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U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, SCIENCE and ECOSYSTEM SUPPORT DIVISION ATHENS, GEORGIA 30605-2720 4SESD-EIB 1 0 MEMORANDUM SUBJECT: Results, June 2000 Polychlorinated Biphenyl Ambient Air Study Anniston, Alabama SESD Project No. 00-0355 FROM: Tim Slagle Air and Superfund Section THRU: Archie Lee, Chief Superfund and Air Sectio TO: D. Karen Knight, CHMM On-Scene Coordinator I have attached the laboratory results, and locations of the samples we collected during the April 2000 Air study that SESD conducted in Anniston, Alabama. cc: Archie Lee Annie Godfrey, Remedial Project Manager Elmer Akin Tim Simpson

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Page 1: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

U.S. ENVIRONMENTAL PROTECTION AGENCYREGION 4, SCIENCE and ECOSYSTEM SUPPORT DIVISION

ATHENS, GEORGIA 30605-2720

4SESD-EIB1 0

MEMORANDUM

SUBJECT: Results, June 2000 Polychlorinated Biphenyl Ambient Air StudyAnniston, AlabamaSESD Project No. 00-0355

FROM: Tim SlagleAir and Superfund Section

THRU: Archie Lee, ChiefSuperfund and Air Sectio

TO: D. Karen Knight, CHMMOn-Scene Coordinator

I have attached the laboratory results, and locations of the samples we collected during the April2000 Air study that SESD conducted in Anniston, Alabama.

cc: Archie LeeAnnie Godfrey, Remedial Project ManagerElmer AkinTim Simpson

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POLYCHLORINATED BIPHENYL AMBIENT AIR STUDYANNISTON, ALABAMA

JUNE 2000

INTRODUCTION

At the request of Karen Knight of the United States Environmental Protection Agency,Region 4, Waste Management Division, Emergency Response and Removal Branch, RemovalOperations Section, Tim Slagle and staff, USEPA Region IV, Science and Ecosystem SupportDivision (SESD) conducted a PCB air investigation around the Solutia facility located inAnniston, Alabama. The investigation was composed of two air sampling events; June 27th thru28th and June 28* thru June 29th.

STUDY DESIGN

The purpose of the study is to assess PCBs (polychlorinated biphenyls) as aroclors andcongener concentrations in ambient air around the Solutia facility (see MAP 1).

Congeners are individual PCBs. Aroclors are mixtures of congeners formulated forspecific high temperature applications, such as insulating oils in electrical transformers, hydraulicfluids and have also been used as a binding agent for sand casting in foundries. Congener analysiswas performed to provide additional information as to origin of contamination sources and willbe used to evaluate total PCB exposure.

The data collected will be used to provide data for HRS (Hazard Ranking System) forpackage submittal for possible CERCLA (Comprehensive Environmental Response,Compensation, and Liability Act) NPL (National Priority Listing).

Air monitoring sites were located within 1/4 mile rings around the suspected primarysource. A background air monitoring site was established upwind of the facility. Each samplingsite is described below:

SITE DESCRIPTIONPD-HV-A Wellborn High School, 135 Pinson Road (Background Site)PD-HV-B South Hunter StreetPD-HV-C Vacant Lot, between Hunter Street and 3rd StreetPD-HV-D Ware Street and 9th Street

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PD-HV-E Clydesdale Avenue and 12th StreetPD-HV-F Head Start School, 1000 West 12th StreetPD-HV-G Lincoln Park, Zinn ParkwayPD-HV-GD (Duplicate) Lincoln Park, Zinn ParkwayPD-HV-H Nobel Street and 13th Street (Downtown Anniston)PD-HV-I Meteorological Station, 7th Street

SITING OBJECTIVES

Air monitoring sites PD-HV-B through PD-HV-G were located throughout thecommunity near the Solutia facility in the city of Anniston, Alabama. The siting criteria werebased on U.S. EPA Region IV requirements. Site PD-HV-A was established at the WellbornHigh School as a background location for this sampling event. It was used to collect ambient airsamples that ascertain the PCB concentrations of the general area, but is not immediately affectedby the Solutia facility. Site PD-HV-H was located in downtown Anniston approximately 1.5miles east of the facility. A meteorological station was established on 7th Street (site PD-HV-I)within the Solutia complex, which was a central location in the study area, to measure windspeed and direction.

SAMPLING PROCEDURE

All samples were collected in accordance with the Environmental InvestigationsStandard Operation Procedures and Quality Assurance Manual (E1SOPQAM), May 1996 Allsamples were analyzed at the SESD laboratory in Athens, Georgia, in accordance with theAnalytical Support Branch Laboratory Operations and Quality Control Manual, December1997. Air samples were collected at a nominal flow rate of 220-liters per minute over an 24-hourinterval.

ANALYTICAL PLAN

The 24 hour high volume air samples were collected and analyzed by the EPA, Region 4,SESD laboratory in Athens, Georgia, for the presence of Polychlorinated Biphenyls (PCBs) asaroclors and PCB congengers in accordance with Method TO-4A as described in the EPACompendium of Methods for the Determination of Toxic Organic Compounds in AmbientAir. A surrogate mixture was added to each PUF/XAD cartridge before extraction. Thepaniculate filter and PUF/XAD cartridge was Soxhlet extracted for approximately 24 hours usinga 5% ether in hexane solution. The sample extract was analyzed for the target PCBs as aroclorsand PCB congeners listed in Table 1 by using a Gas Chromatograph equipped with an ElectronCapture Detector.

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QUALITY ASSURANCE

All polyurethane foam and XAD (PUF-XAD) sampling cartridges were analyzed afterinitial cleanup and prior to sampling to verify the cleanup efficiency. A duplicate set of samples,(PD-HV-G and PD-HV-GD) were taken at the Lincoln Park site. They were used to show theprecision of the monitoring method. Air sampling flow rates were checked at the beginning andend of each sampling run. Two PUF/XAD sampling cartridge field blanks, QA-001-FA and QA-002-FA), were collected. The field blanks were transported into the field and handled like anordinary sample but not exposed to check for operator induced contamination and to check thepossibility of contamination during transport and storage.

RESULTS

The two field blanks QA-001-FA (sampling period 1) and QA-002-FA (sampling period2) collected during the study showed no evidence of being contaminated with PCBs or PCBcongeners.

Windspeed and direction data was collected during the study is contained in Appendix AThe data for the air monitoring investigation study indicates that the predominate wind directionwas from the southwest to the northeast.

The winds during the 1st sampling period (June 27-29) were mainly from the southwestwith hourly average speeds up to 19 miles per hour for about 73% of the time. Winds were calm(less than 2 mph) for 27% of the sampling time, and occurred between the hours of 8pm to 7am.No rain fall was recorded in the sampling area.

The winds during the 2nd sampling period (June 29-30) were also mainly from thesouthwest with hourly average speeds up to 21 miles per hour for about 87% of the time. Windswere calm (less than 2 mph) for 13% of the sampling time, and occurred between mid-night to4am. Heavy rain fall was recorded for one hour, from 9am to 10am on June 29.

Results from the analysis of the high volume air samples for the investigation aresummarized in Table 2, the laboratory analysis sheets are attached as Appendix B.

Site A (PD-HV-A) Wellborn High School; The background or upwind siteapproximately one and one half miles west of the study area, no aroclors, were detected duringeither sampling period. But during the 2nd sampling period, PCB congener 74 was detected at aconcentration of 0.0003 0 ug/m3.

Site B (PD-HV-B) South Hunter Street; No aroclors were detected on either day ofsampling and no PCB congeners were detected during the first sampling period. However, duringthe second sampling period, PCB congeners 28, 60, 74 and 156 were detected. This was the only

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sampling period and location that PCB congener 156 was detected.

Site C (PD-HV-O the vacant lot, between Hunter Street and 3rd Street; PCB-1242and PCB congeners 28 and 74 were detected during both sampling periods.

Site D (PD-HV-D) the monitoring site at Ware Street and 9th Street; The highestconcentrations of PCB-1242 (aroclor 1242) and congeners during the air monitoring investigationwere detected at this site. Concentrations were highest during the 1st sampling period with PCB-1242 (aroclor 1242) at 0.045 ug/m3 and a sum total of the PCB congeners concentrations of0.00833 ug/m3.

Site E (PD-HV-E) the monitoring site at Clydesdale Avenue and 12th Street; PCB-1242 (aroclor 1242) and PCB congeners 28, 60 and 74 were detected during both 24-hoursampling periods.

Site F fPD-HV-F) Head Start School; PCB-1242 (aroclor 1242) and PCB congeners28, 60 and 74 were detected during the 1st sampling period. But only PCB congeners 28 and 60were detected during the 2nd sampling period.

Sites G and G-Duplicate (PD-HV-G and PD-HV-G-Duplicate) the duplicatesampling locations at Lincoln Park; Were chosen based on previous air and soil studies inconjunction with prevailing wind and drainage data. This information indicated this locationwould be the area of highest suspected airborne concentrations of aroclors and PCB congeners.The co-located samples collected at Site G and Site G-Duplicate compared well for very lowconcentrations, but some variability was shown. During the 2nd sampling period PCB congener66 was detected at a concentration of 0.00010 ug/m3 at Site G but not at Site G-Duplicate.

Site H (PD-HV-H) the down town Anniston site; Approximately one and a half mileseast of the study area, no aroclors were detected during either sampling period but during the 2nd

sampling period PCB congener 28 was detected at a concentration of 0.00032 ug/m3.

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Table 1

Target PCB (Aroclor) Analytes

PCB - 1242 (AROCLOR 1242)PCB - 1254 (AROCLOR 1254)PCB - 1221 (AROCLOR 1221)PCB - 1232 (AROCLOR 1232)PCB - 1248 (AROCLOR 1248)PCB - 1260 (AROCLOR 1260)PCB - 1016 (AROCLOR 1016)PCB - 1268 (AROCLOR 1268)

Target PCB Congengers

PCB Congener 28 PCB Congener 163PCB Congener 52 PCB Congener 169PCB Congener 60 PCB Congener 170PCB Congener 66 PCB Congener 180PCB Congener 74 PCB Congener 183PCB Congener 77 PCB Congener 187PCB Congener 81 PCB Congener 194PCB Congener 99 PCB Congener 195PCB Congener 101 PCB Congener 196PCB Congener 105 PCB Congener 201PCB Congener 118 PCB Congener 203PCB Congener 126 PCB Congener 206PCB Congener 138 PCB Congener 208PCB Congener 153 PCB Congener 209PCB Congener 156

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TABLE 2Anniston, Alabama PCB Air Study

Sample Period 1 Beginning June 27, 2000 Ending June 28, 2000Compoundconcentrations in ug/m3

PCB-1242 (Aroclor 1242)

PCB Congener 28

PCB Congener 52

PCB Congener 60

PCB Congener 66

PCB Congener 74

PCB Congener 81

PCB Congener 101

PCB Congener 156

Site ABackgroundPDHVA27

-

-

-

-

-

-

-

-

-

SiteBPDHVB27

~

~

-

-

-

-

~

-

-

SiteCPDHVC27

0.0046

0.0003 IN

--

--

-

0.00030N

-

--

--

SiteDPDHVD27

0.045

0.0044

0.0020N

0.00087N

0.00013N

0.00052

0.000 19N

0.00022N

--

SiteEPDHVE27

0.0073

0.00071

-

0.00037N

-

0.00039N

-

-

--

SiteFPDHVF27

0.0033J

0.00023

-

0.00023N

-

0.00071N

-

-

-

SiteGPDHVG27

-

0.00016J

-

-

-

-

Site G-DupDuplicatePDHVGD27

-

0.00012J

~

-

-

-

-

~

-

SiteHDowntownPDHVH27

-

-

--

-

-

~

-

--

-

Sample Period 2 Beginning June 28, 2000 Ending June 29, 2000

Compoundconcentrations in ug/m3

PCB-1242 (Aroclor 1242)

PCB Congener 28

PCB Congener 52

PCB Congener 60

PCB Congener 66

PCB Congener 74

PCB Congener 8 1

PCB Congener 101

PCB Congener 156

Site ABackgroundPDHVA28

-

-

--

--

-

0.00030N

-

--

--

SiteBPDHVB28

-

0.00017N

-

0.000 18N

--

0.000 17N

--

-

0.00032N

SiteCPDHVC28

0.0088

0.00072

--

-

--

0.0037N

--

--

-

SiteDPDHVD28

0.025

0.0025

-

--

-

0.00039N

--

-

-

SiteEPDHVE28

0.025

0.0022

-

0.00042N

-

0.0003 5N

-

--

--

SiteFPDHVF28

-

0.00084

-

0.00032N

-

-

--

-

--

SiteGPDHVG28

0.0057J

0.00040

-

0.00020N

0.000 10 JN

--

--

--

-

Site G-DupDuplicatePDHVGD28

0.0086

0.00057

-

0.00037N

-

--

--

--

--

SiteHDowntownPDHVH28

-

0.00032JN

-

--

-

--

-

-

-J = Estimated Value N = Presumptive evidence of presence of material — - Below Detection Limits

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MAPIANNISTON, ALABAMA PCB SITE

AIR MONITORING STUDY JUNE 27-29,2000

• Air Sampling LocationsA Meteorological StationO 0.25 mile - Ring Intervals

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Appendix A

Windspeed and Direction Data

Anniston PCB Site, Alabama

June 27-29, 2000

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R M YOUNG CO. TRAVERSE CITY, MI26700 SERIES TRANSLATOR

DATE DATE TIME TIME WS:AVG WS:MAX WD:AVG WD:SDV T:AVG T:MIN T:MAXMON DAY HR MIN MPH MPH DEG DEG DEG F DEG F DEC F

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28282929299Q̂ ̂9Q£t ̂29292929292929292929

89101112131415161718192021222301234567391011121314151617181920212223012345678910111 9x ̂1314

0000000000000000000000000000000000000000000000000000000

3444455454331101641211126456677542333232111143334366566

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Appendix B

Laboratory Analysis Sheets

Anniston PCB Site, Alabama

June 27-29, 2000

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCYRegion 4

Science and Ecosystem Support Division980 College Station Road

Athens, Georgia 30605-2720

MEMORANDUM

Date: 07/19/2000

Subject: Results of PESTICIDES/PCB Sample Analysis00-0649 Anniston PCB Site

Anniston, AL

From: Revells, Lavon

To: Slagle, Tim

CC: SESD/EIB

Thru: Bennett,Acting Chief, Organic Chemistry SectionAnalytical Support Branch

Attached are the results of analysis of samples collected as part of the subject project. If you have anyquestions, please contact me.

ATTACHMENT

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8388 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

p H TQlAr iEProject Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/2000 08:45Program: SFE Ending:

Id/Station: QAFA627/FBMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0022U UG/M3 PCB-1 242 (AROCLOR 1242)0.0022U UG/M3 PCB-1 254 (AROCLOR 1254)0.0022U UG/M3 PCB-1221 (AROCLOR 1221)0.0022U UG/M3 PCB-1 232 (AROCLOR 1232)0.0022U UG/M3 PCB-1 248 (AROCLOR 1248)0.0022U UG/M3 PCB-1 260 (AROCLOR 1260)0.0022U UG/M3 PCB-1 01 6 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-matenal was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8388 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: QAFA627/FBMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 08:45Ending:

RESULTS UNITS ANALYTE0.0022U UG/M3 PCB-1268 (AROCLOR 1268)

0.00018U UG/M3 PCB Congener #280.00018U UG/M3 PCB Congener #520.00018U UG/M3 PCB Congener #600.00018U UG/M3 PCB Congener #660.00018U UG/M3 PCB Congener #740.00018U UG/M3 PCB Congener #770.00018U UG/M3 PCB Congener #810.00018U UG/M3 PCB Congener #990.00018U UG/M3 PCB Congener #1010.00018U UG/M3 PCB Congener #1050.00018U UG/M3 PCB Congener #1180.00018U UG/M3 PCB Congener #1260.00018U UG/M3 PCB Congener #1380.00018U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00018U UG/M3 PCB Congener #1630.00018U UG/M3 PCB Congener #1690.00018U UG/M3 PCB Congener #1700.00018U UG/M3 PCB Congener #1800.00018U UG/M3 PCB Congener #1830.00018U UG/M3 PCB Congener #1870.00018U UG/M3 PCB Congener #1940.00018U UG/M3 PCB Congener #1950.00018U UG/M3 PCB Congener #1960.00018U UG/M3 PCB Congener #2010.00018U UG/M3 PCB Congener #2030.00018U UG/M3 PCB Congener #2060.00018U UG/M3 PCB Congener #2080.00018U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8389 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SCAN Requestor:ruo OUMN Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/2000 09:04Program: SFE Ending:

Id/Station: PDHVA27 / AMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0020U UG/M3 PCB-1242 (AROCLOR 1242)0.0020U UG/M3 PCB-1254 (AROCLOR 1254)0.0020U UG/M3 PCB-1221 (AROCLOR 1221)0.0020U UG/M3 PCB-1232 (AROCLOR 1232)0.0020U UG/M3 PCB-1248 (AROCLOR 1248)0.0020U UG/M3 PCB-1260 (AROCLOR 1260)0.0020U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8389 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVA27 / AMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 09:04Ending:

RESULTS UNITS ANALYTE0.0020U UG/M3 PCB-1268 (AROCLOR 1268)

0.00016U UG/M3 PCB Congener #280.00016U UG/M3 PCB Congener #520.00016U UG/M3 PCB Congener #600.00016U UG/M3 PCB Congener #660.00016U UG/M3 PCB Congener #740.00016U UG/M3 PCB Congener #770.00016U UG/M3 PCB Congener #810.00016U UG/M3 PCB Congener #990.00016U UG/M3 PCB Congener #1010.00016U UG/M3 PCB Congener #1050.00016U UG/M3 PCB Congener #1180.00016U UG/M3 PCB Congener #1260.00016U UG/M3 PCB Congener #1380.00016U UG/M3 PCB Congener #1530.00016U UG/M3 PCB Congener #1560.00016U UG/M3 PCB Congener #1630.00016U UG/M3 PCB Congener #1690.00016U UG/M3 PCB Congener #1700.00016U UG/M3 PCB Congener #1800.00016U UG/M3 PCB Congener #1830.00016U UG/M3 PCB Congener #1870.00016U UG/M3 PCB Congener #1940.00016U UG/M3 PCB Congener #1950.00016U UG/M3 PCB Congener #1960.00016U UG/M3 PCB Congener #2010.00016U UG/M3 PCB Congener #2030.00016U UG/M3 PCB Congener #2060.00016U UG/M3 PCB Congener #2080.00016U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 17: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8390 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN peqUet?r:H TQ,Ar,pProject Leader: TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/27/2000 09:31Program: SFE Ending:

Id/Station: PDHVB27 / BMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1242 (AROCLOR 1242)0.0021 U UG/M3 PCB-1254 (AROCLOR 1254)0.0021U UG/M3 PCB-1221 (AROCLOR 1221)0.0021U UG/M3 PCB-1232 (AROCLOR 1232)0.0021 U UG/M3 PCB-1248 (AROCLOR 1248)0.0021 U UG/M3 PCB-1260 (AROCLOR 1260)0.0021U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 18: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8390 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVB27 / BMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 09:31Ending:

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1268(AROCLOR1268)

0.00017U UG/M3 PCB Congener #280.0001711 UG/M3 PCB Congener #520.00017U UG/M3 PCB Congener #600.00017U UG/M3 PCB Congener #660.00027U UG/M3 PCB Congener #740.00017U UG/M3 PCB Congener #770.00017U UG/M3 PCB Congener #810.00017U UG/M3 PCB Congener #990.00017U UG/M3 PCB Congener #1010.00017U UG/M3 PCB Congener #1050.00017U UG/M3 PCB Congener #1180.00017U UG/M3 PCB Congener #1260.0001711 UG/M3 PCB Congener #1380.00017U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00017U UG/M3 PCB Congener #1630.00017U UG/M3 PCB Congener #1690.00017U UG/M3 PCB Congener #1700.00017U UG/M3 PCB Congener #1800.00017U UG/M3 PCB Congener #1830.00017U UG/M3 PCB Congener #1870.00017U UG/M3 PCB Congener #1940.00017U UG/M3 PCB Congener #1950.00017U UG/M3 PCB Congener #1960.00017U UG/M3 PCB Congener #2010.00017U UG/M3 PCB Congener #2030.00017U UG/M3 PCB Congener #2060.00017U UG/M3 PCB Congener #2080.00017U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 19: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8391 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SCAN Requestor:rv,o OV.MIN Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/200010:00Program: SFE Ending:Id/Station: PDHVC27 / CMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0046 UG/M3 PCB-1242 (AROCLOR 1242)0.0022U UG/M3 PCB-1254 (AROCLOR 1254)0.0045U UG/M3 PCB-1221 (AROCLOR 1221)0.0045U UG/M3 PCB-1232 (AROCLOR 1232)0.0045U UG/M3 PCB-1248 (AROCLOR 1248)0.0022U UG/M3 PCB-1260 (AROCLOR 1260)0.0045U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 20: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8391 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVC27 / CMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 10:00Ending:

RESULTS UNITS ANALYTE0.0022U UG/M3 PCB-1268 (AROCLOR 1268)

0.00031 N UG/M3 PCB Congener #280.00052U UG/M3 PCB Congener #520.000171) UG/M3 PCB Congener #600.00017U UG/M3 PCB Congener #660.00030N UG/M3 PCB Congener #740.00017U UG/M3 PCB Congener #770.00017U UG/M3 PCB Congener #810.00017U UG/M3 PCB Congener #990.00017U UG/M3 PCB Congener #1010.00017U UG/M3 PCB Congener #1050.00017U UG/M3 PCB Congener #1180.00017U UG/M3 PCB Congener #1260.00017U UG/M3 PCB Congener #1380.00017U UG/M3 PCB Congener #1530.00017U UG/M3 PCB Congener #1560.00017U UG/M3 PCB Congener #1630.00017U UG/M3 PCB Congener #1690.00017U UG/M3 PCB Congener #1700.00017U UG/M3 PCB Congener #1800.00017U UG/M3 PCB Congener #1830.00017U UG/M3 PCB Congener #1870.00017U UG/M3 PCB Congener #1940.000171) UG/M3 PCB Congener #1950.00017U UG/M3 PCB Congener #1960.00017U UG/M3 PCB Congener #2010.00017U UG/M3 PCB Congener #2030.00017U UG/M3 PCB Congener #2060.00017U UG/M3 PCB Congener #2080.00017U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 21: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8392 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN *eqUef!°r:. TQ,*r,pProject Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/200010:25Program: SFE Ending:

Id/Station: PDHVD27 / DMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.045 UG/M3 PCB-1242 (AROCLOR 1242)

0.0025U UG/M3 PCB-1254 (AROCLOR 1254)0.040U UG/M3 PCB-1221 (AROCLOR 1221)0.040U UG/M3 PCB-1232 (AROCLOR 1232)0.040U UG/M3 PCB-1248 (AROCLOR 1248)

0.0025U UG/M3 PCB-1260 (AROCLOR 1260)0.040U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 22: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8392 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVD27 / DMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 10:25Ending:

RESULTS UNITS ANALYTE0.0025U UG/M3 PCB-1268 (AROCLOR 1268)0.0044 UG/M3 PCB Congener #280.0020N UG/M3 PCB Congener #52

0.00087N UG/M3 PCB Congener #600.00013N UG/M3 PCB Congener #660.00052 UG/M3 PCB Congener #740.00020U UG/M3 PCB Congener #770.00019N UG/M3 PCB Congener #810.00020U UG/M3 PCB Congener #990.00022N UG/M3 PCB Congener #1010.00021 U UG/M3 PCB Congener #1050.00020U UG/M3 PCB Congener #1180.00020U UG/M3 PCB Congener #1260.00020U UG/M3 PCB Congener #1380.00020U UG/M3 PCB Congener #1530.00020U UG/M3 PCB Congener #1560.00020U UG/M3 PCB Congener #1630.00020U UG/M3 PCB Congener #1690.00020U UG/M3 PCB Congener #1700.00020U UG/M3 PCB Congener #1800.00020U UG/M3 PCB Congener #1830.00020U UG/M3 PCB Congener #1870.00020U UG/M3 PCB Congener #1940.00020U UG/M3 PCB Congener #1950.00020U UG/M3 PCB Congener #1960.00020U UG/M3 PCB Congener #2010.00020U UG/M3 PCB Congener #2030.00020U UG/M3 PCB Congener #2060.00020U UG/M3 PCB Congener #2080.00020U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 23: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8393 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN *eqUe;fr:H ™4n,pProject Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/200010:53Program: SFE Ending:

Id/Station: PDHVE27 / EMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0073 UG/M3 PCB-1242 (AROCLOR 1242)0.0022U UG/M3 PCB-1254 (AROCLOR 1254)0.0070U UG/M3 PCB-1221 (AROCLOR 1221)0.0070U UG/M3 PCB-1232 (AROCLOR 1232)0.0070U UG/M3 PCB-1248 (AROCLOR 1248)0.0022U UG/M3 PCB-1260 (AROCLOR 1260)0.0070U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-matenal was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 24: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8393 FY 2000SPECIFIED TESTSFacility: Anniston PCS SiteProgram: SFEId/Station: PDHVE27/EMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 10:53Ending:

RESULTS UNITS ANALYTE0.0022U UG/M3 PCB-1268 (AROCLOR 1268)

0.00071 UG/M3 PCB Congener #280.0010U UG/M3 PCB Congener #52

0.00037N UG/M3 PCB Congener #600.00018U UG/M3 PCB Congener #660.00039N UG/M3 PCB Congener #740.00018U UG/M3 PCB Congener #770.00018U UG/M3 PCB Congener #810.00018U UG/M3 PCB Congener #990.00018U UG/M3 PCB Congener #1010.00018U UG/M3 PCB Congener #1050.000181) UG/M3 PCB Congener #1180.00018U UG/M3 PCB Congener #1260.00018U UG/M3 PCB Congener #1380.00018U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00018U UG/M3 PCB Congener #1630.00018U UG/M3 PCB Congener #1690.00018U UG/M3 PCB Congener #1700.00018U UG/M3 PCB Congener #1800.00018U UG/M3 PCB Congener #1830.00018U UG/M3 PCB Congener #1870.00018U UG/M3 PCB Congener #1940.00018U UG/M3 PCB Congener #1950.00018U UG/M3 PCB Congener #1960.00018U UG/M3 PCB Congener #2010.00018U UG/M3 PCB Congener #2030.00018U UG/M3 PCB Congener #2060.00018U UG/M3 PCB Congener #2080.00018U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 25: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8394 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN peqUef!°r:H TQIAr iPProject Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/27/200011:16Program: SFE Ending;

Id/Station: PDHVF27 / FMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0033J UG/M3 PCB-1242 (AROCLOR 1242)0.0022U UG/M3 PCB-1254 (AROCLOR 1254)0.0030U UG/M3 PCB-1221 (AROCLOR 1221)0.0030U UG/M3 PCB-1232 (AROCLOR 1232)0.0030U UG/M3 PCB-1248 (AROCLOR 1248)0.0022U UG/M3 PCB-1260 (AROCLOR 1260)0.0030U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 26: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8394 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station :PDHVF27/FMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 11:16Ending:

RESULTS0.0022U

0.000230.00057U0.00023N0.0001 8U0.00071 N0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.00018U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.00018U0.0001 8U0.0001 8U0.0001 8U0.00018U0.00018U0.0001 8U0.0001 8U0.0001 8U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 27: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8395 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SPAN Requestor:r^D OUMIN pro.ect Leader. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/27/200011 "56Program: SFE Ending:

Id/Station: PDHVG27 / GMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0025U UG/M3 PCB-1242 (AROCLOR 1242)0.0025U UG/M3 PCB-1254 (AROCLOR 1254)0.0025U UG/M3 PCB-1221 (AROCLOR 1221)0.0025U UG/M3 PCB-1232 (AROCLOR 1232)0.0025U UG/M3 PCB-1248 (AROCLOR 1248)0.0025U UG/M3 PCB-1260 (AROCLOR 1260)0.0025U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 28: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8395 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVG27 / GMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 11:56Ending:

RESULTS0.0025U

0.0001 6J0.00052U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00022U0.00020U0.00020U0.00020U0.00027U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U0.00020U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: l.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 29: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8396 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN *eqUef!°r:H TQ,Ar,PProject Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning-06/27/200011'56Program: SFE Ending:

Id/Station: PDHVGD27 / GDMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0024U UG/M3 PCB-1242 (AROCLOR 1242)0.0024U UG/M3 PCB-1254 (AROCLOR 1254)0.0024U UG/M3 PCB-1221 (AROCLOR 1221)0.0024U UG/M3 PCB-1232 (AROCLOR 1232)0.0024U UG/M3 PCB-1248 (AROCLOR 1248)0.0024U UG/M3 PCB-1260 (AROCLOR 1260)0.0024U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 30: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8396 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVGD27 / GDMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 11:56Ending:

RESULTS UNITS ANALYTE0.0024U UG/M3 PCB-1268 (AROCLOR 1268)

0.00012J UG/M3 PCB Congener #280.00040U UG/M3 PCB Congener #520.00019U UG/M3 PCB Congener #600.00019U UG/M3 PCB Congener #660.00019U UG/M3 PCB Congener #740.00019U UG/M3 PCB Congener #770.00019U UG/M3 PCB Congener #810.00019U UG/M3 PCB Congener #990.00019U UG/M3 PCB Congener #1010.00019U UG/M3 PCB Congener #1050.00019U UG/M3 PCB Congener #1180.00019U UG/M3 PCB Congener #1260.00019U UG/M3 PCB Congener #1380.00019U UG/M3 PCB Congener #1530.00019U UG/M3 PCB Congener #1560.00019U UG/M3 PCB Congener #1630.00019U UG/M3 PCB Congener #1690.00019U UG/M3 PCB Congener #1700.00019U UG/M3 PCB Congener #1800.00019U UG/M3 PCB Congener #1830.00019U UG/M3 PCB Congener #1870.00019U UG/M3 PCB Congener #1940.00019U UG/M3 PCB Congener #1950.00019U UG/M3 PCB Congener #1960.00019U UG/M3 PCB Congener #2010.00019U UG/M3 PCB Congener #2030.000191) UG/M3 PCB Congener #2060.00019U UG/M3 PCB Congener #2080.00019U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8397 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SCAN Requestor:PCB SCAN Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning-06/27/2000 12'44Program: SFE Ending;

Id/Station: PDHVH27 / HMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1242 (AROCLOR 1242)0.0021U UG/M3 PCB-1254 (AROCLOR 1254)0.0021U UG/M3 PCB-1221 (AROCLOR 1221)0.0021U UG/M3 PCB-1232 (AROCLOR 1232)0.0021U UG/M3 PCB-1248 (AROCLOR 1248)0.0021U UG/M3 PCB-1260 (AROCLOR 1260)0.0021U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 32: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8397 FY 2000 Project: 00-0649SPECIFIED TESTSFacility: Anniston PCB Site Anniston, ALProgram: SFEId/Station: PDHVH27 / HMedia: AMBIENT AIR

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/27/2000 12:44Ending:

RESULTS0.002 1U

0.0001 7U0.00023U0.0001 7U0.0001 7U0.00087U0.0001 7U0.0001 7U0.0001 7U0.0001 71)0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 9U0.00022U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 71)0.0001 7U0.0001 7U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8398 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCBSCAN Requestor:ruo OV.MN Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning-06/28/2000 08:05Program: SFE Ending;

Id/Station: QAFA628 / FBMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0022U UG/M3 PCB-1242 (AROCLOR 1242)0.0022U UG/M3 PCB-1254 (AROCLOR 1254)0.0022U UG/M3 PCB-1221 (AROCLOR 1221)0.0022U UG/M3 PCB-1232 (AROCLOR 1232)0.0022U UG/M3 PCB-1248 (AROCLOR 1248)0.0022U UG/M3 PCB-1260 (AROCLOR 1260)0.0022U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8398 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: QAFA628/FBMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 08:05Ending:

RESULTS0.0022U

0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.00018U0.00018U0.00018U0.0001 81)0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.00018U0.00018U0.00018U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8399 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCS SCAN project Leader. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning- 06/28/2000 09-15Program: SFE Ending.Id/Station: PDHVA28/AMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1242 (AROCLOR 1242)0.0021U UG/M3 PCB-1254 (AROCLOR 1254)0.0021U UG/M3 PCB-1221 (AROCLOR 1221)0.0021 U UG/M3 PCB-1232 (AROCLOR 1232)0.0021U UG/M3 PCB-1248 (AROCLOR 1248)0.0021 U UG/M3 PCB-1260 (AROCLOR 1260)0.0021U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value, NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8399 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVA28 / AMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 09:15Ending:

RESULTS UNITS ANALYTE0.0021 U UG/M3 PCB-1268 (AROCLOR 1268)

0.00017U UG/M3 PCB Congener #280.00020U UG/M3 PCB Congener #520.00017U UG/M3 PCB Congener #600.00017U UG/M3 PCB Congener #660.00030N UG/M3 PCB Congener #740.00017U UG/M3 PCB Congener #770.00017U UG/M3 PCB Congener #810.00017U UG/M3 PCB Congener #990.00017U UG/M3 PCB Congener #1010.00017U UG/M3 PCB Congener #1050.00017U UG/M3 PCB Congener #1180.00017U UG/M3 PCB Congener #1260.00017U UG/M3 PCB Congener #1380.00017U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00017U UG/M3 PCB Congener #1630.00017U UG/M3 PCB Congener #1690.00017U UG/M3 PCB Congener #1700.00017U UG/M3 PCB Congener #1800.00017U UG/M3 PCB Congener #1830.00017U UG/M3 PCB Congener #1870.00017U UG/M3 PCB Congener #1940.00017U UG/M3 PCB Congener #1950.00017U UG/M3 PCB Congener #1960.00017U UG/M3 PCB Congener #2010.00017U UG/M3 PCB Congener #2030.00017U UG/M3 PCB Congener #2060.00017U UG/M3 PCB Congener #2080.00017U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

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PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8400 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SCAN Requestor:

Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/28/2000 09:52Program: SFE Ending:

Id/Station: PDHVB28 / BMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1242 (AROCLOR 1242)0.0021U UG/M3 PCB-1254 (AROCLOR 1254)0.0021U UG/M3 PCB-1221 (AROCLOR 1221)0.0021U UG/M3 PCB-1232 (AROCLOR 1232)0.0021U UG/M3 PCB-1248 (AROCLOR 1248)0.0021U UG/M3 PCB-1260 (AROCLOR 1260)0.0021U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 38: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8400 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVB28 / BMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 09:52Ending:

RESULTS0.002 1U

0.0001 7N0.0001 7U0.0001 8N0.0001 7U0.0001 7N0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.00032N0.00060U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7110.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U0.0001 7U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 39: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS ERA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8401 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCB SCAN Requestor:rwo OO«N Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/28/200010:18Program: SFE Ending:

Id/Station: PDHVC28 / CMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0088 UG/M3 PCB-1242 (AROCLOR 1242)0.0021U UG/M3 PCB-1254 (AROCLOR 1254)0.0085U UG/M3 PCB-1221 (AROCLOR 1221)0.0085U UG/M3 PCB-1232 (AROCLOR 1232)0.0085U UG/M3 PCB-1248 (AROCLOR 1248)0.0021U UG/M3 PCB-1260 (AROCLOR 1260)0.0085U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 40: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8401 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVC28/CMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 10:18Ending:

RESULTS UNITS ANALYTE0.0021U UG/M3 PCB-1268 (AROCLOR 1268)

0.00072 UG/M3 PCB Congener #280.001 OU UG/M3 PCB Congener #52

0.00017U UG/M3 PCB Congener #600.00017U UG/M3 PCB Congener #660.0037N UG/M3 PCB Congener #74

0.00017U UG/M3 PCB Congener #770.00017U UG/M3 PCB Congener #810.00017U UG/M3 PCB Congener #990.00017U UG/M3 PCB Congener #1010.00017U UG/M3 PCB Congener #1050.00017U UG/M3 PCB Congener #1180.00017U UG/M3 PCB Congener #1260.000171) UG/M3 PCB Congener #1380.00017U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00017U UG/M3 PCB Congener #1630.00017U UG/M3 PCB Congener #1690.00017U UG/M3 PCB Congener #1700.00017U UG/M3 PCB Congener #1800.00017U UG/M3 PCB Congener #1830.00017U UG/M3 PCB Congener #1870.00017U UG/M3 PCB Congener #1940.00017U UG/M3 PCB Congener #1950.00017U UG/M3 PCB Congener #1960.00017U UG/M3 PCB Congener #2010.00017U UG/M3 PCB Congener #2030.00017U UG/M3 PCB Congener #2060.00017U UG/M3 PCB Congener #2080.00017U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 41: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8402 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCBSCAN Requestor:PCB SCAN project Leader. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/28/200010:43Program: SFE Ending:

Id/Station: PDHVD28 / DMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.025 UG/M3 PCB-1242 (AROCLOR 1242)

0.0024U UG/M3 PCB-1254 (AROCLOR 1254)0.020U UG/M3 PCB-1221 (AROCLOR 1221)0.020U UG/M3 PCB-1232 (AROCLOR 1232)0.020U UG/M3 PCB-1248 (AROCLOR 1248)

0.0024U UG/M3 PCB-1260 (AROCLOR 1260)0.020U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 42: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8402 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVD28 / DMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 10:43Ending:

RESULTS UNITS ANALYTE0.0024U UG/M3 PCB-1268 (AROCLOR 1268)0.0025 UG/M3 PCB Congener #280.0025U UG/M3 PCB Congener #52

0.00019U UG/M3 PCB Congener #600.00028U UG/M3 PCB Congener #660.00039N UG/M3 PCB Congener #740.00019U UG/M3 PCB Congener #770.00019U UG/M3 PCB Congener #810.00019U UG/M3 PCB Congener #990.00019U UG/M3 PCB Congener #1010.00019U UG/M3 PCB Congener #1050.00019U UG/M3 PCB Congener #1180.00019U UG/M3 PCB Congener #1260.00019U UG/M3 PCB Congener #1380.00019U UG/M3 PCB Congener #1530.00019U UG/M3 PCB Congener #1560.00019U UG/M3 PCB Congener #1630.00019U UG/M3 PCB Congener #1690.00019U UG/M3 PCB Congener #1700.00019U UG/M3 PCB Congener #1800.0001911 UG/M3 PCB Congener #1830.00019U UG/M3 PCB Congener #1870.00019U UG/M3 PCB Congener #1940.00019U UG/M3 PCB Congener #1950.00019U UG/M3 PCB Congener #1960.00019U UG/M3 PCB Congener #2010.000191) UG/M3 PCB Congener #2030.00019U UG/M3 PCB Congener #2060.00019U UG/M3 PCB Congener #2080.00019U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 43: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESO, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8403 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCB SCAN Project Leader: TSLAGLEFacility: Anniston PCB Site Anniston, AL Beginning: 06/28/200011:09Program: SFE Ending:

Id/Station: PDHVE28 / EMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.025 UG/M3 PCB-1242 (AROCLOR 1242)

0.0021U UG/M3 PCB-1254 (AROCLOR 1254)0.020U UG/M3 PCB-1221 (AROCLOR 1221)0.020U UG/M3 PCB-1232 (AROCLOR 1232)0.020U UG/M3 PCB-1248 (AROCLOR 1248)

0.0021U UG/M3 PCB-1260 (AROCLOR 1260)0.020U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 44: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8403 FY 2000SPECIFIED TESTS

Facility: Anniston PCB SiteProgram: SFEId/Station: PDHVE28 / EMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 11:09Ending:

RESULTS UNITS ANALYTE0.0021 U UG/M3 PCB-1268 (AROCLOR 1268)0.0022 UG/M3 PCB Congener #280.0024U UG/M3 PCB Congener #52

0.00042N UG/M3 PCB Congener #600.00026U UG/M3 PCB Congener #660.00035N UG/M3 PCB Congener #740.00017U UG/M3 PCB Congener #770.00017U UG/M3 PCB Congener #810.00017U UG/M3 PCB Congener #990.00017U UG/M3 PCB Congener #1010.00019U UG/M3 PCB Congener #1050.00017U UG/M3 PCB Congener #1180.00017U UG/M3 PCB Congener #1260.00017U UG/M3 PCB Congener #1380.00017U UG/M3 PCB Congener #1530.00017U UG/M3 PCB Congener #1560.00017U UG/M3 PCB Congener #1630.00017U UG/M3 PCB Congener #1690.00017U UG/M3 PCB Congener #1700.00017U UG/M3 PCB Congener #1800.00017U UG/M3 PCB Congener #1830.00017U UG/M3 PCB Congener #1870.00017U UG/M3 PCB Congener #1940.00017U UG/M3 PCB Congener #1950.00017U UG/M3 PCB Congener #1960.00017U UG/M3 PCB Congener #2010.00017U UG/M3 PCB Congener #2030.00017U UG/M3 PCB Congener #2060.00017U UG/M3 PCB Congener #2080.00017U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: l.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 45: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8404 FY 2000 Project: 00-0649 Produced by: Revells, LavonPCBSCAN Requestor:^b &OAN r. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/28/2000 1 1 :38Program: SFE Ending:Id/Station: PDHVF28 / FMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.011U UG/M3 PCB-1 242 (AROCLOR 1242)

0.0023U UG/M3 PCB-1 254 (AROCLOR 1254)0.010U UG/M3 PCB-1221 (AROCLOR 1221)0.01 OU UG/M3 PCB-1 232 (AROCLOR 1232)0.010U UG/M3 PCB-1 248 (AROCLOR 1248)

0.0023U UG/M3 PCB-1 260 (AROCLOR 1260)0.010U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 46: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8404 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVF28 / FMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 11:38Ending:

RESULTS UNITS ANALYTE0.0023U UG/M3 PCB-1268 (AROCLOR 1268)

0.00084 UG/M3 PCB Congener #280.0013U UG/M3 PCB Congener #52

0.00032N UG/M3 PCB Congener #600.00026U UG/M3 PCB Congener #660.00072U UG/M3 PCB Congener #740.00018U UG/M3 PCB Congener #770.00018U UG/M3 PCB Congener #810.00018U UG/M3 PCB Congener #990.00018U UG/M3 PCB Congener #1010.00018U UG/M3 PCB Congener #1050.00018U UG/M3 PCB Congener #1180.00018U UG/M3 PCB Congener #1260.00018U UG/M3 PCB Congener #1380.00018U UG/M3 PCB Congener #1530.00018U UG/M3 PCB Congener #1560.00018U UG/M3 PCB Congener #1630.00018U UG/M3 PCB Congener #1690.00018U UG/M3 PCB Congener #1700.00018U UG/M3 PCB Congener #1800.00018U UG/M3 PCB Congener #1830.00018U UG/M3 PCB Congener #1870.00018U UG/M3 PCB Congener #1940.00018U UG/M3 PCB Congener #1950.00018U UG/M3 PCB Congener #1960.00018U UG/M3 PCB Congener #2010.00018U UG/M3 PCB Congener #2030.00018U UG/M3 PCB Congener #2060.00018U UG/M3 PCB Congener #2080.00018U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 47: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8405 FY 2000 Project: 00-0649 Produced by: Revells, Lavon

PCBSCAN peqUetS!°r;H TQ,Ar ,PProject Leader: TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/28/200012:14Program: SFE Ending:Id/Station: PDHVG28 / GMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0057J UG/M3 PCB-1242 (AROCLOR 1242)0.0024U UG/M3 PCB-1254 (AROCLOR 1254)0.0055U UG/M3 PCB-1221 (AROCLOR 1221)0.0055U UG/M3 PCB-1232 (AROCLOR 1232)0.0055U UG/M3 PCB-1248 (AROCLOR 1248)0.0024U UG/M3 PCB-1260 (AROCLOR 1260)0.0055U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 48: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:28

Sample 8405 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVG28 / GMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 12:14Ending:

RESULTS UNITS ANALYTE0.0024U UG/M3 PCB-1268 (AROCLOR 1268)

0.00040 UG/M3 PCB Congener #280.00081 U UG/M3 PCB Congener #520.00020N UG/M3 PCB Congener #600.00010JN UG/M3 PCB Congener #660.0011U UG/M3 PCB Congener #74

0.00019U UG/M3 PCB Congener #770.00019U UG/M3 PCB Congener #810.00019U UG/M3 PCB Congener #990.00019U UG/M3 PCB Congener #1010.00019U UG/M3 PCB Congener #1050.000191) UG/M3 PCB Congener #1180.00019U UG/M3 PCB Congener #1260.00019U UG/M3 PCB Congener #1380.00019U UG/M3 PCB Congener #1530.00019U UG/M3 PCB Congener #1560.00019U UG/M3 PCB Congener #1630.00019U UG/M3 PCB Congener #1690.00019U UG/M3 PCB Congener #1700.00019U UG/M3 PCB Congener #1800.00019U UG/M3 PCB Congener #1830.00019U UG/M3 PCB Congener #1870.00019U UG/M3 PCB Congener #1940.00019U UG/M3 PCB Congener #1950.000191) UG/M3 PCB Congener #1960.00019U UG/M3 PCB Congener #2010.00019U UG/M3 PCB Congener #2030.00019U UG/M3 PCB Congener #2060.00019U UG/M3 PCB Congener #2080.00019U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 49: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8406 FY 2000 Project: 00-0649 Produced by: Revells, LavonPPR <5CAN Requestor:PCB SCAN project Leader. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/28/200012:14Program: SFE Ending:

Id/Station: PDHVGD28 / GDMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0086 UG/M3 PCB-1242 (AROCLOR 1242)0.0025U UG/M3 PCB-1254 (AROCLOR 1254)0.0085U UG/M3 PCB-1221 (AROCLOR 1221)0.0085U UG/M3 PCB-1232 (AROCLOR 1232)0.0085U UG/M3 PCB-1248 (AROCLOR 1248)0.0025U UG/M3 PCB-1260 (AROCLOR 1260)0.0085U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 50: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8406 FY 2000 Project: 00-0649SPECIFIED TESTSFacility: Anniston PCB Site Anniston, ALProgram: SFEId/Station: PDHVGD28 / GDMedia: AMBIENT AIR

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 12:14Ending:

RESULTS UNITS ANALYTE0.0025U UG/M3 PCB-1268 (AROCLOR 1268)

0.00057 UG/M3 PCB Congener #280.0011U UG/M3 PCB Congener #52

0.00037N UG/M3 PCB Congener #600.00024U UG/M3 PCB Congener #660.0012U UG/M3 PCB Congener #74

0.00020U UG/M3 PCB Congener #770.00020U UG/M3 PCB Congener #810.00020U UG/M3 PCB Congener #990.00020U UG/M3 PCB Congener #1010.00020U UG/M3 PCB Congener #1050.00020U UG/M3 PCB Congener #1180.00020U UG/M3 PCB Congener #1260.00020U UG/M3 PCB Congener #1380.00020U UG/M3 PCB Congener #1530.00020U UG/M3 PCB Congener #1560.00021U UG/M3 PCB Congener #1630.00020U UG/M3 PCB Congener #1690.00020U UG/M3 PCB Congener #1700.00020U UG/M3 PCB Congener #1800.00020U UG/M3 PCB Congener #1830.00020U UG/M3 PCB Congener #1870.00020U UG/M3 PCB Congener #1940.00020U UG/M3 PCB Congener #1950.00020U UG/M3 PCB Congener #1960.00022U UG/M3 PCB Congener #2010.00020U UG/M3 PCB Congener #2030.00020U UG/M3 PCB Congener #2060.00020U UG/M3 PCB Congener #2080.00020U UG/M3 PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: 1 .when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 51: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8407 FY 2000 Project: 00-0649 Produced by: Revells, Lavonorn cr AM Requestor:PCB SCAN project Legder. TSLAGLE

Facility: Anniston PCB Site Anniston, AL Beginning: 06/28/200013:04Program: SFE Ending:Id/Station :pDHVH28/HMedia: AMBIENT AIR

RESULTS UNITS ANALYTE0.0038U UG/M3 PCB-1242 (AROCLOR 1242)0.0023U UG/M3 PCB-1254 (AROCLOR 1254)0.0038U UG/M3 PCB-1221 (AROCLOR 1221)0.0038U UG/M3 PCB-1232 (AROCLOR 1232)0.0038U UG/M3 PCB-1248 (AROCLOR 1248)0.0023U UG/M3 PCB-1260 (AROCLOR 1260)0.0038U UG/M3 PCB-1016 (AROCLOR 1016)

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane

Page 52: U.S. ENVIRONMENTAL PROTECTION AGENCY 4SESD-EIB 1 … · 2018-11-18 · U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, ... Standard Operation Procedures and Quality Assurance Manual

PESTICIDES/PCB SAMPLE ANALYSIS EPA - REGION IV SESD, ATHENS, GA Production Date: 07/19/2000 15:05

Sample 8407 FY 2000SPECIFIED TESTSFacility: Anniston PCB SiteProgram: SFEId/Station: PDHVH28 / HMedia: AMBIENT AIR

Project: 00-0649

Anniston, AL

Produced by: Revells, LavonRequestor:Project Leader: TSLAGLEBeginning: 06/28/2000 13:04Ending:

RESULTS0.0023U

0.00032JN0.00044U0.0001 8U0.0001 8U0.001 OU

0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 9U0.0001 8U0.0001 8U0.00018U0.00018U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.0001 8U0.00018U0.0001 8U

UNITSUG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3UG/M3

ANALYTEPCB-1268 (AROCLOR 1268)PCB Congener #28PCB Congener #52PCB Congener #60PCB Congener #66PCB Congener #74PCB Congener #77PCB Congener #81PCB Congener #99PCB Congener #101PCB Congener #105PCB Congener #11 8PCB Congener #126PCB Congener #138PCB Congener #153PCB Congener #156PCB Congener #163PCB Congener #169PCB Congener #170PCB Congener #180PCB Congener #183PCB Congener #187PCB Congener #194PCB Congener #195PCB Congener #196PCB Congener #201PCB Congener #203PCB Congener #206PCB Congener #208PCB Congener #209

A-average value. NA-not analyzed. NAI-interferences. J-estimated value. N-presumptive evidence of presence of material.K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit.R-qc indicates that data unusable, compound may or may not be present, resampling and reanalysis is necessary for verification.C-confirmed by gems: Lwhen no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane