO_GERG_GC/MSSHIL_GRUB_INVRTSHIL_GRUB_RGRSN

SHIL_GRUB_TSS USGS_31501 USGS_31625 USGS_31633 USGS_31649 USGS_31673 USGS_AA030 USGS_AA035 USGS_BAROMETER USGS_BECK_PHI10USGS_CALCULATEDUSGS_CL039

Procedure Id

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD USDOI/USGS 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

YSI Model 85 DO, Conductivity, Salinity, Temperature InstrumentYSI Model 95 Handheld Dissolved Oxygen and TemperatureSystemYSI Unknown Model DO MeterYSI 3403 Conductivity CellYSI Model 50B Dissolved Oxygen MeterYSI 550 Dissolved Oxygen MeterYSI Temperature Sensor - Model UnknownPortable YSI Meter-Unknown ModelTotal Organic Carbon in WaterChlorophyll a - Corrected for pheophytin, by FluorometerFecal Streptococcus by Membrane FilterHACH 2100P Turbidity MeterHACH 44600 Meter Specific ConductanceAlkalinity by HACH Model 16900-01 Digital TitratorOrion Model 290A pH and Temperature ProbeAir TemperatureTotal Nitrogen by Second Derivative SpectroscopyYSI Model 550 DO MeterYSI Model 55 DO MeterYSI Model 63 pH, Conductivity, and Temperature ProbeRedwood Parks Monitoring Program-Flow Discharge Calculated byStage-Discharge RelationshipRedwood Parks Monitoring Program-Precipitation from Tipping-Bucket Rain GageRedwood Parks Monitoring Program-Suspended SedimentDischarge CalculationRedwood Parks Monitoring Program-Stage Measurement byPressure TransducerBTEX and PAH Analysis at Texas A&M UniverisityShiloh NMP-UM Macroinvertebrate IdentificationShiloh Branch PDL Results Determined by Regression Analysis withTilghman BranchTotal Suspended Solids (TSS) by Drying OvenTotal coliform, mENDO MF methodFecal coliform, M-FC MF (0.7 micron) methodEscherichia coli, m-TEC MF methodEnterococci, m-E MF methodFecal Streptococci, KF streptococcus MF methodPotassium, wf, direct AASSodium, wf, direct AASUSGS Unspecified BarometerBeckman Phi 10, Electrometric ElectrodeUSGS Calculated from Other CharacteristicsNutrients, LL, wf, color

Procedure Name

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Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 45 of 515

National Park Service

USGS_CL048 USGS_CL050 USGS_CL057 USGS_COLM_DO

USGS_CV014 USGS_EL006 USGS_FECALIND USGS_FLOW_POFLUUSGS_FLOW_RANTZUSGS_FLOW_RODVM

USGS_G0017 USGS_GCM62 USGS_GCM63 USGS_GCM64 USGS_GCM65 USGS_GCM66 USGS_GCM67 USGS_GCM68 USGS_GF075 USGS_GF085 USGS_GF094 USGS_GF095 USGS_GF096 USGS_GF097 USGS_GF098 USGS_GF099 USGS_GF100 USGS_GF101 USGS_GF102 USGS_GF103 USGS_GRAVI USGS_HACH_KIT USGS_I-2063 USGS_I-2477 USGS_I-2587 USGS_I-2610 USGS_I-2668 USGS_I-2781 USGS_I-4515 USGS_I-4602 USGS_I-4610 USGS_KJ002

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Nutrients, Cd reduct, colorNutrients, low, Cd reduct, colorNutrients, lowlvl, phosphomolybdMultiple Dissolved Oxygen Procedures Used at Colorado N.M. byUSGSMercury, wf, CV-AFSpH, lab, auto glass electrodeUSGS Unspecified Fecal Indicator Bacteria Procedure90-Degree-Notch Portable FlumeMeasuring Discharge According to Rantz and OthersUSGS Flow Determination by Wading Rod and Pygmy or Price AAVelocity MeterNo information exists for methodVOCs, water, GC-MSVOCs, water, GC-MSVOCs, water, GC-MSVOCs, water, GC-MSVOC, wu, acidified, GCMSVOC, wu, censor at <0.2, GCMSVOC, wu, censor at <0.2, GCMSChromium, wf, GFAASArsenic, wf, GFAASChromium, wu, GFAASMolybdenum, wu, GFAASArsenic, wu, GFAASCadmium, wu, GF-AASCobalt, wu, GF-AASCopper, wu, GF-AASLead, wu, GF-AASNickel, wu, GF-AASSelenium, wu, GFAAS (NWQL)Silver, wu, GF-AASUSGS GravimetricHach Alkalinity Kit, Titration with H2SO4Graphite Furnace Atomic AbsorptionInductively Coupled Plasma/Mass SpectrometryElectrometric ElectrodeColorimetry, Automated-Segmented Flow, Microkjeldahl DigestionGraphite Furnace Atomic AbosrptionElectrometric Wheatstone BridgeSemi Automated Block Digestor ColorimetricColorimetry, Automated-Segmented Flow, PhosphomolybdateColorimetry, Automated-Segmented Flow, Microkjeldahl DigestionNutrients, wf, Kjeldahl, color

Procedure Name

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Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 46 of 515

National Park Service

USGS_KJ005 USGS_KJ008 USGS_KJ009 USGS_LSC04 USGS_MEMFILT USGS_MULTIPARM USGS_O-4127-96 USGS_PARSHALL USGS_PHOS3 USGS_PHOS6 USGS_PLA06 USGS_PLA07 USGS_PLA15 USGS_PLM30 USGS_PLM40 USGS_PLM43 USGS_SD_ELISA USGS_SPIRIT_TH USGS_SSC_GUY USGS_THERM_STD USGS_TT013 USGS_TT017 USGS_TT019 USGS_TT023 USGS_TURBID USGS_UNKNOWN USGS_UNSPEC

USGS_WHT03 USGS_WTW_LF91

USGS_YSI_UNSPECWABA_FISHID WABA_FLIES WABA_MACROINV WABA_SUSSED WRST_MAC_ACTISCWRST_SM16_413C

Procedure Id

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD

11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD 11NPSWRD

Procedure Source

Nutrients, wf, Kjeldahl, colorNutrients, acidified, KjeldahlPhosphorus, wu, microKJ ASF, H+Tritium, LL, wu,enrich liq scintUSGS Membrane Filtration Method for Fecal Indicator BacteriaUSGS Unspecified Multiparameter Meter Field MeasurementVolatile Organic Compounds in Water by GC-MSParshall Flume for Measuring DischargeLaser phosphorim, ext (Eberline)Uranium, wf, ext phosphorescenceTrace elements, wf, ICP/T (Ocala)Trace elements, wu,ICP/T (Ocala)Metals, wu, ICP-AESUSGS Trace elements,wf, ICP-MS(Ocala)Metals, water, ICP-MSMetals, wf, ICP-MSEnzyme Linked Immunosorbent Assay TechniqueUSGS Spirit Filled ThermometerSuspended Sediment Concentration Using the Filtration MethodUSGS Standard Glass ThermometerUSGS Alkalinity, wf, field, incrementBicarbonate, wf, field, incremUSGS Carbonate, wf, field, incrementHydroxide, wf, field, incremUSGS Unspecified Turbidimeter Used in the FieldUSGS Unknown/Unspecified Analytical ProcedureUnspecified USGS Lab Analytical Procedures at NWQL FollowingStandard ProtocolsSpecific cond, lab, autom bridgeWTW Model LF91 Temperature-Compensated SpecificConductance MeterYSI Unspecified Scientific Dissolved Oxygen MeterOklahoma Biological Survey Field Fish IdentificationMayfly, Stonefly, and Caddisfly IdentificationOklahoma Biological Survey Macroinvertebrate IdentificationSuspended Sediment determined by Filtering, Ashing, and WeighingActivon Model PTI-10 Specific Conductance MeterFluoride by SPADNS Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActive

Status11NPSWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 47 of 515

U. S. EPA Region 9 (Monitoring & Assessment Office)

LEGACY ORG-001

Procedure Id

11TOX09 11TOX09

Procedure Source

Legacy STORET Analytical Proceduresfield measurements

Procedure Name

ActiveActive

Status11TOX09

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 48 of 515

Division of Water and Waste Management

1 1103_1 120.1 120.1_M 130.1 130.2 150.1 160.1 160.2 160.2_M 160.3 1652 170.1 200.7(W) 200.8(S) 200.8(W) 200.9 202.1 202.2 204.2 206.2 208.1 210.1 213.1 213.2 215.1 218.1 219.2 220.1 220.2 2310 2320 2340 236.1 236.1_M 236.2 239.1 239.2 242.1 243.1 245.1 245.2 246.1 249.1

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Beta Activity in Airborne ParticulatesE. coli in Water by Membrane FiltrationConductanceConductivity in Industrial WasteTotal HardnessTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsTotal ResidueOil and GreaseTemperatureMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAAluminum by GFAAAntimony by GFAAArsenic by GFAABarium by FLAABeryllium by FLAACadmium by FLAACadmium by GFAACalcium by FLAAChromium by FLAACobalt by GFAACopper by FLAACopper by GFAAAcidity in Water by TitrationAlkalinity in Water by TitrationHardness in Water by EDTA TitrationIron by FLAAIron by FLAAIron by GFAALead by FLAALead by GFAAMagnesium by FLAAManganese by FLAAMercury in Water by CVAAMercury by CVAAMolybdenum by FLAANickel by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status211WVOWR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 49 of 515

Division of Water and Waste Management

2510 2510 2530-B 2540 2540-D 2550 270.2 270.2_M 270.3 272.1 272.2 279.2 282.2 283.2 286.2 289.1 300(A) 300(B) 305.1 305.2 310.1 3112-B 325.2 325.3 335.3 335.4 340.1 340.2 340.3 350.1 350.2(C) 3500-CR(C) 3500-CR(D) 351.2 351.3(A) 351.3(B) 353.2 353.3 354.1 365.1 365.2 365.4 375.2 375.4

Procedure Id

NIOSH APHA APHA NIOSH APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

1-Octanethiol by GC/FPDConductivity in WaterParticulate Floatables in WaterOrganics by HPLC/UVTotal Suspended Solids in WaterTemperature of Water by ThermometerSelenium by GFAASelenium by GFAASelenium by FLAASilver by FLAASilver by GFAAThallium by GFAATin by GFAATitanium by GFAAVanadium by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAcidity by Titration Using a pH MeterAlkalinity by TitrationMercury in Water by CVAAChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryTotal Fluoride by Colorimetric AnalysisFluoride in Water Using an ISEFluoride in Water by ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationChromium in Water by ICPTotal Hexavalent Chromium in WaterTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by ColorimetrySulfate by Turbidimetric Determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status211WVOWR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 50 of 515

Division of Water and Waste Management

405.1 410.1 410.2 410.4 415.1 415.2 425.1 4500-CL-(B) 4500-CN(D) 4500-H 4500-NH3(E) 4500-NO3(B) 4500-NO3(D) 4500-NO3(E) 4500-NOR(B) 4500-NOR(C) 4500-O-G 4500-P-E 5310-B 5310-C 5310-D 6010B 8260B 8270B(W) 8270C(S) 8270C(W) 9040A 9060 9221-E

9222-D 9223-B NITROSUM UNAMM1 WILDLIFE WVFLOW01 WVFLOW02 WVVISUAL01

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

APHA APHA 211WVOWR 211WVOWR 211WVOWR 211WVOWR 211WVOWR 211WVOWR

Procedure Source

5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandLow Level Chemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterMethylene Blue Active SubstancesChloride in Water by Titration- Argentometric MethodCyanide in Water by TitrationpH in WaterAmmonia in Water by Selective Electrode Method (Known Addition)Nitrate in Water by Ultraviolet SpectrophotometryNitrate in Water Using an ISENitrate in Water- Cadmium ReductionTotal Kjeldahl Nitrogen in WaterTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodTotal Organic Carbon in Water- Wet-Oxidation MethodInductively Coupled Plasma AESVolatile Organics by CGC/MSSemivolatile Organics in Water by GC/MSSemivolatile Organic Compounds by CGC/MSSemivolatile Organic Compounds by CGC/MSpH in Water by Electrometric MeasurementTotal Organic Carbon in Water and WasteEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupSum of NO3NO2 and TKNCalculate un-Ionized AmmoniaNotes & Observations on WildlifeField Measurements of Stream FlowStreamflow Data taken from U.S. Geological Survey Gaging SitesVisual Sightings of Stream Conditions

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

Status211WVOWR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 51 of 515

Commonwealth Northern Mariana Islands

150.1 1600

180.1 305.1 305.2 352.1 365.1 4500-P-E 9132 9200 9230-B

9250 CNMI-001 CNMI-002 CNMI-003 CNMI-004 CNMI-005 ENTEROLERT ENTEROLERT2000

Procedure Id

USEPA USEPA

USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA

USEPA 21AQ 21AQ 21AQ 21AQ 21AQ IDEXX IDEXX

Procedure Source

pHEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Turbidity by NephelometryAcidity by Titration with a pH MeterAcidity by Titration Using a pH MeterNitrate Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Coliform by Membrane FilterNitrate in Water by SpectrophotometryFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueChloride by Automated ColorimetrySalinityDissolved OxygenWaether measurementsTide and Sea StageWater temperatureEnterolert Quanti-Tray; Multi Tube, Multi Well, for EnterococciiEnterolert Quanti-Tray/2000; Multi Tube, Multi Well, for Enterococcii

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

Status21AQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 52 of 515

Arizona Department of Environmental Quality

10200-H 120.1 130.2 150.1 160.1 160.2 160.3 160.4 1603

1631 1638 170.1 180.1 200.7(W) 200.8(W) 200.9 202.1 204.2 206.2 208.1 208.1_M 210.2 213.1 213.2 215.1 215.1_M 218.1 218.2 219.1 220.1 220.2 236.1 236.1_M 239.1 239.2 242.1 242.1_M 243.1 243.1_M 245.1 245.2 246.2 249.1

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Mercury in Water by Oxidation, Purge and Trap, and CVAFSTrace Elements in Water by ICP/MSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAAntimony by GFAAArsenic by GFAABarium by FLAABarium by FLAABeryllium by GFAACadmium by FLAACadmium by GFAACalcium by FLAACalcium by FLAAChromium by FLAAChromium by GFAACobalt by FLAACopper by FLAACopper by GFAAIron by FLAAIron by FLAALead by FLAALead by GFAAMagnesium by FLAAMagnesium by FLAAManganese by FLAAManganese by FLAAMercury in Water by CVAAMercury by CVAAMolybdenum by GFAANickel by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 53 of 515

Arizona Department of Environmental Quality

2510 2540-B 2540-C 2540-D 258.1 270.2 272.1 272.2 273.1 273.1_M 279.2 289.1 300(A) 310.1 310.2 3112-B 3114-C 325.2 325.3 335.2 335.3 335.4 340.2 350.1 350.2(A) 350.3 3500-CR(D) 3500-FE(D) 351.1 351.2 351.4 353.2 353.3 365.1 365.2 365.3 365.4 375.2 375.4 405.1 410.4 415.1 4500-CL(D) 4500-F-C

Procedure Id

APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

Procedure Source

Conductivity in WaterTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterPotassium by FLAASelenium by GFAASilver by FLAASilver by GFAASodium by FLAASodium by FLAAThallium by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinity by Colorimetric AnalysisMercury in Water by CVAAMetals in Water by Continuous HYDAAChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen Using an ISETotal Hexavalent Chromium in WaterIron in Water by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen Using an ISENitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionResidual Chlorine in Water by Titration- Amperometric MethodFluoride in Water Using an ISE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 54 of 515

Arizona Department of Environmental Quality

4500-NO2(B) 4500-NO3(E) 4500-NOR(B) 4500-NOR(C) 4500-SO4(E) 5210-B 6010A 6010B 602 7199 7421 7471A 9221-E

9221-F 9222-B 9222-D 9230-B

ASTM D3977 BART TEST BLS-21 BLS-256 CALCULATION COLILERT EPA 1630 EPA 1631 APP EPA 1631E EPA 200.7/208.1EPA 200.7/213.3EPA 200.7/215.1EPA 200.7/236.1EPA 200.7/242.1EPA 200.7/243.1EPA 200.7/273.1EPA 200.7/6010 EPA 200.9 MOD EPA 220.7/236.1EPA 220.7/242.1EPA 245.1/7470 EPA 351.3 EPA 365.2A EPA 365.3 MOD EPA 601/602

Procedure Id

APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA

APHA APHA APHA APHA

21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ

Procedure Source

Nitrite in Water by ColorimetryNitrate in Water- Cadmium ReductionTotal Kjeldahl Nitrogen in WaterTotal Kjeldahl Nitrogen in WaterSulfate by Turbidimetric Analysis5-Day Biochemical Oxygen DemandICP SpectroscopyInductively Coupled Plasma AESPurgeable Aromatics in Wastewater by GCHexavalent Chromium in Water by ICLead by GFAAMercury in Solid or Semisolid WasteEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueEscherichia coli, Multi-tube Fermentation TechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueASTM D3977BART TEST (PRESENTS/ABSENCE)BLS-21BLS-256LABORTORY CALCULATIONCOLILERTEPA 1630EPA 1631 APPMERCURY - TOTAL & DISSOLVED - CLEAN HANDSTOTAL BARIUMEPA 200.7/213.3TOTAL CALCIUMTOTAL IRONTOTAL MAGNESIUMMANGANESETOTAL SODIUMEPA 200.7/6010EPA 200.9 MODEPA 220.7/236.1EPA 220.7/242.1EPA 245.1/7470TOTAL KJELDAHL NITROGEN (AS N)TOTAL PHOSPHATEEPA 365.3 MODVOLATILE ORGANIC COMPOUNDS

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 55 of 515

Arizona Department of Environmental Quality

EPA 8021B FIELD SM 2320B SM 2340 B SM 2580(MOD) SM 3112 SM 3500 MOD SM 407C SM 4500 SM 4500 CN SM 4500 N-O, C SM 4500-N C SM 4500-P BE SM 4500-S SM 4500-S-C,D SM 4500NO3 SM 4500SO4(MOD)STD METH 407C SW846 UNKNOWN WALKLEY BLACK

Procedure Id

21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ 21ARIZ

Procedure Source

EPA 8021BADEQ FIELD PROCEDURESSM 2320BSM 2340 BSTANDARD MEHTOD 2580 (MODIFIED)STANDARD MEHTOD 3112SM 3500 MODTOTAL CHLORIDE IN WATERSTANDARD METHOD 4500STANDARD METHOD 4500 CN (CYANIDE)STANDARD METHOD 4500 N-O, CSTANDARD METHOD 4500-N CSTANDARD METHOD 4500-P BE(=SM 4500-S2) SULFIDESM 4500-S-C,DSTANDARD METHOD 4500 NO3STANDARD MEHTOD 4500SO4 (MODIFIED)TOTAL CHLORIDE WATERSW846UNKNOWNWALKLEY BLACK

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 56 of 515

Arizona Department of Environmental Quality

100 401 403 417 419 600/00-02 600/00-02 7500-RN 900 900 9056 9221-D 9221-E 999 AB AM 15

AM 15

AM18G AM18G AM20GAX

BLS 208 BLS 228 BLS-182 BLS-21 BLS-218 CALCULATION CARBAMATE METHOCARBAMATE METHOCASRL/MOD 300.0COLIFORM COLILERT CU200.7 CUSTOM CHLORO PCUSTOM GC/MS DHG-NEL 8473.00EPA 120.1 EPA 130.2 EPA 150.1 EPA 160.1 EPA 160.2 EPA 160.4 EPA 170.1

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

STATE LAB-VOLATILE PRIORITY POLLUTANT ANALYSISRADIOCHEMICAL ANALYSIS METHOD 401EPA 403RADIOCHEMICAL ANALYSIS METHOD 417RADIOCHEMICAL ANALYSIS METHOD 419GROSS ALPHA ACTIVITY METHOD 600/00-02GROSS ALPHA ACTIVITY METHOD 600/00-02RADIOCHEMICAL ANALYSIS METHOD 7500-RNGROSS BETA ACTIVITY METHOD 900GROSS BETA ACTIVITY METHOD 900anion chromotographyMETHOD 9221-D TOTAL COLIFORM BACTERIA (P/A)METHOD 9221-E TECAL COLIFORM BACTERIARADIOCHEMICAL ANALYSIS METHOD 999RADIONUCLIDESGAS CONCENTRATIONS OF THE DISSOLVED GASSES INWATERGAS CONCENTRATIONS OF THE DISSOLVED GASSES INWATERANALYSIS OF C1-C4 HYDROCARBONS IN WATERANALYSIS OF C1-C4 HYDROCARBONS IN WATERGAS CONCENTRATIONS OF THE DISSOLVED GASSES INWATERCHLORINATED PESTICIDE SCREENCUSTOM GC/MS SCREENMULTIELEMENT METALS SCREENHARDNESS, CALCULATEDGWPL PESTICIDESLABORATORY CALCULATIONADA-PESTICIDES BY GC/MSADA-PESTICIDES BY GC/MSPERCHLORATECOLIFORM - LAKE HAVASUCOLILERT (EDBERG)TOTAL COPPER(DDT, DDE DDD) PARAMETERS DETECTED/IDENTIFIEDPARAMETERS DETECTED/IDENTIFIED BY CUSTOM GC/MSDISSOLVED HYDROCARBON GASES IN WATERSPECIFIC CONDUCTIVITYTOTAL HARDNESSPH-LABTOTAL FILTRATABLE RESIDUETOTAL NONFILTRATABLE RESIDUETOTAL RESIDUEEPA 170.1

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 57 of 515

Arizona Department of Environmental Quality

EPA 180.1 EPA 200.7 EPA 200.7/208.1EPA 200.7/213.3EPA 200.7/215.1EPA 200.7/236.1EPA 200.7/242.1EPA 200.7/243.1EPA 200.7/273.1EPA 200.7/6010 EPA 200.8 EPA 200.9 EPA 202.1 EPA 204.2 EPA 206.2 EPA 206.2/7060 EPA 206.3 EPA 208.1 EPA 210.1 EPA 210.2 EPA 213.1 EPA 213.2 EPA 213.2/7131 EPA 215.1 EPA 218.1 EPA 218.2 EPA 219.2 EPA 220.1 EPA 220.1/220.2EPA 220.2 EPA 220.7/236.1EPA 220.7/242.1EPA 236.1 EPA 239.2 EPA 239.2/7421 EPA 242.1 EPA 243.1 EPA 245.1 EPA 245.1 EPA 245.1/7470 EPA 246.2 EPA 249.1 EPA 258.1 EPA 270.2

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

NTU TURBIDITYMETALSTOTAL BARIUMTOTAL BORONTOTAL CALCIUMTOTAL IRONTOTAL MAGNESIUMMANGANESETOTAL SODIUMEPA 200.7/6010METALSTOTAL ANTIMONY, ARSENIC, AND SELENIUMTOTAL ALUMINUMTOTAL ANTIMONYTOTAL ARSENICEPA 206.2/7060TOTAL ARSENICEPA 208.1EPA 210.1TOTAL BERYLLIUMEPA 213.1TOTAL CADMIUMEPA 213.2/7131EPA 215.1EPA 218.1CHROMIUMTOTAL COBALTTOTAL COPPERTOTAL COPPERTOTAL COPPERDISSOLVED IRONDISSOLVED MAGNESIUMEPA 236.1TOTAL LEADEPA 239.2/7421EPA 242.1EPA 243.1TOTAL MEMORYTOTAL MEMORYEPA 245.1/7470TOTAL MOLYBDENUMTOTAL NICKELTOTAL POTASSIUMTOTAL SELENIUM

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 58 of 515

Arizona Department of Environmental Quality

EPA 270.2/7740 EPA 272.1 EPA 272.2 EPA 273.1 EPA 279.2 EPA 279.2/7841 EPA 282.1 EPA 286.2 EPA 289.1 EPA 300 EPA 300.0 EPA 305 EPA 310.1 EPA 325.2 EPA 325.3 EPA 335.1 EPA 335.2 EPA 335.3 EPA 335.4 EPA 340.2 EPA 350.1 EPA 350.2 EPA 350.3 EPA 351.1 EPA 351.2 EPA 351.3 EPA 351.4 EPA 3510/8015 MEPA 3510/8081A EPA 3510/8081A EPA 3510/8082 EPA 3510/8082 EPA 353.2 EPA 353.2T EPA 353.3 EPA 354.1 EPA 360.1 EPA 365.2 EPA 365.2 EPA 365.2A EPA 365.3 EPA 365.3 MOD EPA 365.4 EPA 375.2

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

EPA 270.2/7740EPA 272.1TOTAL SILVERSODIUMTOTAL THALLIUMEPA 279.2/7841TOTAL TINEPA METHOD 286.2TOTAL ZINCANIONS BY ION CHROMATOGRAPHYEPA 300 METHODEPA METHOD 305 COLIFORM BACTERIAALKALINITY, TOTAL & PHENOLPHTHALEINCHLORIDECHLORIDEEPA 335.1CYANIDECYANIDEEPA 335.4TOTAL FLUORIDENITROGEN, AMMONIA, TOTAL (AS N)EPA 350.2AMMONIA, TOTALEPA 351.1NITROGEN, KJELDAHL, TOTAL (AS N)NITROGEN, KJELDAHL, TOTAL (AS N)EPA 351.4EXTRACTABLE FUEL HYDROCARBONSEPA 3510/8081AEPA 3510/8081AEPA 3510/8082EPA 3510/8082NITRITE PLUS NITRATENITRATE PLUS NITRITE TOTALEPA 353.3NITRITE NITROGEN TOTALEPA 360.1EPA 365.2EPA 365.2TOTAL PHOSPHATETOTAL PHOSPHORUSEPA 365.3 MODTOTAL PHOSPHORUSTOTAL SULFATE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 59 of 515

Arizona Department of Environmental Quality

EPA 375.4 EPA 375.4 EPA 376.1 EPA 405.1 EPA 410.4 EPA 415.1 EPA 415.2 EPA 418.1 EPA 420.1 EPA 425.1 EPA 502.2 EPA 503.1 EPA 5030B EPA 504 EPA 504.1 EPA 507 EPA 508 EPA 515 EPA 515.1 EPA 524.2 EPA 525.2 EPA 525.ML EPA 531.1 EPA 601 EPA 601/602 EPA 601/602 EPA 601/8010 EPA 6010 EPA 6010B EPA 602 EPA 602/8020 EPA 603 EPA 604 EPA 605 EPA 605 EPA 606 EPA 607 EPA 608 EPA 609 EPA 610

EPA 611 EPA 612 EPA 613

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

TOTAL SULFATETOTAL SULFATEEPA 376.1EPA 405.1EPA 410.4EPA 415.1TOTAL ORGANIC CARBONHYDROCARBON IN WATEREPA 420.1EPA 425.1SDW VOCEPA 503.1VOCEDP AND DBCPETHYLENE DIBROMIDEEPA 507ORGANOCHLORINE PESTICIDESSDW HERBICIDESHERBICIDESEPA 524.2EPA 525.2EPA 525 MLCARBAMATE PESTICIDESEPA 601VOCVOCHALOGENATED VOLATILE ORAGANICSEPA 6010EPA 6010BEPA 602EPA 602/8020EPA 603EPA 604BENZIDINESBENZIDINESPHTHALATE ESTERSEPA 607ORGANOCHLORINE PESTICIDES/PCBEPA609POLYNUCLEAR AROMATIC HYRDOCARBONS, PFLC-UV/FLUOR, XTNHALOETHERS, GC-HALL, XTNCHLORINATED HYDROCARBONS, GC-ECD, XTN2,3,7,8-TETRACHLORIODIBENZO-P-DIOXIN, GC/MS, XTN

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 60 of 515

Arizona Department of Environmental Quality

EPA 614 EPA 615 EPA 617 EPA 619 EPA 622 EPA 624 EPA 625 EPA 630

EPA 632 EPA 7041 EPA 7041 EPA 7060A EPA 7091 EPA 7196 EPA 7421 EPA 7470A EPA 7740 EPA 7841 EPA 7841 EPA 8010 EPA 8010/8020 EPA 8015 EPA 8015M EPA 8015M EPA 8020 EPA 8021 EPA 8021 EPA 8021A EPA 8021B EPA 8030 EPA 8040 EPA 8060 EPA 8080 EPA 8090 EPA 8120 EPA 8140 EPA 8141 EPA 8141 EPA 8141A EPA 8141A EPA 8150 EPA 8151 EPA 8151

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

ORGANOPHOSPHAE PESTICIDES, GC-FPD OR NPD, XTNCHLORINATED HERBICIDES (EPA METHOD 615)ORGANOHALIDE PESTICIDES AND PCB'S, GC-ECD, XTNTRIAZINE PESTICIDES, GC-NPD, XTNORGANOPHOSPHATE PESTICIDES, GC-FPD, XTNVOLATILE ORGANICS, GC/MS, P&TSEMI-VOLATILE ORGANICS, GC/MS,XTNDITHIOCARBAMATE PESTICIDES, COLORIMETRIC, CS2LIBERATIONCARBAMATES AND UREA PESTICIDES, HPLC-UV, XTNEPA 7041EPA 7041EPA 7060ABERYLLIUMEPA 7196LEADEPA 7470AEPA 7740EPA 7841EPA 7841HALOGENATED VOLATILE ORGANICSHALOGENATED VOLATILE ORGANICSNON-HALOGENATED VOLATILE ORGANICSNON-HALOGENATED VOLATILE ORGANICS-MODIFIEDNON-HALOGENATED VOLATILE ORGANICS-MODIFIEDAROMATIC VOLATILE ORGANICSEPA 8021EPA 8021EPA 8021AEPA8021BACROLEIN, ACRYLONITRITE, ACETONITRILEPHENOLSPHTHALATE ESTERSORGANOCHLORINE PESTICIDES + PCB'SNITROAROMATICS AND CYCLIC KETONESCHLORONATED HYDROCARBONSORGANOPHOSPHORUS PESTICIDESEPA 8141EPA 8141EPA 8141A-ORGANOPHOSPHORUS PESTICIDESEPA 8141A-ORGANOPHOSPHORUS PESTICIDESCHLORINATED HERBICIDESEPA 8151EPA 8151

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 61 of 515

Arizona Department of Environmental Quality

EPA 8240 EPA 8260 EPA 8260A EPA 8260B EPA 8270 EPA 8270 MODIFIEPA 8270A EPA 8270A EPA 8270C EPA 8310 EPA 900.0 EPA 903.0 EPA 903.0/901.1EPA 9040 EPA 9040 EPA 913.0 EPA M2340B EPA/CLP EPA 625ERI SOP FIELD GC/MS METHOD GC/MS METHOD GFAA

GFAA

GWPL CARBAMATESGWPL HERBICIDESGWPL-CARB GWPL-HERB GWPL-PEST H8190 HACH8000

HACH8000

ISOTOPIC ANALYSISOTOPIC ANALYSLUCAS CELL METHOD BAT MOD EPA 300.0 MOD. EPA 3810 MOD. EPA 3810 MOD. EPA 8015 MOD. EPA 8015/8

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

VOLATILE ORGANICSVOLATILE ORGANICSEPA8260AEPA 8260BSEMI-VOLATILE ORGANICSSEMI-VOLATILE ORGANICSPESTICIDES BY GS/MSPESTICIDES BY GS/MSSEMI-VOLATILE ORGANICS BY GC/MSPOLYNUCLEAR AROMATIC HYDROCARBONSEPA 900.0EPA 903.0EPA 903.0/901.1EPA 9040EPA 9040TOTAL RADON IN WATEREPA M2340BSEMI-VOLATILE ORGANICS, GC/MS, XTNLOW CONCENTRATIONS OF GERMANIUM IN WATER (ERI)FIELD PARAMETERSADA-PESTICIDES BY GS/MSADA-PESTICIDES BY GS/MSGRAPHITE FURNACE ATOMIC ABSORPTIONSPECTROPHOTOMETRYGRAPHITE FURNACE ATOMIC ABSORPTIONSPECTROPHOTOMETRYGWPL CARBAMATES BY GC/HPLCGWPL HERBICIDES BY GC/ECDGWPL CARBAMATESGWPL HERBICIDESGWPL PESTICIDESINORGANIC METHOD FOR TOTAL PHOSPHOROUS (AS P MG/L)FIELD TEST KIT WITH CONCENTRATIONS BASED ON A COLORWHEELFIELD TEST KIT WITH CONCENTRATIONS BASED ON A COLORWHEELISOTOPIC ANALYSISISOTOPIC ANALYSISLUCAS LABS METHOD OF ANALYZING RADONMETHOD BATPERCHLORATEMOD. EPA 3810MOD. EPA 3810VOLATILE FUEL HYDROCARBONS (MOD. EPA 8015)VOLATILE FUEL HYDROCARBONS/BTEX DISTINCTION

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 62 of 515

Arizona Department of Environmental Quality

MODIF.EPA 531.1MOHAVE PESTICIDNOT REPORTED ORGANO-HG PESTICIDES SW 8RA RADIONUCLIDE RSKSOP-175 RSKSOP-175M SM 10200 H SM 2320 B SM 2320B SM 2340 B SM 2510 B SM 2540 C SM 2540C SM 2580B SM 3112 SM 3112 B

SM 3500 SM 3500 CR D SM 403 SM 407C SM 4500 SM 4500 C SM 4500 CL D SM 4500 CN SM 4500 CO2 SM 4500 F-C SM 4500 N-O, C SM 4500 NO2-B SM 4500-N C SM 4500-NH3 BE SM 4500-NH3 BE SM 4500-NH3F SM 4500-P BE SM 4500-S-C,D SM 4500NO3 SM 4500NO3 E SM 5220 C SM 5220 C SM 5310 C SM 5310 C

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

BARBAMATE PESTICIDESMOHAVE SUITE PESTICIDESNOT REPORTED ON LAB SHEETORGANO-HG METHOD FOR MERCURYPESTICIDES SW 846 METHOD 3510, SW 846 METHOD 8270RADIUM-226 & RADIUM- 228RADIONUCLIDE ANALYSISETHANE, ETHYLENE, AND METHANE ANALYSISMETHANE ANALYSISSTANDARD METHOD FOR 10200HSTANDARD METHOD 2320 BSM 2320BSTANDARD METHOD 2340 BCONDUCTIVITY LABORATORY METHODTOTAL DISSOLVED SOLID DRIED AT 180 DEGREES CSTANDARD METHOD 2540STANDARD METHOD 2580B (REDOX)STANDARD METHOD 3112STANDARD METHOD COLD VAPOR ATOMIC ABSORPTIONSPECSTANDARD METHOD 3500STANDARD METHOD 3500 CR DSM 403TOTAL CHLORIDE IN WATERSTANDARD METHOD 4500STANDARD METHOD 4500 CSTANDARD METHOD 4500 FOR CHLORIDESTANDARD METHOD 4500 CN (CYANIDE)STANDARD METHOD 4500-CO2STANDARD METHOD 4500 FOR FLUORIDE /ION ELECTRODE MSTANDARD METHOD 4500 N-O, CSTANDARD METHOD 4500 NO2-BSTANDARD METHOD 4500-N CSTANDARD METHOD 4500-NH3 BESTANDARD METHOD 4500-NH3 BESTANDARD METHOD 4500-NH3FSTANDARD METHOD 4500-P BETOTAL SULFIDESTANDARD METHOD 4500 NO3STANDARD METHOD 4500 NO3 ESTANDARD METHOD 5220 CSTANDARD METHOD 5220 CSTANDARD METHOD 5310 CSTANDARD METHOD 5310 C

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 63 of 515

Arizona Department of Environmental Quality

SM 8015M SM 8020M SM 8021A SM 9222 SM 9222 SM 9222B SM 9222B SM 9222D SM 9222D SM 9223 SM-2320 SM-2320B SM-2540C SMEW&W #3500CRDSTD METH 407C SW8021A SW8260B SW8310 U OF A U OF A/U OF IL U OF IL U-NAT UNION CARBIDE UNKNOWN VARIAN MODIFIC.

Procedure Id

21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW 21ARIZGW

Procedure Source

STANDARD METHOD 8015MSTANDARD METHOD 8020MSTANDARD METHOD 8021ASTANDARD METHOD 9222STANDARD METHOD 9222STANDARD METHOD 9222BSTANDARD METHOD 9222BSTANDARD METHOD 9222DSTANDARD METHOD 9222DSTANDARD METHOD 9223STANDARD METHOD 2320STANDARD METHOD FOR THE EXAMINATION OF WATER ANDSTANDARD METHOD 2540STD MTHDS FOR EXAM. OF WTR & WWTOTAL CHLORIDE IN WATERSW8021ASW8260BSW8310ISOTOPIC ANALYSISISOTOPIC ANALYSISISOTOPIC ANALYSISNATURAL URANIUMUNION CARBIDEUNKNOWNSPECIFIC VOC'S- DIBROMO'S

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21ARIZGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 64 of 515

American Samoa Environmental Protection Agency

9223-B

Procedure Id

APHA

Procedure Source

Enzyme Substrate Test, E. coli, Coliform Group

Procedure Name

Active

Status21AS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 65 of 515

Calif State Water Resources Control Board

1600

200.1 9221-B

9221-E

9222-B 9222-D 9230-B

COLILERT COLILERT-18 COLILERT_18 COLILERT_18_FE COLILERT_18_TO ENTEROLERT ENTEROLERT

Procedure Id

USEPA

USEPA APHA

APHA

APHA APHA APHA

IDEXX IDEXX 21CABCH 21CABCH 21CABCH IDEXX 21CABCH

Procedure Source

Enterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Metals in Marine Waters by ICP/MSStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliCOLILERT_18 to detech E. ColiCOLILERT_18_FECAL to detect Fecal ColiformsCOLILERT_18_TOTAL to detect Total ColiformsEnterolert Quanti-Tray; Multi Tube, Multi Well, for EnterococciiEnterolert uses to detect Enterococcus

Procedure Name

Active

ActiveActive

Active

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

Status21CABCH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 66 of 515

Orange County Sanitation District California

150.1 160.2_M 1652 200.8 REV. B

245.1A

350.1B REV. A BACTERIA FISH01 REV. C

LABS OTTER TRAWL PAR SED01 REV. A

SED02 REV. B

SEDIMENT CHEM TOTAL COLIFORM VMADCP WQ

Procedure Id

USEPA USEPA USEPA 21CAOCSD

21CAOCSD

21CAOCSD 21CAOCSD 21CAOCSD

21CAOCSD 21CAOCSD 21CAOCSD 21CAOCSD

21CAOCSD

21CAOCSD 21CAOCSD 21CAOCSD 21CAOCSD

Procedure Source

pHTotal Suspended SolidsOil and GreaseDetermination of trace metals using inductively coupled plasma -mass spectrometryMercury analysis by cold vapor atomic spectrometric method usingflow injection mercury system (FIMS)Ammonia, water quality; segmented flow procedureBACTERIAPolychlorinated biphenyl congeners and organochlorine pesticidedetermination by gas chromatography / election captureLinear Alkaline BenzeneOTTER TRAWL FIELD SOPPARPolychlorinated biphenyl congeners and organochlorine pesticidedetermination by gas chromatorgraphy electron capturePolycyclic aromatic hydrocarbon determination by gaschromatography / mass spectrometry of ocean sedimentSediment chemistryTOTAL COLIFORMVessel Mounted Acoustic Doppler Current ProfilerWater Quality

Procedure Name

ActiveActiveActiveActive

Active

ActiveActiveActive

ActiveActiveActiveActive

Active

ActiveActiveActiveActive

Status21CAOCSD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 67 of 515

Colorado Dept. of Public Health & Environment

10029

10200-H 120.1 130.2 150.1 160.1 160.2 1603

170.1 200.7(W) 200.8(W) 200.9 2130 2130-B 218.5 2320 2340 245.1 2510 2540-C 2540-D 2550 300(A) 300(B) 310.1 3111-B 335.2 350.1 350.2(B) 3500-CA(B) 3500-CA(D) 351.2 351.3(A) 353.2 360.1 365.1 365.2 365.3 376.2 405.1 4500-CL(D) 4500-CL-(C)

Procedure Id

HACH

APHA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA APHA APHA USEPA APHA APHA USEPA APHA APHA APHA APHA USEPA USEPA USEPA APHA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

Procedure Source

m-ColiBlue24 Method of the Determination of Total Coliforms and E.coliChlorophyll a-b-c DeterminationConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)TemperatureMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAATurbidity in WaterNephelometric MethodHexavalent Chromium by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameTotal Cyanide in WaterAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryCalcium in Water by FLAACalcium in Water by Titration Using EDTATotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetrySulfide by Colorimetric Determination5 Day Biochemical Oxygen DemandResidual Chlorine in Water by Titration- Amperometric MethodChloride in Water by Titration- Mercuric Nitrate Method

Procedure Name

Active

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21COL001

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 68 of 515

Colorado Dept. of Public Health & Environment

4500-CL-(D) 4500-CN(E) 4500-CN(H) 4500-F-E 4500-H 4500-NH3(H) 4500-NO2(B) 4500-NO3(F) 4500-O-G 4500-P-E 4500-SO4(D) 5210-B 5310-B 5310-C 9041A 9221-B.1

9221-C

9221-E

9222-D 9223-B APHA 4500NH3(H)CDPHE - TOTAL NCHL_A D5389 HISTORIC LAKEVERT_1 METER_1 POT DISS METAL1POT DISS METAL2RBP SECCHI_DEPTH UNIONIZED-NH3

UNKNOWN

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA APHA

APHA

APHA

APHA APHA 21COL001 21COL001 21COL001 ASTM 21COL001 21COL001 21COL001 21COL001 21COL001 21COL001 21COL001 21COL001

21COL001

Procedure Source

Chloride in Water by PotentiometryCyanide in Water by ColorimetryCyanides Amenable to Chlorination without DistallationFluoride in Water by ColorimetrypH in WaterAmmonia in Water - Flow Injection AnalysisNitrite in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSulfate in Water by Gravimetric Analysis5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodpH using PaperEscherichia coli Fermentation Technique, Multi-tube FermentationTechniqueEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupAPHA NH3 ANALYSIS BY FLOW INJECTION ANALYSISTotal Nitrogen, Automated Cadmium ReductionChlorophyll a, corrected for pheophytinOpen-Channel Flow Measurement by Acoustic Velocity MeterHistoric Procedure Used for Unknown Legacy MethodsVertically Intregrating Water SamplerVertical Lake Profile using a multi-probe meterPotentially Dissolved Metals Using The ICP-AES MethodPotentially Dissolved Metals Using The ICP/MS MethodUSEPA Rapid Bioassessment ProtocolsSecchi disk transparencyUnionized Ammonia calculated from pH, Temperature and TotalAmmoniaUNKNOWN

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Status21COL001

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 69 of 515

District of Columbia Dept of Health, Water Quality Division

2100 2340 WQD-001 WQD-002 WQD-003 WQD-004 WQD-005 WQD-006 WQD-007 WQD-008 WQD-009 WQD-010 WQD-011 WQD-012 WQD-013 WQD-014 WQD-015 WQD-016 WQD-017 WQD-018 WQD-019 WQD-020 WQD-021 WQD-022 WQD-023 WQD-024 WQD-025 WQD-026 WQD-027 WQD-028 WQD-029 WQD-030 WQD-031 WQD-032 WQD-033 WQD-034 WQD-035 WQD-036 WQD-037 WQD-038 WQD-039 WQD-040 WQD-041

Procedure Id

21DCBAWQ APHA 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ 21DCBAWQ

Procedure Source

Turbidity in water in NTUHardness in Water by EDTA Titrationfield Hydrolab determination of WTemp with probefield Hydrolab determiation of PH with probefield Hydrolab determination of DO with probeField Hydrolab determination of conductivity with probeField measurement of Transparency with Secchi DiskField station visit weather observationField code for Wave state and HeightAkalinity in water, Titrimetric, PH 4.6Turbidity of water in NTUChlorophyll "a" , monochromatic correctedPheophytin "a" , ug/lField In-Site Specific ConductanceHardness in water by Titrimetric, EDTAField secchi disk, transparency , metersOrthosphate in water by colorimetricTotal Dissolved Phosphorus in water by colorimetric, block digestorTotal Phosphorus in water by colorimetric, block digestorTotal Organic Carbon combustion infrared methodDisolved Organic Carbon, combustion infrared method5-Day Biochemical Oxygen DemandTotal Non-filterable ResidueAmmonia in waterTotal Kjeldahl Nitrogen whole water, semi-block degestorNitrate Nitrogen in waterNitrite Nitrogen in waterNitrate Plus Nitrite Nitrogen in water by colorimetricSilica in water by colorimetricSelenium in water by ICP/MSLead in waterMercury in waterCadmium in waterCopper in waterChromium in waterZINC/ZN, in waterIron/FE, in waterArsenic/AS in water, dissolvedSulfate in waterTotal coliform-MPNFecal Coliform-MPNTotal Coliform-membraneFecal Coliform-Membrane

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21DCBAWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 70 of 515

Delaware Department of NREC

150.1 150.1

Procedure Id

21DEBCH USEPA

Procedure Source

pHpH

Procedure Name

ActiveActive

Status21DEBCH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 71 of 515

FL Dept. of Environmental Protection

100300 D.1 10200-F 10200-G 10200-H 110.2 120.1 150.1 160.2 160.4 170.1 180.1 200.7(W) 200.8(S) 200.8(W) 245.1 2520 B 2520-B 2540-E 300(A) 310.1 310.1 340.2 340.2_M 350.1 351.2 353.2 360.1 360.1 365.1 365.4 405.1 415.1 9222-B 9222-D EPA 415.1 EPA600/9-78-018FT1700

Procedure Id

21FLA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLA APHA APHA USEPA USEPA 21FLA USEPA USEPA USEPA USEPA USEPA 21FLA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLA 21FLA 21FLA

Procedure Source

Particle DistributionPhytoplankton Counting TechniquesZooplankton Counting TechniquesChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMercury in Water by CVAASalinitySalinity in Water- Electrical Conductivity MethodFixed and Volatile Solids in WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinityFluoride in Water Using an ISEFluoride with an Ion Selective ElectrodeAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen ProbeDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureTotal Organic CarbonEPA 600/9-78-018 (mod.) Potential algal growth determinationSECCHI DEPTH

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 72 of 515

Alachua County Environmental Protection Department (Florida)

10200-H 110.2 120.1 150.1 160.1 160.2 180.1 200.7(W) 200.8(W) 2120-B 2320 2540-C 272.2 300.0 310.1 325.2 340.2 350.1 351.2 353.2 365.1 365.2 365.3 365.4 375.4 415.1 6010A 6010B 7470A 8260B 8270B(W) 9221-C

9221-E

9222-B 9222-D 9222-E FLOW NTOT TURB

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA 21FLACEP USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

APHA

APHA APHA APHA 21FLACEP 21FLACEP 21FLACEP

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSColor in Water by Visual ComparisonAlkalinity in Water by TitrationTotal Dissolved Solids in WaterSilver by GFAAFluorides by ion chromatography (EPA)Alkalinity by TitrationChloride by Colorimetric Analysis IIFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionICP SpectroscopyInductively Coupled Plasma AESMercury in Liquid Wastes by CVAAVolatile Organics by CGC/MSSemivolatile Organics in Water by GC/MSEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Coliform- Delayed-Incubation ProcedureDetermination of flow velocityTotal NitrogenTubidity

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActive

Status21FLACEP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 73 of 515

Apalachicola National Estuarine Research Reserve (Florida)

ANERR-LAB1 ANERR-LAB2 ANERR-LAB3 ANERR-LAB4 ANERR-LAB5 ANERR-LAB6 ANERR-LAB7 ANERR-LAB8 ANERR-LAB9

Procedure Id

21FLANER 21FLANER 21FLANER 21FLANER 21FLANER 21FLANER 21FLANER 21FLANER 21FLANER

Procedure Source

NH4FNO23FNO3FTURBDINLAB6CHLA_NPO4F DeterminationNO2F Determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLANER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 74 of 515

Avon Park Air Force Range - 18 ASOG DET 1 OL A/CEV

10200-H 110.2 350.1 351.2 353.2 365.1 405.1 9222-B 9222-D HORIBA PYGMY

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLAVON 21FLAVON

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry5 Day Biochemical Oxygen DemandStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureAPAFR TMDL Study Field Parameters Collection ProcedureAPAFR TMDL Study Flow Velocity Collection Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLAVON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 75 of 515

FL Dept. of Environmental Protection

350.1 351.2 353.2 365.1 365.3 365.4 ENT SECCHI SM10200H MOD STANDARDMETH

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA 21FLBFA 21FLBFA 21FLBFA 21FLBFA

Procedure Source

Ammonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionEnterococci AnalysisSecchi Depth MeasurementChlorophyll A and Phaephytin, Monchromatic, WaterStandard Methods for the Examination of Water and Wastewater

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLBFA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 76 of 515

Biological Research Associates (Florida)

10200-H 110.2 160.1 160.2 180.1 200.7(W) 200.8(W) 215.1 2320 236.1 242.1 258.1 273.1 300.0_28D 310.1 325.3 340.2 350.1 351.2 353.2 365.1 365.2 365.4 375.2 405.1 415.1 608 8081/8082(W)

8151(W) 9221-B

9221-E

9222-B 9222-D 9222-E FT 1100 FT 1200 FT 1300 FT 1400 FT 1500 FT 1600 FT 1700

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA 21FLBRA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLBRA

USEPA APHA

APHA

APHA APHA APHA 21FLBRA 21FLBRA 21FLBRA 21FLBRA 21FLBRA 21FLBRA 21FLBRA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSCalcium by FLAAAlkalinity in Water by TitrationIron by FLAAMagnesium by FLAAPotassium by FLAASodium by FLAAChloride, Sulfate, and Fluoride by Ion ChromatographyAlkalinity by TitrationChloride by Mercuric Nitrate TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by Colorimetry5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBs/PCBs as Aroclors by CapillaryColumn GCChlorinated Herbicides in Water by GCStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Coliform- Delayed-Incubation ProcedureField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific Conductance (Conductivity)Field Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved Oxygen (DO)Field Measurement of TurbidityField Measurement of Light Penetration (Secchi Depth andTransparency)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLBRA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 77 of 515

Biological Research Associates (Florida)

QUANTITRAY2000

Procedure Id

21FLBRA

Procedure Source

Total and Fecal Coliform

Procedure Name

Active

Status21FLBRA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 78 of 515

Brevard County Stormwater Utility Department (Florida)

10200-H 110.2 160.2 180.1 200.7(W) 220.2 2320 239.2 300(A) 310.1 350.1 351.2 353.2 365.1 365.4 9222-D FT1100 FT1200 FT1300 FT1400 FT1500 FT1600 FT1700

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA 21FLBREV 21FLBREV 21FLBREV 21FLBREV 21FLBREV 21FLBREV 21FLBREV

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESCopper by GFAAAlkalinity in Water by TitrationLead by GFAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block DigestionFecal Coliform Membrane Filter ProcedureField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of TurbidityField Measurement of Light Penetration (Secchi depth andTransparency)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLBREV

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 79 of 515

Broward Co Dept of Natural Resource Protection (Florida)

10200-H 120.1 150.1 170.1 180.1 220.2 2520-B 350.1 351.2 351.2-350.1 353.2 353.2+351.2 354.1 360.1 365.1 365.4 415.1 9222-B 9222-D 9230C CHLOR A CHLOROA/PHEOA D3867(B) FLOW_DIRECTION 2520B 365.1-PO4 9222B 9222D

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA 21FLBROW USEPA 21FLBROW USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLBROW 21FLBROW 21FLBROW ASTM 21FLBROW 21FLBROW 21FLBROW 21FLBROW 21FLBROW

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHTemperatureTurbidity by NephelometryCopper by GFAASalinity in Water- Electrical Conductivity MethodAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryOrganic NitrogenNitrate-Nitrite Nitrogen by ColorimetryTotal NitrogenNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal StreptococciChlorophyll aChlorophyll A:Pheophytin A RatioNitrite-Nitrate by Manual Cd ReductionTidal StageSalinityOrthophosphateTotal ColiformFecal Coliform

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveSuspSuspSuspSusp

Status21FLBROW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 80 of 515

City of Tampa Bay Study Group (Florida)

SOP-2

Procedure Id

21FLBSG

Procedure Source

To be updated

Procedure Name

Active

Status21FLBSG

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 81 of 515

Choctawhatchee Basin Alliance (Florida)

10200-H 4500-NO3(F) LAKEWATCH_TP PH TURBIDITY

Procedure Id

APHA APHA 21FLCBA 21FLCBA 21FLCBA

Procedure Source

Chlorophyll a-b-c DeterminationNitrate in Water- Automated Cadmium ReductionTotal Phosphorus as PHydrolab pHHydrolab Turbidity

Procedure Name

ActiveActiveActiveActiveActive

Status21FLCBA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 82 of 515

Florida Department of Environmental Protection

10200-H 110.1 110.2 120.1 130.2 150.1 160.1 160.2 160.3 1631 170.1 180.1 200.7(W) 200.8(W) 2520-B 300.0 310.1 340.2 350.1 351.2 353.2 360.1 365.1 365.2 365.4 410.1 410.2 415.1 4500-CL(G) 5210-B 600/9-78-018 9222-B 9222-D EPA 340.2 EPA 415.1 FL-PRO

FT 1000 FT 1100 FT 1200 FT 1300 FT 1400 FT 1500 FT 1700

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA 21FLCEN USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLCEN APHA APHA 21FLCEN 21FLCEN 21FLORL

21FLCEN 21FLCEN 21FLCEN 21FLCEN 21FLCEN 21FLCEN 21FLCEN

Procedure Source

Chlorophyll a-b-c DeterminationColor by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueMercury in Water by Oxidation, Purge and Trap, and CVAFSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSSalinity in Water- Electrical Conductivity MethodDetermination of SO4 and CL by Ino ChromatographyAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionMid-Level Chemical Oxygen DemandLow Level Chemical Oxygen DemandTotal Organic Carbon by CombustionResidual Chlorine by Colorimetry- DPD Colorimetric Method5-Day Biochemical Oxygen DemandPotential algal growth determinationStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFluorideOrganic CarbonTotal recoverable petroleum hydrocarbons in waste samples by GC-FIDTemperature, airpHConductivitySalinitytemperatureDissolved Oxygen (DO)Secchi disk depth

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

Status21FLCEN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 83 of 515

Florida Department of Environmental Protection

HISTORICAL SOP-AB03_1 SOP-AB04 SOP-AB05 SOP-AB10_1 SOP-ANALY

Procedure Id

21FLCEN 21FLCEN 21FLCEN 21FLCEN 21FLCEN 21FLCEN

Procedure Source

Standard Operation ProcedurePhytoplankton Identification - DiatomPhytoplankton Identification - WetDEP Phytoplankton Preparation - Wet TaxaDEP-SOPStandard Analytical Procedure

Procedure Name

ActiveActiveActiveActiveActiveActive

Status21FLCEN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 84 of 515

FDEP Charlotte Harbor Aquatic/Buffer Preserves

10200-H 110.2 180.1 2120-B 2130 351.2 353.2 365.4 4500-NO3(B) 4500-NOR(B) 4500-P-E 9222-D EPA 351.2+353.2FT_1100 FT_1300 FT_1400 FT_1500 FT_1700

SM 10200H

SM 2121B SM 4500-OC SM 9222D

Procedure Id

APHA USEPA USEPA APHA APHA USEPA USEPA USEPA APHA APHA APHA APHA 21FLCHAR 21FLCHAR 21FLCHAR 21FLCHAR 21FLCHAR 21FLCHAR

21FLCHAR

21FLCHAR 21FLCHAR 21FLCHAR

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltTurbidity by NephelometryColor in Water by Visual ComparisonTurbidity in WaterTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionNitrate in Water by Ultraviolet SpectrophotometryTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodFecal Coliform Membrane Filter ProcedureEPA Nitrate/Nitrite + TKN analysisField Measurement of Hydrogen Ion Activity (pH)Field Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of Light Penetration (Secchi Depth andTransparency)Standard Methods Analysis for Chlorophyll a, Uncorrected forpheophytinStandard Methods Analysis for True ColorStandard Methods Dissolved Oxygen analysisStandard Methods Analysis for Total Fecal Coliform

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActive

Status21FLCHAR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 85 of 515

FL Dept. of Environmental Protection

350.1 351.2 353.2 365.1 365.3 CHEM

CHEMETSDO ENT SECCHI STANDARDMETHODS

Procedure Id

USEPA USEPA USEPA USEPA USEPA 21FLCMP

21FLCMP 21FLCMP 21FLCMP 21FLCMP

Procedure Source

Ammonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetryUSEPA Methods for Chemical Analysis or Water and Wastewater;EPA 600/4-79-020Dissolved Oxygen CHEMets /ASTM D888-87USEPA Method 1106.1 for Enterococci analysisSecchi Depth DeterminationStandard Methods for the Examination of Water and Wastewater

Procedure Name

ActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

Status21FLCMP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 86 of 515

Collier County Pollution Control (Florida)

LKTRAFF

Procedure Id

21FLCOLL

Procedure Source

Lake Trafford

Procedure Name

Active

Status21FLCOLL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 87 of 515

City of Tallahassee Stormwater Management Division (Florida)

10200-H 110.2 150.1 180.1 200.7(W) 202.2 206.2 215.1 220.2 231.2 239.2 245.1 310.1 350.1 365.4 405.1 410.4 415.1 4540-84 550 600/8-78

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLCOT USEPA 21FLCOT

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltpHTurbidity by NephelometryMetals in Water by ICP-AESAluminum by GFAAArsenic by GFAACalcium by FLAACopper by GFAAGold by GFAALead by GFAAMercury in Water by CVAAAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionUSGS standard Nitrite AnalysisPolycyclic Aromatic Hydrocarbons by HPLCMicrobiological Monitoring

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLCOT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 88 of 515

City of Port St. Joe Wastewater Treatment Plant (Florida)

2120-B 2130 2540-D 4500-H 5210-B 9221-C

Procedure Id

APHA APHA APHA APHA APHA APHA

Procedure Source

Color in Water by Visual ComparisonTurbidity in WaterTotal Suspended Solids in WaterpH in Water5-Day Biochemical Oxygen DemandEstimation of Coliform Group Density, Multi-tube FermentationTechnique

Procedure Name

ActiveActiveActiveActiveActiveActive

Status21FLCPSJ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 89 of 515

City of Port St. Lucie (Florida)

120.1 150.1 170.1 180.1 220.2 300(A) 350.1 351.2 360.1 365.1 CALCULATED

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLCPSL

Procedure Source

ConductancepHTemperatureTurbidity by NephelometryCopper by GFAAInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by Colorimetryport st_lucie

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLCPSL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 90 of 515

Dade Environmental Resource Management (Florida)

00-01 00-02 00-03 00-04 00-05 00-06 00-07 00-09 0010(B) 0010(BT) 0010(W) 0011-0 0011A 002(A) 002(W) 0023A 004(A) 004(S) 004(W) 005(A) 005(BT) 005(S) 005(W) 008(BT) 008(S) 008(V) 008(W) 1 10 101 101A 102 10200-F 10200-G 10200-H 10200-I 10200-J 103 10300-C 10300-D 104 10400-D 10400-E 105

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA APHA APHA USEPA APHA APHA USEPA

Procedure Source

Gross Alpha and Beta Activity in WaterGross Alpha Activity in Drinking Water by CoprecipitationLead-210 and Polonium-210 in Dried SamplesPlutonium, Thorium & Uranium in Air FiltersThorium and Uranium in Ashed SamplesThorium and Uranium in Ashed SamplesThorium and Uranium in Water SamplesPlutonium and Uranium in MilkTotal Chromatographable Organic MaterialTritium in Biological TissueTritium in WaterSampling for Formaldehyde EmissionsAnalysis of Aldehydes/Ketones by HPLCRadon-222 in AirRadon-222 in WaterSampling for PCDD and PCDF EmissionsRadium-226 and Radium-228 in AirRadium-226 and Radium-228 in SoilRadium-226 and Radium-228 in WaterPlutonium, Uranium and Thorium in AirPlutonium, Uranium and Thorium in TissuePlutonium, Uranium and Thorium in SoilPlutonium, Uranium and Thorium in WaterStrontium-89 and Strontium-90 in TissueStrontium-89 and Strontium-90 in SoilStrontium-89 and Strontium-90 in PlantsStrontium-89 and Strontium-90 in WaterBeta Activity in Airborne ParticulatesCarbon Monoxide Emissions in AirGaseous Mercury in Air by CVAAGaseous Mercury from Sewage/Sludge IncineratorsMercury Emissions - Hydrogen StreamsPhytoplankton Counting TechniquesZooplankton Counting TechniquesChlorophyll a-b-c DeterminationDetermination of Biomass (Standing Crop)Metabolic Rate MeasurementsBeryllium Screening in AirPeriphyton Sample AnalysisPeriphyton Primary ProductivityBeryllium in AirMacrophyton Population EstimatesMacrophyton ProductivityMercury in Sewage Sludge

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 91 of 515

Dade Environmental Resource Management (Florida)

10500-C 106 107 107A 108 10A 10B 11 110.1 110.2 110.3 1103.1

1103_1 1104 1106.1

1106_1 111 114 115 12 (ATM PB) 12 (ISOTOPES) 120.1 120.1_M 13 130.1 130.2 13A 13B 140.1 15 150.1 150.2 150.2_M 16 160.1 160.1_M 160.2 160.2_M 160.3 160.4 160.5 1600

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA NIOSH

Procedure Source

Benthic Macroinvertebrate Sample Processing and AnalysisVinyl Chloride in Stack GasVinyl Chloride - WastewaterVinyl Chloride - Solvent/ResinParticulate and Gaseous ArsenicCarbon Monoxide Emissions in AirCarbon Monoxide Emissions in AirIsotopic Analysis by Ge(Li) DetectorColor by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltColor by Spectrophotometric AnalysisEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)E. coli in Water by Membrane FiltrationE. coli in Drinking Water/EC Medium with Mug TubEnterococci in Water by Membrane Filtration Using membrane-Enterococcus-Esculin Iron Agar (mE-EIA)Enterococci in Water by Membrane FilterPolonium-210 EmissionsRadionuclide EmissionsMonitoring for Radon-222Inorganic Lead Emissions in AirIsotopic Analysis by NaI(Tl) DetectorConductanceConductivity in Industrial WasteKrypton, Xenon and Tritiated MethaneTotal HardnessTotal HardnessTotal Fluoride Emissions in AirTotal Fluoride Emissions in AirOdor in Water Using a Consistent SeriesHydrogen Sulfide, Carbonyl SulfidepHpH by Continuous MonitoringpH in Industrial Waste MaterialsSulfur Emissions from Stationary SourcesFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsTotal ResidueVolatile ResidueSettleable MatterCarbon Disulfide by GC/FPD

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 92 of 515

Dade Environmental Resource Management (Florida)

1600

1601

1602

1603

1604

1605

1613(S) 1613(W) 1618 1620(A) 1620(B) 1620(C) 1620(D) 1622 1623

1624(S) 1624(W) 1625(AW) 1625(BNW) 1625(S) 1631 1632 1636 1637 1638 1639 1640 1648 1649 1650 1651 1652 1653 1654 1656(ECD) 1656(HSD) 1657 1658 1659

Procedure Id

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Enterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Male-specific (F+) and Somatic Coliphage in Water by Two-stepEnrichment ProcedureMale-specific (F+) and Somatic Coliphage in Water by Single AgarLayer (SAL) ProcedureEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Total Coliforms and E. coli in Water by Membrane Filtration Using aSimultaneous Detection Technique (MI Medium)Aeromonas in Finished Water Membrane Filtration Using Ampicillin-Dextrin Agar with Vancomycin (ADA-V)Dioxins and Furans - SolidsDioxins and Furans - WaterPesticides and HerbicidesMetals by Calibrated ICPMetals by GFAAMercury - CVAAMetals by Semi-quantitative ICP ScreenCrytosporidium in Water by Filtration/IMS/FA - April 2001 UpdateCryptosporidium and Giardia in Water by Filtration/IMS/FA - April2001 UpdateVolatiles by Isotope Dilution - SoilVolatiles by Isotope Dilution - WaterSemivolatiles - Acids, GC/MSSemivolatiles - Base/Neutrals, GC/MSSemivolatiles - Soil, GC/MSMercury in Water by Oxidation, Purge and Trap, and CVAFSInorganic Arsenic in Water by Hydride Generation Quartz FurnaceHexavalent Chromium in Ambient Water by Ion ChromatographyTrace Elements in Water by Chelation Preconcentration and GFAATrace Elements in Water by ICP/MSTrace Elements in Water by GFAATrace Elements in Water by Chelation Preconcentration and ICP/MSOrganic Halides by Neutron ActivationOrganic Halides by CoulometryOrganic Halides in WaterDiesel Oil in Muds by GC/FIDOil and GreaseChlorinated Phenolics by GC/MSPolynuclear Aromatic Hydrocarbons in OilOrganohalide Pesticides in WastewaterOrganohalide Pesticides in WastewaterOrganophosphorus Pesticides in WaterPhenoxy-Acid Herbicides in WastewaterDazomet in Wastewater

Procedure Name

Active

Active

Active

Active

Active

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 93 of 515

Dade Environmental Resource Management (Florida)

1660 1661 1662 1663 1664 1665 1666 1667 1671 1673 16A 16B 17 170.1 18 180.1 1A 2.1 (ATM SO2) 2.1 (PART.PM10)2.11 2.1A 2.2 2.3 2.6 2.8 2.9 20 200 200.1 200.1(FLAA) 200.1(GFAA) 200.1(ICP) 200.10_M 200.11 200.12 200.13 200.15 200.62(B) 200.62(C) 200.7(S) 200.7(W) 200.7_M 200.8(S) 200.8(W)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Pyrethrins and Pyrethroids in WaterBromoxynil in Wastewater by HPLC/UVExtractable Material in Mud by SDSDifferentiation of Oil by GC/FIDExtractable Material in Oil and GreaseSemivolatiles by Isotope Dilution GC/MSVOCs by Isotope Dilution GC/MSAldehydes by Derivatization and HPLCVOCs by GC/FIDPEG-600 by Derivatization and HPLCTotal Reduced Sulfur Emissions in AirTotal Reduced Sulfur Emissions in AirParticulate Emissions in AirTemperatureGaseous Organic Compound Emission in AirTurbidity by NephelometrySample and Velocity TraversesSulfur Dioxide in the AtmosphereParticulate Matter as PM10 in AtmosphereParticulate Matter as PM10 in AtmosphereSulfur Dioxide in the AtmosphereSuspended Particulates in the AtmosphereNitrogen Dioxide in the AtmosphereCarbon Monoxide in the AtmosphereLead in Suspended Particulate MatterSulfur Dioxide in the AtmosphereNitrogen Oxides and Sulfur Dioxide in AirMetals by Atomic AbsorptionMetals in Marine Waters by ICP/MSAcid Soluble Metals in Water by FLAAAcid Soluble Metals in Water by GFAAAcid Soluble Metals - ICPInductively Coupled PlasmaMetals in Fish Tissue by ICP-AESElements in Water by Temperature GFAAElements in Water by Chelation with GFAAMetals in Water by Nebulization and ICP-AESPneumatic Nebulization ICP AnalysisHydride Generation ICP AnalysisMetals in Soil by ICP-AESMetals in Water by ICP-AESICP-AES For Trace Element AnalysisMetals in Wastes by ICP/MSMetals in Waters by ICP/MS

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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and Equipment Summary

Page 94 of 515

Dade Environmental Resource Management (Florida)

200.9 201(CSR) 201(EGR) 202 202.1 202.1_M 202.2 202.2_M 202.2_M/HG) 202.62(D) 203 203A 203B 203C 204.1 204.1_M 204.2 204.2_M 206.2 206.2_M 206.3 206.3_M 206.4 206.5 208.1 208.1_M 208.2 208.2_M 210.1 210.1_M 210.2 210.2_M 212.3 2120-B 2120-C 2120-D 2120-E 213.1 213.1_M 213.2 213.2_M 2130 215.1 215.1_M

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA

Procedure Source

Metals by Temperature Stabilized GFAADetermination of PM10 EmissionsDetermination of PM10 EmissionsDetermination of Particulate EmissionAluminum by FLAAAluminum by FLAAAluminum by GFAAAluminum by GFAAMercury in Industrial Wastes by CVAAKOH Fusion Samples by GFAADetermination of Opacity of EmissionsTime-Averaged Opacity of EmissionsOpacity of Emission - Time Exception Regs.Opacity of Emission - Instantaneous Regs.Antimony by FLAAAntimony by FLAAAntimony by GFAAAntimony by GFAAArsenic by GFAAArsenic by GFAAArsenic by HYDAAHydride Generation ICPArsenic by Spectrophotometric AnalysisArsenic Digestion for HYDAABarium by FLAABarium by FLAABarium by GFAABarium by GFAABeryllium by FLAABeryllium by FLAABeryllium by GFAABeryllium by GFAABoron by Colorimetric AnalysisColor in Water by Visual ComparisonColor in Water by SpectrophotometryColor in Water Using Tristimulus FiltersColor in Water Using the ADMI MethodCadmium by FLAACadmium by FLAACadmium by GFAACadmium by GFAATurbidity in WaterCalcium by FLAACalcium by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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and Equipment Summary

Page 95 of 515

Dade Environmental Resource Management (Florida)

215.2 2150 2160-B 2160-C 2170 218.1 218.1_M 218.2 218.2_M 218.3 218.4 218.5 218.6 219.1 219.1_M 219.2 219.2_M 220.1 220.1_M 220.2 220.2_M 221.1 23 231.1 231.2 2310 2320 2340 235.1 235.2 2350-B 2350-C 2350-D 2350-E 236.1 236.1_M 236.2 236.2_M 239.1 239.1_M 239.2 239.2_M 242.1 242.1_M

Procedure Id

USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USFDA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Calcium by EDTA Titrimetric AnalysisOdor in Water by Threshold TestingTaste in Water by Flavor Threshold TestTaste in Water by Flavor RatingTaste and Odor by Profile AnalysisChromium by FLAAChromium by FLAAChromium by GFAAChromium by GFAAChromium by Chelation Extraction FLAAHexavalent Chromium by FLAAHexavalent Chromium by GFAAHexavalent Chromium by Ion ChromatographCobalt by FLAACobalt by FLAACobalt by GFAACobalt by GFAACopper by FLAACopper by FLAACopper by GFAACopper by GFAAChlorophenoxy Acid and PentachlorophenolPCDDs and PCDFs in Air EmissionsGold by FLAAGold by GFAAAcidity in Water by TitrationAlkalinity in Water by TitrationHardness in Water by EDTA TitrationIridium by FLAAIridium by GFAAChlorine Demand/Requirement of WaterChlorine Dioxide Demand/Requirement of WaterOzone Demand or Requirement of Water- Batch MethodOzone Demand or Requirement of Water- Semi-Batch MethodIron by FLAAIron by FLAAIron by GFAAIron by GFAALead by FLAALead by FLAALead by GFAALead by GFAAMagnesium by FLAAMagnesium by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 96 of 515

Dade Environmental Resource Management (Florida)

242.4 243.1 243.1_M 243.2 243.2_M 245.1 245.1_M 245.2 245.2_M 245.3 245.5 245.5_M 245.6 246.1 246.2 249.1 249.1_M 249.2 249.2_M 25 2510 2510 252.1 252.2 2520-B 2520-C 2520-D 253.1 253.2 2530-B 2530-C 2540-B 2540-C 2540-D 2540-E 2540-F 2540-G 255.1 255.2 2550 2560-B 2560-C 2560-D 2570-B

Procedure Id

USFDA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA NIOSH APHA USEPA USEPA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA

Procedure Source

Substituted Urea HerbicidesManganese by FLAAManganese by FLAAManganese by GFAAManganese by GFAAMercury in Water by CVAAMercury in Water by Manual CVAAMercury by CVAAMercury in Water by Automated CVAAMercury in Water by HPLCMercury in Sediment by CVAAMercury in Soil and Sediment by CVAAMercury in Tissue by CVAAMolybdenum by FLAAMolybdenum by GFAANickel by FLAANickel by FLAANickel by GFAANickel by GFAATotal Gaseous Nonmethane Organic Emissions1-Octanethiol by GC/FPDConductivity in WaterOsmium by FLAAOsmium by GFAASalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodSalinity in Water- Algorithm of Practical SalinityPalladium by FLAAPalladium by GFAAParticulate Floatables in WaterFloatable Oil and Grease in WaterTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterSettleable Solids in WaterTotal, Fixed and Volatile SolidsPlatinum by FLAAPlatinum by GFAATemperature of Water by ThermometerParticle Counting by Electrical SensingParticle Counting by Light-BlockageParticle Counting by Light-ScatteringAsbestos in Water by TEM

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 97 of 515

Dade Environmental Resource Management (Florida)

258.1 258.1_M 2580 25A 25B 25C 25D 25E 26 264.1 264.2 265.1 265.2 267.1 267.2 26A 270.2 270.2_M 270.3 272.1 272.1_M 272.2 272.2_M 273.1 273.1_M 273.2 279.1 279.1_M 279.2 279.2_M 2810 282.1 282.2 283.1 283.2 286.1 286.1_M 286.2 286.2_M 289.1 289.1_M 289.2 289.2_M 29

Procedure Id

USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Potassium by FLAAPotassium by FLAAOxidation-Reduction Potential of WaterTotal Gaseous Organic EmissionsTotal Gaseous Organic EmissionsNonmethane Organics in Landfill GasesVolatile Organic Concentration in WasteVapor Phase Organic Concentration in WasteHydrogen Chloride from Stationary SourcesRhenium by FLAARhenium by GFAARhodium by FLAARhodium by GFAARuthenium by FLAARuthenium by GFAAHydrogen Halide/Halogen by IsokineticSelenium by GFAASelenium by GFAASelenium by FLAASilver by FLAASilver by FLAASilver by GFAASilver by GFAASodium by FLAASodium by FLAASodium by GFAAThallium by FLAAThallium by FLAAThallium by GFAAThallium by GFAADissolved Gas SupersaturationTin by FLAATin by GFAATitanium by FLAATitanium by GFAAVanadium by FLAAVanadium by FLAAVanadium by GFAAVanadium by GFAAZinc by FLAAZinc by FLAAZinc by GFAAZinc by GFAAMetals Emissions from Stationary Sources

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 98 of 515

Dade Environmental Resource Management (Florida)

3 3.2-B 3.2-C 3.2-D 3.3-B 3.3-C 3.4 3.5 300(A) 300(B) 300_M 3040 304A 304B 305 305.1 305.2 306 306A 310.1 310.1_M 310.2 3111-B 3111-C 3111-D 3111-E 3112-B 3113-B 3114-B 3114-C 3120 3130 314 320.1 325.1 325.2 325.3 325_M(A) 325_M(B) 330.1 330.2 330.3 330.4 330.5

Procedure Id

USEPA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Gross Alpha and Beta Activity in WaterColiforms in Seawater and ShellfishColiforms in Seawater and ShellfishColiforms in ShellfishColiforms - Cytochrome OxidaseColiforms - IMViCColiforms- Membrane FilterColiforms- Plate CountInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyDetermination of Anions by ICMetals in Oils, Greases and WaxBiodegredation Rates (Vent Option)Biodegredation Rates (Scrubber Option)Emissions of Volatiles in WasteAcidity by Titration with a pH MeterAcidity by Titration Using a pH MeterChromium Emissions from ElectroplatingChromium Emissions from ElectroplatingAlkalinity by TitrationAlkalinity in Water by TitrationAlkalinity by Colorimetric AnalysisMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Extraction/Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by FLAA- Extraction/Nitrous Oxide-Acetylene FlameMercury in Water by CVAAMetals in Water by GFAAMetals in Water by Manual HYDAAMetals in Water by Continuous HYDAAMetals in Water by ICPMetals by Anodic Stripping VoltammetryPerchlorate in Drinking Water using Ion ChromatographyBromide by Titration with IodineChloride by Colorimetric Analysis IChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationChloride in Water by ColorimetryChloride in Water by TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationChlorine by Spectrophotometry with DPD

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 99 of 515

Dade Environmental Resource Management (Florida)

335.1 335.2 335.2(MIDI) 335.2_M(S) 335.2_MA(W) 335.2_MB(W) 335.2_MC(W) 335.3 335.4 335.63 340.1 340.2 340.2_M 340.3 345.1 350.1 350.2(A) 350.2(B) 350.2(C) 350.3 3500-AG(B) 3500-AG(C) 3500-AG(D) 3500-AL(B) 3500-AL(C) 3500-AL(D) 3500-AL(E) 3500-AS(B) 3500-AS(C) 3500-AS(D) 3500-AU 3500-BA(B) 3500-BA(C) 3500-BE(B) 3500-BE(C) 3500-BE(D) 3500-BI 3500-CA(B) 3500-CA(C) 3500-CA(D) 3500-CD(B) 3500-CD(C) 3500-CD(D) 3500-CO(B)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Cyanides Amenable to ChlorinationTotal Cyanide in WaterCyanide Analysis by MIDI DistillationTotal Cyanide in Soils and SedimentsTotal Cyanide in Water by ColorimetryTotal Cyanide in Water by ColorimetryTotal Cyanide in Water by ColorimetryTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryCyanide in Waste by ColorimetryTotal Fluoride by Colorimetric AnalysisFluoride in Water Using an ISEFluoride with an Ion Selective ElectrodeFluoride in Water by ColorimetryIodide in Water by TitrationAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationAmmonia Nitrogen Using an ISESilver in Water by FLAA or GFAASilver in Water by ICPSilver in Water by SpectrophotometryAluminum in Water by FLAA or GFAAAluminum in Water by ICPAluminum in Water by ColorimetryAluminum in Water with an AutoAnalyzerArsenic in Water by GFAA or HYDAAArsenic in Water by SpectrophotometryArsenic in Water by ICPGold in Water by FLAABarium in Water by FLAA or GFAABarium in Water by ICPBeryllium in Water by FLAA or GFAABeryllium in Water by ICPBeryllium in Water by SpectrophotometryBismuth in Water by FLAACalcium in Water by FLAACalcium in Water by ICPCalcium in Water by Titration Using EDTACadmium in Water by FLAA/GFAACadmium in Water by ICPCadmium in Water by SpectrophotometryCobalt in Water by FLAA or GFAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 100 of 515

Dade Environmental Resource Management (Florida)

3500-CO(C) 3500-CR(B) 3500-CR(C) 3500-CR(D) 3500-CR(E) 3500-CS 3500-CU(B) 3500-CU(C) 3500-CU(D) 3500-CU(E) 3500-FE(B) 3500-FE(C) 3500-FE(D) 3500-HG(B) 3500-HG(C) 3500-IR 3500-K-B 3500-K-C 3500-K-D 3500-K-E 3500-LI(B) 3500-LI(C) 3500-LI(D) 3500-MG(B) 3500-MG(C) 3500-MG(D) 3500-MG(E) 3500-MN(B) 3500-MN(C) 3500-MN(D) 3500-MO(B) 3500-MO(C) 3500-NA(B) 3500-NA(C) 3500-NA(D) 3500-NI(B) 3500-NI(C) 3500-OS 3500-PB(B) 3500-PB(C) 3500-PB(D) 3500-PD 3500-PT 3500-RE

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Cobalt in Water by ICPChromium in Water by FLAA or GFAAChromium in Water by ICPTotal Hexavalent Chromium in WaterChromium in Water by Ion ChromatographyCesium in Water by FLAACopper in Water by FLAA or GFAACopper in Water by ICPCopper in Water by Spectrophotometry- Neocuproine MethodCopper in Water by Spectrophotometry- Bathocuproine MethodIron in Water by FLAA or GFAAIron in Water by ICPIron in Water by ColorimetryMercury in Water by CVAAMercury in Water by SpectrophotometryIridium in Water by FLAAPotassium in Water by FLAAPotassium in Water by ICPPotassium in Water by Flame PhotometryPotassium in Water Using an ISELithium in Water by FLAALithium in Water by ICPLithium in Water by Flame PhotometryMagnesium in Water by FLAAMagnesium in Water by ICPMagnesium in Water by Gravimetric AnalysisMagnesium in Water by CalculationManganese in Water by FLAA or GFAAManganese in Water by ICPManganese in Water by SpectrophotometryMolybdenum in Water by FLAAMolybdenum in Water by ICPSodium in Water by FLAASodium in Water by ICPSodium in Water by Flame PhotometryNickel in Water by FLAA or GFAANickel in Water by ICPOsmium in Water by FLAALead in Water by FLAA or GFAALead in Water by ICPLead in Water by SpectrophotometryPalladium in WaterPlatinum in Water by FLAARhenium in Water by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 101 of 515

Dade Environmental Resource Management (Florida)

3500-RH 3500-RU 3500-SB(B) 3500-SB(C) 3500-SE(C) 3500-SE(D) 3500-SE(E) 3500-SE(F) 3500-SE(G) 3500-SE(H) 3500-SE(I) 3500-SN 3500-SR(B) 3500-SR(C) 3500-SR(D) 3500-TH 3500-TI 3500-TL(B) 3500-TL(C) 3500-V-B 3500-V-C 3500-V-D 3500-ZN(B) 3500-ZN(C) 3500-ZN(D) 3500-ZN(E) 3500-ZN(F) 350_M(A) 350_M(B) 350_M(C) 351.1 351.2 351.3(A) 351.3(B) 351.3(C) 351.4 352.1 353.1 353.2 353.2_M 353.3 353.4 354.1 360.1

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Rhodium in Water by FLAARuthenium in Water by FLAAAntimony in Water by FLAA or GFAAAntimony in Water - ICPSelenium in Water by HYDAASelenium in Water by ColorimetrySelenium in Water by FluorimetryVolatile Selenium in WaterNonvolatile Organic Selenium in WaterSelenium in Water by GFAASelenium in Water by ICPTin in Water by FLAA or GFAAStrontium in Water by FLAAStrontium in Water by ICPStrontium in Water by Flame PhotometryThorium in Water by FLAATitanium in Water by FLAAThallium in Water by FLAAThallium in Water by ICPVanadium in Water by FLAAVanadium in Water by ICPVanadium in Water by SpectrophotometryZinc in Water by FLAAZinc in Water by ICPZinc in Water by SpectrophotometryZinc in Water by Spectrophotometry- Dithizone MethodZinc in Water by Spectrophotometry- Dithizone Method IIAmmonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by TitrationAmmonia Nitrogen in WaterTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricTotal Kjeldahl Nitrogen Using an ISENitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionDetermination of Nitrite and NitrateNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 102 of 515

Dade Environmental Resource Management (Florida)

360.2 365.1 365.2 365.3 365.4 365.5 365.6 365_M 370.1 375.1 375.2 375.3 375.4 375_M(A) 375_M(B) 376.1 376.2 377.1 3810 3820 3A 4 405.1 410.1 410.2 410.3 410.4 410_M(A) 410_M(B) 4110-B 4110-C 413.1 413.2 415.1 415.2 415.2_M 418.1 420.1 420.2 420.3 420.4 425.1 430.1 430.2

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA IL/SWSD USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Dissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionOrthophosphate in Water by ColorimetryOrthophosphate in Wet DepositionPhosphorus in Water by ColorimetryDissolved Silica by ColorimetrySulfate by Colorimetry With ChloranilateSulfate in Water by ColorimetrySulfate by Gravimetric DeterminationSulfate by Turbidimetric DeterminationSulfate by ColorimetrySulfate in Water by TurbiditySulfide by Titration with IodineSulfide by Colorimetric DeterminationSulfite in Water by TitrationHeadspace Technique for VolatilesHexadecane Screening for VolatilesOxygen and Carbon Dioxide in AirMoisture Content in Stack Gases5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandLow Level Chemical Oxygen DemandChemical Oxygen Demand in Saline WatersChemical Oxygen Demand by ColorimetryChemical Oxygen Demand by ColorimetryChemical Oxygen Demand by TitrationAnions in Water by Ion ChromatographySingle Column Ion ChromatographyTotal Recoverable Oil and GreaseTotal Recoverable Oil and Grease by IRTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterTotal Organic Carbon in WaterTotal Recoverable Petroleum HydrocarbonsTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterMethylene Blue Active SubstancesNTA by Manual Colorimetric DeterminationNTA by Automated Colorimetric Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 103 of 515

Dade Environmental Resource Management (Florida)

440(S) 440(W) 445 450.1 4500-B-B 4500-B-C 4500-B-D 4500-BR(B) 4500-BR(C) 4500-CL(B) 4500-CL(C) 4500-CL(D) 4500-CL(E) 4500-CL(F) 4500-CL(G) 4500-CL(H) 4500-CL(I) 4500-CL-(B) 4500-CL-(C) 4500-CL-(D) 4500-CL-(E) 4500-CL-(F) 4500-CLO(B) 4500-CLO(C) 4500-CLO(D) 4500-CLO(E) 4500-CN(C) 4500-CN(D) 4500-CN(E) 4500-CN(F) 4500-CN(G) 4500-CN(H) 4500-CN(I) 4500-CN(J) 4500-CN(K) 4500-CN(L) 4500-CN(M) 4500-CO2(B) 4500-CO2(C) 4500-F-B 4500-F-C 4500-F-D 4500-F-E 4500-F-F

Procedure Id

USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Determination of Carbon and NitrogenDetermination of Carbon and NitrogenIn-Vitro Determination of ChlorophyllTotal Organic HalideBoron in Water by Spectrophotometry- Curcumin MethodBoron in Water by Spectrophotometry- Carmine MethodBoron in Water by ICPBromide in Water by SpectrophotometryBromide in Water by Ion ChromatographyResidual Chlorine in Water by Titration- Iodometric Method IResidual Chlorine in Water by Titration- Iodometric Method IIResidual Chlorine in Water by Titration- Amperometric MethodResidual Chlorine in Water by Titration- Low-Level Amperometric MResidual Chlorine in Water by Titration- DPD Ferrous MethodResidual Chlorine by Colorimetry- DPD Colorimetric MethodResidual Chlorine by FACTS- Syringaldazine MethodResidual Chlorine by Iodometirc Electrode TechniqueChloride in Water by Titration- Argentometric MethodChloride in Water by Titration- Mercuric Nitrate MethodChloride in Water by PotentiometryChloride in Water by Colorimetry- Automated Ferricyanide MethodChloride in Water by Ion ChromatographyChlorine Dioxide in Water by Titration- Iodometric MethodChlorine Dioxide in Water by Titration- Amperometric Method IChlorine Dioxide in Water by Colorimetry- DPD MethodChlorine Dioxide in Water by Titration- Amperometric Method IICyanide in Water after DistillationCyanide in Water by TitrationCyanide in Water by ColorimetryCyanide in Water Using ISECyanides Amenable to Chlorination after DistillationCyanides Amenable to Chlorination without DistallationWeak Acid Dissociable Cyanide in WaterCyanogen Chloride in WaterSpot Test for Cyanides for ScreeningCyanates in Waste Using an ISEThiocyanate in WaterCarbon Dioxide in Water by NomographyCarbon Dioxide in Water by TitrationPreliminary Distillation of FluorideFluoride in Water Using an ISEFluoride in Water by SpectrophotometryFluoride in Water by ColorimetryFluoride in Water by Ion Chromatography

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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4500-H 4500-I-(B) 4500-I-(C) 4500-I-B 4500-I-C 4500-NH3(C) 4500-NH3(D) 4500-NH3(E) 4500-NH3(F) 4500-NH3(G) 4500-NH3(H) 4500-NO2(B) 4500-NO2(C) 4500-NO3(B) 4500-NO3(C) 4500-NO3(D) 4500-NO3(E) 4500-NO3(F) 4500-NO3(G) 4500-NO3(H) 4500-NO3(I) 4500-NOR(B) 4500-NOR(C) 4500-O-B 4500-O-C 4500-O-D 4500-O-E 4500-O-F 4500-O-G 4500-O3 4500-P-C

4500-P-D 4500-P-E 4500-P-F

4500-S2(D) 4500-S2(E) 4500-S2(F) 4500-S2(G) 4500-SI(B) 4500-SI(C) 4500-SI(D) 4500-SI(E)

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA

APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

pH in WaterIodide in Water by Spectrophotometry- Leuco Crystal Violet MethodIodide in Water by Spectrophotometry- Catalytic Reduction MethodIodine in Water by SpectrophotometryIodine in Water by TitrationAmmonia in Water by Titrimetric MethodAmmonia in Water by Selective Electrode MethodAmmonia in Water by Selective Electrode Method (Known Addition)Ammonia in Water Using Phenate MethodAmmonia in Water Using Automated Phenate MethodAmmonia in Water - Flow Injection AnalysisNitrite in Water by ColorimetryNitrite in Water by Ion ChromatographyNitrate in Water by Ultraviolet SpectrophotometryNitrate in Water by Ion ChromatographyNitrate in Water Using an ISENitrate in Water- Cadmium ReductionNitrate in Water- Automated Cadmium ReductionNitrate in Water- Titanous Chloride ReductionNitrate in Water- Automated Hydrazine ReductionNitrate in Water- Cadmium Reduction Flow InjectionTotal Kjeldahl Nitrogen in WaterTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Titration- Iodometric MethodTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Titration- Permanganate ModificationTotal Dissolved Oxygen by Titration- Alum Flocculation ModificatiTotal Dissolved Oxygen by Titration- Copper/Sulfate-Sulfamic AcidTotal Dissolved Oxygen by Membrane Electrode MethodResidual Ozone by Indigo Colorimetric MethodPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetryPhosphorus in Water by Stannous Chloride TitrationPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfide in Water by SpectrophotometrySulfide in Water by TitrationSulfide by CalculationSulfide in Water by Ion-Selective Electrode MethodSilica in Water by FLAASilica in Water by Gravimetric AnalysisSilica in Water by Spectrophotometry- Molybdosilicate MethodSilica in Water by Spectrophotometry- Heteropoly Blue Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 105 of 515

Dade Environmental Resource Management (Florida)

4500-SI(F) 4500-SI(G) 4500-SO3(B) 4500-SO3(C) 4500-SO4(B) 4500-SO4(C) 4500-SO4(D) 4500-SO4(E) 4500-SO4(F) 5 5.6 502.1 502.2(ELCD) 502.2(PID) 5021 503.1 5031 5032 504 504.1 5040A 5041 5041A 505 506 507 508 508.1 508A 509 50APP-A 50APP-B 50APP-C 50APP-D 50APP-E 50APP-F 50APP-G 50APP-J 5100 5110 513 515.1 515.2 5210-B

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

Procedure Source

Silica in Water by Automated ColorimetrySilica in Water by ICPSulfite in Water by TitrationSulfite in Water by ColorimetrySulfate in Water by Ion ChromatographySulfate in Water by Gravimetric AnalysisSulfate in Water by Gravimetric AnalysisSulfate by Turbidimetric AnalysisSulfate in Water by ColorimetryParticulate Emissions in AirEnteric VirusesVolatile Halogenated OrganicsVolatile Organic Compounds in WaterVolatile Organic Compounds in WaterVOC Using Equilibrium Headspace AnalysisVolatile Aromatics in Water by GCVolatiles by Azeotropic DistillationVolatiles by Vacuum DistillationEDB and DBCP in Water by GCEDB, DBCP and 123TCP in Water by GCAnalysis of VOST Sorbent CartridgesAnalysis of Sorbent CartridgesDesorption of Sorbent Cartridge by GC/MSOrganohalide Pesticides and PCB in WaterPhthalate and Adipate Esters in WaterNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Pest., Herb. and OrganohalidePCB Screen by Perchlorination and GCEthylene Thiourea in Water by GCSulfur Dioxide in AtmosphereSuspended Particulate MatterCarbon Monoxide in Atmosphere - NDIROzone in the AtmosphereHydrocarbons in AtmosphereNO2 in Atmosphere - ChemiluminescenseLead in Particulate MatterSuspended Particulate Matter (PM10)Volatile Organic Concentration in WasteOrganic Phase Vapor Pressure in WasteTetrachlorodibenzo-p-dioxin in WaterChlorinated Acids in Water by CGC/ECDChlorinated Acids in Water by GC5-Day Biochemical Oxygen Demand

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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5210-C 5220-B 5220-C 5220-D 524.1 524.2 525.1 525.2 531.1 5310-B 5310-C 5310-D 5320-B 547 548 548.1 549 549.1 550 550.1 551 5510-B 5510-C 552 552.1 5520-B 5520-C 5520-D 5520-F 553(LLE) 553(LSE) 5530-C

5530-D 554 5540-C 5540-D 555 5550-B 5560-B 5710-B 5710-C 5710-D 5910-B

Procedure Id

APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA APHA APHA APHA APHA USEPA USEPA APHA

APHA USEPA APHA APHA USEPA APHA APHA APHA APHA APHA APHA

Procedure Source

Ultimate Biochemical Oxygen TestChemical Oxygen Demand by Titration- Open Reflux MethodChemical Oxygen Demand by Titration- Closed Reflux MethodChemical Oxygen Demand by Colorimetry- Closed RefluxPurgeable Organics in Water by GC/MSPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyOrganics in Water by Gas ChromatographyN-Methylcarbamates in Water by HPLCTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodTotal Organic Carbon in Water- Wet-Oxidation MethodDissolved Organic Halogen in WaterGlyphosate in Drinking Water by HPLCEndothall in Water by Gas ChromatographyEndothall in Drinking WaterDiquat and Paraquat in Water by HPLC/UVDiquat and Paraquat in Water by HPLCPolycyclic Aromatic Hydrocarbons by HPLCPolycyclic Aromatic Hydrocarbons by HPLCChlorinated Solvents in Water by GCAquatic Humic Substances in WaterAquatic Humic Substances in WaterHaloacetic Acids in Water by GCHaloacetic Acids in Water by GCOil and Grease by Gravimetric AnalysisOil and Grease by Infrared SpectroscopyOil and Grease by Gravimetric AnalysisHydrocarbons by Gravimetric AnalysisBenzidines and Pesticides in WaterBenzidines and Pesticides in WaterPhenols in Water by Spectrophotometry- Chloroform ExtractionMethPhenols in Water by Spectrophotometry- Direct Photometric MethodCarbonyl Compounds in Water by HPLCAnionic Surfactants in Water as MBASNonionic Surfactants as CTASChlorinated Acids in Water by HPLCTannin and Lignin by ColorimetryNon-Volatile and Volatile Organic AcidsTrihalomethane Formation PotentialTrihalomethane Formation PotentialTrihalomethane Formation PotentialUV - Absorbing Organic Compounds

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

5A 5B 5D 5E 5F 5G 5H 6 (ATM SO2) 6 (FORMALDEHYD)6 (PO-210) 601 6010 6010A 6010B 602 6020 6020_M 603 604(A) 604(B) 604.1 6040-B 6040-C 605 606 607 608 608.1 608.2 609(A) 609(B) 61 610 611 612 613 614 614.1 615 616 617 618 619 620

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA NIOSH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Particulate Emissions in AirNonsulfuric Acid Particulate MatterParticulate Emissions in AirParticulate Emissions in AirNon-Sulfate Particulate Matter in AirParticulate Emissions in AirParticulate Emissions in AirSulfur Dioxide from Stationary SourcesFormaldehyde in Wastewater by GCPolonium-210 in Soil and Air FiltersPurgeable Halocarbons in WastewaterHydrogen Cyanide by Visible AbsorptionICP SpectroscopyInductively Coupled Plasma AESPurgeable Aromatics in Wastewater by GCInductively Coupled Plasma - Mass Spec.Inductively Coupled Plasma - Mass Spec.Acrolein and Acrylonitrile in WastewaterPhenols in Wastewater by GC/FIDPhenols in Wastewater by GC/ECDHexachlorophene and DichlorophenOrganics by Closed Loop StrippingOrganics in Water by Purge and Trap GCBenzidines in Wastewater by HPLCPhthalate Esters in Wastewater by GCNitrosamines in Wastewater by GCOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides in WastewaterOrganochlorine Pesticides in WastewaterNitroaromatics and Isopherone by GCNitroaromatics and IsophoroneHexavalent Chromium in Stack EmissionsPolynuclear Aromatic Hydrocarbons by GCHaloethers in Wastewater by GCChlorinated Hydrocarbons by GCTetrachlorodibenzo-p-dioxin by GC/MSOrganophosphorus Pesticides IOrganophosphorus Pesticides IIChlorinated Herbicides in WastewaterC, H, O Containing Pesticides in WaterOrganohalide Pesticides and PCBsVolatile Pesticides in Water by GCTriazine Pesticides in WastewaterDiphenylamine in Wastewater by GC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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621 6210-B 6210-C 6210-D 6211-B 6211-C 622 622.1 6220-B 6220-C 6220-D 6220-E 6230-B 6230-C 6230-D 6230-E 6231-B 6231-C 6231-D 6232-B 6232-C 6232-D 6233-B 624 624-S 625 625-S 6251-B 6252-B 626 627 629 630 630.1 631 632 632.1 633 633.1 634 635 636 637 638

Procedure Id

USEPA APHA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Carbamate Pesticides - TLCVolatile Organics by Purge and Trap GCVolatile Organics by Purge and Trap GCVolatile Organics by Purge and Trap CGCMethane in Water by Combustable GasMethane in Water by Volumetric AnalysisOrganophosphorus Pesticides III by GCThiophosphate Pesticides in WastewaterVolatile Aromatic Organics in WaterVolatile Aromatic Organics in WaterVolatile Aromatic Organics in WaterVolatile Aromatic Organics in WaterVolatile Halocarbons in Water by GCVolatile Halocarbons in Water by GCVolatile Halocarbons in Water by GCVolatile Halocarbons in Water by GC/MSEDB and DBCP in Water by CGCEDB and DBCP in Water by CGC/MSEDB and DBCP in Water by CGCTrihalomethanes in Water by CGCTrihalomethanes in Water by CGC/MSTrihalomethanes in Water by CGCHaloacetic Acids and TrichlorphenolPurgeable Organics in WastewaterOrganics in Sludge - VolatilesBase/Neutral and Acid Organics in WastewaterOrganics in Sludge - Base/Neutral and AcidDisinfection By-Products: Haloacetic Acids and TrichlorophenolDisinfection By-Products: AldehydesAcrolein and Acrylonitrile by GCDinitroaniline Pesticides in WastewaterCyanazine in Wastewater by HPLCDithiocarbamate Pesticides in WastewaterDithiocarbamate Pesticides in WaterBenomyl and Carbendazim in WastewaterCarbamate Pesticides by HPLC/UVCarbamate Pesticides by HPLC/UVOrganonitrogen Pesticides in WastewaterNitrogen-Containing Pesticides in WaterThiocarbate Pesticides in WastewatersRotenone in Wastewater by HPLCBensulide in Wastewater by HPLC/UVMBTS and TCMTB in Wastewater by HPLCDetermination of Oryzalin in Wastewater

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

639 640 641 6410-B 642 6420-BA 6420-BB 6420-C 643 6431-B 6431-C 644 6440-B 6440-C 645 646 6610-B 6630-B 6630-C 6630-D 6640-B 6651-B 680 6A 6B 6C 7 (ATM NOX) 7 (SR-89/90) 7000A(FLAA) 7000A(GFAA) 7020 7040 7041 7060A 7061A 7062 7063 7080A 7081 7090 7091 7110-B 7110-C 7130

Procedure Id

USEPA USEPA USEPA APHA USEPA APHA APHA APHA USEPA APHA APHA USEPA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA

Procedure Source

Determination of Bendiocarb in WaterMercaptobenzothiazole in WastewatersThiabendazole in Wastewater by HPLCExtractable Semivolatile Organics by GCBiphenyl and Ortho Phenylphenol in WaterPhenols in Water by Gas ChromatographyPhenols in Water by Gas ChromatographyPhenols in Water by Gas ChromatographyDetermination of Bentazon in WastewaterPolychorinated Biphenyls in Water by GCPolychlorinated Biphenyls in Water by GCDetermination of Picloram in WastewaterPolynuclear Aromatic HydrocarbonsPolynuclear Aromatic Hydrocarbons by GCAmine Pesticides and Lethane in WaterDinitro Aromatic Pesticides in WaterCarbamate Pesticides in Water by HPLCOrganochlorine Pesticides in Water by GCOrganochlorine Pesticides in Water by GCOrganochlorine Pesticides in Water by GCChlorinated Phenoxy Herbicides in WaterGlyphosate Herbicide in WaterPesticides and PCBsSulfur Dioxide, Carbon Dioxide, MoistureSulfur Dioxide and Carbon Dioxide in AirSulfur Dioxide from Stationary SourcesNitrogen Oxide from Stationary SourcesStrontium-89 and Strontium-90 in MilkAtomic Absorption - FLAAAtomic Absorption - GFAAAluminum by FLAAAntimony by FLAAAntimony by GFAAArsenic by GFAAArsenic by Gaseous Hydride AAAntimony and Arsenic by GBAAArsenic by ASVBarium by FLAABarium by GFAABeryllium by FLAABeryllium by GFAAGross Alpha and Beta RadioactivityGross Alpha Radioactivity in WaterCadmium by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

7131A 7140 7190 7191 7195 7196A 7197 7198 7199 7200 7201 7210 7211 7380 7381 7420 7421 7430 7450 7460 7461 7470A 7471A 7472 7480 7481 7500-3H(B) 7500-CS(B) 7500-I-B 7500-I-C 7500-I-D 7500-RA(B) 7500-RA(C) 7500-RA(D) 7500-SR(B) 7500-U-B 7500-U-C 7520 7521 7550 7580 7610 7740 7741A

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Cadmium by GFAACalcium by FLAAChromium by FLAAChromium by GFAAHexavalent Chromium (Coprecipitation)Hexavalent Chromium (Colorimetric)Hexavalent Chromium by FLAAHexavalent Chromium by PolarographyHexavalent Chromium in Water by ICCobalt by FLAACobalt by GFAACopper by FLAACopper by GFAAIron by FLAAIron by GFAALead by FLAALead by GFAALithium by FLAAMagnesium by FLAAManganese by FLAAManganese by GFAAMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteMercury by ASVMolybdenum by FLAAMolybdenum by GFAATritium in Water by Liquid ScintillationRadioactive CesiumRadioactive Iodine by PrecipitationRadioactive Iodine by Ion-ExchangeRadioactive Iodine by DistillationRadium in Water by PrecipitationRadium in Water by EmanationRadium in Water by Sequential PrecipitationTotal Radioactive Strontium in WaterUranium in Water by GPC or ScintillationUranium in Water by Isotopic AnalysisNickel by FLAANickel by GFAAOsmium in Various Matrices by FLAAWhite Phosphorous by GCPotassium by FLAASelenium in Various Matrices by GFAASelenium in Water by Gaseous Hydride

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

7742 7760A 7761 7770 7780 7840 7841 7870 7910 7911 7950 7951 7A 7B 7C 7D 7E 8000A 8000B 8010B 8011 8015A 8015B 8020A 8021 8021A(ELCD) 8021A(PID) 8030A 8031 8032 8032A 8033 8040A(ECD) 8040A(FID) 8041 8060(ECD) 8060(FID) 8061 8061A 8070 8070A 8080A 8081(S) 8081(W)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA HACH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Selenium by Gaseous Borohydride AASilver by FLAASilver by GFAASodium by FLAAStrontium by FLAAThallium by FLAAThallium by GFAATin by FLAAVanadium by FLAAVanadium by GFAAZinc by FLAAZinc by GFAANitrogen Oxide from Stationary SourcesNitrogen Oxide from Stationary SourcesNitrogen Oxide from Stationary SourcesNitrogen Oxide from Stationary SourcesNitrogen Oxide from Stationary SourcesOrganic Compounds by Gas ChromatographyOrganic Compounds by Gas ChromatographyHalogenated Volatile Organics by GCEDB and DBCP by Gas ChromatographyNon-Halogenated Volatile OrganicsNon-Halogenated Organics Using GC/FIDAromatic Volatile Organics by GCFree Chlorine in Water by DPDHalogenated and Aromatic VolatilesHalo and Aromatic Volatiles - CGC/PIDAcrolein and Acrylonitrile by GCAcrylonitrile by Gas ChromatographyAcrylamide by Gas ChromatographyAcrylamide by Gas ChromatographyAcetonitrile by GC/NPDPhenols by Gas ChromatographyPhenols by Gas ChromatographyPhenols by Capillary Column GCPhthalate Esters by Gas ChromatographyPhthalate Esters by Gas ChromatographyPhthalate Esters by Gas ChromatographyPhthalate Esters by Capillary GC/ECDNitrosamines by Gas ChromatographyNitrosamines by Gas ChromatographyPesticides and PCBsOrganochlorine Pesticides and PCBsOrganochlorine Pesticides and PCBs

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

8081A(SNB) 8081A(SWB) 8081A(WNB) 8081A(WWB) 8082(S) 8082(W) 8090(ECD) 8090(FID) 8091 8100 8110 8111(S) 8111(W) 8120A 8121 8131 8140 8141(S) 8141(W) 8141A(S) 8141A(W) 8150B 8151(S) 8151(W) 8240B(S) 8240B(W) 8250A 8260A 8260B 8270B(S) 8270B(W) 8270C(S) 8270C(W) 8275 8275A 8280(S) 8280(W) 8280A(O) 8280A(S) 8280A(W) 8290 8310 8315 8315A(LLE)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Organochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBs by GCPCBs as Aroclors by Capillary Column GCPCBs as Aroclors by Capillary Column GCNitroaromatics and Cyclic KetonesNitroaromatics and Cyclic KetonesNitroaromatics and Cyclic KetonesPolynuclear Aromatic Hydrocarbons by GCHaloethers by Gas ChromatographyHaloethers by Gas ChromatographyHaloethers by Gas ChromatographyChlorinated Hydrocarbons by GCChlorinated Hydrocarbons by GCAniline by GC: Capillary ColumnOrganophosphorus Pesticides by GCOrganophosphorus Compounds in Soil by GCOrganophosphorus Compounds in WaterOrganophosphorus Compounds in Soil by GCOrganophosphorus Compounds in WaterChlorinated Herbicides by GCChlorinated Herbicides in Soils by GCChlorinated Herbicides in Water by GCVolatile Organics in Soil by GC/MSVolatile Organics in Water by GC/MSSemivolatile Organics in Water by GC/MSVolatile Organics in Waste by CGC/MSVolatile Organics by CGC/MSSemivolatile Organics in Soil by GC/MSSemivolatile Organics in Water by GC/MSSemivolatile Organic Compounds by CGC/MSSemivolatile Organic Compounds by CGC/MSScreening Semivolatile OrganicsPAHs and PCBs in Soils/Wastes: TE/GC/MSPolychorinated Dioxins and FuransPolychlorinated Dioxins and FuransPolychorinated Dioxins and FuransPolychorinated Dioxins and FuransPolychorinated Dioxins and FuransPolychlorinated PCDDs and PCDFs by HRGC/HRMSPolynuclear Aromatic HydrocarbonsCarbonyl Compounds by HPLCCarbonyl Compounds by HPLC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

8315A(LSE) 8316 8318(S) 8318(W) 8321 8321A 8325(CRT) 8325(DSK) 8325(LLE) 8330(S) 8330(W) 8331(S) 8331(W) 8332 8410(A) 8410(BN) 8430 8440 8515 8520 9 (OPACITY) 9 (TRITIUM) 900 900.1 901 901.1 9010A(A) 9010A(B) 9012 9012A 9013 902 9020B 9021 9022 9023 903 903.1 9030A 9031 9035 9036 9038 904

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Carbonyl Compounds by HPLCAcrylamide, Acetonitrile and Acroleinn-Methylcarbamates by HPLCn-Methylcarbamates by HPLCNon-Volatile Compounds by HPLCNon-Volatile Compounds by HPLC/TS/MSNon-Volatile Compounds by HPLC/PB/MSNon-Volatile Compounds by HPLC/PB/MSNon-Volatile Compounds by HPLC/PB/MSNitroaromatics and Nitramines by HPLCNitroaromatics and Nitramines by HPLCTetrazene in Soil by HPLCTetrazene in Water by HPLCNitroglycerine by HPLCSemivolatile Organics by GC/FTIRSemivolatile Organics by GC/FTIR, B/N ExtrctBis(2-Chloroethyl)Ether Products by GC/FTIRTRPH by Infrared SpectrophotometryColorimetric Method for TNT in SoilFormaldehyde in Ambient AirOpacity of Air EmissionsLow Level Tritium in WaterGross Alpha and Beta Activity in WaterRadium in Drinking WaterRadioactive Cesium in Drinking WaterGamma Emitters in Drinking WaterTotal and Amenable Cyanides by ColorimetryTotal and Amenable Cyanides by TitrationTotal and Amenable CyanidesTotal and Amenable Cyanide (Auto UV)Cyanide Extraction for Solids and OilsRadioactive Iodine in WaterTotal Organic Halides by CoulometryPurgeable Organic Halides in WaterTotal Oganic Halides, Neutron ActivationExtractable Organic Halides in SolidsRadium in Drinking WaterRadium-226 in Drinking WaterAcid Soluble and Acid Insoluble SulfidesExtractable Sulfides by TitrationSulfate by Automated ColorimetrySulfate by Automated ColorimetrySulfate by Turbidimetric DeterminationRadium-228 in Drinking Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

9040A 9041A 9045B 905 9050 9050A 9056 9057 906 9060 9060AM 9065 9066 9067 907 9070 9071A 9075 9076 9077(A) 9077(B) 9077(C) 9078 9079 908 908.1 9080 9081 9131 9132 9200 9200A 9210 9211 9212 9213 9213-D 9214 9215 9215-B 9215-C 9215-D 9216-B 9221-B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA APHA APHA APHA

Procedure Source

pH in Water by Electrometric MeasurementpH using PaperSoil and Waste pHRadioactive Strontium in WaterSpecific ConductanceSpecific ConductanceAnion Chromatography MethodImpinger Solutions for Cl- by ICPTritium in Drinking WaterTotal Organic Carbon in Water and WasteTotal Volatile Organic CarbonTotal Phenolics by SpectroscopyTotal Phenolics by Automated ColorimetryTotal Phenolics by SpectrophotometryActinides in Drinking WaterTotal Recoverable Oil and GreaseOil and Grease in Sludge and SedimentTotal Chlorine in Petroleum ProductsTotal Chlorine in Petroleum ProductsTotal Chlorine in Petroleum ProductsTotal Chlorine in Petroleum ProductsTotal Chlorine in Petroleum ProductsScreening for PCBs in SoilScreening for PCBs in Transformer OilUranium in Drinking WaterUranium in Drinking WaterCation-Exchange Capacity of SoilsCation-Exchange Capacity of SoilsTotal Coliform by Multiple Tube FermentationTotal Coliform by Membrane FilterNitrate in Water by SpectrophotometryNitrate in Water by SpectrophotometryNitrate in Water by ISEBromide in Water by ISEChloride in Water by ISECyanide in Water by ISEE. coli methodFluoride in Water by ISESulfide in Water by ISEHeterotrophic Plate Count- Pour Plate MethodHeterotrophic Plate Count- Spread Plate MethodHeterotrophic Plate Count- Membrane Filter MethodDirect Total Microbial Count- Epifluorescence MethodStandard Total Coliform Fermentation Technique, Multi-tube

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

9221-B.1

9221-C

9221-D 9221-E

9221-F 9222-(B+B.5c)

9222-B 9222-C 9222-D 9222-E 9222-F 9223-B 9230-B

9230-C 9240-B 9250 9250-B 9251 9252A 9253 9310 9315 9320 9510-G 9711-B 9711-C AM-01 B0001 B0005 B0025 B0030 B0035 B0040 B0045 B0050 B0051 B0055 B0060 B0065

Procedure Id

APHA

APHA

APHA APHA

APHA APHA

APHA APHA APHA APHA APHA APHA APHA

APHA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Fermentation TechniqueEscherichia coli Fermentation Technique, Multi-tube FermentationTechniqueEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueEscherichia coli, Multi-tube Fermentation TechniqueTotal Coliform Fermentation Technique, Multi-tube Fermentationwith Enrichment TechniqueStandard Total Coliform Membrane Filter ProcedureStandard Total Coliform- Delayed-Incubation ProcedureFecal Coliform Membrane Filter ProcedureFecal Coliform- Delayed-Incubation ProcedureKlebsiella- Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter TechniqueEnumberation-Enrichment & Isolation of Iron and Sulfur BacteriaChloride by Automated ColorimetryActinomycete Plate CountChloride by Automated ColorimetryChloride in Water and Waste by TitrationChloride in Water and Waste by TitrationGross Alpha and BetaAlpha Emitting Radium Isotopes in WaterRadium-228Assay and Identification of Viruses in Sample ConcentratesImmunofluorescence Method for Giarda & CrytosporidiumProtozoa: Entamoeba histolytica in WaterAmericium-241 in Ashed SamplesStandard Plate Count- Membrane Filter MethodTotal Bacteria- Epifluorescence MethodTotal Coliform Bacteria- Immediate Incubation TestTotal Coliform Bacteria- Delayed Incubation TestTotal Coliform Bacteria- Presumptive Test- MPN MethodTotal Coliform Bacteria- Presumptive Onsite Test- MPN MethodTotal Coliform Bacteria- Confirmation Test- MPN MethodFecal Coliform Bacteria- Immediate Incubation TestFecal Coliform Bacteria- Presumptive Test- MPN MethodFecal Streptococcal Bacteria- Immediate Incubation TestFecal Streptococcal Bacteria- Confirmation TestFecal Streptococcal Bacteria- Presumptive/Confirmation- MPN

Procedure Name

Active

Active

ActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

B0100 B0105 B0400 B0420 B0430 B1505 B1520 B2501 B2520 B3401 B3501 B3520 B3545 B4520 B5001 B5020 B5040 B5050 B6020 B6501 B6520 B6530 B6540 B6560 B6601 B6620 B6630 B6640 B6660 B6700 B8001 B8020 B8040 B8100 B8120 B8502 C-001-1 C-002-1 C-003-1 C-004-1 C-005-1 C-006-1 C-007-1

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

MethoSalmonella and Shigella- Plate CountPseudomonas aeruginosa- Plate CountSulfate-Reducing Bacteria- MPN MethodNitrifying Bacteria- MPN MethodDenitrifying and Nitrate-reducing Bacteria- MPN MethodPhytoplankton Enumberation- Counting Cell MethodPhytoplankton Enumberation- Inverted-Microscope MethodZooplankton Enumberation- Counting Cell MethodZooplankton- Gravimetric Method for Biomass DeterminationSeston- Glass-fiber Filter MethodPeriphyton Enumberation- Sedgwick-Rafter MethodPeriphyton- Gravimetric Method for Biomass DeterminationPeriphyton Enumberation- Inverted-Microscope MethodMacrophytes- Distribution and Abundance (quantitative method)Benthic Invertebrates- Faunal Survey (qualitative method)Benthic Invertebrates- Numerical AssessmentBenthic Invertebrates- Distribution and Abundance (quantitative mBenthic Invertebrate Drift DeterminationAquatic Vertebrates- Life History (quantitative method)Chlorophyll a-b-c in Phytoplankton by SpectroscopyChlorophyll a-b in Phytoplankton by Chromatography/SpectroscopyChlorophyll a-b in Phytoplankton by HP Liquid ChromatographyChlorophyll a-b in Phytoplankton by Chromatography/FluorometryBiomass/Chlorophyll Ratio for PhytoplanktonChlorophyll a-b-c in Periphyton by SpectroscopyChlorophyll a-b in Periphyton by Chromatography/SpectroscopyChlorophyll a-b in Periphyton by HP Liquid ChromatographyChlorophyll a-b in Periphyton by Chromatography/FluorometryBiomass/Chlorophyll Ratio in PeriphytonAdenosine triphosphate (ATP) Determination in Water SampleProductivity- Oxygen Light/Dark-Bottle Method for PhytoplanktonProductivity- Carbon-14 Light/Dark-Bottle Method for PhytoplanktoProductivity- Oxygen Light/Dark-Enclosure Method for PeriphytonProductivity & Community Matabolism by Diel O2-Curve Stratified WProductivity & Community Metabolism by Diel O2-Curve StreamsAlgal Growth Potential (AGP) Spikes for Nutrient LimitationAlkalinity of Water by TitrationCOD by Open RefluxAnions by Ion ChromatographyTotal Hardness by ColorimetryOil and Grease by Extraction/GravimetryTotal Dissolved Solids in WaterTotal Organic Carbon in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

C-008-1 C-01 C-010-1 C-011-1 C-012-1 C-013-1 C-014-1 C-015-1 C-017-1 C-018-1 C-019-1 COLIFORM CR-01 CTM-001 CTM-002 CTM-004 CTM-005 CTM-006 CTM-010 CTM-011 D1125(A) DIOX(O) DIOX(S) DIOX(W) E-SPEC(CMPX) E-SPEC(IR) E-SPEC(PRCP) E-SPEC(UV) EV-024 EV-025 FE-01 FP H-01 H-02 H-03 HERL_001 HERL_002 HERL_003 HERL_004 HERL_005 HERL_006 HERL_007 HERL_008 HERL_009

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLDADE USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA ASTM USEPA USEPA USEPA USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USEPA USEPA USEPA 21FLDADE USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Total Suspended Solids in WaterCarbon-14 in Aqueous SamplesSoil Extractable Organics by GravimetrySoil % Moisture by GravimetryFree Liquid in Wastes by FiltrationSoil pHSpecific Gravity of SoilTotal Carbon in Soil by CombustionWater Level Measurement in WellsControlled Pumping Test in WellsSlug Test for Hydraulic ConductivityColiformChromium-51 in Water SamplesDetermination of Butadiene EmissionsDetermination of Particulate MatterDetermination of HCl EmissionsDetermination of Condensable EmissionsChromium Emissions from ElectroplatersPerchloroethylene of Wet Waste MaterialsDetermination of Halogenated OrganicsConductivity and Resistivity in WaterPCDD and PCDF in Chemical Waste by CGC/MSPCDD and PCDF in Soil by CGC/MSPCDD and PCDF in Water by CGC/MSMinor Elements by ComplexingMinor Elements by Residue-IRMinor Elements by PrecipitationMinor Elements by Residue-UVTin and Triorganotin in WastewaterTin and Triorganotin in WastewaterIron-55 in Water SamplesField ParameterTritium in Milk, Soil, Urine and BiotaTritium in WaterTritium in WaterOrganchlorine Pesticides in TissueHCB and Mirex in TissuePesticides in Tissue and Human MilkPesticides in Blood or SerumPentachlorophenol in BloodPentachlorophenol and Salts in UrineBis(p-Chlorophenyl) Acetic Acid in Urine2,4-D and 2,4,5-T in UrineKepone in Blood and Environmental Samples

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

HERL_010 HERL_011 HERL_012 HERL_013 HERL_014 HERL_016 HERL_017 HERL_018 HERL_020 HERL_021 HERL_022 HERL_023 HERL_024 HERL_025 HERL_026 HERL_030 HYDRO I-001-1 I-002-1 I-003-1 I-004-1 I-005-1 I-006-1 I-01 I-02 I-03 I1020 I1030 I1051 I1052 I1054 I1055 I1060 I1062 I1084 I1095 I1110 I1112 I1114 I1125 I1135 I1136 I1137 I1152

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLDADE USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Pesticides and Metabolites in TissueMetabolites or Hydrolysis Productspara-Nitrophenol in UrineCholinesterase Activity in Blood1-Naphthol in UrinePesticides in AirPCBs in Human Milk by Macro MethodPCBs in Human Milk by Micro MethodPCBs in Adipose TissueTCDD ResiduesAnalysis of Water for PesticidesAnalysis of Water for HerbicidesInsecticides in Soils and HousedustInsecticides in Bottom SedimentPesticides in Human Tissue and MilkInfrared SpectroscopyHydrolab Field MeasurementMetals in Soil by XRFDigestion/Analysis of Soil by Flame AAHexavalent ChromiumDigestion/Analysis of Waters by FLAAMercury by CVAAMercury by CVAAIodine-131 in Drinking WaterIodine-131 in MilkLow Level Iodine-131 in MilkAcidity in Water by TitrationAlkalinity in Water by TitrationAluminum in Water by FLAAAluminum in Water by Chelation and FLAAAluminum by D-C Plasma SpectrometryAntimony in Water by Hydride AAArsenic in Water by ColorimetryArsenic in Water by HYDAABarium in Water by FLAABeryllium in Water by FLAABoron in Water by ColorimetryBoron in Water by ColorimetryBoron in Water by DC Plasma SpectrometryBromide in Water by TitrationCadmium in Water by FLAACadmium in Water by Chelation and FLAACadmium in Water by GFAACalcium in Water by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Dade Environmental Resource Management (Florida)

I1183 I1184 I1187 I1230 I1232 I1235 I1236 I1238 I1239 I1240 I1241 I1250 I1270 I1271 I1272 I1300 I1325 I1327 I1370 I1371 I1381 I1399 I1400 I1401 I1425 I1447 I1454 I1455 I1456 I1462 I1472 I1490 I1499 I1500 I1501 I1520 I1524 I1540 I1550 I1586 I1600 I1601 I1602 I1630(S)

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Chloride in Water by TitrationChloride in Water by TitrationChloride in Water by ColorimetryHexavalent Chromium by ColorimetryHexavalent Chromium in Water by FLAAChromium in Water by GFAAChromium in Water by FLAAChromium in Water by Chelation and FLAACobalt in Water by FLAACobalt in Water by Chelation and FLAACobalt in Water by GFAAColor in Water by Visual ComparisonCopper in Water by FLAACopper in Water by Chelation and FLAACopper in Water by GFAACyanide in Water by ColorimetryFluoride in Water by ColorimetryFluoride in Water Using an ISEIodide in Water by TitrationIodide in Water by ColorimetryIron in Water by FLAALead in Water by FLAALead in Water by Chelation and FLAALead in Water by GFAALithium in Water by FLAAMagnesium in Water by FLAAManganese in Water by FLAAManganese in Water by GFAAManganese in Water by Chelation and FLAAMercury in Water by CVAAMetals in Water by ICPMolybdenum by Chelation and FLAANickel in Water by FLAANickel in Water by Chelation and FLAANickel in Water by GFAAAmmonia Nitrogen by NesslerizationAmmonia Nitrogen in Water Using an ISENitrite-Nitrogen in Water by ColorimetryAmmonia plus Organic Nitrogen in WaterWater pHDissolved Phosphorus by ColorimetryOrthophosphate-Phosphorus by ColorimetryOrthophosphate plus Hydrolyzable PhosphorousPotassium in Bottom Material by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Dade Environmental Resource Management (Florida)

I1630(W) I1667(S) I1667(W) I1700 I1702 I1720 I1735(S) I1735(W) I1749 I1750 I1780 I1800(S) I1800(W) I1820 I1866 I1880 I1900(S) I1900(W) I1901 I2030 I2057 I2058 I2062 I2115 I2128 I2129 I2187 I2188 I2302 I2327 I2462 I2521 I2522 I2523 I2539 I2540 I2543 I2545(S) I2545(W) I2552 I2558 I2598 I2599 I2600(S)

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Potassium in Water by FLAASelenium in Bottom Material by HYDAASelenium in Water by HYDAASilica in Water by ColorimetrySilica in Water by FLAASilver in Water by Chelation and FLAASodium in Bottom Material by FLAASodium in Water by FLAAResidue by Evaporation and GravimetricResidue by Evaporation and GravimetricSpecific ConductanceStrontium in Bottom Material by FLAAStrontium in Water by FLAASulfate in Water by TitrationThallium in Water by GFAAVanadium in Water by ColorimetryZinc in Bottom Material by FLAAZinc in Water by FLAAZinc in Water by GFAAAlkalinity in Water by TitrationAnions in Water by Ion ChromatographyAnions in Water by Ion ChromatographyArsenic in Water by HYDAABoron in Water by Automated ColorimetryBromide in Water by Ion ChromatographyBromide in Water by ColorimetryChloride in Water by Automated ColorimetryChloride in Water by ColorimetryCyanide in Water by ColorimetryFluoride in Water Using an ISEMercury in Water by CVAAAmmonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by ColorimetryNitrite-Nitrogen in Water by ColorimetryNitrite-Nitrogen in Water by ColorimetryNitrite- plus Nitrate-Nitrogen in WaterNitrite- Plus Nitrate-Nitrogen in SolidsNitrite- Plus Nitrate-Nitrogen in WaterAmmonia plus Organic Nitrogen in WaterAmmonia plus Organic Nitrogen in WaterOrthophosphate-Phosphorus by ColorimetryPhosphorus by Auto-Discrete ColorimetryPhosphorus in Solids by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Dade Environmental Resource Management (Florida)

I2600(W) I2601 I2602 I2667(S) I2667(W) I2700 I2822 I2823 I2851(S) I2851(W) I2880 I3051 I3052 I3054 I3055 I3060 I3062 I3084 I3095 I3110 I3112 I3135 I3136 I3152 I3153 I3236 I3238 I3239 I3240 I3270 I3271 I3300 I3325 I3381 I3399 I3400 I3425 I3447 I3448 I3454 I3462 I3490 I3499 I3500

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Phosphorus in Water by ColorimetryOrthophosphate-Phosphorus by ColorimetryHydrolyzable plus Orthophosphate-PhosphorousSelenium in Bottom Material by HYDAASelenium in Water by HYDAASilica in Water by ColorimetrySulfate in Water by ColorimetrySulfate in Water by TurbidimetryTin in Bottom Material by HYDAATin in Water by HYDAAVanadium in Water by ColorimetryAluminum in Water by FLAAAluminum in Water by Chelation and FLAAAluminum by D-C Plasma SpectrometryAntimony in Water by Hydride AAArsenic in Water by ColorimetryArsenic in Water by HYDAABarium in Water by FLAABeryllium in Water by FLAABoron in Water by ColorimetryBoron in Water by ColorimetryCadmium in Water by FLAACadmium in Water by Chelation and FLAACalcium in Water by FLAACalcium in Water by FLAAChromium in Water by FLAAChromium in Water by Chelation and FLAACobalt in Water by FLAACobalt in Water by Chelation and FLAACopper in Water by FLAACopper in Water by Chelation and FLAACyanide in Water by ColorimetryFluoride in Water by ColorimetryIron in Water by FLAALead in Water by FLAALead in Water by Chelation and FLAALithium in Water by FLAAMagnesium in Water by FLAAMagnesium in Water by Direct EPA FLAAManganese in Water by FLAAMercury in Water by CVAAMolybdenum by Chelation and FLAANickel in Water by FLAANickel in Water by Chelation and FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 122 of 515

Dade Environmental Resource Management (Florida)

I3524 I3561 I3562(S) I3562(W) I3631 I3736 I3750 I3765 I3840 I3860 I4062 I4302 I4327 I4521 I4522 I4523 I4552 I5051 I5055 I5060 I5062 I5084 I5095 I5110 I5135 I5152 I5236 I5239 I5270 I5300 I5381 I5399 I5425 I5447 I5454 I5462 I5473 I5474 I5475 I5490 I5499 I5553 I6062 I6302

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Ammonia Nitrogen in Water Using an ISEChemical Oxygen Demand by ColorimetryChemical Oxygen Demand by TitrationChemical Oxygen Demand by TitrationPotassium in Water by FLAASodium in Water by FLAAResidue by Evaporation and GravimetricResidue by Evaporation and GravimetricSulfide in Water by TitrationNephelometric Turbidity in WaterArsenic in Water by HYDAACyanide in Water by ColorimetryFluoride in Water Using an ISEAmmonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by ColorimetryAmmonia Plus Organic Nitrogen in WaterAluminum in Bottom Material by FLAAAntimony in Bottom Material by HYDAAArsenic in Bottom Material by ColorimetryArsenic in Bottom Material by HYDAABarium in Bottom Material by FLAABeryllium in Bottom Material by FLAABoron in Bottom Material by ColorimetryCadmium in Bottom Material by FLAACalcium in Bottom Material by FLAAChromium in Bottom Material by FLAACobalt in Bottom Material by FLAACopper in Bottom Material by FLAACN in Bottom Material by ColorimetryIron in Bottom Material by FLAALead in Bottom Material by FLAALithium in Bottom Material by FLAAMagnesium in Bottom Material by FLAAManganese in Bottom Material by FLAAMercury in Bottom Material by CVAAMetals in Sediment by FLAAMetals in Sediment by FLAAMetals in Sediment by HYDAAMolybdenum by Chelation and FLAANickel in Bottom Material by FLAAAmmonia plus Organic Nitrogen in SolidsArsenic in Bottom Material by HYDAACN in Bottom Material by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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I6522 I6523 I6552 I7051 I7052 I7054 I7055 I7060 I7062 I7084 I7095 I7110 I7112 I7135 I7136 I7152 I7236 I7238 I7239 I7240 I7270 I7271 I7325 I7327 I7381 I7399 I7400 I7425 I7447 I7454 I7462 I7490 I7499 I7500 I7552 ICP-AES IM-002-1 IM-003-1 INTERIM1 INTERIM2 IP-10A IP-10B IP-1A IP-1A-B

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Ammonia Nitrogen by Colorimetry in SolidAmmonia Nitrogen by Colorimetry in SolidAmmonia Plus Organic Nitrogen in SolidsAluminum in Water by FLAAAluminum in Water by Chelation and FLAAAluminum by D-C Plasma SpectrometryAntimony in Water by Hydride AAArsenic in Water by ColorimetryArsenic in Water by HYDAABarium in Water by FLAABeryllium in Water by FLAABoron in Water by ColorimetryBoron in Water by ColorimetryCadmium in Water by FLAACadmium in Water by Chelation and FLAACalcium in Water by FLAAChromium in Water by FLAAChromium in Water by Chelation and FLAACobalt in Water by FLAACobalt in Water by Chelation and FLAACopper in Water by FLAACopper in Water by Chelation and FLAAFluoride in Water by ColorimetryFluoride in Water Using an ISEIron in Water by FLAALead in Water by FLAALead in Water by Chelation and FLAALithium in Water by FLAAMagnesium in Water by FLAAManganese in Water by FLAAMercury in Water by CVAAMolybdenum by Chelation and FLAANickel in Water by FLAANickel in Water by Chelation and FLAAAmmonia Plus Organic Nitrogen in WaterInductively Coupled PlasmaField Screening by Portable XRFMetals by Flame AAHydrogen Cyanide Released from WastesHydrogen Sulfide Released from WastesRespirable Particulates in Indoor AirRespirable Particulates in Indoor AirVolatiles in Air - SUMMA CanisterVolatiles in Air - Portable GC/PID

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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IP-1A-C IP-1B IP-2A IP-2B IP-3A IP-3B IP-3C IP-5A IP-5B IP-5C IP-6A IP-6B IP-6C IP-7-A IP-7-B IP-8 ITM-001 KR-01 LC_PEST LC_SV LC_VOA MC_PEST(S) MC_PEST(W) MC_SVOA MC_SVOA(LS) MC_SVOA(MS) MC_SVOA(W) MC_VOA MC_VOA(LS) MC_VOA(MS) MC_VOA(W) O-001-1 O-002-1 O-003-1 O-004-1 O-005-1 O-006-1 O-008-1 O-009-1 O1105 O3100 O3104 O3105 O3106

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Installation and Operation ProcedureVolatiles in Air - Adsorbent TubesNicotine in Indoor Air - XAD-4Nicotine in Indoor Air-CassetteCarbon Monoxide in Air - NDIRCarbon Monoxide in Air - GFCCarbon Monoxide in Air - ECONitrogen Dioxide - Air, LuminescenceNitrogen Dioxide - Air, Palmes TubesNitrogen Dioxide - Air, IONCHRFormaldehyde - Indoor Air, HPLCFormaldehyde in Air - ColorimetricFormaldehyde in Air - Passive SamplingB(a)P in Air by GC/FID and GC/MSB(a)P and PAHs in Air by HPLCOrganochlorine Pesticides - Indoor AirMetals Emissions from Stationary SourcesKrypton-85 in Environmental Air SamplesLow Concentration Water for PesticidesSemivolatiles in Low Concentration WaterVolatile Organics in Low Concentration WaterOrganic Analysis For Pesticides/AroclorsOrganic Analysis For Pesticides/AroclorsScreening Semivolatile Organic ExtractsSemivolatile Organics in Low Conc. SoilsSemivolatile Organics in Medium Conc. SoilSemivolatile Organics in WatersScreening of Hexadecane ExtractsVolatile Organics in Low Concentration SoilsVolatile Organics in Medium Conc. SoilsVolatile Organics in Multi-Conc. WatersPentachlorophenol in SoilTPH in Soil by IR of Freon ExtractTPH in Soil by GC/PID of Methanol ExtractTPH in Soil by GC/FID of CH2Cl2 ExtractsPhenols in Water and Soil by GCTPH by Headspace GC/PIDPentachlorophenol in Soil by GC/ECDTPH in Soil by GC/FID of CH2Cl2 ExtractsDissolved Chlorophenoxy Acids in WaterTotal Organic Carbon in WaterOrganochlorine and -phosphorous in WaterTotal Chlorophenoxy Acids in WaterTotal Recoverable Triazines in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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O3107 O3108 O3109 O3110 O3111 O3112 O3113 O3114 O3115 O3117 O3118 O5101 O5104 O5105 O5108 O7100 O7104 O7105 O9104 OA-001-1 OA-002-1 OA-003-1 OA-004-1 OA-005-1 OA-006-1 OHC OSW-A OSW-B P-001-1 P-002-1 P-003-1 P-004-1 P-005-1 P-006-1 P-007-1 P-008-1 P-009-1 P-01 P-011-1 P-02 PAH-001(S) PAH-001(W) PAH-002 PAH-005

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Carbamate Pesticides in WaterExtractable Oil and Grease in WaterLight Fuel Oils in WaterTotal Recoverable Phenols in WaterMethylene Blue Active Substance in WaterTNT, RDX and Picric Acid in WaterPolynuclear Aromatic HydrocarbonsEthylene and Propane in WaterPurgeable Organic Compounds in WaterAcid Extractable Compounds in WaterBase/Neutral Extractable CompoundsTotal Carbon in Bottom MaterialOrganochlorine and -phosphorous in SolidChlorophenoxy Acids in Bottom MaterialExtractable Oil and GreaseSuspended Organic Carbon in WaterOrganochlorine and -phosphorous in SolidChlorophenoxy Acids in SedimentOrganochlorine Compounds in Fish TissueField Use of Sentex Scentograph GCVOCs by GC/MS of Cartridges/CylindersField Survey with PID Vapor DetectorField Use of Photovac Portable GCField Use of Photovac Portable GCPhotovac Portable GC for Soil/Water/AirOrganics Analysis, Multi-Media, Hi-ConcMetals in Incinerator ExhaustsHexavalent Chromium in Stack EmissionsChlorinated Pesticides in SoilField Screen for Chlorinated PesticidesChlorinated Pesticides in WaterField Screen for Chlorinated PesticidesOrganophosphorus Pesticides in WaterOrganophosphorus Pesticides in SoilPhenoxyherbicides in Soil/SedimentPhenoxyherbicides in WaterCLP Pesticide/PCB in Water/Soil by GC/ECPhosphorus-32 in Fish MuscleChlorinated Pesticides in Soil by GC/ECDStable Phosphorous in Biological SamplesField Analysis of PAHs by GC/FIDField Analysis of PAHs by GC/FIDPAHs in Water by GC/FIDPolycyclic Aromatic Hydrocarbons in Soil

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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PAH-006 PAH-008 PAH-009 PAH-011 PAH-012 PART_1 PART_2 PART_3 PB-01 PCB-002 PCB-003 PCB-004 PCB-005 PCB-006 PCB-008 PCB-009 PM-01 PM-02 PMD-ACA PMD-ACG(GC) PMD-ACG(LC1) PMD-ACG(LC2) PMD-AKY(GC1) PMD-AKY(GC2) PMD-AM-S PMD-AMN PMD-AMT PMD-ANF(GC) PMD-ANF(IR) PMD-ANT PMD-ANY PMD-AS(ATE) PMD-AS(ITE) PMD-AS(TIT1) PMD-AS(TIT2) PMD-AS(TIT3) PMD-AS(TIT4) PMD-AS(TIT5) PMD-ASU PMD-ATR PMD-ATR(GC1) PMD-ATR(GC2) PMD-ATR(IR) PMD-ATR(LC)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Polycyclic Aromatic Hydrocarbons in WaterTotal PAHs in SoilAnalysis of PAHs by GC/FID and GC/PIDAnalysis of PAHs in Soil by GC/FIDAnalysis of PAHs in Soil by HPLCTrihalomethanes in Water by Purge and TrapTrihalomethanes in Drinking Water by GCMaximum Total Trihalomethane PotentialLead-210 in Water and Solid SamplesField Screening of PCBs in SoilPCBs in WaterScreening for PCBs in WaterPCBs and Pesticide in SoilPCBs in Soil as Decachlorobiphenyl by GCField Analysis of PCBs in SoilPCBs in Soil and OilPromethium-147 in Aqueous and Urine SamplesPromethium-147 in Feces AshAcifluorfen by HPLCAcephate, Dicofol and Triforine by GCDicofol by HPLCTriforine by HPLCAlachlor by GCAlachlor by GCAMS by Sodium Nitrate Titration4-Aminopyridine by UV SpectroscopyAmitrole by Visible SpectroscopyAnilazine by GCAnilazine by IR SpectroscopyAntimycin A by UV SpectroscopyANTU by UV SpectroscopyArsenate by TitrationSodium Arsenite by TitrationTotal Arsenic by TitrationTotal Arsenic by TitrationInorganic Arsenic Compounds by TitrationOrganic Arsenic by Digestion and TitrationArsenic in Organic Compounds by TitrationAsulam by UV SpectroscopyAtrazine and Metolachlor by GC/FIDAtrazine by GCAtrazine and Metolachlor by GCAtrazine by IR SpectroscopyAtrazine by HPLC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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PMD-AZN PMD-BDX PMD-BEB(IR) PMD-BEB(LC) PMD-BEB(UV) PMD-BEE(GC) PMD-BEE(IR) PMD-BEH(IR) PMD-BEH(UV) PMD-BEL(IR) PMD-BEL(LC) PMD-BEN(LC) PMD-BEN(UV) PMD-BEO PMD-BIL PMD-BIN PMD-BOR PMD-BRA PMD-BRO PMD-BYA(GC1) PMD-BYA(GC2) PMD-BYA(LC1) PMD-BYA(LC2) PMD-CAO PMD-CAP(GC1) PMD-CAP(GC2) PMD-CAP(IR) PMD-CAP(LC) PMD-CAV(LC) PMD-CAV(UV) PMD-CBF PMD-CBX(IR) PMD-CBX(UV) PMD-CD PMD-CGV PMD-CHP PMD-CIB PMD-CJL PMD-CJO(LC) PMD-CJO(UV1) PMD-CJO(UV2) PMD-CKA PMD-CKL(GC) PMD-CKL(IR)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Azinphos-Methyl by IR SpectroscopyBenalaxyl by GCBendiocarb by IR SpectroscopyBendiocarb by HPLCBendiocarb by UV SpectroscopyBenefin by GCBenefin by IR SpectroscopyBenomyl by IR SpectroscopyBenomyl by UV SpectroscopyBensulide by IR SpectroscopyBensulide by HPLCBentazon by HPLCBentazon by UV SpectroscopyThiobencarb by GC/FIDBitertanol by GCBinapacryl by IR SpectroscopyBoron Compounds by Ignition and TitrationBromadiolone by HPLCBromacil by GCButylate by GCButylate by GCButylate by HPLCButylate by HPLCCaptafol by IR SpectroscopyCaptan by GCCaptan, Carbaryl and Naled by GCCaptan by IR SpectroscopyCaptan by HPLCCarbaryl by HPLCCarbaryl by UV SpectroscopyCarbofuran by IR SpectroscopyCarboxin by IR SpectroscopyCarboxin by UV SpectroscopyCadmium by AASChlorbromuron by GCChlorflurecol-Methyl Ester by UV Spec.Chlorobenzilate by GCChloroneb by UV SpectroscopyChlorophacinone by HPLCChlorophacinone by UV SpectroscopyChlorophacinone by UV SpectroscopyChloropicrin and 1,3-DCPs by GCChlorothalonil by GCChlorothalonil by IR Spectroscopy

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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PMD-CKR(GC) PMD-CKR(IR) PMD-CLD(GC) PMD-CLD(IR) PMD-CLD(UV) PMD-CLV PMD-CMN PMD-COQ PMD-COR(GC) PMD-COR(IR) PMD-COR(LC) PMD-CPH PMD-CRO PMD-CU-S PMD-CUC PMD-CYZ(GC1) PMD-CYZ(GC2) PMD-CYZ(GC3) PMD-DAL PMD-DCA(GC1) PMD-DCA(GC2) PMD-DEE(GC) PMD-DEE(LC) PMD-DFN PMD-DGL PMD-DGV PMD-DIC PMD-DJA PMD-DJG PMD-DME PMD-DMF PMD-DNE PMD-DNR PMD-DNZ(IR) PMD-DNZ(TITR) PMD-DOG PMD-DOZ(LC1) PMD-DOZ(LC2) PMD-DOZ(UV) PMD-DPA(GC) PMD-DPA(IR) PMD-DPF PMD-DQT PMD-DSN(GC)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chloroxuron by GCChloroxuron in Dust by IR SpectroscopyChlorpyrifos by GCChlorpyrifos by IR SpectroscopyChlorpyrifos by UV SpectroscopyChlorsulfuron by HPLCCinmethalin by GCCoumafuryl by UV SpectroscopyCoumaphos by GCCoumaphos by IR SpectroscopyCoumaphos by HPLCChlorophenoxy Herbicide Technical DataCrotoxyphos by GCCupric Ion by Ion ChromatographyCyanazine by IR SpectroscopyCyromazine in Trigard 75W by GCCyromazine in Armor by GCCyromazine in Armor Premix by GCDalapon by IR Spectroscopy2,4-D and 2,4,5-T Esters by GC2,4-D and Silvex by Derivatization GCDEET by GCDEET by HPLCDiazinon by HPLCDibutyl Succinate by TitrationDichlone by IR SpectroscopyDICA by HPLCDichloran in Dusts by IR SpectroscopyDicrotophos by IR SpectroscopyDimethoate by GCDioxins in 2,4-D and 2,4,5-T by GC/MSDimethyl Phthalate by GCDinitramine by GCDinocap by IR SpectroscopyDinocap by TKN and TitrationDinoseb by IR SpectroscopyDiphacinone by HPLCDiphacinone by HPLCDiphacinone in Baits by UV SpectroscopyDiphenamid by GCDiphenamid by IR SpectroscopyDiphenylamine by GCDiquat (Dibromide) by HPLCDisulfoton and Fensulfothion by GC/FID

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

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PMD-DSN(IR) PMD-DUR(IR) PMD-DUR(LC) PMD-EDF PMD-ENA PMD-ENB(GC) PMD-ENB(TITR) PMD-EPI PMD-EPT PMD-ETF PMD-ETI(GC) PMD-ETI(IR) PMD-ETN(GC) PMD-ETN(IR) PMD-EUX(GC) PMD-EUX(TITR) PMD-EZN PMD-FBP PMD-FBR PMD-FCL(GC) PMD-FCL(IR) PMD-FKN PMD-FLM PMD-FLM(IR) PMD-FLM(UV) PMD-FOL PMD-FON PMD-GLP PMD-HXE PMD-HXO(GC) PMD-HXO(LC) PMD-INB PMD-KAR(IR) PMD-KAR(LC) PMD-LIN PMD-LIU(IR) PMD-LIU(LC) PMD-LIU(UV) PMD-LMG PMD-LTF(LC1) PMD-LTF(LC2) PMD-MAL(IR) PMD-MAL(LC) PMD-MAU(GC1)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Disulfoton by IR SpectroscopyDiuron by IR SpectroscopyDiuron by HPLCEdifenphos by GCEndosulfan by IR SpectroscopyEndothall by GCEndothall by TitrationEpichlorohydrin by GCEPTC by HPLCEthofumesate by GCEthion by GCEthion by IR SpectroscopyEthoprop by GCEthoprop by IR SpectroscopyEthyl Hexanediol by GC/TCDEthyl Hexanediol by Acetylation & TitrationEthiozin by HPLCFenamiphos by GC/FIDFenarimol by GC/FIDRonnel by GC/FIDRonnel by IR SpectroscopyFluchloralin by GC/TCDAtrazine and Metolachlor by GCFluometuron by IR SpectroscopyFluometuron by UV SpectroscopyFolpet by IR SpectroscopyFonofos by IR SpectroscopyGlyphosate by HPLCHexachlorophene by HPLCHexazinone by GC/TCDHexazinone by HPLCIndolebutyric Acid by UV SpectroscopyKarbutilate by IR SpectroscopyKarbutilate by HPLCLindane by IR SpectroscopyLinuron by IR SpectroscopyLinuron by HPLCLinuron by UV SpectroscopyLemongrass Oil by GC/TCDLactofen by HPLCLactofen by HPLCMalathion by IR SpectroscopyMalathion by HPLCEthylenethiourea by GC/TCD

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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PMD-MAU(GC2) PMD-MBL PMD-MBT(TITR) PMD-MBT(UV) PMD-MDZ PMD-MEA(GC) PMD-MEA(IR) PMD-MEL PMD-MEM PMD-MER PMD-MET PMD-MEY(GC) PMD-MEY(IR) PMD-MEY(LC) PMD-MFX PMD-MGC PMD-MGU(GC) PMD-MGU(IR) PMD-MHX PMD-MHY(LC) PMD-MHY(UV) PMD-MOK(GC) PMD-MOK(IR) PMD-MON(IR) PMD-MON(TITR) PMD-MON(UV) PMD-NA-D PMD-NA-H PMD-NAP PMD-NBL PMD-NCS PMD-NEB(IR) PMD-NEB(UV) PMD-NIC PMD-NOB PMD-NTP(TIT1) PMD-NTP(TIT2) PMD-ORY PMD-OVO PMD-OXB PMD-P-HS PMD-PAD(GC) PMD-PAD(IR) PMD-PAP

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Ethylenethiourea by GC/FIDMyclobutanil by GC/FID2-Mercaptobenzothiazole by Titration2-Mercaptobenzothiazole by UV SpectroscopyMerphos by Internal Standard GCMetaldehyde by GC/TCDMetaldehyde by IR SpectroscopyMethidathion by GC/FIDMethiocarb by IR SpectroscopyMethomyl by HPLCMethoprene by Internal Standard GCMethoxychlor by GC/FIDMethoxychlor by IR SpectroscopyMethoxychlor by HPLCMetalaxyl by Internal Standard GCMethyl Nonyl Ketone (MNK) by GC/TCDMetobromuron by GC/TCDMetobromuron by IR SpectroscopyMexacarbate by GC/TCDMaleic Hydrazide (MH) by HPLCMaleic Hydrazide by UV SpectroscopyMonocrotophos by GC/FIDMonocrotophos by IR SpectroscopyMonuron by IR SpectroscopyMonuron by Hydrolysis and TitrationMonuron by UV SpectroscopySodium Chlorate and Metaborate by TitrationSodium Fluoride by Ion ChromatographyNaphthaleneacetic Acid by HPLCNaptalam by UV SpectroscopyNicosulfuron by HPLCNeburon by IR SpectroscopyNeburon by UV SpectroscopyNicotine by HPLCNorbormide by UV SpectroscopyNitrophenols by TitrationNitrophenols by TitrationOryazlin by UV SpectroscopyOvex by IR SpectroscopyOxamyl by HPLCPhosphorus by Digestion and Gravimetryp-Dichlorobenzene by GCp-Dichlorobenzene by IR SpectroscopyParaquat by HPLC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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PMD-PAR(GC) PMD-PAR(LC) PMD-PBS PMD-PCP(GC) PMD-PCP(LC) PMD-PFH(GC) PMD-PFH(TD) PMD-PFI PMD-PGM PMD-PIE(LC) PMD-PIE(UV) PMD-PIO PMD-PIX PMD-PJB PMD-PJE(GC) PMD-PJM PMD-PNM(GC) PMD-PNM(LC) PMD-POD PMD-POJ PMD-POT(GC) PMD-POT(IR) PMD-PPD PMD-PYA(IR) PMD-PYA(UV) PMD-PYR(GC1) PMD-PYR(GC2) PMD-PYR(LC1) PMD-PYR(LC2) PMD-PYR(TD) PMD-PYR(TITR) PMD-QAC(COLR) PMD-QAC(TD) PMD-QAC(TIT1) PMD-QAC(TIT2) PMD-QAC(TIT3) PMD-RES(GC1) PMD-RES(GC2) PMD-RES(IR) PMD-RES(LC) PMD-ROT PMD-S-UF(GRV1 PMD-S-UF(GRV2 PMD-S-UF(GRV3

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Parathion in Carbaryl by GC/FIDParathion by HPLCPolybrominated Salicylanilides by UVPentachlorophenol by GC/FIDPentachlorophenol by HPLCPhenols and Chlorophenols by GC/TCDPhenols and Chlorophenols Technical DataPhenothiazine by IR SpectroscopyPhorate by IR SpectroscopyPindone by HPLCPindone by UV SpectroscopyPiperonyl Butoxide Qualitative TestPendimethalin by GC/TCDPirimicarb by UV SpectroscopyPirimiphos-Ethyl by GC/FIDPirimiphos-Methyl by GC/FIDProchloraz by GC/FIDProchloraz by HPLCPrometon and Simazine by GC/FIDPropylene Glycol by GC/TCDPropargite by GC/TCDPropargite by IR SpectroscopyPropionic Acid by GC/FIDPyrazon by IR SpectroscopyPyrazon by UV SpectroscopyPyrethrins by GC/FIDPyrethrins, MGK-264 and PBTO by HPLCPyrethrins by HPLCPyrethrins, MGK-264 and PBTO by HPLCPyrethrins, Technical DataPyrethrins I and II by TitrationQuaternary Ammonium Compounds QualitativeQuaternary Ammonium Compound Technical DataQuaternary Ammonium Compounds FerricyanideQuaternary Ammonium Compounds, Epton Titr.Quaternary Ammonium Cl and Br by TitrationResmethrin in Aerosols by GCResmethrin by GC/FIDResmethrin by IR SpectroscopyResmethrin in Aerosols by HPLCRotenone by HPLCSulfur by CS2 Extraction and GravimetrySulfur by Oxidation and GravimetrySulfur by CS2 Extraction and Gravimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

PMD-S-UO PMD-SAE PMD-SEU PMD-SIM PMD-SN PMD-STM(UV) PMD-STM(VIS) PMD-STY(GRAV) PMD-STY(LC) PMD-STY(UV) PMD-TBU PMD-TDU PMD-TDZ PMD-TEI PMD-TFB PMD-TFK PMD-TFM PMD-TFU PMD-TFZ PMD-THN PMD-THO PMD-THR(IR) PMD-THR(LC) PMD-THR(UV) PMD-TLC(OTP) PMD-TLC(TLC1) PMD-TLC(TLC2) PMD-TLL PMD-TPR PMD-TQA PMD-TQO PMD-TRC(GC1) PMD-TRC(GC2) PMD-TRC(IR) PMD-TRC(LC) PMD-TSU PMD-VAE PMD-VER(IR) PMD-VER(LC) PMD-WAR PMD-WAR(LC) PMD-WAR(UV) PMD-WTY PMD-ZIR

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Sulfur Dioxide by TitrationSalicylanilide by UV SpectroscopySiduron by UV SpectroscopySimazine by UV SpectroscopyTin in Organotins by TitrationStreptomycin by UV SpectroscopyStreptomycin by Visible SpectroscopyStrychnine by Acid PrecipitationStrychnine by HPLCStrychnine by UV SpectroscopyTribenuron Methyl Ester by HPLCTebuthiuron by UV SpectroscopyTechnazene by GC/FIDTerbacil by UV SpectroscopyTetrachlorvinphos by GC/FIDTetramethrin by GC/FIDTriflumizole by HPLCLamprecid by UV SpectroscopyThiabendazole by GC/FIDThiophanate by UV SpectroscopyThiophanate-Methyl by UV SpectroscopyThiram by IR SpectroscopyThiram by HPLCThiram by UV SpectroscopyOrganothiophosphates by TLCTLC Systems for Pesticide IdentificationTLC Systems for Pesticide IdentificationTriadimenol by GC/FIDTriclopyr by HPLCTriallate by GC/FIDbis(Tri-n-butyltin) Oxide by GCTrichlorfon by GC/FIDTrichlorfon by Derivatization and GC/FIDTrichlorfon by IR SpectroscopyTrichlorfon by HPLCTrifluralin by IR SpectroscopyPMP by UV SpectroscopyVernolate by IR SpectroscopyVernolate by HPLCWarfarin and Sulfaquinoxaline by HPLCWarfarin by HPLCWarfarin by UV SpectroscopyTriethylene Glycol by GC/TCDZiram by UV Spectroscopy

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

PMD-ZN-T(GC) PMD-ZN-T(TITR PU-01 PU-02 R-001-1 R-002-1 R-004-1 R-005-1 R-006-1 R-007-1 R-008-1 R1110 R1130 R1140 R1141 R1142 R1150 R1160 R1171 R1172 R1173 R1174 R1180 R1181 R1182 RA-01 RA-02 RA-03 RA-04 RA-05 S-001-1 S-002-1 S-003-1 S-004-1 SFSAS_1 SFSAS_10 SFSAS_11 SFSAS_12 SFSAS_13 SFSAS_14 SFSAS_15 SFSAS_16 SFSAS_17 SFSAS_18

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Zinc Phosphide by GC/FPDZinc Phosphide by TitrationPlutonium in Water and Ashed SamplesPlutonium-236 Tracer SolutionQC for Alpha/Beta Sample AnalysisGross Alpha/Beta Activity in SoilGross Alpha/Beta Activity in WaterGross Alpha/Beta Activity in WaterGross Alpha and Beta Activity in SoilGross Alpha/Beta Activity in BiotaGross Alpha/Beta Activity in Biota, ExtendedCesium-137 and 134, DissolvedLead-210RadiumRadium-226Radium-228RadiorutheniumStrontium-90Tritium - Liquid Scintillation, Denver LabTritium - Electrolytic, Denver LabTritium - Liquid Scintillation, Reston LabTritium - Electrolytic, Reston LabUranium - FluorometricUranium - Fluorometric, ExtractionUranium - Alpha SpectroscopyRadium-226 in SolidsRadium-226 in UrineRadium-226 in Water SamplesRadium-226 De-emanation ProcedureRadium-228 in Water SamplesSemivolatiles in Water by CS2 ExtractionField Screening Semivolatiles in WaterSemivolatiles in Soil (MeCl2 Extraction)Field Screening Semivolatiles in SoilTotal Organic Carbon in SedimentPhenols in SedimentMercury in SedimentMercury in FishMetals in SedimentMetals in FishArsenic and Selenium in SedimentOrganics in SedimentEthylene Glycol in WaterTotal Organic Carbon in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Dade Environmental Resource Management (Florida)

SFSAS_19 SFSAS_2 SFSAS_20 SFSAS_21 SFSAS_22 SFSAS_23 SFSAS_24 SFSAS_25 SFSAS_26 SFSAS_27 SFSAS_28 SFSAS_29 SFSAS_3 SFSAS_4 SFSAS_5 SFSAS_6 SFSAS_7 SFSAS_8 SFSAS_9 SOP SR-01 SR-02 SR-03 SR-04 TH-01 TO-1 TO-10 TO-11 TO-12 TO-13 TO-14 TO-14B TO-2 TO-3 TO-4 TO-5 TO-6 TO-7 TO-8 TO-9 U-01 VA-001-1 VA-002-1 VA-003-1

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLDADE USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Total Organic Carbon in SedimentPCBs in Transformer Fluid and Waste OilTotal Phosphates in WaterSoil Volume by Volumetric MethodSoil Volume by Displacement MethodFlow of Water Through SoilPermeability of Cohesionless SoilPermeability of SoilPermeability of Soil with Back PressurePermeability of Soil with ConsolidometerPermeability of Soil Using Constant-HeadOrganics in Biological TissueChlorinated Pesticides in SedimentsChlorinated Pesticides in FishPurgeable Organics in FishOrganics in FishPurgeable Organics in SedimentCyanide in SedimentCyanide in FishDERM SOPRadiostrontium in Food Ash and SolidsRadiostrontium in MilkStrontium-90 in UrineRadiostrontium in Aqueous MediaThorium-234 Tracer SolutionVolatile Nonpolar Organics in AirOrganochlorine Pesticides in AirFormaldehyde in Ambient AirNon-Methane Organic in Ambient AirBenzo(a)Pyrene and PAHs - Ambient AirVolatile Organics in Air by GCVolatile Organics by Portable GCHighly Volatile Nonpolar OrganicsVolatile Nonpolar Organics in AirO-C Pesticides and PCB - Ambient AirAldehydes and Ketones in AirPhosgene Determination in AirN-Nitrosodimethylamine in AirCresols and Phenols in Air by HPLCDioxin in Air by HRGC/HRMSUranium-232 Tracer SolutionVOCs in Air by GC of Sorbent TubesHalogenated VOCs in Air by GC/ELCDVOCs in Air by Portable GC/PID

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 135 of 515

Dade Environmental Resource Management (Florida)

VA-004-1 VA-005-1 VA-006-1 VA-007-1 VA-008-1 VG-001-1 VG-002-1 VG-003-1 VG-004-1 VG-005-1 VG-006-1 VG-007-1 VG-008-1 VG-009-1 VG-010-1(ECD) VG-010-1(PID) VG-011-1 VS-001-1 VS-002-1 VS-003-1 VS-004-1 VS-005-1 VS-006-1 VW-001-1 VW-002-1 VW-003-1 VW-004-1 VW-005-1 VW-006-1 VW-007-1 VW-008-1 VW-010-1(S) VW-010-1(W) VW-011-1 VW-012-1 VW-013-1 VW-014-1 XENO X_89_176(N) X_89_176(P)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Halogenated VOCs in Air by Direct GC/ECVOCs in Air by Purge and Trap GCVOCs in Ambient Air by Portable GC/PIDVOCs in Ambient Air by Direct GC/PIDVOCs in Air by Automated Portable GCVOCs in Soil Gas by Adsorbent TubeHalogenated VOCs in Soil Gas by GC/ELCDHalogenated VOCs in Soil Gas by GC/ECHalogenated VOCs in Soil Gas by GC/ECDHalogenated VOCs in Soil Gas by GC/PIDVOCs in Soil Gas by Purge and Trap GCVOCs in Air by Thermal Desorption GCVOCs in Soil Gas by GC of Sorbent TubesVOCs in Soil Gas by Direct GC/PIDVOCs in Soil Gas by Portable GCVOCs in Soil Gas by Portable GCVOCs in Gas by Purge and Trap GC/ELCD/PIDVOCs in Soil by Purge and Trap GCVOCs in Soil by Automated Headspace GCVOCs in Soil by GC/ECD of ExtractVOCs in Soil by GC/FID of CS2 ExtractsVOCs in Soil by Headspace GC/PIDVOCs in Water/Soil by Purge and Trap GCVOCs in Water by Purge and Trap GCVOCs in Water by Automated Headspace GCVOCs in Water by Automated Headspace GCVOCs in Water by Manual Headspace GCVOCs in Water by GC/ECD of ExtractsVOCs in Water by GC/FID of CS2 ExtractsVOCs in Water by Headspace GC/PIDVOCs in Water by Purge and Trap GCVOCs in Water/Soil by Headspace GC/PIDVOCs in Water/Soil by Headspace GC/PIDVOCs in Water/Soil by Purge and Trap GCVOCs in Water/Soil by Purge and Trap GCVOCs in Water/Soil by Headspace GC/FIDVOCs in Water by Purge and Trap GCXenobiotic Contaminants in FishChlorinated Herbicides by LC/MSChlorinated Herbicides by LC/MS

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLDADE

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Page 136 of 515

Division of Environmental Health, Bureau of Water (Florida)

ENTERO FECAL

Procedure Id

21FLDOH 21FLDOH

Procedure Source

EnterococcusFecal coliform

Procedure Name

ActiveActive

Status21FLDOH

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Page 137 of 515

Lee County (Florida)

10200-H 110.2 120.1 130.2 150.1 160.2 160.4 1600 1600

1631 170.1 180.1 200.7(W) 200.8(W) 200.9 202.1 202.2 204.2 206.2 208.1 208.2 210.1 210.2 2120-B 213.1 213.2 218.1 218.2 218.4 219.2 220.1 220.2 2320 2340 239.1 239.1_M 239.2 243.1 245.1 245.2 249.1 249.2 2510

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA 21FLEECO USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHNon-Filterable Residue - TSSVolatile ResidueMembrane Filter Test Method for Enterococci in WaterEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Mercury in Water by Oxidation, Purge and Trap, and CVAFSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAAluminum by GFAAAntimony by GFAAArsenic by GFAABarium by FLAABarium by GFAABeryllium by FLAABeryllium by GFAAColor in Water by Visual ComparisonCadmium by FLAACadmium by GFAAChromium by FLAAChromium by GFAAHexavalent Chromium by FLAACobalt by GFAACopper by FLAACopper by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationLead by FLAALead by FLAALead by GFAAManganese by FLAAMercury in Water by CVAAMercury by CVAANickel by FLAANickel by GFAAConductivity in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLEECO

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Page 138 of 515

Lee County (Florida)

2520-B 2540-C 2540-E 270.2 270.3 272.1 272.2 273.1 279.1 279.2 289.1 300(A) 310.1 3111-B 3111-D 3113-B 325.3 330.4 335.4 350.1 3500-CA(B) 3500-CR(B) 351.2 353.2 354.1 360.1 360.2 365.1 365.4 370.1 375.4 376.1 405.1 40CFR114,142 410.1 410.4 413.1 415.1 415.2 418.1 4500-CL-(B) 4500-CL-(F) 4500-CLO(D) 4500-CLO(E)

Procedure Id

APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLEECO USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA

Procedure Source

Salinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterFixed and Volatile Solids in WaterSelenium by GFAASelenium by FLAASilver by FLAASilver by GFAASodium by FLAAThallium by FLAAThallium by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAChloride by Mercuric Nitrate TitrationTotal Residual Chlorine by TitrationCyanide by Semi-Automated ColorimetryAmmonia Nitrogen by ColorimetryCalcium in Water by FLAAChromium in Water by FLAA or GFAATotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate by Turbidimetric DeterminationSulfide by Titration with Iodine5 Day Biochemical Oxygen DemandAsbestos FibersMid-Level Chemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterTotal Recoverable Petroleum HydrocarbonsChloride in Water by Titration- Argentometric MethodChloride in Water by Ion ChromatographyChlorine Dioxide in Water by Colorimetry- DPD MethodChlorine Dioxide in Water by Titration- Amperometric Method II

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLEECO

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Page 139 of 515

Lee County (Florida)

4500-CN(E) 4500-F-C 4500-I-(B) 4500-P-C

4500-SI(F) 504 505 507 508 515.1 5210-B 5210-C 5220-B 525.2 5310-B 548 6010A 7060A 7470A 7500-U-C 8071 83-15 9012 9215-B 9221-B

9221-E

9222-B 9222-D 9230-B

9230-C ACS RC7 P601 AMMONIUM ANSI/AWWAB601-0AWWA B300-87 AWWA B303-88 COLOR DEP SOP 02/01 DTKN + NOX ELEVATION EPA 501.2 EPA1311-6010

Procedure Id

APHA APHA APHA APHA

APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA APHA HACH 21FLEECO USEPA APHA APHA

APHA

APHA APHA APHA

APHA 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO

Procedure Source

Cyanide in Water by ColorimetryFluoride in Water Using an ISEIodide in Water by Spectrophotometry- Leuco Crystal Violet MethodPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetrySilica in Water by Automated ColorimetryEDB and DBCP in Water by GCOrganohalide Pesticides and PCB in WaterNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandUltimate Biochemical Oxygen TestChemical Oxygen Demand by Titration- Open Reflux MethodOrganics in Water by Gas ChromatographyTotal Organic Carbon by Combustion-Infrared MethodEndothall in Water by Gas ChromatographyICP SpectroscopyArsenic by GFAAMercury in Liquid Wastes by CVAAUranium in Water by Isotopic AnalysisSulfite in Water by TitrationFormaldehydeTotal and Amenable CyanidesHeterotrophic Plate Count- Pour Plate MethodStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter TechniqueSodium HydroxideAmmonium AnalysisSodium bisulfiteChlorine in Sodium HypochloriteSodium ChloriteColor at 654nmFDEP SOP for Lab AnalysisDissolved NitrogenWater Surface ElevationChloroformTCLP Metals Analysis

Procedure Name

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLEECO

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Page 140 of 515

Lee County (Florida)

FDOT 924-2.2 FL PRO NITRATE ONIT SECCHI SM 4500-S2 SM20 4500-CO2 DSM20 4500CO2 TH - TA TKN + NOX TKN - NH3 TOTAL NITROGEN USGS I-2700-85

Procedure Id

21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO 21FLEECO

Procedure Source

Total Alkalinity PercentFL PRO Total Petroleum HydrocarbonsNitrogen, Nitrate (NOx-NO2)Nitrogen, Organic (TKN-NH3)Secchi diskUnionized Hydrogen SulfideAlkalinity, CarbonateAlkalinity, HydroxideTotal Hardness, AlkalinityTotal Nitrogen AnalysisOrganic NitrogenNitrogen, Total (TKN+NOx)Colorimetry analysis for Silica

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLEECO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 141 of 515

Environmental Research and Design, Inc (Florida)

10200-H 110.3 120.1 150.1 160.2 180.1 310.1 350.1 353.3 4500-P-E 9222-D ALKPERDIG

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLERDI

Procedure Source

Chlorophyll a-b-c DeterminationColor by Spectrophotometric AnalysisConductancepHNon-Filterable Residue - TSSTurbidity by NephelometryAlkalinity by TitrationAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionPhosphorus in Water by Colorimetry- Ascorbic Acid MethodFecal Coliform Membrane Filter ProcedureAlkaline Persulfate Digestion

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLERDI

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Page 142 of 515

Florida Fish & Wildlife C C / Marine Research Institute

00-01 00-02 00-03 110.2 180.1 200.7(S) 200.8(S) 245.1 350.1 351.2 353.2 353.4 365.1 365.2 365.5 370.1 415.1 445 502.1 502.2(ELCD) 505 507 508 515.1 524.1 525.1 525.2 531.1 553(LLE) 601 604.1 607 609(A) 610 611 617 619 633 645 8081(S) 8141A(S) 8250A 8270B(S) 8275A

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Gross Alpha and Beta Activity in WaterGross Alpha Activity in Drinking Water by CoprecipitationLead-210 and Polonium-210 in Dried SamplesColor Analysis Using Platinum/CobaltTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Wastes by ICP/MSMercury in Water by CVAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDetermination of Nitrite and NitratePhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryOrthophosphate in Water by ColorimetryDissolved Silica by ColorimetryTotal Organic Carbon by CombustionIn-Vitro Determination of ChlorophyllVolatile Halogenated OrganicsVolatile Organic Compounds in WaterOrganohalide Pesticides and PCB in WaterNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECDPurgeable Organics in Water by GC/MSOrganics in Water by Gas ChromatographyOrganics in Water by Gas ChromatographyN-Methylcarbamates in Water by HPLCBenzidines and Pesticides in WaterPurgeable Halocarbons in WastewaterHexachlorophene and DichlorophenNitrosamines in Wastewater by GCNitroaromatics and Isopherone by GCPolynuclear Aromatic Hydrocarbons by GCHaloethers in Wastewater by GCOrganohalide Pesticides and PCBsTriazine Pesticides in WastewaterOrganonitrogen Pesticides in WastewaterAmine Pesticides and Lethane in WaterOrganochlorine Pesticides and PCBsOrganophosphorus Compounds in Soil by GCSemivolatile Organics in Water by GC/MSSemivolatile Organics in Soil by GC/MSPAHs and PCBs in Soils/Wastes: TE/GC/MS

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLFMRI

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Page 143 of 515

Florida Fish & Wildlife C C / Marine Research Institute

PROC 1 SCP-ALL

Procedure Id

21FLFMRI 21FLFMRI

Procedure Source

Hydrolab Field Sample ProceduresEMAP Field Lab Collection Procedures

Procedure Name

ActiveActive

Status21FLFMRI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 144 of 515

Florida Department of Environmental Protection

10200-G 10200-H 110.2 120.1 150.1 160.1 160.1_M 160.2 160.2_M 170.1 180.1 200.1 200.10_M 200.7(W) 200.8(W) 202.1 2120-B 2130 215.1 236.1 242.1 245.1 245.2 2510 2520-B 2540-C 2540-D 258.1 273.1 300(A) 310.1 325.3 330.5 340.2 350.1 351.1 351.2 353.2 353.3 354.1 360.1 360.2 365.1 365.2

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Zooplankton Counting TechniquesChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsTemperatureTurbidity by NephelometryMetals in Marine Waters by ICP/MSInductively Coupled PlasmaMetals in Water by ICP-AESMetals in Waters by ICP/MSAluminum by FLAAColor in Water by Visual ComparisonTurbidity in WaterCalcium by FLAAIron by FLAAMagnesium by FLAAMercury in Water by CVAAMercury by CVAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterPotassium by FLAASodium by FLAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Mercuric Nitrate TitrationChlorine by Spectrophotometry with DPDFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryPhosphorus by Single Reagent Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLFTM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 145 of 515

Florida Department of Environmental Protection

365.4 365.5 370.1 405.1 415.1 4500-CL(B) 4500-CL-(B) 4500-H 4500-O-G 5210-B 5220-B 6010B 6020 614 8081(W) 8141A(W) 9221-B

9222-B 9222-D D5176 DEPSOP 001/01 EPA 600 FT_1100 FT_1200 FT_1300 FT_1400 FT_1500 FT_1600 FT_1700

FT_1800 FT_1900 GC-011-5 GC-012-3 LC-001 LC-001-1 LC-006-2 LC-008-3 P3-1 P3-2 P3-4 SOP-AB03_1 SOP-AB04

Procedure Id

USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA

APHA APHA ASTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM

21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM 21FLFTM

Procedure Source

Total Phosphorus After Block DigestionOrthophosphate in Water by ColorimetryDissolved Silica by Colorimetry5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Titration- Argentometric MethodpH in WaterTotal Dissolved Oxygen by Membrane Electrode Method5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Open Reflux MethodInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Organophosphorus Pesticides IOrganochlorine Pesticides and PCBsOrganophosphorus Compounds in WaterStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureNitrogen in Water by Pyrolysis DetectionDEP Field Analytical ProceduresEPA 600/9-78-018 (mod.) - AGP AnalysisField measurement of pHField measurement of Specific ConductanceField measurement of SalinityField measurement of TemperatureField measurement of Dissolved OxygenField measurement of TurbidityField measurement of Light Penetration (Secchi Depth andTransparency)Field measurement of Water Flow and VelocityContinuous Monitoring with Installed MetersDEP SOP: GC-011-5 (based on EPA 608 and 617)DEP SOP: GC-012-3 (based on EPA 614, 619, 622, 633 and 507)DEP SOP: LC-001-1DEP SOP: LC-001-1 (based on EPA 8321A)DEP SOP: LC-006-2 (based on EPA 531.1)DEP SOP: LC-008-3total coliformTDSTOCPhytoplankton-Quantitative-#Diatom TaxaPhytoplankton-Quantitative-# Wet Taxa

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLFTM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 146 of 515

Florida Department of Environmental Protection

SOP-AB05 SOP-BB15_5

Procedure Id

21FLFTM 21FLFTM

Procedure Source

DEP Phytoplankton (Diatom) Analysis ProcedureDEP Sediment Analysis Procedure

Procedure Name

ActiveActive

Status21FLFTM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 147 of 515

Georgia Environmental Protection Division

110.2 130.2 150.1 160.2 180.1 200.7(W) 200.8(W) 2320 245.1 2510 2510 351.1 353.2 365.1 405.1 4500-NH3(G) 4500-O-G 5210-B 5310-B 5550-B 6010B 9221-E

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA NIOSH APHA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA APHA

Procedure Source

Color Analysis Using Platinum/CobaltTotal HardnesspHNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSAlkalinity in Water by TitrationMercury in Water by CVAA1-Octanethiol by GC/FPDConductivity in WaterTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry5 Day Biochemical Oxygen DemandAmmonia in Water Using Automated Phenate MethodTotal Dissolved Oxygen by Membrane Electrode Method5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodTannin and Lignin by ColorimetryInductively Coupled Plasma AESEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechnique

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLGAEP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 148 of 515

National Health and Environmental Effect Research-NHEERL(FL)

160.2_M 2540-G CHE.03.09 INS.01.04

Procedure Id

USEPA APHA 21FLGBO1 21FLGBO1

Procedure Source

Total Suspended SolidsTotal, Fixed and Volatile SolidsCHE.03.09 - Astoria Pacific API 300 autoanalyzerINS.01.04-Fluorometric determination of Chlorophyll-a using a non-acidification method (Welschmeyer) with Methanol

Procedure Name

ActiveActiveActiveActive

Status21FLGBO1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 149 of 515

Gilcrist County Well Watch (Florida)

2510 353.2 8008 8021 8039 8167 8192 8507

Procedure Id

APHA USEPA HACH HACH 21FLGCWW HACH 21FLGCWW HACH

Procedure Source

Conductivity in WaterNitrate-Nitrite Nitrogen by ColorimetryTotal Iron in WaterFree Chlorine in Water by DPDNitrate, HR (0 to 30.0 mg/L ) NO3- NTotal Chlorine in Water by DPDNitrate, LR (0 to 0.5 mg/L) NO3- NNitrite in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

Status21FLGCWW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 150 of 515

Florida Fish and Wildlife Conservation Commission

10200-H 2130 2320 2320 FIELD

2340-B 2510 2540-B 2540-D 2540-E 2540-G 2550 2580 310.1 3111-B 3500-FE(D) 375.4 419-D 4500-F-C 4500-H 4500-NH3-B,C 4500-NOR(B) 4500-NORG-B 4500-O-B 4500-O-G 4500-P-D 5550-B 9212 STATION OBS STATION WEATHER

Procedure Id

APHA APHA APHA 21FLGFWF

21FLGFWF APHA APHA APHA APHA APHA APHA APHA USEPA APHA APHA USEPA 21FLGFWF APHA APHA 21FLGFWF APHA 21FLGFWF APHA APHA APHA APHA USEPA 21FLGFWF 21FLGFWF

Procedure Source

Chlorophyll a-b-c DeterminationTurbidity in WaterAlkalinity in Water by TitrationAlkalinity in Water by field titration using phenophthalein andbromcresol green indicatorsHardness by calculationConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterTotal, Fixed and Volatile SolidsTemperature of Water by ThermometerOxidation-Reduction Potential of WaterAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameIron in Water by ColorimetrySulfate by Turbidimetric DeterminationNitrate in Water by the Brucine MethodFluoride in Water Using an ISEpH in WaterAmmonia in Water by Distillation and NesslerizationTotal Kjeldahl Nitrogen in WaterOrganic Nitrogen by Macro-Kjeldahl Method and NesslerizationTotal Dissolved Oxygen by Titration- Iodometric MethodTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Stannous Chloride TitrationTannin and Lignin by ColorimetryChloride in Water by ISEField Station Visit Direct Physical Measurements and ObservationsField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLGFWF

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 151 of 515

Gulf Power Company (Florida)

150.1 160.2 170.1 180.1 200.7(W) 220.2 2340 245.1 310.1 325.2 351.2 360.1 365.4 375.4 415.1 4500-SO4(D) 9050A FT 1100 FT 1200 FT 1400 FT 1500 SM 2320B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA 21FLGPC 21FLGPC 21FLGPC 21FLGPC 21FLGPC

Procedure Source

pHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESCopper by GFAAHardness in Water by EDTA TitrationMercury in Water by CVAAAlkalinity by TitrationChloride by Colorimetric Analysis IITotal Kjeldahl Nitrogen by ColorimetryDissolved Oxygen Using an ISETotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionSulfate in Water by Gravimetric AnalysisSpecific ConductanceField measurement of Hydrogen Ion Activity (pH)Field measurement of Specific ConductanceField measurement of TemperatureField measurement of Dissolved OxygenAlkalinity determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLGPC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 152 of 515

Guana Tolomato Matanzas (GTM) Esturarine (NERR - Florida)

10200-H 2120-B 2130 2540-D 4500-H 4500-NO3(F) 4500-P-E 4500-SI(D) AMMONIA

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA 21FLGTM

Procedure Source

Chlorophyll a-b-c DeterminationColor in Water by Visual ComparisonTurbidity in WaterTotal Suspended Solids in WaterpH in WaterNitrate in Water- Automated Cadmium ReductionPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSilica in Water by Spectrophotometry- Molybdosilicate MethodPhotometric determination of ammonia in seawater

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLGTM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 153 of 515

FL Dept. of Environmental Protection

10200-F 10200-G 10200-H 10300-C 110.2 1103_1 120.1 150.1 160.1 160.2 170.1 180.1 200.7_M 200.8(W) 300_M 310.1 340.2 350.1 351.2 351.2 SEDIMENT 353.2 360.1 365.1 365.4 365.4 SEDIMENT 415.1 5210-B 600 6010B 6020 8260B 8270C(S) 900456 903.1 9230-C EPA 8081/8082

FT1100GW FT1200GW FT1300GW FT1400GW FT1500GW FT1700GW FT1800GW

Procedure Id

APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLGW USEPA USEPA USEPA USEPA 21FLGW USEPA APHA NIOSH USEPA USEPA USEPA USEPA 21FLGW USEPA APHA 21FLGW

21FLGW 21FLGW 21FLGW 21FLGW 21FLGW 21FLGW 21FLGW

Procedure Source

Phytoplankton Counting TechniquesZooplankton Counting TechniquesChlorophyll a-b-c DeterminationPeriphyton Sample AnalysisColor Analysis Using Platinum/CobaltE. coli in Water by Membrane FiltrationConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryICP-AES For Trace Element AnalysisMetals in Waters by ICP/MSDetermination of Anions by ICAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTOTAL KJELDAHL NITROGEN IN SOLID MATRICESNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionTOTAL PHOSPHORUS IN SOLID MATRICESTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandRespirable Particulates by GravimetricInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Volatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSQA Plan #900456Radium-226 in Drinking WaterFecal Streptococcus and Enterococcus, Membrane Filter TechniqueORGANOCHLORINE PESTICIDES IN SEDIMENT MATRICES BYGC/ECDpH, fieldSpecific conductance, fieldSalinity, fieldTemperature, fieldDissolved oxygen, fieldSeechi depth, fieldStream Flow, Instantaneous

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

Status21FLGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 154 of 515

FL Dept. of Environmental Protection

GC-011-5 GC-012-3 HG-008-3

LC-006-2 NU-076-1

Procedure Id

21FLGW 21FLGW 21FLGW

21FLGW 21FLGW

Procedure Source

DEP SOP: GC-011-5 (based on EPA 608 and 617)DEP SOP: GC-012-3 (based on EPA 614, 619, 622, 633 and 507)MERCURY IN SOLID SAMPLES USING COLD VAPOR AASPECTOROSCOPYDEP SOP: LC-006-2 (based on EPA 531.1 and 8321A)PERCENT CARBON IN SOLID MATRICES

Procedure Name

ActiveActiveActive

ActiveActive

Status21FLGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 155 of 515

Harbor Branch Oceanographic Institution (Florida)

350.1 353.2 365.1

Procedure Id

USEPA USEPA USEPA

Procedure Source

Ammonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry

Procedure Name

ActiveActiveActive

Status21FLHBOI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 156 of 515

Hillsborough County Environmental (Florida)

10200-H 110.2 160.1 160.2 160.3 1600

180.1 200.7(W) 213.1 215.1 218.1 220.1 236.1 239.1 242.1 243.1 245.1 249.1 2550 258.1 273.1 289.1 340.2 350.1 351.2 365.4 370.1 375.4 4500-CL-(E) 4500-NH3(H) 4500-NO3(F) 4500-P-F

5210-B 9222-B 9222-D 9230-C AIRTEMP COLOR CONDUCTANCE DEPTHO DEPTHPD DO

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA

APHA APHA APHA 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Turbidity by NephelometryMetals in Water by ICP-AESCadmium by FLAACalcium by FLAAChromium by FLAACopper by FLAAIron by FLAALead by FLAAMagnesium by FLAAManganese by FLAAMercury in Water by CVAANickel by FLAATemperature of Water by ThermometerPotassium by FLAASodium by FLAAZinc by FLAAFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate by Turbidimetric DeterminationChloride in Water by Colorimetry- Automated Ferricyanide MethodAmmonia in Water - Flow Injection AnalysisNitrate in Water- Automated Cadmium ReductionPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMetho5-Day Biochemical Oxygen DemandStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Strep - membrane filterTemperature, AirColor - Pt/Co unitsSpecific ConductanceDepth by chain or ropeWater Depth by Pressure TransducerDO, field

Procedure Name

ActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLHILL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 157 of 515

Hillsborough County Environmental (Florida)

EPA 1600 NTOT PH PLANKTON SALINITY SECCHI SILICA TOC

Procedure Id

21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL 21FLHILL

Procedure Source

Enterococcus bacteriaTotal NitrogenpH fieldPlankton CountSalinityLight PenetrationsilicaTOTAL ORGANIC CARBON

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

Status21FLHILL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 158 of 515

IMC Agrico (Florida)

10200-H 110.2 120.1 150.1 160.1 160.2 170.1 180.1 200.7(W) 300(A) 310.1 350.1 351.2 353.2 360.1 365.1 365.4 405.1 900 903

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandGross Alpha and Beta Activity in WaterRadium in Drinking Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLIMCA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 159 of 515

City of Jacksonville

10200-H 110.2 130.1 150.1 160.2 180.1 245.2 325.2 350.1 351.2 353.1 365.1 5210-B 6010B 7061A 7741A 9221-E

9222-D NTOT

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA APHA

APHA 21FLJXWQ

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltTotal HardnesspHNon-Filterable Residue - TSSTurbidity by NephelometryMercury by CVAAChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry5-Day Biochemical Oxygen DemandInductively Coupled Plasma AESArsenic by Gaseous Hydride AASelenium in Water by Gaseous HydrideEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFecal Coliform Membrane Filter ProcedureTotal Nitrogen - Calculated

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

Status21FLJXWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 160 of 515

City of Key West (Florida)

1600 2540-D 4500-NH3(F) 4500-NO3(B) 4500-P-E 9222-D

Procedure Id

NIOSH APHA APHA APHA APHA APHA

Procedure Source

Carbon Disulfide by GC/FPDTotal Suspended Solids in WaterAmmonia in Water Using Phenate MethodNitrate in Water by Ultraviolet SpectrophotometryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActive

Status21FLKEYW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 161 of 515

The Nature Conservancy of the Florida Keys

170.1 2520-B 360.1 D6503-99

Procedure Id

USEPA APHA USEPA 21FLKTNC

Procedure Source

TemperatureSalinity in Water- Electrical Conductivity MethodDissolved Oxygen Using an ISED6503-99 Standard Test Method for Enterococci in Water UsingEnterolertTM

Procedure Name

ActiveActiveActiveActive

Status21FLKTNC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 162 of 515

Florida LAKEWATCH

LAKEWATCH_V

Procedure Id

21FLKWAT

Procedure Source

LAKEWATCH Volunteer Water Quality Monitoring ProgramField/Lab Procedures

Procedure Name

Active

Status21FLKWAT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 163 of 515

Lee County Hyacinth Control District (Florida)

10200-H 120.1 130.2 150.1 180.1 350.1 351.2 353.3 354.1 365.1 ALKALINITY

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLLCHD

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnesspHTurbidity by NephelometryAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryAlkalinity- Lee Co. Hyacinth Control District

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLLCHD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 164 of 515

Lake County Water Resource Management (Florida)

DEP-SOP-001/01

EPA350.1 EPA351.2 EPA353.2 EPA365.1 EPA365.4 EPA375.4 EPA415.1 LCQSM SJRWMDWQM

SM10200 SM2120B SM2130B SM2320B SM2340B SM2340C SM2540C SM2540D SM3111B-CU SM3111BFE SM3111BMG SM3111BNA SM3111BNI SM3111BZN SM35111BMN SM3511BCA SM3511BK SM45002510B SM4500CLB SM4500CLG SM4500H+B SM4500OG SM5210B SM5220D SM9222B SM9222D SM9223B

Procedure Id

21FLLCPC

21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC

21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC 21FLLCPC

Procedure Source

DEP STANDARD OPERATING PROCEDURES FOR FIELDACTIVITIESNH3 + NH4 NITROGENTOTAL KJELDAHL NITROGENNITRATE + NITRITE NITROGENORTHO PHOSPHATE AS PTOTAL PHOSPHORUSSULFATETOTAL ORGANIC CARBONLAKE COUNTY QUALITY SYSTEMS MANUALWATER QUALITY MANUAL FOR VOLUNTEERS IN THE ST.JOHNS RIVER WATER MANAGEMENT DISTRICTCHLOROPHYLL ACOLORTURBIDITYTOTAL ALKALINITY AS CaCO3HARDNESS, CA + MGTOTAL HARDNESS AS CaCO3TOTAL DISSOLVED SOLIDSTOTAL SUSPENDED SOLIDSCOPPER BY FLAME AAIRON BY FLAME AAMAGNESIUM BY FLAME AASODIUM BY FLAME AANICKEL BY FLAME AAZINC BY FLAME AAMANGANESE BY FLAME AACALCIUM BY FLAME AAPOTASSIUM BY FLAME AASPECIFIC CONDUCTANCECHLORIDETOTAL RESIDUAL CHLORINEpHDISSOLVED OXYGENBOD 5DAYCHEMICAL OXYGEN DEMANDTOTAL COLIFORM BY MEMBRANE FILTRATIONFECAL COLIFORM BY MEMBRANE FILTRATIONTOTAL COLIFORM BY CHROMOGENIC SUBSTRATE

Procedure Name

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLLCPC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 165 of 515

Leon County Public Works (Florida)

10200-H 10200-H 10200-H (MOD) 110.2 120.1 130.2 150.1 160.1 160.2 160.2_M 170.1 180.1 200.7(W) 200.8(W) 2120-B 283.2 300(A) 310.1 310.1_M 325.2 340.2 350.1 350.2 351.2 351.3(C) 353.2 353.3 354.1 360.1 365.1 365.2 365.2 365.3 365.4 405.1 415.1 425.1 445 4500-F-C 4500-NO2(B) 4500-NO3(E) 5210-B 5540-C 600/8-78-017

Procedure Id

21FLLEON APHA 21FLLEON USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLLEON USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLLEON USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA 21FLLEON

Procedure Source

Chlorophyll a, corrected for pheophytinChlorophyll a-b-c DeterminationChlorophyll a, corrected for pheophytinColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSColor in Water by Visual ComparisonTitanium by GFAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinity in Water by TitrationChloride by Colorimetric Analysis IIFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryNitrogen, ammonia as NTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen - PotentiometricNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus, orthophosphate as PPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionMethylene Blue Active SubstancesIn-Vitro Determination of ChlorophyllFluoride in Water Using an ISENitrite in Water by ColorimetryNitrate in Water- Cadmium Reduction5-Day Biochemical Oxygen DemandAnionic Surfactants in Water as MBASFecal Coliform

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLLEON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 166 of 515

Leon County Public Works (Florida)

6010A 8270C(W) 9221-B

9221-C

9221-E

9222-B 9222-D D3977 D422 D4779 FT_1700 GC-030-1

Procedure Id

USEPA USEPA APHA

APHA

APHA

APHA APHA ASTM ASTM ASTM 21FLLEON 21FLLEON

Procedure Source

ICP SpectroscopySemivolatile Organic Compounds by CGC/MSStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureSuspended-Sediment in WaterParticle-Size Analysis of SoilsTotal, Organic and Inorganic CarbonSechi Disk DepthCaffeine

Procedure Name

ActiveActiveActive

Active

Active

ActiveActiveActiveActiveActiveActiveActive

Status21FLLEON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 167 of 515

Loxahatchee River District (Florida)

10200-H 120.1 130.2 150.1 160.1 160.2 170.1 180.1 200.8(S) 200.8(W) 2120-B 2520-B 3.4 310.1 330.4 350.2(B) 351.2 353.2 360.1 365.2 365.4 375.2 405.1 415.1 4500-CL-(B) 9222-B 9222-D EPA 608 MOD.

N&P PEST. 614M

SECCHI

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA 21FLLOX

21FLLOX

21FLLOX

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Wastes by ICP/MSMetals in Waters by ICP/MSColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodColiforms- Membrane FilterAlkalinity by TitrationTotal Residual Chlorine by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by Colorimetry5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionChloride in Water by Titration- Argentometric MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureOrganochlorine pesticides in water by GC/ECD-Meth. organicanalysis of muni. and indu. wastewaterOrganonitrogen and phosphorus pesticides in water EPA Method614 mod.Secchi

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

Status21FLLOX

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 168 of 515

Loxahatchee River District (Florida)

10500-C

Procedure Id

APHA

Procedure Source

Benthic Macroinvertebrate Sample Processing and Analysis

Procedure Name

Active

Status21FLLOXB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 169 of 515

Manatee County Environmental Management Dept (Florida)

10200-H 120.1 2120-B 2130 2340 2520-B 2540-C 2540-D 2550 3111-B 350.1 352.1 354.1 365.4 375.4 405.1 445 4500-F-C 4500-H 4500-O-G 4500-P-E 9222-B 9222-D 9230-C BOD CHL A CHL B CHL C COLOR F COLI F STREP FLUORIDE GENERIC

NH3 N NO2+3 N NO3 N ORTHO P PHEOPHYTIN T COLI TDS TKN TP TSS

Procedure Id

APHA USEPA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA

21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA 21FLMANA

Procedure Source

Chlorophyll a-b-c DeterminationConductanceColor in Water by Visual ComparisonTurbidity in WaterHardness in Water by EDTA TitrationSalinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerMetals in Water by FLAA- Direct Air-Acetylene FlameAmmonia Nitrogen by ColorimetryNitrate Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryTotal Phosphorus After Block DigestionSulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandIn-Vitro Determination of ChlorophyllFluoride in Water Using an ISEpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueBiochemical Oxygen DemandChlorophyll A by trichromatic methodChlorophyll B by trichromatic methodChlorophyll C by trichromatic methodColorFecal ColiformFecal StreptococcusFluorideGeneral Listing of Field and Lab Analytical Procedures for ManateeCountyAmmonia NitrogenNitrite+Nitrate NitrogenNitrate NitrogenOrtho-PhosphorusPheophytin by trichromatic methodTotal ColiformTotal Dissolved SolidsTotal Kjeldal NitrogenTotal PhosphorusTotal Suspended Solids

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLMANA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 170 of 515

Manatee County Environmental Management Dept (Florida)

TURBIDITY

Procedure Id

21FLMANA

Procedure Source

Turbidity

Procedure Name

Active

Status21FLMANA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 171 of 515

McGlynn Laboratories, Inc

10200-H 110.2 120.1 150.1 160.1 160.2 1604

170.1 180.1 310.1 325.3 350.3 351.4 353.3 354.1 360.1 365.2 405.1 9222-D 9230-C SOP-1

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLMCGL

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Coliforms and E. coli in Water by Membrane Filtration Using aSimultaneous Detection Technique (MI Medium)TemperatureTurbidity by NephelometryAlkalinity by TitrationChloride by Mercuric Nitrate TitrationAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen Using an ISENitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent Colorimetry5 Day Biochemical Oxygen DemandFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueAnalytical Procedure SOP

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLMCGL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 172 of 515

Marine Resources Council of East Florida

FT_1100 FT_1200 FT_1300 FT_1400 FT_1500 FT_1600 FT_1700

PH

Procedure Id

21FLMRC 21FLMRC 21FLMRC 21FLMRC 21FLMRC 21FLMRC 21FLMRC

21FLMRC

Procedure Source

Field Measurement Of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement Of SalinityField Measurement Of TemperatureField Measurement Of Dissolved OxygenField Measurement Of TurbidityField Measurement Of Light Penetratino (Secchi Depth andTransparency)pH Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Active

Status21FLMRC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 173 of 515

City of Naples (Florida)

10200-H 110.2 1106_1 200.7(W) 200.8(W) 2120-B 2120-B 2130 2320 2340 2540-D 3111-B 350.1 351.2 353.2 365.3 365.4 375.4 405.1 415.1 4500-CL(E) 4500-CL-(B) 4500-NO2(B) 4500-NORG D 4500-P-E 5210-B 6010B 6010B 9222-B 9222-D FT_1100 FT_1200 FT_1300 FT_1400 FT_1500 FT_1700

HARDNESS, CA+MGPMD-BEO PMD-BIL TOTAL_N

Procedure Id

APHA USEPA USEPA USEPA USEPA APHA 21FLNAPL APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA 21FLNAPL APHA APHA 21FLNAPL USEPA APHA APHA 21FLNAPL 21FLNAPL 21FLNAPL 21FLNAPL 21FLNAPL 21FLNAPL

21FLNAPL USEPA USEPA 21FLNAPL

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltEnterococci in Water by Membrane FilterMetals in Water by ICP-AESMetals in Waters by ICP/MSColor in Water by Visual ComparisonColor in water by visual comparisonTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationTotal Suspended Solids in WaterMetals in Water by FLAA- Direct Air-Acetylene FlameAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionResidual Chlorine in Water by Titration- Low-Level Amperometric MChloride in Water by Titration- Argentometric MethodNitrite in Water by ColorimetryTotal Kjeldahl NitrogenPhosphorus in Water by Colorimetry- Ascorbic Acid Method5-Day Biochemical Oxygen DemandMetals, USBiosystemsInductively Coupled Plasma AESStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of Light Penetration (Secchi Depth andTransparency)calculation of hardnessThiobencarb by GC/FIDBitertanol by GCCalculation of Total Nitrogen

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

Status21FLNAPL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 174 of 515

Northwest Florida Water District

110.1 110.2 110.3 1103_1 1106_1 120.1 130.1 130.2 140.1 150.1 150.2 160.1 160.2 160.3 160.4 160.5 170.1 180.1 200 200.1 200.1(FLAA) 200.1(GFAA) 200.1(ICP) 200.11 200.12 200.13 200.15 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 202.1 202.2 204.1 204.2 206.2 206.3 206.4 206.5 208.1 208.2 210.1 210.2

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Color by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltColor by Spectrophotometric AnalysisE. coli in Water by Membrane FiltrationEnterococci in Water by Membrane FilterConductanceTotal HardnessTotal HardnessOdor in Water Using a Consistent SeriespHpH by Continuous MonitoringFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueSettleable MatterTemperatureTurbidity by NephelometryMetals by Atomic AbsorptionMetals in Marine Waters by ICP/MSAcid Soluble Metals in Water by FLAAAcid Soluble Metals in Water by GFAAAcid Soluble Metals - ICPMetals in Fish Tissue by ICP-AESElements in Water by Temperature GFAAElements in Water by Chelation with GFAAMetals in Water by Nebulization and ICP-AESMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAAluminum by GFAAAntimony by FLAAAntimony by GFAAArsenic by GFAAArsenic by HYDAAArsenic by Spectrophotometric AnalysisArsenic Digestion for HYDAABarium by FLAABarium by GFAABeryllium by FLAABeryllium by GFAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLNWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 175 of 515

Northwest Florida Water District

212.3 213.1 213.2 215.1 215.2 218.1 218.2 218.3 218.4 218.5 218.6 219.1 219.2 220.1 220.2 236.1 236.2 239.1 239.2 242.1 243.1 243.2 245.1 245.2 245.3 245.5 245.6 249.1 249.2 253.1 253.2 255.1 255.2 258.1 265.1 265.2 267.1 272.1 272.2 273.1 273.2 282.1 282.2 283.1

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Boron by Colorimetric AnalysisCadmium by FLAACadmium by GFAACalcium by FLAACalcium by EDTA Titrimetric AnalysisChromium by FLAAChromium by GFAAChromium by Chelation Extraction FLAAHexavalent Chromium by FLAAHexavalent Chromium by GFAAHexavalent Chromium by Ion ChromatographCobalt by FLAACobalt by GFAACopper by FLAACopper by GFAAIron by FLAAIron by GFAALead by FLAALead by GFAAMagnesium by FLAAManganese by FLAAManganese by GFAAMercury in Water by CVAAMercury by CVAAMercury in Water by HPLCMercury in Sediment by CVAAMercury in Tissue by CVAANickel by FLAANickel by GFAAPalladium by FLAAPalladium by GFAAPlatinum by FLAAPlatinum by GFAAPotassium by FLAARhodium by FLAARhodium by GFAARuthenium by FLAASilver by FLAASilver by GFAASodium by FLAASodium by GFAATin by FLAATin by GFAATitanium by FLAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLNWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 176 of 515

Northwest Florida Water District

283.2 286.1 286.2 289.1 289.2 300(A) 300(B) 305.1 305.2 310.1 310.2 320.1 325.1 325.2 325.3 330.1 330.2 330.3 330.4 330.5 335.1 335.2 335.3 335.4 340.1 340.2 340.3 345.1 350.1 350.1 (MARCH83)350.2(A) 350.2(B) 350.2(C) 350.3 351.1 351.2 351.2 (MARCH83)351.3(A) 351.3(B) 351.3(C) 351.4 352.1 353.1 353.2

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLNWFD USEPA USEPA USEPA USEPA USEPA USEPA 21FLNWFD USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Titanium by GFAAVanadium by FLAAVanadium by GFAAZinc by FLAAZinc by GFAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAcidity by Titration Using a pH MeterAlkalinity by TitrationAlkalinity by Colorimetric AnalysisBromide by Titration with IodineChloride by Colorimetric Analysis IChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationTotal Residual Chlorine by TitrationChlorine by Spectrophotometry with DPDCyanides Amenable to ChlorinationTotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryTotal Fluoride by Colorimetric AnalysisFluoride in Water Using an ISEFluoride in Water by ColorimetryIodide in Water by TitrationAmmonia Nitrogen by ColorimetryNitrogen, ammonia as NAmmonia Nitrogen Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl NitrogenTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricTotal Kjeldahl Nitrogen Using an ISENitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLNWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 177 of 515

Northwest Florida Water District

353.2 (MARCH83)353.3 353.4 354.1 360.1 360.2 365.1 365.1 (MARCH83)365.2 365.3 365.4 365.5 370.1 375.1 375.2 375.3 375.4 376.1 376.2 377.1 405.1 410.1 410.2 410.3 410.4 413.1 413.2 415.1 420.1 420.2 420.3 420.4 D1125(A) D1889 DEP-AGP DEP-BENTHIC MACDEP-COLIFORM-F1DEP-COLIFORM-T1DEP-PERIPHYTON EPA 2510 WELCH (1948)

Procedure Id

21FLNWFD USEPA USEPA USEPA USEPA USEPA USEPA 21FLNWFD USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA ASTM ASTM 21FLNWFD 21FLNWFD 21FLNWFD 21FLNWFD 21FLNWFD 21FLNWFD 21FLNWFD

Procedure Source

Nitrite/NitrateNitrate-Nitrite Nitrogen by Cd ReductionDetermination of Nitrite and NitrateNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryOrtho-Phosphate-PPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionOrthophosphate in Water by ColorimetryDissolved Silica by ColorimetrySulfate by Colorimetry With ChloranilateSulfate in Water by ColorimetrySulfate by Gravimetric DeterminationSulfate by Turbidimetric DeterminationSulfide by Titration with IodineSulfide by Colorimetric DeterminationSulfite in Water by Titration5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandLow Level Chemical Oxygen DemandChemical Oxygen Demand in Saline WatersChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Recoverable Oil and Grease by IRTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterConductivity and Resistivity in WaterTurbidity of WaterALGAL GROWTH POTENTIALBENTHIC MACROINVERTEBRATESCOLIFORM, FECAL-MFCOLIFORM,TOTAL-MFPERIPHYTON-DEP SOP #BA-30ConductivitySecchi Depth

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLNWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 178 of 515

Orange County Environmental Protection (Florida)

10200-H 10200H 110.2 120.1 130.1 150.1 160.1 160.2 160.3 160.4 1664 170.1 180.1 200.7(W) 200.8(W) 200.9 204.2 206.2 210.2 2120-B 213.2 2310B 2320 2340 2340C 239.2 245.1 270.2 272.2 279.2 3020A 310.1 3113-B 3113B 325.2 325.3 350.1 350.2 350.3 351.2 353.2 354.1 360.1 360.2

Procedure Id

APHA 21FLORAN USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA 21FLORAN APHA APHA 21FLORAN USEPA USEPA USEPA USEPA USEPA 21FLORAN USEPA APHA 21FLORAN USEPA USEPA USEPA 21FLORAN USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationChlorophyll a, b, c series and phaeophytinColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAntimony by GFAAArsenic by GFAABeryllium by GFAAColor in Water by Visual ComparisonCadmium by GFAAAcidityAlkalinity in Water by TitrationHardness in Water by EDTA TitrationHardness Calculation, Ca & MgLead by GFAAMercury in Water by CVAASelenium by GFAASilver by GFAAThallium by GFAAMetals PrepAlkalinity by TitrationMetals in Water by GFAAMetals AnalysisChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetryDissolved OxygenAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler Technique

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLORAN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 179 of 515

Orange County Environmental Protection (Florida)

365.1 365.4 375.4 405.1 410.4 425.1 500.1 600.1 6010B 7060A 7131A 7421 9222-B 9222-D 9222B 9222D 9222H 9230-C EPA100.1 EPA120.1 EPA130.1 EPA150.1 EPA160.2 EPA160.3 EPA160.4 EPA170.1 EPA200.7 EPA200.8 EPA210.2 EPA213.2 EPA239.2 EPA245.1 EPA270.2 EPA272.2 EPA279.2 EPA350.1 EPA351.2 EPA353.2 EPA365.1 EPA410.4 EPD100.1 SM10200H SM2120B SM2310B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA 21FLORAN 21FLORAN USEPA USEPA USEPA USEPA APHA APHA 21FLORAN 21FLORAN 21FLORAN APHA 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN

Procedure Source

Phosphorus by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryMethylene Blue Active SubstancesOrganic NitrogenTotal NitrogenInductively Coupled Plasma AESArsenic by GFAACadmium by GFAALead by GFAAStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureTotal ColiformFecal Coliform MFTotal Fecal ColiformFecal Streptococcus and Enterococcus, Membrane Filter TechniqueSample DepthSecific ConductanceHardness, carbonateSecchiTSSTSFixed SolidsDissolved OxygenMetals AnalysisMetals in Water by ICP/MSBerylliumCadmiumLeadMercurySeleniumSilverThalliumAmmoniaTKNNOxPhosphorusCODDepth, Secchi disk depthChlorphyll a, b, c series and phaeophytinColorAcidity

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLORAN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 180 of 515

Orange County Environmental Protection (Florida)

SM2320B SM2340B SM3113B SM9222B SM9222D SM9230C 9132

Procedure Id

21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN 21FLORAN USEPA

Procedure Source

Alkalinity, TotalHardness, Ca, MgMetals AnalysisTotal ColiformTotal Fecal ColiformStreptococcus, FecalTotal Coliform by Membrane Filter

Procedure Name

ActiveActiveActiveActiveActiveActiveSusp

Status21FLORAN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 181 of 515

Orlando Streets Drainage Stormwater Utility Bureau(Florida)

10200-H 120.1 130.2 160.1 160.2 160.4 200.7(W) 210.2 2120-B 213.2 215.1 218.2 220.2 2340 236.1 239.2 242.1 245.1 270.2 272.2 289.1 300(A) 310.1 310.1_M 350.1 351.2 353.2 354.1 365.1 365.2 365.4 405.1 5210-B 9222-D 973.48 FT_1100 FT_1200 FT_1400 FT_1500 FT_1700

SOP-4 SOP-5 SOP-6

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA AOAC 21FLORL 21FLORL 21FLORL 21FLORL 21FLORL

21FLORL 21FLORL 21FLORL

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnessFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueMetals in Water by ICP-AESBeryllium by GFAAColor in Water by Visual ComparisonCadmium by GFAACalcium by FLAAChromium by GFAACopper by GFAAHardness in Water by EDTA TitrationIron by FLAALead by GFAAMagnesium by FLAAMercury in Water by CVAASelenium by GFAASilver by GFAAZinc by FLAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinity in Water by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen Demand5-Day Biochemical Oxygen DemandFecal Coliform Membrane Filter ProcedureTotal Nitrogen in WaterField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of Light Penetration (Secchi Depth andTransparency)Percent Cloud CoverWind Direction and VelocityWave Height

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

Status21FLORL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 182 of 515

Palm Beach County Environmental Resources Managemnt(Florida)

10200-H 130.2 160.2 180.1 200.7(S) 200.8(W) 200.9 213.2 2130 2320 2340 239.2 2510 2520-B 2540-D 2550 289.1 3.4 300(A) 300(B) 310.1 3111-C 350.1 351.2 353.2 365.1 365.4 405.1 410.4 445 4500-H 4500-O-G 6010 6010B 9222-D FT_1100 FT_1200 FT_1300 FT_1400 FT_1500 FT_1600 FT_1700

FT_1800

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA APHA APHA APHA APHA USEPA APHA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA NIOSH USEPA APHA 21FLPBCH 21FLPBCH 21FLPBCH 21FLPBCH 21FLPBCH 21FLPBCH 21FLPBCH

21FLPBCH

Procedure Source

Chlorophyll a-b-c DeterminationTotal HardnessNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAACadmium by GFAATurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationLead by GFAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Suspended Solids in WaterTemperature of Water by ThermometerZinc by FLAAColiforms- Membrane FilterInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Extraction/Air-Acetylene FlameAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryIn-Vitro Determination of ChlorophyllpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodHydrogen Cyanide by Visible AbsorptionInductively Coupled Plasma AESFecal Coliform Membrane Filter ProcedureField Measurements of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of TurbidityField Measurement of Light Penetration (Secchi Depth andTransparency)Field Measurement of Water Flow and Velocity

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Status21FLPBCH

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and Equipment Summary

Page 183 of 515

Palm Beach County Environmental Resources Managemnt(Florida)

FT_1900 YSI

Procedure Id

21FLPBCH 21FLPBCH

Procedure Source

Continuous Monitoring with Installed MetersYSI 600 XL Probe

Procedure Name

ActiveActive

Status21FLPBCH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 184 of 515

PROJECT COAST - Southwest Florida Water Management District

10200-H_M

150.1 170.1 2120-C 360.1 4500-NO3(F)_M

4500-P-E_M

PROJECT COAST

Procedure Id

21FLPCSW

USEPA USEPA APHA USEPA 21FLPCSW

21FLPCSW

21FLPCSW

Procedure Source

Chlorophyll concentrations were determined spectrophotometricallyMethod 10200-H APHApHTemperatureColor in Water by SpectrophotometryDissolved Oxygen Using an ISETotal nitrogen concentrations (µg/L) determined by oxidizing watersamples with persulfateTotal phosphorus concentrations were determined using theprocedures of Murphy and Riley (1962)Project Coast Field and Lab Analytical Procedures

Procedure Name

Active

ActiveActiveActiveActiveActive

Active

Active

Status21FLPCSW

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and Equipment Summary

Page 185 of 515

Pinellas County Dept. of Environmental Management (Florida)

350.1 351.2 353.2 365.4 375.4 9223-B ENTEROLERT EPA 200.7 EPA 351.2 EPA 365.4 EPA 6010 EPA 6010 AL EPA 6010 AL TOTEPA 6010 CAD EPA 6010 IRON EPA 6010 LEAD EPA 6010 ZINC EPA6010 F COLIFORM F STREP FISH MEASURE FLOW 001 FT 1000 HABITAT FIELD HYDROLAB 001 HYDROLAB 002 HYDROLAB 003 HYDROLAB 004 HYDROLAB 005 HYDROLAB 006 HYDROLAB 007 HYDROLAB 009 HYDROLAB004 LIGHT ATTENUATISECCHI 001 SM 10200 H SM 2120 B SM 2320 B SM 2340 B SM 2540 B SM 5210 B SM 9222B SM 9222D SM 9223 B

Procedure Id

USEPA USEPA USEPA USEPA USEPA APHA 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM

Procedure Source

Ammonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationEnzyme Substrate Test, E. coli, Coliform GroupEnterococcus Group BacteriaAluminum, dissolvedNitrogen, TotalTotal Phosphorus after block digestionMagnesiumAluminum, DissolvedAluminum, TotalCadmiumIronLeadZincCalciumFecal Coliform BacteriaFecal Strep BacteriaField determination of whole fish physical charactoristicsFlowField Measurements and ObservationsField station visit habitat measurements and observationsDepth measurment in field with probeTemperature measurement in field with probepH measurement in field with probeDissolved oxygen (DO)Conductivity measurement in field with probeORP measurement in field with probeSalinity measurement in field with probetotal depth measurement with probeDissolved Oxygen measurement with probeLight attenuation coefficientSecchi depth measurement in fieldChlorophyll a, corrected for pheophytinColor, TrueAlkalinityHardness, Ca,MgTotal Suspended Solids (TSS)BOD, Biochemical oxygen demandTotal ColiformTotal Fecal ColiformTotal Coliforms

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLPDEM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 186 of 515

Pinellas County Dept. of Environmental Management (Florida)

SM10200 H 001 SM10200 H 002 SM10200 H 003 SM10200 H 004 SM2130 B SM2540 B SM2540 D SM4500 NH3H SM4500 NO3 F SM4500-CL B SM4500-P F SM5210 B STATION OBS TCOLI TEMP 001 TRANSMISSIVITY WEATHER 001

Procedure Id

21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM 21FLPDEM

Procedure Source

Chlorophyll AChlorophyll bChlorophyll cPheophytin ATurbidityResidue, Total (TSS)Total Suspended Solids (TSS)Ammonia NH3Nitrate + Nitrite NOXChlorideOrthophosphate as PBiochemical Oxygen Demand 5 dayField station visit physical direct measurements and observationsTotal Coliform BacteriaTemperature degrees C, Hydrolab probe method # 2550 BLight, transmissivityField station visits general weather observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLPDEM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 187 of 515

Florida Department of Environmental Protection

110.2 160.1 160.2 180.1 200.1(FLAA) 200.7 MOD

200.8 MOD 200.8(W) 245.2 2540G SM 300(A) 300.0 310.1 340.2 350.1 351.2 353.2 365.1 365.3 365.4 415.1 5210-B 6010 MOD

6020 ICP MS 625 625/8270 MOD 8081(S) 8141A(S) 8270 MOD

8290 9222-B 9222-D 9230-C HG-008-3 PART_1 SECCHI SM10200H MOD STANDMETH WIND

Procedure Id

USEPA USEPA USEPA USEPA USEPA 21FLPNS

21FLPNS USEPA USEPA 21FLPNS USEPA 21FLPNS USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA 21FLPNS

21FLPNS USEPA 21FLPNS USEPA USEPA 21FLPNS

USEPA APHA APHA APHA 21FLPNS USEPA 21FLPNS 21FLPNS 21FLPNS 21FLPNS

Procedure Source

Color Analysis Using Platinum/CobaltFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryAcid Soluble Metals in Water by FLAAMetals,tot.recoverable in aq. samples by trace-ICP emissionspectroscopyMetals, tot. recoverable in aq. samples by ICP mass spec.Metals in Waters by ICP/MSMercury by CVAAPercent Solids in Sediment - Dry WeightInorganic Anions by Ion ChromatographyInorganic ions - chloride, sulfate in aqueous samplesAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandMetals, tot. recoverable, in solid samples by trace-ICP emissionspectroscopyICP Mass Spectrophotometry for Metals in SedimentBase/Neutral and Acid Organics in WastewaterSemi-volatile, base neutral extractable organics in water by GC/MSOrganochlorine Pesticides and PCBsOrganophosphorus Compounds in Soil by GCSemi-volatile organic pollutants, excluding PCBs and Toxaphene, insoils/sediments by GC/MSPolychlorinated PCDDs and PCDFs by HRGC/HRMSStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueDEP SOP Method - Mercury in SedimentTrihalomethanes in Water by Purge and TrapSecchi Depth ProtocolChlorophyll A and Phaephytin Monochromatic, WaterStandard Methods for the Examination of Water and WastewaterWind Velocity

Procedure Name

ActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLPNS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 188 of 515

Polk County Water Resources (Florida)

00-01 10200 10200 H 10200-H 150.1 160.4 1600 2120-B 2130 2130 B 2320 2320 B 2340 2340 B 2340 C 2510 2510 B 2510-B 2520-B 2540-C 2540-D 2540-E 2550 3111-B 3111-D 3113-B 3500-AL(D) 351.2 351.2 TKN DISS 351.2-350.1 351.2-4500 NO3F365.4 375.4 415.1 4500 - NH3 H 4500 H+ B 4500 TP DISS 4500-CL(E) 4500-CL(G) 4500-CL-(E) 4500-F-C 4500-NH3(F) 4500-NH3(G) 4500-NO3(F)

Procedure Id

USEPA 21FLPOLK 21FLPOLK APHA USEPA USEPA 21FLPOLK APHA APHA 21FLPOLK APHA 21FLPOLK APHA 21FLPOLK 21FLPOLK APHA 21FLPOLK 21FLPOLK APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA 21FLPOLK 21FLPOLK 21FLPOLK USEPA USEPA USEPA 21FLPOLK 21FLPOLK 21FLPOLK APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Gross Alpha and Beta Activity in WaterChlorophyl aChlorophyl aChlorophyll a-b-c DeterminationpHVolatile ResidueEnterococci, MFColor in Water by Visual ComparisonTurbidity in WaterTurbidityAlkalinity in Water by TitrationAlkalinity totalHardness in Water by EDTA TitrationCalcium HardnessHardness TotalConductivity in WaterConductance, specific (lab)Conductance, specific (lab)Salinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterTemperature of Water by ThermometerMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAAluminum in Water by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrogen, TKN DissolvedOrganic NitrogenTotal NitrogenTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionNitrogen, ammoniapH (lab)Phosphorus Total DissolvedResidual Chlorine in Water by Titration- Low-Level Amperometric MResidual Chlorine by Colorimetry- DPD Colorimetric MethodChloride in Water by Colorimetry- Automated Ferricyanide MethodFluoride in Water Using an ISEAmmonia in Water Using Phenate MethodAmmonia in Water Using Automated Phenate MethodNitrate in Water- Automated Cadmium Reduction

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLPOLK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 189 of 515

Polk County Water Resources (Florida)

4500-O-G 4500-P-F

5210-B 5310-C 78 8000 9221-D 9222-B 9222-D 9230 C 9230-C 9230-C D516 DEP SOP 2/12/01DEP SOP FT 1100DEP SOP FT 1200DEP SOP FT 1400DEP SOP FT 1500DEP SOP FT 1720DEP SOP10/3/83 FS 2100 FT 1600 MERCK PCNRD HACH8326 SD YSI

Procedure Id

APHA APHA

APHA APHA 21FLPOLK HACH APHA APHA APHA 21FLPOLK 21FLPOLK APHA ASTM 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK 21FLPOLK

Procedure Source

Total Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMetho5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Ultraviolet Oxidation MethodSecchi DiskChemical Oxygen DemandEstimation of Bacterial Density- MPN DeterminationStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnterococciEnterococci, MFFecal Streptococcus and Enterococcus, Membrane Filter TechniqueSulfate in Water by TurbidimeterUninonized NH3pHConductance, specificTemperature, waterDissolved oxygenSecchi transparencyUnionized AmmoniaTotal ColiformTurbidity in FieldEnterococci, P/A - Merck ChromocultAluminumSecchi DiskYSI

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLPOLK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 190 of 515

Reedy Creek Improvement District - Env Services (FLORIDA)

10200-H 110.2 120.1 150.1 160.1 160.1_M 160.2 160.2_M 1664 170.1 180.1 200.7(W) 200.8(W) 2340 245.1 300(A) 310.1 325.2 350.1 351.2 353.1 354.1 360.1 365.1 415.1 515.1 5210-B 608 608.2 624 6640-B 8000 8141(W) 8270B(W) 9221-B

9221-C

9230-B

9230-C

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA APHA HACH USEPA USEPA APHA

APHA

APHA

APHA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Water by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides in WastewaterPurgeable Organics in WastewaterChlorinated Phenoxy Herbicides in WaterChemical Oxygen DemandOrganophosphorus Compounds in WaterSemivolatile Organics in Water by GC/MSStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Coliform Group Density, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter Technique

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

Active

Status21FLRCID

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 191 of 515

Sarasota County Environmental Services (Florida)

10200-F 10200-H 120.1 2120-B 2130 2520-B 2540-D 2540-E 350.1 351.2 353.2 365.1 365.4 405.1 445 FT-1100 FT-1200 FT-1300 FT-1400 FT-1500 FT-1700

SOP-10 SOP-11 SOP-12 SOP-13 SOP-2 SOP-4 SOP-5 SOP-6 SOP-7 SOP-8 SOP-9

Procedure Id

APHA APHA USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA

21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA 21FLSARA

Procedure Source

Phytoplankton Counting TechniquesChlorophyll a-b-c DeterminationConductanceColor in Water by Visual ComparisonTurbidity in WaterSalinity in Water- Electrical Conductivity MethodTotal Suspended Solids in WaterFixed and Volatile Solids in WaterAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandIn-Vitro Determination of ChlorophyllField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of Light Penetration (Secchi Depth andTransparency)Percent Saturation of Dissolved OxygenDissolved inorganic NitrogenTotal NitrogenTotal Organic NitrogenStandard MethodPercent Cloud CoverWind Direction and VelocityWave HeightDepth to bottomDepth of Observation/SampleAttenuation Coefficient

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSARA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 192 of 515

Sanibel Captiva Conservation Foundation (Florida)

CHLA COLOR NOX PHAE PTOT TKN TSS

Procedure Id

21FLSCCF 21FLSCCF 21FLSCCF 21FLSCCF 21FLSCCF 21FLSCCF 21FLSCCF

Procedure Source

Chlorophyll aColorNitrate-nitritePhaeophytinTotal phosphorusTotal Kjeldahl NitrogenTotal suspended solids

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status21FLSCCF

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 193 of 515

Florida Department of Environmental Protection

2130 2520-B 2550 973.41 973.45 978.23 FIELD_MSR

Procedure Id

APHA APHA APHA AOAC AOAC AOAC 21FLSEAS

Procedure Source

Turbidity in WaterSalinity in Water- Electrical Conductivity MethodTemperature of Water by ThermometerpH of WaterOxygen (Dissolved) in WaterFecal Coliforms in Shellfish WatersField Msr/Obs for Wind Velocity and Direction

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status21FLSEAS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 194 of 515

Seminole County (Florida)

10200-H 110.2 130.2 160.2 200.7(W) 2130 2320 2340 245.1 2510 279.2 300(A) 310.1 310.1_M 335.2 350.1 351.2 353.2 365.1 365.4 405.1 410.4 413.1 420.1 420.2 4500-H 4500-O-G 4500-P-F

6010A 9065 9222-D FT1100 FT1200 FT1400 FT1500 FT1600 FT1700 SECCHI YSI

Procedure Id

APHA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA NIOSH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA

USEPA USEPA APHA 21FLSEM 21FLSEM 21FLSEM 21FLSEM 21FLSEM 21FLSEM 21FLSEM 21FLSEM

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltTotal HardnessNon-Filterable Residue - TSSMetals in Water by ICP-AESTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAA1-Octanethiol by GC/FPDThallium by GFAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinity in Water by TitrationTotal Cyanide in WaterAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoICP SpectroscopyTotal Phenolics by SpectroscopyFecal Coliform Membrane Filter ProcedurepH by FDEP StandardsSpecific Conductivity by FDEP StandardsTemperature, Water by FDEP StandardsDissolved Oxygen (DO) by FDEP StandardsTurbidity by FDEP StandardsSecchi Disk Depth by FDEP StandardsSecchi DepthYSI Incorporated 6-series Environmental Monitoring

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSEM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 195 of 515

South Florida Water Management District

204.2 210.2 245.1 279.2 BULK DENSITY CACO3 CATION EXCHANGECORRECTED

FIELD ALKALINITFP-1 FREON-EXT HALOWAX 1000 HALOWAX 1099 IODIDE-ORGANIC TITRATION WQ-1

Procedure Id

USEPA USEPA USEPA USEPA 21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM

21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM 21FLSFWM

Procedure Source

Antimony by GFAABeryllium by GFAAMercury in Water by CVAAThallium by GFAABulk Density of SoilCalcium Carbonate (Original description)Original Description = Cation Exchange CapacityOriginal Information in STORET (corrected for phaeophytin). InDBHYDRO = A2Field AlkalinityProcedures for Field ParametersFreon Extraction MethodHalowax 1000Halowax 1099iodide in organic compounds, Water, WHOLEAlkalinity by TitrationLaboratory Procedures for Water Quality Chemical Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSFWM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 196 of 515

St. Johns Water Management District

10 10200-F 10200-G 10200-H 110.2 120.1 150.1 160.1 160.2 160.4 170.1 180.1 200.7 200.7(W) 200.8 200.8(W) 202.2 206.2 2120-B 213.2 215.1 218.2 220.2 236.1 239.2 242.1 243.2 245.1 249.2 2540-G 258.1 270.2 272.2 273.1 282.2 300(A) 300.0 310.1 3120 325.2 340.2 350.1 3500 351.2

Procedure Id

USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLSJWM USEPA 21FLSJWM USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA 21FLSJWM USEPA APHA USEPA USEPA USEPA NIOSH USEPA

Procedure Source

Carbon Monoxide Emissions in AirPhytoplankton Counting TechniquesZooplankton Counting TechniquesChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometrySJR-200.7Metals in Water by ICP-AESSJR-200.8Metals in Waters by ICP/MSAluminum by GFAAArsenic by GFAAColor in Water by Visual ComparisonCadmium by GFAACalcium by FLAAChromium by GFAACopper by GFAAIron by FLAALead by GFAAMagnesium by FLAAManganese by GFAAMercury in Water by CVAANickel by GFAATotal, Fixed and Volatile SolidsPotassium by FLAASelenium by GFAASilver by GFAASodium by FLAATin by GFAAInorganic Anions by Ion ChromatographySJR-300.0Alkalinity by TitrationMetals in Water by ICPChloride by Colorimetric Analysis IIFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryFormaldehyde by Visible Absorption Spec.Total Kjeldahl Nitrogen by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSJWM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 197 of 515

St. Johns Water Management District

353.2 360.1 365.1 365.2 365.3 365.4 370.1 375.4 4 405.1 415.1 5 909A.1 9221-B

9221-D 9221-E

9222-B 9222-D 9230-C B0051 B0065

I2700 MICROBIO OTHER/UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLSJWM APHA

APHA APHA

APHA APHA APHA USDOI/USGS USDOI/USGS

USDOI/USGS 21FLSJWM 21FLSJWM

Procedure Source

Nitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate by Turbidimetric DeterminationMoisture Content in Stack Gases5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionParticulate Emissions in AirSJR-909A.1Standard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueFecal Coliform Bacteria- Presumptive Test- MPN MethodFecal Streptococcal Bacteria- Presumptive/Confirmation- MPNMethoSilica in Water by ColorimetrySJR-MICROBIOOther or Unknown Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActive

ActiveActiveActive

Status21FLSJWM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 198 of 515

SMR Communities, Inc. (Florida)

10200-H 110.2 160.1 160.2 160.2_M 180.1 2120-B 300(A) 350.1 350.2(B) 351.2 353.2 365.1 415.1 445 5210-B 5310-C 6010B 9060 9222-B 9222-D FT_1100 FT_1200 FT_1400 FT_1500 FT_1600 FT_1800 NO2+NO3 TN TP

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA APHA APHA 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC 21FLSMRC

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsTurbidity by NephelometryColor in Water by Visual ComparisonInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Organic Carbon by CombustionIn-Vitro Determination of Chlorophyll5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Ultraviolet Oxidation MethodInductively Coupled Plasma AESTotal Organic Carbon in Water and WasteStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of TurbidityField Measurement of Water Flow and VelocityNitrogen, Nitrite (NO2) + Nitrate (NO3) as NTotal NitrogenTotal Phosphate

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSMRC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 199 of 515

Suwannee River Water Management District (Florida)

10200 SM 10200-H 110.2 120.1 150.1 160.1 160.2 160.4 170.1 180.1 200.7(W) 300(A) 310.1 350.1 351.2 353.2 360.1 415.1 5310-B 6010A 6010B 9222-B 9222-D 9230-C NOT REPORTED

Procedure Id

21FLSUW APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA APHA 21FLSUW

Procedure Source

CHLOROPHYLL A-B-CChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryMetals in Water by ICP-AESInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISETotal Organic Carbon by CombustionTotal Organic Carbon by Combustion-Infrared MethodICP SpectroscopyInductively Coupled Plasma AESStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueMethod not reported

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSUW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 200 of 515

Southwest Florida Water Management District

10200-G 10200-H 120.1 150.1 170.1 200 200.7(W) 2120-B 2130 2320 2340 2520-B 2540-C 2540-D 2540-E 300(A) 310.1 3111-B 3111-D 3113-B 340.2 351.2 353.2 354.1 360.1 365.1 415.1 4500-F-C 4500-NH3(G) 4500-P-F

4500-SI(F) 5310-B 9222-B 9222-D D5176 FT-1100 FT-1200 FT-1300 FT-1400 FT-1500 FT-1600 FT-1700

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA

APHA APHA APHA APHA ASTM 21FLSWFD 21FLSWFD 21FLSWFD 21FLSWFD 21FLSWFD 21FLSWFD 21FLSWFD

Procedure Source

Zooplankton Counting TechniquesChlorophyll a-b-c DeterminationConductancepHTemperatureMetals by Atomic AbsorptionMetals in Water by ICP-AESColor in Water by Visual ComparisonTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationSalinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAFluoride in Water Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionFluoride in Water Using an ISEAmmonia in Water Using Automated Phenate MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSilica in Water by Automated ColorimetryTotal Organic Carbon by Combustion-Infrared MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureNitrogen in Water by Pyrolysis DetectionField Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of SalinityField Measurement of TemperatureField Measurement of Dissolved OxygenField Measurement of TurbidityField Measurement of Light Penetration (Secchi Depth andTransparency)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLSWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 201 of 515

Southwest Florida Water Management District

FT-1800 FT-1900

Procedure Id

21FLSWFD 21FLSWFD

Procedure Source

Field Measurement of Water Flow and VelocityContinuous Monitoring With Installed Meters

Procedure Name

ActiveActive

Status21FLSWFD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 202 of 515

Tampa Bay Water

10200-H 160.2 2120-B 300(A) 325.2 350.1 351.2 353.2 365.2 FIELD

Procedure Id

APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA 21FLTBW

Procedure Source

Chlorophyll a-b-c DeterminationNon-Filterable Residue - TSSColor in Water by Visual ComparisonInorganic Anions by Ion ChromatographyChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryIn Situ Profile

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLTBW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 203 of 515

Florida Department of Environmental Protection

10200-H 110.2 160.1 160.2 180.1 200.7(W) 200.8(S) 200.8(W) 300(A) 310.1 340.2 350.1 351.2 353.2 365.1 365.4 405.1 410.3 415.1 5210-B 5220-C 600/9-78-018 9222-B 9222-D FT1100 FT1200 FT1300 FT1400 FT1500 FT1700 SOP-2

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21FLTPA APHA APHA 21FLTPA 21FLTPA 21FLTPA 21FLTPA 21FLTPA 21FLTPA 21FLTPA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSInorganic Anions by Ion ChromatographyAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandChemical Oxygen Demand in Saline WatersTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Closed Reflux MethodAlgal Growth Potential in waterStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedurepHSpecific conductivitySalinityTemperatureDissolved oxygenDepth, Secchi disk depthTo be updated

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLTPA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 204 of 515

Volusa County Environmental Health Lab (Florida)

10200-H 110.2 1106_1 120.1 150.1 160.1 160.2 1600

170.1 180.1 2120-B 2120B 350.1 3500-CD(D) 351.2 353.2 360.1 365.1 365.4 8008 8317 8506 9222-B 9222-D 9222D 9230-C 9230C EPA FECAL COL EPA TOTAL COL HCT154 SOP-2 VCEHLP-002 VCEHLP-003 VCEHLP-004 WEATHER-001

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA APHA 21FLVEMD USEPA APHA USEPA USEPA USEPA USEPA USEPA HACH 21FLVEMD HACH APHA APHA 21FLVEMD APHA 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD 21FLVEMD

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltEnterococci in Water by Membrane FilterConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)TemperatureTurbidity by NephelometryColor in Water by Visual ComparisonTrue ColorAmmonia Nitrogen by ColorimetryCadmium in Water by SpectrophotometryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionTotal Iron in WaterLeadCopper in WaterStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal ColiformFecal Streptococcus and Enterococcus, Membrane Filter TechniqueEnteroccocus BacteriaDirect Membrane Filter Method for Fecal ColiformSingle-Step Membrane Filter Method for Total ColiformCadmium VolusiaField/Lab Analytical Standard Operation ProcedureField Station Visit Salinity MeasurementField Station Visit Secchi MeasurementChlorophyllField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLVEMD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 205 of 515

Florida Department of Environmental Protection

10200-H 10200H(2)(B)

10200H(2)(C)

110.2 150.1 160.1 160.2 160.4 170.1 180.1 200.10_M 200.7(S) 200.7(W) 200.7_M 200.8(S) 200.8(W) 2120B 2130B 2320B 2340C 245.1 245.6 2510B 2520B 2540B 2540B1 2540C 2540D 2540E 2580B 300(A) 300(B) 300.0 300_M 310.1 320.1 335.3 340.2 350.1 3500-CR-C 3500-PB-C 351.2

Procedure Id

APHA 21FLWPB

21FLWPB

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLWPB 21FLWPB 21FLWPB 21FLWPB USEPA USEPA 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB USEPA USEPA 21FLWPB USEPA USEPA USEPA USEPA USEPA USEPA 21FLWPB 21FLWPB USEPA

Procedure Source

Chlorophyll a-b-c DeterminationSTANDARD METHODS 10200(2)(B) - CHLOROPHYLL A,PHAEOPHYTIN CORRECTION METHODCHLOROPHYLL BY TRICHROAMTIC METHOD - STANDARDMETHODS 10200H(2)(C)Color Analysis Using Platinum/CobaltpHFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryInductively Coupled PlasmaMetals in Soil by ICP-AESMetals in Water by ICP-AESICP-AES For Trace Element AnalysisMetals in Wastes by ICP/MSMetals in Waters by ICP/MSSTANDARD METHODS 2120B COLOR BY VISUALSTANDARD METHODS 2130B TURBIDITY NTUSTANDARD METHODS 2320B - ALKALINITYSTANDARD METHODS 2340C - HARDNESSMercury in Water by CVAAMercury in Tissue by CVAASTANDARD METHODS 2510B CONDUCTIVITYSTANDARD METHODS 2520B - SALINITYSTANDARD METHODS 2540B - TOTAL SOLIDSSTANDARD METHODS - 2540B1 - FIXED SOLIDS % RESIDUESTANDARD METHODS 2540C - TOTAL DISSOLVED SOLIDSSTANDARD METHODS 2540D - TSSSTANDARD METHODS - 2540E - % VOLATILE SOLIDSSTANDARD METHODS 2580B - ORP - STORET 00090Inorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographySulfateDetermination of Anions by ICAlkalinity by TitrationBromide by Titration with IodineTotal Cyanide by Colorimetric AnalysisFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryStandard Methods-Total ChromiumTotal leadTotal Kjeldahl Nitrogen by Colorimetry

Procedure Name

ActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLWPB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 206 of 515

Florida Department of Environmental Protection

351.2 W/O DIG 353.2 354.1 365.1 365.4 375.4 376.1 415.1 4500 4500-CLC 4500-PF 4500CL 4500F 4500H 4500N 4500SI 5210B 5220-B 5220B 5540C 600/9222-D 6010B 7471A 7471_M 8010F 8081(S) 8081/8082_M

8082(S) 8141A(S) 8141A(S)_M 8270B(S) 8270C(S) 9222-D 9222B 9222D 9230C

D3857 DEP-SED-SOP-003DEP-SED-SOP-007DEP-SED-SOP-011DEP-SED-SOP-012DEP-SED-SOP-015

Procedure Id

21FLWPB USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB APHA 21FLWPB 21FLWPB 21FLWPB USEPA USEPA 21FLWPB 21FLWPB USEPA 21FLWPB

USEPA USEPA 21FLWPB USEPA USEPA APHA 21FLWPB 21FLWPB 21FLWPB

ASTM 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB

Procedure Source

USEPA/ORD METHOD 351.2 AMMONIA WITHOUT DIGESTIONNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationSulfide by Titration with IodineTotal Organic Carbon by CombustionSTANDARD METHODS 4500 - DISSOLVED OXYGEN BY PROBESTANDARD METHODS - 4500-CLC - CHLORIDESTANDARD METHODS - 4500-PF- ORTHO PHOSPHORUSSTANDARD METHODS 4500CL - CHLORINESTANDARD METHODS 4500F - FLUORIDESTANDARD METHODS 4500H - pH BY PROBESTANDARD METHODS 4500N - NITROGEN - STORET 00600 -STANDARD METHODS 4500SI - SILICASTANDARD METHODS 5210B - Biological Oxygen Demand - 5 DayChemical Oxygen Demand by Titration- Open Reflux MethodSTANDARD METHODS 5220 B - CODSTANDARD METHODS 5540C - MBAS - STORET 38260EPA 600/8-78-017; SM 9222 D for FCOLIInductively Coupled Plasma AESMercury in Solid or Semisolid WasteMercury in Solid or Semi-solid WasteSTANDARD METHODS - UNIONIZED AMMONIAOrganochlorine Pesticides and PCBsOrganochlorine Pesticides and PCB's as Arochlors by CapillaryCloumn GCPCBs as Aroclors by Capillary Column GCOrganophosphorus Compounds in Soil by GCOrganophosphorus Compounds in Soil by GCSemivolatile Organics in Soil by GC/MSSemivolatile Organic Compounds by CGC/MSFecal Coliform Membrane Filter ProcedureSTANDARD METHODS 9222B - TOTAL COLIFORMS MEMBRANESTANDARD METHODS 9222D - FECAL COLIFORM MEMBRANESTANDARD METHODS 9230C - FECAL STREPTOCOCCUS -MEMBRANEWater Velocity in Open ChannelsAmmonia-NH3 Automated Phenate MethodChloride-Titrimetric MethodHardness, Total (mg/l as CaCO3)Nitrate-Nitrite (NO2+3)Reactive Orthophosphate

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

Status21FLWPB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 207 of 515

Florida Department of Environmental Protection

DEP-SED-SOP-019DEP-SED-SOP-021DEP-SED-SOP-023DEPSOP-GC-011-5DEPSOP-GC-012-3

DEPSOP:HG-008-3FT_1100 FT_1200 FT_1300 FT_1400 FT_1500 FT_1600 FT_1700

SM3500-AS.C SM3500-CU.C SM3500-MN.C SM3500-NI.C SM3500-PB.C

Procedure Id

21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB

21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB

21FLWPB 21FLWPB 21FLWPB 21FLWPB 21FLWPB

Procedure Source

Total Kjeldahl Nitrogen (TKN) Salicylate MethodTotal Phosphorus (TP) Colorimetric Automated Block Digester AAIITurbidityOrganochlorine pesticides and PCB's in water matrices by GC/ECDOrganonitrogen and phosporus pesticides in water matrices byGC/NPDMercury in Sediment - Tallahassee Central LaboratoryFIELD MEASUREMENT OF HYDROGEN ION ACTIVITY (pH)FIRLD MEASUREMENT OF SPECIFIC CONDUCTANCEFIELD MEASUREMENT OF SALINITYFIELD MEASUREMENT OF TEMPERATUREFIELD MEASUREMENT OF DISSOLVED OXYGENFIELD MEASUREMENT OF TURBIDITYFIELD MEASUREMENT OF LIGHT PENETRATION (SECCHIDEPTH AND TRANSPARENCY)ARSENIC BY ICPMSCOPPER BY ICPMSMANGANESE BY ICPMSNICKEL BY ICPMSLEAD BY ICPMS

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

Status21FLWPB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 208 of 515

City of West Palm Beach (Florida)

110.1 110.2 120.1 130.2 150.1 160.2 1664 170.1 180.1 200.7(W) 204.2 208.1 210.2 2120-C 213.2 218.1 2320 2340 245.1 249.2 2540-C 272.2 279.2 310.1 3111-B 3111-D 3113-B 325.1 325.3 335.3 340.3 350.1 350.2(B) 3500-CR(D) 351.2 352.1 352.1+354.1 353.3 354.1 360.1 365.1 365.4 405.1 410.4

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA USEPA USEPA APHA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA 21FLWPBH USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Color by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHNon-Filterable Residue - TSSExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals in Water by ICP-AESAntimony by GFAABarium by FLAABeryllium by GFAAColor in Water by SpectrophotometryCadmium by GFAAChromium by FLAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAANickel by GFAATotal Dissolved Solids in WaterSilver by GFAAThallium by GFAAAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAChloride by Colorimetric Analysis IChloride by Mercuric Nitrate TitrationTotal Cyanide by Colorimetric AnalysisFluoride in Water by ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryTotal Hexavalent Chromium in WaterTotal Kjeldahl Nitrogen by ColorimetryNitrate Nitrogen by ColorimetryNITROGEN ,TOTALNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandChemical Oxygen Demand by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLWPBH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 209 of 515

City of West Palm Beach (Florida)

415.1 4500-CL(B) 4500-CL-(B) 4500-H 4500-O-G 9222-B 9222-D

Procedure Id

USEPA APHA APHA APHA APHA APHA APHA

Procedure Source

Total Organic Carbon by CombustionResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Titration- Argentometric MethodpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status21FLWPBH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 210 of 515

Florida Department of Environmental Protection

10200-G 10200-H 110.2 120.1 150.1 160.1 160.2 1652 170.1 180.1 200.7(W) 200.8(W) 2340 245.1 245.5 2520-B 2580 300(A) 310.1 340.2 350.1 351.2 353.2 360.1 365.1 365.4 370.1 375.4 376.1 415.1 5210-B 6010B 608 614 8081A(SNB) 8270C(S) 8270C(W) 8321 9222-B 9222-D 9230-C DEP-SOP-BB14 DEP-SOP-BB15_5 DEP-SOP-FT 1800

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA 21FLWQA 21FLWQA 21FLWQA

Procedure Source

Zooplankton Counting TechniquesChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSOil and GreaseTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Water by CVAAMercury in Sediment by CVAASalinity in Water- Electrical Conductivity MethodOxidation-Reduction Potential of WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate by Turbidimetric DeterminationSulfide by Titration with IodineTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandInductively Coupled Plasma AESOrganochlorine Pesticides and PCBs by GCOrganophosphorus Pesticides IOrganochlorine Pesticides and PCBs by GCSemivolatile Organic Compounds by CGC/MSSemivolatile Organic Compounds by CGC/MSNon-Volatile Compounds by HPLCStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueMeasurement of Sediment Total Dry WeightLaser Measurement of Sediment Particle SizeField Measurement of Water Flow and Velocity

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLWQA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 211 of 515

Florida Department of Environmental Protection

DEP-SOP-FT-1700

DEP-SOP-NU-076 EPA 10200G EPA 10200H EPA 160.2 EPA 200.7

EPA 200.8

EPA 245.2 EPA 340.2 EPA 415.1 EPA 5210B EPA 9222B

EPA 9222D

Procedure Id

21FLWQA

21FLWQA 21FLWQA 21FLWQA 21FLWQA 21FLWQA

21FLWQA

21FLWQA 21FLWQA 21FLWQA 21FLWQA 21FLWQA

21FLWQA

Procedure Source

Field Measurement of Light Penetration (Secchi Depth andTransparency)Percent Carbon in Solid MatricesEPA Standard Method 10200 G (mod.)Chlorophyll determined by EPA Method Standard Method 10200HTotal Suspended Solids determined by EPA Standard Method 160.2Metals, Total Recoverable, in aqueous samples using trace-ICPemission spectroscopy, ModMetals, Total Recoverable, in aqueous samples using ICP massspectroscopy, mod.Mercury in aqueous samples using cold vapor AA spectroscopyFlouride detected by EPA Standard Method 340.2EPA Method 415.1 for Total Organic Carbon in aqueous matricesBiological Oxygen Demand by EPA Standard Method 5210bTotal Coliform determination by EPA Method Standard Method9222BFecal Coliform determination by EPA Method Standard Method9222D

Procedure Name

Active

ActiveSuspSuspSuspSusp

Susp

SuspSuspSuspSuspSusp

Susp

Status21FLWQA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 212 of 515

FDEP, Water Quality Standards and Special Projects (Florida)

10200-H 110.2 350.1 351.2 353.2 365.1 415.1 FT1100 FT1600

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA 21FLWQSP 21FLWQSP

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Organic Carbon by CombustionFIELD MEASUREMENT OF HYDROGEN ION ACTIVITY (pH)FT 1600 FIELD MEASUREMENT OF TURBIDITY

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21FLWQSP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 213 of 515

Georgia Environmental Protection Division

10200-H 110.2 130.2 150.1 160.1 160.2 1600

180.1 200.7(W) 2320 245.1 2520-B 300_M 365.1 405.1 4500-NH3(G) 4500-O-G 502.1 5220-D 5550-B 6010B 8001(A2) 8157 8260B 9221-C

9221-D 9221-E

9221-F D1889 I2600(W) UNKNOWN

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA APHA USEPA APHA USEPA USEPA USEPA APHA APHA USEPA APHA APHA USEPA HACH HACH USEPA APHA

APHA APHA

APHA ASTM USDOI/USGS 21GAEPD

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Turbidity by NephelometryMetals in Water by ICP-AESAlkalinity in Water by TitrationMercury in Water by CVAASalinity in Water- Electrical Conductivity MethodDetermination of Anions by ICPhosphorus by Colorimetry5 Day Biochemical Oxygen DemandAmmonia in Water Using Automated Phenate MethodTotal Dissolved Oxygen by Membrane Electrode MethodVolatile Halogenated OrganicsChemical Oxygen Demand by Colorimetry- Closed RefluxTannin and Lignin by ColorimetryInductively Coupled Plasma AESTotal, Fecal and E. Coli ColiformDissolved Oxygen in WaterVolatile Organics by CGC/MSEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueEscherichia coli, Multi-tube Fermentation TechniqueTurbidity of WaterPhosphorus in Water by ColorimetryUnknown Field/Lab Procedure code defined for DNR-GA

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActive

Status21GAEPD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 214 of 515

Guam Environmental Protection Agency

9223-B GUAM01

Procedure Id

APHA 21GUAM

Procedure Source

Enzyme Substrate Test, E. coli, Coliform GroupLegacy Guam EPA Analytical Procedures

Procedure Name

ActiveActive

Status21GUAM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 215 of 515

Hawaii Dept. of Health

180.1 2580 8311 9050 BACTI SAMP 01 BACTI SAMP 02 BACTI SAMP 03 CHEM SAMP 01 CHEM SAMP 02 CHEM SAMP 03 CHEM SAMP 04 HISTORIC

Procedure Id

USEPA APHA HACH USEPA 21HI 21HI 21HI 21HI 21HI 21HI 21HI 21HI

Procedure Source

Turbidity by NephelometryOxidation-Reduction Potential of WaterOzone in WaterSpecific ConductanceEnterococcusClostridium perfringensFecal ColiformSalinity, Temperature, DOTurbiditypHNitrate, Total N, Total P, Si, TSS, Ammonia N, Chlorophyll 'a';Hawaii historic procedures for Legacy STORET

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21HI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 216 of 515

Hawaii Department of Health Special Monitoring (HI)

HISPEC

Procedure Id

21HISPEC

Procedure Source

Hawaii Special Monitoring Legacy Monitoring

Procedure Name

Active

Status21HISPEC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 217 of 515

Iowa Dept. of Natural Resources

00-02 10200-H 130.2 150.1 160.1 160.4 1603

180.1 200.7(W) 200.8(W) 200.9 2130-B 2340 245.1 245.2 2510 2540-C 2550 279.2 300(A) 310.1 3113-B 314 325.3 335.2 340.2 350.1 351.1 351.2 353.2 365.1 365.2 365.4 370.1 405.1 410.2 415.1 415.2 445 4500-CL(G) 4500-CN(E) 4500-H 4500-O-G

Procedure Id

USEPA APHA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA

Procedure Source

Gross Alpha Activity in Drinking Water by CoprecipitationChlorophyll a-b-c DeterminationTotal HardnesspHFilterable Residue - TDSVolatile ResidueEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Turbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAANephelometric MethodHardness in Water by EDTA TitrationMercury in Water by CVAAMercury by CVAAConductivity in WaterTotal Dissolved Solids in WaterTemperature of Water by ThermometerThallium by GFAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by GFAAPerchlorate in Drinking Water using Ion ChromatographyChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by Colorimetry5 Day Biochemical Oxygen DemandLow Level Chemical Oxygen DemandTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterIn-Vitro Determination of ChlorophyllResidual Chlorine by Colorimetry- DPD Colorimetric MethodCyanide in Water by ColorimetrypH in WaterTotal Dissolved Oxygen by Membrane Electrode Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21IOWA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 218 of 515

Iowa Dept. of Natural Resources

4500-P-E 4500-SI(D) 507 508 515.1 5210-B 524.2 5310-B 547 6020 625 7471A 8082(S) 8082(W) 900 903 9213-D 9221-B

9221-E

9221-F 9222-D 9223-B APHA 8010F APHA 9222 G APHA 9223 B ASTM D6503-99 ASTM D888-05(C)EPA 515.3 EPA 7471A-UHL EPA 8081A GLYCOL LC/MS HYDROLAB I3765 LAC10-107-06-1JLAC10-107-06-2EPHARMA LC-1 SU-IMI/LCMS TIM 380-75WE UHL 8260 UHL OA-2 UHL8270 UHLESA/OXA

Procedure Id

APHA APHA USEPA USEPA USEPA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

APHA

APHA APHA APHA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA USDOI/USGS 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA 21IOWA

Procedure Source

Phosphorus in Water by Colorimetry- Ascorbic Acid MethodSilica in Water by Spectrophotometry- Molybdosilicate MethodNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandPurgeable Organics in Water by CGC/MSTotal Organic Carbon by Combustion-Infrared MethodGlyphosate in Drinking Water by HPLCInductively Coupled Plasma - Mass Spec.Base/Neutral and Acid Organics in WastewaterMercury in Solid or Semisolid WastePCBs as Aroclors by Capillary Column GCPCBs as Aroclors by Capillary Column GCGross Alpha and Beta Activity in WaterRadium in Drinking WaterE. coli methodStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueEscherichia coli, Multi-tube Fermentation TechniqueFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupToxicity Test Systems, Matrials, and ProceduresFecal coliform- MF Partition ProceduresEnzyme Substrate Coliform TestStandard Test Method for Enterococci in Water Using EnterolertDissolved Oxygen by Luminescence-based SensorDETERMINATION OF CHLORINATED ACIDS IN DRINKINGMercury in Solid or Semisolid Waste (UHL version)Organochlorine Pesticides and PCBs by GCGLYCOL LC/MS (UHL)HYDROLABResidue by Evaporation and GravimetricLAC10-107-06-1J (UHL)LAC10-107-06-2E (UHL)PHARMA LC-1 (UHL)SU-IMI/LCMS (UHL)TIM 380-75WE (UHL)GC/MS VolatilesTotal Extractable HydrocarbonsSemiVolatiles by GC/MSESA/OXA LC/MS(UHL)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21IOWA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 219 of 515

Iowa Dept. of Natural Resources

UHLIMA USGS CA8

Procedure Id

21IOWA 21IOWA

Procedure Source

Immunoassay for triazine herbicidesUSGS Flow Measurement

Procedure Name

ActiveActive

Status21IOWA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 220 of 515

Kansas Dept. of Health & Environment

10200-H 1104 120.1 150.1 160.2 170.1 180.1 200.7(W) 200.8(W) 2340 245.1 300(A) 310.1 350.1 351.1 360.1 365.1 405.1 5210-B 5310-B 608 615 900 9222-D 9230-C I751-8

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA APHA APHA 21KAN001

Procedure Source

Chlorophyll a-b-c DeterminationE. coli in Drinking Water/EC Medium with Mug TubConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Water by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by Colorimetry5 Day Biochemical Oxygen Demand5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodOrganochlorine Pesticides and PCBs by GCChlorinated Herbicides in WastewaterGross Alpha and Beta Activity in WaterFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueTotal Dissolved Solids

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21KAN001

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 221 of 515

Kentucky Division of Water

$6240 $6260 % DO SATURATION160.2_M 160.3 1631 180.1 200.7(W) 200.8(W) 305.1 310.1 350.1 351.2 353.2_M 365.1 375.1 415.1 507 508 515.2 531.1 547 555 8081A(SWB) 8260B 8270C(S) EUPHOTIC ZONE MAXIMUM DEPTH SECCHI DISK SM 1002 G.2 SM2340 B SM2510 B SM2550 B SM4500-CL B SM4500-H+ B SM4500-O G SM5310C SM9222 D

TAPEDOWN

Procedure Id

21KY 21KY 21KY USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21KY 21KY 21KY 21KY 21KY 21KY 21KY 21KY 21KY 21KY 21KY 21KY

21KY

Procedure Source

Determination of Nitrogen-Phosphorus Pesticides in WaterDetermination of Pesticides in Water% DO saturationTotal Suspended SolidsTotal ResidueMercury in Water by Oxidation, Purge and Trap, and CVAFSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSAcidity by Titration with a pH MeterAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryPhosphorus by ColorimetrySulfate by Colorimetry With ChloranilateTotal Organic Carbon by CombustionNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Acids in Water by GCN-Methylcarbamates in Water by HPLCGlyphosate in Drinking Water by HPLCChlorinated Acids in Water by HPLCOrganochlorine Pesticides and PCBs by GCVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSDEPTH OF 1% LIGHT PENETRATIONMAXIMUM LAKE DEPTHSECCHI DISK VISIBILITYFluorometric Metdod for Chlorophyll aHARDNESS BY CALCULATIONLABORATORY METHOD FOR CONDUCTIVITYLABORATORY AND FIELD METHODS FOR TEMPERATUREARGENTOMETRIC METHOD FOR CHLORIDEELECTROMETRIC METHOD FOR pH MEMBRANE ELECTRODE METHOD FOR DISSOLVED OXYGENTOTAL ORGANIC CARBONMEMBRANE FILTER TECHNIQUE FOR FECAL COLIFORMBACTERIABRIDGE TAPEDOWN

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Status21KY

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 222 of 515

Michigan Department of Environmental Quality

MDEQ-EPA

Procedure Id

21MICH

Procedure Source

MDEQ Field/Lab Analytical Procedure

Procedure Name

Active

Status21MICH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 223 of 515

MS. Dept. of Environmental Quality

10200-H 120.1 130.1 150.1 160.1 160.1_M 160.2 160.2_M 160.3 160.4 1664 170.1 180.1 200.7(S) 200.7(W) 200.7_M 200.9 2120-B 215.2 245.1 2520-B 300(A) 305.1 310.1 325.1 330.4 330.5 335.1 335.2 335.2_MB(W) 340.2 340.2_M 350.1 350.2(B) 3500-CR(B) 351.2 351.3(A) 351.3(B) 351.3(C) 351.4 353.2 354.1 360.1 365.2

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnesspHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsTotal ResidueVolatile ResidueExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESICP-AES For Trace Element AnalysisMetals by Temperature Stabilized GFAAColor in Water by Visual ComparisonCalcium by EDTA Titrimetric AnalysisMercury in Water by CVAASalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAlkalinity by TitrationChloride by Colorimetric Analysis ITotal Residual Chlorine by TitrationChlorine by Spectrophotometry with DPDCyanides Amenable to ChlorinationTotal Cyanide in WaterTotal Cyanide in Water by ColorimetryFluoride in Water Using an ISEFluoride with an Ion Selective ElectrodeAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryChromium in Water by FLAA or GFAATotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricTotal Kjeldahl Nitrogen Using an ISENitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21MSWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 224 of 515

MS. Dept. of Environmental Quality

375.4 376.2 377.1 405.1 410.4 415.1 420.1 5540-C 8015B 8082(S) 8082(W) 8151(S) 8151(W) 8260B 8270C(S) 8270C(W) 9010A(A) 9040A 9045B 9060 9221-D 9221-E

9222-B 9222-D 9230-B

ASTM_D6503-99 MS10200H MS1030F-5 MS106.4 MS1600 MS1983 MS200.7F MS200.7SP MS200.9F MS200.9S MS353.2(S) MS353.2A MS353.2AW MS353.2_I MS445N MS446 MS8015B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

APHA APHA APHA

21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ

Procedure Source

Sulfate by Turbidimetric DeterminationSulfide by Colorimetric DeterminationSulfite in Water by Titration5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterAnionic Surfactants in Water as MBASNon-Halogenated Organics Using GC/FIDPCBs as Aroclors by Capillary Column GCPCBs as Aroclors by Capillary Column GCChlorinated Herbicides in Soils by GCChlorinated Herbicides in Water by GCVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSSemivolatile Organic Compounds by CGC/MSTotal and Amenable Cyanides by ColorimetrypH in Water by Electrometric MeasurementSoil and Waste pHTotal Organic Carbon in Water and WasteEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueMDEQ ASTM D6503-99Standard Methods 10200 HStandard Methods 1030F-5EPA Method 106.4EPA1600WETZEL 1983MDEQ Method 200.7 for Fish TissueMDEQ Method 200.7 for Special SubstancesMDEQ Method 200.9 Fish TissueMDEQ Metals by Temp Stabilized GFAA in SoilMDEQ Nitrate-Nitrite Nitrogren in Soil by ColorometryMDEQ 353.2 NitrateMDEQ 353.2 Dissolved Nitrate in WaterMDEQ 353.2 Nitrite in SoilNon-acidification (Welchmeyer)SpectrophotometerMDEQ DRO by GC Mass Spectrometer

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21MSWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 225 of 515

MS. Dept. of Environmental Quality

MS8081A MS8270F MS9221 MS9222 MS_EPA_DIESEL MS_EPA_DIESL(S)UNKNWN

Procedure Id

21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ 21MSWQ

Procedure Source

MDEQ Organochlorine PesticidesMDEQ Semivolatile Organic Compounds in Fish TissueStandard Methods 9221Standard Methods 9222EPA Proposed Diesel Range OrganicsEPA Proposed Diesel Range Organics in SoilMethod Unknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Status21MSWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 226 of 515

NCDENR-DWQ

10200-H 110.1 110.2 120.1 130.2 150.1 160.1 160.2 160.3 160.4 1664 170.1 180.1 200.7(W) 200.8(W) 206.2 213.2 218.4 220.2 239.2 245.1 272.2 305.1 310.1 310.2 325.3 335.2 340.2 350.1 350.2(A) 350.2(B) 350.2(C) 3500-CR(B) 351.1 351.2 353.2 360.1 365.1 365.2 370.1 375.4 376.2 413.1 415.1

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationColor by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSArsenic by GFAACadmium by GFAAHexavalent Chromium by FLAACopper by GFAALead by GFAAMercury in Water by CVAASilver by GFAAAcidity by Titration with a pH MeterAlkalinity by TitrationAlkalinity by Colorimetric AnalysisChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationChromium in Water by FLAA or GFAATotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryDissolved Silica by ColorimetrySulfate by Turbidimetric DeterminationSulfide by Colorimetric DeterminationTotal Recoverable Oil and GreaseTotal Organic Carbon by Combustion

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NC01WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 227 of 515

NCDENR-DWQ

420.1 425.1 445 5210-B 5220-B 9222-B 9222-D ACALK_FIELD ACALK_LAB

ALK_PHFIELD ALK_PHNPHTH CHLA_FLUOR CHLA_SPEC CHLA_TRICH CLR_PH76 CLR_PHSAMP COD_HIGH COD_LOW ECOLI_MFMTEC ENT_MFME FEC_MF FEC_MPNEC FLOW_SPLWY GO_FREON

GO_SEVERITY GO_SOX

MICRO NO2_AS_N NO2_AS_NO2 NO3_ASN NO3_ASNO3 PHEO_FLUOR PHEO_SPEC PH_FIELD PH_LAB REF_POINT

RES_105 RES_180 SED_DRY

SED_WET

Procedure Id

USEPA USEPA USEPA APHA APHA APHA APHA 21NC01WQ 21NC01WQ

21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ

21NC01WQ 21NC01WQ

21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ

21NC01WQ 21NC01WQ 21NC01WQ

21NC01WQ

Procedure Source

Total Recoverable Phenolics in WaterMethylene Blue Active SubstancesIn-Vitro Determination of Chlorophyll5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Open Reflux MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFIELD DETERMINATION OF ACIDITY/ALKALINITYLAB DETERMINATION OF ACIDITY/ALKALINITY FROMPRESERVED SAMPLEFIELD DETERMINATION OF PHENOLPHTHALEIN ALKALINITYLAB DETERMINATION OF PHENOLPHTHALEIN ALKALINITYCHLOROPHYLL A FLUOROMETRIC METHODCHLOROPHYLL A SPECTROPHOTOMETRIC METHODCHLOROPHYLL A TRICHROMATIC METHODTRUE COLOR DETERMINED AT PH 7.6TRUE COLOR DETERMINED AT UNADJUSTED SAMPLE PHCOD HIGH RANGE, 0.25N K2CR2O7 AS REAGENTCOD LOW RANGE 0.025N K2CR2O7 AS REAGENTE COLI, MF, MTECENTEROCOCCI, MF,MEFECAL COLIFORM, MF, MFC AGAR, 44.5CFECAL COLIFORM, MPN, EC MEDIUM, 44.5CSPILLWAY DISCHARGE INSTANTANEOUS FLOWOIL AND GREASE, FREON EXTRACTION, TOTALRECOVERABLEGREASE AND OIL SEVERITY, FIELD OBSERVATIONOIL AND GREASE, SOXHLET EXTRACTION, TOTALRECOVERABLEMICROBIOLOGICAL ANALYTICAL METHODSNITRITE NITROGEN MG/L AS NNITRITE NITROGEN MG/L AS NO2NITRATE NITROGEN MG/L AS NNITRATE NITROGEN MG/L AS NO3PHEOPHYTIN A FLUOROMETRIC METHODPHEOPHYTIN A SPECTROPHOTOMETRIC ACID. METHODPH FIELD MEASUREMENTPH LAB ANALYSIS FROM SAMPLEREFERENCE POINT READING; HEIGHT OF RP FROM WATERSURFACERESIDUE DRIED AT 105CRESIDUE DRIED AT 180CANALYTE AS DRY WEIGHT, UNKNOWN EPA-APPROVEDMETHOD FOR SEDIMENT ANALYSISANALYTE AS WET WEIGHT, UNKNOWN EPA-APPROVED

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

Active

Status21NC01WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 228 of 515

NCDENR-DWQ

SETT_RATE STRP_MFENT

STRP_MFKF TOTAL_IMM TOTAL_IMM_LES TOTAL_MPNCONFRMUNKNOWN WQS SOP

Procedure Id

21NC01WQ 21NC01WQ

21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ 21NC01WQ

Procedure Source

METHOD FOR SEDIMENT ANALYSISSETTLEABLE MATTER M/L/HRFECAL STREPTOCOCCI,MF,M-ENTEROCOCCUS MEDIUM, 35C48HRFECAL STREPTOCOCCI, MF,KF MEDIUM, 35C 48HRTOTAL COLIFORM, MF,IMMEDIATE,M-ENDO AGAR, 35CTOTAL COLIFORM, MF, LES ENDO AGAR, 35CTOTAL COLIFORM, MPN, CONFIRMED TEST 35CUNKNOWN EPA-APPROVED METHODWATER QUALITY SECTION SOP

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActive

Status21NC01WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 229 of 515

NCDENR-DWQ (2nd)

110.1 110.2 120.1 130.2 160.1 160.2 160.3 160.4 1664 180.1 200.7(W) 200.8(W) 206.2 213.2 220.2 239.2 245.1 2540-B 2540-C 2540-D 272.2 300(A) 300(B) 305.1 310.1 310.2 325.3 335.2 340.2 350.1 350.2(A) 350.2(B) 350.2(C) 351.1 351.2 353.2 365.1 365.2 375.4 413.1 415.1 420.1 425.1 445

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Color by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltConductanceTotal HardnessFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueExtractable Material in Oil and GreaseTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSArsenic by GFAACadmium by GFAACopper by GFAALead by GFAAMercury in Water by CVAATotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSilver by GFAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAlkalinity by TitrationAlkalinity by Colorimetric AnalysisChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetrySulfate by Turbidimetric DeterminationTotal Recoverable Oil and GreaseTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterMethylene Blue Active SubstancesIn-Vitro Determination of Chlorophyll

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NC02WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 230 of 515

NCDENR-DWQ (2nd)

5210-B 5220-B 8000 9222-B 9222-D ACALK_FIELD COLOR_PH7.6 COLOR_SAMPLE PHFORMALDEHYDE HARDNESS_CAL OIL_GREASE WQS SOP

Procedure Id

APHA APHA HACH APHA APHA 21NC02WQ 21NC02WQ 21NC02WQ 21NC02WQ 21NC02WQ 21NC02WQ 21NC02WQ

Procedure Source

5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Open Reflux MethodChemical Oxygen DemandStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureAlkalinity FieldTrue Color at pH of 7.6True Color at Sample pH, ADMIFormaldehydeHardness by CalculationOil and GreaseWater Quality Section SOP

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NC02WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 231 of 515

North Dakota Department of Health

00-04 100 10200-H 10200-J 1030 1030-F 10300-C 107 1103.1

120.1 150.1 200 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 2320 245.1 300 300(A) 305.2 310.1 340.2 350.1 3500-CR(E) 351.2 353.2 365.1 4110-B 4500-CL-(E) 4500-NH3(C) 4500-NOR(B) 4500-O-G 4500-SO4(B) 504.1 508 515.1 5210-B 524.2 525.2 531.1 5310-C

Procedure Id

USEPA 21NDHDWQ APHA APHA 21NDHDWQ 21NDHDWQ APHA USEPA USEPA

USEPA USEPA 21NDHDWQ USEPA USEPA USEPA USEPA USEPA APHA USEPA 21NDHDWQ USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA APHA USEPA USEPA USEPA APHA

Procedure Source

Plutonium, Thorium & Uranium in Air Filters100 CountChlorophyll a-b-c DeterminationMetabolic Rate MeasurementsData QualityChecking Correctness of AnalysesPeriphyton Sample AnalysisVinyl Chloride - WastewaterEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)ConductancepH200 CountMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationMercury in Water by CVAA300 CountInorganic Anions by Ion ChromatographyAcidity by Titration Using a pH MeterAlkalinity by TitrationFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryChromium in Water by Ion ChromatographyTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryAnions in Water by Ion ChromatographyChloride in Water by Colorimetry- Automated Ferricyanide MethodAmmonia in Water by Titrimetric MethodTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodSulfate in Water by Ion ChromatographyEDB, DBCP and 123TCP in Water by GCChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyN-Methylcarbamates in Water by HPLCTotal Organic Carbon in Water- Ultraviolet Oxidation Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NDHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 232 of 515

North Dakota Department of Health

552 6610-B 9221-C

9222-B 9222-D 9230-C 9240-B 999 AMPULE I-1-37 STANDARD METHODUNKOWN YSIMETER

Procedure Id

USEPA APHA APHA

APHA APHA APHA APHA 21NDHDWQ 21NDHDWQ 21NDHDWQ 21NDHDWQ 21NDHDWQ 21NDHDWQ

Procedure Source

Haloacetic Acids in Water by GCCarbamate Pesticides in Water by HPLCEstimation of Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueEnumberation-Enrichment & Isolation of Iron and Sulfur BacteriaEntire CountTest for Chemical Oxygen DemandSOP Using Microwave DigestionStandard MethodsUnknownYSI Environmental Operations Meter

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NDHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 233 of 515

Nebraska Dept. of Environmental Quality

10200-H 1106_1 120.1 150.1 150.2 160.1 160.2 160.2_M 1618 1653 170.1 180.1 200.8(W) 206.2 208.1 212.3 213.1 215.1 219.1 220.1 236.1 236.2 239.2 242.1 243.1 245.1 249.1 258.1 272.1 272.2 273.1 279.1 286.1 289.1 310.1 310.2 325.2 350.1 351.2 353.2 360.2 365.1 365.4 365.5

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationEnterococci in Water by Membrane FilterConductancepHpH by Continuous MonitoringFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsPesticides and HerbicidesChlorinated Phenolics by GC/MSTemperatureTurbidity by NephelometryMetals in Waters by ICP/MSArsenic by GFAABarium by FLAABoron by Colorimetric AnalysisCadmium by FLAACalcium by FLAACobalt by FLAACopper by FLAAIron by FLAAIron by GFAALead by GFAAMagnesium by FLAAManganese by FLAAMercury in Water by CVAANickel by FLAAPotassium by FLAASilver by FLAASilver by GFAASodium by FLAAThallium by FLAAVanadium by FLAAZinc by FLAAAlkalinity by TitrationAlkalinity by Colorimetric AnalysisChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryTotal Phosphorus After Block DigestionOrthophosphate in Water by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NEB001

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 234 of 515

Nebraska Dept. of Environmental Quality

365_M 375.2 375.4 405.1 410.4 410_M(B) 4500-H 4500-NO3(B) 4500-NO3(D) 4500-P-E 524.2 525.2 7190 8060(ECD) DISCHARGE E. COLI ENTEROCOCCI EPA1990MACROFLDF488 PMD-AM-S PMD-DCA(GC1)

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA 21NEB001 21NEB001 21NEB001 21NEB001 ASTM USEPA USEPA

Procedure Source

Phosphorus in Water by ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryChemical Oxygen Demand by TitrationpH in WaterNitrate in Water by Ultraviolet SpectrophotometryNitrate in Water Using an ISEPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyChromium by FLAAPhthalate Esters by Gas ChromatographyDischarge, CFSE. ColiENTEROCOCCI METHODSMacroinvertebrate Field & Laboratory MethodsBacterial Count in WaterAMS by Sodium Nitrate Titration2,4-D and 2,4,5-T Esters by GC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NEB001

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 235 of 515

Nevada Dept. of Conservation and Natural Resources

110.2 1106.1

1106_1 120.1 150.1 150.2 160.1 160.1_M 160.2 1664 180.1 200.7(W) 200.7_M 200.8(S) 200.8(W) 2120-B 2120-C 215.1 2160-C 2320 242.1 245.2 245.2_M 2510 2540-C 2540-E 258.1 273.1 279.1 300(A) 300(B) 300_M 310.1 3113-B 350.1 351.2 353.2 360.1 365.1 4500-CL-(F) 4500-CN(E) 4500-F-C 4500-NH3(F)

Procedure Id

USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA APHA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA

Procedure Source

Color Analysis Using Platinum/CobaltEnterococci in Water by Membrane Filtration Using membrane-Enterococcus-Esculin Iron Agar (mE-EIA)Enterococci in Water by Membrane FilterConductancepHpH by Continuous MonitoringFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSExtractable Material in Oil and GreaseTurbidity by NephelometryMetals in Water by ICP-AESICP-AES For Trace Element AnalysisMetals in Wastes by ICP/MSMetals in Waters by ICP/MSColor in Water by Visual ComparisonColor in Water by SpectrophotometryCalcium by FLAATaste in Water by Flavor RatingAlkalinity in Water by TitrationMagnesium by FLAAMercury by CVAAMercury in Water by Automated CVAAConductivity in WaterTotal Dissolved Solids in WaterFixed and Volatile Solids in WaterPotassium by FLAASodium by FLAAThallium by FLAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyDetermination of Anions by ICAlkalinity by TitrationMetals in Water by GFAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryChloride in Water by Ion ChromatographyCyanide in Water by ColorimetryFluoride in Water Using an ISEAmmonia in Water Using Phenate Method

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NEV-1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 236 of 515

Nevada Dept. of Conservation and Natural Resources

4500-NO2(B) 4500-NO2(C) 4500-NOR(B) 4500-P-E 5210-B 5220-C 8001(1) 8156 9222-D 9223-B 9230-C D2972(A) D2972(B) D2972(C) FLOW

Procedure Id

APHA APHA APHA APHA APHA APHA HACH HACH APHA APHA APHA ASTM ASTM ASTM 21NEV-1

Procedure Source

Nitrite in Water by ColorimetryNitrite in Water by Ion ChromatographyTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid Method5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Closed Reflux MethodTotal, Fecal and E. Coli ColiformpH in WaterFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Membrane Filter TechniqueArsenic in Water Using SpectrophotometryArsenic in Water Using HYDAAArsenic in Water by GFAAStream flow determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NEV-1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 237 of 515

NJ Department of Environmental Protection

10200-H 1103.1 130.1 160.2 1600 1664 180.1 200.7(S) 200.7(W) 200.9 206.5 2060 2120-B 213.2 218.2 220.2 2310 2320 2340-B 239.2 245.1 245.2 249.2 2510 2520-B 2540-B 2540-C 2540-D 2540-F 300.0 300_M 350.1 350.4 351.1 351.2 353.2 353.2 353.3 360.2 365.1 365.2 365.4 365.5 365.5

Procedure Id

APHA 21NJDEP1 USEPA USEPA 21NJDEP1 USEPA USEPA USEPA USEPA USEPA USEPA 21NJDEP1 APHA USEPA USEPA USEPA APHA APHA 21NJDEP1 USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA 21NJDEP1 USEPA USEPA 21NJDEP1 USEPA USEPA 21NJDEP1 USEPA USEPA USEPA USEPA USEPA USEPA 21NJDEP1 USEPA

Procedure Source

Chlorophyll a-b-c DeterminationEscherichia coli - Membrane FiltrationTotal HardnessNon-Filterable Residue - TSSEnterococcus - Membrane FilterExtractable Material in Oil and GreaseTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals by Temperature Stabilized GFAAArsenic Digestion for HYDAA(USGS) Pesticides in Filtered WaterColor in Water by Visual ComparisonCadmium by GFAAChromium by GFAACopper by GFAAAcidity in Water by TitrationAlkalinity in Water by TitrationHardness by CalculationLead by GFAAMercury in Water by CVAAMercury by CVAANickel by GFAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSettleable Solids in WaterInorganic Anions by Ion ChromatographyDetermination of Anions by ICAmmonia Nitrogen by ColorimetryAmmonia in seawaterTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate (as N) Automated Diazotization w/o Cd Reduction ColumnNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionLeeds PhosphorusOrthophosphate in Water by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NJDEP1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 238 of 515

NJ Department of Environmental Protection

365.8 376.2 418.1 420.1 440(W) 445 4500-CL-(B) 4500-CN(E) 4500-F-C 4500-H 4500-I-(B) 4500-N 4500-O-C 4500-S2(E) 4500-SI(D) 4500-SO4(E) 5210-B 5310-C 5320-B 5540-C 5910-B 6010B 608 624 625 7471

9215-B 9221-B

9221-B-2 (3T) 9221-B-2 (5T) 9221-C

9221-E

9221-E-1 (12T) 9221-E-1 (3T) 9221-E-1(5T) 9221-E-2 (3T) 9222-B 9222-D 9230-B 9230-C

Procedure Id

21NJDEP1 21NJDEP1 USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA 21NJDEP1 APHA APHA APHA APHA APHA APHA APHA APHA APHA 21NJDEP1 USEPA USEPA USEPA 21NJDEP1

APHA APHA

21NJDEP1 21NJDEP1 APHA

APHA

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 APHA APHA 21NJDEP1 21NJDEP1

Procedure Source

Hydrolyzable PhosphorusSulfide in Water by SpectrophotometryTotal Recoverable Petroleum HydrocarbonsTotal Recoverable Phenolics in WaterDetermination of Carbon and NitrogenIn-Vitro Determination of ChlorophyllChloride in Water by Titration- Argentometric MethodCyanide in Water by ColorimetryFluoride in Water Using an ISEpH in WaterIodide in Water by Spectrophotometry- Leuco Crystal Violet MethodPersulfate Method (proposed)Total Dissolved Oxygen by Titration- Azide ModificationSulfide in Water by TitrationSilica in Water by Spectrophotometry- Molybdosilicate MethodSulfate by Turbidimetric Analysis5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Ultraviolet Oxidation MethodDissolved Organic Halogen in WaterAnionic Surfactants in Water as MBASUV - Absorbing Organic CompoundsInductively Coupled Plasma-Atomic Emission SpectrometryOrganochlorine Pesticides and PCBs by GCPurgeable Organics in WastewaterBase/Neutral and Acid Organics in WastewaterMercury in Solid or Semisolid Waste (Manual Cold-VaporTechnique)Heterotrophic Plate Count- Pour Plate MethodStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueStandard Total Coliform Fermentation Technique (3 Tube Test)Standard Total Coliform Fermentation Technique 5 Tube TestEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFecal Coliform Direct Test (A-1 Medium) 12 Tube TestFecal Coliform Direct Test (A-1 Medium) 3 Tube TestFecal Coliform Direct Test (A-1 Medium) 5 Tube TestFecal Coliform Test (EC Medium) 3 Tube TestStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus - Multiple-Tube TechniqueFecal Streptococcus and Enterococcus - Membrane FilterTechnique

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActive

Status21NJDEP1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 239 of 515

NJ Department of Environmental Protection

AIRTEMP BARPRES COD

DO F+RNA COLIPHAGE

FFLOW FLOW HOBO HYDROLAB-QUANTAI-1233 I-1472 I-2030-89 I-2138 I-2274 I-2339 I-2403 I-2477

I-2515

I-2587-89 I-2668 I-2724 I-3233 I-3860-89 I-4063 I-4403 I-4471 I-4515

I-4668 I-4724 I-4729 I-6063 I-6600 I-6668 I1230 I1472 I1630(W) I2057 I2062 I2327 I2462

Procedure Id

21NJDEP1 21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1

21NJDEP1

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS

Procedure Source

Procedure for Air Temperature MeasurementsProcedure for Measuring Air PreassureChemical Oxygen Demand (COD) Vial Digestion /SpectrophotometricField Measurement - Dissolved OxygenMembrane Filter Adsorption-Elution Method with Elute Assay by theDouble Agar Layer (DAL) Method using F-amp Host CellFacility Flow(USGS) FLOWHOBO Underwater Temperature Logger (H20-001)Hach Hydrolab Quanta(USGS) Determination of chromium in water by GFAAS(USGS) Metals in Water by ICP(USGS) Alkalinity in water(USGS) Cadmium by GFAAS(USGS) Copper by GFAAS(USGS) Chromium in water by GFAAS(USGS) Lead in water by GFAA(USGS) Determination of Metals in Water by Inductively CoupledPlasma-Mass Spectrometry(USGS) Ammonium + Organic Nitrogen by a Kjeldahl Digestion Geldiffusion cleanup automated phenate finish(USGS) pH(USGS) Arsenic and Selenium by GFAAS(USGS) Silver(USGS) Chromium by GFAAS(USGS) Turbidity(USGS) Arsenic and Selenium in Water by GFAAS(USGS) Lead in Water(USGS) Elements in Water Using ICP and ICP/MS(USGS) TKN by Automated Photometric Digestion with GasDiffusion cleanup(USGS) Arsenic and Selenium in Water by GFAAS(USGS) Silver in Water(USGS) Metals in Water by ICP(USGS) Arsenic and Selenium by GFAAS(USGS) Phosphours in Bottom Material(USGS) Selenium by GFAASHexavalent Chromium by ColorimetryMetals in Water by ICPPotassium in Water by FLAAAnions in Water by Ion ChromatographyArsenic in Water by HYDAAFluoride in Water Using an ISEMercury in Water by CVAA

Procedure Name

ActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NJDEP1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 240 of 515

NJ Department of Environmental Protection

I2521 I2522 I2540 I2545(S) I2545(W) I2601 I2700 I3381 I3462 I3561 I3860 I5135 I5236 I5270 I5381 I5399 I5454 I5462 I5499 I6522 I6552 MAR NWIS O-1100-83 O-1126 O-1126-02 O-2060-01

O-4127-96 O-5101-83

O-5102-83 O-5130-95 O-7100-83 P-2330 PCB PH PH-SED R-0006 R-1120 R1110 SC SONDE SONDE-HYDRO

Procedure Id

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 USDOI/USGS 21NJDEP1 21NJDEP1 21NJDEP1

Procedure Source

Ammonia Nitrogen in Water by ColorimetryAmmonia Nitrogen in Water by ColorimetryNitrite-Nitrogen in Water by ColorimetryNitrite- Plus Nitrate-Nitrogen in SolidsNitrite- Plus Nitrate-Nitrogen in WaterOrthophosphate-Phosphorus by ColorimetrySilica in Water by ColorimetryIron in Water by FLAAMercury in Water by CVAAChemical Oxygen Demand by ColorimetryNephelometric Turbidity in WaterCadmium in Bottom Material by FLAAChromium in Bottom Material by FLAACopper in Bottom Material by FLAAIron in Bottom Material by FLAALead in Bottom Material by FLAAManganese in Bottom Material by FLAAMercury in Bottom Material by CVAANickel in Bottom Material by FLAAAmmonia Nitrogen by Colorimetry in SolidAmmonia Plus Organic Nitrogen in SolidsMultiple Antibiotic Resistance (MAR)unable to determine from USGS NWIS Web data(USGS) TOC Dissolved(USGS) Pesticides in Water by C-18 Solid Phase Extraction(USGS) Pesticides, Water, Filtered, SPE-C18, Lab Extracted(USGS) Determination of pesticides in water by graphitized carbon-based solid-phase extraction and HPLC/MS(USGS) VOC in Water by GC/MS Including DLs < RLs(USGS) Carbon, Inorganic Plus Organic, Total in Bottom Material,dry weight, induction furnace(USGS) Total Inorganic Carbon in Sediment(USGS) Semivolitile Organic Compounds in Bottom Sediment(USGS) TOC Particulate(USGS) Procedure for Sive-pipet Method of Particle Size Analysis(USGS) PCB in Bottom MaterialField Measurement - pH(USGS) Field Measurement of pH of Sediment(USGS) Radioactivity, Alpha(USGS) Radioactivity, BetaCesium-137 and 134, DissolvedField Measurement - Specific ConductanceMulti-probe Data SondeMulti-probe Data Sonde (Hydrolab)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NJDEP1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 241 of 515

NJ Department of Environmental Protection

SONDE-YSI T TURB TWRI UNKNOWN USEPA REGION IIUSGS 524.2 WDML SOP001

YSI5.13 2340B

Procedure Id

21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1 21NJDEP1

21NJDEP1 21NJDEP1

Procedure Source

Multi-probe Data Sonde (YSI)Field Measurement - TemperatureField Measurement - TurbidityTechniques of Water-Resources Investigations ReportsUnknown ProcedureMethod for BOD20 and CBOD20(USGS) VO IN GROUNDWATERDetermination of Total Mercury in Water by Oxidation, Purge andTrap, and Cold Vapor Atomic Fluorescence SpectrometryIn vivo Fluorometric Chlorophyll DeterminationHardness by ICP

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveSusp

Status21NJDEP1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 242 of 515

NM Environmental Dept./SWQB

004(W) 110.2 1103.1

1103_1 120.1 160.1 160.1_M 160.2 160.2_M 1664 200.7(W) 200.8(W) 200.9 202.1 206.2 2130 220.1 236.1 236.1_M 239.2 245.1 245.1_M 2510 2520-C 2550 270.2 270.2_M 300(A) 300_M 310.1 335.4 340.2 350.1 351.2 353.2 353.2_M 365.1 365.4 405.1 415.1 425.1 4500-CN(I) 4500-H

Procedure Id

USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

Procedure Source

Radium-226 and Radium-228 in WaterColor Analysis Using Platinum/CobaltEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)E. coli in Water by Membrane FiltrationConductanceFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsExtractable Material in Oil and GreaseMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAArsenic by GFAATurbidity in WaterCopper by FLAAIron by FLAAIron by FLAALead by GFAAMercury in Water by CVAAMercury in Water by Manual CVAAConductivity in WaterSalinity in Water- Density MethodTemperature of Water by ThermometerSelenium by GFAASelenium by GFAAInorganic Anions by Ion ChromatographyDetermination of Anions by ICAlkalinity by TitrationCyanide by Semi-Automated ColorimetryFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionMethylene Blue Active SubstancesWeak Acid Dissociable Cyanide in WaterpH in Water

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NMEX

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 243 of 515

NM Environmental Dept./SWQB

4500-O-G 508.1 515.2 525.2 531.1 547 608 7500-U-C 8000 8081A(SNB) 8260B 8270B(W) 8270C(W) 8275 8280(W) 900 900.1 901.1 903.1 904 9221-C

9222-C 9222-D 9223-B CALC-001 COLILERT-18 LIT-PHARM LIT-PHARM-02

LIT-RAD SM 2130B SM 2510A SM 2550A SM 4500H SM 4500OG SM 7500-U-C SM 9221C

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA HACH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

APHA APHA APHA 21NMEX IDEXX 21NMEX 21NMEX

21NMEX 21NMEX 21NMEX 21NMEX 21NMEX 21NMEX 21NMEX 21NMEX

Procedure Source

Total Dissolved Oxygen by Membrane Electrode MethodChlorinated Pest., Herb. and OrganohalideChlorinated Acids in Water by GCOrganics in Water by Gas ChromatographyN-Methylcarbamates in Water by HPLCGlyphosate in Drinking Water by HPLCOrganochlorine Pesticides and PCBs by GCUranium in Water by Isotopic AnalysisChemical Oxygen DemandOrganochlorine Pesticides and PCBs by GCVolatile Organics by CGC/MSSemivolatile Organics in Water by GC/MSSemivolatile Organic Compounds by CGC/MSScreening Semivolatile OrganicsPolychlorinated Dioxins and FuransGross Alpha and Beta Activity in WaterRadium in Drinking WaterGamma Emitters in Drinking WaterRadium-226 in Drinking WaterRadium-228 in Drinking WaterEstimation of Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform- Delayed-Incubation ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupSimple CalculationsColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliPharmaceuticalsLC/MS/CM for oxytetracycline, tetracycline, and chlortetracycline inwater.Method for RadionuclidesTurbidity, Nephelometric MethodConductivityTemperature pH Value Dissolved Oxygen, Membrane Electrode Method Uranium, Isotopic MethodEstimation of Bacterial Density

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

ActiveSuspSuspSuspSuspSuspSuspSusp

Status21NMEX

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 244 of 515

NYS Dept. of EnCon, Division of Water

120.1 130.2 150.1 160.1 160.2 160.3 160.4 180.1 200.7(W) 200.8(W) 206.3_M 245.1 300(A) 310.1 325.2 350.1 351.2 353.2 365.1 415.1 415.2 420.2 420.4 524.2 601 9222-B 9222-D RIBS-FIELD RIBS-OBSRV

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA 21NYDECA 21NYDECA

Procedure Source

ConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHydride Generation ICPMercury in Water by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterPurgeable Organics in Water by CGC/MSPurgeable Halocarbons in WastewaterStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureRIBS Field Data Measurement (Hydrolab, YSI instruments)RIBS Field Observations (weather, flow, etc)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21NYDECA

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and Equipment Summary

Page 245 of 515

Division of Drinking and Ground Water (Ohio)

03908 110.1 120.1 130.1 130.3 160.1 200.7(W) 210.1 220.11 230.1 240.1 240.2 245.1 250.1 250.2 250.3 250.4 250.5 260.1 270.2 280.1 310.1 310.1 320.3 320.4 32102 32103 325.1 335.1 340.1 34020 34392 34423 34501 34506 34511 34516 34551 34571 34696 350.1 351.2 375.2 38760

Procedure Id

21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW USEPA 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW USEPA 21OHDGW 21OHDGW 21OHDGW 21OHDGW USEPA 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW USEPA USEPA USEPA 21OHDGW

Procedure Source

CymeneSpecific Conductance, Lab, 25 deg. CpH, Lab, 25 deg. CResidue, TotalSolids, TotalDissolved SolidsMetals in Water by ICP-AESAcidityAlkalinity, TotalChloride, TotalCyanide, TotalCyanide, FreeMercury, TotalAmmonia, NitrogenTotal Kjeldahl NitrogenNitrate-Nitrite, NitrogenNitrogen, NitriteNitrogen, NitratePhosphorus, TotalSulfate, TotalFluoride, Total_pre 2005Biochemical Oxygen Demand, 5-dayAlkalinity by TitrationChemical Oxygen DemandCOD, 20mg/LCarbon TetrachlorideDICHLOROETHANE, 1,2-Chloride by Colorimetric Analysis ITotal Organic CarbonPhenolics, Total RecoverableXYLENE, ORTHOHEXACHLOROBUTADIENEDICHLOROMETHANEVINYLIDENE CHLORIDETRICHLOROETHANE, 1,1,1-TRICHLOROETHANE, 1,1,2-TETRACHLOROETHANE, 1,1,2,2-TRICHLOROBENZENE, 1,2,4-DICHLOROBENZENE, PARA-NAPHTHALENEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetrySulfate in Water by ColorimetryDBCP, 1,2-DIBROMO-3-CHLOROPROPANE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21OHDGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 246 of 515

Division of Drinking and Ground Water (Ohio)

401.1 407.1 417.2 524.2 524.2 525.2 620.1 625.0 77222 77223 77224 77226 77443 77562 77613 77651 85795 MTBE ORP-001 PH-001 SM 2540C SM 3113B SM 4500-FC SM 5220D SM 5310B SP.COND.-001 TDS-001 TEMP-001 TRIT

Procedure Id

21OHDGW 21OHDGW 21OHDGW 21OHDGW USEPA 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW 21OHDGW

Procedure Source

Metals, Total, ICPMetals, Total, GFAA_pre 2005Chromium, hexavalent dissolvedVolatile Organic CompoundsPurgeable Organics in Water by CGC/MSHerbicide/PesticideTotal Fecal ColiformBase Neutral & Acid ExtractableTRIMETHYLBENZENE, 1,2,4-CumenePROPYLBENZENE, N-TRIMETHYLBENZENE, 1,3,5-TRICHLOROPROPANE, 1,2,3-TETRACHLOROETHANE, 1,1,1,2-TRICHLOROBENZENE, 1,2,3-ETHYLENE DIBROMIDE (EDB)XYLENES, M & P MIXMTBEField determination of ORPField Determination of water pHTotal Dissolved SolidsTotal Metals by GFAATotal FluorideCOD determinationTOC determinationField Determination of water specific conductivityField determination of TDSField Determination of water temperatureTritium, electrolytic

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21OHDGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 247 of 515

Pennsylvania Department of Environmental Protection

00-01 0010(W) 160.5 1624(W) 1664 180.1 200.7(W) 200.8(W) 218.6 2310 2320 2340 245.1 2510 300(A) 325.2 335.4 350.1 3500-CR(D) 353.2 365.1 365_M 375.2 410.4 420.4 450.1 4500-H 4500-NOR(B) 5210-B 5310-D 608 8081(W) DEPCYAN DEPMBAS DEPOSPRESS EPA SW 846 305 EQL-05 92-086 FLOW FSTREP GALPHA GBETA H3 I1586 I3750

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA 21PA 21PA 21PA 21PA 21PA 21PA 21PA 21PA 21PA 21PA USDOI/USGS USDOI/USGS

Procedure Source

Gross Alpha and Beta Activity in WaterTritium in WaterSettleable MatterVolatiles by Isotope Dilution - WaterExtractable Material in Oil and GreaseTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHexavalent Chromium by Ion ChromatographAcidity in Water by TitrationAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAConductivity in WaterInorganic Anions by Ion ChromatographyChloride by Colorimetric Analysis IICyanide by Semi-Automated ColorimetryAmmonia Nitrogen by ColorimetryTotal Hexavalent Chromium in WaterNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus in Water by ColorimetrySulfate in Water by ColorimetryChemical Oxygen Demand by ColorimetryTotal Recoverable Phenolics in WaterTotal Organic HalidepH in WaterTotal Kjeldahl Nitrogen in Water5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Wet-Oxidation MethodOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBsCyanide in Water DEP methodDetergents and sufactantsOsmotic PressureStream Sediment ContaminentsHi Volume PotassiumStream FlowStrep-FecalAlpha-BHCbeta-BHCTritiumWater pHResidue by Evaporation and Gravimetric

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21PA

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and Equipment Summary

Page 248 of 515

Pennsylvania Department of Environmental Protection

I3765 LIPIDS PAFECAL SM209C

Procedure Id

USDOI/USGS 21PA 21PA 21PA

Procedure Source

Residue by Evaporation and Gravimetric% Lipids in Fish TissueFecal ColiformResidue, Total Filterable at 105 C

Procedure Name

ActiveActiveActiveActive

Status21PA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 249 of 515

SC Dept. of Health & Environmental Control

160.2 200.7_M 200.9 2120-B 2320 2340 245.1_M 2540-D 3112-B 3120 350.2(B) 353.2_M 415.1 445 5210-B 608 624 624-S 625 625-S 6640-B 9221-E

9222-D C-011-1 DO FIELD PARMS LAB PH

Procedure Id

USEPA USEPA USEPA APHA APHA APHA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA

APHA USEPA 21SC60WQ 21SC60WQ 21SC60WQ

Procedure Source

Non-Filterable Residue - TSSICP-AES For Trace Element AnalysisMetals by Temperature Stabilized GFAAColor in Water by Visual ComparisonAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by Manual CVAATotal Suspended Solids in WaterMercury in Water by CVAAMetals in Water by ICPAmmonia Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryTotal Organic Carbon by CombustionIn-Vitro Determination of Chlorophyll5-Day Biochemical Oxygen DemandOrganochlorine Pesticides and PCBs by GCPurgeable Organics in WastewaterOrganics in Sludge - VolatilesBase/Neutral and Acid Organics in WastewaterOrganics in Sludge - Base/Neutral and AcidChlorinated Phenoxy Herbicides in WaterEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFecal Coliform Membrane Filter ProcedureSoil % Moisture by GravimetryDissolved OxygenField parameter measurementLaboratory measured pH

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveSusp

Status21SC60WQ

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and Equipment Summary

Page 250 of 515

SC Dept of Health & Environmental Control

ENTEROLERT

Procedure Id

IDEXX

Procedure Source

Enterolert Quanti-Tray; Multi Tube, Multi Well, for Enterococcii

Procedure Name

Active

Status21SCBCH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 251 of 515

SC Dept. of Health & Environmental Control

160.2 200.7_M 245.1_M 3112-B 3120 415.1 5210-B 608 624 624-S 625 6640-B 9222-D DO FIELD PARMS H-02 TRITIUMH20

Procedure Id

USEPA USEPA USEPA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA APHA APHA 21SCESOP 21SCESOP USEPA 21SCESOP

Procedure Source

Non-Filterable Residue - TSSICP-AES For Trace Element AnalysisMercury in Water by Manual CVAAMercury in Water by CVAAMetals in Water by ICPTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandOrganochlorine Pesticides and PCBs by GCPurgeable Organics in WastewaterOrganics in Sludge - VolatilesBase/Neutral and Acid Organics in WastewaterChlorinated Phenoxy Herbicides in WaterFecal Coliform Membrane Filter ProcedureDissolved OxygenField measurementsTritium in WaterTritium analysis in water.

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21SCESOP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 252 of 515

SC Dept. of Health & Environmental Control

160.2 200.7_M 200.9 2320 2340 245.1_M 3120 340.2_M 353.2_M 415.1 D1293(B)

Procedure Id

USEPA USEPA USEPA APHA APHA USEPA APHA USEPA USEPA USEPA ASTM

Procedure Source

Non-Filterable Residue - TSSICP-AES For Trace Element AnalysisMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by Manual CVAAMetals in Water by ICPFluoride with an Ion Selective ElectrodeNitrate and Nitrite by ColorimetryTotal Organic Carbon by CombustionpH of Water By Routine Measurement

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21SCGW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 253 of 515

Santee Cooper - South Carolina Public Service Authority

10200-H 2120-B 2130 2320 2510 2540-B 2540-D 3.4 3500-AS(B) 3500-CA(B) 3500-CD(B) 3500-CR(B) 3500-CU(B) 3500-FE(B) 3500-HG(B) 3500-K-B 3500-MG(B) 3500-MN(B) 3500-NA(B) 3500-NI(B) 3500-PB(B) 3500-SE(H) 3500-ZN(B) 4110-B 4500-BR(C) 4500-CL(G) 4500-CL-(F) 4500-F-F 4500-H 4500-NH3(G) 4500-NO2(B) 4500-NO2(C) 4500-NO3(C) 4500-NO3(F) 4500-NOR(B) 4500-NOR(C) 4500-O-G 4500-P-F

4500-SO4(B) 4500-SO4(E) 5210-B 5710-D FLOW

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA APHA 21SCSANT

Procedure Source

Chlorophyll a-b-c DeterminationColor in Water by Visual ComparisonTurbidity in WaterAlkalinity in Water by TitrationConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Suspended Solids in WaterColiforms- Membrane FilterArsenic in Water by GFAA or HYDAACalcium in Water by FLAACadmium in Water by FLAA/GFAAChromium in Water by FLAA or GFAACopper in Water by FLAA or GFAAIron in Water by FLAA or GFAAMercury in Water by CVAAPotassium in Water by FLAAMagnesium in Water by FLAAManganese in Water by FLAA or GFAASodium in Water by FLAANickel in Water by FLAA or GFAALead in Water by FLAA or GFAASelenium in Water by GFAAZinc in Water by FLAAAnions in Water by Ion ChromatographyBromide in Water by Ion ChromatographyResidual Chlorine by Colorimetry- DPD Colorimetric MethodChloride in Water by Ion ChromatographyFluoride in Water by Ion ChromatographypH in WaterAmmonia in Water Using Automated Phenate MethodNitrite in Water by ColorimetryNitrite in Water by Ion ChromatographyNitrate in Water by Ion ChromatographyNitrate in Water- Automated Cadmium ReductionTotal Kjeldahl Nitrogen in WaterTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfate in Water by Ion ChromatographySulfate by Turbidimetric Analysis5-Day Biochemical Oxygen DemandTrihalomethane Formation PotentialStream Flow, Inst. (cfs)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

Status21SCSANT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 254 of 515

Santee Cooper - South Carolina Public Service Authority

UNKNOWN

Procedure Id

21SCSANT

Procedure Source

UNKNOWN

Procedure Name

Active

Status21SCSANT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 255 of 515

SC Dept of Health and Environmental Control

9221-D 9222-E

Procedure Id

APHA APHA

Procedure Source

Estimation of Bacterial Density- MPN DeterminationFecal Coliform- Delayed-Incubation Procedure

Procedure Name

ActiveActive

Status21SCSHL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 256 of 515

SD Dept of Environmental & Natural Resources

10400-D 120.1 130.1 130.2 150.1 160.1 160.1_M 160.2 160.2_M 160.3 160.4 1618 1624(W) 170.1 180.1 200.7(S) 200.7(W) 200.7_M 200.8(S) 200.8(W) 206.2 206.5 208.2 210.2 213.1 213.2 215.1 218.1 218.2 218.5 219.2 21SDAK01 220.1 220.2 231.2 2320 2340 236.2 239.1 239.2 242.1 243.2 245.1 245.1_M

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21SDAK01 USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Macrophyton Population EstimatesConductanceTotal HardnessTotal HardnesspHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsTotal ResidueVolatile ResiduePesticides and HerbicidesVolatiles by Isotope Dilution - WaterTemperatureTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESICP-AES For Trace Element AnalysisMetals in Wastes by ICP/MSMetals in Waters by ICP/MSArsenic by GFAAArsenic Digestion for HYDAABarium by GFAABeryllium by GFAACadmium by FLAACadmium by GFAACalcium by FLAAChromium by FLAAChromium by GFAAHexavalent Chromium by GFAACobalt by GFAASARCopper by FLAACopper by GFAAGold by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationIron by GFAALead by FLAALead by GFAAMagnesium by FLAAManganese by GFAAMercury in Water by CVAAMercury in Water by Manual CVAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21SDAK01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 257 of 515

SD Dept of Environmental & Natural Resources

246.2 249.1 249.2 2510 2540-B 2540-C 2540-D 2540-E 258.1 270.2 272.1 272.2 273.1 279.1 289.1 289.2 300_M 310.1 3111-B 325.1 325.2 325.3 335.2 335.3 335.4 340.3 350.1 350.2(B) 351.1 351.2 351.3(A) 351.3(C) 352.1 353.1 353.2 353.2_M 360.1 360.2 365.1 365.2 365.4 365.5 375.1 375.2

Procedure Id

USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Molybdenum by GFAANickel by FLAANickel by GFAAConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterPotassium by FLAASelenium by GFAASilver by FLAASilver by GFAASodium by FLAAThallium by FLAAZinc by FLAAZinc by GFAADetermination of Anions by ICAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameChloride by Colorimetric Analysis IChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryFluoride in Water by ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - PotentiometricNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionOrthophosphate in Water by ColorimetrySulfate by Colorimetry With ChloranilateSulfate in Water by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21SDAK01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 258 of 515

SD Dept of Environmental & Natural Resources

375.4 405.1 410.4 415.1 4500-CN(C) 4500-CN(I) 4500-F-C 4500-H 4500-NH3(G) 4500-NH3(H) 4500-NH3(H) 4500-NO2(I) 4500-NO3(F) 4500-NO3(I) 4500-NO3(I) 4500-NOR(B) 4500-P-E 4500-SO4(F) 4500-SO4(G) 500 507 MODIFIED 6010A 610 612 619 8081(W) 9221-B

9221-D 9221-E

9222-B 9222-D 9223-B 970.52 ALKALINITY P CATION-ANION BAD2036(A) DEPTH HISTORIC NONE TDS VISUAL WRAP

Procedure Id

USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA 21SDAK01 21SDAK01 APHA APHA 21SDAK01 APHA APHA APHA 21SDAK01 NIOSH 21SDAK01 USEPA USEPA USEPA USEPA USEPA APHA

APHA APHA

APHA APHA APHA AOAC 21SDAK01 21SDAK01 ASTM 21SDAK01 21SDAK01 21SDAK01 21SDAK01 21SDAK01 21SDAK01

Procedure Source

Sulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionCyanide in Water after DistillationWeak Acid Dissociable Cyanide in WaterFluoride in Water Using an ISEpH in WaterAmmonia in Water Using Automated Phenate MethodAmmonia in Water - Flow Injection AnalysisAmmonia nitrogen in water - Flow injected analysisNitrite nitrogen in water - Flow injected cadmium reductionNitrate in Water- Automated Cadmium ReductionNitrate in Water- Cadmium Reduction Flow InjectionNitrate nitrogen in water - Flow injected cadmium reductionTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSulfate in Water by ColorimetrySulfate in water - Methylthymol blue flow injection analysisTotal Particulates by Gravimetric TechniqueNitrogen and phosphorus pesticides ICP SpectroscopyPolynuclear Aromatic Hydrocarbons by GCChlorinated Hydrocarbons by GCTriazine Pesticides in WastewaterOrganochlorine Pesticides and PCBsStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupOrgano Pesticide Residues - MultiresidueALKALINITY PCation-Anion BalanceCyanides in Water After DistillationDepthHistoricNoneTDSVisualWater Resources Assistance Program

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status21SDAK01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 259 of 515

Virginia Department of Environmental Quality (VADEQ)

200 200.7(W) D3590(B) D3867(A)

Procedure Id

USEPA USEPA ASTM ASTM

Procedure Source

Metals by Atomic AbsorptionMetals in Water by ICP-AESTKN by AutoAnalyzerNitrite-Nitrate Automated Cd Reduction

Procedure Name

ActiveActiveActiveActive

Status21VASWCB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 260 of 515

Louisiana Dept of Environmental Quality

110.2 120.1 130.2 160.1 160.2 180.1 200.7(W) 200.9 245.1 300(A) 300(B) 310.1 350.3 351.2 353.2 365.4 6010B 624 625 7470A 8260B 8270C - SVOC 8270C PEST/PCB BMP-FLD D1889 NUTRIENTS-1

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 22LAGWTR 22LAGWTR 22LAGWTR 22LAGWTR ASTM 22LAGWTR

Procedure Source

Color Analysis Using Platinum/CobaltConductanceTotal HardnessFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals by Temperature Stabilized GFAAMercury in Water by CVAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionInductively Coupled Plasma AESPurgeable Organics in WastewaterBase/Neutral and Acid Organics in WastewaterMercury in Liquid Wastes by CVAAVOC's in Water - 8260BSEMIVOLATILE ORGANIC COMPOUNDS IN WATER 8270CPESTICIDES AND PCB'S IN WATER 8270CField MeasuresTurbidity of WaterNutrients in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status22LAGWTR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 261 of 515

Montana Dept. of Environmental Quality

1600

180.1 305.1 305.2 365.1 9132 9200 9250 CNMI-001 CNMI-002 CNMI-003 CNMI-004 CNMI-005

Procedure Id

USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA 21AQ 21AQ 21AQ 21AQ 21AQ

Procedure Source

Enterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Turbidity by NephelometryAcidity by Titration with a pH MeterAcidity by Titration Using a pH MeterPhosphorus by ColorimetryTotal Coliform by Membrane FilterNitrate in Water by SpectrophotometryChloride by Automated ColorimetrySalinityDissolved OxygenWaether measurementsTide and Sea StageWater temperature

Procedure Name

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status22MTHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 262 of 515

Delaware River Basin Commission

10200-H 1103_1 1106_1 120.1 130.2 150.1 160.1 160.1_M 160.2 160.2_M 160.4 170.1 180.1 200.7(W) 2310 2320 2550 305.1 310.1 325.2 350.1 3500-CR(D) 3500-CU(C) 3500-ZN(C) 351.2 353.2 354.1 360.1 360.2 365.1 405.1 415.1 4500-CL-(D) 4500-P-F

4500-SI(D) 4500-SI(E) 5210-B 524.1 524.2 525.1 5310-B 601 602

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA

APHA APHA APHA USEPA USEPA USEPA APHA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationE. coli in Water by Membrane FiltrationEnterococci in Water by Membrane FilterConductanceTotal HardnesspHFilterable Residue - TDSTotal Dissolved SolidsNon-Filterable Residue - TSSTotal Suspended SolidsVolatile ResidueTemperatureTurbidity by NephelometryMetals in Water by ICP-AESAcidity in Water by TitrationAlkalinity in Water by TitrationTemperature of Water by ThermometerAcidity by Titration with a pH MeterAlkalinity by TitrationChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Hexavalent Chromium in WaterCopper in Water by ICPZinc in Water by ICPTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by Colorimetry5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionChloride in Water by PotentiometryPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSilica in Water by Spectrophotometry- Molybdosilicate MethodSilica in Water by Spectrophotometry- Heteropoly Blue Method5-Day Biochemical Oxygen DemandPurgeable Organics in Water by GC/MSPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyTotal Organic Carbon by Combustion-Infrared MethodPurgeable Halocarbons in WastewaterPurgeable Aromatics in Wastewater by GC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

Status31DELRBC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 263 of 515

Delaware River Basin Commission

900 906 9222-D

Procedure Id

USEPA USEPA APHA

Procedure Source

Gross Alpha and Beta Activity in WaterTritium in Drinking WaterFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActive

Status31DELRBC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 264 of 515

Delaware River Basin Commission

10200-H 1103_1 120.1 130.1 160.1_M 160.2_M 170.1 180.1 2550 300(A) 310.1 350.2(C) 351.3(C) 365.2 4500-H 4500-O-G 9222-B 9222-D 9230-C DO % SAT. DO SAT VALUE F.COLIFORM FECAL FLOW GAGEHT US EPA 365.1 USEPA 445.0

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA 31DRBCSP 31DRBCSP 31DRBCSP 31DRBCSP 31DRBCSP 31DRBCSP 31DRBCSP 31DRBCSP

Procedure Source

Chlorophyll a-b-c DeterminationE. coli in Water by Membrane FiltrationConductanceTotal HardnessTotal Dissolved SolidsTotal Suspended SolidsTemperatureTurbidity by NephelometryTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by TitrationTotal Kjeldahl Nitrogen - PotentiometricPhosphorus by Single Reagent ColorimetrypH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter Techniquedissolved oxygen % saturationDissolved oxygen saturation valueFecal Coliform Analysis by National Park ServiceFecal Coliform analysis by NPSStream Flowstream gage hieghtDissolved Phosphorus AnalysisUSEPA 445.0

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status31DRBCSP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 265 of 515

Interstate Sanitation Commission (New York)

10200-H 170.1 2520-B 2520-C 2520-D 2530-B 360.1 360.2 ISC-SOP-37 ISC-SOP-38 ISC-SOP-39 ISC-SOP-40 ISC-SOP-55 SOP 25 SOP XI SOP XIA

Procedure Id

APHA USEPA APHA APHA APHA APHA USEPA USEPA 31ISC2RS 31ISC2RS 31ISC2RS 31ISC2RS 31ISC2RS 31ISC2RS 31ISC2RS 31ISC2RS

Procedure Source

Chlorophyll a-b-c DeterminationTemperatureSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodSalinity in Water- Algorithm of Practical SalinityParticulate Floatables in WaterDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniqueFloating Debris DeterminationSea Wave DeterminationCloud Cover DeterminationDepth DeterminationSECCHI DEPTH DETERMINATIONConductivityFecal and Total Coliform DeterminationFecal Streptococcus and Enterococcus Determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status31ISC2RS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 266 of 515

Ohio River Sanitation Commission

130.2 160.2 1638 200.7 200.8 2340 245.1 325.3 335.2 350.3 3500CR D 353.3 365.3 415.1 420.1 4500-NOR(B) 8051 8156 9213D 9222D

Procedure Id

USEPA USEPA USEPA 31ORWUNT 31ORWUNT APHA 31ORWUNT USEPA USEPA USEPA 31ORWUNT USEPA USEPA USEPA USEPA APHA HACH HACH 31ORWUNT 31ORWUNT

Procedure Source

Total HardnessNon-Filterable Residue - TSSTrace Elements in Water by ICP/MSICP Recoverable MetalsICPMS Recoverable MetalsHardness in Water by EDTA TitrationMercury, CVAAChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterAmmonia Nitrogen Using an ISEChromium HexavalentNitrate-Nitrite Nitrogen by Cd ReductionPhosphorus by Two Reagent ColorimetryTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterTotal Kjeldahl Nitrogen in WaterSulfate in WaterpH in WaterE. ColiFecal Coliform

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status31ORWUNT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 267 of 515

Susquehanna River Basin Commission

160.1_M 160.2_M 160.3 180.1 200.7(W) 215.2 325.2 350.1 352.1 353.2 353.2_M 354.1 365.1 365.3 375.2 415.2 4500-N-D ACID-FLD ALK-FLD DO-FLD PH-FLD SPCOND-FLD TEMP-FLD USGS-FLOW

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA 42SRBCWQ 42SRBCWQ 42SRBCWQ 42SRBCWQ 42SRBCWQ 42SRBCWQ 42SRBCWQ 42SRBCWQ

Procedure Source

Total Dissolved SolidsTotal Suspended SolidsTotal ResidueTurbidity by NephelometryMetals in Water by ICP-AESCalcium by EDTA Titrimetric AnalysisChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetrySulfate in Water by ColorimetryLow Level Total Organic Carbon in WaterTotal NitrogenAcidity, Field TritrationAlkalinity, Field TritrationDissolved Oxygen, Field MeterpH, FieldConductivity, Filed MeterTemerature, FieldStream Discharge Measurements

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Status42SRBCWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 268 of 515

Alaska Soil and Water Conservation District

120.1 150.1 170.1 180.1 200.8(W) 2320 2340 245.1 2510 353.2_M 365.2 9222-D CEMP1.0 D1498 D3858 D4409 D888(B) FIELDOBS

Procedure Id

USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA USEPA USEPA APHA ALASSWCD ASTM ASTM ASTM ASTM ALASSWCD

Procedure Source

ConductancepHTemperatureTurbidity by NephelometryMetals in Waters by ICP/MSAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAConductivity in WaterNitrate and Nitrite by ColorimetryPhosphorus by Single Reagent ColorimetryFecal Coliform Membrane Filter ProcedureColiscan EasygelOxidation-Reduction Potential for WaterOpen-Channel Flow Measurement by AreaOpen-Channel Flow by RECMDissolved Oxygen by Instrumental ProbeField Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusALASSWCD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 269 of 515

Alliance For A Living Ocean

BOTTOM-1 DEPTH-1 DO-1 PH-1 SALINITY-1 TEMP-1 TRANS-1

Procedure Id

ALO ALO ALO ALO ALO ALO ALO

Procedure Source

Bottom DepthWater DepthDissolved Oxygen in WaterPH in WaterSalinity in WaterField Determination of Water Temperature, ProbeTransparency

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

StatusALO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 270 of 515

Wampanoag Tribe of Gay Head (Aquinnah) - Massachusetts

8000 8043 8048 8190 8507 CHLORAPHYLL-A ENTEROCOCCUS

IDEXX NH3-N NITRATE-N ON SITE DATA LOSILICA TPH

Procedure Id

HACH HACH HACH HACH HACH AQUINNAH AQUINNAH

AQUINNAH AQUINNAH AQUINNAH AQUINNAH AQUINNAH AQUINNAH

Procedure Source

Chemical Oxygen DemandBiological Oxygen Demand in WaterReactive Phosphorus in WaterTotal Phosphorus in WaterNitrite in WaterChloraphyll-A, Pheophytin-a and Algae BiomassEnterococcus Bacteria for Marine and Fressh Water SwimmingBeachesTotal Coliform and E.coli BacteriaAmmonia NitrogenNitrate NitrogenYSI 6600Silica Heteropoly Blue MethodTPH Immunoassay Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

StatusAQUINNAH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 271 of 515

Arkansas Dept. of Environmental Quality

10200-G 200.7(W) 200.8(W) 2130 2320 2510 2540-C 2540-D 2550 300(A) 4500-CL(D) 4500-CN(C) 4500-CN(D) 4500-CN(E) 4500-H 4500-NH3(D) 4500-NH3(G) 4500-O-G 5210-B 5310-B 8270C(W) 9222-D

Procedure Id

APHA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA APHA

Procedure Source

Zooplankton Counting TechniquesMetals in Water by ICP-AESMetals in Waters by ICP/MSTurbidity in WaterAlkalinity in Water by TitrationConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyResidual Chlorine in Water by Titration- Amperometric MethodCyanide in Water after DistillationCyanide in Water by TitrationCyanide in Water by ColorimetrypH in WaterAmmonia in Water by Selective Electrode MethodAmmonia in Water Using Automated Phenate MethodTotal Dissolved Oxygen by Membrane Electrode Method5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodSemivolatile Organic Compounds by CGC/MSFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusARDEQH2O

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 272 of 515

City of Aurora (Colorado)

120.1 170.1 2130 2320 2340 2510 2540-C 2540-D 3113-B 4110-B 4500-H 4500-NH3(D) 4500-NO2(B) 4500-O-G 4500-P-E 5310-C 9222-D 9223-B YSI-DS

Procedure Id

USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA AURORA

Procedure Source

ConductanceTemperatureTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterMetals in Water by GFAAAnions in Water by Ion ChromatographypH in WaterAmmonia in Water by Selective Electrode MethodNitrite in Water by ColorimetryTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupDissolved Solids via YSI Sonde

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusAURORA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 273 of 515

American Water Company (Illinois)

150.1 180.1

Procedure Id

USEPA USEPA

Procedure Source

pHTurbidity by Nephelometry

Procedure Name

ActiveActive

StatusAWC_WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 274 of 515

Alaska Dept. of Environmental Conservation

170.1 2120-B 2130 2320 2510 2520-B 2520-C 2540-C 2540-D 2540-F 2550 2580 300(A) 365.2 415.1 4500-H 4500-NH3(D) 4500-NH3(F) 4500-NOR(B) 4500-O-C 4500-O-G 602 610 624 8156 9222-D 9223-B D5128 D888(B) FIELD I1250 I1586

Procedure Id

USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA HACH APHA APHA ASTM ASTM AWQDECJN USDOI/USGS USDOI/USGS

Procedure Source

TemperatureColor in Water by Visual ComparisonTurbidity in WaterAlkalinity in Water by TitrationConductivity in WaterSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSettleable Solids in WaterTemperature of Water by ThermometerOxidation-Reduction Potential of WaterInorganic Anions by Ion ChromatographyPhosphorus by Single Reagent ColorimetryTotal Organic Carbon by CombustionpH in WaterAmmonia in Water by Selective Electrode MethodAmmonia in Water Using Phenate MethodTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Membrane Electrode MethodPurgeable Aromatics in Wastewater by GCPolynuclear Aromatic Hydrocarbons by GCPurgeable Organics in WastewaterpH in WaterFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GrouppH of Water of Low ConductivityDissolved Oxygen by Instrumental ProbeField MeasurementsColor in Water by Visual ComparisonWater pH

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusAWQDECJN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 275 of 515

Bad River Tribe

1001 1002 1003

Procedure Id

BADRIVER BADRIVER BADRIVER

Procedure Source

Specific ConductivityTurbidityColiscan Easygel Method for Bacteria

Procedure Name

ActiveActiveActive

StatusBADRIVER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 276 of 515

Bear Creek Reservoir (Colorado)

120.1 150.1 160.2 200.7(W) 206.2 245.1 310.1 350.1 350.2(A) 353.2 365.1 365.A 405.1 4500-H 9221-E

CHLOR-A COND DOMETR FLOMTR FLOW NO3 PHMTR PHOSPART SECCHI TEMP 001

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA BEAR CRK USEPA APHA APHA

BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK BEAR CRK

Procedure Source

ConductancepHNon-Filterable Residue - TSSMetals in Water by ICP-AESArsenic by GFAAMercury in Water by CVAAAlkalinity by TitrationAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISENitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus, total by Auto Ascorbic Acid (digest)5 Day Biochemical Oxygen DemandpH in WaterEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueChlorophyll-aSpecific ConductanceOxygen, gaseousDischarge VelocityInstantaneous flowNitrate as NitrogenpHPhosphorus, total particulateSecchiField Determination of Water Temperature, Probe

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusBEAR_CRK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 277 of 515

Big Lagoon Rancheria (California)

QAPP

Procedure Id

BIGLAG

Procedure Source

Quality Assurance Procedures and Policy

Procedure Name

Active

StatusBIGLAG

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 278 of 515

Region 8 Superfund: Black Foot Post and Pole

ILM05 ILM05.3 OLC03 OLM04

Procedure Id

BLCKFOOT BLCKFOOT BLCKFOOT BLCKFOOT

Procedure Source

ILM05ILM05.3OLC03OLM04

Procedure Name

ActiveActiveActiveActive

StatusBLCKFOOT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 279 of 515

Bay Mills Indian Community

351.2 353.2 365.2 COLILERT-18

Procedure Id

USEPA USEPA USEPA IDEXX

Procedure Source

Total Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coli

Procedure Name

ActiveActiveActiveActive

StatusBMIC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 280 of 515

Superfund Bountiful UT

160.1 300(A) 310.1 353.2 415.1 6010B 8021 OLC03 OLM04.2 TO-15 UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA HACH BOUNTIFL BOUNTIFL BOUNTIFL BOUNTIFL

Procedure Source

Filterable Residue - TDSInorganic Anions by Ion ChromatographyAlkalinity by TitrationNitrate-Nitrite Nitrogen by ColorimetryTotal Organic Carbon by CombustionInductively Coupled Plasma AESFree Chlorine in Water by DPDOLC03CLP Organic Low/Medium Concentration Waters and SoilsTO-15Unknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusBOUNTIFL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 281 of 515

City of Brighton (Colorado)

150.1 180.1 2340 2540-D 2550 3500-CU(B) 360.1 415.1 4500-NO3(F) 5210-B 8038 8221 9221-E

FLOW

Procedure Id

USEPA USEPA APHA APHA APHA APHA USEPA USEPA APHA APHA HACH HACH APHA

BRIGHTON

Procedure Source

pHTurbidity by NephelometryHardness in Water by EDTA TitrationTotal Suspended Solids in WaterTemperature of Water by ThermometerCopper in Water by FLAA or GFAADissolved Oxygen Using an ISETotal Organic Carbon by CombustionNitrate in Water- Automated Cadmium Reduction5-Day Biochemical Oxygen DemandAmmonia Nitrogen in WaterAlkalinity by Buret TitrationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFlow

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

StatusBRIGHTON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 282 of 515

Bunker Hill Mining and Metallurgical Complex

150.1 150.2 160.2 200.7(S) 200.7(W) 200.8(W) 245.1_M 245.5 ABA ALK-USGS AVS/SEM BP-USGS D422 DO-001 DO-USGS FC-USGS FLOW-001 FLOW-AVG FLOW-MAX FLOW-USGS I1229 I1630 I1900 I2063 I2138 I2274 I2403 I2477 I2503 I2525 I2542 I2545 I2546

I2587 I2606 I2607 I2610

I2667

I2668 I2724 I2781

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA BUNKER BUNKER BUNKER BUNKER ASTM BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER

BUNKER BUNKER BUNKER BUNKER

BUNKER

BUNKER BUNKER BUNKER

Procedure Source

pHpH by Continuous MonitoringNon-Filterable Residue - TSSMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSMercury in Water by Manual CVAAMercury in Sediment by CVAAAcid-Base AccountingAlkalinity and Associated Measurements, USGS Field MethodAcid Volatile Sulfides / Simult. Extractable MetalsBarometric Pressure, USGS Field MethodParticle-Size Analysis of SoilsField Determination of Dissolved OxygenDissolved Oxygen,USGS Field MethodFecal Coliform, USGS Field MethodField Determination of FlowField Determination of Average FlowField Determination of Maximum FlowField Determination of Flow by USGSUSGS Method I-1229-87 Chromium in filtered water, by DCP-AESUSGS Method I-1630-85 Potassium in filtered water by direct AASUSGS Method I-1900-85 Zinc in filtered water by direct AASUSGS Method I-2063-98 Arsenic in Filtered Water by GFAASUSGS Method I-2138-89 Cadmium in filtered water, by GF-AASUSGS Method I-2274-89 Copper in filtered water, by GF-AASUSGS Method I-2403-89 Lead in filtered water, by GF-AASUSGS Method I-2477-92 Metals in Filtered Water by ICP-MSUSGS Method I-2503-89 Nickel in filtered water, by GF-AASUSGS Method I-2525-89 Ammonia in low ionic strength waterUSGS Method I-2542-89 Nitrite in low ionic strength waterUSGS Method I-2545-90 Nitrite plus nitrate in filtered waterUSGS Method I-2546-91 Nitrite plus nitrate in low ionic strengthwaterUSGS Method I-2587-85 pH, lab, by automated glass electrodeUSGS Method I-2606-89 Orthophosphate in low ionic-strength waterUSGS Method I-2607-90 Phosphorus in low ionic-strength waterUSGS Method I-2610-91 Total Phosphorus in Filtered Water byKjeldahl DigestionUSGS Method I-2667-85 Selenium in filtered water by automatedhydride generation and AASUSGS Method I-2668-98 Selenium in Filtered Water by GFAASUSGS Method I-2724-89 Silver in filtered water, by GF-AASUSGS Method I-2781-85 Specific conductance, lab, automated, byWheatstone bridge

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

Active

ActiveActiveActive

StatusBUNKER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 283 of 515

Bunker Hill Mining and Metallurgical Complex

I3492

I3630

I3735

I3800

I3900

I4063

I4138 I4243

I4403

I4471

I4503

I4515

I4600

I4607

I4610

I4668

I4724

I8000 IN-CLP IN-CLP-LOW LIM-USGS O1100 OBS-USGS PH-001 PH-USGS PURGERT REDOX-001 SAL-001 SC-001 SC-USGS SOL-USGS

Procedure Id

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER

BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER

Procedure Source

USGS Method I-3492-96 Molybdenum Recoverable from UnfilteredWater by GFAASUSGS Method I-3630-85 Potassium recoverable from unfilteredwater by dilute HCl digestion and direct AASUSGS Method I-3735-85 Sodium recoverable from unfiltered waterby dilute HCl digestion and direct AASUSGS Method I-3800-85 Strontium recoverable from unfilteredwater by dilute HCl digestion and direct AASUSGS Method I-3900-85 Zinc recoverable from unfiltered water bydilute HCl digestion and direct AASUSGS Method I-4063-98 Arsenic Recoverable from Unfiltered Waterby GFAASUSGS Method I-4138-89 Cadmium in unfiltered water, by GF-AASUSGS Method I-4243-89 Cobalt recoverable from unfiltered water,by GF-AASUSGS Method I-4403-89 Lead recoverable from unfiltered water, byGF-AASUSGS Method I-4471-97 Metals Recoverable from Unfiltered WaterICP-OES or ICP-MSUSGS Method I-4503-89 Nickel recoverable from unfiltered water,by GF-AASUSGS Method I-4515-91 Kjeldahl nitrogen in unfiltered water bymercury(II)-catalyzed digestion and colorimetric analysisUSGS Method I-4600-85 Phosphorus in unfiltered water by ASFphosphomolybdate formation and colorimetryUSGS Method I-4607-90 Total Phosphorus in water, byphosphomolybdate colorimetry and automated-segmented flowanalyzerUSGS Method I-4610-91 Total Phosphorus in Unfiltered Water byKjeldahl DigestionUSGS Method I-4668-98 Selenium Recoverable from UnfilteredWater by GFAASUSGS Method I-4724-89 Silver, recoverable from unfiltered water,by GF-AASUSGS Forty Element ICP-AESMetals by CLPMetals by CLP Low Conc.Limnology, USGS Field MethodUSGS Method O-1100-83 Carbon, organic, dissolved, wet oxidationDirect Observation by USGSField Determination of pHpH, USGS Field MethodPurge Rate DeterminationField Determination of Oxygen Reduction PotentialField Determination of SalinityField Determination of Specific ConductivitySpecific Conductance, USGS Field MethodSolar Measurements, USGS Field Method

Procedure Name

Active

Active

Active

Active

Active

Active

ActiveActive

Active

Active

Active

Active

Active

Active

Active

Active

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusBUNKER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 284 of 515

Bunker Hill Mining and Metallurgical Complex

SULFUR TEMP-001 TEMP-USGS TRB-001 UNK-CH2M USGS_HIST

USGS_UNKN

Procedure Id

BUNKER BUNKER BUNKER BUNKER BUNKER BUNKER

BUNKER

Procedure Source

Speciated SulfurField Determination of Water Temperature, ProbeTemperature, USGS Field MethodField Determination of TurbidityUnknown Method for CH2M Hill DataHistorical Profile of Quality of Water Laboratories and Activities,1879-1973Unspecified USGS Laboratory Method

Procedure Name

ActiveActiveActiveActiveActiveActive

Active

StatusBUNKER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 285 of 515

California State Water Resources Control Board

1600

9221-B

9221-E

9222-B 9222-D 9230-B

9230-C COLILERT COLILERT-18 COLILERT-182000COLILERT/2000 ENTEROLERT ENTEROLERT2000

Procedure Id

USEPA

APHA

APHA

APHA APHA APHA

APHA IDEXX IDEXX IDEXX IDEXX IDEXX IDEXX

Procedure Source

Enterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Standard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueFecal Streptococcus and Enterococcus, Membrane Filter TechniqueColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliColilert-18 Quanti-Tray/2000; MPN - Multi Tube, Multi Well for E.coliColilert Quanti-Tray/2000; MPN - Multi Tube, Multi Well for E.coliEnterolert Quanti-Tray; Multi Tube, Multi Well, for EnterococciiEnterolert Quanti-Tray/2000; Multi Tube, Multi Well, for Enterococcii

Procedure Name

Active

Active

Active

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

StatusCABEACH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 286 of 515

California Department of Pesticide Regulation Surface Water

DPR-001

Procedure Id

CADPR

Procedure Source

dpr pesticide methods

Procedure Name

Active

StatusCADPR

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Page 287 of 515

California Department of Water Resources

10200-H 120.1 150.1 160.1 160.2 160.4 170.1 180.1 200.7(W) 213.2 2130 218.2 220.2 236.2 239.2 243.2 245.1 2510 2540-C 289.2 300(A) 3111-B 3111-C 3114-C 325.2 350.1 350.2(A) 350.2(C) 3500-AS(C) 351.2 351.3(A) 351.3(B) 353.2 353.2 DWR MOD 353.2_M 360.1 360.2 365.1 365.1 DWR MOD 365.4 405.1 4500-CL(B) 4500-H 4500-NO3(F)

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA CADWR USEPA USEPA USEPA USEPA CADWR USEPA USEPA APHA APHA APHA

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryMetals in Water by ICP-AESCadmium by GFAATurbidity in WaterChromium by GFAACopper by GFAAIron by GFAALead by GFAAManganese by GFAAMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterZinc by GFAAInorganic Anions by Ion ChromatographyMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Extraction/Air-Acetylene FlameMetals in Water by Continuous HYDAAChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen by TitrationArsenic in Water by SpectrophotometryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationNitrate-Nitrite Nitrogen by ColorimetryDWR modification of EPA 353.2Nitrate and Nitrite by ColorimetryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryDWR Modification of EPA 365.1Total Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandResidual Chlorine in Water by Titration- Iodometric Method IpH in WaterNitrate in Water- Automated Cadmium Reduction

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCADWR

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California Department of Water Resources

4500-O-G 4500-P-D 4500-P-F

4500-SI(D) 5210-B 608 CADWR-001 CADWR-002 CADWR-003 CADWR-004 CADWR-005 CADWR-006 CADWR-007 CADWR-008 I1700

Procedure Id

APHA APHA APHA

APHA APHA USEPA CADWR CADWR CADWR CADWR CADWR CADWR CADWR CADWR USDOI/USGS

Procedure Source

Total Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Stannous Chloride TitrationPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSilica in Water by Spectrophotometry- Molybdosilicate Method5-Day Biochemical Oxygen DemandOrganochlorine Pesticides and PCBs by GCMethod for Tide Stage Code1% Light depthDepth of WaterFluorescenceMethod for Stream StageSecchi disk depthTideMethod for Field IdentificationSilica in Water by Colorimetry

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCADWR

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and Equipment Summary

Page 289 of 515

Fresno River Water Quality Monitoring

150.1 180.1 2520-B 300(A) 4500-H 4500-NH3(C) 4500-NO3(C) 4500-O-G 4500-P-E 8075 9222-B 9223-B YSI85

Procedure Id

USEPA USEPA APHA USEPA APHA APHA APHA APHA APHA CAFRESNO APHA APHA CAFRESNO

Procedure Source

pHTurbidity by NephelometrySalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographypH in WaterAmmonia in Water by Titrimetric MethodNitrate in Water by Ion ChromatographyTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodHach Total Kjeldahl NitrogenStandard Total Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupYSI85 Temperature Probe

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCAFRESNO

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Page 290 of 515

CA Surface Water Monitoring Program (California)

10200H-2A 10200H-2B 160.2 1631B 1631EM

1638M 200.7 200.8(D) 2320-B 2340-C 2540-B 2540-C 2540-D 300(A) 300_M 314 340.2 350.3 351.2 351.3(C) 353.3 365.3 415.1 445.0M 4500-B-B 4500-F-C 4500-NH3(H) 4500-NO2(B) 4500-P-E 604M 619M 7742M 8015M 8081AM 8082M 8141AM 8260 8270B(W) 8270M 8310 8310M 8507 9060

Procedure Id

CALSWAMP CALSWAMP USEPA CALSWAMP CALSWAMP

CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CALSWAMP APHA APHA APHA APHA APHA CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP USEPA CALSWAMP USEPA CALSWAMP HACH USEPA

Procedure Source

Spectrophotometric determination of Pheophytin aSpectrophotometric determination of Chlorophyll aNon-Filterable Residue - TSSMercury in Water by Oxidation, Purge and Trap, and CVAFSModified Mercury in Water by Oxidation, Purge and Trap, andCVAFSModified Trace Elements in Water by ICP/MSMetals in Water and Sediment by ICP-AESMetals in Waters and Sediment by ICP/MSAlkalinity in Water by TitrationHardness in Water by EDTA TitrationTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterInorganic Anions by Ion ChromatographyDetermination of Anions by ICPerchlorate in Drinking Water using Ion ChromatographyFluoride in Water Using an ISEAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen - PotentiometricNitrate-Nitrite Nitrogen by Cd ReductionPhosphorus by Two Reagent ColorimetryTotal Organic Carbon by CombustionModified In-Vitro Determination of ChlorophyllBoron in Water by Spectrophotometry- Curcumin MethodFluoride in Water Using an ISEAmmonia in Water - Flow Injection AnalysisNitrite in Water by ColorimetryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodModified Phenols in Wasterwater by GC/FID or GC/ECDModified Triazine Pesticides in WastewaterModified Selenium by Gaseous Borohydride AAModification of Non-Halogenated Volatile OrganicsModification of Organochlorine Pesticieds and PCB's by GCModification of PCB's as Aroclors by Capillary Column GCModified Organophosphorus CompoundsVolatile Organics by GC/MSSemivolatile Organics in Water by GC/MSModification of Semivolitale Organics in Water by GC/MSPolynuclear Aromatic HydrocarbonsModifcation of Polynuclear Aromatic HydrocarbonsNitrite in WaterTotal Organic Carbon in Water and Waste

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCALSWAMP

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and Equipment Summary

Page 291 of 515

CA Surface Water Monitoring Program (California)

D3977 D422 DFG_SOP_103 ELISA_SOP_3.3 FIELDOBS NONE PCB-NEWMAN PROBE QC_10107041B QC_10107062E QC_10115011D QC_10115011M QC_10303311A

Procedure Id

ASTM ASTM CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP CALSWAMP

Procedure Source

Suspended-Sediment in WaterParticle-Size Analysis of SoilsDepartment of Fish & Game Metals and Trace ElementsDepartment of Fish & Game Pesticides MethodField ObservationsNonePCB Methods Referenced by Newman et alProbeQC Method for Nitrate and Nitrite AnionsQC Method for Total Kjeldahl NitrogenQC Nutrients Method for PhosphorusQC Nutrients Method for Ortho-phosphate as PMiscellaneous Lab Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCALSWAMP

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Page 292 of 515

City of Cape Coral (Florida)

10200-H 130.2 150.1 160.1 160.2 160.4 170.1 180.1 200.7(S) 200.7(W) 202.1 206.3 213.1 2130 218.1 220.1 2320 236.1 239.1 245.1 245.2 245.5 249.1 2510 2510 2520-B 2540-C 2540-D 2540-E 2580 289.1 300(A) 300_M 310.1 3111-E 3112-B 350.2(C) 351.3(A) 353.1 365.2 405.1 413.1 445 4500-H

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA NIOSH APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

Procedure Source

Chlorophyll a-b-c DeterminationTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESAluminum by FLAAArsenic by HYDAACadmium by FLAATurbidity in WaterChromium by FLAACopper by FLAAAlkalinity in Water by TitrationIron by FLAALead by FLAAMercury in Water by CVAAMercury by CVAAMercury in Sediment by CVAANickel by FLAA1-Octanethiol by GC/FPDConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterOxidation-Reduction Potential of WaterZinc by FLAAInorganic Anions by Ion ChromatographyDetermination of Anions by ICAlkalinity by TitrationMetals in Water by FLAA- Extraction/Nitrous Oxide-Acetylene FlameMercury in Water by CVAAAmmonia Nitrogen by TitrationTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent Colorimetry5 Day Biochemical Oxygen DemandTotal Recoverable Oil and GreaseIn-Vitro Determination of ChlorophyllpH in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCAPECRD

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Page 293 of 515

City of Cape Coral (Florida)

4500-NH3(E) 4500-NO2(B) 4500-NO3(E) 4500-NOR(B) 4500-P-E 5210-B 6010A 7020 7020 7060A 7061A 7130 7131A 7190 7191 7210 7211 7380 7381 7420 7421 7470A 7471A 7520 7950 7951 8156 9222-D 9230-B

D1125(A) D1125(B) D1293(A) D1293(B) D1889 D5089 D888(B) DEPTH HM-PONAR NO3N NOXN OPO4 ORGN ORGP

Procedure Id

APHA APHA APHA APHA APHA APHA USEPA NIOSH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA HACH APHA APHA

ASTM ASTM ASTM ASTM ASTM ASTM ASTM CAPECRD CAPECRD CAPECRD CAPECRD CAPECRD CAPECRD CAPECRD

Procedure Source

Ammonia in Water by Selective Electrode Method (Known Addition)Nitrite in Water by ColorimetryNitrate in Water- Cadmium ReductionTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid Method5-Day Biochemical Oxygen DemandICP SpectroscopyCalcium by Atomic AbsorptionAluminum by FLAAArsenic by GFAAArsenic by Gaseous Hydride AACadmium by FLAACadmium by GFAAChromium by FLAAChromium by GFAACopper by FLAACopper by GFAAIron by FLAAIron by GFAALead by FLAALead by GFAAMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteNickel by FLAAZinc by FLAAZinc by GFAApH in WaterFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueConductivity and Resistivity in WaterConductivity and Resistivity in WaterpH of Water By Precise Lab MeasurementpH of Water By Routine MeasurementTurbidity of WaterVelocity of Water,electromagnetic metersDissolved Oxygen by Instrumental ProbeDepthBenthic Dredge sediment sampleNO3 Nitrogen (Calculated NOXN-NO2N)Nitrogen, NOx calculatedPhosphorus, OrthophosphateOrganic Nitrogen (Calculated TKN-NH3N)Organic Phosphorous (Calculated Total PO4-Ortho PO4)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCAPECRD

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Page 294 of 515

City of Cape Coral (Florida)

SECCHI DISK TOT N

Procedure Id

CAPECRD CAPECRD

Procedure Source

Secchi Disk DepthTotal Nitrogen (NOx+TKN)

Procedure Name

ActiveActive

StatusCAPECRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 295 of 515

Central Coast Ambient Monitoring Program (California)

10200-H 160.1_M 160.2_M 353.2_M 365_M 9221-B

9221-C

9221-D 9221-E

CCAMP02 CCAMP_AP001

Procedure Id

APHA USEPA USEPA USEPA USEPA APHA

APHA

APHA APHA

CCAMP CCAMP

Procedure Source

Chlorophyll a-b-c DeterminationTotal Dissolved SolidsTotal Suspended SolidsNitrate and Nitrite by ColorimetryPhosphorus in Water by ColorimetryStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueField Sampling Procedure?Water Quality Multi-probe

Procedure Name

ActiveActiveActiveActiveActiveActive

Active

ActiveActive

ActiveActive

StatusCCAMP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 296 of 515

Century Reality/Schreuder, Inc.

00-02 120.1 150.1 160.1 2510B 300(A) 350.1 351.2 353.2 900 9040A C-017-1 DS FL-PRO FT_1100 FT_1200 FT_1400 TN

Procedure Id

USEPA USEPA USEPA USEPA CENTREAL USEPA USEPA USEPA USEPA USEPA USEPA USEPA CENTREAL CENTREAL CENTREAL CENTREAL CENTREAL CENTREAL

Procedure Source

Gross Alpha Activity in Drinking Water by CoprecipitationConductancepHFilterable Residue - TDSSpecific ConductanceInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryGross Alpha and Beta Activity in WaterpH in Water by Electrometric MeasurementWater Level Measurement in WellsDissolved Solids - Field measurementHydrocarbons, Petroleum (Unspecified Mix)Field Measurement of Hydrogen Ion Activity (pH)Field Measurement of Specific ConductanceField Measurement of TemperatureTotal Nitrogen - Calculated

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCENTREAL

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and Equipment Summary

Page 297 of 515

U.S. Army Corps of Engineers Walla Walla District

10200-H 160.2 2130 2320 2340 2540-C 2540-D 2810 300(A) 310.1 3111-B 365.3 4500-CL(B) 4500-H 4500-NH3(G) 4500-NO2(C) 4500-NO3(G) 4500-NOR(B) 4500-P-C

4500-P-F

4500-SI(F) 4500-SO4(F) 5210-B D1293(B) D1889 D3858 D3977

Procedure Id

APHA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA USEPA APHA APHA APHA APHA APHA APHA APHA

APHA

APHA APHA APHA ASTM ASTM ASTM ASTM

Procedure Source

Chlorophyll a-b-c DeterminationNon-Filterable Residue - TSSTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationTotal Dissolved Solids in WaterTotal Suspended Solids in WaterDissolved Gas SupersaturationInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlamePhosphorus by Two Reagent ColorimetryResidual Chlorine in Water by Titration- Iodometric Method IpH in WaterAmmonia in Water Using Automated Phenate MethodNitrite in Water by Ion ChromatographyNitrate in Water- Titanous Chloride ReductionTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetryPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSilica in Water by Automated ColorimetrySulfate in Water by Colorimetry5-Day Biochemical Oxygen DemandpH of Water By Routine MeasurementTurbidity of WaterOpen-Channel Flow Measurement by AreaSuspended-Sediment in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActive

StatusCENWWEDH

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Page 298 of 515

Chatfield Reservoir (Colorado)

120.1 150.1 160.2 200.7 (W) 200.8(W) 350.1 3500 CR-D 353.2 365.1 405.1 9221-E

ASA NO.9 29 CHATFLD CHLOROPHYLL A COND D422 FIELD FLOW HACH 8039 HACH 8048 HORRIBU HORRIBU U-10 M365.1 M6010B ICP M7471 CVAA M7742 NO(3NO2)-N02 NO3(N) PERSULFT DIGESTPH SM22340B SM3500-SE TEMP TOTALK 200.7(W) 206.2 245.1 310.1

Procedure Id

USEPA USEPA USEPA CHATFLD USEPA USEPA CHATFLD USEPA USEPA USEPA APHA

CHATFLD CHATFLD CHATFLD CHATFLD ASTM CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD CHATFLD USEPA USEPA USEPA USEPA

Procedure Source

ConductancepHNon-Filterable Residue - TSSMetals in WaterMetals in Waters by ICP/MSAmmonia Nitrogen by ColorimetryHexavalent ChromiumNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry5 Day Biochemical Oxygen DemandEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueCarbon, Total organic (TOC)Cyanide (SM4500-CN)Chlorophyll aSpecific ConductanceParticle-Size Analysis of SoilsUnknownFlow, instantaneousField Nitrate Nitrogen MeasurementPhosphorusSpecific Conductance Field MeterDissolved OxygenPhosphorus, total by Auto Ascorbic Acid (digest)Metals in SoilMercury in SoilModified, AA-H Total Selenium in SoilNitrate as N, dissolvedNitrate as N, dissolvedTotal NitrogenpHHardnessSelenium, dissolvedTemperatureAlkalinity, TotalMetals in Water by ICP-AESArsenic by GFAAMercury in Water by CVAAAlkalinity by Titration

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveSuspSuspSuspSusp

StatusCHATFLD

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Page 299 of 515

Cherokee Nation (Oklahoma)

CN_QAPP

Procedure Id

CHEROKEE

Procedure Source

Cherokee Nation Quality Assurance Project Plan

Procedure Name

Active

StatusCHEROKEE

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and Equipment Summary

Page 300 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 120.1 150.1 160.2 1600

170.1 180.1 2120-B 2520-B 350.1 351.2 353.2 354.1 360.1 365.1 415.1 4500-SI(F) 5210-B 5310-B 9222-D NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA

USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA CHNEPCHB CHNEPCHB

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)TemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionSilica in Water by Automated Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodFecal Coliform Membrane Filter ProcedureTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPCHB

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and Equipment Summary

Page 301 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 2120-B 2520-B 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.4 415.1 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHENPCHE CHNEPCHE

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionICP SpectroscopyTotal NitrogenLight

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPCHE

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Page 302 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 200.7(W) 2120-B 2520-B 2520-C 2540-G 2550 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.3 365.4 370.1 415.1 4500-H 4500-O-G 5310-B 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA CHNEPCHP CHNEPCHP

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodTotal, Fixed and Volatile SolidsTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetryTotal Organic Carbon by CombustionpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodTotal Organic Carbon by Combustion-Infrared MethodICP SpectroscopyTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPCHP

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and Equipment Summary

Page 303 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 2120-B 2520-B 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.4 415.1 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHNEPCHW CHNEPCHW

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionICP SpectroscopyTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPCHW

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Page 304 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 120.1 150.1 160.2 1600

170.1 180.1 2120-B 2520-B 350.1 351.2 353.2 354.1 360.1 365.1 415.1 4500-SI(F) 5210-B 5310-B 9222-D NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA

USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA CHNEPEB CHNEPEB

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)TemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionSilica in Water by Automated Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodFecal Coliform Membrane Filter ProcedureTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPEB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 305 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 2120-B 2520-B 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.4 415.1 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHNEPLLB CHNEPLLB

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionICP SpectroscopyTotal NitrogenLight

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPLLB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 306 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 2120-B 2130 2540-C 2540-D 4500-H 4500-NH3(G) 4500-NO3(B) 4500-NOR(B) 4500-P-E 5310-B 5310-C 5310-D 9222-D PAR

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA CHNEPMP

Procedure Source

Chlorophyll a-b-c DeterminationColor in Water by Visual ComparisonTurbidity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterpH in WaterAmmonia in Water Using Automated Phenate MethodNitrate in Water by Ultraviolet SpectrophotometryTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodTotal Organic Carbon in Water- Wet-Oxidation MethodFecal Coliform Membrane Filter ProcedurePar

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPMP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 307 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 120.1 150.1 160.2 1600

170.1 180.1 2120-B 2520-B 350.1 351.2 353.2 354.1 360.1 365.1 415.1 4500-SI(F) 5210-B 5310-B 9222-D NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA

USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA CHNEPPIS CHNEPPIS

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)TemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionSilica in Water by Automated Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodFecal Coliform Membrane Filter ProcedureTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPPIS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 308 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 150.1 160.2 180.1 300(A) 350.1 351.2 353.1 354.1 365.4 415.1 NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHNEPSCB CHNEPSCB

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltpHNon-Filterable Residue - TSSTurbidity by NephelometryInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionTotal nitrogenLight

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPSCB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 309 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 120.1 150.1 160.2 1600

170.1 180.1 2120-B 2520-B 350.1 351.2 353.2 354.1 360.1 365.1 415.1 4500-SI(F) 5210-B 5310-B 9222-D NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA

USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA CHNEPTCR CHNEPTCR

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)TemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Organic Carbon by CombustionSilica in Water by Automated Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodFecal Coliform Membrane Filter ProcedureTotal NitrogenPAR

Procedure Name

ActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPTCR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 310 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 2120-B 2520-B 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.4 415.1 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHNEPTMR CHNEPTMR

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionICP SpectroscopyTotal NitrogenLight

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPTMR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 311 of 515

Charlotte Harbor National Estuaries Program (Florida)

10200-H 110.2 120.1 150.1 160.2 170.1 180.1 2120-B 2520-B 300(A) 350.1 350.3 351.2 353.1 353.2 354.1 360.1 365.2 365.4 415.1 6010A NTOT PAR

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CHNEPTPR CHNEPTPR

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltConductancepHNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryColor in Water by Visual ComparisonSalinity in Water- Electrical Conductivity MethodInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionICP SpectroscopyTotal NitrogenLight

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCHNEPTPR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 312 of 515

Cook Inlet Keeper (Alaska)

10200-H 120.1 150.1 160.5 170.1 180.1 200.7(W) 200.9 2130 2510 2520-B 2580 360.1 360.2 4500-H 4500-NO3(E) 4500-O-C 4500-O-G 4500-P-E 8021A(ELCD) 8021A(PID) 8038 8048 9222-D AK101 AK102 AK103 CIK-001 CIK-002 CIK-003 CIK-004 CIK-005 CIK-006 CIK-007 CIK-008 CIK-009 CIK-010 CIK-011

CIK-012 CIK-013

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA USEPA USEPA HACH HACH APHA CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK CIKEEPAK

CIKEEPAK CIKEEPAK

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHSettleable MatterTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals by Temperature Stabilized GFAATurbidity in WaterConductivity in WaterSalinity in Water- Electrical Conductivity MethodOxidation-Reduction Potential of WaterDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquepH in WaterNitrate in Water- Cadmium ReductionTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodHalogenated and Aromatic VolatilesHalo and Aromatic Volatiles - CGC/PIDAmmonia Nitrogen in WaterReactive Phosphorus in WaterFecal Coliform Membrane Filter ProcedureGasoline Range Organics (GRO) - by GCFID: 25-1,000,000,000Diesel Range Organics (DRO) - by GCFID: 50-1,000,000Residual Range Organics (RRO) by GCFID: 500-1,000,000Hanna Water Test MeterTurbidity-Secchi Disk Depth (LaMotte 0171)Coliscan for ColiformApparent Color - Boger Color System (LaMotte)Nitrogen-Nitrate - Cadmium Reduction (Chemetrics 6902)Apparent Color - Platinum-Cobalt (Hach 8025)Nitrogen-Nitrate - Cadmium Reduction (Hach 8192)Nitrogen-Nitrate Zinc Reduction (LaMotte 3354)Orthophosphate - Ascorbic Acid (LaMotte 3121)pH Octet Comparator (LaMotte 5858)Tot Phosphorus in Water - Tot Acid Persulfate Digestion (Hach8190)Salinity - Hydrometer (LaMotte 3-00011)Suspended Solids - Photometric (Hach 8006)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

StatusCIKEEPAK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 313 of 515

City of Fort Collins (Colorado)

120.1 130.1 150.1 1631 170.1 200.7(W) 212.3 272.2 350.1 351.2 353.2 405.1

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

ConductanceTotal HardnesspHMercury in Water by Oxidation, Purge and Trap, and CVAFSTemperatureMetals in Water by ICP-AESBoron by Colorimetric AnalysisSilver by GFAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Colorimetry5 Day Biochemical Oxygen Demand

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCITYFTCO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 314 of 515

City of Punta Gorda (Florida)

110.2 160.2 180.1 2120-C 2130 2320 2340 2510 2520-B 2520-C 2540-C 2550 300.0 350.2 3500-FE(D) 351.2 353+351 353.2 365.3 365.5 370.1 445 445.0 4500-CL(B) 4500-H 4500-O-G 4500-SO4(E) 5310-B LICOR

Procedure Id

USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA CITYOFPG CITYOFPG APHA USEPA CITYOFPG USEPA USEPA USEPA USEPA USEPA CITYOFPG APHA APHA APHA APHA APHA CITYOFPG

Procedure Source

Color Analysis Using Platinum/CobaltNon-Filterable Residue - TSSTurbidity by NephelometryColor in Water by SpectrophotometryTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodTotal Dissolved Solids in WaterTemperature of Water by ThermometerChlorideAmmonia NitrogenIron in Water by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal NitrogenNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Two Reagent ColorimetryOrthophosphate in Water by ColorimetryDissolved Silica by ColorimetryIn-Vitro Determination of ChlorophyllPheophytinResidual Chlorine in Water by Titration- Iodometric Method IpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodSulfate by Turbidimetric AnalysisTotal Organic Carbon by Combustion-Infrared MethodLicor

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCITYOFPG

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 315 of 515

Des Moines River - Corp of Engineers (IOWA)

APHA 10200 H APHA 2130 B APHA 2320 B APHA 2340 C APHA 2540 D APHA 2550 APHA 3111 B APHA 3500-CA B APHA 4110 B

APHA 4500-CO2 CAPHA 4500-H B APHA 4500-NH3 GAPHA 4500-NO3 FAPHA 4500-O C APHA 4500-P F APHA 4500-SIO2EAPHA 5210 B APHA 5310 C APHA 9222 D APHA 9222 G IONPAC USEPA 245.1 USEPA 351.2 USEPA 365.4 USGS CA8

Procedure Id

COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU

COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU COE/ISU

Procedure Source

Chlorophyll a-b-c- DeterminationTurbidity - Nephelometric MethodAlkalinity - Titration MethodHardness - EDTA Titrimetric MethodTotal Suspended Solids Dried at 103-105Temperature of Water by ThermometerMetals by FLAA - Direct Air-Acetylene Flame MethodCalcium - EDTA Titrimetric MethodDetermination of Anioins by Ion Chromatography with ChemicalSuppression of Eluent ConductivityCarbon Dioxide - Titrimetric Method for Free Carbon DioxidepH Value - Electrometric MethodNitrogen (Ammonia) - Automated Phenate MethodNitrogen (Nitrate) - Automated Cadmium Reduction MethodOxygen (dissolved) - Azide ModificationPhosporous - Automated Ascorbic Acid Reduction MethodSilica - Automated Method for Molybdate-Reactive SilicaBiochemical Oxygen Demand - 5-Day BOD TestTOC - Persulfate-Ultraviolet or Heated-Persulfate Oxidation MethodFecal Coliform Membrane Filter ProcedureMembrane filter technique - MF Partition ProceduresIon chromatograhpy with IONPACMercury in Water by CVAATotal Kjeldahl Nitrogen by ColorimetryTotal Phosphorus After Block DigestionUSGS Flow Measurement

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCOE/ISU

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 316 of 515

The Rivers of Colorado Water Watch Network (RiverWatch)

1 150.1 160.2 2 200 200.11 200.7(W) 2340 2540-B 3 300(A) 310.1 325.1 350.1 350.3 353.2 365.1 365.3 365.4 375.1 375.4 4 5 8156 8157 9253 UNKNOWN

Procedure Id

CORIVWCH USEPA USEPA CORIVWCH USEPA USEPA USEPA APHA APHA CORIVWCH USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA CORIVWCH CORIVWCH HACH HACH USEPA CORIVWCH

Procedure Source

Tempurature by ThermometerpHNon-Filterable Residue - TSSPhysical HabitatMetals by Atomic AbsorptionMetals in Fish Tissue by ICP-AESMetals in Water by ICP-AESHardness in Water by EDTA TitrationTotal Solids Dried 103-105C in WaterMacroinvertebrateInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISENitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate by Colorimetry With ChloranilateSulfate by Turbidimetric DeterminationDissolved Oxygen - DOFLOWpH in WaterDissolved Oxygen in WaterChloride in Water and Waste by TitrationUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusCORIVWCH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 317 of 515

Confed Tribes of Coos, Lower Umpqua & Siuslaw Indians (OR)

150.2 170.1 180.1 2520-D 360.1 9040A 973.4

Procedure Id

USEPA USEPA USEPA APHA USEPA USEPA AOAC

Procedure Source

pH by Continuous MonitoringTemperatureTurbidity by NephelometrySalinity in Water- Algorithm of Practical SalinityDissolved Oxygen Using an ISEpH in Water by Electrometric MeasurementSpecific Conductance of Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

StatusCTCLUSI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 318 of 515

Connecticut Dept. of Environmental Protection

ASTM D6503 COLILERT

Procedure Id

CT_DEP01 CT_DEP01

Procedure Source

Standard Test Method for Enterococci in water using Enterolert (tm)multiple well most probable number test e coli and total coliform

Procedure Name

ActiveActive

StatusCT_DEP01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 319 of 515

Coyote Valley Tribal Council (California)

QAPP

Procedure Id

CVTEPA

Procedure Source

Quality Assurance Procedures Policy

Procedure Name

Active

StatusCVTEPA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 320 of 515

Centennial Water and Sanitation District

200.7(W) 200.8(W) 200.9 2130 2320 2340 245.1_M 2510 2520-B 2540-B 2540-C 2540-D 2550 300_M 3113-B 340.2 3500-CA(D) 351.2 353.2 415.1 4500-H 4500-NH3(D) 4500-NH3(F) 4500-NH3(G) 4500-NO2(B) 4500-NO3(F) 4500-O-C 4500-O-G 4500-P-E 4500-SO3(C) 4500-SO4(C) 5210-B 5320-B 9215-B 9215-D 9221-B

9222-D 9223-B FLOW IDEXX

Procedure Id

USEPA USEPA USEPA APHA APHA APHA USEPA APHA APHA APHA APHA APHA APHA USEPA APHA USEPA APHA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

APHA APHA CWSD CWSD

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAATurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by Manual CVAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerDetermination of Anions by ICMetals in Water by GFAAFluoride in Water Using an ISECalcium in Water by Titration Using EDTATotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Organic Carbon by CombustionpH in WaterAmmonia in Water by Selective Electrode MethodAmmonia in Water Using Phenate MethodAmmonia in Water Using Automated Phenate MethodNitrite in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSulfite in Water by ColorimetrySulfate in Water by Gravimetric Analysis5-Day Biochemical Oxygen DemandDissolved Organic Halogen in WaterHeterotrophic Plate Count- Pour Plate MethodHeterotrophic Plate Count- Membrane Filter MethodStandard Total Coliform Fermentation Technique, Multi-tubeFermentation TechniqueFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFLOWIDEXX

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

StatusCWSD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 321 of 515

Dan's DUMMY test organizarion

1103.1

D4190 QAPP

Procedure Id

USEPA

ASTM DEMO-002

Procedure Source

Escherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)Metals by Argon Emission SpectroscopyKaruk

Procedure Name

Active

ActiveActive

StatusDANTEST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 322 of 515

Denver Department of Environmental Health

2320 2340 2510 2540-C 2540-D 270.2 4500-CL(G) 4500-H 4500-NH3(H) 4500-NO2(B) 4500-NO3(I) 4500-NOR(B) 4500-O-F 4500-P-F

4500-SO4(B) 4500-SO4(F) 5310-C 9222-D

Procedure Id

APHA APHA APHA APHA APHA USEPA APHA APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA APHA

Procedure Source

Alkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSelenium by GFAAResidual Chlorine by Colorimetry- DPD Colorimetric MethodpH in WaterAmmonia in Water - Flow Injection AnalysisNitrite in Water by ColorimetryNitrate in Water- Cadmium Reduction Flow InjectionTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Titration- Copper/Sulfate-Sulfamic AcidPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfate in Water by Ion ChromatographySulfate in Water by ColorimetryTotal Organic Carbon in Water- Ultraviolet Oxidation MethodFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

StatusDDEH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 323 of 515

Interstate Sanitation Commission

00-01 00-02 00-03 10001 10002 1001

10018 10027 10028 10029

10200-F 10200-G 10200-H 10200-I 10400-D 110.1 110.2 110.3 120.1 120.1_M 130.1 150.1 160.1 160.2 160.2_M 160.3 160.4 160.5 1613(W) 170.1 180.1 200 200.1 200.11 200.7(W) 200.8(W) 200.9 202.1 2120-B 2120-E 2130 220.2

Procedure Id

USEPA USEPA USEPA HACH HACH HACH

HACH HACH HACH HACH

APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA

Procedure Source

Gross Alpha and Beta Activity in WaterGross Alpha Activity in Drinking Water by CoprecipitationLead-210 and Polonium-210 in Dried SamplesNitrogen, Ammonia, ElectrodeNitrogen, Ammonia, Electrode, Known AdditionDetermination of Lead, for use in Lead and Copper Rule compliancemonitoringTotal and Fecal Coliforms, E. Coli, P/AFecal Coliforms, MPN (sludges)Fecal Coliforms, MPN (sludges)m-ColiBlue24 Method of the Determination of Total Coliforms and E.coliPhytoplankton Counting TechniquesZooplankton Counting TechniquesChlorophyll a-b-c DeterminationDetermination of Biomass (Standing Crop)Macrophyton Population EstimatesColor by Calculating ADMI ValuesColor Analysis Using Platinum/CobaltColor by Spectrophotometric AnalysisConductanceConductivity in Industrial WasteTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsTotal ResidueVolatile ResidueSettleable MatterDioxins and Furans - WaterTemperatureTurbidity by NephelometryMetals by Atomic AbsorptionMetals in Marine Waters by ICP/MSMetals in Fish Tissue by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAColor in Water by Visual ComparisonColor in Water Using the ADMI MethodTurbidity in WaterCopper by GFAA

Procedure Name

ActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 324 of 515

Interstate Sanitation Commission

2340 245.1 245.2 2510 2520-B 2520-C 2540-B 2540-C 2540-D 2550 3.4 300.0 310.1 3111-B 325.2 325.3 350.1 3500-AG(C) 3500-CA(B) 3500-CU(B) 3500-HG(C) 3500-K-D 3500-NA(D) 351.2 351.2-350.1 351.3(B) 351.3(C) 352.1 353.1 353.2 353.2+351.2 353.4 354.1 360.1 360.2 365.1 365.2 365.4 365.5 370.1 375.4 405.1 410_M(A) 415.1

Procedure Id

APHA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA DEMOTEST USEPA APHA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA DEMOTEST USEPA USEPA USEPA USEPA USEPA DEMOTEST USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Hardness in Water by EDTA TitrationMercury in Water by CVAAMercury by CVAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerColiforms- Membrane FilterSulfateAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetrySilver in Water by ICPCalcium in Water by FLAACopper in Water by FLAA or GFAAMercury in Water by SpectrophotometryPotassium in Water by Flame PhotometrySodium in Water by Flame PhotometryTotal Kjeldahl Nitrogen by ColorimetryOrganic NitrogenTotal Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal NitrogenDetermination of Nitrite and NitrateNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionOrthophosphate in Water by ColorimetryDissolved Silica by ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by Combustion

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 325 of 515

Interstate Sanitation Commission

4500-CL-(C) 4500-H 4500-O-G 4500-P-C

4500-SO4(B) 4500CL 5001 5029 5030 50APP-B 5210-B 6010B 7470A 7471A 7543 7890 8000 8000(A1) 8000(A2) 8001(1) 8001(2) 8001(3) 8001(A1) 8001(A2) 8001(A3) 8005 8008 8009 8010 8013 8021 8023 8024 8025 8027 8029 8033 8034 8037 8038 8043 8047 8048

Procedure Id

APHA APHA APHA APHA

APHA DEMOTEST NIOSH NIOSH NIOSH USEPA APHA USEPA USEPA USEPA DEMOTEST DEMOTEST HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH

Procedure Source

Chloride in Water by Titration- Mercuric Nitrate MethodpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetrySulfate in Water by Ion ChromatographySTANDARD METHODS 4500CL - CHLORINE2,4-D by HPLC/UV4,4'-Methylenedianiline by HPLCCyanuric Acid by HPLC/UVSuspended Particulate Matter5-Day Biochemical Oxygen DemandInductively Coupled Plasma AESMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteCloud CoverFloating DebrisChemical Oxygen DemandChemical Oxygen DemandChemical Oxygen DemandTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformOil and Grease in WaterTotal Iron in WaterZinc in WaterAcidity by TitrationArsenic in WaterFree Chlorine in Water by DPDHexavalent Chromium in WaterTotal Chromium in WaterColor, APHA Platinum-CobaltCyanide in WaterFluoride in WaterLead in WaterManganese in WaterNickel in WaterAmmonia Nitrogen in WaterBiological Oxygen Demand in WaterPhenols in WaterReactive Phosphorus in Water

Procedure Name

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

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Interstate Sanitation Commission

8051 8071 8074(A) 8074(B) 8081A(WWB) 8082(W) 8116 8131 8156 8157 8158 8160 8163 8164 8165 8167 8168 8172 8186 8190 8195 8219 8221 8222 8224 8225 8226 8229 8230 8241 8260B 8270C(W) 8271 8276 8277 8311 8323 8334 8368 8375 8506 8507 9012A 9131

Procedure Id

HACH HACH HACH HACH USEPA USEPA HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH USEPA USEPA HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH USEPA USEPA

Procedure Source

Sulfate in WaterSulfite in Water by TitrationTotal, Fecal and E. Coli ColiformTotal, Fecal and E. Coli ColiformOrganochlorine Pesticides and PCBs by GCPCBs as Aroclors by Capillary Column GCChemical Oxygen Demand in WaterSulfide in WaterpH in WaterDissolved Oxygen in WaterTotal Nonfilterable Residue SolidsConductivity in Water by Direct MeasurementTotal Filterable SolidsVolatile Nonfilterable Solids in WaterSettleable Matter Solids in WastewaterTotal Chlorine in Water by DPDTotal Chlorine in Water by TitrationFecal Streptococci, MPNSilica, ColorimetricTotal Phosphorus in WaterDetermination of TurbidityAcidity in WaterAlkalinity by Buret TitrationCalcium Hardness in WaterChloride by Buret TitrationChloride by TitrationTotal Hardness in WaterDissolved Oxygen in WaterChemical Oxygen Demand in WaterHeterotrophic Bacteria, Pour PlateVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSResidue, Total SolidsTotal Volatile and Fixed SolidsResidue, Volatile, Filterable (dissolved)Ozone in WaterFluoride, ElectrodeFree Chlorine in Water by TitrationColiform Bacteria, Fecal MPNTemperature, ThermometricCopper in WaterNitrite in WaterTotal and Amenable Cyanide (Auto UV)Total Coliform by Multiple Tube Fermentation

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

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Interstate Sanitation Commission

9132 9221-E

9222-B 9222-D 9230C 972.23 973.48 974.14 993.1 ANIONS B0001 B1505 B8502 C-008-1 CHLOR A CHLOROA/PHEOA D1068(B) D1125(A) D1125(B) D1889 D3223 D3534(ELCD) D3559(C) D3590(B) D3867(A) D3867(B) D4183(A) DO-001 FISH MEASURES FLOW_DIRECTION I1550 I1601 I2539 I2545(W) I2600(W) I2700 METALS METHOD 777 PESTICIDIES PH IN WATER PHYTOPLANKTON PMD-CBF PMD-CD

Procedure Id

USEPA APHA

APHA APHA DEMOTEST AOAC AOAC AOAC AOAC DEMOTEST USDOI/USGS USDOI/USGS USDOI/USGS USEPA DEMOTEST DEMOTEST ASTM ASTM ASTM ASTM ASTM ASTM ASTM ASTM ASTM ASTM ASTM DEMOTEST DEMOTEST DEMOTEST USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS DEMOTEST DEMOTEST DEMOTEST DEMOTEST DEMOTEST USEPA USEPA

Procedure Source

Total Coliform by Membrane FilterEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureFecal StreptococciLead in FishTotal Nitrogen in WaterMercury in FishClostridium perfringens from ShellfishanionsStandard Plate Count- Membrane Filter MethodPhytoplankton Enumberation- Counting Cell MethodAlgal Growth Potential (AGP) Spikes for Nutrient LimitationTotal Suspended Solids in WaterChlorophyll aChlorophyll A; Pheophytin A RatioIron in Water by Chelation and FLAAConductivity and Resistivity in WaterConductivity and Resistivity in WaterTurbidity of WaterTotal Mercury in Water by CVAAPCBs in Water by Gas ChromatographyLead in Water by PolarographyTKN by AutoAnalyzerNitrite-Nitrate Automated Cd ReductionNitrite-Nitrate by Manual Cd ReductionTotal Recoverable Organic PhosphorusField Method for Determination of Dissolved Oxygen, ProbeField Determination of Whole Fish Physical CharacteristicsTidal StageAmmonia plus Organic Nitrogen in WaterOrthophosphate-Phosphorus by ColorimetryNitrite-Nitrogen in Water by ColorimetryNitrite- Plus Nitrate-Nitrogen in WaterPhosphorus in Water by ColorimetrySilica in Water by ColorimetryICP MetalsNew method number 777Herbicides and Insecticides in WaterpHPhytoplanktonCarbofuran by IR SpectroscopyCadmium by AAS

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

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Interstate Sanitation Commission

PMD-DCA(GC1) PMD-DCA(GC2) PMD-FLM PMD-MAL(IR) RBP-FIELD SEDIMENT SOP-3 STATION OBS TEMP-001 WEATHER-001

Procedure Id

USEPA USEPA USEPA USEPA DEMOTEST DEMOTEST DEMOTEST DEMOTEST DEMOTEST DEMOTEST

Procedure Source

2,4-D and 2,4,5-T Esters by GC2,4-D and Silvex by Derivatization GCAtrazine and Metolachlor by GCMalathion by IR SpectroscopyField RBP ProceduresField Sediment AnalysisStandard Analytical ProcedureField Station Visit Physical Direct Measurements and ObsField Determination of Water Temperature, ProbeField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusDEMOTEST

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Environmental Monitoring and Assessment Program

AIA-CTNCA AKRFA300 ARM67:WA ARM67N:WA ASTM D-422 ASTM E-1367-90

ASTM1993

B/W67:WA

CHLA-NCA CTD CAST-NCA-NYCTD-NCA-CT CVAA CVAA-NCA CVAA-VP EPA 445.0M EPA 9060/1986 EPA-160.2 EPA-300.0 EPA-349.0 EPA-350.1 EPA-353.2 EPA-353.3 EPA-353.4PD EPA-365.2 EPA-365.5 EPA-365.5PD EPA-366 EPA-415.1 EPA-445.0 EPA200.7 EPA200.8 EPA204.2 EPA206.2 EPA213.2 EPA239.2 EPA245.5 EPA270.2 EPA272.2 EPA282.2 FAA FAAS: NCA-GULF FIMS

Procedure Id

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

Procedure Source

Automated ion analyzer/colorimetricAlpKem RFA 300 Series Nutrient AnalyzerSilicate-Armstrong et al. '67: EMAP-West, Washington StateNitrate/nitrite-Armstrong et al. '67: EMAP-West, Washington StateASTM D-422: NCA-Gulf 2000 for TOCStandard guide for conducting 10-day static sediment toxicity testsw/ marine organismsStandard guide for conducting 10-day static sediment toxicity testsw/ marine organismsO-Phosphate-Bernhardt and Wilhelms '67: EMAP-West, WashingtonStateTD700 FluorometerSeabird CTD cast-NCA-NYSeabird CTD cast-NCA-CTCold vapor atomic absorption analysisCold vapor atomic absorption analysisCold vapor atomic absorption analysisEPA-445.0: NCA-Gulf 2000 for Chlorophyll 'a'EPA 9060/1986: NCA-Gulf 2000 for sediment grain sizeEPA-160.2: EMAP-West and NCA-Gulf for TSSEPA-300.0: NCA-Gulf 2000 for NO2 and NO3EPA-350.1: NCA-Gulf 2000 for NH4EPA-350.1: EMAP-West for NH4EPA-353.2: EMAP-West for NO2+NO3EPA-353.3: NCA-Gulf 2000 for NO2+NO3EPA-353.4PD: NCA-Gulf 2000 for TDNEPA-365.2: EMAP-West for PO4EPA-365.5: NCA-Gulf 2000 for PO4EPA-365.5PD: NCA-Gulf 2000 for TDPEPA-366: NCA-Gulf 2000 for SIEPA-415.1: EMAP-West for TOCEPA-445.0: EMAP-West for Chla/PhaeoEPA200.7 for AL, FEEPA200.8EPA204.2 - AntimonyEPA206.2EPA213.2EPA239.2 LeadMercury in sediment (cold vapor with permanganate digestion)EPA270.2EPA272.2EPA282.2 - TinFlame Atomic Absorption SpectrometerFlame Atomic Absorption Spectrometer-HF: NCA-Gulf 2000Flow Injection Mercury System

Procedure Name

ActiveActiveActiveActiveActiveActive

Active

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusEMAP-CS

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Environmental Monitoring and Assessment Program

FISH MEASURES FLUORO GC/ECD GC/ECD(NCA) GC/ECD(VP) GC/MS GC/MS(NCA) GC/MS-SIM GCECD GCMS GFAA GFAA-HF GFAA-NCA GFAA-VP

GRN-NCA GRV HAA HGAF-NCA HRGC/FP

HYDRO-NCA HYDRO-SE_GU HYDROLAB CAST HYDRO_HI02

ICP-AES(NCA) ICP-AES(VP) ICP-ES-HG

ICP-ES-HNO3

ICP-MS-HF ICPAES ICPMS ICPOES

LI-190SA LI-193SA LICOR LIGHT METER PARMARPCN IV MBH54AR MOIS-NCA NA

Procedure Id

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS

EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

Procedure Source

Field Fish MeasurementsTurner Designs 10-005R Fluorometer: EMAP-WestGas chromatography / electron capture detectionGas chromatography/electron capture detectionGas chromatography/electron capture detectionGas Chromatograph/Mass SpectrometerGas Chromatograph/Mass SpectrometerGas Chromatograph/Mass Spectrometer-SIM: NCA-Gulf 2000Gas chromatography/electron capture detectionGas Chromatograph/Mass SpectrometerGraphite Furnace Atomic Absorption AnalysisGraphite Furnace Atomic Absorption Analysis: Gulf 2000Graphite Furnace Atomic Absorption AnalysisGraphite Furnace Atomic Absorption Analysis (Zeeman-corrected,stabilized temperature)Analysis and calculation of sediment grain sizeGravimetricHydride Atomic Absorption AnalysisHydride Generation Atomic FluorescenceHigh resolution gas chromatography and flame photometricdetectionHydrolab Handheld CastHydrolab Multi Probe Handheld InstrumentHydrolab Handheld Cast: EMAP-West 1999-2000 CA and ORHydrolab H2O Datasonde-EMAP-West Insular Province Hawaii2002Inductively Coupled Plasma Atomic Emission SpectrometerInductively Coupled Plasma Atomic Emission SpectrometerInductively Coupled Plasma Atomic Emission Spectrometer-HG:NCA-GulfInductively Coupled Plasma Atomic Emission Spectrometer-HNO3:NCA-GulfInductively Coupled Plasma Mass Spectrometer-HF: NCA-Gulf 2000Inductively Coupled Plasma Atomic Emission SpectrometerInductively Coupled Plasma Mass SpectrometerInductively Coupled Plasma Optical Emission Spectroscopy: NCA-HI2002Li-Cor LI-190SA Quantum SensorLi-Cor LI-193SA Spherical Quantum SensorLicor sensors for NCA-Gulf and SE: ambient and underwaterLight Meter Determination of PARMARPCN IVMettler H54AR BalanceProcedure/calculation for moistureNot analyzed

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

ActiveActiveActiveActive

ActiveActiveActive

Active

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

StatusEMAP-CS

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Environmental Monitoring and Assessment Program

NOTREC NR NUT-HI02 NUTRNT-NCA PSEP-TOC PSEP86 S/M72:WA SAL_HI02

SEABIRD CAST SECCHI CAST SECCHI-NCA SISE

SM2540D SM4500NH3 SM4500NO3 SM4500P SW6010 SW7060 SW7740 SW8081 SW80818082 SW8270 TOC-HI TOC-NCA TOX_TEST-HI TOX_TEST-NCA TSS-NCA TURB_HI02

WSA YSI-NCA

Procedure Id

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS EMAP-CS

EMAP-CS EMAP-CS

Procedure Source

Not recordedNot relevantNutrient analyses: EMAP-West Insular Province Hawaii 2002API 300 Flow AnalyzerPSEP-TOCPSEP86: sediment grain sizeAmmonium-Slawyk/MacIsaac '72: EMAP-West, Washington StateAGE laboratory salinometer - EMAP-West Insular Province Hawaii2002Seabird Data Logger/Profiler CastSecchi Disk CastSecchi disc cast-NCASulfide ion-specific electrode measure the trapped, evolvedhydrogen sulfide in solutionSM2540D: EMAP-West CA 1999-2000 for TSSSM4500NH3: EMAP-West CA 99-00 for NH4-N and NO3-NSM4500NO3: EMAP-West CA 1999-2000 for NO2SM4500P: EMAP-West CA 1999-2000 for PO4SW6010SW7060 for ASSW7740 for SEFrom Standard MethodsSW80818082: From Standard MethodsFrom Standard MethodsTOC AnalyzerAnalysis of Total Organic CarbonSediment Toxicity test method-NCA Hawaii 02Sediment Toxicity test method-NCADry/weigh filter pads rinsed in DI water to remove saltsTurbidity measurements for EMAP-West Insular Province Hawaii2002Wet Sieve AnalysisYSI model 6600_M used by NH and NY-NCA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

StatusEMAP-CS

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Coyote Valley Tribal Council (California)

QAPP

Procedure Id

EPACANAW

Procedure Source

Quality Assurance Procedures Policy

Procedure Name

Active

StatusEPACANAW

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and Equipment Summary

Page 333 of 515

EPA Office of Research & Development

1604

ENTEROLERT

Procedure Id

USEPA

IDEXX

Procedure Source

Total Coliforms and E. coli in Water by Membrane Filtration Using aSimultaneous Detection Technique (MI Medium)Enterolert Quanti-Tray; Multi Tube, Multi Well, for Enterococcii

Procedure Name

Active

Active

StatusEPAORD

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Page 334 of 515

Eastern Shawnee Tribe of Oklahoma

130.1 150.1 1631 1632 1637 180.1 200.7(W) 350.1 353.2 365.2 8507 9223-B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA HACH APHA

Procedure Source

Total HardnesspHMercury in Water by Oxidation, Purge and Trap, and CVAFSInorganic Arsenic in Water by Hydride Generation Quartz FurnaceTrace Elements in Water by Chelation Preconcentration and GFAATurbidity by NephelometryMetals in Water by ICP-AESAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryNitrite in WaterEnzyme Substrate Test, E. coli, Coliform Group

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusESTO

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and Equipment Summary

Page 335 of 515

SUPERFUND EUREKA MILLS

ILM05 ILM05.2 ILM05.3

Procedure Id

EUREKA EUREKA EUREKA

Procedure Source

ILM05ILM05.2ILM05.3

Procedure Name

ActiveActiveActive

StatusEUREKA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 336 of 515

FOREST COUNTY POTAWATOMI COMMUNITY (Wisconson)

10200-H 170.1 180.1 2320 2520-B 2810 365.1 365.4 375.4 4500-CL(B) 4500-CL-(E) 4500-H 4500-NH3(C) 4500-NH3(E) 4500-NO3(F) 4500-NO3(H) 4500-NOR(B) 4500-O-G 4500-P-E 9060 9060AM COLILERT/2000 D3858 D516 I3765

Procedure Id

APHA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA IDEXX ASTM ASTM USDOI/USGS

Procedure Source

Chlorophyll a-b-c DeterminationTemperatureTurbidity by NephelometryAlkalinity in Water by TitrationSalinity in Water- Electrical Conductivity MethodDissolved Gas SupersaturationPhosphorus by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Colorimetry- Automated Ferricyanide MethodpH in WaterAmmonia in Water by Titrimetric MethodAmmonia in Water by Selective Electrode Method (Known Addition)Nitrate in Water- Automated Cadmium ReductionNitrate in Water- Automated Hydrazine ReductionTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Organic Carbon in Water and WasteTotal Volatile Organic CarbonColilert Quanti-Tray/2000; MPN - Multi Tube, Multi Well for E.coliOpen-Channel Flow Measurement by AreaSulfate in Water by TurbidimeterResidue by Evaporation and Gravimetric

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusFCPC

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and Equipment Summary

Page 337 of 515

Peace River Manasota Regional Water Supply Authority (FL)

10200-H 110.2 160.2 160.4 180.1 200.7(W) 236.1 2520-C 2540-G 2550 310.1 325.2 350.1 351.2 353+351 353.2 365.2 365.3 365.4 370.1 415.1 445 4500-CL(C) 4500-H 4500-O-G 5310-B CHLOROPHYL C CHLOROPHYLL A CHLOROPHYLL B DOC I-1250-85 I-142-87 I-2030-85 I-2057-84 I-2781-84 I-3765-84 I-3767-85 I-3860-85 I-4522-85 I-4540-84 I-4545-84 I-4552-84 I-4600-84 I-4601-84

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA FLPRMRWS USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltNon-Filterable Residue - TSSVolatile ResidueTurbidity by NephelometryMetals in Water by ICP-AESIron by FLAASalinity in Water- Density MethodTotal, Fixed and Volatile SolidsTemperature of Water by ThermometerAlkalinity by TitrationChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal NitrogenNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetryTotal Organic Carbon by CombustionIn-Vitro Determination of ChlorophyllResidual Chlorine in Water by Titration- Iodometric Method IIpH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodTotal Organic Carbon by Combustion-Infrared MethodChlorophyl cChlorophyll A performed by USGSChlorophyll bDissolved Inorganic CarbonCOLORSILICA, DISSOLVEDALKALINITY, TOTAL AS CaCO3CHLORIDE, DISSOLVEDSPECIFIC CONDUCTANCERESIDUE, TOTAL NON-FILTERABLE AT 105 DEG CRESIDUE, VOLITILE NON-FILTERABLETURBIDITYNITROGEN ,AMMONIANITROGEN, NITRATENITROGEN, NO2 + NO3TKNPHOSPHORUS, AS P TOTALPHOSPHORUS, ORTHOPHOSPHATE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusFLPRMRWS

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Page 338 of 515

Peace River Manasota Regional Water Supply Authority (FL)

LICOR NO2 O-0004-78 PHEOPHYTIN TCOL TSS

Procedure Id

FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS FLPRMRWS

Procedure Source

LicorNITRATE NITROGENCARBON, INORGANIC TOTALPHEOPHYTIN ANALYSISTOTAL COLIFORM BACTERIATotal Suspended Solids

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusFLPRMRWS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 339 of 515

Fond Du Lac Band of Chippewa (MN)

FDL_QAPP UNKNOWN

Procedure Id

FONDULAC FONDULAC

Procedure Source

Fond Du Lac Quality Assurance Project PlanUNKNOWN

Procedure Name

ActiveActive

StatusFONDULAC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 340 of 515

Assiniboine & Sioux Tribes Fort Peck Indian Reservation (MT)

10200-H 1103.1

1106.1

120.1 150.1 160.2 180.1 200.7(W) 200.8(W) 218.4 2320 2340 245.1 2540-C 2550 325.3 350.1 351.3(A) 353.2 365.2 375.3 4500-CL(G) 4500-CN(C) 4500-F-C 4500-O-G 5210-B B0051 B0065

FPTQAPP S-1.60 TN-CALC

Procedure Id

APHA USEPA

USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USDOI/USGS USDOI/USGS

FORTPECK FORTPECK FORTPECK

Procedure Source

Chlorophyll a-b-c DeterminationEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)Enterococci in Water by Membrane Filtration Using membrane-Enterococcus-Esculin Iron Agar (mE-EIA)ConductancepHNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSHexavalent Chromium by FLAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAATotal Dissolved Solids in WaterTemperature of Water by ThermometerChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetrySulfate by Gravimetric DeterminationResidual Chlorine by Colorimetry- DPD Colorimetric MethodCyanide in Water after DistillationFluoride in Water Using an ISETotal Dissolved Oxygen by Membrane Electrode Method5-Day Biochemical Oxygen DemandFecal Coliform Bacteria- Presumptive Test- MPN MethodFecal Streptococcal Bacteria- Presumptive/Confirmation- MPNMethoFort Peck Tribes Quality Assurance Project PlanS-1.60Total Nitrogen, Mixed Forms, Calculated

Procedure Name

ActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

StatusFORTPECK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 341 of 515

Florida Keys NMS - Water Quality Monitoring Program

APA DENSITY RATIO SI SRP TN TOC TURBIDITY VATC

Procedure Id

FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP FWC-WQMP

Procedure Source

Alkaline Phosphatase ActivityDensitySimple Ratio CalculationSilicateSoluble Reactive PhosphorusTotal NitrogenTotal Organic Carbon ProcedureTurbidityVertical Light Attenuation Coefficient

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusFWC-WQMP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 342 of 515

Fish Wildlife Conservation / Wildlife Research Institute(FL)

CREMP

Procedure Id

FWC/FWRI

Procedure Source

Coral Reef Evaluation and Monitoring Project

Procedure Name

Active

StatusFWC/FWRI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 343 of 515

Florida Fish and Wildlife Conservation Commission (Florida)

10200-H 120.1 150.1 160.2 1631 200.7(W) 2130 2320 2340-B 245.6 2510 2540-B 2540-D 2540-E 2540-G 2550 2580 300(A) 300(B) 310.1 3111-B 350.1 3500-FE(D) 351.2 353.2 365.1 375.4 415.1 419-D 4500-F-C 4500-H 4500-NH3-B,C 4500-NOR(B) 4500-NORG-B 4500-O-B 4500-O-G 4500-P-D 5550-B 9212 SPEC TURBIDITY STATION OBS STATION WEATHER

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA APHA APHA FWCLOCAL USEPA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA FWCLOCAL APHA APHA FWCLOCAL APHA FWCLOCAL APHA APHA APHA APHA USEPA FWCLOCAL FWCLOCAL FWCLOCAL

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSMercury in Water by Oxidation, Purge and Trap, and CVAFSMetals in Water by ICP-AESTurbidity in WaterAlkalinity in Water by TitrationHardness by calculationMercury in Tissue by CVAAConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterTotal, Fixed and Volatile SolidsTemperature of Water by ThermometerOxidation-Reduction Potential of WaterInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameAmmonia Nitrogen by ColorimetryIron in Water by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetrySulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionNitrate in water by the Brucine MethodFluoride in Water Using an ISEpH in WaterAmmonia in Water by Distillation and NesslerizationTotal Kjeldahl Nitrogen in WaterOrganic Nitrogen by Macro-Kjeldahl Method and NesslerizationTotal Dissolved Oxygen by Titration- Iodometric MethodTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Stannous Chloride TitrationTannin and Lignin by ColorimetryChloride in Water by ISETurbidity using spectrophotometerField Station Visit Direct Physical Measurements and ObservationsField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusFWCLOCAL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 344 of 515

City of Glendale (Colorado)

170.1 200.7(W) 200.9 2320 2340 2510 2540-C 2540-D 375.2 4500-H 4500-NH3(F) 4500-NO2(B) 4500-NO3(F) 4500-O-G 4500-P-E 5210-B 5310-B 9221-E

FLOW

Procedure Id

USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA

GLENDALE

Procedure Source

TemperatureMetals in Water by ICP-AESMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSulfate in Water by ColorimetrypH in WaterAmmonia in Water Using Phenate MethodNitrite in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid Method5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueFlow

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

StatusGLENDALE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 345 of 515

MATCH-E-BE-NASH-SHE-WISH BAND OF POTAWATOMI (MI)

120.1 150.1 170.1 360.1

Procedure Id

USEPA USEPA USEPA USEPA

Procedure Source

ConductancepHTemperatureDissolved Oxygen Using an ISE

Procedure Name

ActiveActiveActiveActive

StatusGNLK01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 346 of 515

Region 8 Superfund: Gold Hill Town and Mine

ILM05

Procedure Id

GOLDHILL

Procedure Source

ILM05

Procedure Name

Active

StatusGOLDHILL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 347 of 515

GRAND PORTAGE Band of CHIPPEWA INDIANS (MN)

111.1 351.2 353.2 365.2

Procedure Id

GPORTAGE USEPA USEPA USEPA

Procedure Source

Grand Portage Test FLPTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent Colorimetry

Procedure Name

ActiveActiveActiveActive

StatusGPORTAGE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 348 of 515

Hanalei Watershed Study (Region 9) - Kauai, Hawaii

160.2_M 8156 8157 8160 8195 8375 ENTEROLERT2000 FLOW SUSPENDED SED TECHNICON

Procedure Id

USEPA HACH HACH HACH HACH HACH IDEXX HANALEI HANALEI HANALEI

Procedure Source

Total Suspended SolidspH in WaterDissolved Oxygen in WaterConductivity in Water by Direct MeasurementDetermination of TurbidityTemperature, ThermometricEnterolert Quanti-Tray/2000; Multi Tube, Multi Well, for EnterococciiFlow measurement - cfsSuspended Sediment Concentration (SSC)AutoAnalyzer II

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusHANALEI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 349 of 515

HANNAHVILLE TRIBAL COMMUNITY

160.1 170.1 180.1 200.7_M 2520-B 2580 2810 300_M 350.1 351.2 353.2 365.2 4500-H 4500-O-G 8141A(W) 9223-B 973.48

Procedure Id

USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA AOAC

Procedure Source

Filterable Residue - TDSTemperatureTurbidity by NephelometryICP-AES For Trace Element AnalysisSalinity in Water- Electrical Conductivity MethodOxidation-Reduction Potential of WaterDissolved Gas SupersaturationDetermination of Anions by ICAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetrypH in WaterTotal Dissolved Oxygen by Membrane Electrode MethodOrganophosphorus Compounds in WaterEnzyme Substrate Test, E. coli, Coliform GroupTotal Nitrogen in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusHANNAHWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 350 of 515

City and county of Honolulu

150.1 160.2 1624(S) 1625(S) 1664 170.1 180.1 200 200.1 200.1(FLAA) 200.1(GFAA) 200.1(ICP) 200.11 200.12 200.13 200.15 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 3111-B 3112-B 3113-B 335.2 335.2_M(S) 350.1 350.2(C) 3500-CR(D) 351.3(A) 353.2 353.2_M 353.3 365.3 365.4 405.1 413.1 445 6010B 603 608 613 614 624

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

pHNon-Filterable Residue - TSSVolatiles by Isotope Dilution - SoilSemivolatiles - Soil, GC/MSExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryMetals by Atomic AbsorptionMetals in Marine Waters by ICP/MSAcid Soluble Metals in Water by FLAAAcid Soluble Metals in Water by GFAAAcid Soluble Metals - ICPMetals in Fish Tissue by ICP-AESElements in Water by Temperature GFAAElements in Water by Chelation with GFAAMetals in Water by Nebulization and ICP-AESMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAMetals in Water by FLAA- Direct Air-Acetylene FlameMercury in Water by CVAAMetals in Water by GFAATotal Cyanide in WaterTotal Cyanide in Soils and SedimentsAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by TitrationTotal Hexavalent Chromium in WaterTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandTotal Recoverable Oil and GreaseIn-Vitro Determination of ChlorophyllInductively Coupled Plasma AESAcrolein and Acrylonitrile in WastewaterOrganochlorine Pesticides and PCBs by GCTetrachlorodibenzo-p-dioxin by GC/MSOrganophosphorus Pesticides IPurgeable Organics in Wastewater

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusHI301H

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 351 of 515

City and county of Honolulu

625 7471A 8081A(SWB) 8082(S) 8141A(S) 8270C(S) 8280A(S) 8290 9222-D 9230-C CTD CVAA SOLIDS ENT EPA603 MODIFIEDFLOW HI301H ICP-AES SOLIDS ICP-MS SOLIDS PERCENT LIPIDS PERCENT SOLIDS PLUMB

SEDAVS SEDTOC STL-ALKYLTINS

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA HI301H HI301H HI301H HI301H HI301H HI301H HI301H HI301H HI301H HI301H HI301H

HI301H HI301H HI301H

Procedure Source

Base/Neutral and Acid Organics in WastewaterMercury in Solid or Semisolid WasteOrganochlorine Pesticides and PCBs by GCPCBs as Aroclors by Capillary Column GCOrganophosphorus Compounds in Soil by GCSemivolatile Organic Compounds by CGC/MSPolychorinated Dioxins and FuransPolychlorinated PCDDs and PCDFs by HRGC/HRMSFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueCTD ProfilerMercury in solids by CVAAEnterococcus EPA 1600EPA 603 modified with use of MS for detectorflow measurement by recorder or totalizerAsbestosMetals for sediment and fish tissue by ICP-AESMetals in sediment and fish tissue by ICP-MSPERCENT LIPIDSPERCENT SOLIDSProcedures for Handling and Chemical Analysis of Sediment andWater SamplesSediment Acid Volatile SulfidesSediment Total Organic CarbonSTL (contract lab) Status & Trends GC-FPD method for Tributyltin

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

StatusHI301H

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 352 of 515

Ho-Chunk Nation (WI)

180.1 2320 2520-B 2540-D 2550 353.3 375.4 4500-CL-(B) 4500-H 4500-NH3(D) 4500-NOR(B) 4500-O-G 4500-P-E

Procedure Id

USEPA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA

Procedure Source

Turbidity by NephelometryAlkalinity in Water by TitrationSalinity in Water- Electrical Conductivity MethodTotal Suspended Solids in WaterTemperature of Water by ThermometerNitrate-Nitrite Nitrogen by Cd ReductionSulfate by Turbidimetric DeterminationChloride in Water by Titration- Argentometric MethodpH in WaterAmmonia in Water by Selective Electrode MethodTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusHO-CHUNK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 353 of 515

Iowa DNR's Animal Feeding Operation

H2O

Procedure Id

IAAFO

Procedure Source

Water level measurement

Procedure Name

Active

StatusIAAFO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 354 of 515

Iowa Geological Survey (Iowa)

160.1 1603

350.1 351.1 351.2 353.2 365.4 507 9222-D APHA 9222G I3765

Procedure Id

USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA APHA IASNAPST USDOI/USGS

Procedure Source

Filterable Residue - TDSEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Ammonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionNitrogen and Phosphorus PesticidesFecal Coliform Membrane Filter ProcedureFecal coliform-MF Partition ProceduresResidue by Evaporation and Gravimetric

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusIASNAPST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 355 of 515

Illinois EPA

10200-H 120.1 120.6 150.6 160.1 160.2 160.4 200.6 200.7 200.8 200.8(S) 200.8(W) 2320 2540-E 300(A) 310.1 325.2 325.3 335.2 335.3 340.2 350.1 350.3 351.3(A) 351.3(C) 351.4 352.1 353.2 365.1 365.2 375.2 375.4 415.2 420.1 420.2 4500-CN(I) 515.1 515.3 5310-C 8081 8081(S) 8082 8082(S) 8141

Procedure Id

APHA USEPA IL/SWSD IL/SWSD USEPA USEPA USEPA IL/SWSD IL_EPA IL_EPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA IL_EPA APHA IL_EPA USEPA IL_EPA USEPA IL_EPA

Procedure Source

Chlorophyll a-b-c DeterminationConductanceSpecific Conductance - Acid DepositionpH of Wet Deposition - pH MeterFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueCa, Mg, K and Na in Wet DepositionMetals by ICP-AESMetals by ICP/MSMetals in Wastes by ICP/MSMetals in Waters by ICP/MSAlkalinity in Water by TitrationFixed and Volatile Solids in WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - PotentiometricTotal Kjeldahl Nitrogen Using an ISENitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric DeterminationLow Level Total Organic Carbon in WaterTotal Recoverable Phenolics in WaterTotal Recoverable Phenolics in WaterWeak Acid Dissociable Cyanide in WaterChlorinated Acids in Water by CGC/ECDChlorinated Acids by GC/ECDTotal Organic Carbon in Water- Ultraviolet Oxidation MethodOrganochlorine Pesticides by GC-ECDOrganochlorine Pesticides and PCBsPCBs as Aroclors by Capillary Column GCPCBs as Aroclors by Capillary Column GCOrganophosphorus Compounds by GC

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusIL_EPA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 356 of 515

Illinois EPA

8141(S) 9050A 9060 FIELD HYDROLAB INL029 LAB ORL018

Procedure Id

USEPA USEPA USEPA IL_EPA IL_EPA IL_EPA IL_EPA IL_EPA

Procedure Source

Organophosphorus Compounds in Soil by GCSpecific ConductanceTotal Organic Carbon in Water and WasteMEASURED IN FIELDHydrolab MultimeterMercury in FishANAYLZED IN LABChlorinated Pesticides/PCBs in Fish

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

StatusIL_EPA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 357 of 515

Indiana STORET

10200-H 120.1 130.1 130.2 150.1 160.2 1631 1636 1638 1664 180.1 200.9 204.2 206.2 206.3 208.1 213.2 2130-B 215.2 218.2 218.6 220.2 2320 2340 239.2 245.1 245.5 249.2 2510 2540-B 2540-D 2540-G 2550-B(2) 270.2 279.2 283.2 289.1 310.1 310.2 3112-B 325.2 335.1 335.2 335.4

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA INSTOR USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA APHA APHA APHA APHA INSTOR USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationConductanceTotal HardnessTotal HardnesspHNon-Filterable Residue - TSSMercury in Water by Oxidation, Purge and Trap, and CVAFSHexavalent Chromium in Ambient Water by Ion ChromatographyTrace Elements in Water by ICP/MSExtractable Material in Oil and GreaseTurbidity by NephelometryMetals by Temperature Stabilized GFAAAntimony by GFAAArsenic by GFAAArsenic by HYDAABarium by FLAACadmium by GFAATurbidityCalcium by EDTA Titrimetric AnalysisChromium by GFAAHexavalent Chromium by Ion ChromatographCopper by GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationLead by GFAAMercury in Water by CVAAMercury in Sediment by CVAANickel by GFAAConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Suspended Solids in WaterTotal, Fixed and Volatile SolidsWater TemperatureSelenium by GFAAThallium by GFAATitanium by GFAAZinc by FLAAAlkalinity by TitrationAlkalinity by Colorimetric AnalysisMercury in Water by CVAAChloride by Colorimetric Analysis IICyanides Amenable to ChlorinationTotal Cyanide in WaterCyanide by Semi-Automated Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusINSTOR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 358 of 515

Indiana STORET

340.2 350.1 3500-CA(D) 3500-CR(D) 3500-FE(B) 3500-K-D 3500-MN(B) 3500-NA(D) 351.2 351.4 353.1 353.2 354.1 365.1 365.2 370.1 375.2 375.4 376.2 405.1 410.1 410.2 410.4 413.1 415.1 415.2 418.1 425.1 4500-CN(E) 4500-CN(G) 4500-CN(I) 4500-O-G 4500-P-E 4500-SI(D) 4500-SO4(F) 5210-B 5210-C 524.2 525.2 5310-C 547 5520-C 5520-D 6010B

Procedure Id

USEPA USEPA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA USEPA APHA APHA USEPA

Procedure Source

Fluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryCalcium in Water by Titration Using EDTATotal Hexavalent Chromium in WaterIron in Water by FLAA or GFAAPotassium in Water by Flame PhotometryManganese in Water by FLAA or GFAASodium in Water by Flame PhotometryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen Using an ISENitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryDissolved Silica by ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric DeterminationSulfide by Colorimetric Determination5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandLow Level Chemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterTotal Recoverable Petroleum HydrocarbonsMethylene Blue Active SubstancesCyanide in Water by ColorimetryCyanides Amenable to Chlorination after DistillationWeak Acid Dissociable Cyanide in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSilica in Water by Spectrophotometry- Molybdosilicate MethodSulfate in Water by Colorimetry5-Day Biochemical Oxygen DemandUltimate Biochemical Oxygen TestPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyTotal Organic Carbon in Water- Ultraviolet Oxidation MethodGlyphosate in Drinking Water by HPLCOil and Grease by Infrared SpectroscopyOil and Grease by Gravimetric AnalysisInductively Coupled Plasma AES

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusINSTOR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 359 of 515

Indiana STORET

6020 608 624 625 7041 7060A 7470A 7471A 7740 7761 7841 8310 9012 9036 9060 9222-B 9222-D 9223-B D422

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA ASTM

Procedure Source

Inductively Coupled Plasma - Mass Spec.Organochlorine Pesticides and PCBs by GCPurgeable Organics in WastewaterBase/Neutral and Acid Organics in WastewaterAntimony by GFAAArsenic by GFAAMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteSelenium in Various Matrices by GFAASilver by GFAAThallium by GFAAPolynuclear Aromatic HydrocarbonsTotal and Amenable CyanidesSulfate by Automated ColorimetryTotal Organic Carbon in Water and WasteStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupParticle-Size Analysis of Soils

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusINSTOR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 360 of 515

Superfund Intermountain Waste Oil Refinery

160.1 2320 2540-C 300(A) 300(B) 310.1 353.2 353.3 415.1 8015B 8260B 8270C(W) 9045B 9045D ICP-AES ILM04.0 ILM04.1 ILM05 ILM05.3 OLC03 OLM04.2 TNRR1005 TO-15

Procedure Id

USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA INTRMTN USEPA INTRMTN INTRMTN INTRMTN INTRMTN INTRMTN INTRMTN INTRMTN INTRMTN

Procedure Source

Filterable Residue - TDSAlkalinity in Water by TitrationTotal Dissolved Solids in WaterInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionTotal Organic Carbon by CombustionNon-Halogenated Organics Using GC/FIDVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MSSoil and Waste pHSoil and Waste pH (SW846-9045D)Inductively Coupled PlasmaILM04.0ILM04.1ILM05ILM05.3OLC03CLP Organic Low/Medium Concentration Waters and SoilsTotal Petroleum HydrocarbonsVOCs collected in canisters

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusINTRMTN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 361 of 515

Iowa Volunteer Water Monitoring Program

CHEMPHYS

Procedure Id

IOWATER

Procedure Source

IOWATER Chemical/Physical Assessment

Procedure Name

Active

StatusIOWATER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 362 of 515

Iowa Tribe of Oklahoma

120.1 6020 IT_QAPP

Procedure Id

USEPA USEPA IOWATROK

Procedure Source

ConductanceInductively Coupled Plasma - Mass Spec.Quality Assurance Project Plans (QAPP)

Procedure Name

ActiveActiveActive

StatusIOWATROK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 363 of 515

Iron Mountain Mine Superfund Site

120.1 130.1 130.2 150.1 160.1 160.2 200.7(W) 213.2 220.2 310.1 375.4 415.2 6010A 7000A(FLAA) 7131A 7210 7211 7950 9060 ANSP DFG DFG/DIESELHORSTDFG/KESWICK DFG/L-027-95 DFG/L-028-95 DFG/L-029-95 DFG/L-030-95 DFG/SAC RIVER INTERNAL TMCO

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT IRONMT

Procedure Source

ConductanceTotal HardnessTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSMetals in Water by ICP-AESCadmium by GFAACopper by GFAAAlkalinity by TitrationSulfate by Turbidimetric DeterminationLow Level Total Organic Carbon in WaterICP SpectroscopyAtomic Absorption - FLAACadmium by GFAACopper by FLAACopper by GFAAZinc by FLAATotal Organic Carbon in Water and WasteAcademy of Natural Sciences of PhiladelphiaDFGDFG DieselhorstDFG KeswickDFG/L-027-95DFG/L-028-95DFG/L-029-95DFG/L-030-95DFG/Sac RiverIron Mountain Mine Analytical ProcedureTme Mountain Copper Co., LTD

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusIRONMT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 364 of 515

Jamestown SKlallam Tribe

QAPP

Procedure Id

JSKTRIBE

Procedure Source

Quality Assurance Project Plan

Procedure Name

Active

StatusJSKTRIBE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 365 of 515

KARUK Department of Natural Resources (DNR)

QAPP

Procedure Id

KARUKDNR

Procedure Source

Karuk Quality Assurance Project Plan

Procedure Name

Active

StatusKARUKDNR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 366 of 515

Region 6 Katrina Emergency Monitoring Data

1664A 200.2 200.7 245.1 2540G 335.3 335.4 350.1 350.2 350.3 3500-CR D 365.1 365.2 405.1 420.1 420.2 515.4 6010B 7000A 7196A 8015B 8015M 8081A 8082 8141 8151A 8260B 8270 9071M 9213D 9222 B 9222 D ABN 8270 A_VOC_IH BACT BIOLOGY E. COLIB_ECOLI B_TOTCOL CN E160.2 E1665A E200.7 E245.1 E335.3

Procedure Id

KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6

Procedure Source

1664A200.2200.7Metals Mercury 245.12540 G (Dry Weight)335.3335.4350.1350.2350.33500-Cr D365.1365.2405.1420.1420.2P/P 515.4 HerbicidesMetals ICP 6010B7000A7196A8015B8015MP/P NOLA 8081A8082P/P NOLA 81418151A8260B82709071M9213D9222 B9222 DABN 8270A_VOC_IHBACTBiology E. ColiBiology E. ColiBiology Total ColiformCNE160.2E1665AE200.7E245.1E335.3

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusKATRINA6

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 367 of 515

Region 6 Katrina Emergency Monitoring Data

E350.1 E353.2 E415.1 E624 E625 EPA 200.7 EPA 608 HACH 8000 ICP 200.7 M5210 B MERCURY 245.1 N5506 O&G 1664A P/P 515.4 HERB P/P NOLA 8081A P/P NOLA 8141 PHEN REAC_SOP 1805 SM-3500CR_D SM5210B SW-846 6010B SW-846 7470A SW-846 7471A SW-846 8015B SW-846 8015BGASSW-846 8015MOD SW-846 8081A SW-846 8082 SW-846 8151A SW-846 8260B SW-846 8270C SW6010B SW7470A SW8260B TOTAL COLIFORM TPH 1664A VOA 8260

Procedure Id

KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6 KATRINA6

Procedure Source

E350.1E353.2E415.1E624E625EPA 200.7EPA 608HACH 8000ICP 200.7M5210 BMercury 245.1N5506O&G 1664AP/P 515.4 HerbP/P NOLA 8081AP/P NOLA 8141PHENREAC_SOP 1805SM-3500CR_DSM5210BSW-846 6010BSW-846 7470ASW-846 7471ASW-846 8015BSW-846 8015B GASSW-846 8015ModSW-846 8081ASW-846 8082SW-846 8151ASW-846 8260BSW-846 8270CSW6010BSW7470ASW8260BTotal ColiformTPH 1664AVOA 8260

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusKATRINA6

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 368 of 515

Katrina Response Special Projects

2540G 335.3 350.3 3500-CR D 365.1 415.1 420.2 8260B 8270 9071M 9213D 9222 B 9222D A2540G D2216 EPA 160.2 EPA 353.2 EPA 405.1 EPA160 HACH 8000 O&G 1664A SW-846 6010B SW-846 7470A SW-846 7471A SW-846 8015B SW-846 8081 SW-846 8081A SW-846 8082 SW-846 8151A SW-846 8270 SW-846 8720 SW-846_6010BICPSW-846_8015BGASSW846 6010 SW846 7470 SW846 7471 SW846 8121 SW846 8260 SW846 8270 TM-SOLID TPH 1664A

Procedure Id

KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ KATSPROJ

Procedure Source

2540 G (Dry Weight)335.3350.33500-Cr D365.1415.1420.28260B82709071M9213D9222 B9222DA2540GD2216EPA 160.2EPA 353.2EPA 405.1EPA160HACH 8000O&G 1664ASW-846 6010BSW-846 7470ASW-846 7471ASW-846 8015BSW-846 8081SW-846 8081ASW-846 8082SW-846 8151ASW-846 8270SW-846 8720SW-846_6010B ICPSW-846_8015B GASSW846 6010SW846 7470SW846 7471SW846 8121SW846 8260SW846 8270TM - SolidTPH 1664A

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusKATSPROJ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 369 of 515

Kaw Nation of Oklahoma

10029 10200-H 120.1 160.1 200.7(W) 200.8(W) 200.9 245.1 300(A) 310.1 350.2(A) 365.2 4500-P-E 5310-C 6010A 608 619 7470A 8081A(SNB) 8141A(W) 9222-D KAW_SOP

Procedure Id

KAWNATON APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA KAWNATON

Procedure Source

Kaw Standard Operating ProcedureChlorophyll a-b-c DeterminationConductanceFilterable Residue - TDSMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAMercury in Water by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen Using an ISEPhosphorus by Single Reagent ColorimetryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodICP SpectroscopyOrganochlorine Pesticides and PCBs by GCTriazine Pesticides in WastewaterMercury in Liquid Wastes by CVAAOrganochlorine Pesticides and PCBs by GCOrganophosphorus Compounds in WaterFecal Coliform Membrane Filter ProcedureKaw standard operating procedures

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusKAWNATON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 370 of 515

Kickapoo Tribe of Oklahoma Department of Environmental Progr

KICKAPOO_AP

Procedure Id

KICKAPOO

Procedure Source

Kickapoo Analytical Procedures

Procedure Name

Active

StatusKICKAPOO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 371 of 515

Keystone Watershed Montioring Network (Pennsylvania)

8156 ALKALINITY CHLOROPHYLL A

COND. METER HACH ALKALINITYHACH COLORIMETEHACH DO KIT HACH NO3 KIT HACH PO4 KIT HACH POCKET PALHACH S04 KIT HANNA PH LAMOTTE 1066 LAMOTTE 2117 LAMOTTE 3119 LAMOTTE 3119 N LAMOTTE 3354 LAMOTTE 3703 LAMOTTE 3976 LAMOTTE 5422 LAMOTTE 5860 LAMOTTE 6459 LAMOTTE THERM PH STRIPS SECCHI THERMOMETER TITRATOR TOTAL N TSS TURBIDITY YSI DO

Procedure Id

HACH KWMNDATA KWMNDATA

KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA KWMNDATA

Procedure Source

pH in WaterAlkalinity Test, Titration with Sulfuric Acid, DEP LabChlorophyll a Corrected for Pheophytin, National Standard,SpectrophotometerOakton Instruments Conducitivity Meter, ECTester LowHach Alkalinity Test Kit, Model AL-AP MG/L, Cat. No. 24443-01Hach Colorimeter, Model DR/850Hach Dissolved Oxygen Test Kit, Model OX-2P, Cat. No. 1469-00Hach Nitrate Test Kit, Model NI-14, Cat. No. 14161-33Hach Test Kit for Phosphate Model P0-24, Cat. No. 2250-01Hach Pocket Pal pH TesterHach Sulfate Test Kit, Model SF-1, Cat. No. 2251-00Hanna Pocket pH MeterWater TemperaturepH in WaterOrtho-phosphateNitrate-Nitrogen, using Lamotte 3119Nitrate-NitrogenLamotte Nitrate Wide Range CTA TesTabsLamotte Dissolved Oxygen TestabsLamotte Phosphorus TesTabsDissolved OxygenLamotte Wide Range pH Test Tabs, 6459Lamotte ThermometerpH in Water using pH stripsSecchi DiskThermometer for Water TemperatureHach Digital Titrator, Model 16900Total Nitrogen, DEP LaboratoryTotal Suspended SolidsTurbidityYSI 52 Dissolved Oxygen Meter

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusKWMNDATA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 372 of 515

Louisiana Dept of Env Quality Katrina Monitoring Data

245.1 3500-CR D 515.4 8081A 8260B 8270 9222 D ABN 8270 BACT E200.7 E245.1 E335.3 E624 E625 EPA 200.7 EPA 608 ICP 200.7

Procedure Id

LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT LADEQKAT

Procedure Source

Metals Mercury 245.13500-Cr DP/P 515.4 HerbicidesP/P NOLA 8081A8260B82709222 DABN 8270 Routine ListBACTE200.7E245.1E335.3E624E625EPA 200.7EPA 608Metals ICP 200.7

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusLADEQKAT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 373 of 515

LDEQ/Watershed Planning Division

110.2 120.1 130.2 160.1 160.2 1631 1632 1638 1639 1640 180.1 200.7_M 300(A) 300(B) 300_M 310.1 350.3 351.2 353.2 365.4 415.1 420.1 601 602 LDEQ-FMO UK_LAB

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA LADEQWPD LADEQWPD

Procedure Source

Color Analysis Using Platinum/CobaltConductanceTotal HardnessFilterable Residue - TDSNon-Filterable Residue - TSSMercury in Water by Oxidation, Purge and Trap, and CVAFSInorganic Arsenic in Water by Hydride Generation Quartz FurnaceTrace Elements in Water by ICP/MSTrace Elements in Water by GFAATrace Elements in Water by Chelation Preconcentration and ICP/MSTurbidity by NephelometryICP-AES For Trace Element AnalysisInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyDetermination of Anions by ICAlkalinity by TitrationAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterPurgeable Halocarbons in WastewaterPurgeable Aromatics in Wastewater by GCLDEQ - Field Collection ProceduresUnkown Lab Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusLADEQWPD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 374 of 515

City of Lakeland (Florida)

AMMONIA UN-ION120.1 130.2 2120-C 2540-C 2540-D 310.1 3111-B 3111-D 3113-B 350.1 353.2 365.1 365.4 4500-H 4500-NH3(G) 9222-B 9222-D CHLA - 4.3.1 EPA 5.1

NITROGEN OXYGEN PHYTOPLANKTON SECCHI TEMP TSI TURB

Procedure Id

LAKELAND USEPA USEPA APHA APHA APHA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA APHA APHA APHA LAKELAND LAKELAND

LAKELAND LAKELAND LAKELAND LAKELAND LAKELAND LAKELAND LAKELAND

Procedure Source

Un-ionized AmmoniaConductanceTotal HardnessColor in Water by SpectrophotometryTotal Dissolved Solids in WaterTotal Suspended Solids in WaterAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by FLAA- Direct Nitrous Oxide-Acetylene FlameMetals in Water by GFAAAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block DigestionpH in WaterAmmonia in Water Using Automated Phenate MethodStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter Procedurechlorophyl "a" analysisMacroinvertebrate Field and Laboratory Methods for Evaluating theBiological Integrity of Surface WatersTotal NitrogenDissolved OxygenPhytoplankton AnalysisSecchi DepthTemperatureTrophic State IndexTurbidity

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

StatusLAKELAND

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 375 of 515

Littleton/Englewood Wastewater Treatment Plant (Colorado)

10129 120.1 130.2 160.1 160.2 170.1 180.1 200.7(W) 200.8(W) 200.9 2320 245.1 2510 300_M 350.1 350.3 351.1 360.1 415.1 4500-H 4500-NH3(F) 4500-NO2(B) 4500-NO3(F) 4500-O-G 5210-B 8000 8001(A1) 8038 8190 8195 8507 9222-D COLILERT COLILERT FLOW UNKNOWN

Procedure Id

LEWWTP USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA HACH HACH HACH HACH HACH HACH APHA IDEXX LEWWTP LEWWTP LEWWTP

Procedure Source

Hach Method for Organic CarbonConductanceTotal HardnessFilterable Residue - TDSNon-Filterable Residue - TSSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationMercury in Water by CVAAConductivity in WaterDetermination of Anions by ICAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryDissolved Oxygen Using an ISETotal Organic Carbon by CombustionpH in WaterAmmonia in Water Using Phenate MethodNitrite in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Membrane Electrode Method5-Day Biochemical Oxygen DemandChemical Oxygen DemandTotal, Fecal and E. Coli ColiformAmmonia Nitrogen in WaterTotal Phosphorus in WaterDetermination of TurbidityNitrite in WaterFecal Coliform Membrane Filter ProcedureColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliColilertFlowUnknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusLEWWTP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 376 of 515

Little River Band of Ottawa Indians

10200-H 130.1 150.1 160.1_M 160.2_M 170.1 180.1 2340 2540-C 310.1 325.2 351.2 353.1 360.1 365.1 9050

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationTotal HardnesspHTotal Dissolved SolidsTotal Suspended SolidsTemperatureTurbidity by NephelometryHardness in Water by EDTA TitrationTotal Dissolved Solids in WaterAlkalinity by TitrationChloride by Colorimetric Analysis IITotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetrySpecific Conductance

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusLRBOI

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 377 of 515

Lower Sioux Indian Community (MN)

180.1 353.2 365.1 4500-NOR(B) 9222-D COLILERT D1293(B)

Procedure Id

USEPA USEPA USEPA APHA APHA IDEXX ASTM

Procedure Source

Turbidity by NephelometryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Kjeldahl Nitrogen in WaterFecal Coliform Membrane Filter ProcedureColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.colipH of Water By Routine Measurement

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

StatusLSIOUX

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 378 of 515

Little Traverse Bay Bands of Odawa Indians

10200-H 2540-D 325.2 351.2 353.1 365.1

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationTotal Suspended Solids in WaterChloride by Colorimetric Analysis IITotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusLTBBWATR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 379 of 515

LummiNation (Washington)

10200-H 150.1 160.2_M 160.4 1652 1664 170.1 180.1 2320 2340 245.2 2510 2520-B 2520-D 2550 300(A) 3111-B 350.1 351.2 353.2 360.1 360.2 365.1 376.2 405.1 410.4 415.1 4500-O-G 5540-C 6010B 6020 8015B 8260B 9050 9050A 9222-D 9253 D5413(A) D6503 D888(B)

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA APHA APHA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA ASTM ASTM ASTM

Procedure Source

Chlorophyll a-b-c DeterminationpHTotal Suspended SolidsVolatile ResidueOil and GreaseExtractable Material in Oil and GreaseTemperatureTurbidity by NephelometryAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury by CVAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodSalinity in Water- Algorithm of Practical SalinityTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyMetals in Water by FLAA- Direct Air-Acetylene FlameAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by ColorimetrySulfide by Colorimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Organic Carbon by CombustionTotal Dissolved Oxygen by Membrane Electrode MethodAnionic Surfactants in Water as MBASInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Non-Halogenated Organics Using GC/FIDVolatile Organics by CGC/MSSpecific ConductanceSpecific ConductanceFecal Coliform Membrane Filter ProcedureChloride in Water and Waste by TitrationWater Levels Using Nonrecording DevicesStandard Test Method for Enterococci in Water Using EnterolertDissolved Oxygen by Instrumental Probe

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusLUMMINSN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 380 of 515

Region 8 Superfund: East Macos Watershed

ILM05 ILM05.3

Procedure Id

MACOS MACOS

Procedure Source

ILM05ILM05.3

Procedure Name

ActiveActive

StatusMACOS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 381 of 515

Makah Tribe (Washington)

QAPP

Procedure Id

MAKAH

Procedure Source

Quality Assurance Project Plan

Procedure Name

Active

StatusMAKAH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 382 of 515

Montana Bureau of Mines and Geology

PEBBLE

Procedure Id

MBMG

Procedure Source

Pebble Count

Procedure Name

Active

StatusMBMG

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 383 of 515

Muscogee (Creek) Nation

150.1 160.1 180.1 310.1 325.2 350.1 353.2 375.4 4500-P-E

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA

Procedure Source

pHFilterable Residue - TDSTurbidity by NephelometryAlkalinity by TitrationChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetrySulfate by Turbidimetric DeterminationPhosphorus in Water by Colorimetry- Ascorbic Acid Method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMCNCREEK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 384 of 515

Maryland Dept. of the Environment Dredging Ambient Data

116 180 181 182 183 184 185 186 23 24 25 26 27 28 30 304 305 306 307 308 309 31 310 311 312 313 314 315 316 317 32 33 34 35 36 37 38 39 40 41 42 43 44 45

Procedure Id

MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01

Procedure Source

Organic MethodsBoxCore Sampling-Standard Sedimentological ProceduresChromium in sedimentsCopper in sedimentsIron in sedimentsManganese in sedimentsNickel in sedimentsZinc in sedimentsArsenic (As) in Sediments/tissueArsenic (As) in waterCadmium (Cd) in sediments/tissue/sestonCadmium (Cd) in sediments/tissue/sestonCadmium (Cd) in waterChromium (Cr) in sediments/tissueChromium (Cr) in Tissue/SestonChromium (Cr) in estuarine bottom sedimentsCopper (Cu) in estuarine bottom sedimentsIron (Fe) in estuarine bottome sedimentsManganese (Mn) in estuarine bottom sedimentsNickel (Ni) in estuarine bottom sedimentsZinc (Zn) in estuarine bottom sedimentsMercury (Hg) in tissue/sedimentChromium (Cr) in estuarine bottom sedimentsCopper (Cu) in estuarine bottom sedimentsIron (Fe) in estuarine bottome sedimentsManganese (Mn) in estuarine bottom sedimentsNickel (Ni) in estuarine bottom sedimentsZinc (Zn) in estuarine bottom sedimentsCadmium (Cd) in estuarine bottom sedimentsLead (Pb) in estuarine bottome sedimentsMercury (Hg) in waterNickel (Ni) in tissue/sedimentNickel (Ni) in tissue/sedimentNickel (Ni) in waterSelenium (Se) in tissue/sedimentLead (Pb) in tissue/sediment/sestonLead (Pb) in tissue/sedimentLead (Pb) in waterIron (Fe) in tissue/sediment/sestonTin (Sn) in tissue/sedimentTin (Sn) in tissue/sedimentTin (Sn) in waterManganese (Mn) in tissue/sedimentManganese (Mn) in tissue/sediment

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEDAT01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 385 of 515

Maryland Dept. of the Environment Dredging Ambient Data

46 47 48 49 50 51 52 53 56 57

58

59

67 206.3 206.5 213.2 218.1 218.2 220.1 220.2 239.2 243.1 243.2 245.5 249.1 249.2 282.2 289.1 289.2

Procedure Id

MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01 MDEDAT01

MDEDAT01

MDEDAT01

MDEDAT01 USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Manganese (Mn) in waterZinc (Zn) in tissue/sedimentZinc (Zn) in tissue/sedimentZinc (Zn) in waterCopper (Cu) in tissue/sedimentCopper (Cu) in tissue/sedimentCopper (Cu) in tissue/sedimentPesticides in tissue/sedimentSurficial Sampling - Standard Sedimentological ProceduresBox Cores Sampling - Standard Sedimentological Procedures 0 - 5Centimeter DepthBox Cores Sampling - Standard Sedimentological Procedures 5 - 10Centimeter DepthBox Cores Sampling Standard Sedimentological Procedures 10 - 15cmSeleniumArsenic by HYDAAArsenic Digestion for HYDAACadmium by GFAAChromium by FLAAChromium by GFAACopper by FLAACopper by GFAALead by GFAAManganese by FLAAManganese by GFAAMercury in Sediment by CVAANickel by FLAANickel by GFAATin by GFAAZinc by FLAAZinc by GFAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

ActiveSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSuspSusp

StatusMDEDAT01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 386 of 515

Maryland Dept. of the Environment Toxics Data

1631 200.1 531.1 608.2 CARB-UM METHODS 1638 NITR-UM PAH-006 PCB-003 TDN=CALC

Procedure Id

USEPA USEPA USEPA USEPA MDEDAT03 MDEDAT03 MDEDAT03 USEPA USEPA MDEDAT03

Procedure Source

Mercury in Water by Oxidation, Purge and Trap, and CVAFSMetals in Marine Waters by ICP/MSN-Methylcarbamates in Water by HPLCOrganochlorine Pesticides in WastewaterCarbon in WaterTrace metalsNitrogen in WaterPolycyclic Aromatic Hydrocarbons in WaterPCBs in WaterTotal Dissolved Nitrogen-Calculated

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEDAT03

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 387 of 515

MD Dept. Environment In House Water Data

10200-H 120.1 150.1 160.2 160.3 160.4 160.5 170.1 180.1 200.7(W) 202.1 213.1 215.1 236.1 242.1 2510 2520-B 2520-C 2540-E 258.1 273.1 300(A) 305.1 310.1 310.1_M 350.1 351.2 353.2 360.1 365.1 365.4 370.1 375.2 405.1 415.1 415.2 440(S) 4500-NO3(C) 4500-O-G 4500-SI(F) 4500-SO4(B) 5310-B 6040-C 9222-B

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Chlorophyll a-b-c DeterminationConductancepHNon-Filterable Residue - TSSTotal ResidueVolatile ResidueSettleable MatterTemperatureTurbidity by NephelometryMetals in Water by ICP-AESAluminum by FLAACadmium by FLAACalcium by FLAAIron by FLAAMagnesium by FLAAConductivity in WaterSalinity in Water- Electrical Conductivity MethodSalinity in Water- Density MethodFixed and Volatile Solids in WaterPotassium by FLAASodium by FLAAInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAlkalinity by TitrationAlkalinity in Water by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate in Water by Colorimetry5 Day Biochemical Oxygen DemandTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterDetermination of Carbon and NitrogenNitrate in Water by Ion ChromatographyTotal Dissolved Oxygen by Membrane Electrode MethodSilica in Water by Automated ColorimetrySulfate in Water by Ion ChromatographyTotal Organic Carbon by Combustion-Infrared MethodOrganics in Water by Purge and Trap GCStandard Total Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEDAT04

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 388 of 515

MD Dept. Environment In House Water Data

9222-D DEPTH-F01 E. COLI ECOC F01 MISC_CALC PC-CALC PN-CALC PN/PC PP/PIP REACTIVE AL SEC-F01 SONDE TDN-CALC TDN/TDP TIDE-F01 TITRATION_ANC TN TP-CALC WEATHER-F01

Procedure Id

APHA MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04 MDEDAT04

Procedure Source

Fecal Coliform Membrane Filter ProcedureDepthE. Coli DeterminationEnterococci DeterminationInstantaneous StreamflowMiscellaneous Calculations for NutrientsCalculated Particulate CarbonCalculated Particulate NitrogenParticulate Nitrogen and CarbonParticulate PhosphorusReactive Aluminum in WaterSecchi DepthHydrolab DataloggerTotal Dissolved Nitrogen - CalculatedTotal Dissolved Nitrogen and PhosphorusTides and CurrentsANC TirtrationTotal NitrogenCalculated Total PhosphorusWeather Conditions

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEDAT04

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 389 of 515

Maryland Department of Natural Resources Data

EPA SEC. 19.0

Procedure Id

MDEDAT05

Procedure Source

pH

Procedure Name

Active

StatusMDEDAT05

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 390 of 515

Private Groups,/Local Subdivision Data

100.1 MDE

Procedure Id

MDEDAT06 MDEDAT06

Procedure Source

pHField Office procedures

Procedure Name

ActiveActive

StatusMDEDAT06

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 391 of 515

Maryland Dept. of the Environment Shellfish Data

3.2-B

Procedure Id

APHA

Procedure Source

Coliforms in Seawater and Shellfish

Procedure Name

Active

StatusMDEDAT07

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 392 of 515

Maryland Department Of Environment Beaches Data

COLIQUANT ENTQUANT SONDE TIDE-F01

Procedure Id

MDEDAT08 MDEDAT08 MDEDAT08 MDEDAT08

Procedure Source

Colilert QuantitrayEnterolert QuantitrayHydrolab DataloggerTides and Currents

Procedure Name

ActiveActiveActiveActive

StatusMDEDAT08

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 393 of 515

Maryland Dept. of the Environment Risk Assessment Data

200.11 243.1_M 6010B 617 630 630.1 680 8260A COMAR HERL_020

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MDEDAT09 USEPA

Procedure Source

Metals in Fish Tissue by ICP-AESManganese by FLAAInductively Coupled Plasma AESOrganohalide Pesticides and PCBsDithiocarbamate Pesticides in WastewaterDithiocarbamate Pesticides in WaterPesticides and PCBsVolatile Organics in Waste by CGC/MS08.02.13PCBs in Adipose Tissue

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEDAT09

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 394 of 515

MD Dept. of the Environment Private Pier Aquaculture Program

9222-D

Procedure Id

APHA

Procedure Source

Fecal Coliform Membrane Filter Procedure

Procedure Name

Active

StatusMDEDAT10

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 395 of 515

Montana DEQ - Water Quality Division

10018 10200-H 10200-I 10300-C 1050(A) 110.1 120.1 150.1 160.1 160.2 160.2_M 1631 170.1 180.1 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 2130 215.2 2320 2340 245.1 245.1_M 245.2 2510 2540-C 2540-D 2540-E 300(A) 300(B) 310.1 310.2 325.2 325.3 335.3 335.4 350.1 3500-K-D 3500-NA(D) 351.1 351.2 351.3(A)

Procedure Id

HACH APHA APHA APHA MDEQ-WQ USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA APHA APHA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA

Procedure Source

Total and Fecal Coliforms, E. Coli, P/AChlorophyll a-b-c DeterminationDetermination of Biomass (Standing Crop)Periphyton Sample AnalysisAnion - Cation BalanceColor by Calculating ADMI ValuesConductancepHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsMercury in Water by Oxidation, Purge and Trap, and CVAFSTemperatureTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAATurbidity in WaterCalcium by EDTA Titrimetric AnalysisAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAMercury in Water by Manual CVAAMercury by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyAlkalinity by TitrationAlkalinity by Colorimetric AnalysisChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationTotal Cyanide by Colorimetric AnalysisCyanide by Semi-Automated ColorimetryAmmonia Nitrogen by ColorimetryPotassium in Water by Flame PhotometrySodium in Water by Flame PhotometryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by Titration

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEQ-WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 396 of 515

Montana DEQ - Water Quality Division

351.3(B) 351.3(C) 353.2 365.1 365.2 365.4 375.2 375.3 405.1 446.0

4500-CL(B) 4500-CL(I) 4500-NH3(G) 4500-NO3(E) 4500-NO3(F) 4500-NOR(C) 4500-P-E 4500-P-F

4500-SO4(E) 5310-B 5310-C 5310-D 6010A 6010B 6020 7470A 7471A 8015B 8082(S) 8270D(W) 9222-D BAR-PRESSURE CN-ANALYSIS

COLILERT FLOW-ESTIMATED FLOW-METER FLOW-STAFF GAGEFLOW-VISUAL ESTHARD-CALC I2600(S) ICAP-SCAN LECO

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MDEQ-WQ

APHA APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MDEQ-WQ APHA MDEQ-WQ MDEQ-WQ

IDEXX MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ USDOI/USGS MDEQ-WQ MDEQ-WQ

Procedure Source

Total Kjeldahl Nitrogen - NesslerizationTotal Kjeldahl Nitrogen - PotentiometricNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by ColorimetrySulfate by Gravimetric Determination5 Day Biochemical Oxygen DemandChlorophylls and Pheopigments in Phytoplankton bySpectrophotometryResidual Chlorine in Water by Titration- Iodometric Method IResidual Chlorine by Iodometirc Electrode TechniqueAmmonia in Water Using Automated Phenate MethodNitrate in Water- Cadmium ReductionNitrate in Water- Automated Cadmium ReductionTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfate by Turbidimetric AnalysisTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Ultraviolet Oxidation MethodTotal Organic Carbon in Water- Wet-Oxidation MethodICP SpectroscopyInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Mercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteNon-Halogenated Organics Using GC/FIDPCBs as Aroclors by Capillary Column GCSemivolatile Organic Compounds in Water by GC/MSFecal Coliform Membrane Filter ProcedureBarometric Pressure from Field MeterCarbon and Nitrogen Content of Benthic and Floating AlgaeSamplesColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliFlow Estimated by Float MethodFlow from Field MeterFlow from Staff GageFlow Visually EstimatedHardness Calculated from Mg and Ca laboratory determinationsPhosphorus in Solids by ColorimetryMetals Scan via Inductively Coupled Argon Plasma SpectroscopyLECO

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEQ-WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 397 of 515

Montana DEQ - Water Quality Division

NONE P-ANALYSIS PEBBLE PERIPHYTONCOUNTPHY-PROD-CALC ROSGENPEBBLE SAR-CALC TDG-METER TDS-METER TN-CALC UNKNOWN USEPA-7473 USEPA-8021B USGS I 1030

Procedure Id

MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ MDEQ-WQ

Procedure Source

No Field/Lab Analysis PerformedAshing Method for Total PhosphateWolman Pebble Count - Substrate CharacterizationPeriphyton AnalysisLight and Dark Bottle Technique for Phytoplankton ProductivityRosgen Pebble CountSodium Adsorption Ratio CalculationTotal Dissolved Gas Field MeterTotal Dissolved Solids - meter reading - calculated from conductivityTotal Nitrogen, TN - SUM of TKN + NO3 + NO2Unknown Method or ProcedureMercury in solidsAromatic and Halogenated Volatiles by Gas ChromatographyUSGS I 1030

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMDEQ-WQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 398 of 515

Maine Department of Environmental Protection

10200-H 1631 2130 245.2 2530-C 2550 325.2 350.1 353.2 353.4 365.1 365.5 5210-B 5310-B 9050 973.49(E) B6660 D1067(A) D1292 D4183(A) D5389 D888(B) NITRO-16

Procedure Id

APHA USEPA APHA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA AOAC USDOI/USGS ASTM ASTM ASTM ASTM ASTM USDOC/NOAA

Procedure Source

Chlorophyll a-b-c DeterminationMercury in Water by Oxidation, Purge and Trap, and CVAFSTurbidity in WaterMercury by CVAAFloatable Oil and Grease in WaterTemperature of Water by ThermometerChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDetermination of Nitrite and NitratePhosphorus by ColorimetryOrthophosphate in Water by Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon by Combustion-Infrared MethodSpecific ConductanceNitrogen (Ammonia) in WaterBiomass/Chlorophyll Ratio in PeriphytonAcidity or Alkalinity of WaterOdor in WaterTotal Recoverable Organic PhosphorusOpen-Channel Flow Measurement by Acoustic Velocity MeterDissolved Oxygen by Instrumental ProbeTotal Kjehdahl Nitrogen

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMEDEP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 399 of 515

SUPERFUND MIDVALE RAILYARD

ILM04.1 ILM05.3 OLC03.2 OLM04 OLM04.2

Procedure Id

MIDVALE MIDVALE MIDVALE MIDVALE MIDVALE

Procedure Source

ILM04.1ILM05.3OLC03.2OLM04OLM04.2

Procedure Name

ActiveActiveActiveActiveActive

StatusMIDVALE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 400 of 515

Minnesota Pollution Control Agency

10027 10029

10200-H 110.2 110.3 1103.1

1103_1 120.1 130.2 150.1 150.2 160.1 160.2 160.3 160.4 1600

1603

1631 180.1 200.7(W) 200.8(W) 2120-B 2130 2130-B 2320 2340 2510 2510 253.2 2540-B 2540-C 2540-D 2540-E 2540-F 2540-G 2550 300(A) 305 310.1 310.2 3111-B

Procedure Id

HACH HACH

APHA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA

USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA NIOSH APHA USEPA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA APHA

Procedure Source

Fecal Coliforms, MPN (sludges)m-ColiBlue24 Method of the Determination of Total Coliforms and E.coliChlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltColor by Spectrophotometric AnalysisEscherichia coli in Water by Membrane Filtration Using membrane-Thermotolerant E. coli Agar (mTEC)E. coli in Water by Membrane FiltrationConductanceTotal HardnesspHpH by Continuous MonitoringFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueEnterococci in Water by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)Escherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Mercury in Water by Oxidation, Purge and Trap, and CVAFSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSColor in Water by Visual ComparisonTurbidity in WaterNephelometric MethodAlkalinity in Water by TitrationHardness in Water by EDTA Titration1-Octanethiol by GC/FPDConductivity in WaterPalladium by GFAATotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterSettleable Solids in WaterTotal, Fixed and Volatile SolidsTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyEmissions of Volatiles in WasteAlkalinity by TitrationAlkalinity by Colorimetric AnalysisMetals in Water by FLAA- Direct Air-Acetylene Flame

Procedure Name

ActiveActive

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 401 of 515

Minnesota Pollution Control Agency

3113-B 325.1 325.2 325.3 350.1 350.2(A) 350.3 351.1 351.2 351.3(A) 352.1 353.1 353.2 353.2_M 353.3 354.1 360.1 365.1 365.2 365.3 365.4 370.1 375.2 375.4 410.2 410.4 4110-B 415.1 415.2_M 4500-CL(B) 4500-CL-(B) 4500-CL-(C) 4500-CL-(E) 4500-H 4500-NH3(C) 4500-NH3(D) 4500-NH3(E) 4500-NH3(F) 4500-NH3(G) 4500-NH3(H) 4500-NO3(D) 4500-NO3(E) 4500-NO3(F) 4500-NO3(H)

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Metals in Water by GFAAChloride by Colorimetric Analysis IChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate and Nitrite by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionDissolved Silica by ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric DeterminationLow Level Chemical Oxygen DemandChemical Oxygen Demand by ColorimetryAnions in Water by Ion ChromatographyTotal Organic Carbon by CombustionTotal Organic Carbon in WaterResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Titration- Argentometric MethodChloride in Water by Titration- Mercuric Nitrate MethodChloride in Water by Colorimetry- Automated Ferricyanide MethodpH in WaterAmmonia in Water by Titrimetric MethodAmmonia in Water by Selective Electrode MethodAmmonia in Water by Selective Electrode Method (Known Addition)Ammonia in Water Using Phenate MethodAmmonia in Water Using Automated Phenate MethodAmmonia in Water - Flow Injection AnalysisNitrate in Water Using an ISENitrate in Water- Cadmium ReductionNitrate in Water- Automated Cadmium ReductionNitrate in Water- Automated Hydrazine Reduction

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 402 of 515

Minnesota Pollution Control Agency

4500-NOR(B) 4500-NORGD 4500-P-C

4500-P-E 4500-P-F

4500-S2(D) 4500-SI(D) 4500-SI(F) 4500-SO4(B) 5210-B 5220-D 524.2 5310-C 5910-B 6010B 6020 7471A 8000 8021A(ELCD) 8038 8048 8051 8074(B) 8156 8160 8190 8195 8221 8225 9221-C

9221-D 9221-E

9221-F 9222-B 9222-D 9223-B 9230-C APHA 1002G APHA 2340-B APHA 2340-C APHA 390-A

Procedure Id

APHA MNPCA1 APHA

APHA APHA

APHA APHA APHA APHA APHA APHA USEPA APHA APHA USEPA USEPA USEPA HACH USEPA HACH HACH HACH HACH HACH HACH HACH HACH HACH HACH APHA

APHA APHA

APHA APHA APHA APHA APHA MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

Total Kjeldahl Nitrogen in WaterNitrogen, Total, by Block Digestion and Flow Injection AnalysisPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetryPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfide in Water by SpectrophotometrySilica in Water by Spectrophotometry- Molybdosilicate MethodSilica in Water by Automated ColorimetrySulfate in Water by Ion Chromatography5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Colorimetry- Closed RefluxPurgeable Organics in Water by CGC/MSTotal Organic Carbon in Water- Ultraviolet Oxidation MethodUV - Absorbing Organic CompoundsInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Mercury in Solid or Semisolid WasteChemical Oxygen DemandHalogenated and Aromatic VolatilesAmmonia Nitrogen in WaterReactive Phosphorus in WaterSulfate in WaterTotal, Fecal and E. Coli ColiformpH in WaterConductivity in Water by Direct MeasurementTotal Phosphorus in WaterDetermination of TurbidityAlkalinity by Buret TitrationChloride by TitrationEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Bacterial Density- MPN DeterminationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueEscherichia coli, Multi-tube Fermentation TechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Membrane Filter TechniqueChlorophyll a, Monochromatic by SpectrometryHardness Calculation MethodHardness by EDTA TitrationHardness Calculation Method

Procedure Name

ActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 403 of 515

Minnesota Pollution Control Agency

APHA 420A&417G APHA 4500-N-C APHA 4500-NO3 APHA 4500-NORGEAPHA 4500NH3(H)ASTM D3731-87 AWRESRCH NT031

AXYS PFCS CHUBCK_FC CLMP-CONDSUIT-1CLMP-SD-1 COLILERT COLILERT-18 CSMP-CONDSUIT-1CSMP-RAIN-24H CSMP-RAIN-Y/N CSMP-TD CSMP-TTUBE100 CSMP-TTUBE60 D1125(A) D3590(A) D5089 D515(A) D516 DO PROBE DO SATURATION DO WINKLER EPA SW846 3510CETS-8-044.0 FLD ALK FLD BAROMETRIC FLD CONDUCTANCEFLD PH FLD SALINITY FLD STAGE EST FLD STR FLOW 1 FLD STR FLOW 2 FLD STR FLOW 3 FLD STR FLOW 4 FLD STR FLOW DMFLD STR FLOW HD

FLD STR FLOW HU

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 IDEXX IDEXX MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 ASTM ASTM ASTM ASTM ASTM MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

MNPCA1

Procedure Source

Total Kjeldahl Nitrogen in WaterTotal Nitrogen in WaterNitrogen, Nitrate (NO2) + Nitrate (NO3) as NTotal Kjeldahl Nitrogen in WaterNitrogen, AmmoniumChlorophyll-a and Pheophytin-aNitrogen, Total, by Oxidizing Organic and Ammonium Nitrogen toNitrate and then Measuring NitratePerfluorinated Compounds (PFCs) by LC/MS/MSFecal ColiformCLMP Lake Condition & Suitability AssessmentsCLMP Secchi Disk TransparencyColilert Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliCSMP Stream Condition & Suitability AssessmentsCSMP Rainfall, 24-hourCSMP Rainfall Event Observed (0=No, 1=Yes)CSMP Tape-down Measurement to Water SurfaceCSMP Transparency Tube, 100 cmCSMP Transparency Tube, 60 cmConductivity and Resistivity in WaterTKN by Ion Selective ElectrodeVelocity of Water,electromagnetic metersPhosphorus in Water by Colorimetric ReductionSulfate in Water by TurbidimeterDissolved Oxygen, Membrane Electrode MethodDissolved Oxygen SaturationDissolved Oxygen, Iodometric Method with Azide ModificationCaffeine by Separatory Funnel Liquid-Liquid ExtractionPerfluorobutanoic acid (PFBA) in water by direct injectionAlkalinity, Probe MethodBarometric pressureConductance, Specific - umhos at 25 deg CpH, Electrometric MethodSalinity, Probe MethodStream Water Level, Relative Visual ObservationStream Flow, Instantaneous, at Milestone SitesStream Flow, Instantaneous, Unknown MethodStream Flow, Instantaneous, MeasuredStream Flow, Instantaneous, Estimated from Established RatingStream Flow, Daily MeanStream Flow, Hydstra Daily Value, Computed from EstablishedRating CurveStream Flow, Hydstra Unit Value, Computed from EstablishedRating Curve

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 404 of 515

Minnesota Pollution Control Agency

FLD STR STAGE 1FLD STR STAGE 2FLD STR STAGE 3FLD STR STAGE 4FLD STR STAGE 5FLD STR STAGE 6FLD STR STAGE 7FLD STR STAGE 8FLD STR STAGE 9FLD STR STG 10 FLD TDS PROBE FLD TEMP FLD TTUBE120 FLD TURB FLD TURB PROBE FRONTIER-AS FRONTIER-HG FRONTIER-MTLS HACH 10020 HACH 8039 HACH COLOR HACH NO23 SPEC

I1540 I2540 I2601 I3765 LAB TEMP LEG_P00001 LEG_P00004 LEG_P00005 LEG_P00009 LEG_P00011 LEG_P00020 LEG_P00023 LEG_P00024 LEG_P00030 LEG_P00036 LEG_P00062 LEG_P00065 LEG_P00067 LEG_P00069 LEG_P00070 LEG_P00071

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

USDOI/USGS USDOI/USGS USDOI/USGS USDOI/USGS MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

Stream Stage, Relative Water Level at Milestone SitesStream Stage, Relative Water Level, Tape-Down MethodStream Stage, Relative Water Level, USGS GageStream Stage, Relative Water Level, Non-USGS GageStream Stage, Relative Water Level, Staff GageStream Stage, Relative Water Level, Wire WeightStream Stage, Relative Water Level, Automated Stage RecorderStream Stage, Relative Water Level, Pool/Tailwater ElevationStream Stage, Relative Water Level, Other MethodStream Stage, Relative Water Level, CSMPSolids, Total Dissolved, Probe MethodTemperature, waterTransparency Tube, 120 cmTurbidity, Nephelometric MethodTurbidity, Probe MethodArsenic by HG-AFSMercury by CV-AFSTrace Metals by ICP/MSNitrate, Chromotropic Acid MethodNitrate, Cadmium Reduction MethodApparent Color, Hach Color Wheel MethodNitrate and Nitrite, Total, Using Spectrophotometer VIS/UV 4000,Nitrate 2500 MethodNitrite-Nitrogen in Water by ColorimetryNitrite-Nitrogen in Water by ColorimetryOrthophosphate-Phosphorus by ColorimetryResidue by Evaporation and GravimetricLab sample temperatureX-SEC. LOC., HORIZ (FT. FROM R BANK LOOK UPSTR.)STREAM WIDTH (FEET)X-SEC. LOC., VERTICAL (PERCENT OF TOTAL DEPTH)X-SEC. LOC.(FT FROM LEFT BANK LOOKING DOWNSTRM)TEMPERATURE, WATER (DEGREES FAHRENHEIT)TEMPERATURE, AIR (DEGREES CENTIGRADE)SAMPLE WEIGHT IN POUNDSSAMPLE LENGTH IN INCHESLIGHT, INCIDENT, SUNLIGHT RADIATION INTENSITYWIND DIRECTION IN DEGREES FROM TRUE N (CLOCKWISE)ELEVATION, RESERVOIR SURFACE WATER IN FEETSTAGE, STREAM (FEET)TIDE STAGE (REFER TO APPENDIX FOR CODES)SEA WAVES(0=NONE;1=0-3";2=4-20";3=21-48";4=4-8')TURBIDITY, (JACKSON CANDLE UNITS)TURBIDITY HELLIGE (JACKSON CANDLE UNITS) JCU

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 405 of 515

Minnesota Pollution Control Agency

LEG_P00076 LEG_P00077 LEG_P00080 LEG_P00081 LEG_P00085 LEG_P00090 LEG_P00091 LEG_P00092 LEG_P00095 LEG_P00149 LEG_P00156 LEG_P00162 LEG_P00199 LEG_P00290 LEG_P00295 LEG_P00304 LEG_P00307 LEG_P00308 LEG_P00309 LEG_P00310 LEG_P00311 LEG_P00313 LEG_P00314 LEG_P00319 LEG_P00324 LEG_P00335 LEG_P00339 LEG_P00340 LEG_P00341 LEG_P00400 LEG_P00401 LEG_P00403 LEG_P00405 LEG_P00410 LEG_P00425 LEG_P00430 LEG_P00431 LEG_P00436 LEG_P00440 LEG_P00445 LEG_P00500 LEG_P00505 LEG_P00510 LEG_P00515

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

TURBIDITY,HACH TURBIDIMETER (FORMAZIN TURB UNIT)TRANSPARENCY, SECCHI DISC (INCHES)COLOR (PLATINUM-COBALT UNITS)COLOR,APPARENT(UNFILTERED SAMPLE) PLAT-COB UNITSODOR (THRESHOLD NUMBER AT ROOM TEMPERATURE)OXIDATION REDUCTION POTENTIAL (MILLIVOLTS)FLOW, MINIMUM OF FLOW RANGE CFSFLOW, MAXIMUM OF FLOW RANGE CFSSPECIFIC CONDUCTANCE (UMHOS/CM @ 25C)ALPHA EMITTING RADIUM ISOTOPES, DISSOLVED(PC/L)IS00CTYL 2,4,5-T,WHOLE WATER, UG/LSILVER, IN THE WHOLE WATER SAMPLE KILOGRAMS/BATCHLIGHT, DEPTH TO 50 PERCENT OF SURFACE LIGHT (FEET)OXYGEN,DISSOLVED,UPTAKE,LIGHT BOTTLE,IN 24HR MG/LOXYGEN, DISSOLVED ML/LBOD, 2 DAY, 20 DEG C MG/LBOD, NITROGEN INHIB.,DISS., 5 DAY, 20 DEG C MG/LBOD, NITROGEN INHIB.,TOTAL, 20 DAY, 20 DEG C MG/LBOD, NITROGEN INHIB.,DISS., 20 DAY, 20 DEG C MG/LBOD, 5 DAY, 20 DEG C MG/LBOD, DISSOLVED, 5 DAY MG/LBOD, DISSOLVED, 20 DAY, 20 DEG C MG/LBOD, NITROGEN INHIB.,TOTAL, 5 DAY, 20 DEG C MG/LBOD, ULTIMATE ALL STAGES, 20 DEG C MG/LBOD, 20 DAY, 20 DEG C MG/LCOD, .025N K2CR2O7 MG/LCOD, BOTTOM DEPOSITS, DRY WEIGHT MG/KGCOD, .25N K2CR2O7 MG/LCOD, DISSOLVED, .25N K2CR2O7 MG/LPH (STANDARD UNITS)CATIONS MINUS ANIONS MILLIEQUIVALENTSPH, LAB, STANDARD UNITS SUCARBON DIOXIDE (MG/L AS CO2)ALKALINITY, TOTAL (MG/L AS CACO3)ALKALINITY, BICARBONATE (MG/L AS CACO3)ALKALINITY, CARBONATE (MG/L AS CACO3)ALKALINITY TOATL FIELD, (MG/L AS CACO3)ACIDITY, MINERAL (METHYL ORANGE) (MG/L AS CACO3)BICARBONATE ION (MG/L AS HCO3)CARBONATE ION (MG/L AS CO3)RESIDUE, TOTAL (MG/L)RESIDUE, TOTAL VOLATILE (MG/L)RESIDUE, TOTAL FIXED (MG/L)RESIDUE, TOTAL FILTRABLE (DRIED AT 105C),MG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 406 of 515

Minnesota Pollution Control Agency

LEG_P00530 LEG_P00535 LEG_P00540 LEG_P00545 LEG_P00550 LEG_P00556 LEG_P00566 LEG_P00600 LEG_P00605 LEG_P00607 LEG_P00608 LEG_P00609 LEG_P00610 LEG_P00611 LEG_P00612 LEG_P00613 LEG_P00615 LEG_P00616 LEG_P00618 LEG_P00619 LEG_P00620 LEG_P00623 LEG_P00625 LEG_P00626 LEG_P00627 LEG_P00629 LEG_P00630 LEG_P00631 LEG_P00633 LEG_P00650 LEG_P00660 LEG_P00665 LEG_P00666 LEG_P00667 LEG_P00668 LEG_P00670 LEG_P00671 LEG_P00672 LEG_P00680 LEG_P00681 LEG_P00685 LEG_P00689 LEG_P00690 LEG_P00720

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

RESIDUE, TOTAL NONFILTRABLE (MG/L)RESIDUE, VOLATILE NONFILTRABLE (MG/L)RESIDUE, FIXED NONFILTRABLE (MG/L)RESIDUE, SETTLEABLE (ML/L)OIL & GREASE (SOXHLET EXTRACTION) TOTAL,REC.,MG/LOIL & GREASE (FREON EXTR.-GRAV METH) TOT,REC,MG/LIMCO NOS. 1,2,3,6, GPDNITROGEN, TOTAL (MG/L AS N)NITROGEN, ORGANIC, TOTAL (MG/L AS N)NITROGEN, ORGANIC, DISSOLVED (MG/L AS N)NITROGEN, AMMONIA, DISSOLVED (MG/L AS N)TOTAL AMMONIA NITROGEN, 30 DAY ,(MG/L AS N)NITROGEN, AMMONIA, TOTAL (MG/L AS N)NITROGEN, AMMONIA, BOTTOM DEPOSITS (MG/KG-N)Ammonia, Unionized, calculated as N, from Legacy STORETNITRITE NITROGEN, DISSOLVED (MG/L AS N)NITRITE NITROGEN, TOTAL (MG/L AS N)NITRITE NITROGEN, BOTTOM DEPOS. (MG/KG-N DRY WGT)NITRATE NITROGEN, DISSOLVED (MG/L AS N)Ammonia, Unionized, calculated as NH3, from Legacy STORETNITRATE NITROGEN, TOTAL (MG/L AS N)NITROGEN, KJELDAHL, DISSOLVED (MG/L AS N)NITROGEN, KJELDAHL, TOTAL, (MG/L AS N)NITROGEN,ORG. KJEL.,BOT. DEPOS. (MG/KG-N DRY WGT)NITROGEN KJELDAHL TOTAL BOTTOM DEP DRY WT MG/KGNITROGEN, ORGANIC KJELDAHL, TOTAL (MG/L AS N)NITRITE PLUS NITRATE, TOTAL 1 DET. (MG/L AS N)NITRITE PLUS NITRATE, DISS. 1 DET. (MG/L AS N)NITRITE PLUS NITRATE,BOT. DEPOS. (MG/KG-N DRY WT)PHOSPHATE, TOTAL (MG/L AS PO4)PHOSPHATE, ORTHO (MG/L AS PO4)PHOSPHORUS, TOTAL (MG/L AS P)PHOSPHORUS, DISSOLVED (MG/L AS P)PHOSPHORUS, SUSPENDED (MG/L AS P)PHOSPHORUS,TOTAL,BOTTOM DEPOSIT (MG/KG-P DRY WGT)PHOSPHORUS, TOTAL ORGANIC (MG/L AS P)PHOSPHORUS, DISSOLVED ORTHOPHOSPHATE (MG/L AS P)PHOSPHORUS, DISSOLVED HYDROLYZABLE (MG/L AS P)CARBON, TOTAL ORGANIC (MG/L AS C)CARBON, DISSOLVED ORGANIC (MG/L AS C)CARBON, TOTAL INORGANIC (MG/L AS C)CARBON, SUSPENDED ORGANIC (MG/L AS C)CARBON, TOTAL (MG/L AS C)CYANIDE, TOTAL (MG/L AS CN) MG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 407 of 515

Minnesota Pollution Control Agency

LEG_P00721 LEG_P00745 LEG_P00746 LEG_P00800 LEG_P00900 LEG_P00910 LEG_P00915 LEG_P00916 LEG_P00920 LEG_P00924 LEG_P00925 LEG_P00927 LEG_P00929 LEG_P00930 LEG_P00935 LEG_P00937 LEG_P00940 LEG_P00941 LEG_P00945 LEG_P00946 LEG_P00950 LEG_P00951 LEG_P00955 LEG_P00956 LEG_P00958 LEG_P00969 LEG_P00970 LEG_P00971 LEG_P00972 LEG_P00973 LEG_P00974 LEG_P00975 LEG_P00976 LEG_P00977 LEG_P00978 LEG_P01000 LEG_P01002 LEG_P01003 LEG_P01004 LEG_P01005 LEG_P01007 LEG_P01012 LEG_P01019 LEG_P01020

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

CYANIDE IN BOTTOM DEPOSITS (MG/KG AS CN DRY WGT)SULFIDE, TOTAL (MG/L AS S)SULFIDE, DISSOLVED (MG/L AS S)NITZSCHIA KUTZINGIANA HILSE (NO/LITER)HARDNESS, TOTAL (MG/L AS CACO3)CALCIUM (MG/L AS CACO3)CALCIUM, DISSOLVED (MG/L AS CA)CALCIUM, TOTAL (MG/L AS CA)MAGNESIUM (MG/L AS CACO3)MAGNESIUM IN BOTTOM DEPOS. (MG/KG AS MG DRY WGT)MAGNESIUM, DISSOLVED (MG/L AS MG)MAGNESIUM, TOTAL (MG/L AS MG)SODIUM, TOTAL (MG/L AS NA)SODIUM, DISSOLVED (MG/L AS NA)POTASSIUM, DISSOLVED (MG/L AS K)POTASSIUM, TOTAL MG/L AS K)CHLORIDE,TOTAL IN WATER MG/LCHLORIDE, DISSOLVED IN WATER MG/LSULFATE, TOTAL (MG/L AS SO4)SULFATE, DISSOLVED (MG/L AS SO4)FLUORIDE, DISSOLVED (MG/L AS F)FLUORIDE, TOTAL (MG/L AS F)SILICA, DISSOLVED (MG/L AS SI02)SILICA, TOTAL (MG/L AS SI02)SILICATE, UNFILTERED REACTIVE (MG/L SIO3 AS SI)CHRYSOTILE ASBESTOS FIBERS/LITERTREMOLITE AMPHIBOLE FIBERS/LITERHORNBLENDE AMPHIBOLE FIBERS/LITERAMBIGUOUS AMPHIBOLE FIBERS/LITERAMPHIBOLE ASBESTOS FIBERS/LITERACTINOLITE AMPHIBOLE FIBERS/LITERCUMMINGTON-GRUNERITE AMPHIBOLE FIBERS/LITERAMBIGUOUS ASBESTOS FIBERS/LITERNON-AMPHIBOLE NON-CHRYSOTILE ASBESTOS FIBERS/LITERARSENIC,TOTAL RECOVERABLE IN WATER AS AS UG/LARSENIC, DISSOLVED (UG/L AS AS)ARSENIC, TOTAL (UG/L AS AS)ARSENIC IN BOTTOM DEPOSITS (MG/KG AS AS DRY WGT)ARSENIC TOTAL IN FISH OR ANIMAL WET WT MG/KGBARIUM, DISSOLVED (UG/L AS BA)BARIUM, TOTAL (UG/L AS BA)BERYLLIUM, TOTAL (UG/L AS BE)CADMIUM (CD), BOTTOM DEPOSITS, TOTAL, WET WT,MG/KGBORON, DISSOLVED (UG/L AS B)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 408 of 515

Minnesota Pollution Control Agency

LEG_P01022 LEG_P01025 LEG_P01027 LEG_P01028 LEG_P01029 LEG_P01030 LEG_P01032 LEG_P01034 LEG_P01035 LEG_P01037 LEG_P01040 LEG_P01042 LEG_P01043 LEG_P01045 LEG_P01046 LEG_P01047 LEG_P01049 LEG_P01051 LEG_P01052 LEG_P01053 LEG_P01055 LEG_P01056 LEG_P01059 LEG_P01062 LEG_P01064 LEG_P01065 LEG_P01067 LEG_P01068 LEG_P01069 LEG_P01074 LEG_P01077 LEG_P01082 LEG_P01087 LEG_P01090 LEG_P01092 LEG_P01093 LEG_P01097 LEG_P01102 LEG_P01105 LEG_P01106 LEG_P01108 LEG_P01113 LEG_P01114 LEG_P01119

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

BORON, TOTAL (UG/L AS B)CADMIUM, DISSOLVED (UG/L AS CD)CADMIUM, TOTAL (UG/L AS CD)CADMIUM,TOTAL IN BOTTOM DEPOSITS (MG/KG,DRY WGT)CHROMIUM,TOTAL IN BOTTOM DEPOSITS (MG/KG,DRY WGT)CHROMIUM, DISSOLVED (UG/L AS CR)CHROMIUM, HEXAVALENT (UG/L AS CR)CHROMIUM, TOTAL (UG/L AS CR)COBALT, DISSOLVED (UG/L AS CO)COBALT, TOTAL (UG/L AS CO)COPPER, DISSOLVED (UG/L AS CU)COPPER, TOTAL (UG/L AS CU)COPPER IN BOTTOM DEPOSITS (MG/KG AS CU DRY WGT)IRON, TOTAL (UG/L AS FE)IRON, DISSOLVED (UG/L AS FE)IRON, FERROUS (UG/L AS FE)LEAD, DISSOLVED (UG/L AS PB)LEAD, TOTAL (UG/L AS PB)LEAD IN BOTTOM DEPOSITS (MG/KG AS PB DRY WGT)MANGANESE IN BOTTOM DEPOSITS (MG/KG AS MN DRY WGT)MANGANESE, TOTAL (UG/L AS MN)MANGANESE, DISSOLVED (UG/L AS MN)THALLIUM, TOTAL (UG/L AS TL)MOLYBDENUM, TOTAL (UG/L AS MO)TELLURIUM, TOTAL IN WHOLE WATER SAMPLE (UG/L)NICKEL, DISSOLVED (UG/L AS NI)NICKEL, TOTAL (UG/L AS NI)NICKEL, TOTAL IN BOTTOM DEPOSITS (MG/KG,DRY WGT)NICKEL, TOTAL IN FISH OR ANIMALS-WET WEIGHT MG/KGNICKEL,TOTAL RECOVERABLE IN WATER AS NI UG/LSILVER, TOTAL (UG/L AS AG)STRONTIUM, TOTAL (UG/L AS SR)VANADIUM, TOTAL (UG/L AS V)ZINC, DISSOLVED (UG/L AS ZN)ZINC, TOTAL (UG/L AS ZN)ZINC IN BOTTOM DEPOSITS (MG/KG AS ZN DRY WGT)ANTIMONY, TOTAL (UG/L AS SB)TIN, TOTAL (UG/L AS SN)ALUMINUM, TOTAL (UG/L AS AL)ALUMINUM, DISSOLVED (UG/L AS AL)ALUMINUM IN BOTTOM DEPOSITS (MG/KG AS AL DRY WGT)CADMIUM,TOTAL RECOVERABLE IN WATER AS CD UG/LLEAD,TOTAL RECOVERABLE IN WATER AS PB UG/LCOPPER,TOTAL RECOVERABLE IN WATER AS CU UG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 409 of 515

Minnesota Pollution Control Agency

LEG_P01132 LEG_P01142 LEG_P01143 LEG_P01145 LEG_P01147 LEG_P01149 LEG_P01152 LEG_P01170 LEG_P01200 LEG_P01501 LEG_P01503 LEG_P01505 LEG_P01519 LEG_P03501 LEG_P03503 LEG_P03505 LEG_P03520 LEG_P04225 LEG_P07000 LEG_P07017 LEG_P09501 LEG_P11501 LEG_P13501 LEG_P30192 LEG_P30295 LEG_P31501 LEG_P31503 LEG_P31504 LEG_P31505 LEG_P31506 LEG_P31507 LEG_P31613

LEG_P31615 LEG_P31616 LEG_P31625 LEG_P31633 LEG_P31639 LEG_P31664 LEG_P31673

LEG_P31679 LEG_P31680 LEG_P32101

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

MNPCA1 MNPCA1 MNPCA1

Procedure Source

LITHIUM, TOTAL (UG/L AS LI)SILICON, TOTAL (UG/L AS SI)SILICON, IN SILICATE (UG/L SIO3 AS SI)SELENIUM, DISSOLVED (UG/L AS SE)SELENIUM, TOTAL (UG/L AS SE)SELENIUM, TOTAL IN FISH OR ANIMALS WET WGT MG/KGTITANIUM, TOTAL (UG/L AS TI)IRON IN BOTTOM DEPOSITS (MG/KG AS FE DRY WGT)SELENIUM IN TERRESTRIAL SOIL DRY WEIGHT MG/KGALPHA, TOTALALPHA, DISSOLVEDALPHA, SUSPENDEDRADIATION, GROSS ALPHA, WHOLE WATER PC/LBETA, TOTALBETA, DISSOLVEDBETA, SUSPENDEDRADIATION,GROSS BETA UC/MLCATION AND ANION SUMMATION, QC CHECK % DIFFERNCETRITIUM (1H3),TOTAL (PICOCURIES/LITER)TRITIUM, TOTAL (TRITIUM UNITS)RADIUM 226, TOTALRADIUM 228, TOTALSTRONTIUM 90, TOTALMCPA, WATER, WHOLE, RECOVERABLE UG/LPROPACHLOR, WATER, WHOLE, RECOVERABLE, UG/LCOLIFORM,TOT,MEMBRANE FILTER,IMMED.M-ENDO MED,35CCOLIFORM,TOT,MEMBR FILTER,DELAYED,M-ENDO MED,35 CCOLIFORM,TOT,MEMBR FILTER,IMMED,LES ENDO AGAR,35CCOLIFORM,TOT,MPN,CONFIRMED TEST,35C (TUBE 31506)COLIFORM,TOT,MPN, CONFIRMED TEST, TUBE CONFIG.COLIFORM,TOT,MPN,COMPLETED TEST,35C (TUBE 31508)Fecal Coliform, Membrane Filter Agar Technique, from LegacySTORETFECAL COLIFORM,MPN,EC MED,44.5C (TUBE 31614)FECAL COLIFORM,MEMBR FILTER,M-FC BROTH,44.5 CFECAL COLIFORM, MF,M-FC, 0.7 UME.COLI,THERMOTOL,MF,M-TEC,IN SITU UREASE #/100MLENTEROCOCCI GROUP D,MF TRANS,M-E,EIA #/100MLDICLOFOP METHYL, WHOLE WATER UG/LFecal Streptococcus, Membrane Filter KF Agar Technique, fromLegacy STORETFECAL STREPTOCOCCI,MF M-ENTEROCOCCUS AGAR,35C,48HFECAL STREPTCOCCI,MF-KF BROTH,35C,4BH #/100 MLBROMODICHLOROMETHANE,WHOLE WATER,UG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 410 of 515

Minnesota Pollution Control Agency

LEG_P32102 LEG_P32103 LEG_P32104 LEG_P32105 LEG_P32106 LEG_P32209 LEG_P32210 LEG_P32211 LEG_P32212 LEG_P32214 LEG_P32218 LEG_P32219 LEG_P32230 LEG_P32730 LEG_P32731 LEG_P32732 LEG_P32733 LEG_P32734 LEG_P34203 LEG_P34208 LEG_P34223 LEG_P34233 LEG_P34245 LEG_P34250 LEG_P34301 LEG_P34311 LEG_P34323 LEG_P34371 LEG_P34379 LEG_P34384 LEG_P34391 LEG_P34406 LEG_P34413 LEG_P34418 LEG_P34423 LEG_P34445 LEG_P34464 LEG_P34472 LEG_P34475 LEG_P34480 LEG_P34488 LEG_P34496 LEG_P34501 LEG_P34506

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

CARBON TETRACHLORIDE,WHOLE WATER,UG/L1,2-DICHLOROETHANE,WHOLE WATER,UG/LBROMOFORM,WHOLE WATER,UG/LDIBROMOCHLOROMETHANE,WHOLE WATER,UG/LCHLOROFORM,WHOLE WATER,UG/LCHLOROPHYLL A UG/L FLUOROMETRIC CORRECTEDCHLOROPHYLL-A UG/L TRICHROMATIC UNCORRECTEDCHLOROPHYLL-A UG/L SPECTROPHOTOMETRIC ACID. METH.CHLOROPHYLL-B UG/L TRICHROMATIC UNCORRECTEDCHLOROPHYLL-C UG/L TRICHROMATIC UNCORRECTEDPHEOPHYTIN-A UG/L SPECTROPHOTOMETRIC ACID. METH.PHEOPHYTIN RATIO(OD 663)SPECTRO,BEFORE/AFTER ACIDCHLOROPHYLL A (MG/L)PHENOLICS, TOTAL, RECOVERABLE (UG/L)PHENOLICS IN BOTTOM DEPOSITS (MG/KG DRY WGT)PHENOLICS,DISSOLVED,UG/LPHENOLICS,SUSPENDED,UG/LPHENOLICS,TISSUE,WET WEIGHT,MG/KGACENAPHTHYLENE DRY WGTBOTUG/KGACENAPHTHENE DRY WGTBOTUG/KGANTHRACENE DRY WGTBOTUG/KGBENZO(B)FLUORANTHENE,SEDIMENTS,DRY WGT,UG/KGBENZO(K)FLUORANTHENE, DRY WT, SEDIMENT UG/KGBENZO-A-PYRENE DRY WGTBOTUG/KGCHLOROBENZENE TOTWUG/LCHLOROETHANE TOTWUG/LCHRYSENE DRY WGTBOTUG/KGETHYLBENZENE TOTWUG/LFLUORANTHENE DRY WGTBOTUG/KGFLUORENE DRY WGTBOTUG/KGHEXACHLOROBUTADIENE TOTWUG/LINDENO (1,2,3-CD) PYRENE DRY WGTBOTUG/KGMETHYL BROMIDE TOTWUG/LMETHYL CHLORIDE TOTWUG/LMETHYLENE CHLORIDE TOTWUG/LNAPHTHALENE DRY WGTBOTUG/KGPHENANTHRENE DRY WGTBOTUG/KGPYRENE DRY WGTBOTUG/KGTETRACHLOROETHYLENE TOTWUG/LTHALLIUM DRY WGTBOTMG/KGTRICHLOROFLUOROMETHANE TOTWUG/L1,1-DICHLOROETHANE TOTWUG/L1,1-DICHLOROETHYLENE TOTWUG/L1,1,1-TRICHLOROETHANE TOTWUG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 411 of 515

Minnesota Pollution Control Agency

LEG_P34511 LEG_P34516 LEG_P34524

LEG_P34529

LEG_P34536 LEG_P34541 LEG_P34546 LEG_P34551 LEG_P34559 LEG_P34566 LEG_P34571 LEG_P34576 LEG_P34668 LEG_P34669 LEG_P34670 LEG_P34671 LEG_P34674 LEG_P34680 LEG_P34682 LEG_P34685 LEG_P34686 LEG_P34688 LEG_P34689 LEG_P34690 LEG_P34691 LEG_P34696 LEG_P34699 LEG_P34704 LEG_P34754 LEG_P34764 LEG_P38260 LEG_P38477 LEG_P38578 LEG_P38680 LEG_P38697 LEG_P38710 LEG_P38740 LEG_P38787 LEG_P39023 LEG_P39032 LEG_P39053 LEG_P39055

Procedure Id

MNPCA1 MNPCA1 MNPCA1

MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

1,1,2-TRICHLOROETHANE TOTWUG/L1,1,2,2-TETRACHLOROETHANE TOTWUG/LBENZO(GHI)PERYLENE1,12-BENZOPERYLENDRYWGTBOTUG/KGBENZO(A)ANTHRACENE1,2-BENZANTHRACENDRYWGTBOTUG/KG1,2-DICHLOROBENZENE TOTWUG/L1,2-DICHLOROPROPANE TOTWUG/LTRANS-1,2-DICHLOROETHENE, TOTAL, IN WATER UG/L1,2,4-TRICHLOROBENZENE TOTWUG/L1,2,5,6-DIBENZANTHRACENE DRY WGTBOTUG/KG1,3-DICHLOROBENZENE TOTWUG/L1,4-DICHLOROBENZENE TOTWUG/L2-CHLOROETHYL VINYL ETHER TOTWUG/LDICHLORODIFUOROMETHANE TOTWUG/LPCB - 1248 WET WGTTISMG/KGPCB - 1260 WET WGTTISMG/KGPCB - 1016 TOTWUG/LPCB - 1016 WET WGTTISMG/KGALDRIN IN FISH TISSUE WET WEIGHT MG/KGCHLORDANE(TECH MIX & METABS),TISSUEWET WGTT,MG/KGENDRIN WET WGTTISMG/KGHEPTACHLOR EPOXIDE WET WGTTISMG/KGHEXACHLOROBENZENE WET WGTTISMG/KGPCB - 1242 WET WGTTISMG/KGPCB - 1254 WET WGTTISMG/KGTOXAPHENE WET WGTTISMG/KGNAPHTHALENE TOTWUG/LTRANS-1,3-DICHLOROPROPENETOTAL IN WATER UG/LCIS-1,3-DICHLOROPROPENE TOTAL IN WATER UG/L2,3,7,8-TETRACHLORODIBENZO-P-DIOXIN TISWETWTPG/GALDRIN, WET WEIGHT, TISSUE UG/GMETHYLENE BLUE ACTIVE SUBST. (DETERGENTS, ETC.)LINURON WATER, TOTUG/LPROPAZINE, TOTAL, WATER UG/LCHLOROTOLUENE,2-, TOTAL, WATER UG/LPCB, TOTAL, MISC MATRIX, WET WEIGHT UG/GBENTAZON WATER, TOTUG/LCHLORPYRIFOS-METHYL WATER, TOTUG/LETHALFLURALIN WATER, TOTUG/LPHORATE, FLAME IONIZATION, WATER SAMPLE (UG/L)PCP (PENTACHLOROPHENOL) WHOLE WATER SAMPLE UG/LALDICARB IN WHOLE WATER (UG/L)SIMAZINE IN WHOLE WATER (UG/L)

Procedure Name

ActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 412 of 515

Minnesota Pollution Control Agency

LEG_P39056 LEG_P39060 LEG_P39061 LEG_P39062 LEG_P39063 LEG_P39064 LEG_P39065 LEG_P39066 LEG_P39067 LEG_P39068 LEG_P39069 LEG_P39071 LEG_P39072 LEG_P39073 LEG_P39074 LEG_P39076 LEG_P39105 LEG_P39175 LEG_P39180 LEG_P39300 LEG_P39301 LEG_P39302 LEG_P39305 LEG_P39306 LEG_P39307 LEG_P39310 LEG_P39311 LEG_P39312 LEG_P39315 LEG_P39316 LEG_P39320 LEG_P39321 LEG_P39322 LEG_P39323 LEG_P39325 LEG_P39327 LEG_P39328 LEG_P39329 LEG_P39330 LEG_P39333 LEG_P39337 LEG_P39340 LEG_P39343 LEG_P39350

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

PROMETONE IN WHOLE WATER (UG/L)PCP (PENTACHLOROPHENOL) IN TISSUE WET WGT UG/GPCP (PENTACHLOROPHENOL) IN BOT DEPOS DRY SOL UG/KGCHLORDANE-CIS ISOMER,WHOLE WATER SAMPL (UG/L)CHLORDANE-CIS ISOMER,TISSUE WET WGT (UG/G)CHLORDANE-CIS ISOMER BOTTOM DEPOS (UG/KG DRY SOLCHLORDANE-TRNS ISOMER,WHOLE WATER SAMPL (UG/L)CHLORDANE-TRANS ISOMER,TISSUE WET WGT (UG/G)CHLORDANE-TRANS ISOMER,BOTTOM DEPOS(UG/KG DRY SLCHLORDANE-NONACHLOR,CIS ISO,WHOLE WTR (UG/L)CHLORDANE-NONACHLOR,CIS ISO,TISSUE WET WGT(UG/G)CHLORDANE-NONACHLOR,TPANS ISO,WHOLE WTR (UG/L)CHLORDANE-NONACHLOR,TRANS ISO,TISSUE,WET WT,UG/GCHLORDANE-NONACHLOR,TRANS ISO,BOTTOM DEP UG/KGBHC-ALPHA ISOMER,TISSUE UG/G WET WGTBHC-ALPHA ISOMER, BOTTOM DEPOS (UG/KG DRY SOL)PERCENT FAT HEXANE EXTRACTIONVINYL CHLORIDE-WHOLE WATER SAMPLE-UG/LTRICHLOROETHYLENE-WHOLE WATER SAMPLE-UG/LP,P' DDT IN WHOLE WATER SAMPLE (UG/L)P,P' DDT IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)P P DDT IN TISSUE WET WGT (UG/G)O,P' DDT IN WHOLE WATER SAMPLE (UG/L)O,P' DDT IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)O P DDT IN TISSUE WET WGT (UG/G)P,P' DDD IN WHOLE WATER SAMPLE (UG/L)P,P' DDD IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)P P DDD IN TISSUE WET WGT (UG/G)O,P' DDD IN WHOLE WATER SAMPLE (UG/L)O,P' DDD IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)P,P' DDE IN WHOLE WATER SAMPLE (UG/L)P,P' DDE IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)P,P'-DDE IN TISSUE WET WGT MG/KGP P DDE IN TISSUE, FAT BASIS (UG/G)O,P DDD IN TISSUE WET WGT (UG/G)ORTHO PARA DDE IN WHOLE WATER SAMPLE (UG/L)O,P'DDE IN BOTTOM DEPOS (UG/KG DRY SOLIDS)O,P DDE IN TISSUE, WET WGT(UG/G)ALDRIN IN WHOLE WATER SAMPLE (UG/L)ALDRIN IN BOTTOM DEPOS. (UG/KILOGRAM DRY SOLIDS)ALPHA BENZENE HEXACHLORIDE IN WHOLE WATER SAMPGAMMA-BHC(LINDANE),WHOLE WATER,UG/LGAMMA-BHC(LINDANE),SEDIMENTS,DRY WGT,UG/KGCHLORDANE(TECH MIX & METABS),WHOLE WATER,UG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 413 of 515

Minnesota Pollution Control Agency

LEG_P39351

LEG_P39356 LEG_P39359 LEG_P39365 LEG_P39370 LEG_P39376 LEG_P39379 LEG_P39380 LEG_P39383 LEG_P39390 LEG_P39393 LEG_P39400 LEG_P39404 LEG_P39405 LEG_P39410 LEG_P39420 LEG_P39480 LEG_P39481 LEG_P39482 LEG_P39497 LEG_P39499 LEG_P39504 LEG_P39505 LEG_P39507 LEG_P39508 LEG_P39511 LEG_P39512 LEG_P39514 LEG_P39515 LEG_P39516 LEG_P39519 LEG_P39570 LEG_P39600 LEG_P39630 LEG_P39700 LEG_P39701 LEG_P39720 LEG_P39730 LEG_P39740 LEG_P39755 LEG_P39758 LEG_P39760 LEG_P39782

Procedure Id

MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

CHLORDANE(TECH MIX&METABS),SEDIMENTS,DRYWGT,UG/KGMETOLACHLOR(DUAL) IN WHOLE WATER UG/LDDT SUM ANALOGS IN SEDIMENT UG/KG DRY WEIGHTDDE IN WHOLE WATER SAMPLE (UG/L)DDT IN WHOLE WATER SAMPLE (UG/L)DDT SUM ANALOGS INTISSUE WET WGT BASISSUM OF ALL DDT,DDE& DDD VALUES IN WHL WATER SAMPDIELDRIN IN WHOLE WATER SAMPLE (UG/L)DIELDRIN IN BOTTOM DEPOS. (UG/KILOGRAM DRY SOL.)ENDRIN IN WHOLE WATER SAMPLE (UG/L)ENDRIN IN BOTTOM DEPOS. (UG/KILOGRAM DRY SOLIDS)TOXAPHENE IN WHOLE WATER SAMPLE (UG/L)DIELDRIN IN TISSUE WET WGT (UG/G)DIELDRIN IN TISSUE, FAT BASIS (UG/G)HEPTACHLOR IN WHOLE WATER SAMPLE (UG/L)HEPTACHLOR EPOXIDE IN WHOLE WATER SAMPLE (UG/L)METHOXYCHLOR IN WHOLE WATER SAMPLE (UG/L)METHOXYCHLOR IN BOTTOM DEPOSITS (UG/KG DRY SOL.)METHOXYCHLOR IN FISH - UG/KGPCB - 1242 IN FISH OR ANIMALS WET WGT UG/KGPCB - 1242 BOT. DEP.,PCB-SERIES DRY SOL UG/KGPCB - 1254 PCB SERIES WHOLE WATER SAMPLE UG/LPCB - 1254 IN FILT. FRAC. OF WAT. SAMPLE UG/LPCB - 1254 IN BOTTOM DEPOS. DRY SOLIDS UG/KGPCB - 1260 PCB SERIES WHOLE WATER SAMPLE UG/LPCB - 1260 IN BOTTOM DEPOS. DRY SOLIDS UG/KGPCB - 1254 IN FISH OR ANIMALS WET WGT UG/KGPCB - 1016 IN BOTTOM SEDIMENTS DRY WT UG/KGPCBS (MG/KG) FISH TISSUE MG/KGPCBS IN WHOLE WATER SAMPLE (UG/L)PCBS IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)DIAZINON IN WHOLE WATER SAMPLE (UG/L)METHYL PARATHION IN WHOLE WATER SAMPLE (UG/L)ATRAZINE(AATREX) IN WHOLE WATER SAMPLE (UG/L)HEXACHLOROBENZENE IN WHOLE WATER SAMPLE (UG/L)HEXACHLOROBENZENE IN BOT DEPOS (UG/KG DRY SOLIDS)PICLORAM IN WHOLE WATER SAMPLE (UG/L)2,4-D IN WHOLE WATER SAMPLE (UG/L)2,4,5-T IN WHOLE WATER SAMPLE (UG/L)MIREX, TOTAL (UG/L)MIREX, BOTTOM MATERIAL (UG/KG DRY SOLIDS)SILVEX IN WHOLE WATER SAMPLE (UG/L)LINDANE IN WHOLE WATER SAMPLE (UG/L)

Procedure Name

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 414 of 515

Minnesota Pollution Control Agency

LEG_P39783 LEG_P39785 LEG_P39810 LEG_P45570 LEG_P45636 LEG_P46123 LEG_P46313 LEG_P46317 LEG_P46491 LEG_P46502 LEG_P46570 LEG_P49490 LEG_P49701 LEG_P50040 LEG_P50050 LEG_P50060 LEG_P50086 LEG_P50284 LEG_P60050 LEG_P60100 LEG_P60150 LEG_P60200 LEG_P60300 LEG_P60350 LEG_P60370 LEG_P60990 LEG_P70299 LEG_P70300 LEG_P70301 LEG_P70311 LEG_P70314 LEG_P70318 LEG_P70320 LEG_P70322 LEG_P70348 LEG_P70507 LEG_P71825 LEG_P71870 LEG_P71875 LEG_P71885 LEG_P71890 LEG_P71900 LEG_P71901 LEG_P71921

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

LINDANE IN BOTTOM DEPOSITS (UG/KG DRY SOLIDS)GAMMA-BHC(LINDANE),TISSUE,WET WEIGHT,MG/KGCHLORDANE,GAMMA,IN WHOLE WATER SAMPLE (UG/L)PCBS IN ADIPOSE TISSUE (MG/KG)TURBIDITY, LAB MG/LIRON, FERROUS, AS FE MG/LPHORATE IN WHOLE WATER SAMPLE (UG/L)LASSO IN WHOLE WATER SAMPLE (UG/L)METHYL TERTIARY BUTYL ETHER(MTBE),TOTAL,WATER UG/LZOOPLANKTON, TOTAL COUNT /LITERHARDNESS, CA MG CALCULATED (MG/L AS CACO3)VISUAL OBSERVATION, SUSPENDED, WATER CODETRANSPARENCY, SECCHI DISK, WATER FTELEVATION OF WATER LEVEL WITH REF.TO MEAN SEA L FTFLOW, IN CONDUIT OR THRU A TREATMENT PLANT MGDCHLORINE, TOTAL RESIDUAL (MG/L)SETTLEABLE MATTER (ML/L/HR)MERCURY,METHYL-,WAT,UNFILTERED,RECOVERABLE NG/LALGAE, TOTAL (CELLS/ML)ALGAE, COCCOID BLUE-GREEN (CELLS/ML)ALGAE, FILAMENTOUS BLUE-GREEN (CELLS/ML)ALGAE, COCCOID GREEN (CELLS/ML)ALGAE, FLAGELLATE GREEN (CELLS/ML)ALGAE, FLAGELLATE OTHER (CELLS/ML)ALGAE, DIATOMS (CELLS/ML)ZOOPLANKTON OTHER (/LITER)SOLIDS, SUSP. - RESIDUE ON EVAP. AT 180 C (MG/L)RESIDUE,TOTAL FILTRABLE (DRIED AT 180C),MG/LSOLIDS, DISSOLVED-SUM OF CONSTITUENTS (MG/L)PH, CACO3 STABILITY (STANDARD UNITS)DACONIL(C8CL4N2) IN WATER UG/LSOLIDS, TOTAL, PERCENT OF WET SAMPLEMOISTURE CONTENT (PERCENT OF TOTAL WET WEIGHT)SOLIDS, VOLATILE, PERCENT OF TOTAL SOLIDSSOLIDS, SETTLEABLE ML/LPHOSPHORUS,IN TOTAL ORTHOPHOSPHATE (MG/L AS P)ACIDITY, TOTAL (MG/L AS H)BROMIDE (MG/L AS BR)HYDROGEN SULFIDE (MG/L)IRON (UG/L AS FE)MERCURY, DISSOLVED (UG/L AS HG)MERCURY, TOTAL (UG/L AS HG)MERCURY,TOTAL RECOVERABLE IN WATER AS HG UG/LMERCURY,TOT. IN BOT. DEPOS. (MG/KG AS HG DRY WGT)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 415 of 515

Minnesota Pollution Control Agency

LEG_P71930 LEG_P71936 LEG_P71937 LEG_P71938 LEG_P71939 LEG_P71940 LEG_P72017 LEG_P72018 LEG_P72019 LEG_P72109 LEG_P73010 LEG_P73540 LEG_P74010 LEG_P74020 LEG_P74995 LEG_P75980 LEG_P75981 LEG_P77004 LEG_P77015 LEG_P77018 LEG_P77034 LEG_P77093 LEG_P77119 LEG_P77128 LEG_P77134 LEG_P77135 LEG_P77166 LEG_P77168 LEG_P77170 LEG_P77173 LEG_P77222 LEG_P77223 LEG_P77224 LEG_P77226 LEG_P77342 LEG_P77350 LEG_P77353 LEG_P77443 LEG_P77562 LEG_P77596 LEG_P77613 LEG_P77651 LEG_P77652 LEG_P77699

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

MERCURY,TOTAL IN FISH OR ANIMAL-WET WEIGHT BASISLEAD,TOTAL IN FISH OR ANIMALS-WET WEIGHT BASISCOPPER,TOTAL IN FISH OR ANIMALS-WET WEIGHT BASISZINC,TOTAL IN FISH OR ANIMALS-WET WEIGHT BASISCHROMIUM,TOT IN FISH OR ANIMALS-WET WEIGHT BASISCADMIUM,TOTAL IN FISH OR ANIMAL-WET WEIGHT BASISSERIES CODE (BM WELL DATA)SYSTEM CODE (BM WELL DATA)DEPTH TO WATER LEVEL (FEET BELOW LAND SURFACE)DEPTH TO WATER LEVEL FROM A MEASURING POINT (FEET)ETHYL ETHER BY GAS CHROMATOGRAPH (MG/L)CARBMOTHACID,(1METHETH),S-(2,3DICL2PROP)ESTOTWUG/LIRON, TOTAL (MG/L AS FE)FLOW, PUMP OUT MGDANATOMY CODE (SEE APPENDIX FOR ANATOMY LIST)ATRAZINE,DE-ISOPROPYL-, WATER, TOTAL UG/LATRAZINE,DE-ETHYL-, WATER, TOTAL UG/LETHANOL WHOLE WATER,UG/LISOPROPYL ALCOHOL(C3H8O) WHOLE WATER SAMPLE UG/L1-PROPANOL(N-PROPYL ALCOHOL) WHOLE WATER,UG/L1-BUTANOL (N-BUTYL ALCOHOL) WHOLE WATER,UG/LCIS-1,2-DICHLOROETHYLENE WHOLE WATER,UG/LDICHLOROMONOFLUOROMETHANE WHOLE WATER,UG/LSTYRENE WHOLE WATER,UG/L1,3-DIMETHYLBENZENE(M-XYLENE) WHOLE WATER,UG/LO-XYLENE WHOLE WATER,UG/L2,3-DICHLOROPROPENE WHOLE WATER,UG/L1,1-DICHLOROPROPENE WHOLE WATER,UG/L2,2-DICHLOROPROPANE WHOLE WATER,UG/L1,3-DICHLOROPROPANE WHOLE WATER,UG/L1,2,4-TRIMETHYLBENZENE WHOLE WATER,UG/LISOPROPYLBENZENE WHOLE WATER,UG/LN-PROPYLBENZENE WHOLE WATER,UG/L1,3,5-TRIMETHYLBENZENE WHOLE WATER,UG/LN-BUTYLBENZENE WHOLE WATER,UG/LSEC-BUTYLBENZENE WHOLE WATER,UG/LTERT-BUTYLBENZENE WHOLE WATER,UG/L1,2,3-TRICHLOROPROPANE WHOLE WATER,UG/L1,1,1,2-TETRACHLOROETHANE WHOLE WATER,UG/LMETHYLENE BROMIDE WHOLE WATER,UG/L1,2,3-TRICHLOROBENZENE WHOLE WATER,UG/L1,2-DIBROMOETHANE WHOLE WATER,UG/L1,1,2-TRICHLORO-1,2,2-TRIFLUOROET*WHOLE WATER,UG/L4-CHLORO-O-TOLOXY ACETIC ACID (M*WHOLE WATER,UG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 416 of 515

Minnesota Pollution Control Agency

LEG_P77700 LEG_P77825 LEG_P78093 LEG_P78109 LEG_P78110 LEG_P78121 LEG_P78124 LEG_P78131 LEG_P78132 LEG_P78460 LEG_P78881 LEG_P78926 LEG_P79027 LEG_P80029 LEG_P80080 LEG_P80081 LEG_P80082 LEG_P80083 LEG_P80084 LEG_P80086 LEG_P80087 LEG_P80088 LEG_P80089 LEG_P80114 LEG_P80153 LEG_P80154 LEG_P80273 LEG_P81284 LEG_P81294 LEG_P81309 LEG_P81327 LEG_P81364 LEG_P81403 LEG_P81405 LEG_P81408 LEG_P81410 LEG_P81501 LEG_P81551 LEG_P81552 LEG_P81555 LEG_P81576 LEG_P81585 LEG_P81595 LEG_P81596

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

CARBARYL WHOLE WATER,UG/LALACHLOR WHOLE WATER,UG/LTRI(CHLOROETHYL)PHOSPHATE IN WATER UG/LALLYLCHLORIDE,TOTAL,WHOLE WATER SAMPLE UG/LDICHLOROACETONITRILE,TOT,WHOLE WATER SAMPLE UG/LP-XYLENE + O-XYLENE,TOTAL,WHOLE WATER SAMPLE UG/LBENZENE IN WATER (VOLATILE ANALYSIS) UG/LTOLUENE IN WHOLE WATER (VOLATILE ANALYSIS) UG/LP-XYLENE IN WHOLE WATER UG/LURANIUM 234+235+238, SUMMATION, WATER, WHOLE,PCI/LPHOSPHAMIDON (DIMECRON), WHOLE WATER UG/LFAT, PERCENT, IN TISSUE, WET WEIGHT %OCTACHLOR EPOXIDE IN FISH WET WGT MG/KGALPHA GROSS TOTAL AS URANIUM NATURAL PC/LBOD, CARBONACEOUS, 1 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 3 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 5 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 7 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 10 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 15 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 20 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 30 DAY, 20 DEG C MG/LBOD, CARBONACEOUS, 40 DAY, 20 DEG C MG/LCOLOR, CONCENTRATION AT WAVE LENGTH IN MG/LCARBON, ORGANIC, IN SEDIMENT (% AS C)SUSP. SEDIMENT CONCENTRATION-EVAP. AT 110C (MG/L)BOD, CARBONACEOUS, 25 DAY, 20 DEG C MG/LTRIFLURALIN(C13H16F3N3O4) WHOLE WATER SAMPLE UG/LDYFONATE(CU/H15OPS2) WHOLE WATER SAMPLE UG/LCARBONDISULFIDE(CS2) WHOLE WATER SAMPLE UG/LDICHLOROPROPANE WHOLE WATER SAMPLE UG/LRDX IN WHOLE WATER SAMPLE UG/LDURSBAN(CHLOROPYRIFOS)WHOLE WATER SAMPLE (UG/L)CARBOFURAN (EURADAN) WHOLE WATER SAMPLE UG/LMETRIBUZIN (SENCOR), WATER, WHOLE UG/LBUTYLATE (SUTAN),WHOLE WATER SAMPLE,UG/LPENTACHLOROETHANE WHL WATER SMPL UG/LXYLENE WHL WATER SMPL UG/LACETONE WHL WATER SMPL UG/LBROMOBENZENE WHL WATER SMPL UG/LDIETHYL ETHER WHL WATER SMPL UG/LETHYL ACETATE WHL WATER SMPL UG/LMETHYL ETHYL KETONE WHL WATER SMPL UG/LMETHYL-ISOBUTYL KETONE WHL WATER SMPL UG/L

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

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and Equipment Summary

Page 417 of 515

Minnesota Pollution Control Agency

LEG_P81607 LEG_P81614 LEG_P81666 LEG_P81757 LEG_P81888 LEG_P81894 LEG_P81896 LEG_P81897 LEG_P81903 LEG_P81984 LEG_P82005 LEG_P82028 LEG_P82032 LEG_P82033 LEG_P82051 LEG_P82076 LEG_P82079 LEG_P82088 LEG_P82093 LEG_P82368 LEG_P82369 LEG_P82407 LEG_P82408 LEG_P82410 LEG_P82545 LEG_P82546 LEG_P82559 LEG_P82584

LEG_P82586 LEG_P82587 LEG_P82614 LEG_P84005 LEG_P84007 LEG_P84008 LEG_P84014 LEG_P84015 LEG_P84100 LEG_P84168 LEG_P84169 LEG_P84170 LEG_P85795 LEG_UNKNOWN LK DEPTH BOTTOM

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

TETRAHYDROFURAN WHL WATER SMPL UG/LNUMBER OF INDIVIDUALS IN THE SAMPLEALUMINUM IN FISH TISSUE WET WEIGHT MG/KGCYANAZINE IN THE WHOLE WATER SAMPLE UG/LDISULFOTON IN WHOLE WATER SAMPLE UG/LEPTC (EPTAM) IN WHOLE WATER SAMPLE UG/LDDE TOTAL IN TISSUE WET WEIGHT MG/KGDDD TOTAL IN TISSUE WET WEIGHT MG/KGDEPTH OF BOTTOM OF WATER BODY @ SAMPLE SITE, FEETTOTAL SEDIMENT PARTICLE SIZE %COARSER THAN 8.00PHIPERCENT TOTAL CARBON(INORG.&ORG.) IN SED DRY WGTRATIO OF FECAL COLIFORM TO FECAL STREPTOCOCCI(CAL)CALCIUM - TOTAL UG/L (AS CA)MAGNESIUM - TOTAL UG/L(AS MG)AMIBEN (CHLORAMBEN) WHOLE WATER,UG/LEXPOSURE AREA (REPORTED IN SQUARE CM.)TURBIDITY,LAB NEPHELOMETRIC TURBIDITY UNITS, NTUTERBUFOS (COUNTER) TOTAL WHOLE WATER,UG/LPHYTOPLANKTON, TOTAL NVMBER/LITERCALCIUM DISSOLVED IN WATER AS CACO3 MG/LMAGNESIUM DISSOLVED AS CACO3 IN WATER MG/LFONOFOS IN FISH TISSUE (DYFONATE) WET WEIGHT MG/KGFONOFOS IN SEDIMENT (DYFONATE) DRY WEIGHT UG/KGPENOXALIN IN WHOLE WATER(PROWL) TOTAL UG/LWATER LEVEL RELATIVE TO MEAN SEA LEVEL (FEET)WATER LEVEL,DISTANCE FROM MEASURING POINT (FEET)HYDROCARBONS,VOLATILE, IN WATER TOTALUG/L3-HYDROXY CARBOFURAN, WATER,TOTALRECOVERABLE,UG/LALDICARB SULFOXIDE, WATER, TOTAL RECOVERABLE UG/LALDICARB SULFONE, WH WATER, TOTAL RECOVERABLE,UG/LDYFONATE (FONOFOS), WATER, TOTAL RECOVERABLE, UG/LFISH SPECIES CODE-FISH & WILDLIFE SERANATOMY ALPHA CODELIFE STYLE/HABITAT OF THEINDIVIDUALS IN THE SAMPLESPECIES SEX CODEAGE IN YEARS OF SPECIMEN COLLECTED YEARSSEX(1-MALE,2-FEMALE,3-MIXED,4-UNKNOWN) NUM CODEAVIAN SPECIES ALPHA CODE (BIRDS)MAMMALIAN ALPHA SPECIES CODEALPHA AGE TEXT CODEXYLENE, META & PARA, WATER, WHOLE UG/LLegacy STORET migration; analytical procedure not specifiedDepth, bottom

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 418 of 515

Minnesota Pollution Control Agency

MCES COD MCES DOC MCES FC MCES HARDNESS MCES TOC MCES VSS MDH001 MDH001D MDH002 MDH002C MDH003 MDH003_W MDH004 MDH005D MDH011D MDH012 MDH013B MDH014 MDH018 MDH019 MDH022G MDH023F MDH028D MDH030B MDH050B MDH058C MDH059C MDH060 MDH063C MDH064C MDH065 MDH067 MDH068 MDH069E MDH070C MDH073 MDH077C MDH078E MDH083G MDH095 MDH096G MDH097E MDH098 MDH099

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

Chemical Oxygen Demand, USEPA 410.4Dissolved Organic Carbon in WaterFecal Coliform, EPA 600/18-78-017Hardness in Water, APHA 2340-CTotal Organic Carbon in WaterSolids, Suspended Volatile, USGS 1-3767-78Solids, TotalSolids, TotalSolids, VolatileSolids, Total VolatileSolids, SuspendedSolids, Suspended, Whole Water AnalysisSolids, Suspended VolatileSolids, Total DissolvedTurbidityColorpHConductance at 25 degrees CentigradeAlkalinity, CarbonateAlkalinity, BicarbonateAlkalinity, TotalChloride, TotalSulfate, Total, TurbidimetricSilica, Reactive, TotalSilica, DissolvedPhosphorus, Total, Low LevelPhosphorus, TotalPhosphorus, DissolvedOrthophosphate, TotalAmmonia Nitrogen, TotalOrganic Nitrogen, TotalNitrite Nitrogen, TotalKjeldahl Nitrogen, TotalNitrate and Nitrite Nitrogen, TotalOrthophosphate, DissolvedNitrite Nitrogen, DissolvedAmmonia Nitrogen, DissolvedNitrate and Nitrite Nitrogen, DissolvedCarbonaceous Biochemical Oxygen Demand, 5 dayBiochemical Oxygen Demand, 20 day, TotalBiochemical Oxygen Demand, 5 day, TotalChemical Oxygen Demand, Hach Vial MethodTotal Organic CarbonDissolved Organic Carbon

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 419 of 515

Minnesota Pollution Control Agency

MDH152 MDH152C MDH154 MDH166 MDH194 MDH203 MDH204 MDH208F MDH209F MDH228 MDH239 MDH255F MDH257G MDH261 MDH262 MDH264 MDH293 MDH310A MDH311A MDH313A MDH355 MDH356 MDH402 MDH450 MDH451 MDH452 MDH465 MDH468 MDH498 MDH555 MDH614 MDH631 MDH793 MDH794 NRRI 4500-NORGDNRRI CHLA-PHEO P0002561 PRTCLESZ_0.063 PRWD_GAGE PRWD_GAGE-CLVRTPRWD_GAGE-DNSTRPRWD_GAGE-MID PRWD_GAGE-MPCA PRWD_GAGE-SALLI

Procedure Id

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

Iron, Total, High LevelIron in Water, Total, High LevelIron in Water, Dissolved, High LevelManganese, Total, High LevelZinc in Water, Total, High LevelVolatiles in Soil or Sediment, Percent, by GravimetryMoisture in Soil or Sediment, Percent, by GravimetryCalcium as CaCO3 SDWA, TotalMagnesium in Water, Total, as CACO3Molybdenum in Water by ICP/MS, Total, Low LevelHardness in Water, Ca + Mg, Total, as CACO3Potassium in Water, TotalSodium in Water, TotalWater Content in SedimentPhosphorus in Sediment, TotalChemical Oxygen Demand in SedimentSulfate, Total, Ion ChromatographyMF - Fecal ColiformMF - Escherichia ColiMF - Fecal StreptococcusMicrocystinSaxitoxinSVOCs in Water by GCMSChlorophyll A (H2O), field filteredPheophytin-A (H2O)Chlorophyll A (H2O), lab filteredVOCs in WaterVOCs in Water by GCMS (USEPA 524.2)VOCs in Water by GCMS (USEPA 8260B)Perfluorinated Compounds (PFCs) by LC/MS/MSBoron in Water by ICP-AES, TotalAluminum in Water, Total, High LevelMercury, TotalMercury, DissolvedNitrogen, Total, by Block Digestion and Flow Injection AnalysisChlorophyll-a and Pheophytin by SpectrometryPerfluoronated compounds (PFCs) by Exygen Protocol P0002561Particle Size, Percent Smaller than 0.063mmPelican River Watershed District Stream GaugePelican River Watershed District Stream Gauge - CulvertPelican River Watershed District Stream Gauge - DownstreamPelican River Watershed District Stream Gauge - MiddlePelican River Watershed District Stream Gauge - MPCAPelican River Watershed District Stream Gauge - Sallie at Dunton

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 420 of 515

Minnesota Pollution Control Agency

PRWD_GAGE-TAIL PRWD_GAGE-UPSTRQC10-107-04-1-C

QC10-107-06-1-CQC10-115-01-1-AQC10-115-01-1-CQC20-107-04-1B REDOX TDD USEPA 300.0 USEPA 8270D USGS I-4540-85 UW-MAD-HG WSLH-CAMG WSLH-HG WSLH-MTLS DUMMY

Procedure Id

MNPCA1 MNPCA1 MNPCA1

MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1 MNPCA1

Procedure Source

LocksPelican River Watershed District Stream Gauge - TailPelican River Watershed District Stream Gauge - UpstreamNitrate and Nitrite Nitrogen, Total, by QuikChem method 10-107-04-1-CAmmonia Nitrogen, Total, by QuikChem method 10-107-06-1-COrthophosphate, Total, by QuikChem method 10-115-01-1-APhosphorus, Total, by QuikChem method 10-115-01-1-CNitrogen, Total, by QuickChem method 20-107-04-1BOxidation-Reduction PotentialTape-down Distance Measurement to Water SurfaceInorganic Anions by Ion ChromatographySemivolatile Organic Compounds by GC/MSNitrogen, Total Nitrite by ASF diazotization and colorimetryMercury by CV-AFSCalcium and Magnesium by ICP/AESMercury by CV-AFSTrace Metals by ICP/MSDummy procedure to assign when SIM refuses a genuine procedure

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveSusp

StatusMNPCA1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 421 of 515

Minnesota Pollution Control Agency Biological Monitoring

DO PROBE FLD CONDUCTANCEFLD PH FLD TEMP MDH003 MDH005 MDH011D MDH012 MDH023F MDH028D MDH059C MDH068 MDH098 MDH251 MDH253 MDH450 MDH451

Procedure Id

MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB MNPCAB

Procedure Source

Dissolved Oxygen, Membrane Electrode MethodConductance, Specific - umhos at 25 deg CpH, Electrometric MethodTemperature , waterSolids, SuspendedSolids, Total DissolvedTurbidityColorChloride, TotalSulfate, Total, TurbidimetricPhosphorus, TotalKjeldahl Nitrogen, TotalTotal Organic CarbonCa as CaCO3 HL, Total, H2OMg as CaCO3 - HL, Total, H2OChlorophyll A (H2O), field filteredPheophytin-A (H2O)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCAB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 422 of 515

Minnesota Pollution Control Agency

4500-CL-(E) 4500-NO3(F) 524.2 BACTERIA FLD ALKALINITY FLD CHLORIDE FLD DO FLD IRON FE+2 FLD NH4-N FLD NO3-N FLD ORP FLD PH FLD SO4-S FLD SPEC COND FLD TEMP GENCHEM P0002561 PESTICIDE SEMIVOLATILE TRITIUM VOC

Procedure Id

APHA APHA USEPA MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP MNPCAP

Procedure Source

Chloride in Water by Colorimetry- Automated Ferricyanide MethodNitrate in Water- Automated Cadmium ReductionPurgeable Organics in Water by CGC/MSBacteria analysis by unspecified methodAlkalinity, Total, by Field Kit or MeterChloride by Field Kit or MeterDissolved Oxygen by Field Kit or MeterIron, Ferrous, Fe+2 by Field Kit or MeterNitrogen, Ammonium (NH4) as N, by Field Kit or MeterNitrogen, Nitrate (NO3) as N, by Field Kit or MeterOxidation Reduction Potential by Field Kit or MeterpH by Field Kit or MeterSulfur, Sulfate (SO4) as S, by Field Kit or MeterSpecific Conductance by Field Kit or MeterTemperature, Water, by Field Kit or MeterChemical analysis by unspecified methodPerfluoronated chemicals (PFCs) by Exygen Protocol P0002561Pesticide analysis by unspecified methodSemivolatile compound analysis by unspecified methodTritium analysis by unspecified methodVOC analysis by unspecified method

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMNPCAP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 423 of 515

Montana Department of Environmental Quality

10200-H 110.1 120.1 150.1 150.2_M 16 160.1 160.2 160.4 170.1 180.1 200.7(S) 200.7(W) 200.8(W) 200.9 202.1 202.1OR2\200.7 202.2 213.2 2130 215.1 218.5 220.1 220.1OR2\200.7 220.2 2320 236.1 236.1OR2\200.7 236.2 239.2 242.1 243.1 243.1OR2\200.7 243.2 245.1 245.2 249.1 249.1OR2\200.7 249.2 2540-C 2540-D 270.2 270.3 286.2

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MONT-DEQ USEPA USEPA APHA USEPA USEPA USEPA MONT-DEQ USEPA APHA USEPA MONT-DEQ USEPA USEPA USEPA USEPA MONT-DEQ USEPA USEPA USEPA USEPA MONT-DEQ USEPA APHA APHA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationColor by Calculating ADMI ValuesConductancepHpH in Industrial Waste MaterialsSulfur Emissions from Stationary SourcesFilterable Residue - TDSNon-Filterable Residue - TSSVolatile ResidueTemperatureTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAluminum by FLAAAluminum by AA Flame or Furnace 202.1 or 202.2 or 200.7 ICPAluminum by GFAACadmium by GFAATurbidity in WaterCalcium by FLAAHexavalent Chromium by GFAACopper by FLAACopper by AA Flame or Furnace 220.1 or 220.2 or 200.7 ICPCopper by GFAAAlkalinity in Water by TitrationIron by FLAAIron by AA - Flame or Furnace 236.1or 236.2 or ICP 200.7Iron by GFAALead by GFAAMagnesium by FLAAManganese by FLAAManganese by AA - Flame or Furnace 243.1 or 243.2 or 200.7 ICPManganese by GFAAMercury in Water by CVAAMercury by CVAANickel by FLAANickel by AA - Flame or Furnace 249.1 or 249.2 or ICP 200.7Nickel by GFAATotal Dissolved Solids in WaterTotal Suspended Solids in WaterSelenium by GFAASelenium by FLAAVanadium by GFAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMONT-DEQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 424 of 515

Montana Department of Environmental Quality

289.1 289.1OR2\200.7 289.2 300(A) 305.1 310.1 310.1_M 310.2 325.2 325.3\DIONEX 340.2 350.1 351.1 351.3(A) 352.1 353.1 353.2 360.1 365.1 365.4 375.2 375.3\DIONEX 376.2 405.1 410.1 413.1 415.1 420.1 4500-NH3(G) 4500-NO3(F) 4500-P-F

4500-SI(D) 4500-SO4(B) 505 508 515.1 524.2 525.1 531.1 5310-B 5310-D 552.1 6010A

Procedure Id

USEPA MONT-DEQ USEPA USEPA USEPA USEPA USEPA USEPA USEPA MONT-DEQ USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MONT-DEQ USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA

APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA

Procedure Source

Zinc by FLAAZinc by AA - Flame or Furnace 289.1 or 289.2 or 200.7 ICPZinc by GFAAInorganic Anions by Ion ChromatographyAcidity by Titration with a pH MeterAlkalinity by TitrationAlkalinity in Water by TitrationAlkalinity by Colorimetric AnalysisChloride by Colorimetric Analysis IIChloride by 325.3 Titration or Dionex - Ion ChromatographyFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionSulfate in Water by ColorimetrySulfate by 375.3 Gravimetric or Dionex - Ion ChromatographySulfide by Colorimetric Determination5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandTotal Recoverable Oil and GreaseTotal Organic Carbon by CombustionTotal Recoverable Phenolics in WaterAmmonia in Water Using Automated Phenate MethodNitrate in Water- Automated Cadmium ReductionPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSilica in Water by Spectrophotometry- Molybdosilicate MethodSulfate in Water by Ion ChromatographyOrganohalide Pesticides and PCB in WaterChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECDPurgeable Organics in Water by CGC/MSOrganics in Water by Gas ChromatographyN-Methylcarbamates in Water by HPLCTotal Organic Carbon by Combustion-Infrared MethodTotal Organic Carbon in Water- Wet-Oxidation MethodHaloacetic Acids in Water by GCICP Spectroscopy

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMONT-DEQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 425 of 515

Montana Department of Environmental Quality

6010B CA-215.1OR200.7CD-213.2OR200.7DO-001 FISH MEASURES HG-245.1OR245.2HISTORIC ICAPSCAN K-258.1OR200.7 MG-242.1OR200.7MT-FM-DO MT-FM-PH MT-FM-SAL MT-FM-SPC MT-FM-TEMP MT-FMO-FLOW MT-FMO-FLOW-ESTMT-PCLSCBMW NA-273.1OR200.7PB-239.2OR200.7PEBBLE PESTICIDIES RBP-FIELD SE-270.2OR270.3SEDIMENT STATION OBS TDS-METER TDS-SUM TEMP-001 UNKNOWN V-286.2OR200.7 WEATHER-001

Procedure Id

USEPA MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ MONT-DEQ

Procedure Source

Inductively Coupled Plasma AESCalcium by 215.1 Flame AA or 200.7 ICPCadmium by 213.2 AA - Furnace or 200.7 ICPField Method for Determination of Dissolved Oxygen, ProbeField Determination of Whole Fish Physical CharacteristicsMercury by AA - Cold vapor, manual or automated 245.1 or 245.2Historic Data Migrated from STOREASE; Procedure UnknownICAPSCANPotassium by 258.1 Flame AA or 200.7 ICPMagnesium by 242.1 Flame AA or 200.7 ICPDissolved Oxygen, Field Determination by Membrane ElectrodepH, Water, Field Determination by ProbeSalinity, Field Determination by ProbeSpecific Conductance, Field Determination, by ProbeTemperature, Water, Field Determination by ProbeFlow, Field Determination w/ Current MeterFlow, Field determination, EstimatedHistoric Coalstrip Well DataSodium by 273.1 Flame AA or 200.7 ICPLead by AA - Furnace 239.2 or 200.7Wolman Pebble Count - Substrate CharacterizationHerbicides and InsecticidesField RBP ProceduresSelenium by AA - Furnace or Hydride 270.2 or 270.3Field Sediment AnalysisField Station Visit Physical Direct Measurements and ObsTotal Dissolved Solids - meter reading - calculated from conductivityTDS-SUMField Determination of Water Temperature, ProbeUnknown Method or ProcedureVanadium by AA - Furnace 286.2 or 200.7 ICPField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMONT-DEQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 426 of 515

PPL Corporation (Montana)

150.1 160.2 180.1 200.7(W) 200.8(W) 2320 2540-C 2540-D 300(A) 350.1 353.2 365.1 4500-H 4500-N-D 8195 FLOW-STAFFGAGE HARD-CALC HYDROLAB PERIPHYTONCOUNT

Procedure Id

USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA APHA MONT-PPL HACH MONT-PPL MONT-PPL MONT-PPL MONT-PPL

Procedure Source

pHNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSAlkalinity in Water by TitrationTotal Dissolved Solids in WaterTotal Suspended Solids in WaterInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetrypH in WaterNitrogen Persulfate MethodDetermination of TurbidityFlow Determined by Staff GageHardness CalcationField Measurements Using the Hydrolab Datasonde 4Periphyton Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMONT-PPL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 427 of 515

Morongo Band of Mission Indians (CA)

QAPP

Procedure Id

MORONGO1

Procedure Source

Quality Assurance Project Plan

Procedure Name

Active

StatusMORONGO1

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 428 of 515

Marine Research

BENTHBIO BENTHCHEM CTD-VERT EFFCHEM EFFCOMP EFFGRAB EFFMEAS MET OCEAN SAEFFCOMP

SAEFFGRAB

SAEFFTRAV

SECCHI SURFZONE

Procedure Id

MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB MRSENVMB

MRSENVMB

MRSENVMB

MRSENVMB MRSENVMB

Procedure Source

Benthic Infaunal BiologyChemical Analysis of Benthic SedimentsCTD casts conducted in a vertical profiling modeSemiAnnual and Annual Effluent ChemistryEffluent Composite SampleEffluent Grab SampleEffluent MeasurementMeteorological ConditionsSea ConditionsChemical Analysis of SemiAnnual and Annual Effluent CompositeSamplesChemical Analysis of SemiAnnual and Annual Effluent GrabSamplesChemical Analysis of SemiAnnual and Annual Effluent Travel BlankSamplesSecchi depth in metersShoreline water samples collected for coliform analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

ActiveActive

StatusMRSENVMB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 429 of 515

Region 8 Superfund: Mount Olivet Cemetery Plume

OLM04

Procedure Id

MTOLIVET

Procedure Source

OLM04

Procedure Name

Active

StatusMTOLIVET

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 430 of 515

Montana Volunteer Water Quality Monitoring

BOD COLISCAN FLOW_ESTIMATED FLOW_METER FLOW_STAFFGAGE HACH_FIELD HARD_CALC LAMOTTE_FIELD PERIPHYTONCOUNTPH_POCKET

PH_STRIP PROBE TDS_CALC

TDS_METER TPN-4500-N_C TURBIDITY_METERUNKNOWN

Procedure Id

MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM

MTVOLWQM MTVOLWQM MTVOLWQM

MTVOLWQM MTVOLWQM MTVOLWQM MTVOLWQM

Procedure Source

Biological Oxygen DemandE coli and Total Coliform using ColiscanEstimation of flow by timed float and average cross-sectionFlow obtained from a field meterFlow, Determination from Staff GageHach field kit using color change or titrationHardness Calculated from Mg and Ca laboratory determinationsLaMotte field kit using color change or titration.Periphyton AnalysispH determination using Hach Pocket Pal, Oakton or other individualpH handheld meterpH determination using pH test stripsProbe or field meter.TDS calcuated from specfic conductance measurement using a TDSconstand default valueTDS determination using handheld probe.Persulfate Nitrogen MethodTurbidity using field colorimeter or turbidimeterUnknown Method or Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

ActiveActiveActiveActive

StatusMTVOLWQM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 431 of 515

Montana Watershed Data

10200-H 1050(A) 150.1 150.2 160.1 160.2 180.1 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 2130-B 2320 2340 245.1 2510 2540-C 2540-D 300(A) 310.1 350.1 351.1 351.2 353.2 365.1 365.4 446.0

4500-CL(B) 4500-CL-(F) 4500-NH3(G) 4500-NO3(F) 4500-NOR(C) 4500-P-E 4500-P-F

4500-SO4(B) 4500-SO4(E) 5310-D 6010B 6020 7471A B8020

Procedure Id

APHA MTWTRSHD USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA MTWTRSHD

APHA APHA APHA APHA APHA APHA APHA

APHA APHA APHA USEPA USEPA USEPA USDOI/USGS

Procedure Source

Chlorophyll a-b-c DeterminationAnion - Cation BalancepHpH by Continuous MonitoringFilterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAANephelometric MethodAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterInorganic Anions by Ion ChromatographyAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block DigestionChlorophylls and Pheopigments in Phytoplankton bySpectrophotometryResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Ion ChromatographyAmmonia in Water Using Automated Phenate MethodNitrate in Water- Automated Cadmium ReductionTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfate in Water by Ion ChromatographySulfate by Turbidimetric AnalysisTotal Organic Carbon in Water- Wet-Oxidation MethodInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Mercury in Solid or Semisolid WasteProductivity- Carbon-14 Light/Dark-Bottle Method for Phytoplankto

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActive

StatusMTWTRSHD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 432 of 515

Montana Watershed Data

CNEIL-CORE COLILERT-18 D1941 FLOW-ESTIMATED FLOW-METER FLOW-SEAMETRICSFLOW-STAFF GAGEHARD-CALC PAR-METER PEBBLE PERIPHYTONCOUNTSAL-CALC SAR-CALC TDS-CALC TEMPLOGGER TN-CALC TPN-4500-N_C UNKNOWN USEPA-446.0

Procedure Id

MTWTRSHD IDEXX ASTM MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD MTWTRSHD

Procedure Source

McNeil Core Sediment SamplerColilert-18 Quanti-Tray; MPN - Multi Tube, Multi Well for E.coliOpen Channel Flow Measurement by FlumeFlow, EstimatedFlow, Average Velocity times Cross Sectional AreaPipe Flow Measurement by Insertion Flow SensorFlow, Determination from Staff GageHardness Calculated from Mg and Ca laboratory determinationsSurface/Subsurface PAR MeterPebble CountPeriphyton AnalysisSalinity CalculationSodium Adsorption Ratio CalculationTotal Dissolved Solids CalculationTemperature LoggerTotal Nitrogen, TN - SUM of TKN + NO3 + NO2Persulfate Nitrogen MethodUnknown Method or ProcedureChlorophylls and Pheopigments in Phytoplankton bySpectrophotometry

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMTWTRSHD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 433 of 515

Metro Waste Water Reclamation District (Colorado)

10200-H 1103_1 120.1 130.2 150.1 160.1 170.1 180.1 200.7(W) 206.2 213.2 220.2 239.2 245.2 270.2 272.2 310.1 320.1 325.2 335.3 350.1 351.1 353.1 353.3 360.1 365.1 365.4 375.1 415.1 5210-B 9131 9221-E

9222-B C-008-1 USGS FLOW UNKNOWN

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA APHA

APHA USEPA MWRD MWRD

Procedure Source

Chlorophyll a-b-c DeterminationE. coli in Water by Membrane FiltrationConductanceTotal HardnesspHFilterable Residue - TDSTemperatureTurbidity by NephelometryMetals in Water by ICP-AESArsenic by GFAACadmium by GFAACopper by GFAALead by GFAAMercury by CVAASelenium by GFAASilver by GFAAAlkalinity by TitrationBromide by Titration with IodineChloride by Colorimetric Analysis IITotal Cyanide by Colorimetric AnalysisAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionDissolved Oxygen Using an ISEPhosphorus by ColorimetryTotal Phosphorus After Block DigestionSulfate by Colorimetry With ChloranilateTotal Organic Carbon by Combustion5-Day Biochemical Oxygen DemandTotal Coliform by Multiple Tube FermentationEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureTotal Suspended Solids in WaterUSGS Flow station records. Flow reportsunknown analytical procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveSusp

StatusMWRD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 434 of 515

Metropolitan Water Reclamation District of Greater Chicago

10200-H 1664 2130 2320 2500 2540-B 2540-C 2540-D 2550 2580 3112-B 3120 340.2 350.1 3500-CR(D) 351.2 353.2 365.4 375.4 420.1 4500-CL(D) 4500-CL-(B) 4500-CN(C) 4500-CN(E) 4500-CN(G) 4500-CN(I) 4500-H 4500-O-C 4500-SO4(F) 5210-B 5310-C 5310-D 9222-D

Procedure Id

APHA USEPA APHA APHA NIOSH APHA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Chlorophyll a-b-c DeterminationExtractable Material in Oil and GreaseTurbidity in WaterAlkalinity in Water by TitrationMethyl Ethyl Ketone by GC/FIDTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerOxidation-Reduction Potential of WaterMercury in Water by CVAAMetals in Water by ICPFluoride in Water Using an ISEAmmonia Nitrogen by ColorimetryTotal Hexavalent Chromium in WaterTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationTotal Recoverable Phenolics in WaterResidual Chlorine in Water by Titration- Amperometric MethodChloride in Water by Titration- Argentometric MethodCyanide in Water after DistillationCyanide in Water by ColorimetryCyanides Amenable to Chlorination after DistillationWeak Acid Dissociable Cyanide in WaterpH in WaterTotal Dissolved Oxygen by Titration- Azide ModificationSulfate in Water by Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Ultraviolet Oxidation MethodTotal Organic Carbon in Water- Wet-Oxidation MethodFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusMWRDSTOR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 435 of 515

EPA National Aquatic Resource Survey Data

160.2 180.1 206.2 213.2 215.1 239.2 242.1 258.1 270.2 273.1 289.1 289.2 300(A) 350.1 415.2 FTIS_LIPID I1250 ORG_FTIS_GCII

UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA NARS USDOI/USGS NARS

NARS

Procedure Source

Non-Filterable Residue - TSSTurbidity by NephelometryArsenic by GFAACadmium by GFAACalcium by FLAALead by GFAAMagnesium by FLAAPotassium by FLAASelenium by GFAASodium by FLAAZinc by FLAAZinc by GFAAInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryLow Level Total Organic Carbon in WaterLipids in FishColor in Water by Visual ComparisonOrganic Analysis of Fish by GC II, Analysis of Freeze-Dried FishTissue by LVI-GCUnknown Field/Lab Analytical Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

StatusNARS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 436 of 515

NEIARCD (Iowa)

1603

350.1 353.2 365.4 IMMUNOASSAY

Procedure Id

USEPA

USEPA USEPA USEPA NEIARCD

Procedure Source

Escherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Ammonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryTotal Phosphorus After Block DigestionUHL Immunoassay

Procedure Name

Active

ActiveActiveActiveActive

StatusNEIARCD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 437 of 515

Nooksack Indian Tribe

D4409

Procedure Id

ASTM

Procedure Source

Open-Channel Flow by RECM

Procedure Name

Active

StatusNOOKSACK

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 438 of 515

Region 8 Superfund: West North Temple Plume

ILM05 OLM04

Procedure Id

NTEMPLE NTEMPLE

Procedure Source

ILM05OLM04

Procedure Name

ActiveActive

StatusNTEMPLE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 439 of 515

Otoe Missouria Tribe of Oklahoma

150.1 160.1 180.1 325.3 350.1 352.1 353.3 354.1 365.2 375.4 OM-ALK OM-FLOW

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA O-MTRIBE O-MTRIBE

Procedure Source

pHFilterable Residue - TDSTurbidity by NephelometryChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetryNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by Single Reagent ColorimetrySulfate by Turbidimetric DeterminationOtoe-Missouria Alkalinity Analytical ProcedureOtoe-Missouria Flow Analytical Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusO-MTRIBE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 440 of 515

Oklahoma Conservation Commission

00-01 10200-H 1103_1 130.1 160.1 200.7(W) 2130 2320 2340 2510 2540-C 2540-D 2550 300(A) 300.7 325.2 350.1 350.2(A) 350.2(B) 351.2 351.3(A) 353.2 365.1 365.3 375.4 4500-CL(C) 4500-H 4500-NH3(C) 4500-NO2(B) 4500-NO3(B) 4500-NO3(D) 4500-NO3(E) 4500-NOR(B) 4500-O-G 4500-P-D 4500-P-E 4500-SO4(E) 6010A 9056 9222-D 9230-C AG-UNK AL-UNK AS-UNK

Procedure Id

USEPA APHA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA USEPA IL/SWSD USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA USEPA USEPA APHA APHA OKCONCOM OKCONCOM OKCONCOM

Procedure Source

Gross Alpha and Beta Activity in WaterChlorophyll a-b-c DeterminationE. coli in Water by Membrane FiltrationTotal HardnessFilterable Residue - TDSMetals in Water by ICP-AESTurbidity in WaterAlkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerInorganic Anions by Ion ChromatographyNa, NH4, Mg, K and Ca - IONCHRChloride by Colorimetric Analysis IIAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISEAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Two Reagent ColorimetrySulfate by Turbidimetric DeterminationResidual Chlorine in Water by Titration- Iodometric Method IIpH in WaterAmmonia in Water by Titrimetric MethodNitrite in Water by ColorimetryNitrate in Water by Ultraviolet SpectrophotometryNitrate in Water Using an ISENitrate in Water- Cadmium ReductionTotal Kjeldahl Nitrogen in WaterTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Stannous Chloride TitrationPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSulfate by Turbidimetric AnalysisICP SpectroscopyAnion Chromatography MethodFecal Coliform Membrane Filter ProcedureFecal Streptococcus and Enterococcus, Membrane Filter TechniqueLab's Analytical Method used for Silver analysis is unknownLab's Analytical Method used for Aluminum analysis is unknownLab's Analytical Method used for Arsenic analysis is unknown

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusOKCONCOM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 441 of 515

Oklahoma Conservation Commission

BA-UNK BE-UNK BT-AIRTEMP BT-CL BT-DO BT-NH3 BT-NO3 BT-P BT-PH BT-SECCHI BT-WTEMP CA-UNK CB-FISH CD-UNK CO-UNK CR-UNK CU-UNK FE-UNK HG-UNK K-UNK MG-UNK MN-UNK MO-UNK NI-UNK OCC-1 OCC-2 OCC-3 OCC-4 OCC-5 OCC-6 OCC-7 OCC-EST OCC-METERED OCC-TIMED OCC-UNK PB-UNK RIFFLE SB-UNK SE-FISH SE-UNK SH-FISH STR VEG TL-UNK WOODY

Procedure Id

OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM OKCONCOM

Procedure Source

Lab's Analytical Method used for Barium analysis is unknownLab's Analytical Method used for Beryllium analysis is unknownBlue Thumb Air Temperature ReadingsBlue Thumb Ammonia-Nitrogen TestBlue Thumb Dissolved Oxygen TestBlue Thumb Ammonia-Nitrogen TestBlue Thumb Nitrate-Nitrogen TestBlue Thumb Orthophosphate-Phosphorus TestBlue Thumb pH TestBlue Thumb Water Clarity/Secchi Depth TestBlue Thumb Ammonia-Nitrogen TestLab's Analytical Method used for Calcium analysis is unknownSeine Fish Collection Procedure-Combined ProcessesLab's Analytical Method used for Cadmium analysis is unknownLab's Analytical Method used for Cobalt analysis is unknownLab's Analytical Method used for Chromium analysis is unknownLab's Analytical Method used for Copper analysis is unknownLab's Analytical Method used for Iron analysis is unknownLab's Analytical Method used for Mercury analysis is unknownLab's Analytical Method used for Potassium analysis is unknownLab's Analytical Method used for Maganesium analysis is unknownLab's Analytical Method used for Manganese analysis is unknownLab's Analytical Method used for Molybdenum analysis is unknownLab's Analytical Method used for Nickel analysis is unknownEPA #1/SM 9221-FEPA 9056/EPA 300.1EPA 351.3/SM 4500-NOR(B)EPA 160.1/SM 2540-CEPA 160.2/SM 2540-CEPA 160.1/SM 2540-DEPA 160.2/SM 2540-DEstimated DischargeMetered DischargeTimed DischargeUnknownLab's Analytical Method used for Lead analysis is unknownBenthic Kick Procedure for Riffle HabitatsLab's Analytical Method used for Antimony analysis is unknownSeine Fish Collection ProcedureLab's Analytical Method used for Selenium analysis is unknownElectroshocking Fish Collection ProcedureProcedure for Streamside Vegetation HabitatsLabs' Analytical Method used for Thallium analysis is unknownBenthic Kick Procedure for Woody Debris Habitats

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusOKCONCOM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 442 of 515

Oklahoma Conservation Commission

ZN-UNK

Procedure Id

OKCONCOM

Procedure Source

Labs' Analytical Method used for Zinc analysis is unknown

Procedure Name

Active

StatusOKCONCOM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 443 of 515

Oklahoma Corporation Commission

CC-001

Procedure Id

OKCORCOM

Procedure Source

OKCORCOM Procedure

Procedure Name

Active

StatusOKCORCOM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 444 of 515

Oklahoma Dept. of Agriculture, Food and Forestry

120.1 150.1 350.1 365.1 9056 9222D

Procedure Id

OKDAFF OKDAFF OKDAFF OKDAFF OKDAFF OKDAFF

Procedure Source

(Lab) Conductivity(Lab) pHAmmonia NitrogenPhosphorusNitrate NitrogenFecal Coliform

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusOKDAFF

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 445 of 515

Oklahoma Dept. of Environmental Quality

10600D 120.1 130.1 150.1 160.1 160.2 1600 200.7 200.8 215.2 245.1 245.6 2550B 300

300.1 A

310.1 310.2 325.2 353.2

360.1 375.4 515.3 6010 608 614 8081 8082 8141 8151 9222D 9223B D-6503

Procedure Id

OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ

OKDEQ

OKDEQ OKDEQ OKDEQ OKDEQ

OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ OKDEQ

Procedure Source

Population StructureConductance (Specific Conductance)Hardness, Total (Colorimetric, Automated EDTA)pH (Electrometric)Filterable Residue (Gravimetric, Dried At 180°C)Non-filterable Residue (Gravimetric, Dried At 103-105°C)Enterococcus in WaterDrinking Water Metals by ICPDrinking Water Metals by ICP-MSCalcium (Titrimetric, EDTA)Mercury in Water by the Manual Cold Vapor Atomic AbsorptionMercury in Tissues by Cold Vapor (CV/AAS)Water TemperaturInorganic Anions In Drinking Water By Ion Chromatography;Common AnionsDetermination of Inorganic Anions in Drinking Water by IonChromatographyAlkalinity (Titrimetric, pH 4.5)Total Alkalinity by FIAChloride (Colorimetric, Automated Ferricyanide AAII)Nitrogen, Nitrate-Nitrite (Colorimetric, Automated, CadmiumReduction)Oxygen, Dissolved (Membrane Electrode)Sulfate (Turbidimetric)HERBICIDESMetalsOrganochlorine Pesticides and PCBsPesticidePCB/PESTICIDES IN SEDIMENTPCBS IN SEDIMENTPesticides in SedimentPCBS IN SEDIMENTFecal Coliform DensityE. coli-Total Coliform, Most Probable NumberEnterococci, Most Probable Number

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusOKDEQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 446 of 515

Oklahoma Water Resources Board

OKWRB-001

Procedure Id

OKWRB

Procedure Source

OKWRB Procedure

Procedure Name

Active

StatusOKWRB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 447 of 515

ONEIDA TRIBE OF WISCONSIN (Wisconson)

160.1 160.2 180.1 200.7_M 300_M 310.1 350.1 351.2 353.2 365.2 9222-D 973.48

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA AOAC

Procedure Source

Filterable Residue - TDSNon-Filterable Residue - TSSTurbidity by NephelometryICP-AES For Trace Element AnalysisDetermination of Anions by ICAlkalinity by TitrationAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryFecal Coliform Membrane Filter ProcedureTotal Nitrogen in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusONEIDA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 448 of 515

Osage Nation

120.1 150.1 160.1 180.1 325.3 352.1 353.3 354.1 365.2 375.4 9223-B ON_SCP YSI 6820

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA OSAGENTN OSAGENTN

Procedure Source

ConductancepHFilterable Residue - TDSTurbidity by NephelometryChloride by Mercuric Nitrate TitrationNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by Single Reagent ColorimetrySulfate by Turbidimetric DeterminationEnzyme Substrate Test, E. coli, Coliform GroupOSAGE Nation Field/Lab ProcedureYSI Multi-Parameter 6820 Sonde

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusOSAGENTN

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 449 of 515

Potomac Appalachian Trail Club Volunteer Monitoring - VA,MD

FIELD01 MATH_COUNT PROBE METHOD

Procedure Id

PATCMON PATCMON PATCMON

Procedure Source

Test Strip DeploymentCounted or Computed valuesField deployment of automated probe.

Procedure Name

ActiveActiveActive

StatusPATCMON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 450 of 515

Prairie Island Community (MN)

160.1_M 160.2_M B0051 FLOW-07QAPP PH-07QAPP TURB-07QAPP

Procedure Id

USEPA USEPA USDOI/USGS PIIC PIIC PIIC

Procedure Source

Total Dissolved SolidsTotal Suspended SolidsFecal Coliform Bacteria- Presumptive Test- MPN MethodFlow Quality Assurance Project Plan (QAPP) 2007pH Quality Assurance Project Plan (QAPP) 2007Turbidity Quality Assurance Project Plan (QAPP) 2007

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusPIIC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 451 of 515

Pawnee Nation Dept of Environmental Conservation and Safety

150.1 160.2 1603

180.1 310.1 352.1 360.1 365.2 8038 8074(A) 8225 9050 D3858

Procedure Id

USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA HACH HACH HACH USEPA ASTM

Procedure Source

pHNon-Filterable Residue - TSSEscherichia coli in Water by Membrane Filtration Using Modifiedmembrane-Thermotolerant E. coli Agar (Modified mTEC)Turbidity by NephelometryAlkalinity by TitrationNitrate Nitrogen by ColorimetryDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryAmmonia Nitrogen in WaterTotal, Fecal and E. Coli ColiformChloride by TitrationSpecific ConductanceOpen-Channel Flow Measurement by Area

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusPNDECS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 452 of 515

Elem Indian Colony Environmental (California)

QAPP

Procedure Id

POMO989

Procedure Source

Quality Assurance Procedures Policy

Procedure Name

Active

StatusPOMO989

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 453 of 515

Puerto Rico Environmental Quality Board Beach

130.2 206.2 213.2 218.2 220.2 239.2 245.1 249.2 270.2 289.1 350.1 351.2 353.2 608 EPA 160.5 EPA 1623

EPA 208.1 EPA 243.1 EPA 243.2 EPA 365.2 EPA 365.4 PREQB SOP-035 PREQB 028 PREQB SM 10200HPREQB SOP 021.1PREQB SOP 021.2PREQB SOP 021.3PREQB SOP 021.4PREQB SOP 022

PREQB SOP 024 PREQB SOP 025 PREQB SOP 027 PREQB SOP 028 PREQB SOP 034 PREQB SOP-021.3PREQB SOP-024 PREQB SOP-033

PREQB-028 PREQB=SOP 28 SECHI-DISK SM 2130B PREQB SM 4500-B.B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

Procedure Source

Total HardnessArsenic by GFAACadmium by GFAAChromium by GFAACopper by GFAALead by GFAAMercury in Water by CVAANickel by GFAASelenium by GFAAZinc by FLAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryOrganochlorine Pesticides and PCBs by GCEPA 160.5 SOLIDS SETTLEABLEEPA 1623- PROTOZOA PARASITES DETERMINATIONCRYPTOSPORIDIUM, GIARDIA LAMBIAEPA 208.1 BARIUMEPA 243.1 MANGANESEEPA 243.2 CADMIUMEPA 365.2 ORTHOPHOSPHATE AS PO4EPA 365.4 TOTAL PHOSPHOROUSPREQB SOP -035 EPA 413.1 OIL AND GREASEPREQB 028 EPA 160.2 TOTAL SOLIDS SUSPENDEDPREQB SM 10200H CHLOROPHILL "A"PREQB SOP 021.1 - TEMPERATUREPREQB SOP 021.2 - pHPREQB SOP 021.3 SalinityPREQB SOP 021.4-DISSOLVED OXYGENPREQB SOP 022, SM, 18 Ed. 9222D Microbiological Determination,Fecal Coliform, Total Coliform, EnterococcusEPA 353.2 NITRATE-N, NITRITE-NPREQB SOP 025 EPA - 350.1 AMMONIA-NPREQB SOP 027 TURBIDITY SM 2130BPREQB SOP 028 EPA 160.1 TOTAL SOLIDS DISSOLVEDPREQB SOP 034 SM 1020H - CHLOROPHYLL APREQB SOP-021.3 SALINITYPREQB SOP-024 NO2 + NO3-NPREQB SOP-033 DISSOLVED OXYGEN SM METHOD 360.2 O.C.FOR WINKLERPREQB-028 EPA 160.1 TOTAL SOLIDS SUSPENDEDPREQB=SOP 28 EPA 160.3 TOTAL SOLIDS DISSOLVEDSechi-diskSM 2130B PREQB SOP -027 TurbiditySM 4500-B.B BORON

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

StatusPR-BEACH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 454 of 515

Puerto Rico Environmental Quality Board Beach

365.4

Procedure Id

USEPA

Procedure Source

Total Phosphorus After Block Digestion

Procedure Name

Susp

StatusPR-BEACH

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 455 of 515

Puerto Rico Environmental Quality Board Coastal (Beach)

130.2 206.2 213.2 218.2 220.2 239.2 245.1 249.2 270.2 289.1 350.1 351.2 353.2 608 EPA 160.5 EPA 1623

EPA 208.1 EPA 243.1 EPA 243.2 EPA 365.2 EPA 365.4 PREQB SOP-035 PREQB 028 PREQB SM 10200HPREQB SOP 021.1PREQB SOP 021.2PREQB SOP 021.3PREQB SOP 021.4PREQB SOP 022

PREQB SOP 024 PREQB SOP 025 PREQB SOP 027 PREQB SOP 028 PREQB SOP 034 PREQB SOP-021.3PREQB SOP-024 PREQB SOP-033

PREQB-028 PREQB=SOP 28 SECHI-DISK SM 2130B PREQB SM 4500-B.B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

Procedure Source

Total HardnessArsenic by GFAACadmium by GFAAChromium by GFAACopper by GFAALead by GFAAMercury in Water by CVAANickel by GFAASelenium by GFAAZinc by FLAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryOrganochlorine Pesticides and PCBs by GCEPA 160.5 SOLIDS SETTLEABLEEPA 1623- PROTOZOA PARASITES DETERMINATIONCRYPTOSPORIDIUM, GIARDIA LAMBIAEPA 208.1 BARIUMEPA 243.1 MANGANESEEPA 243.2 CADMIUMEPA 365.2 ORTHOPHOSPHATE AS PO4EPA 365.4 TOTAL PHOSPHOROUSPREQB SOP -035 EPA 413.1 OIL AND GREASEPREQB 028 EPA 160.2 TOTAL SOLIDS SUSPENDEDPREQB SM 10200H CHLOROPHILL "A"PREQB SOP 021.1 - TEMPERATUREPREQB SOP 021.2 - pHPREQB SOP 021.3 SalinityPREQB SOP 021.4-DISSOLVED OXYGENPREQB SOP 022, SM, 18 Ed. 9222D Microbiological Determination,Fecal Coliform, Total Coliform, EnterococcusEPA 353.2 NITRATE-N, NITRITE-NPREQB SOP 025 EPA - 350.1 AMMONIA-NPREQB SOP 027 TURBIDITY SM 2130BPREQB SOP 028 EPA 160.1 TOTAL SOLIDS DISSOLVEDPREQB SOP 034 SM 1020H - CHLOROPHYLL APREQB SOP-021.3 SALINITYPREQB SOP-024 NO2 + NO3-NPREQB SOP-033 DISSOLVED OXYGEN SM METHOD 360.2 O.C.FOR WINKLERPREQB-028 EPA 160.1 TOTAL SOLIDS SUSPENDEDPREQB=SOP 28 EPA 160.3 TOTAL SOLIDS DISSOLVEDSechi-diskSM 2130B PREQB SOP -027 TurbiditySM 4500-B.B BORON

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

StatusPR-COAST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 456 of 515

Puerto Rico Environmental Quality Board Coastal (Beach)

365.4

Procedure Id

USEPA

Procedure Source

Total Phosphorus After Block Digestion

Procedure Name

Susp

StatusPR-COAST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 457 of 515

Puerto Rico Environmental Quality Board (Surface Water)

130.2 206.2 213.2 218.2 220.2 239.2 245.1 249.2 270.2 289.1 350.1 351.2 353.2 608 EPA 160.5 EPA 1623

EPA 208.1 EPA 243.1 EPA 243.2 EPA 365.2 EPA 365.4 PREQB SOP-035 PREQB 028 PREQB SM 10200HPREQB SOP 021.1PREQB SOP 021.2PREQB SOP 021.3PREQB SOP 021.4PREQB SOP 022

PREQB SOP 024 PREQB SOP 025 PREQB SOP 027 PREQB SOP 028 PREQB SOP 034 PREQB SOP-021.3PREQB SOP-024 PREQB SOP-033

PREQB-028 PREQB=SOP 28 SECHI-DISK SM 2130B PREQB SM 4500-B.B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

Procedure Source

Total HardnessArsenic by GFAACadmium by GFAAChromium by GFAACopper by GFAALead by GFAAMercury in Water by CVAANickel by GFAASelenium by GFAAZinc by FLAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryOrganochlorine Pesticides and PCBs by GCEPA 160.5 SOLIDS SETTLEABLEEPA 1623- PROTOZOA PARASITES DETERMINATIONCRYPTOSPORIDIUM, GIARDIA LAMBIAEPA 208.1 BARIUMEPA 243.1 MANGANESEEPA 243.2 CADMIUMEPA 365.2 ORTHOPHOSPHATE AS PO4EPA 365.4 TOTAL PHOSPHOROUSPREQB SOP -035 EPA 413.1 OIL AND GREASEPREQB 028 EPA 160.2 TOTAL SOLIDS SUSPENDEDPREQB SM 10200H CHLOROPHILL "A"PREQB SOP 021.1 - TEMPERATUREPREQB SOP 021.2 - pHPREQB SOP 021.3 SalinityPREQB SOP 021.4-DISSOLVED OXYGENPREQB SOP 022, SM, 18 Ed. 9222D Microbiological Determination,Fecal Coliform, Total Coliform, EnterococcusEPA 353.2 NITRATE-N, NITRITE-NPREQB SOP 025 EPA - 350.1 AMMONIA-NPREQB SOP 027 TURBIDITY SM 2130BPREQB SOP 028 EPA 160.1 TOTAL SOLIDS DISSOLVEDPREQB SOP 034 SM 1020H - CHLOROPHYLL APREQB SOP-021.3 SALINITYPREQB SOP-024 NO2 + NO3-NPREQB SOP-033 DISSOLVED OXYGEN SM METHOD 360.2 O.C.FOR WINKLERPREQB-028 EPA 160.1 TOTAL SOLIDS SUSPENDEDPREQB=SOP 28 EPA 160.3 TOTAL SOLIDS DISSOLVEDSechi-diskSM 2130B PREQB SOP -027 TurbiditySM 4500-B.B BORON

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

StatusPR-LAKES

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 458 of 515

Puerto Rico Environmental Quality Board (Surface Water)

365.4

Procedure Id

USEPA

Procedure Source

Total Phosphorus After Block Digestion

Procedure Name

Susp

StatusPR-LAKES

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 459 of 515

Puerto Rico Environmental Quality Board (Rivers)

130.2 206.2 213.2 218.2 220.2 239.2 245.1 249.2 270.2 289.1 350.1 351.2 353.2 608 EPA 160.5 EPA 1623

EPA 208.1 EPA 243.1 EPA 243.2 EPA 365.2 EPA 365.4 PREQB SOP-035 PREQB 028 PREQB SM 10200HPREQB SOP 021.1PREQB SOP 021.2PREQB SOP 021.3PREQB SOP 021.4PREQB SOP 022

PREQB SOP 024 PREQB SOP 025 PREQB SOP 027 PREQB SOP 028 PREQB SOP 034 PREQB SOP-021.3PREQB SOP-024 PREQB SOP-033

PREQB-028 PREQB=SOP 28 SECHI-DISK SM 2130B PREQB SM 4500-B.B

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

PREQB-SW PREQB-SW PREQB-SW PREQB-SW PREQB-SW

Procedure Source

Total HardnessArsenic by GFAACadmium by GFAAChromium by GFAACopper by GFAALead by GFAAMercury in Water by CVAANickel by GFAASelenium by GFAAZinc by FLAAAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryOrganochlorine Pesticides and PCBs by GCEPA 160.5 SOLIDS SETTLEABLEEPA 1623- PROTOZOA PARASITES DETERMINATIONCRYPTOSPORIDIUM, GIARDIA LAMBIAEPA 208.1 BARIUMEPA 243.1 MANGANESEEPA 243.2 CADMIUMEPA 365.2 ORTHOPHOSPHATE AS PO4EPA 365.4 TOTAL PHOSPHOROUSPREQB SOP -035 EPA 413.1 OIL AND GREASEPREQB 028 EPA 160.2 TOTAL SOLIDS SUSPENDEDPREQB SM 10200H CHLOROPHILL "A"PREQB SOP 021.1 - TEMPERATUREPREQB SOP 021.2 - pHPREQB SOP 021.3 SalinityPREQB SOP 021.4-DISSOLVED OXYGENPREQB SOP 022, SM, 18 Ed. 9222D Microbiological Determination,Fecal Coliform, Total Coliform, EnterococcusEPA 353.2 NITRATE-N, NITRITE-NPREQB SOP 025 EPA - 350.1 AMMONIA-NPREQB SOP 027 TURBIDITY SM 2130BPREQB SOP 028 EPA 160.1 TOTAL SOLIDS DISSOLVEDPREQB SOP 034 SM 1020H - CHLOROPHYLL APREQB SOP-021.3 SALINITYPREQB SOP-024 NO2 + NO3-NPREQB SOP-033 DISSOLVED OXYGEN SM METHOD 360.2 O.C.FOR WINKLERPREQB-028 EPA 160.1 TOTAL SOLIDS SUSPENDEDPREQB=SOP 28 EPA 160.3 TOTAL SOLIDS DISSOLVEDSechi-diskSM 2130B PREQB SOP -027 TurbiditySM 4500-B.B BORON

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

StatusPR-RIVER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 460 of 515

Puerto Rico Environmental Quality Board (Rivers)

365.4

Procedure Id

USEPA

Procedure Source

Total Phosphorus After Block Digestion

Procedure Name

Susp

StatusPR-RIVER

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 461 of 515

Puerto Rico

130.2 160.1_M 204.2_M 210.2_M 213.2_M 215.1_M 218.2_M 220.2_M 236.1_M 239.2_M 242.1_M 243.1_M 245.1_M 249.2_M 258.1_M 272.2_M 273.1_M 310.2 325.3 325_M(B) 335.2 335.3 340.2_M 350.1 365.5 375.2 4500-B-B 5310-B 608 624 625 PREQB SOP 021.1PREQB SOP 021.2PREQB SOP 021.4PREQB SOP 022

PREQB SOP 022 T

PREQB SOP-024

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA PREQB-GW PREQB-GW PREQB-GW PREQB-GW

PREQB-GW

PREQB-GW

Procedure Source

Total HardnessTotal Dissolved SolidsAntimony by GFAABeryllium by GFAACadmium by GFAACalcium by FLAAChromium by GFAACopper by GFAAIron by FLAALead by GFAAMagnesium by FLAAManganese by FLAAMercury in Water by Manual CVAANickel by GFAAPotassium by FLAASilver by GFAASodium by FLAAAlkalinity by Colorimetric AnalysisChloride by Mercuric Nitrate TitrationChloride in Water by TitrationTotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisFluoride with an Ion Selective ElectrodeAmmonia Nitrogen by ColorimetryOrthophosphate in Water by ColorimetrySulfate in Water by ColorimetryBoron in Water by Spectrophotometry- Curcumin MethodTotal Organic Carbon by Combustion-Infrared MethodOrganochlorine Pesticides and PCBs by GCPurgeable Organics in WastewaterBase/Neutral and Acid Organics in WastewaterPREQB SOP 021.1 - TEMPERATURE, DEGREES CPREQB SOP 021.2 - PHPREQB SOP 021.4 - CONDUCTIVITYPREQB SOP 022 - SM 9222D MICROBIOLOGICALDETERMINATIONS - FECAL COLIFORMSPREQB SOP 022 SM 9222B MICROBIOLOGICALDETERMINATIONS - TOTAL COLIFORMSPREQB SOP-024 Nitrogen Nitrite (NO2) automated, Nitrogen Nitrate(NO3-N) automated

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

Active

StatusPREQB-GW

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 462 of 515

Puyallup Tribe Of Indians (Washington)

QAPP

Procedure Id

PUYALLUP

Procedure Source

Quality Assurance Project Plan

Procedure Name

Active

StatusPUYALLUP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 463 of 515

Quapaw Tribe of Oklahoma

200.8(W) 300(A) 365.2 376.1 8074(A) QUAPAW_SP

Procedure Id

USEPA USEPA USEPA USEPA HACH QUAPAWTR

Procedure Source

Metals in Waters by ICP/MSInorganic Anions by Ion ChromatographyPhosphorus by Single Reagent ColorimetrySulfide by Titration with IodineTotal, Fecal and E. Coli ColiformQuapaw Tribe standard procedure

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusQUAPAWTR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 464 of 515

Quileute Natural Resources (Washington)

QAPP

Procedure Id

QUILEUTE

Procedure Source

Quality Assurance Project Plan

Procedure Name

Active

StatusQUILEUTE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 465 of 515

New York

2550 4500-O-C 9222-D EPA1600

Procedure Id

APHA APHA APHA R2-LAB

Procedure Source

Temperature of Water by ThermometerTotal Dissolved Oxygen by Titration- Azide ModificationFecal Coliform Membrane Filter ProcedureMethod 1600: Membrane Filter Test Method for Enterococci inWater

Procedure Name

ActiveActiveActiveActive

StatusR2-LAB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 466 of 515

EPA Region 4 Athens Lab (Georgia)

200.2 200.8(S) 200.8(W) 245.1 353.2 365.1 415.1 6010B 780-86T(S) 780-86T(W) 8081A(SWB) 8081A(WWB) 8082(S) 8082(W) 8260B 8270D ASB107C ILM04.1 NAREL RA-04 NARELGAM-01 OLM04.2 R4SOP US-786-86T(S) US-786-86T(W) XC299

Procedure Id

R4ATHENS USEPA USEPA USEPA USEPA USEPA USEPA USEPA R4ATHENS R4ATHENS USEPA USEPA USEPA USEPA USEPA R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS R4ATHENS

Procedure Source

% MoistureMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMercury in Water by CVAANitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Organic Carbon by CombustionInductively Coupled Plasma AESAmmonia -soil/sed.Ammonia -waterOrganochlorine Pesticides and PCBs by GCOrganochlorine Pesticides and PCBs by GCPCBs as Aroclors by Capillary Column GCPCBs as Aroclors by Capillary Column GCVolatile Organics by CGC/MS8270DTOC in Sediment/SoilInorganics CLP SOWNAREL RA-04NAREL GAM-01Organics CLP SOW OLM04.2Special Analytical ServiceTKN soil/sedimentTKN- waterContract Analysis

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusR4ATHENS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 467 of 515

Volunteer Monitoring Groups in EPA Region 9 (CALIFORNIA)

2130 2320 2510 4500-NH3(D) 4500-NO3(C) 4500-O-B 4500-O-C 4500-O-D 4500-O-E 4500-O-F 4500-O-G 4500-P-D 4500-P-E 4500-P-F

Procedure Id

APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA APHA

Procedure Source

Turbidity in WaterAlkalinity in Water by TitrationConductivity in WaterAmmonia in Water by Selective Electrode MethodNitrate in Water by Ion ChromatographyTotal Dissolved Oxygen by Titration- Iodometric MethodTotal Dissolved Oxygen by Titration- Azide ModificationTotal Dissolved Oxygen by Titration- Permanganate ModificationTotal Dissolved Oxygen by Titration- Alum Flocculation ModificatiTotal Dissolved Oxygen by Titration- Copper/Sulfate-Sulfamic AcidTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Stannous Chloride TitrationPhosphorus in Water by Colorimetry- Ascorbic Acid MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMetho

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusR9VOL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 468 of 515

Region 8 Superfund: Rocky Flats Indstrl Pk Thoro-Aerrco-GWI

ILM05 ILM05.3 OLC03 OLM04

Procedure Id

RCKYFLTS RCKYFLTS RCKYFLTS RCKYFLTS

Procedure Source

ILM05ILM05.3OLC03OLM04

Procedure Name

ActiveActiveActiveActive

StatusRCKYFLTS

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 469 of 515

Red Lake Band of Chippewa (MN)

10200-H 150.1 170.1 180.1 360.2 365.2

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationpHTemperatureTurbidity by NephelometryDissolved Oxygen by Winkler TechniquePhosphorus by Single Reagent Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusREDLAKE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 470 of 515

Hurricane Rita Emergency Response Monitoring

160.2 1664A 2540G 335.3 335.4 350.1 350.2 350.3 3500-CR D 353.2 365.1 365.2 365.4 405.1 410.4 415.1 420.1 6010B 7470A 8015B 8015M 8081A 8082 8151A 8260B 8270 8270C 9071M 9213D 9222 B 9222 D 9222D A_VOC_IH B_ECOLI E624 E625 HACH 8000 N5506 O&G 1664A REAC_SOP 1805 SM-3500CR_D SW-846 6010B SW-846 7470A SW-846 7471A

Procedure Id

RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6

Procedure Source

160.2EPA 1664A2540G335.3335.4350.1350.2350.33500 CR DEPA 353.2365.1365.2365.4405.1410.4415.1EPA 420.1Metals ICP 6010B7470A8015B8015MP/P NOLA 8081A80828151A8260B82708270C9071M9213D9222 B9222 D9222DA_VOC_IHB_ECOLIE624E625HACH 8000N5506O&G 1664AREAC_SOP 1805SM-3500CR_DSW-846 6010BSW-846 7470ASW-846 7471A

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusRITA6

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 471 of 515

Hurricane Rita Emergency Response Monitoring

SW-846 8015B SW-846 8015BGASSW-846 8015MOD SW-846 8081A SW-846 8082 SW-846 8151A SW-846 8260B SW-846 8270 SW-846 8270C TNRCC 1005/LA 1TNRCC 1006/LA 1TPH 1664A

Procedure Id

RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6 RITA6

Procedure Source

SW-846 8015BSW-846 8015BGASSW-846 8015ModSW-846 8081ASW-846 8082SW-846 8151ASW-846 8260BSW-846 8270SW-846 8270CTNRCC 1005/LA 1005TNRCC 1006/LA 1006TPH 1664A

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusRITA6

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 472 of 515

South Adams County Water and Sanitation District (Colorado)

1103_1 170.1 200.7(W) 200.8(W) 2320 2340 2510 2540-D 365.1 375.1 375.2 376.2 415.1 4500-H 4500-NH3(C) 4500-NH3(E) 4500-NO3(E) 4500-O-F 4500-O-G 9222-D FLOW UNKNOWN

Procedure Id

USEPA USEPA USEPA USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA APHA APHA SACWSD SACWSD

Procedure Source

E. coli in Water by Membrane FiltrationTemperatureMetals in Water by ICP-AESMetals in Waters by ICP/MSAlkalinity in Water by TitrationHardness in Water by EDTA TitrationConductivity in WaterTotal Suspended Solids in WaterPhosphorus by ColorimetrySulfate by Colorimetry With ChloranilateSulfate in Water by ColorimetrySulfide by Colorimetric DeterminationTotal Organic Carbon by CombustionpH in WaterAmmonia in Water by Titrimetric MethodAmmonia in Water by Selective Electrode Method (Known Addition)Nitrate in Water- Cadmium ReductionTotal Dissolved Oxygen by Titration- Copper/Sulfate-Sulfamic AcidTotal Dissolved Oxygen by Membrane Electrode MethodFecal Coliform Membrane Filter ProcedureFlowDefault Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSACWSD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 473 of 515

Saginaw Chippewa Planning Department (MI)

2130 2510 2550 4500-H 4500-O-G

Procedure Id

APHA APHA APHA APHA APHA

Procedure Source

Turbidity in WaterConductivity in WaterTemperature of Water by ThermometerpH in WaterTotal Dissolved Oxygen by Membrane Electrode Method

Procedure Name

ActiveActiveActiveActiveActive

StatusSAGIN01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 474 of 515

Shoaltwater Bay Tribe (Washington)

9222-D

Procedure Id

APHA

Procedure Source

Fecal Coliform Membrane Filter Procedure

Procedure Name

Active

StatusSBITENV

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 475 of 515

STOCKBRIDGE-MUNSEE COMMUNITY (Wisconson)

10200-H 150.1 160.2 2340 300.6 310.2 350.1 351.2 353.2 365.2 365.4 6010B 7470A 9222-D D1889 D5389

Procedure Id

APHA USEPA USEPA APHA IL/SWSD USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA ASTM ASTM

Procedure Source

Chlorophyll a-b-c DeterminationpHNon-Filterable Residue - TSSHardness in Water by EDTA TitrationCl, PO4, NO3 and SO4 - IONCHRAlkalinity by Colorimetric AnalysisAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetryTotal Phosphorus After Block DigestionInductively Coupled Plasma AESMercury in Liquid Wastes by CVAAFecal Coliform Membrane Filter ProcedureTurbidity of WaterOpen-Channel Flow Measurement by Acoustic Velocity Meter

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSBMUNSEE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 476 of 515

SD Dept of Environmental & Natural Resources

10300-C 10300-D 120.1 130.1 130.2 150.1 160.1 160.2 160.3 160.4 1604

1664 200.8(W) 202.1 206.2 206.2_M 208.1 210.2 213.1 2130 215.1 218.2 220.1 220.1_M 2320 2340 239.1 239.2 242.1 245.1 245.1_M 249.1 249.2 2510 2540-B 2540-C 2540-D 2540-E 258.1 270.2 270.2_M 272.1 272.2

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA

Procedure Source

Periphyton Sample AnalysisPeriphyton Primary ProductivityConductanceTotal HardnessTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueVolatile ResidueTotal Coliforms and E. coli in Water by Membrane Filtration Using aSimultaneous Detection Technique (MI Medium)Extractable Material in Oil and GreaseMetals in Waters by ICP/MSAluminum by FLAAArsenic by GFAAArsenic by GFAABarium by FLAABeryllium by GFAACadmium by FLAATurbidity in WaterCalcium by FLAAChromium by GFAACopper by FLAACopper by FLAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationLead by FLAALead by GFAAMagnesium by FLAAMercury in Water by CVAAMercury in Water by Manual CVAANickel by FLAANickel by GFAAConductivity in WaterTotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterPotassium by FLAASelenium by GFAASelenium by GFAASilver by FLAASilver by GFAA

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSDWRAP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 477 of 515

SD Dept of Environmental & Natural Resources

273.1 286.2 289.1 289.1_M 310.1 3111-B 325.2 325.3 335.4 350.1 350.2(B) 350.3 351.2 351.3(A) 351.3(B) 352.1 353.2 353.3 354.1 365.1 365.2 365.3 365.4 365_M 375.2 375.4 405.1 410.1 410.4 413.1 415.1 415.2 415.2_M 4500-CL(B) 4500-CL-(B) 4500-CO2(C) 4500-F 4500-F-C 4500-NH3(G) 4500-NH3(H) 4500-NH3(H) 4500-NO2(I) 4500-NO3(F) 4500-NO3(G)

Procedure Id

USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA SDWRAP APHA APHA APHA SDWRAP SDWRAP APHA APHA

Procedure Source

Sodium by FLAAVanadium by GFAAZinc by FLAAZinc by FLAAAlkalinity by TitrationMetals in Water by FLAA- Direct Air-Acetylene FlameChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationCyanide by Semi-Automated ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen - NesslerizationNitrate Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by Cd ReductionNitrite Nitrogen by SpectophotometryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryTotal Phosphorus After Block DigestionPhosphorus in Water by ColorimetrySulfate in Water by ColorimetrySulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandMid-Level Chemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Organic Carbon by CombustionLow Level Total Organic Carbon in WaterTotal Organic Carbon in WaterResidual Chlorine in Water by Titration- Iodometric Method IChloride in Water by Titration- Argentometric MethodCarbon Dioxide in Water by Titration Nitrite nitrogen in water - Flow injected cadmium reductionFluoride in Water Using an ISEAmmonia in Water Using Automated Phenate MethodAmmonia in Water - Flow Injection AnalysisAmmonia nitrogen in water - Flow injected analysisNitrite nitrogen in water - Flow injected cadmium reductionNitrate in Water- Automated Cadmium ReductionNitrate in Water- Titanous Chloride Reduction

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSDWRAP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 478 of 515

SD Dept of Environmental & Natural Resources

4500-NO3(I) 4500-NO3(I) 4500-SO4(F) 4500-SO4(G) 505 507 507(MODIFIED) 508 515.1 5210-B 525.2 525.2 525.5 531.1 5310-C 547 6010A 7470A 7471A 8080A 8081(S) 8081(W) 8141(W) 9010A(A) 9222-B 9222-D 9223-B ESCHERICHIA IDEXX-ELT LANGELIER SECCHI DISK USGS CAFFEINE WRAPCALC WRAPFLD

Procedure Id

APHA SDWRAP APHA SDWRAP USEPA USEPA SDWRAP USEPA USEPA APHA SDWRAP USEPA SDWRAP USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA SDWRAP SDWRAP SDWRAP SDWRAP SDWRAP SDWRAP SDWRAP

Procedure Source

Nitrate in Water- Cadmium Reduction Flow InjectionNitrate nitrogen in water - Flow injected cadmium reductionSulfate in Water by ColorimetrySulfate in water - Methylthymol blue flow injection analysisOrganohalide Pesticides and PCB in WaterNitrogen and Phosphorus PesticidesNitrogen and phosphorus pesticidesChlorinated Pesticides in Water by GCChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandOrganics in water by gas chromotographyOrganics in Water by Gas ChromatographyOrganics in Water by Gas ChromotographyN-Methylcarbamates in Water by HPLCTotal Organic Carbon in Water- Ultraviolet Oxidation MethodGlyphosate in Drinking Water by HPLCICP SpectroscopyMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WastePesticides and PCBsOrganochlorine Pesticides and PCBsOrganochlorine Pesticides and PCBsOrganophosphorus Compounds in WaterTotal and Amenable Cyanides by ColorimetryStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupEscherichiaEnterococciLangelier IndexSECCHICaffeineWRAPCALCWater Resource Assistance Program Field Procedures

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSDWRAP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 479 of 515

Shell Chemical Yabucoa (Puerto Rico)

160.3 1613(W) 1631 200.8(W) 335.2 335.4 5 7471A 7740 8081A 8081A(WWB) 8082 8082(W) 8260B 8270C SIM 8270C(W) 9012A

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA SHELLYAB USEPA USEPA SHELLYAB USEPA SHELLYAB USEPA USEPA SHELLYAB USEPA USEPA

Procedure Source

Total ResidueDioxins and Furans - WaterMercury in Water by Oxidation, Purge and Trap, and CVAFSMetals in Waters by ICP/MSTotal Cyanide in WaterCyanide by Semi-Automated Colorimetry200.8Mercury in Solid or Semisolid WasteSelenium in Various Matrices by GFAA8081AOrganochlorine Pesticides and PCBs by GC8082PCBs as Aroclors by Capillary Column GCVolatile Organics by CGC/MS8270C SIMSemivolatile Organic Compounds by CGC/MSTotal and Amenable Cyanide (Auto UV)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSHELLYAB

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 480 of 515

Shoshone-Paiute Tribes (Nevada)

120.1 150.1 170.1 245.1 300(A) 300(B) 351.2 353.2 360.1 QAPP

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA SHOPAITR

Procedure Source

ConductancepHTemperatureMercury in Water by CVAAInorganic Anions by Ion ChromatographyInorganic Anions by Ion ChromatographyTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEShoshone-Paiute Tribes QAPP

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSHOPAITR

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 481 of 515

Shakopee Mdewakanton (MN)

10200-H 2540-D 350.1 351.2 353.1 365.3

Procedure Id

APHA APHA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationTotal Suspended Solids in WaterAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Two Reagent Colorimetry

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusSMSCGOV

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 482 of 515

Seminole Nation of Oklahoma Environmental Protection Office

SNEPOAP

Procedure Id

SNEPO

Procedure Source

SNEPO Analytical Procedures

Procedure Name

Active

StatusSNEPO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 483 of 515

Sokaogon Chippewa Community (Wisconsin)

8021 LACHAT UNKNOWN

Procedure Id

SOKAOGON SOKAOGON SOKAOGON

Procedure Source

Halogenated and Aromatic VolatilesLachat 20-107-04-1BUnknown

Procedure Name

ActiveActiveActive

StatusSOKAOGON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 484 of 515

St. Regis Mohawk Tribe (New York)

170.1 180.1 340.2 360.1 360.2 505 608 7471A 8080A 9040A 9050A 9214 PAH-009 SFSAS_12

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA

Procedure Source

TemperatureTurbidity by NephelometryFluoride in Water Using an ISEDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniqueOrganohalide Pesticides and PCB in WaterOrganochlorine Pesticides and PCBs by GCMercury in Solid or Semisolid WastePesticides and PCBspH in Water by Electrometric MeasurementSpecific ConductanceFluoride in Water by ISEAnalysis of PAHs by GC/FID and GC/PIDMercury in Fish

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusSRMTAKNY

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 485 of 515

Region 8 Superfund: Standard Mine

200.7(W) 200.8(W) 2340 300(A) 310.1 415.1

Procedure Id

USEPA USEPA APHA USEPA USEPA USEPA

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationInorganic Anions by Ion ChromatographyAlkalinity by TitrationTotal Organic Carbon by Combustion

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusSTANDARD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 486 of 515

Stroud Water Research Center (Pennsylvania)

COND1.0 DOC1.0 FLOW1.0 NH4N PH1.0 TSS_VSS1.0

Procedure Id

STROUD STROUD STROUD STROUD STROUD STROUD

Procedure Source

Specific ConductivityDOCFlow Data Download from MinitrollAmmonia+Ammonium-NPHTSS_VSS

Procedure Name

ActiveActiveActiveActiveActiveActive

StatusSTROUD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 487 of 515

Southwest Florida Water Management District (FLDEP)

10200-H 2120-B 2130 2540-C 2540-D 353.2 365.1 4500-NH3(C) 4500-NH3(D) 4500-NH3(E) 4500-NH3(F) 4500-NH3(G) 4500-P-F

5310-B D5176

Procedure Id

APHA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA

APHA ASTM

Procedure Source

Chlorophyll a-b-c DeterminationColor in Water by Visual ComparisonTurbidity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryAmmonia in Water by Titrimetric MethodAmmonia in Water by Selective Electrode MethodAmmonia in Water by Selective Electrode Method (Known Addition)Ammonia in Water Using Phenate MethodAmmonia in Water Using Automated Phenate MethodPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoTotal Organic Carbon by Combustion-Infrared MethodNitrogen in Water by Pyrolysis Detection

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActive

StatusSWFMDDEP

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 488 of 515

Santa Ynez Chumash Environmental Office (California)

DHS-LUFT

Procedure Id

SYCEO

Procedure Source

DHS-LUFT

Procedure Name

Active

StatusSYCEO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 489 of 515

Pueblo of Taos (New Mexico)

150.1 180.1 TP-FLOW

Procedure Id

USEPA USEPA TAOSPBLO

Procedure Source

pHTurbidity by NephelometryTaos Pueblo Flow

Procedure Name

ActiveActiveActive

StatusTAOSPBLO

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 490 of 515

Tennessee Department of Environment and Conservation

1103_1 1106_1 120.1 130.2 150.1 160.1 160.2 170.1 200.7(S) 200.9 202.1 206.2 208.1 212.3 213.1 215.1 218.1 219.1 220.1 236.2 239.1 242.1 243.2 245.1 245.5 249.2 258.1 270.3 272.1 273.1 289.2 335.2 335.3 350.1 351.2 354.1 360.1 365.4 375.4 410.4 5210-B 9060 9071A 9222-D

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA APHA

Procedure Source

E. coli in Water by Membrane FiltrationEnterococci in Water by Membrane FilterConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTemperatureMetals in Soil by ICP-AESMetals by Temperature Stabilized GFAAAluminum by FLAAArsenic by GFAABarium by FLAABoron by Colorimetric AnalysisCadmium by FLAACalcium by FLAAChromium by FLAACobalt by FLAACopper by FLAAIron by GFAALead by FLAAMagnesium by FLAAManganese by GFAAMercury in Water by CVAAMercury in Sediment by CVAANickel by GFAAPotassium by FLAASelenium by FLAASilver by FLAASodium by FLAAZinc by GFAATotal Cyanide in WaterTotal Cyanide by Colorimetric AnalysisAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISETotal Phosphorus After Block DigestionSulfate by Turbidimetric DeterminationChemical Oxygen Demand by Colorimetry5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water and WasteOil and Grease in Sludge and SedimentFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusTDECDOE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 491 of 515

Tennessee Department of Environment and Conservation

9223-B 9230-B

A.18.4 A.18.9.1 A.23.1 C-005-1 EPA 249.2 MS MS+ECD PARTSIZE R.1.3 R.6 SOLIDS TDS

Procedure Id

APHA APHA

TDECDOE TDECDOE TDECDOE USEPA TDECDOE TDECDOE TDECDOE TDECDOE TDECDOE TDECDOE TDECDOE TDECDOE

Procedure Source

Enzyme Substrate Test, E. coli, Coliform GroupFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueNO3 & NO2 NITROGENTotal PhosphateTotal PhenolsOil and Grease by Extraction/GravimetryPetroleum Hydrocarbons (TPH)Mass spec for extractable organicsMass spec and electron captureParticle size distribution of sedimentGross Alpha & BetaGamma radionuclidesPercent SolidsTotal Dissolved Solids

Procedure Name

ActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusTDECDOE

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 492 of 515

Tennessee Department of Environment and Conservation

10200-H 110.2 1106.1

1CONDUCTIVITY 1DO 1FLOW 1PH 1TEMPERATURE 200 200.7(W) 200.9 2120-B 2130 218.4 2310 2320 2340 245.1 2540-B 2540-C 2540-D 2540-F 2550 272.2 3111-B 3113-B 325.3 350.1 3500-CA(B) 351.1 351.2 365.4 375.4 405.1 445 4500-CL-(C) 4500-CN(E) 4500-NO3(F) 4500-P-F

515.1 5210-B 5220-B

Procedure Id

APHA USEPA USEPA

TDECWPC TDECWPC TDECWPC TDECWPC TDECWPC USEPA USEPA USEPA APHA APHA USEPA APHA APHA APHA USEPA APHA APHA APHA APHA APHA USEPA APHA APHA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA APHA

USEPA APHA APHA

Procedure Source

Chlorophyll a-b-c DeterminationColor Analysis Using Platinum/CobaltEnterococci in Water by Membrane Filtration Using membrane-Enterococcus-Esculin Iron Agar (mE-EIA)SPECIFIC CONDUCTIVITYDISSOLVED OXYGENFLOWPHTEMPERATUREMetals by Atomic AbsorptionMetals in Water by ICP-AESMetals by Temperature Stabilized GFAAColor in Water by Visual ComparisonTurbidity in WaterHexavalent Chromium by FLAAAcidity in Water by TitrationAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAATotal Solids Dried 103-105C in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterSettleable Solids in WaterTemperature of Water by ThermometerSilver by GFAAMetals in Water by FLAA- Direct Air-Acetylene FlameMetals in Water by GFAAChloride by Mercuric Nitrate TitrationAmmonia Nitrogen by ColorimetryCalcium in Water by FLAATotal Kjeldahl Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryTotal Phosphorus After Block DigestionSulfate by Turbidimetric Determination5 Day Biochemical Oxygen DemandIn-Vitro Determination of ChlorophyllChloride in Water by Titration- Mercuric Nitrate MethodCyanide in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoChlorinated Acids in Water by CGC/ECD5-Day Biochemical Oxygen DemandChemical Oxygen Demand by Titration- Open Reflux Method

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActive

StatusTDECWPC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 493 of 515

Tennessee Department of Environment and Conservation

5220-D 5310-B 5520-B 9222-B 9222-D 9223-B 9223-B ED 9230-B

DEMO -004 SQBANK SQKICK SQSH TDS FIELD TURBIDITY FIELD

Procedure Id

APHA APHA APHA APHA APHA APHA TDECWPC APHA

TDECWPC TDECWPC TDECWPC TDECWPC TDECWPC TDECWPC

Procedure Source

Chemical Oxygen Demand by Colorimetry- Closed RefluxTotal Organic Carbon by Combustion-Infrared MethodOil and Grease by Gravimetric AnalysisStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupE Coli-diluFecal Streptococcus and Enterococcus, Multi-tube FermentationTechniqueDEMOSQBANKSQKICKsemi quantitative single habitatTOTAL DISSOLVED SOLIDSTURBIDITY FIELD

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActiveActive

StatusTDECWPC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 494 of 515

City of Thornton (Colorado)

200.7(W) 200.8(W) 200.9 2320 2340 245.1 2510 2540-C 2540-D 2550 2560-B 300_M 415.1 4500-H 4500-NH3(F) 4500-NO2(B) 4500-NO3(F) 4500-O-G 4500-P-C

4500-P-F

4500-SO4(B) 5210-B 5310-C 9221-E

FLOW

Procedure Id

USEPA USEPA USEPA APHA APHA USEPA APHA APHA APHA APHA APHA USEPA USEPA APHA APHA APHA APHA APHA APHA

APHA

APHA APHA APHA APHA

THORNTON

Procedure Source

Metals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationHardness in Water by EDTA TitrationMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerParticle Counting by Electrical SensingDetermination of Anions by ICTotal Organic Carbon by CombustionpH in WaterAmmonia in Water Using Phenate MethodNitrite in Water by ColorimetryNitrate in Water- Automated Cadmium ReductionTotal Dissolved Oxygen by Membrane Electrode MethodPhosphorus in Water by Vanadomolybdophosphoric AcidColorimetryPhosphorus in Water by Colorimetry- Automated Ascorbic AcidMethoSulfate in Water by Ion Chromatography5-Day Biochemical Oxygen DemandTotal Organic Carbon in Water- Ultraviolet Oxidation MethodEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueflow

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActive

Active

StatusTHORNTON

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 495 of 515

Tri-State Water Quality Council (EPA Region 8)

10200-H 1050(A) 150.1 160.1 180.1 200.7(W) 200.8(W) 200.9 2130 2540-C 2540-D 350.1 351.1 353.2 365.1 365.4 FLOW-METER FLOW-STAFF_GAGEPEBBLE PERIPHYTONCOUNTSAR-CALC TDS_METER TN-CALC TPN-4500-N_C UNKNOWN

Procedure Id

APHA TSWQC USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA TSWQC TSWQC TSWQC TSWQC TSWQC TSWQC TSWQC TSWQC TSWQC

Procedure Source

Chlorophyll a-b-c DeterminationAnion - Cation BalancepHFilterable Residue - TDSTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAATurbidity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryTotal Phosphorus After Block DigestionFlow, Average Velocity times Cross Sectional AreaFlow, Determination from Staff GagePebble CountPeriphyton AnalysisSodium Adsorption Ratio CalculationTDS determination using handheld probe.Total Nitrogen, TN - SUM of TKN + NO3 + NO2Persulfate Nitrogen MethodUnknown Method or Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusTSWQC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 496 of 515

Upper Deschutes Watershed Council (Oregon)

2550

Procedure Id

APHA

Procedure Source

Temperature of Water by Thermometer

Procedure Name

Active

StatusUDWC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 497 of 515

US Army Corps of Engineers, Nashville District (Tennessee)

10200-H 160.1 160.2 160.3 200.7(S) 200.7(W) 200.8(W) 2340 245.5 300(A) 350.1 351.2 353.2 365.1 375.4 415.1 5310-C 8081(S) 8082(S) 8260B 8270C(S)

Procedure Id

APHA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA USEPA USEPA

Procedure Source

Chlorophyll a-b-c DeterminationFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Waters by ICP/MSHardness in Water by EDTA TitrationMercury in Sediment by CVAAInorganic Anions by Ion ChromatographyAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetrySulfate by Turbidimetric DeterminationTotal Organic Carbon by CombustionTotal Organic Carbon in Water- Ultraviolet Oxidation MethodOrganochlorine Pesticides and PCBsPCBs as Aroclors by Capillary Column GCVolatile Organics by CGC/MSSemivolatile Organic Compounds by CGC/MS

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUSACOEND

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 498 of 515

Umatilla National Forest (Washington and Oregon)

2130 2510 2540-D 2550 4500-H 8008 8156 8171 8229 9222 B 9222-D

Procedure Id

APHA APHA APHA APHA APHA HACH HACH USFS0614 HACH USFS0614 APHA

Procedure Source

Turbidity in WaterConductivity in WaterTotal Suspended Solids in WaterTemperature of Water by ThermometerpH in WaterTotal Iron in WaterpH in WaterHach Nitrate, MRDissolved Oxygen in WaterTotal Coliform, E. ColiFecal Coliform Membrane Filter Procedure

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUSFS0614

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 499 of 515

New Mexico Ecological Services Field Office (New Mexico)

120.1 130.2 150.1 160.1 160.2 160.3 170.1 180.1 245.6 300(A) 310.1 314 350.1 351.2 353.2 354.1 360.1 365.3 405.1 410.4 6010B 6020 7470A 7471A 8081A(SWB) 8141A(W) 8151(W) 8260B 8310 8330(W) 9012A 9056 9060 9071A D422 D5388 D5389 ITM-001

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA ASTM USFWS-NM ASTM USEPA

Procedure Source

ConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSTotal ResidueTemperatureTurbidity by NephelometryMercury in Tissue by CVAAInorganic Anions by Ion ChromatographyAlkalinity by TitrationPerchlorate in Drinking Water using Ion ChromatographyAmmonia Nitrogen by ColorimetryTotal Kjeldahl Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryNitrite Nitrogen by SpectophotometryDissolved Oxygen Using an ISEPhosphorus by Two Reagent Colorimetry5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryInductively Coupled Plasma AESInductively Coupled Plasma - Mass Spec.Mercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteOrganochlorine Pesticides and PCBs by GCOrganophosphorus Compounds in WaterChlorinated Herbicides in Water by GCVolatile Organics by CGC/MSPolynuclear Aromatic HydrocarbonsNitroaromatics and Nitramines by HPLCTotal and Amenable Cyanide (Auto UV)Anion Chromatography MethodTotal Organic Carbon in Water and WasteOil and Grease in Sludge and SedimentParticle-Size Analysis of SoilsDischarge, instantaneousOpen-Channel Flow Measurement by Acoustic Velocity MeterMetals Emissions from Stationary Sources

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUSFWS-NM

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 500 of 515

Government US Virgin Islands

1106_1 160.2_M 2130 2540-D 351.2 365.4 405.1 4500-H 8021 9222-D DEPTH FINDER

DOTEMP GPS KJELDAHL SALINITY SECCHI

Procedure Id

USEPA USEPA APHA APHA USEPA USEPA USEPA APHA HACH APHA USVIST

USVIST USVIST USVIST USVIST USVIST

Procedure Source

Enterococci in Water by Membrane FilterTotal Suspended SolidsTurbidity in WaterTotal Suspended Solids in WaterTotal Kjeldahl Nitrogen by ColorimetryTotal Phosphorus After Block Digestion5 Day Biochemical Oxygen DemandpH in WaterFree Chlorine in Water by DPDFecal Coliform Membrane Filter ProcedureDepth Determination by Handheld Depth Finder SpeedtechInstrumentYSI Dissolved Oxygen / Water Temperature ProbeTrimble GeoExplorer II Global Positioning SystemTotal Kjeldahl Nitrogen SamplingYSI Salinity ProbeSecchi Depth Determination

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

ActiveActiveActiveActiveActive

StatusUSVIST

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 501 of 515

Utah Department Of Environmental Quality

00-02 10200-F 10200-H 10300-C 10500-C 110.2 1103_1 120.1 140.1 150.1 160.1 160.2 160.2_M 160.4 160.5 1664 180.1 200.7(S) 200.7(W) 200.8(S) 200.8(W) 200.9 2320 2330B 245.1 245.6 2540-C 2540-D 2540-E 2540-F 2540-G 300(A) 3114-C 314 325.2 325.3 335.1 335.2 335.4 350.1 350.3 3500-CR(D) 351.3(A) 351.4

Procedure Id

USEPA APHA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA UTAHDWQ USEPA USEPA APHA APHA APHA APHA APHA USEPA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA USEPA

Procedure Source

Gross Alpha Activity in Drinking Water by CoprecipitationPhytoplankton Counting TechniquesChlorophyll a-b-c DeterminationPeriphyton Sample AnalysisBenthic Macroinvertebrate Sample Processing and AnalysisColor Analysis Using Platinum/CobaltE. coli in Water by Membrane FiltrationConductanceOdor in Water Using a Consistent SeriespHFilterable Residue - TDSNon-Filterable Residue - TSSTotal Suspended SolidsVolatile ResidueSettleable MatterExtractable Material in Oil and GreaseTurbidity by NephelometryMetals in Soil by ICP-AESMetals in Water by ICP-AESMetals in Wastes by ICP/MSMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAAlkalinity in Water by TitrationCorrosivityMercury in Water by CVAAMercury in Tissue by CVAATotal Dissolved Solids in WaterTotal Suspended Solids in WaterFixed and Volatile Solids in WaterSettleable Solids in WaterTotal, Fixed and Volatile SolidsInorganic Anions by Ion ChromatographyMetals in Water by Continuous HYDAAPerchlorate in Drinking Water using Ion ChromatographyChloride by Colorimetric Analysis IIChloride by Mercuric Nitrate TitrationCyanides Amenable to ChlorinationTotal Cyanide in WaterCyanide by Semi-Automated ColorimetryAmmonia Nitrogen by ColorimetryAmmonia Nitrogen Using an ISETotal Hexavalent Chromium in WaterTotal Kjeldahl Nitrogen by TitrationTotal Kjeldahl Nitrogen Using an ISE

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUTAHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 502 of 515

Utah Department Of Environmental Quality

353.2 365.1 365.2 365.3 370.1 375.2 376.2 405.1 410.4 413.1 420.4 4500-F-C 4500-NH3(H) 4500-NOR(B) 502.2(ELCD) 502.2(PID) 504 505 507 508 508.1 515.1 515.1DEQWQ 5210-B 524.2 524.2 DEQWQ 525.1 525.2 525.2 L1 525.2DEQ 526 528 531.1 5310-B 5320-B 547 548 549 551 552 5540-C 5910B 601 6010A

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA UTAHDWQ APHA USEPA UTAHDWQ USEPA USEPA UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA UTAHDWQ USEPA USEPA

Procedure Source

Nitrate-Nitrite Nitrogen by ColorimetryPhosphorus by ColorimetryPhosphorus by Single Reagent ColorimetryPhosphorus by Two Reagent ColorimetryDissolved Silica by ColorimetrySulfate in Water by ColorimetrySulfide by Colorimetric Determination5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseTotal Recoverable Phenolics in WaterFluoride in Water Using an ISEAmmonia in Water - Flow Injection AnalysisTotal Kjeldahl Nitrogen in WaterVolatile Organic Compounds in WaterVolatile Organic Compounds in WaterEDB and DBCP in Water by GCOrganohalide Pesticides and PCB in WaterNitrogen and Phosphorus PesticidesChlorinated Pesticides in Water by GCChlorinated Pest., Herb. and OrganohalideChlorinated Acids in Water by CGC/ECDChlorinated Acids for Water Quality5-Day Biochemical Oxygen DemandPurgeable Organics in Water by CGC/MSVolitiles For Water QualityOrganics in Water by Gas ChromatographyOrganics in Water by Gas ChromatographySemivol Org UCMR List 1Semivolalitiles for DEQSemivol Org UCMR List 2SemiVol Org UCMR List 2N-Methylcarbamates in Water by HPLCTotal Organic Carbon by Combustion-Infrared MethodDissolved Organic Halogen in WaterGlyphosate in Drinking Water by HPLCEndothall in Water by Gas ChromatographyDiquat and Paraquat in Water by HPLC/UVChlorinated Solvents in Water by GCHaloacetic Acids in Water by GCAnionic Surfactants in Water as MBASUV absorption @ 254 nmPurgeable Halocarbons in WastewaterICP Spectroscopy

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUTAHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

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Page 503 of 515

Utah Department Of Environmental Quality

602 6020 608 608.2 614 615 619 6233-B 624 624DEQWQ 625 6251-B 6251B/552 7470A 7471A 7500-RA(B) 7500B 8015A 8015B 8020A 8021A(ELCD) 8021A(PID) 8021B 8140 8141(W) 8150B 8260B 8270B(W) 900 903.1 9030A 904 9070 908 913.0 9215-D 9221-C

9221-E

9222-B 9222-D 9223-B 9230C

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA APHA USEPA UTAHDWQ USEPA APHA UTAHDWQ USEPA USEPA APHA UTAHDWQ USEPA USEPA USEPA USEPA USEPA UTAHDWQ USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA UTAHDWQ APHA APHA

APHA

APHA APHA APHA UTAHDWQ

Procedure Source

Purgeable Aromatics in Wastewater by GCInductively Coupled Plasma - Mass Spec.Organochlorine Pesticides and PCBs by GCOrganochlorine Pesticides in WastewaterOrganophosphorus Pesticides IChlorinated Herbicides in WastewaterTriazine Pesticides in WastewaterHaloacetic Acids and TrichlorphenolPurgeable Organics in WastewaterVolatiles for Water QualityBase/Neutral and Acid Organics in WastewaterDisinfection By-Products: Haloacetic Acids and TrichlorophenolHaloacetic AcidsMercury in Liquid Wastes by CVAAMercury in Solid or Semisolid WasteRadium in Water by PrecipitationRadonNon-Halogenated Volatile OrganicsNon-Halogenated Organics Using GC/FIDAromatic Volatile Organics by GCHalogenated and Aromatic VolatilesHalo and Aromatic Volatiles - CGC/PIDAromatic and Halogenated Aromatics (BTEX)Organophosphorus Pesticides by GCOrganophosphorus Compounds in WaterChlorinated Herbicides by GCVolatile Organics by CGC/MSSemivolatile Organics in Water by GC/MSGross Alpha and Beta Activity in WaterRadium-226 in Drinking WaterAcid Soluble and Acid Insoluble SulfidesRadium-228 in Drinking WaterTotal Recoverable Oil and GreaseUranium in Drinking WaterRadonHeterotrophic Plate Count- Membrane Filter MethodEstimation of Coliform Group Density, Multi-tube FermentationTechniqueEstimation of Fecal Coliform Group Density, Multi-tube FermentationTechniqueStandard Total Coliform Membrane Filter ProcedureFecal Coliform Membrane Filter ProcedureEnzyme Substrate Test, E. coli, Coliform GroupFecal Step membrane filter

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActive

StatusUTAHDWQ

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Page 504 of 515

Utah Department Of Environmental Quality

COILERT COLILERT D5072 DRC FIELD MEASURES FIELD TURBIDITYGENERIC METHOD

GENERIC METHOD2

GSLPERI MACRO1 MACRO2 PERI1 PHYTO1 SLC FLOWS THM DEQ USEPA7473 USGSFLOW

Procedure Id

UTAHDWQ UTAHDWQ ASTM UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ

UTAHDWQ

UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ UTAHDWQ

Procedure Source

Field Coliform analyses by coilertColilertRadon in Drinking WaterMetals by ICPMS w/ DRCField Measurements performed by Utah DWQTurbidiy determined in the fieldUsed for all methods where historical methodology may not beavailable.Used for half of methods where historical methodology may not beavailable.Periphyton sampling and analysis in GSL WetlandsMacroinvertabrates analyzed at BYUMacroinvertabrates analyzed at USUPeriphyton Counting By Rushforth EcologyPhytoplankton Counting By Sam RushforthFlows determined by Salt Lake County Water ReclaimationTHM by 524.2 for Water QualityMercury in FishFlow measurements taken by the USGS

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

Active

ActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusUTAHDWQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 505 of 515

University of N H Center for Freshwater Biology (New Hampsh)

10200-H 2120-B 4500-P-E LLMP-SECCHI SM 20 2320-B

Procedure Id

APHA APHA APHA U_NH01 U_NH01

Procedure Source

Chlorophyll a-b-c DeterminationColor in Water by Visual ComparisonPhosphorus in Water by Colorimetry- Ascorbic Acid MethodSecchi Disk TransparencyLow Alkalinity Titration to pH 4.5

Procedure Name

ActiveActiveActiveActiveActive

StatusU_NH01

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 506 of 515

Valley Improvement Association

120.1 150.1 160.1 200.8(W) 300(A) 310.1 QAPP

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA VALENCIA

Procedure Source

ConductancepHFilterable Residue - TDSMetals in Waters by ICP/MSInorganic Anions by Ion ChromatographyAlkalinity by TitrationQuality AssuranceProgram Procedures

Procedure Name

ActiveActiveActiveActiveActiveActiveActive

StatusVALENCIA

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 507 of 515

Wasilla SWCD (Alaska)

170.1 2130 2510 2540-C 2550 3.5 352.1 360.2 365.5 4500-H 4500-NO3(D) 8156

Procedure Id

USEPA APHA APHA APHA APHA APHA USEPA USEPA USEPA APHA APHA HACH

Procedure Source

TemperatureTurbidity in WaterConductivity in WaterTotal Dissolved Solids in WaterTemperature of Water by ThermometerColiforms- Plate CountNitrate Nitrogen by ColorimetryDissolved Oxygen by Winkler TechniqueOrthophosphate in Water by ColorimetrypH in WaterNitrate in Water Using an ISEpH in Water

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusWASISWCD

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 508 of 515

Lac Du Flambeau Band of Lake Superior Chippewa Indians DNR

245.2

Procedure Id

USEPA

Procedure Source

Mercury by CVAA

Procedure Name

Active

StatusWATERLDF

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 509 of 515

Wiyot Tribe (California)

150.1 160.2 1604

170.1 180.1 200.7(W) 200.8(W) 200.9 245.1 2520-B 2540-D 300(A) 350.3 351.4 360.1 365.2 4500-NH3(D) 4500-NOR(B) 4500-P-E 8015B 8082(W) 8270C(W) 9050 QAPP

Procedure Id

USEPA USEPA USEPA

USEPA USEPA USEPA USEPA USEPA USEPA APHA APHA USEPA USEPA USEPA USEPA USEPA APHA APHA APHA USEPA USEPA USEPA USEPA WIYOT

Procedure Source

pHNon-Filterable Residue - TSSTotal Coliforms and E. coli in Water by Membrane Filtration Using aSimultaneous Detection Technique (MI Medium)TemperatureTurbidity by NephelometryMetals in Water by ICP-AESMetals in Waters by ICP/MSMetals by Temperature Stabilized GFAAMercury in Water by CVAASalinity in Water- Electrical Conductivity MethodTotal Suspended Solids in WaterInorganic Anions by Ion ChromatographyAmmonia Nitrogen Using an ISETotal Kjeldahl Nitrogen Using an ISEDissolved Oxygen Using an ISEPhosphorus by Single Reagent ColorimetryAmmonia in Water by Selective Electrode MethodTotal Kjeldahl Nitrogen in WaterPhosphorus in Water by Colorimetry- Ascorbic Acid MethodNon-Halogenated Organics Using GC/FIDPCBs as Aroclors by Capillary Column GCSemivolatile Organic Compounds by CGC/MSSpecific ConductanceWiyot Quality Assurance Project Plan

Procedure Name

ActiveActiveActive

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusWIYOT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 510 of 515

Region 8 Superfund: Welby Rail Yard

ILM05 ILM05.3 OLM04

Procedure Id

WLBYRAIL WLBYRAIL WLBYRAIL

Procedure Source

ILM05ILM05.3OLM04

Procedure Name

ActiveActiveActive

StatusWLBYRAIL

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 511 of 515

Wyandotte Nation (Oklahoma)

WNENVDPT_AP

Procedure Id

WNENVDPT

Procedure Source

WNENVDPT Analytical Procedures

Procedure Name

Active

StatusWNENVDPT

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 512 of 515

Wind River Environmental Quality Commission (Wyoming)

200.7(W) 200.9 206.4 2320 245.1 2510 2540-C 2540-D 353.2 365.2 8156 8160

Procedure Id

USEPA USEPA USEPA APHA USEPA APHA APHA APHA USEPA USEPA HACH HACH

Procedure Source

Metals in Water by ICP-AESMetals by Temperature Stabilized GFAAArsenic by Spectrophotometric AnalysisAlkalinity in Water by TitrationMercury in Water by CVAAConductivity in WaterTotal Dissolved Solids in WaterTotal Suspended Solids in WaterNitrate-Nitrite Nitrogen by ColorimetryPhosphorus by Single Reagent ColorimetrypH in WaterConductivity in Water by Direct Measurement

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusWREQC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 513 of 515

Water Sentinels Sierra Club (Epa Region 7)

8038 8156 8157 8160 8190 8229 D1293(B) D1889 D3867(B) I2600(W) TEMP WEATHER001

Procedure Id

HACH HACH HACH HACH HACH HACH ASTM ASTM ASTM USDOI/USGS WSSC WSSC

Procedure Source

Ammonia Nitrogen in WaterpH in WaterDissolved Oxygen in WaterConductivity in Water by Direct MeasurementTotal Phosphorus in WaterDissolved Oxygen in WaterpH of Water By Routine MeasurementTurbidity of WaterNitrite-Nitrate by Manual Cd ReductionPhosphorus in Water by Colorimetrytemperature, waterField Station Visit Weather Observations

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusWSSC

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 514 of 515

Wyoming Dept. of Environmental Quality

120.1 130.1 150.1 160.1 160.2 160.5 170.1 180.1 213.2 215.1 220.1 236.1 239.2 243.1 289.1 310.1 325.2 330.5 350.1 353.2 360.1 360.2 365.3 375.2 403 APHA 405.1 410.4 413.1 903.1 BENTHOS FCB FLOW

Procedure Id

USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA USEPA WY-DEQ USEPA USEPA USEPA USEPA WY-DEQ WY-DEQ WY-DEQ

Procedure Source

ConductanceTotal HardnesspHFilterable Residue - TDSNon-Filterable Residue - TSSSettleable MatterTemperatureTurbidity by NephelometryCadmium by GFAACalcium by FLAACopper by FLAAIron by FLAALead by GFAAManganese by FLAAZinc by FLAAAlkalinity by TitrationChloride by Colorimetric Analysis IIChlorine by Spectrophotometry with DPDAmmonia Nitrogen by ColorimetryNitrate-Nitrite Nitrogen by ColorimetryDissolved Oxygen Using an ISEDissolved Oxygen by Winkler TechniquePhosphorus by Two Reagent ColorimetrySulfate in Water by ColorimetryAlkalinity5 Day Biochemical Oxygen DemandChemical Oxygen Demand by ColorimetryTotal Recoverable Oil and GreaseRadium-226 in Drinking WaterLab-benthosFecal Coliform Bacteria EPA MethodDischarge (Cubic feet per Second)

Procedure Name

ActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActiveActive

StatusWY-DEQ

October 27, 2008 14:37:36Field/Lab Analytical Procedures

and Equipment Summary

Page 515 of 515

The Yurok Tribe Environemtal Program (CALIFORNIA)

YUROK

Procedure Id

YUROKTEP

Procedure Source

Yurok lab/field procedures

Procedure Name

Active

StatusYUROKTEP