degumming and centrifuge selection, optimization and ... · pdf filedegumming and centrifuge...
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![Page 1: Degumming and Centrifuge Selection, Optimization and ... · PDF fileDegumming and Centrifuge Selection, Optimization and Maintenance IUPAC-AOCS Workshop on Fats, Oils and Oilseeds](https://reader031.vdocuments.site/reader031/viewer/2022020315/5ab3c7527f8b9a00728e7c4f/html5/thumbnails/1.jpg)
Degumming and Centrifuge Selection, Optimization and MaintenanceIUPAC-AOCS Workshop on Fats, Oils and Oilseeds Analysis and Production
Andrew LoganAlfa Laval Copenhagen A/S
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AlkaliNeutralisationAlkaliNeutralisation
SpecialDegummingSpecialDegumming
WaterDegummingWaterDegumming
GumsdryingGumsdrying
SoapstocksplittingSoapstocksplitting
DewaxingDewaxingDewaxingDewaxing
BleachingBleachingBleachingBleaching
DeodorisationDeodorisationDeacidification/DeodorisationDeacidification/Deodorisation
PhysicalRefining
ChemicalRefining
Crude Oil
CrudeLecithin
Acid Gums Acid Oil
HydrogenationHydrogenation
To meal or feed lecithin
Fatty Acid Distillate
Edible Oil Edible Oil
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Purpose of Degumming
• Commercial Lecithin production
• Prevent crude oil settling during storage or transport
• Waste water (prevent acidulation of gums)
• Physical Refining
• Reduction in neutralisation losses
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Physical Refining
Feedstock Parameters
• Seed Oil (Soybean, Rapeseed, Sunflower)
– FFA < 2%• higher FFA indicates low quality oil and may not be suitable for
physical refining
– Phosphorous < 5 ppm, <2 desired
– Iron < 0.2 ppm
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Chemical Refining
Feedstock Parameters
• Seed Oil (Soybean, Rapeseed, Sunflower)
– FFA < 3%
– Phosphorous < 1200 ppm, < 200 ppm desired
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Water Degumming Process Steps
• Heat oil to 60 - 70 °C
• Water addition and mixing
• Hydration mixing 30 minutes
• Centrifugal separation of hydrated gums
• Vacuum drying of degummed oil
• Gums - dried for edible lecithin or recombined in meal
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Water Degumming
WaterCrude
oil
Heater
MixerReactor
Separator
Gums
HeaterSteam
Vacuum
Vacuum dryer
To storage
Steam
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Water Degumming
Target Results:
• Phosphorous in oil - 50 to 200 ppm max.
• AI% in dried gums - 65 to 70%.
• Moisture in dried oil - < 0.1%.
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Acid Degumming Process Steps
• Heat oil to 60 - 70 °C
• Acid addition and mixing
• Hydration mixing 30 minutes
• Centrifugal separation of hydrated gums
• Vacuum drying of degummed oil
• Gums - recombined in meal
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Acid Degumming
To drying/storage
Reactor
Mixer
MixerWater
SteamCrude
oil
Heater Acid Separator
Gums
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Acid Degumming
Target Results:
• Phosphorous in oil - 20 to 50 ppm max.
• AI% in dried gums - 65 to 70%
• Moisture in dried oil - < 0.1%
![Page 12: Degumming and Centrifuge Selection, Optimization and ... · PDF fileDegumming and Centrifuge Selection, Optimization and Maintenance IUPAC-AOCS Workshop on Fats, Oils and Oilseeds](https://reader031.vdocuments.site/reader031/viewer/2022020315/5ab3c7527f8b9a00728e7c4f/html5/thumbnails/12.jpg)
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Major Deep Degumming Methods
• Alfa Laval Special Degumming
• Super/Uni Degumming
• TOP Degumming
• Organic Refining Process
• Soft Degumming
• Enzymatic Degumming
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Deep Degumming
• Deep degumming utilizes a reagent like acid to chelate Iron, Calcium, and Magnesium away from the NHP complex. Once the Iron, Calcium, and Magnesium are removed from the NHP complex the phosphatidebecomes hydratable
• Enzymatic degumming utilizes an enzyme to modify the NHP into a hydratable form.
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Alfa Laval Special Degumming
• Heat oil to 60 oC
• 0.05-0.2 % Phosphoric Acid with intensive mixing
• Partially neutralise with dilute lye (hydration water)
• Gentle mixing and holding for 60 minutes
• Gums centrifugation
• Optional water wash step for lower phosphorous
• Oil drying
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Alfa Laval Special Degumming
Mixer Mixer
Crudeoil
Heater
Steam
Acid
Lye
WaterOil temperature
trimmer Separator
Gums
Todrying/storage
Reactor
Coolingwater
Steam
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Alfa Laval 2-stage Special Degumming
Crudeoil
Steam
Heater
Mixer Mixer
Acid Lye
Neutralisingroute
Reactor Coolingwater
Steam
Mixer
To drying/storage
Wastewater
SeparatorSeparatorOil
temperaturetrimmer
Water
Gumsor
soap-stock
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Alfa Laval Special Degumming
Target Results:
• Phosphorous in oil - 20 to 30 ppm max.
• Phosphorous in oil - 8 to 10 ppm max. with washing
• AI% in dried gums - 50 to 60%
• Moisture in dried oil - < 0.1%
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Disc Stack CentrifugesAlternative name: High Speed Separators (HSS)
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Gravitational to Centrifugal Force
>5000 g
1.
2.
3.
Centrifugal separationvessel with disc-stack
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Clarification
• Removal of solids
phase from a mixture
of liquid and solids
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Concentration
• Liquid/liquid separation
(also solids if present)
• Maximum cleaning of
the heavy phase
• Therefore holes in
disc-stack closer to
the centre
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Purification
• Liquid/liquid separation
(also solids if present)
• Maximum cleaning of
the light phase
• Therefore holes in
disc-stack closer to
the periphery
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HSS – Bowl Development
1890 1948 1993
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HSS – Unit Capacities
0200400600800
1000120014001600
1892
1934
1948
1956
1959
1970
1972
1977
1984
1993
1997
1998
2001
Year
Capa
city
(TPD
)