stl-st. louis severn stl' · stl-st. louis analytical report revised norm lot #: f6l150102...

STL-ST. LOUIS

ANALYTICAL REPORT

REVISED

NORM

Lot #: F6L150102

Frank Virginia

AET Environmental Inc14 Lakeside Lane

Denver, CO 80212

S E V E R N

T R E N T

SFUND RECORDS CTR

2118406

STL'STL St. Louis13715 Rider Trail NorthEarth City, MO 63045

Tel: 314 298 8566 Fax.- 3142988757www.stl-inc.com

SEVERN TRENT LABORATORIES, INC.

Brian O'DonnellProject Manager

Leaders in Environmental Testing

January 29, 2007

Severn Trent Laboratories, Inc.

LOT# F6L150102 1 of 36

STL ST. LOUIS

Revised 1/29/07Case Narrative

LOT NUMBER: F6L150102

This report contains the analytical results for the three samples received under chain of custody bySTL St. Louis on December 15, 2006. These samples are associated with your NORM project.

The analytical results included in this report meet all applicable quality control procedure requirementsexcept as noted on the following page.

The test results in this report meet all NELAP requirements for parameters in which accreditations areheld by STL St. Louis. Any exceptions to NELAP requirements are noted in the case narrative. Thecase narrative is an integral part of this report.

All chemical analysis results are based upon sample as received, wet weight, unless noted otherwise.All radiochemistry results are based upon sample as dried and ground with the exception of tritium,unless requested wet weight by the client.

Observations/NonconformancesReference the chain of custody and condition upon receipt report for any variations on receipt conditionsand temperature of samples on receipt.

Revision: Samples F6L150102 (1) and F6L150102 (2)forTCLP Mercury analysis were re-extracted andreported.

Gross Alpha by 9310 MOD

The Gross Alpha reporting limit was not met due to a shortened count time attributed to the high activityof the samples. The analytical results are reported.Affected Samples:F6L150102(1): DRUM 1

Metals bv 601 OB

Batch 6362091-The MS (MSD) recovery for Arsenic, Cadmium, and Lead is outside the established QClimits. The said analyte concentration in the original sample is greater than four times the amountspiked, making percent recovery information ineffective. Method performance is demonstrated byacceptable LCS recovery. No further action is required.

The MS (MSD) recovery for Silver, Barium, and Chromium is outside the established QC limits.' TheRPD is within method acceptance criteria indicating possible matrix interference. Method performance isdemonstrated by acceptable LCS recovery. No further action is required.

The samples were analyzed at a dilution due to high concentrations of target and.non-target analytes,caused in part by Zinc and Iron. The reporting limit has been adjusted only for those targets reportedfrom the dilution run.Affected Samples:F6L150102 (1): DRUM 1 F6L150102 (3): DRUM 3F6L150102(2): DRUM 2

LOT# F6L150102 . . . 2 of 36

STL ST. LOUIS

Gamma Spectroscopy by GA-01-R MOD

The reporting limit for Radium-226 analyzed by gamma Spectroscopy was not met due to the presenceof the nuclide in the sample. The data is reported with the MDA achieved.Affected Samples:F6L150102(1): DRUM 1 F6L150102 (2): DRUM 2

Mercury by 7471A

QC Batch# 6354161 (solids). The MS (MSD) recovery for Mercury is outside the established QC limits.The said analyte concentration in the original sample is greater than four times the amount spiked,making percent recovery information ineffective. Method performance is demonstrated by acceptableLCS recovery. No further action is required.Affected Samples:F6L150102 (1): DRUM 1 F6L150102 (3): DRUM 3F6L150102(2):.DRUM2

Mercury by 7470A

QC Batch# 7023102 (TCLP). Mercury was observed in the method blank above the reporting limit.Associated samples which are either non-detect for the contaminant or exhibit concentrations greaterthan ten (10) times the concentrations observed in the method blank, do not require re-analysis. Originalresults are reported. ,Affected Samples:F6L150102(3): DRUMS ,

QC Batch# 7023102 (TCLP) Mercury. There was an unusually high level of contamination isolated to theTCLP method blank. This also affected the method LCS since it is matrix-matched from the methodblank. Samples : F6L150102-001 and F6L150102-002 were re-extracted, sample F6L150102-003 wasnon-detect for Mercury and is reported as such.Affected Samples:F6L150102(1):DRUM1 F6L150102 (3): DRUM 3F6L150102(2):DRUM2

LOTtt F6L150102 • . 3 of 36

STL ST. LOUIS

METHODS SUMMARY

F6L150102

PARAMETERANALYTICALMETHOD

Gamma Spectroscopy - Radium-226•& HitsGross Alpha/Beta by GFPCInductively Coupled Plasma (ICP) MetalsInductively Coupled Plasma (ICP) MetalsMercury in Liquid Waste (Manual Cold-Vapor)Mercury in Solid Waste (Manual Cold-Vapor)Percent Moisture

References:

EML GA-01-R MODSW846 9310 MODSW846 6010BSW846 6010BSW846 7470ASW846 7471AMCAWW 160.3 MOD

PREPARATIONMETHOD

SW846 9310 MOD

SW846SW846SW846MCAWW

1311/30101311/74707471A160.3 MOD

EML "ENVIRONMENTAL MEASUREMENTS LABORATORY PROCEDURES MANUAL"HASL-300 28TH EDITION, VOLUME I and II DEPARTMENT OF ENERGY

MCAWW "Methods for Chemical Analysis of Water and Wastes",EPA-600/4-79-020, March 1983 and subsequent revisions.

SW846 "Test Methods for Evaluating Solid Waste-, Physical/ChemicalMethods", Third Edition, November 1986 and its updates.

LOT# F6L150102 4 of 36

STL ST. LOUIS•*>

SAMPLE SUMMARY

F6L150102

SAMPLED SAMPWO # SAMPLE* CLIENT SAMPLE ID DATE TIME

JLJA6 001 DRUM 1 12/11/06 09:00JLJCG 002 DRUM 2 " 12/11/06 09:0(JLJCK 003 DRUM 3 ' 12/11/06 09:0(

NOTE(S) : r- The analytical results of the samples listed above are presented on tie following pages.

- All calculations are performed before rounding to avoid round-off errors in calculated results.

- Results noted as "ND" were not detected at or above the stated limit

- This report must not be reproduced, except in full, without the written approval of the laboratory.

- Results for the following parameters ore never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitability, layers, odor,

paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight.

LOT# F6L150102 . . 5 of 36

STL ST. LOUIS

Lot-Sample #Date Sampled% Moisture

AET Environmental Inc

Client Sample ID: DRUM 1

TOTAL Metals

F6L150102-00112/11/05 09:00 Date Received..: 12/13/060.88

Matrix. SOLID

PARAMETER RESULT

Prep Batch *. . . : 6354161Mercury 782

Prep Batch #. . . : 6362091Silver 5.4

Arsenic 542

Barium 255

Cadmium 13 . 1

Chromium 36.9

Lead 962

Selenium ND

NOTE(S) :

REPORTINGLIMIT UNITS

33.6Dilution

2.0Dilution

40.4Dilution

10.1Dilution

2.5Dilution

2.0Dilution

50.4Dilution

101Dilution

ug/kgFactor: 1

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 5

mg/kgFactor: 2

mg/kgFactor: 5

mg/kgFactor : 5

' METHOD

SW846Analysis

SW846Analysis

SW846Analysis

SH846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

7471ATime. . : 17:48

6010BTime. . : 16:53

6010BTime..: 16:53

6010BTime.. : 16:53

6010BTime..: 10:31

6010BTime.. : 16:53

6010BTime..: 10:31

6010BTime..: 10:31

PREPARATION-ANALYSIS DATE

12/20/06

12/28-01/04/07

12/28-01/04/07

12/28-01/04/07

12/28-01/05/07

12/28-01/04/07

12/28-01/05/07

12/28-01/05/07

WORKORDER #

JLJA61AM

JLJA61AB

JLJA61AF

JLJA61AG

JLJA61AH

JLJA61AJ

JLJA61AK

JLJA61AL

Results and reporting limits have been adjusted for dry weight.

LOT# F6L150102 6 of 36

ST.L: ST. LOUIS

Lot-Sample #.Date Sampled.



TCLP Metals

F6L150102-00112/11/06 09:00 Date Received..: 12/13/06

Matrix : SOLID

PARAMETER RESULT

Prep Batch #...: 7023198Arsenic ND

Barium 243

Chromium ND

Lead 222 B

Cadmium 97 . 8

Selenium ND

Silver ND


500Dilution

125Dilution

62 .5Dilution

250Dilutiony

12.5Dilution

500

Dilution

25.0Dilution

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor : 1

METHOD

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846

Analysis

SW846

Analysis

6010B

Time..: 09:32

6010BTime. . : 09 :32

6010B

Time. . : 09 : 32

6010BTime. . : 09:32

6010BTime.. : 09:32

6010B

Time. . : 09:32

6010B

Time. . : 09:32


01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

WORK

ORDER #/

JLJA61A8

JLJA61A9

JLJA61CA

JLJA61CC

JLJA61CD

JLJA61CE

JLJA61CF

Prep Batch #...: 7026137Mercury ND

NOTE(S):

1.0 ug/LDilution Factor: 1

SW846 7470A 01/26/07Analysis Time. . : 15:08

JLJA62CG

Analysis performed in accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311

B Estimated result. Result is less than RL.

LOT# F6L1501.02 7 . o f 36

^ STL ST. LOUIS^S



General Chemistry

Lot-Sample*...: FSL150102-001 Work Order #...: JLJA6 Matrix : SOLIDDate Sampled...: 12/11/OS 09:00 Date Received..: 12/13/06% Moisture : 0 . 8 8

PREPARATION- PREPPARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH #Percent Moisture 0.88 0.10 % MCAWW 160.3 MOD 12/21-12/22/06 6355044

Dilution Factor: 1 Analysis Time..: 0 0 : 0 0

LOT# F6L15bl02 . " • 8 of 36

STL ST. LOUIS

Lot-Sample #.Date Sampled.



TOTAL Metals

F6L150102-002

12/11/06 09:00 Date Received..: 12/13/06

Matrix . : SOLID

PARAMETER RESULT

Prep Batch. #...: 6354161Mercury 785

Prep Batch #...: 6362091Silver 2.4

Arsenic '273

Barium 377

Cadmium 15 . 2

Chromium 99 . 3

Lead 1000

Selenium ND

NOTE(S):

RE FOR1

LIMIT

33.5Dilution

2.0Dilution

40.3Dilution

10.1Dilution

5.0Dilution

2.0Dilution

101Dilution

201Dilution

TINGUNITS

ug/kgFactor: 1

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 10

mg/kgFactor: 2

mg/kgFactor: 10

mg/kgFactor: 10

METHOI

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SH846Analysis

SW846Analysis

3

7471ATime..: 17:58

6010BTime..: 17:25

6010BTime. . : 17:25

6010BTime.. : 17:25

6010BTime. . : 10:49

eoioBTime.. : 17:25

6010BTime. . : 10:49

6010BTime . . : 10:49


12/20/06

12/28-01/04/07

12/28-01/04/07

12/28-01/04/07

12/28-01/05/07

12/28-01/04/07

12/28-01/05/07

12/28-01/05/07

WORKORDER #

JLJCG1AM

OLJCGIAE

JLJCG1AF

-

JLJCG1AG

JLJCG1AH

JLJCG1AJ

JLJCG1AK

JLJCG1AL


LOT# F6L150102 9 of 36

STL ST.- LOUIS



TCLP Metals

Lot- Sample #. .Date Sampled. .Leach. Date

PARAMETER

Prep Batch # . .Arsenic

Barium

Chromium

Lead

Cadmium

Selenium

Silver

Prep Batch #. .Mercury

NOTB(S):

.: F6L15010;

.: 12/11/06• 01/22/07

RESULT

.: 7023198119 B

550

ND

515

259

ND

ND

,.: 7026137ND

2-00209:00 Date Received. . :

Leach Batch # . . :


500Dilution

125Dilution

62.5Dilution

250Dilution

12.5Dilution

500Dilution

25.0Dilution

1.0Dilution

ug/LFactor : 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: 1

ug/L1

Factor: 1

12/13/06P702217

METHOD

SW846 6010BAnalysis Time..: 09:50

SW846 6010BAnalysis Time. . : 09:50

SW846 6010BAnalysis Time.. : 09:50

SW846 6010BAnalysis 'Time. . : 09:50

SW846 6010BAnalysis Time. . : 0 9 : 5 0

SW846 6010BAnalysis Time.. : 09 :50

SW846 6010BAnalysis Time. . : N09 : 50

SW846 7470AAnalysis Time . . • 15:16

Matrix :


01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

•

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/26/07

SOLID

WORKORDER #

OLJCG1AN

JLJCG1AP

JLJCG1AQ

OLJCG1AR

JLJCG1AT

JLJCG1AU

JLJCG1AV

JLJCG2AW


B Estimated result. Result is less than RL.

LOT# F6L150102 10 of 36

STL ST. LOUIS


Client Sample ID: DRUM 2.

General Chemistry

Lot-Sample fl...: F6L150102-002 Work Order #...: JLJCG Matrix : SOLIDDate Sampled : 12/11/06 09:00 Date Received..: 12/13/06% Moisture : 0.67

PREPARATION- PREPPARAMETER RESULT RL. UNITS METHOD ANALYSIS DATE BATCH #Percent Moisture 0.67 0.10 % MCftWW 160.3 MOD 12/21-12/22/06 6355044

Dilution Factor: 1 Analysis Time. . : 0 0 : 0 0

LOT# F6L150102 11 of 36

STL ST. LOUIS

Lot-Sample #

Date Sampled% Moisture



TOTAL Metals

F6L150102-003

12/11/06 09:00 Date Received..: 12/13/06

0.46

Matrix : SOLID

PARAMETER RESULT

Prep Batch # : 6354161Mercury 1180

Prep Batch #. . . : 6362091Silver 3.4

Arsenic 288

Barium 362

Cadmium 11 . 3

rh-rrmi nm . 57.4

Lead 1140

Selenium ND

NOTE(S) :


33.5Dilution

2.0,Dilution

40.2Dilution

10.0Dilution

5.0Dilution

2.0Dilution

100Dilution

201Dilution

ug/kgFactor: 1

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 2

mg/kgFactor: 10

mg/kgFactor: 2

mg/kgFactor: 10

mg/kgFactor: 10

METHOD

SW846Analysis

SW846. Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

7471ATime. . : 18:00

6010BTime. . : 17 :29

6010BTime..: 17:29

6010BTime.. : 17:29

6010BTime. . : 10 : 53

6010BTime..: 17:29

eoioBTime. . : 10:53

6010B

Time. . : 10:53


12/20/06

12/28-01/04/07

12/28-01/04/07

12/28-01/04/07

12/28-01/05/07

12/28-01/04/07

12/28-01/05/07

12/28-01/05/07

WORKORDER #

JLJCK1AM

JLJCK1AE

JLJCK1AF

JLJCK1AG

JLJCK1AH

JLJCK1AJ

JLJCKIAK

JLJCK1AL


LOT# F6L150102 12 of 36

STL ST. LOUIS

Lot-Sample #Date SampledLeach Date



TCLP Metals

F6L150102-00312/11/06 09:00 Date Received..: 12/13/06

Matrix : SOLID

PARAMETER RESULT

Prep Batch #. . . : 7023102Mercury ND

Prep Batch #...: 7023198Arsenic ND

Barium 575

Chromium . ND

Lead 552

Cadmium 92 . 6

Selenium ND

Silver ND

NOTE(S) :

REPOR'LIMIT

1.0Dilution

500Dilution

125Dilution

62 .5Dilution

250Dilution

12.5Dilution

500Dilution

25.0Dilution

TINGUNITS

ug/LFactor: 1

ug/LFactor : 1

ug/LFactor: 1

ug/LFactor: 1

ug/LFactor: l

ug/LFactor: 1

' ug/LFactor : 1

ug/LFactor: 1

METHOI

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

3

7470ATime. . : 19:16

6010BTime. . : 09 : 54

eoioBTime..: 09:54

6010BTime. . : 09:54

6010BTime. . : 09 : 54

6010BTime. . : 09:54

6010B

Time..: 09:54

6010B

Time. . : 09 : 54


01/23/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

01/23-01/24/07

WORKORDER #

JLJCK1AW

JLJCK1AN

JLJCK1AP

JLJCK1AQ

JIuJCKlAR

JLJCK1AT

JLJCK1AU

JLJCK1AV


LOT# F6L150102 13 of 36

STL ST. LOUIS

AST Environmental Inc


General Chemistry

Lot-Sample # : F6L150102-003 Work Order #...: JLJCK Matrix : SOLIDDate Sampled : 12/11/06 09:00 Date Received..: 12/13/06% Moisture : 0.46

PREPARATION- PREPPARAMETER ' RESULT RL UNITS METHOD ANALYSIS DATE BATCH #Percent Moisture 0.46 0.10 % MCRWW 160.3 MOD 12/21-12/22/06 6355044

Dilution Factor: 1 Analysis Time.. : 0 0 : 0 0

LOT# F6L150102 14 of 36

STL ST. LOUIS

METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: F6L150102

PARAMETER RESULTREPORTINGLIMIT UNITS METHOD

Matrix. SOLID

PREPARATION- WORKANALYSIS DATE ORDER #

MB Lot-Sample #: F6L200000-161 Prep Batch # . . .Mercury ND 33.3 ug/kg

Dilution Factor: lAnalysis Time..: 17:44

: 6354161SW846 7471A 12/20/06 JLT891AA

MB Lot-Sample #: F6L280000-091 Prep Batch #..Arsenic ND 20 .0 mg/kg

Dilution Factor: 1Analysis Time.. : 16:45

Barium

Cadmium

Chromium

Lead

Selenium

Silver

NOTB(S):

ND

ND

ND

ND

ND

ND

5.0 mg/kgDilution Factor: lAnalysis Time..: 16:45

0.50 mg/kgDilution Factor: 1Analysis T ime . . : 16:45

1.0 mg/kgDilution Factor: 1Analysis. Time..: 16:45

10.0 mg/kgDilution Factor: 1

Analysis Time..: 16:45

2 0 . 0 mg/kgDilution Factor: 1


1.0 mg/kgDilution Factor: 1Analysis Time..: 16:45

6362091SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

12/28-01/04/07 JL7DE1AC

12/28-01/04/07 JL7DE1AD

12/28-01/04/07 JL7DE1AE

12/28-01/04/07 JL7DE1AF

12/28-01/04/07 JL7DE1AG

12/28-01/04/07 JL7DE1AH

12/28-01/04/07 JL7DE1AA

Calculations are performed before rounding to avoid round-off errors in calculated results.

LOT# F6L150102 15 of 36

..STL ST. LOUIS

METHOD BLANK REPORT

TCLP Metals

Client Lot #...-. F6L150102 Matrix : SOLID

PARAMETER RESULT

REPORTING

LIMIT UNITS METHOD

PREPARATION- WORK

ANALYSIS DATE ORDER #

MB Lot-Sample #:Leach Date :Arsenic

Barium

Chromium

Lead

Cadmium

Selenium

Silver

F7A220000-292 Prep Batch #-.01/22/07 Leach Batch #.

ND ' 500 ug/LDilution Factor: 1Analysis Time..: 09:24

ND

ND

ND

ND

ND

ND

125 ug/LDilution Factor: 1

iAnalysis Time..: 09:24



250 ug/L

Dilution Factor: 1Analysis T ime . . : 09 :24



500 ug/LDilution Factor: 1Analysis Time..: 09:24

2 5 . 0 ug/LDilution Factor: 1

Analysis Time.. : 09:24

: 7023198: P702217

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

01/23-01/24/07 JM6VA1AA

01/23-01/24/07 JM6VA1AC

01/23-01/24/07 JM6VA1AD

01/23-01/24/07 JM6VA1AE

01/23-01/24/07 JM6VA1AF

01/23-01/24/07 JM6VA1AG

01/23-01/24/07 JM6VA1AH

MB Lot-Sample #: F7A220000-292 Prep Batch # . . . :Leach Date .: 01/22/07 Leach Batch # . . :Mercury 93.0 5.0 ug/L

Dilution Factor: 5Analysis Time..: 18:57

7023102

P702217

SW846 7470A 01/23/07 JM6VA1AJ

MB Lot-Sample #: F7A250000-374 Prep Batch #...: 7026137

Leach Date : 01/25/07 Leach Batch #..: P702516

Mercury ND 1.0 ug/L SW846 7470A

Dilution Factor: 1


(Continued on next page)

01/26/07 JNEF71AA

LOT# F6L150102 16 of 36

STL "ST. LOUIS

METHOD BLANK REPORT

TCLP Metals

Client Lot #...: F6L150102

NOTB(S):

Matrix. SOLID

Calculations are performed before rounding to avoid round-off errors in calculated results.

LOT# F6L150102 17 of 36

STL ST. LOUIS

LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot # : F6L150102 Matrix :' SOLID

PERCENT RECOVERY PREPARATION-PARAMETBR RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER #

LCS Lot-Sample**: F6L200000-161 Prep Batch #...: 6354161Mercury . 76 (65 - 135) SW846 7471A 12/20/06 JLT891AC

Dilution Factor: 1 Analysis Time..: 17:46

LCS Lot-Sample*: F6L280000-091 Prep Batch #...: 6362091Silver 116 (53 - 147) SW846 6010B 12/28-01/04/07 JL7DE1AJ


Arsenic 106 (80 - 120) SW846 6010B 12/28-01/04/07 JL7DE1AKDilution Factor: 1 Analysis Time..: 16:49

Barium 105 (82 - 118) SW846 6010B 12/28-01/04/07 JL7DE1ALDilution Factor: 1 Analysis Time.. : 16:49

Cadmium 103 (81 - 119) SW846 6010B 12/28-01/04/07 JL7DE1AMDilution Factor: 1 Analysis Time...- 16:49

Chromium 101 (78 - 121) SW846 6010B 12/28-01/04/07 JL7DE1ANDilution Factor: 1 Analysis Time..: 16:49

Lead 104 (80 - 120) SW846 6010B 12/28-01/04/07 JL7DE1AP• . Dilution Factor: 1 .Analysis Time..: 16:49

Selenium 107 (76 - 124) SW846 6010B 12/28-01/04/07 JL7DE1AQDilution Factor: 1 Analysis Time..: 16:49

MOTE(S) :Calculations are performed before rounding to avoid round-off errors in calculated results.

LOT# F6L150102 18 of 36

v-, STL ST. LOUIS

LABORATORY CONTROL SAMPLE EVALUATION REPORT

TCLP Metals

Client Lot #...: F6L150102 Matrix : SOLID

PERCENT RECOVERY PREPARATION-PARAMETER^ RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER #

LCS Lot-Sample*: F7A230000-102 Prep Batch #...: 7023102Mercury 531 N . (80 - 120) SW846 7470A 01/23/07 JM7LM1AA

Dilution Factor: S Analysis T ime . . : 19:01

LCS Lot-Sample*: F7A230000-198 Prep Batch #...: 7023198Arsenic 102 (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1AA

Dilution Factor: 1 Analysis Time.. : 09 :28

Barium 93 . (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1ACDilution Factor: 1 Analysis Time..: 09:28

Chromium 95 • (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1ADDilution Factor: l . Analysis Time..: 09:28

Lead 94 (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1AEDilution Factor: 1 Analysis Time.. : 09:28

Cadmium 99 (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1AFDilution Factor: 1 Analysis Time..: 09:28

Selenium 100 (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1AGDilution Factor: 1 Analysis Time..: 09:28

Silver 96 (80 - 120) SW846 6010B 01/23-01/24/07 JM73D1AHDilution Factor: 1 Analysis Time. . : 09:28 '

LCS Lot-Sample*: F7A260000-137 Prep Batch #...: 7026137Mercury. 104 (80 - 120) SW846 7470A - 01/26/07 JNFCJ1AA


MDTB(S):Calculations are performed before rounding to avoid round-off errors in calculated results.N Spiked analyte recoveiy is outside stated control limits.

LOT# F6L150102 19 of 36

STL ST. LOUIS

MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: F6L150102Date Sampled...: 12/11/06 09:00 Date Received..: 12/13/06

PERCENT RECOVERY RPDPARAMETER RECOVERY LIMITS RPD LIMITS METHOD

Matrix. SOLID


MS Lot-Sample #-. F6L150102-001 Prep Batch #...: 6354161

% Moisture : 0.88Mercury 162 N (80 -• 120) SW846 7471A 12/20/06 JLJA61AN

92 (80 - 120) 12 (0 -30) SW846 7471A 12/20/06 JLJA61APDilution Factor: 1


MS Lot-Sample #: F6L150102-001 Prep Batch #...: 6362091

Arsenic 27 N (75 - 125) SW846 6010B35 N (75 - 125) 1.4 (0-30) SW846 6010B


Barium 81 (75 - 125) SW846 6010B66 N • (75 - 125) 4.4 (0-30) SW846 6010B


Cadmium 0.0 N (75 - 125) • SW846 6010B421 N . (75 - 125) 0.0 (0-30) SW846 6010B

Dilution Factor: 5


Chromium 52 N (75 - 125) SW846 6010B6.6 N (75 - 125) 11 ( 0 - 3 0 ) SW846 6010B


Lead 0.0 N (75 - 125) SW846 6010B0.0 N (75 - 125) 0.0 (0-30) SW846 6010B

Dilution Factor: 5


Selenium 97 (75 - 125) SW846 6010B95 (75 - 125) 2.2 (0-30) SW846 6010B

Dilution Factor: 5


(Continued on next page)

% Moisture : 0.8812/28-01/04/07 JLJA61AU12/28-01/04/07 JLJA61AV

12/28-01/04/07 JLJA61AW12/28-01/04/07 JLJA61AX

12/28-01/05/07 JLJA61AO12/28-01/05/07 JLJA61A1

12/28-01/04/07 JLJA61A212/28-01/04/07 JLJA61A3

12/28-01/05/07 JLJA61A412/28-01/05/07 JLJA61A5

12/28-01/05/07 JLJA61A612/28-01/05/07 JLJA61A7

LOT# F6L150102 20 of 36

STL ST. LOUIS


TOTAL Metals

Client Lot # : F6L150102 Matrix : SOLIDDate Saiqpled.. . : 12/11/06 09:00 Date Received..: 12/13/06

PERCENT RECOVERY RPD . PREPARATION- WORKPARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER #Silver 29 N (75 - 125) SW846 6010B 12/28-01/04/07 JLJA61AR

96 (75 - 125). 24 (0-30) SW846 6010B .12/28-01/04/07 JLJA61ATDilucion Factor: 2

. Analysis Time..: 17:16

NOTB(S) :Calculations are performed before rounding to avoid round-off errors in calculated results.


N Spiked analyte recovery is outside stated control limits.

LOT# F6L150102 21 of 36

STL ST. LOUIS


TCLP Metals

Client Lot #..-: F6L150102Date Sampled...: 12/11/06 09:00 Date Received..: 12/13/06

Matrix. SOLID

PARAMETERPERCENT RECOVERYRECOVERY LIMITS

RPDRPD LIMITS METHOD

MS Lot-Sample #: F6L150102-001 Prep Batch #...: 7023198Leach Date.Arsenic

Barium

Chromium

Lead

Cadmium

Selenium

Silver

...: 01/22/07 Leach Batch #..: P702217104 (75 - 125) . SW846 6010B109 (75 - 125) 4.5 (0-20) SW846 6010B

Dilution Factor: 1


93 (75 - 125)98 (75 - 125) 4.9 (0-20)

Dilution Factor: 1

Analysis Time. . : 09:41

95 (75 - 125)99 (75 - 125) 4.1 (0-20)

Dilution Factor: 1


89 (75 - 125)94 (75 - 125) 4.5 (0-20)


88 (75 - 125)99 (75 - 125) 4.2 (0-20)

Dilution Factor: 1


88 (75 - 125)92 (75 - 125) 4.4 (0 -20)

Dilution Factor: 1


107 (75 - 125)

114 (75 - 125) 6.3 ( 0 - 2 0 )Dilution Factor: 1


SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B


01/23-01/24/07 JLJA61CK01/23-01/24/07 JLJA61CL

01/23-01/24/07 JLJA61CM01/23-01/24/07 JLJA61CN

01/23-01/24/07 JLJA61CP01/23-01/24/07 JLJA61CQ

01/23-01/24/07 JLJA61CR01/23-01/24/07 JLJA61CT

01/23-01/24/07 JLJA61CU01/23-01/24/07 JLJA61CV

01/23-01/24/07 JLJA61CW01/23-01/24/07 JLJA61CX

01/23-01/24/07 JLJA61CO01/23-01/24/07 JLJA61C1

MS Lot-Sample #:Leach Date :

F6L150102-00101/25/07

Prep Batch #...: 7026137Leach Batch #..: P702516(Continued on next page)

LOT# F6L150102 22 of 36

STL ST. LOUIS


TCLP Metals

Client Lot # : F6L150102 Matrix : SOLIDDate Sampled....- 12/11/06 09:00 Date Received..: 12/13/06

PERCENT RECOVERY RPD PREPARATION- WORKPARAMETER RECOVERY LIMITS _ RPD LIMITS METHOD ANALYSIS DATE ORDER #Mercury 108 (70 - 130) SW846 7470A 01/26/07 JLJA61C2

101 (70 - 130} 6.7 (0-20) SW846 7470A • 01/26/07 JLJA61C3Dilution Factor: 1Analysis Time..: 15:10

KOTE(S) :Calculations are performed before rounding to avoid round-off errors in calculated results.

LOT# F6L150102 . 23 of 36

-. STL ST.. LOUIS

SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Client Lot # . . . : F6L150102 Work Order # . . . : JLQOD-SMP Matrix : SOLIDJLQOD-DUP

Date Sampled...: 12/18/06 16:00 Date Received..: 12/19/06% Moisture -.9.9

DUPLICATE RPD PREPARATION- PREPPARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH flPercent Moisture SD Lot-Sample #: F6L190144-002

9.9 9.1 % 8.2 (0 -30 ) MCAWW 160.3 MOD 12/21-12/22/06 6355044Dilution Factor: 1 Analysis Time. . : 0 0 : 0 0

LOT# F6L150102 • ' . 24 of 36

STL ST. LOUIS


Client Sanrole ID: DRUM 1

Severn Trent Laboratories - Radiochemistry

Lab Sample ID: F6L150102-001Work Order: JLJA6.Matrix:

Parameter

SOLID

Result Qual

GROSS A/B BY GFPC SW846 9310 MOD

Gross Alpha

Gross Beta

Gamma Ra-226 &Actinium 228Bismuth-210MBismuth 212

Bismuth 214Cesium 137

Lead 210Lead 212

Lead 214

148006550

KitB By DOE GA-01-R Mod.1.8 U

-3.20 U -

0.7 U

701

-b.oi u362

-16.1 U

720

Protactinium 234M 920Radium (226)Radium 228 •Radium 224Thallium 208Thorium 232

Thorium 234Uranium 238

Other DetectedActinium 227

Protactinium 231

Thorium 227

Uranium 235

701

1.8 U

1260

-0.80 U

1.8 U

409

409

Radionuclides —39.5

30

39.5

43.8

Date Collected: 12/11/06 0900Date Received: 12/13/06 1145

TotalUncert .(2 <j+/-> RJ,

pCi/g1500 10660 10

PCi/gl.l0.93

4 . 3

41'0 .99

35

1.8

42

160

41 1

1.1

77

0.69

1-1

35

35

.4.9

260

4.9

5.8

MDC

Batch

10

7

Batch4 . 0

1.5

7 . 0

2

1.6

24

2 . 4

3

120

2

4 .0

19

1.1

4.0

19

19

5.2

30

5.2

6.3

Prep AnalysisDate Date

#6355409 Yld %12/22/06 12/22/06

12/22/06 12/22/06

# 6355392 Yld %12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07 '

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07.

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

NOTE(S)

Data are incomplete without the case narrative.

MDC is determined by instrument performance only.Bold results are greater than the MDC

U Result is less than the sample detection limit.

LOT# 'F6L150102. 25 of 36

STL ST. LOUIS


Client Samole ID: DRUM 1 DUP


Lab Sample ID: F6L150102-001X. Work Order: JLJA6Matrix: SOLID

Parameter Result: ' Qual

Gamma Ra-226 &Actinium 228

Bismuth-210M

Bismuth 212

Bismuth 214

Cesium 137

Lead 210

Lead 212

Lead 214

Hits By DOE GA-01-R Mod.

2.7 U

-0.88 U •

-1.2 U

699

-0.08 U

366

-27.3 U

712

Protactinium 234M 920

Radium (226)

Radium 228

Radium 224

Thallium 208

: Thorium 232

Thorium 234

Uranium 238

Other Detected

Actinium 227

Potassium 40

Protactinium 231

Thorium 227

Thorium 231

Uranium 235

699

2.7 U

1260

-1.35 U

2.7 U

394

394

Radionuclides

35.9

19.4

49

35.9

45.6

45.6


TotalUncert . Prep

(2o+/-> , RL MDC Dat°

pci/g1-7

0.94

3.8

41

1.1-

39

2.3

41

120

41 1

1.7

77

0.62

1.7

35

35

6.2

9.6

37

6.2

6.3

6.3

Batch3.8

1.6

6.3

2

1.8

29

2.4

3

100

2

3.8

19

0.97

3.8

22

22

6.3

8.5

22

6.3

6.7

6.7

# 6355392

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

AnalysisDate

Yld %

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/.07

01/11/07

01/11/07

(01/11/07

01/11/07

NOTE(S)

Data, are incomplete without the case narrative.

MDC is determined by instrument performance only.Bold results are greater than the HOC


LOT# F6L150102 26 of 36

STL" ST. LOUIS




Lab Sample

Work Order

Matrix:

Parameter

GROSS A/B BY

Gross Alpha

Gross Beta

Gamma. Ra-226

Actinium 228

Bismuth-210M

Bismuth 212

Bismuth 214

Cesium 137

Lead 210

Lead 212

Lead 214

ID: F6L150102-002

: JLJCG

SOLID

'Result Qual

GFPC SW846 9310 MOD

7220

3200

& Hits By DOE GA-01-R Mod.

1.7 U

-0.84 U

-0.9 U

337

-1.86 U

125

-7.6 . U

331


TotalUncert .

(2 c+/-) RL

pCi/g

730 10

320 10

pci/g

1.3

0.66

2.8

20

0.52

16

1.1

19

Protactinium 234M 362 47

Radium (226)

Radium 228

Radium 224

Thallium 208

Thorium 232 •

Thorium 234

Uranium 238

337

1.7 U

570

-0.42 U

1.7 U

117

117

20 1

1.3

36

0.51

1.3

13

13

MDC

. Batch

86

Batch

2. 71.1

4.7

1

0.82

16

•1.6

2

61

1

2.7

13

0.74

2.7

11

11

PrepDate

# 6355409

12/22/06

12/22/06

# 6355392

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

AnalysisDate

Yld %

12/22/06

12/22/06

Yld %

01/11/07

01/11/07

01/11/07

01/11/0701/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

NOTE(S)

Data ace incomplete without the case narrative.



LOTtt F6L150102 27 of 36

STL ST. LOUIS




Lab Sample ID: F6L150102-003Work Order: JLJCKMatrix: SOLID

Date Collected:Date Received:

12/11/06 090012/13/06 1145

Parameter

GROSS A/B BY

Gross Alpha

Gross Beta

Gamma Ra-226Actinium 228

Bismuth-210M

Bismuth 212

Bismuth 214

Cesium 137

Lead 210

Lead 212

Lead 214

Result Qual

GFPC 3W846 9310 MOD

6840

2760

& Hits By DOE GA-01-R Mod.

0.1 U

0.23 U

0.02 U

187

0.05 D

92

-3.95 U

188

Protactinium 234M 240

Radium (226)-Radium 228

Radium 224

' Thallium 208

Thorium 232

Thorium 234

Uranium 238

187

0.1 U.

11.2

-0.26 U

0.1 U

80

80

TotalUncert .

(2 o+/-) RL

pci/g700 10

280 10

pCi/g1.2

0.38

2.1

11

0.20

13

0.77

1165

11 1

1.2

6.2

0.38

1.2

10

10

MDC

Batch

8

5

Batch

2.0 .

0.63

'3.4

0.9

0.34

12

1.1

1

54

0.9

2.0

10

0.52

2.0

9

9

Prep AnalysisDate Date

# 6355409 Yld %

12/22/06 12/22/06

12/22/06 12/22/06

# 6355392 Yld %

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 ' 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

- — Other Detected Radionuclides

Actinium 227

Thorium 227

Thorium 231

Uranium 235

11.0

11.0

12.4

12.4

2.2

2.2

2.8

2.8

2.5

2.5

3.0

3.0

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

12/21/06 01/11/07

NOTE(S)




LOT# F6L150102 28 of 36

STL ST. LOUIS

METHOD BLANK REPORT


Client Lot ID:

Matrix:

Parameter •

F6L150102SOLID

Result Qual

Totaluncert .

(2 0+/-1

GROSS A/B BY GFPC SW846 9310 MOD

Gross Alpha

Gross Beta

Gamma Ra-226 &Actinium 228Bismuth-210MBismuth 212Bismuth 214Cesium 137Lead 210Lead 212Lead 214Protactinium 234M

Radium (226)

Radium 228

Radium 224Thallium 208Thorium 232 •Thorium 234Uranium 238

2 . 3

5.2

Hits By DOE-0.04 •

0.012

-0.03

-0.002

0.0 ,

0.6

, 0.042-0.012

0.0

-0.002

-0.04

0.00005

0.003

-0.04

-0.14

-0.14

U

J

GA-01-R Mod.

U

0

U

U

U

U

U

U

U

U

U

U

U

U

U

U

3

2

0

0

0

0

0

10

0

0

0

0

. 0

0

0

0

0

PCi/g.1

.4

PCi/g.98

.032

.28

.076

.025

.0

.057

.095

.85

.076

.98

.50

.036

.98

.84

.84

RL MDC

Batch # 6355409 Yld ?

10.0 5.

10.0 3.

14

Batch # 6355392 Yld °-

0.

0.

0.

0.

0.

1.0.

0.

3.

1.00 0.

0.

0.

0.

0.

0.

0.

28

056

51

15

050

6

098

14

1

152891075288686

PrepDate

Lab Sample ID

AnalysisDate

', F6L210000-409B

12/22/06

12/22/06

12/22/06

12/22/06

i F6L210000-392B

12/21/06

12/21/06

12/21/06

12/21/0612/21/06

12/21/06

12/21/0612/21/06

12/21/06

12/21/06

12/21/06

12/21/06

12/21/06

i 12/21/06

12/21/0612/21/06

01/11/07

01/11/0701/11/07

01/11/07

01/11/07 '01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

01/11/07

NOTE(S)


MDC is determined using instrument performance onlyBold results are greater than the MDC

J Result is greater than sample detection limit but less than stated reporting limit.


LOT# F6L150102 29 of 36

ST. LOUIS

Client Lot ID:Matrix:

Laboratory Control Sample Report

Severn Trent Laboratories - Radi©chemistry

F6L150102SOLID

Parameter

Gamma Ra-226Mod.Radium (226)

Thorium 232

GROSS A/B BY

Gross AlphaGross Beta

Spike Amount Result

& Hits By DOE GA-01-R

12.2 11.6

9.50 12.3

Batch #:

GFPC SW846 9310 MOD

34.0

37.0

Batch #:

6355392

34 .7

24.8

6355409

TotalUncert .

(2 o+ / - )

pCi/g

1.0

a 1.3

PCi/g8.0

4.2

MDC

GA-01-R MOD

0.5

0 . 6

Analysis Date:

9310 MOD

4.9

3.4

Analysis Date:

Lao £

H Yld % Rec

lampie ID

QC ControlLimits

F6L210000-392C

95 (78 - 108)

129 a (84 - 123)

01/16/07

F6L210000-409C

102

67

12/22/06

(43 - 123)

' (55 - 125)

NOTE(S>

HOC is determined by instrument performance onlyCalculations are performed before rounding to avoid round-off error in calculated results

a Spiked analyte outside of stated QC limits.

LOT# F6L150102 30 of 36

.STL ST. LOUIS

DUPLICATE EVALUATION REPORT


Client Lot ID:Matrix:

Parameter

F6L150102SOLID

SAMPLEResult

GROSS A/B BY GFFC SW846 9310 MOD

Gross AlphaGross Beta

Gamma Ra-226 & Hits

Actinium 228Bismuth 212'Bismuth 214Bismuth-210MCesium 137Lead 210Lead 212Lead 214Protactinium 234MRadium (226)Radium 224.Radium 228Thallium 208Thorium 232Thorium 234Uranium 238

19.230'. 7

Batch #:

By DOE GA-01-R

1.8 U0.7 U701

-3.20 U-0.01 U362

-16.1 U720

920

701

12601.8 U-0.80 U1.8 U409

409

Other Dedected RadionuclidesActinium 227 39.5

Protactinium 231Thorium 227Uranium 235

30

39.543.8

Batch S:

TotalUncart .

pci/g

5.8

5.1

6355409 (Sample)

Mod. pCi/g

1.14.3

41

0.93

0 .99

35

1.8

42

160

41

77

l-.l

0 .69

1.1

35

35

4.9

260

4.9

5.8

6355392 (Sample)

DUPLICATEL Result

Date Sampled:

Date Received

TotalUncert .

(2 < j + / - ) '

9310 MOD

22.128.0

6355409

GA-01-R

2.7 U-1.2 U699

-0.88 U-0.08 U366

-27.3 U712

920

699

'12602.7 U-1.35 U2.7 U394

394

35.949

35.945.6

6355392

6.5

4.3

(Duplicate)

MOD

1.7

3.8

41

0 . 9 4

1.1

39

2.3

41

120

41

77

1.7

0.62

1.7

35

35

6.2

37

6.2

6.3

(Duplicate)

12/13/06: 12/14/06

QC Sample ID

^ Y13 Precision

F6L140320-001

14

9

F6L150102-001

39

745 "

0 .4

114

154

1

52

1

0.02

0.4

0 .6

39

51

39

4

4

10

35

10

4

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD .

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

• %RPD

%RPD

%RPD

%RPD

NOTE(S)


Calculations are performed before rounding to avoid round-off error in calculated results


LOT# F6L150102 31 of 36

tr1O

Ol

(JlO

OK)

STL St. lootsJJ7IS K4» -tnUWonb

ROS13BM61TFrttaymct

LS.tS JO*'V«t»lirrank

2

Chain of Custody Record

rrtjtrt Wafff,: M BC>»»TO

aaaa

5

1-ltB. J-HO; >HHCM! «-B?(OJ; *-««O«,-«-DliCT

rpcdM fivtiadliiia/QC Re^[firattJrt»4 Cb

Sm«i* Bvort ( A

STLSman Tra I UfcmtnJ^Int

tf(mipfw«»™oli«=j anjtrifmn I meant*— ' fitttmfdr utxttx

CO

a

caUl

OJ0U)4X(JlCO-vl

aro

U)(Tl

St. Louis

- 5394 -

Client:Quote No:

rWV\ COC/RFANo:Initiated By:

Condition Upon Receipt FormDateTime: ;

Shipper Name:Shipping #

Shipping InformationMultiple Packages Y N N/ASample Temperature (s):

2.3.4.5.

Z f i w t y n b '&• i. (WuW" e.011 ° ' 7. • 2> • 7.

8. 3. 8.9. 4. 9.

10. 5. 10.+Numbered shipping lines correspond to Numbered Sample Temp lines **SamplB must be received at 4°C ± 2°C- If not, note contents below. Temperature

'^ . variance does NOTaffect the following: Metals-Liquid or Rad tests- Liquid or Solids

ConditiojyQrcle "Y" for yes, "N" for no and "N/A" for not applicable):

1.

2.

3.

4.

>5.

6.

7.-

Y(N •)

Y N^N/^)

Y N.

(Y>

/Y>

Y N(*N/A)rv>

Was sample received broken?Was sample received with properpH1 ? (rf not, make note below)If N/A-Was pH taken by originalSTL Lab?Sample received in propercontainers?Sample volume sufficient foranalysis?Headspace in VOA or TOX liquidsamples? -(If Yes, note sample ID's below)

Were.contents of the cooler 'frisked after opening

8.

9.

10.

11.

12.

13.

14.

^N

^Y>

Y(N>A

Yrfft

Y N N/A

Y N

Sample received with Chain of Custody?Chain of Custody matches sample ID's oncontainer(s)?

Are there custody seals present on cooler?Do custody seals on cooler appear to be tamperedwith?

Are there custody seals present on bottles?Do custody seals on bottles appear to be tamperedwith?

Was Internal COC/Workshare received?1 For DOE-AL (Pantex, LANL, Sandia) sites, pH of ALL containers received must he verified, EXCEPT VOA, TOX and soils.

Notes: .

Corrective Action:D Client Contact Name:D Sample(s) processed "as is"D Sample(s) on hold until:Project Management Review:THIS FORM MUST BE COMPLETEDTHE INITIATOR, THEN THAT PERSi

LOT# F6L150102

Informed by:

^f If released, notify:Date:

I ITEMS'ARE BEING CHECKED IN. IF ANV ifcfiM'lS COMPLETED BY SOMEONE OTHER THANI IS REQUIRED TO APPLY THEIR INITIAL AND THE DATE NEXT TO THAT ITEM.

ADMIN-0004, RE VISED 03/01/06\\Slsvr01\QA\FORMS\ST-LOUIS\ADMIN\AdminQ04030106.doc

33 Of 36

STL ST. LOUIS

F6L150102 CLIENT ANALYSIS SDMIMARY Storage Loc

DateProject Manager: BTO Quote #: 73561 . SDG:

AnalyticalProject: NORM

ReportPO#: Report to: Frank Virginia

Report Type:Client: 512882 AET Environmental Inc #SMPS in LOT: 3 EDO Code:

SAMPLE # CLIENT SAMPLE ID

1 DRUM 1

SAMPLE COMMENTS:HG O9 SW846 7471A Mercury (7471A. Cold Vapor) -

Solids

SE

AS

BA

CD

CR

PB

AG

XX

XX

XX

QO

QO

QO

QO

QO

QO

QO

OB

ZA

WM

SW846

SW846

SW846

SW84S

SWB46

SW846

SW846

EML

SW846

MCAWW

SAMPLE #

2 DRUM

601 OB

6010B

60108

6010B

601 OB

601 OB

601 OB

GA-01-RMOD9310MOD160.3MOD

Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(60 108)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)Gamma Ra-226 & Hits By DOEGA-01-R Mod.GROSS A/B BY GFPC SW8469310 MODMoisture, Percent(160.3)

70

GK

GK

GK

GK

GK

GK

GK

J9

FS

88

CLIENT SAMPLE ID

2

Sile ID Client Matrix

METALS. TOTAL (Method 01Exclusive) - SolidsMETALS. TOTAL - 2%HCLMETALS, TOTAL - 2%HCLMETALS, TOTAL - 2%HCLMETALS, TOTAL • 2%HCLMETALS, TOTAL - 2%HCLMETALS, TOTAL - 2%HCLMETALS, TOTAL - 2%HCLDry, Grind, and Fill Geometry -> 21day In-jrowthDry, Grind, Thin Layer onPlanchetNO SAMPLE PREPARATIONPERFORMED / DIRECT

01

01

01

01

01

01

01

01

01

01

Site IP Client Matrix

DATE/TIME SAMPLED

2006-12-1 1/ 900

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STAN CARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

DATE/TIME SAMPLED

2006-12-1 1/ 900

2-208Received: 2006-12-15

Due Date: 2007-01-10

Due Date: 2007-01-12

B .Standard Report

00

WORKORDER A

JLJA6

PROT: A WRKLOC

PROT:

PROT:

PROT:

PROT:

PROT:

PROT:

PROT:

PROT:

PROT:

PROT:

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

SOLID

06

06

06

06

06

06

06

06

06

06

06

WORKORDER A

JLJCG SOLID

SAMPLE COMMENTS:

HG

AG

AS

BA

. CD

SE

PB

CR

XX

XX

XX

09

QO

QO

QO

QO

QO

QO

QO

OB

ZA

WM

SWB46

SW846

SW846

SWB46

SW846

SW846

SW846

SW846

EML

SW846

MCAWW

SAMPLE #

3 DRUM

7471 A

601 OB

601 OB

601 OB

601 OB

601 OB

601 OB

601 OB

GA-01-RMOD9310MOO160.3MOD

CLIENT

3

Mercury (7471A. Cold Vapor) -SolidsInductively Coupled Plasma(6010B)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)Inductively Coupled Plasma(6010B)Gamma Ra-Z26 & Hits By DOEGA-01-R Mod.GROSS A/B BY GFPC SW8469310 MOOMoisture, Percent(160.3)

SAMPLE ID .

70

GK

GK

GK

GK

GK

GK

GK

J9

FS

88

METALS, TOTAL (MethodExclusive) - SolidsMETALS. TOTAL - 2%HCLMETALS. TOTAL - 2%HCLMETALS. TOTAL - 2%HCLMETALS. TOTAL - 2%HCLMETALS, TOTAL • 2%HCLMETALS, TOTAL - 2%HCLMETALS, TOTAL - 2%HCLDry. Grind, and Fill Geometry -> 21day in-growthDry, Grind, Thin Layer onPlanchetNO SAMPLE PREPARATIONPERFORMED / DIRECT

01

01

01

01

01

01

01

01

01

01

01

Site ID Client Matrix

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

DATEfTIME SAMPLED

2006-12-11 / 900

PROP

PROT.

PROP

PROT:

PROT:

PROT:

PROT:

PROT.

PROT:

PROT:

PROT:

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

06

06

06

06

06

06

06

06

06

06

06

WORKORDER A

JLJCK SOLID

SAMPLE COMMENTS:

HQ-

AS

SE

PB

CR

BA

STL - St.

'09

QO

QO

QO

QO

QO

Louis

SW846

SW646

SWB46

SW646

SW846

SW846

7471A

601 OB

601 OB

6010B

601 OB

601 OB

Mercury (7471A, Cold Vapor) -SolidsInductively Coupled Plasma(6010B)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(601 OB)

Logged in by: BRELJEC

70

GK

GK

GK

GK

GK

2006-

METALS, TOTAL (MathodExclusive) - SolidsMETALS. TOTAL - 2%HCLMETALS. TOTAL • 2%HCLMETALS. TOTAL - 2%HCLMETALS, TOTAL - 2% .HCLMETALS. TOTAL -2%.HCL

12-15 7:16:07

01

01

01

01

01

01

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

STANDARD TEST SET

printed on: Friday. December 15

PROT:

PROT:

PROT

PROT:

PROT:

PROT

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

A WRKLOC

,2006 08:16 A

06

06

06

06

06

06

Page 1 of 2

LOT# F6L150102 34 of 36

STL ST. LOUIS

F6L150102Project Manager: BTO

Project:

PO#:

Client: 512882

CLIENT ANALYSIS SUMMARY storage LOC.

Quote*: 73561 SDG:

NORM

Report to: Frank Virginia

AET Environmental Inc#SMPS in LOT: 3

Date Received:

Analytical Due Date:

Report Due Date:

Report Type: B

EDO Code: 00

2-2082006-12-15

2007-01-10

2007-01-12

Standard Report

AG QO SWB46 601 OB

CD QO SW846 601 OB

XX OB EML GA-01-RMOD

XX ZA SW846 9310MOD

XX WM MCAW 160.3W MOD

Inductively Coupled Plasma(6010B)Inductively Coupled Plasma(6010B)Gamma Ra-226 & Hits By DOEGA-01-R Mod.GROSS A/B BY GFPC SWW69310 MODMoisture, Percent(160.3)

GK METALS. TOTAL - 2%HCL

GK METALS. TOTAL - 2%HCL

jg Dry. Grind, and Fill Geometry -> 21day in-orowth

FS ^Y' Grind, Thin Layer onPlanchet

88 NO SAMPLE PREPARATIONPERFORMED/DIRECT

01 STANDARD TEST SET PROT: A



01 STANDARD TEST SET ' PROT: A


WRK 06LOCWRK 06LOCWRK 06LOCWRK 06LOCWRK 06LOC

STL - St. Louis Logged in by: BRELJEC 2006-12-15 7:16:07 printed on: Friday, December 15, 2006 08.16 A Page 2 of 2

LOT# F6L150102 35 of 36

STL ST. LOUIS . .

F6L150102 CLIENT COMMENTS SUMMARY storage LOC: 2-208'Date Received: 2006-12-15

Project Manager: BTO Quote*: 73561 SDG:Analytical Due Date: .2007-01-10

Project: NORMReport Due Date: 2007-01-12

PO#: Report to: Frank VirginiaReport Type: B Standard Report

Client: 512882 AET Environments, Inc #SMPS in LOT: 3 EDDCode: 00

STL-St.Louis Loggedlnby: BRELJEC 2006-12-15 7:16:07 printed on: Friday, December 15.2006 08:16 A Page 1 of 1

LOT# F6L150102 , 36 of 36

stl-st. louis severn stl' · stl-st. louis analytical report revised norm lot #: f6l150102...

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