zetium (wdxrf) and iso 13032 (edxrf) in this example an iso-octane certified reference material...

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Petro edition ZETIUM

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Page 1: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

Petro edition

ZETIUM

Page 2: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

ZETIUM PETRO EDITION

Elemental innovation Continuous development, improved customer experienceScientifically-sound, benefits-driven innovations implemented

in the Petro edition of the Zetium spectrometer make it the

most powerful multipurpose tool for the analysis of a wide

range of fuels, oils, catalysts as well as chemicals.

Elemental intelligence Advanced analytical software for advanced analytical hardwareA quantum step for our renowned SuperQ software gives

access to new technology combinations and analytical

possibilities. Starring the Virtual Analyst, it enhances the user

experience in setting up and operating the system.

Page 3: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

The Petro edition of the Zetium spectrometer

provides a flexible tool for the compliant analysis

of petrochemicals, oils and fuels to meet the

demanding requirements in regulated environments.

To meet customer’s expectations, spectrometers

can be optimized to your budget and performance

requirements.

Elemental technology 60 years of experience and heritage - the ideal starting pointThe Petro edition of the Zetium spectrometer represents the

next generation of a remarkably successful series of WDXRF

platforms, including the Axios, MagiX and PW2400. Proven

technology has been refined and brought forward onto the

Zetium platform, infusing a level of heritage and prestige.

Elemental support Transparent and reliable support in your neighborhoodFrom service to expertise, training to laboratory analysis

the Petro edition of the Zetium spectrometer is supported

from every angle. With a worldwide network of experienced

engineers coupled with the industry’s largest pool of

application scientists, PANalytical is always on hand to help you

meet your analytical requirements.

Page 4: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

ZETIUM PETRO EDITION

Guaranteed complianceThe Petro edition of the Zetium XRF spectrometer delivers unrivalled analytical performance, speed and

robustness through the seamless amalgamation of PANalytical’s core and innovative technologies.

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Consistent long-term measurements across the power range The Petro edition of the Zetium spectrometer

incorporates the flexibility to cater for different

requirements. Zetium can be configured as an

economical 1 kW configuration or up to a 4 kW

configuration, delivering the fastest time to results and

the lowest detection limits. The unique drift-free SST

R-mAX X-ray tubes with ZETA technology eliminate the

largest source of instrument drift, resulting in stable

calibrations that can be used for many months.

Faster fuel and oil analysisExcellent detection limits can be achieved even faster,

due to the incorporation of laterally curved crystals,

which deliver 30% more intensity.

Combined technologies, unlimited benefits A single platform combines sequential and simultaneous

analysis. SumXcore technology, an innovative

combination of WD- and EDXRF technologies, offers

WD- and EDXRF norm compliance on one spectrometer

and a fast and powerful screening tool for XRF analysis.

The entire spectrum can also be rapidly collected

during routine analyis facilitating rapid detection of

contaminants during process control.

In-house expertise with Virtual Analyst The Virtual Analyst, delivered with our latest version of

SuperQ analytical software, ensures that specialist-level

expertise is available to you 24/7, for the development of

new applications. Virtual Analyst actively calculates the

ideal measurement conditions, taking into account the

configuration of the spectrometer, sample preparation

information, the required analytical range, detection

limits and required precision.

Page 5: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

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Compliance guarantee with the fuels and lubrication oils compliance moduleKeep your licence to operate!

The accuracy of your results is supported by

independent checks using NIST traceable reference

materials. The fuels and lubrication oils compliance

package is factory pre-calibrated according to

ASTM D2622 and D6443 standard test methods.

It contains application templates and a Quick Start

Guide to create your own petrochemical methods,

the official documents of the standard test methods

together with a calibration set and a QC sample to

verify the pre-calibration.

Standards for refining catalysts Developed to provide the best calibration materials

for accurate analysis of refining catalysts such as

fluid cracking, hydro-treating and more, the WROXI

calibration module consists of methods and setup

samples for the accurate analysis of 21 elements

including Mg, Al, Si, Mo, V, Fe, Ni, Co and Hf.

Improved catalyst-killer detection. The Petro edition of the Zetium spectrometer

further reduces the detection limits for important

'catalyst killer' elements such as V and Ni thanks to

its unique duplex detector.

Page 6: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

ZETIUM PETRO EDITION

SumXcore technology for proven WD- and EDXRF complianceAnalysis of sulfur in gasoline using SumXcore technologyTrust in your elemental analysis is supported by compliant

measurements and results. The Petro edition of the Zetium

spectrometer, equipped with our revolutionary SumXcore

delivers compliance to both wavelength dispersive X-ray

fluorescence (WDXRF) and energy dispersive X-ray fluorescence

(EDXRF) international test methods related to the analysis

of petrochemicals. Of the most commonly used EDXRF and

WDXRF test methods for the analysis of sulfur (S) in gasoline:

ISO 13032, 20884 and ASTM International D4294, D2622, two

of the most stringent methods were chosen. Analysis was

performed using certified reference materials to demonstrate

compliance.

The integration of the ED core into the Zetium platform sees

two technologies, namely WD- and EDXRF, converging to

make up a unique and powerful analytical heart that we call

SumXcore, which delivers unique benefits for petrochemical

applications.

Analysis of sulfur compliant to D2622 (WDXRF) and ISO 13032 (EDXRF)In this example an iso-octane certified reference material

containing 15 mg/kg sulfur was analyzed according to

norm requirements. Iso-octane is a commonly used material

to simulate gasoline in XRF analysis, as its hydrocarbon

composition is similar to the composition of gasoline.

The results, summarized in the table, demonstrate that the

repeatability is well within the boundaries set by both the most

stringent ISO and ASTM International standard test methods.

The Petro edition of the Zetium XRF spectrometer,

is capable of meeting the requirements for both EDXRF

and WDRF international standard test methods for the analysis

of S in gasoline on a single platform.

EDcore WDcoreAverage sulfur concentration (mg/kg) 14.8 14.9

Maximum repeatability difference (mg/kg)

0.9 0.4

Maximum repeatability difference allowed ISO13032 (mg/kg)

1.1 -

Maximum repeatability difference allowed ASTM D2622 (mg/kg)

- 1.1WD core + ED core = SumXcore• Dual compliance

• Reduced analysis times by up to 50 %

• Identify and flag unexpected elements

• Fast sample screening

• Spectrum archiving

Page 7: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

1. SERVICE 3. TRAINING & EDUCATION

2. EXPERTISE 4. ANALYSIS & STANDARDS PREPARATION

Analytical services to ISO 17025

compliance at a dedicated

facility: PANalytical Nottingham

Accredited analysis of customer

samples e.g. in-house standards

Production of customized

standards

Regular courses worldwide in

various languages

Customized training to cater for

beginners and advanced users,

delivered on-site or at one of our

competence centers

Access to a wide and expanding

published knowledge center

Regular webinars with

on-demand access

Regional workshops and user

days

Access to the industry’s largest

pool of application specialists

either by phone, remote

connection or on-site visit.

Complete analytical solutions

including:

• Sample preparation

• In-house fusion expertise

• Ready-to-go application

solutions

• Design and integration of

automation solutions

• Method development and

optimization

• Method maintenance to ensure

independent validation

• Multi-laboratory

standardization - SOP

Participation in development of

international norms

Worldwide network of

experienced engineers backed

by regional and headquarter

specialists

Tailor-made support packages

with three tiers of support by

phone, by remote connection,

or on site

Performance certificates after

every service

Rapid dispatch of spare parts

Guaranteed 10 year replacement

of parts after production of your

instrument

Software and hardware upgrades

are available if your requirements

change or if new innovations

arise.

Elemental support

Page 8: ZETIUM (WDXRF) and ISO 13032 (EDXRF) In this example an iso-octane certified reference material containing 15 mg/kg sulfur was analyzed according to norm requirements. Iso-octane is

ZETIUM PETRO EDITION

Although diligent care has been used to ensure that the information herein is accurate, nothing contained herein can be construed to imply any representation or warranty as to the accuracy, currency or completeness

of this information. The content hereof is subject to change without further notice. Please contact us for the latest version of this document or further information. © PANalytical B.V. 2009. 9498 707 47011 PN9764

www.panalytical.com/zetium

Global and near PANalytical B.V.

Lelyweg 1, 7602 EA Almelo

P.O. Box 13, 7600 AA Almelo

The Netherlands

T +31 546 534 444

F +31 546 534 598

[email protected]

www.panalytical.com

Regional sales offices

Americas

T +1 508 647 1100

F +1 508 647 1115

Europe, Middle East, Africa

T +31 546 834 444

F +31 546 834 969

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T +65 6741 2868

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Care AgreementsOur customer support solutions have been developed with your business in mind. They are formulated as a family of four Care Agreements which can be tailored to your specific needs and provide fast, secure and reliable support.

• ECONOMY: indispensable coverage for self-sufficient operations

• ADVANCED: cost-effective support for routine usage

• PREMIUM: flexible package for high equipment usage

• ELITE: most comprehensive package

for demanding environments

About PANalyticalPANalytical’s mission is to enable people to get valuable insight into their materials and processes. Our customers can be found in virtually every industry segment, from building materials to pharmaceuticals and from metals and mining to nanomaterials. The combination of our software and instrumentation, based on X-ray diffraction (XRD), X-ray fluorescence (XRF), near-infrared (NIR) and optical emission (OES) spectroscopy and pulsed fast thermal neutron activation (PFTNA), provides our customers with highly reliable and robust elemental and structural information on their materials and is applied in scientific research and industrial process and quality control.

PANalytical employs over 1,000 people worldwide. The company’s headquarters are in Almelo, the Netherlands. Fully equipped application laboratories are established in Japan, China, the US, Brazil, and the Netherlands. PANalytical’s research activities are based in Almelo (NL) and on the campus of the University of Sussex in Brighton (UK). Supply and competence centers are located on two sites in the Netherlands: Almelo (X-ray instruments) and Eindhoven (X-ray tubes), in Nottingham, UK (XRF applications and standards), in Quebec, Canada (fusion sample preparation) and in Boulder CO, US (near-infrared instruments). PANalytical is active in all but a few countries of the world. This worldwide sales and service network ensures unrivalled levels of customer support. The company is certified in accordance with ISO 9001 and ISO 14001.

Visit www.panalytical.com for more information about our activities.

PANalytical is part of Spectris plc, the productivity-enhancing instrumentation and controls company.

Access to expertiseWith the largest service network we are able

to offer the most comprehensive support

package possible.

Expertise:

• On-site training available

• XRF training courses

• Performance optimization

• Customizable expertise programs

• Assistance with multi-laboratory

standardization