calibration - · pdf file# id update time quant time acquisition time 1 1 apr 13 15:16 2011...

Quantitation Report (QT Reviewed)

Data Path : C: \MSDChem \l \DATA \NDMA 1 4 Dioxane \20121017\ Data File : 10 -17 -12 10.D Acq On : 17 Oct 2012 6:29 pm Operator : QN Sample : 312205 -004 Misc ALS `Dial : 10 Sample Multiplier: 1

Quant Time: Oct 18 15:19:28 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M -Quant Title .

QLast Update : Wed May 05 16:21:01 2010 Response via : Initial Calibration

Internal Standards R.T.

1) 1,4-Dioxane d8 3) NDMA-d6 5) NDEA-d10

Target Compounds 2) 1,4- Dioxane

7.40 9.12

11.30

7.45

QIon Response

96 311386 80 442309

112 450920

88 8395m

Conc Units Dev(Min)

20.00 ug/L -0.18 20.00 ug/L -0.17 20.00 ug/L -0.17

/ 0.58\ug /L Qvalue

( #) = qualifier out of range (m) = manual integration ( +) = signals summed

1625 M 041311F2.M Thu Oct 18 15:19:48 2012

1çY ..,Fps

Page: 1

c: 0E1270 n

CONFIDENTIAL LMC- PET -00002169

Quantitation Report (Not Reviewed)

Data Path : C: \MSDCHEM \1 \DATA \NDMA 1 4 DIOXANE \20121017\ Data File : 10 -17 -12 10.D Acq On : 17 Oct 2012 6:29 pm Operator : QN Sample : 312205 -004 Misc ALS Vial : 10 Sample Multiplier: 1

Quant Time: Oct 17 18:46:50 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M -Quant Title .


Internal Standards R.T. QIon Response Conc Units Dev(Min)

1) 1,4-Dioxane d8 3) NDMA-d6 5) NDEA-d10

Target Compounds 2) 1,4- Dioxane

7.40 96 311386 9.12 80 442309

11.30 112 450920

7.45 88 13551

20.00 ug/L -0.18 20.00 ug/L -0.17 20.00 ug/L -0.17

Qvalue 0.94 ug/L 89


1625M 041311F2.M Wed Oct 17 18:46:50 2012

CONFIDENTIAL

Page: 1

LMC- PET -00002170



Quant Time: Oct 17 19:13:15 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625 -Quant Title .

M 041311F2.M


Internal Standards R.T. QIon Response

1) 1,4-Dioxane d8 7.41 96 535656 3) NDMA-d6 9.12 80 787681 5) NDEA-d10 11.30 112 733523

Target Compounds

Conc Units Dev(Min)

20.00 ug/L -0.17 20.00 ug/L -0.17 20.00 ug/L -0.17

Qvalue


1625 M 041311F2.M Wed Oct 17 19:13:15 2012 Page: 1

LAE : PIPPE272




Quant Time: Oct 17 19:13:15 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M Quant Title QLast Update : Wed May 05 16:21:01 2010 Response via : Initial Calibration

Abundance 48000

46000

44000

42000

40000

38000

36000

34000

32000

30000

28000

26000

24000

22000.

20000

18000

16000

14000

12000

10000

8000

6000

4000

2000

2 z

TIC: 10-17-12_11.D

\,-

Time -> 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50

1625 M 041311F2.M Wed Oct 17 19:13:16 2012

CONFIDENTIAL

Page: 2

LAB :7 7'a

LMC- PET -00002172


Data Path : C: \MSDChem \1 \DATA \NDMA 1 4 Dioxane \20121017\ Data File : ICV @lOppb -02.D Acq On : 17 Oct 2012 7:22 pm Operator : QN Sample : ICV @lOppb Misc : W -6204 ALS Vial : 100 Sample Multiplier: 1

Quant Time: Oct 18 15:20:29 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625_M_041311F2.M

_Quant Title .


I. bundance

190000

180000

170000

160000

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140000

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TIC: [email protected]

m

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1625 M 041311F2.M Thu Oct 18 15:20:46 2012

CONFIDENTIAL

Page: 2

A L i : Ezi

LMC- PET -00002173


Data Path : C: \MSDChem \1 \DATA \NDMA 1 4 Dioxane \20121017\

Data File : ICV @lOppb -02.D Acq On : 17 Oct 2012 7:22 pm

Operator : QN Sample : ICV @lOppb Misc : W -6204 ALS Vial : 100 Sample Multiplier: 1

Quant Time: Oct 18 15:20:29 2012 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M

Quant Title .



1) 1,4-Dioxane d8 .3) NDMA-d6 5) NDEA-d10

7.41 96 1898343 20.00 ug/L -0.17

9.11 80 2902619 20.00 ug/L -0.18

11.29 112 2568711 20.00 ug/L -0.18

Target Compounds Qvalue

' 2) 1,4-Dioxane 7.46 88 911626 10.39 ug/L 98

4) NDMA 9.15 74 1234236 9.58 ug/L 99

6) NDEA 11.34 102 1251225 11.20 ug/L 97


1625 M 041311F2.M Thu Oct 18 15:20:30 2012

CONFIDENTIAL

Page: 1

.e..0^i x F g.- ---,.

LMC- PET -00002174

Calibration Status Report SVOA -MS1

Method Path Method File Title Last Update Response Via

# ID Conc

:

:

:

:

C: \MSDCHEM \1 \METHODS\ 1625 M 041311F2.M

Wed May 05 16:21:01 2010 Initial Calibration

ISTD Path \File Conc

1 1 2 20 C:\MSDChem\1\DATA\NDMA 1 4 Dioxane\20110413\ca11.D

2 2 5 20 C:\MSDChem\1\DATA\NDMA_1_4_Dioxane\20090108\Jan08001.D 3 3 10 20 C: \MSDChem\1\DATA\NDMA 1 4 Dioxane\20090108\Jan08002.D

4 4 20 20 C:\MSDChem\l\DATA\NDMA-1-4-Dioxane\20090108\Jan08003.D 5 5 50 20 C:\MSDChem\1\DATA\NDMA_114_Dioxane\20090108\Jan08004.D 6 6 100 20 C:\MSDChem\1\DATA\NDMA 1 4 Dioxane\20090108\Jan08005.D

# ID Update Time Quant Time Acquisition Time

1 1 Apr 13 15:16 2011 Apr 13 14:59 2011 13 Apr 2011 12:42 pm

2 2 Apr 13 15:17 2011 Apr 13 14:59 2011 13 Apr 2011 12:42 pm

3 3 Apr 13 15:17 2011 Apr 13 14:59 2011 13 Apr 2011 12:42 pm

4 4 Apr 13 15:18 2011 Apr 13 14:59 2011 13 Apr 2011 12:42 pm

5 5 Apr 13 15:20 2011 Apr 13 14:59 2011 13 Apr 2011 12:42 pm

6 6 Apr 13 15:20 2011 Apr 13 14:59 2011 13 Apr 2011 12 :42 pm

1625 M 041311F2.M Wed Oct 17 12:14:14 2012

A ë t


Response Ratio

3.5-

3-

2.5-

2-

1.5-

1-

0.5-

NDMA

0

0 1

1 I I 1

2 3 4 5

Amount Ratio

Resp Ratio = 8.88e -001 * Amt RF Rel Std Dev = 6.9% Curve Fit: Avg RF

Method Name: C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M Calibration Table Last Updated: Wed May 05 16:21:01 2010

CONFIDENTIAL

AS : gtM-7-17= 7 ;.

LMC- PET -00002176

NDEA Response Ratio

4.5-

4-

3.5-

3-

2.5-

2-

1.5-

0.5-

0

0 1

'

2 3 4 5

Amount Ratio


Method Name: C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M Calibration Table Last Updated: Wed May 05 16:21:01 2010


Response Ratio

4.5-1

4-

3-

2.5-

2-

1.5-

1-

0.5-

-

0 )2

/ D/

1,4-Dioxane

/

/ 0

/

I 1 I I

0 1 2 3 4 5

Amount Ratio


Method Name: C: \MSDCHEM \l \METHODS \1625 M 041311F2.M Calibration Table Last Updated: Wed May-0-5- 16:21:01 2010

CONFIDENTIAL

ÿ m- g ___

LMC- PET -00002178


Data Path : C: \MSDChem \l\ DATA\ NDMA _1_4_Dioxane \z20098270MData \20090108\ Data File : Jan08008.D Acq On 8 Jan 2009 9:19 pm Operator : SD Sample : 1625 ICV- Old lOppm Misc : w -5133, Spike =10, IS =20 ALS Vial : 1 Sample Multiplier: 1

Quant Time: Jan 09 11:25:24 2009 Quant Method : C: \MSDCHEM \1 \METHODS \1625 -Quant Title .

M 010809.M

QLast Update : Fri Jan 09 10:23:29 2009 Response via : Initial Calibration


1) 1,4-Dioxane d8 7.63 96 1878033 20.00 ug/L 0.00__

3) NDMA-d6 9.34 80 2920326 20.00 ug/L 0.00

5) NDEA-dl0 11.52 112 2501029 20.00 ug/L 0.00

Target Compounds Qvalue

2) 1,4- Dioxane 7.68 88 843346 9.72 ug /L 100

4) NDMA 9.38 74 1289108 9.94 ug /L 99

6) NDEA 11.57 102 1132556 10.41 ug /L 100


1625 M 041311F2.M Wed Oct 17 12:19:37 2012

CONFIDENTIAL

Page: 1

LB a3-

LMC- PET -00002179


Data Path : C: \MSDChem \1\ DATA\ NDMA _1_4_Dioxane \z20098270MData \20090108\ Data File : Jan08008.D Acq On 8 Jan 2009 9:19 pm Operator : SD Sample : 1625 ICV- Old_l0ppm Misc : w -5133, Spike =10, IS =20 ALS Vial : 1 Sample Multiplier: 1

Quant Time: Jan 09 11:25:24 2009 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 010809.M Quant Title .

QLast Update : Fri Jan 09 10:23:29 2009 Response via : Initial Calibration

Abundance TIC: Jan08008.D

220000

210000

200000

190000

6 180000 -Z

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0 0 150000 x

0

z

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1625 M 041311F2.M Wed Oct 17 12:19:39 2012

CONFIDENTIAL

Page: 2

-10-21-11

LMC-PET-00002180


Data Path : C: \MSDChem \l\ DATA\ NDMA _1_4_Dioxane \z20118270MData \20110413\ Data File : Apr13- CCVÎ.D Acq On : 13 Apr 2011 5:54 pm Operator : QN Sample : ICV @lOppb Misc : w -5913 ALS Vial : 100 Sample Multiplier: 1

Quant Time: Apr 14 12:32:42 2011 Quant Method : C: \MSDCHEM \1 \METHODS \1625_M_041311F2.M "Quant Title : 1ppm method QLast Update : Wed Apr 13 15:21:31 2011 Response via : Initial Calibration


1) 1,4-Dioxane d8 7.53 96 1010029 20.00 ug/L -0.04 3) NDMA-d6 9.25 80 1395845 20.00 ug/L -0.04 .5) NDEA-d10 11.44 112 1411218 20.00 ug/L -0.03

Target Compounds Qvalue 2) 1,4- Dioxane 7.58 88 462323 9.92 ug /L 92

4) NDMA 9.29 74 650596 10.19 ug /L # 79

6) NDEA 11.48 102 662698 10.48 ug /L 87


1625 M 041311F2.M Wed Oct 17 12:21:20 2012

t: r. _ x , .. CONFIDENTIAL

Page: 1

LMC- PET -00002181


Data Path : C: \MSDChem \1\ DATA\ NDMA _1_4_Dioxane \z20118270MData \20110413\ Data File : Apr13- CCV1.D Acq On : 13 Apr 2011 5:54 pm Operator : QN Sample : ICV @lOppb Misc : w -5913 ALS Vial : 100 Sample Multiplier: 1

Quant Time: Apr 14 12:32:42 2011 Quant Method : C: \MSDCHEM \1 \METHODS \1625 M 041311F2.M

' Quant Title : 1ppm method QLast Update : Wed Apr 13 15:21:31 2011 Response via : Initial Calibration

Abundance TIC: Apr13-CCV1.D

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1625 M 041311F2.M Wed Oct 17 12:21:22 2012

CONFIDENTIAL

Page: 2

A? AB : 91 1712 3

LMC- PET -00002182

Appendix E

Hydrographs for Wells with Transducers


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Appendix F

Hydrographs for Manually Gauged Wells


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calibration - · pdf file# id update time quant time acquisition time 1 1 apr 13 15:16 2011...

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