site assessment report phase ii...chemical impacts exceeding idem risc idcls from 0 to 2 feet bgs...

Phase II Environmental Site Assessment Report

NBD Bank Trust/Zaleski Property East of Cline Avenue

Between Chicago Avenue and Gary Avenue Gary, Indiana, 46406

Prepared for: Gary/Chicago International Airport Authority

Submitted by:

Quality Environmental Professionals, Inc.

September 24, 2007

Table of Contents Executive Summary .......................................................................................................................1 1.0 Introduction ........................................................................................................................3 2.0 Physical Description...........................................................................................................4 2.1 Site Description ........................................................................................................4

2.2 Physical Setting ........................................................................................................4 3.0 Summary of Findings ........................................................................................................6 3.1 Sampling Methodology ............................................................................................6

3.2 Groundwater Flow ...................................................................................................6

3.3 Soil Sample Results .................................................................................................7

3.4 Groundwater Sample Results ...................................................................................8

4.0 Conclusions & Recommendation......................................................................................9 5.0 Report Disclaimer ............................................................................................................11 6.0 References Cited...............................................................................................................12 7.0 Signature Page ..................................................................................................................13

List of Figures Site Location Map (Topographic) ........................................................................................ Figure 1

Site Location Map w/ Soil Boring Locations ...................................................................... Figure 2

Groundwater Flow Map ....................................................................................................... Figure 3

VOCs Soil Analytical Map ................................................................................................ Figure 4a

cPAHs Soil Analytical Map ............................................................................................... Figure 4b

PCBs Soil Analytical Map ................................................................................................. Figure 4c

Metals Soil Analytical Map ............................................................................................... Figure 4d

VOCs Groundwater Analytical Map ................................................................................. Figure 5a

cPAHs Groundwater Analytical Map ................................................................................ Figure 5b

Metals Soil Analytical Map ............................................................................................... Figure 5c

Table of Contents (Continued)

List of Tables

VOC/TPH Soil Analytical Table .......................................................................................... Table 1

cPAHs Soil Analytical Table ................................................................................................ Table 2

PCBs Soil Analytical Table .................................................................................................. Table 3

Metals Soil Analytical Table Groundwater Analytical Table ............................................... Table 4

VOC/TPH Groundwater Analytical Table............................................................................ Table 5

cPAHs Groundwater Analytical Table ................................................................................. Table 6

Metals Groundwater Analytical Table .................................................................................. Table 7

List of Appendices Soil Boring Logs ............................................................................................................ Appendix A

Soil Laboratory Analytical Reports ............................................................................... Appendix B

Phase II Environmental Site Assessment NBD Bank Trust Properties

East of Cline Avenue between Chicago Avenue and Gary Avenue in Gary, Indiana Page 1

Executive Summary This Phase II Environmental Site Assessment (Phase II ESA) report was prepared for the Gary/Chicago International Airport Authority (GCIAA) to evaluate subsurface impacts to soil and groundwater for a portion of the NBD Bank Trust/Zaleski property, located east of Cline Avenue between Chicago Avenue and Gary Avenue in Gary, Indiana. The assessment area consisted of four parcels of primarily undeveloped land totaling approximately 84 acres of land. The site was vacant with the exception of one office trailer located in the truck parking lot along the western border of the southernmost parcel. The area of assessment consisted of the two southernmost parcels of the properties collectively referred to as the NBD Bank Trust/Zaleski property. This document has been prepared for the use of the GCIAA. A site location map has been provided as Figure 1. Quality Environmental Professionals, Inc. (Qepi) has performed a Phase II ESA for the NBD Bank Trust/Zaleski property, located to the east of Cline Avenue between Chicago Avenue and Gary Avenue in Gary, Indiana. This assessment consisted of the advancement of 10 soil borings and the installation of 6 groundwater monitoring wells throughout the parcels. The assessment revealed the following:

• 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding IDEM Risk Integrated System of Closure (RISC) Default Industrial Cleanup Levels (IDCLs) for total petroleum hydrocarbons (TPH) gasoline range organics (GRO) from a depth of 0 to 2 feet below ground surface (bgs). Additionally 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding RISC Default Industrial cleanup objectives for TPH (GRO) from a depth of 2 to 4 feet bgs.

• 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding IDEM RISC IDCLs for hydrocarbons TPH extended range organics (ERO) from a depth of 0 to 2 feet bgs. Additionally 3 of the 10 soil borings advanced exhibited chemical concentrations exceeding RISC Default Industrial cleanup objectives for TPH (ERO) from a depth of 2 to 4 feet bgs.

• 2 of the 10 soil borings advanced exhibited chemical concentrations above IDEM RISC IDCLS from a depth of 0 to 2 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. Additionally, one of these soil borings had a chemical concentration for benzo(a)pyrene and dibenzo(a,h)anthracene exceeding IDEM RISC IDCLs from 2 to 4 feet bgs and one of these soil borings also had chemical impacts exceeding IDEM RISC IDCLs from 2 to 4 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. One soil boring advanced had chemical impacts exceeding IDEM RISC IDCLs from a depth of 0 to 2 feet bgs for benzo(a)pyrene and dibenzo(a,h)anthracene. An additional soil boring advanced had chemical impacts exceeding IDEM RISC IDCLs from 0 to 2 feet bgs for benzo(a)pyrene and from 2 to 4 feet bgs for benzo(a)pyrene, benzo(b)fluroanthene and dibenzo(a,h)anthracene. Chemical impacts exceeding IDEM RISC IDCLs for phenathrene were also found in one soil boring from 0 to 2 feet bgs and 2 to 4 feet bgs.

Executive Summary (Continued)



• 1 of the 10 soil borings advanced exhibited chemical concentrations exceeding IDEM RISC IDCLs for lead from a depth of 0 to 2 feet bgs. Additionally, 2 of the 10 soil borings exhibited arsenic concentrations above IDEM RISC IDCLs from 0 to 2 feet bgs. One soil borings (B-7) exhibited concentrations exceeding IDEM RISC IDCLs for arsenic from 2 to 4 feet bgs.

• 3 of the 6 groundwater monitoring wells installed exhibited chemical concentrations above IDEM RISC IDCLs for TPH (ERO). Additionally, one of the monitoring wells exhibited chemical concentrations above IDEM RISC IDCLs for arsenic.

Based on the results of this assessment, impacts to both soil and groundwater exceeding IDEM RISC IDCLs were present for portions of the subject site. Qepi was provided with previously completed Phase II Environmental Site Assessments for the northern parcels of the site. Qepi will utilize data obtained from this assessment in concert with previously collected data to provide the GCIAA with remedial alternatives for soil and groundwater. Qepi will provide a Corrective Action Plan report to the GCIAA under separate cover.



1.0 Introduction Qepi was contracted by the Gary/Chicago International Airport Authority (GCIAA) to conduct a Phase II Environmental Site Assessment (Phase II ESA) for the two southernmost parcels of the property referred to as the NBD Bank Trust/Zaleski property, located to the east of Cline Avenue between Chicago Avenue and Gary Avenue in Gary, Indiana, herein referred to as the “site.” The GCIAA requested this Phase II ESA be conducted for redevelopment of the NBD Trust/Zaleski property for relocation of a portion of the Elgin, Joliet and Eastern Railroad and for extension of the GCIAA runway. This document is prepared for the sole use of the GCIAA and is a document upon which they may rely. This Phase II ESA was conducted in general conformance with American Society of Testing and Materials (ASTM) Standards for Phase II Environmental Site Assessments (ASTM E 1903). This assessment was conducted for the purpose of evaluating subsurface impacts to soil and groundwater throughout the two southernmost parcels of the property, which currently encompasses four separate parcels. A site map depicting the assessment area is provided as Figure 2. Based on the historic use of the site and under the direction of the GCIAA, the prospective chemicals of concerns (COCs) included in this assessment are volatile organic compounds (VOCs), carcinogenic polyaromatic hydrocarbons (cPAHs), polychlorinated biphenyls (PCBs), total petroleum hydrocarbons (TPH) gasoline range organics (GRO) and extended range organics (ERO) and Resource, Conservation and Recovery Act (RCRA) 8 metals. Qepi advanced a total of 10 soil borings to a maximum of depth of 14 feet below ground surface (bgs). In 7 of the 10 soil borings advanced, two soil samples were submitted for laboratory analysis of VOCs, cPAHs, PCBs, TPH (GRO/ERO) and RCRA 8 metals. The first soil sample collected from each soil borings was collected from the initial subsurface interval encountered. The second soil sample collected was collected from the depth encountered immediately above the first encountered saturated zone in 7 of the 10 borings. Three soil borings advanced (B-1, B-9 and B-10) were sampled from only sampled from the initial encountered subsurface interval due to the presence of a shallow water table. Soil boring locations are depicted on Figure 2. The purpose of this subsurface assessment was to determine the extent of impacts to soil and groundwater throughout the site and to provide the GCIAA with an evaluation of subsurface impacts encountered. This assessment was limited to the parameters sampled for and limited to the depths and areas sampled. Groundwater samples were collected from the monitoring wells installed during this assessment.



2.0 Physical Description

2.1 Site Description The subject property was located directly east of Cline Avenue, between Chicago Avenue and Gary Avenue in Gary, Indiana. The site was roughly rectangular in shape and bounded to the north and east by the Beemsterboer Slag Ballast property, to the north by Amerigas Propane and Chicago Avenue, to the south by Gary Avenue and the Elgin, Joliet and Eastern Railroad, to the east by the main runway of the Gary/Chicago International Airport and the former Conservation Chemical Company of Illinois property, and to the west by Cline Avenue. The site was located directly northwest of the Gary/Chicago International Airport, situated between Lake Michigan and the Grand Calumet River in Gary, Indiana. The subject property is located in the northeast quarter of Section 35, Township 37 North, and Range 9 West in Lake County, Indiana. The site has been represented on Figure 1 on the United States Geological Survey (USGS) 7.5 Minute Topographic Map of the Highland, Indiana Quadrangle. The site consisted of four vacant parcels of land with overgrowth vegetation and marshy lands on approximately 84 acres. An asphalt parking area was situated along the western boundary of the property, utilized for parking semi-trailers. A small office trailer was located along the western portion of the parking area. The site was roughly rectangular shaped. A gravel covered parking lot was located adjacent to the maintenance building. The site can be accessed via two paved entrance into the parking area running off of an access road located directly east of Cline Avenue. The site bordered to the north by Chicago Avenue and to the south by Gary Avenue. The assessment area consisted of the two southernmost parcels of the properties, Parcel # 25-40-0150-002 and Parcel # 25-40-0150-0011. The parcels were predominately undeveloped, with overgrowth vegetation and marshy lands encompassing a majority of the parcels. An asphalt parking area was present along the western portion of the parcels. Overgrowth vegetation and marsh lands present at the site were consistent with wetlands. Areas were noted where vegetation has grown atop asphalt debris. Staining was noted on surface soils and an oily sheen was noted on standing water present in numerous areas around the properties. Areas of distressed vegetation were present throughout the parcels. It should be noted that several monitoring wells were noted at the site in the eastern portion of the property, along with several drainage ditches. Based on files reviewed pertaining to the Conservation Chemical facility, located directly east of the site, these additional monitoring wells were related to the monitoring well network for that facility. These monitoring wells were not sampled as part of this assessment.

2.2 Physical Setting According to the USGS topographic map, the topography of the site is relatively flat with an elevation of approximately 590 feet above mean sea level (amsl). The site is located in the Calumet Lacustrine Plain Physiographic Region. The site is located in the Lake Michigan Basin

2.0 Physical Description (Continued)



(INDNR, 1987). The area is characterized by beach ridges, dunes and interridge marshes. Surficial deposits are predominately sand and gravel. Most of the surficial material was deposited during Wisconsinan and pre-Wisconsinan Glaciation. The predominate soils types in the project site area are Oakville-Tawas association soils consisting of steep, nearly level, very poorly drained and excessively drained and coarse textured to moderately coarse textured soils. These soils are developed in organic materials and in sandy mineral soil materials (Benton, 1977). The Oakville series found at the site consists of deep, excessively-drained soils formed in sandy dunes and beach ridges. Permeability is very rapid and it has a low available water capacity. Organic matter content is high in the surface layer. Runoff is slow. Slope ranges from 0 to 6 percent (Benton, 1977). Unconsolidated deposits in the vicinity of the subject site are approximately 150 feet thick (Gray, 1983). Underlying bedrock is the Devonian Muscatatuck Group overlapping and truncating the Silurian Niagaran Salamonie Dolomite (Gray, Ault, and Keller, 1987). The Muscatatuck Group predominately consists of beds of dolomite and sandy dolomitic quartz sandstone. The Salamonie Dolomite consists of beds dolomite and chert-rich limestone. (Shaver, et al, 1986). The bedrock surface underlying the site slopes to the southeast (Gray, 1982). Based upon area topography, surface drainage in the area of the site was likely towards the marshy lands located primarily in the center of the property. Previously conducted assessments determined groundwater flow to the south-southeast, which was based on survey data collected from previously installed groundwater monitoring wells. Regional groundwater flow direction in the area of the site is most likely south towards the Grand Calumet River (Beaty and Clendenon, 1987).



3.0 Summary of Finding

3.1 Sampling Methodology

A total of 10 soil borings (B-1 through SB-10) were advanced to depths ranging from 10 to 14 feet bgs at the site from August 7 to August 9, 2007. Each boring was advanced using direct push technology and logged on Qepi boring logs. Boring logs are provided as Appendix A. Drilling activities were conducted by D & T Drilling, Inc. of Osceola, Indiana under oversight by Qepi personnel. Soil was logged in 2-foot intervals and screened with a photo-ionization detector (PID). In 7 of the 10 borings, both the 2-foot interval at the initial soil surface and the 2-foot interval immediately above the first encountered saturated zone were submitted to Microbac Laboratories, Inc. of Merrillville, Indiana for laboratory analysis. Additionally, 3 of the soil borings were advanced (B-1, B-9 and B-10 with the initial soil surface interval sampled. Soil samples collected were submitted for laboratory analysis using United States Environmental Protection Agency (US EPA) SW-846 Method 8260 for VOCs, US EPA SW-846 Method 8270 for cPAHs, US EPA SW-846 Method 8270SIM, for PCBs using US EPA SW-846 Method 8082, for TPH (GRO/ERO) using US EPA SW-846 Method 8015 and US EPA SW-846 Method 6010B/7471A for RCRA 8 Metals. Samples collected were placed into laboratory-prepared sample containers and stored in a secured, iced cooler (at 4◦C) under Qepi chain of custody. In addition to the soil borings, Qepi installed 6 monitoring wells to depths ranging from 13 to 15 feet bgs. Following development of the wells, Qepi personnel measured and recorded static water levels of the monitoring well network. Monitoring wells were sampled using low flow sampling techniques. Groundwater monitoring well samples were submitted for laboratory analysis using US EPA SW-846 Method 8260 for VOCs, US EPA SW-846 Method 8270 for cPAHs, US EPA SW-846 Method 8270SIM, for PCBs using US EPA SW-846 Method 8082, for TPH (GRO/ERO) using US EPA SW-846 Method 8015 and US EPA SW-846 Method 6010B/7471A for RCRA 8 Metals. Samples collected were placed into laboratory-prepared sample containers and stored in a secured, iced cooler (at 4◦C) under Qepi chain of custody.

3.2 Groundwater Flow

On August 26, 2007, Qepi personnel measured and recorded the static water levels of the monitoring well network. Water was encountered at depths ranging from 3.00 feet to 10.61 feet in monitoring wells MW-1 and MW-5 respectively. Based on the static water level measurements collected on June 15, 2007, groundwater flow at the site is to the south toward the Grand Calumet River. A groundwater flow map is provided as Figure 3.

3.0 Summary of Findings (Continued)



3.3 Soil Analytical Results

3.3.1 Volatile Organics Compounds/Total Petroleum Hydrocarbons Soil impacts exceeding IDEM RISC IDCLs were encountered in 4 soil borings advanced (B-1, B-2, B-5, B-6) from a depth of 0 to 2 feet bgs and in 4 soil borings advanced (B-2, B-5, B-6, B-7) from a depth of 2 to 4 feet bgs for TPH (GRO). Additionally, soil impacts exceeding IDEM RISC IDCLs were encountered in 4 soil borings (B-1, B-2, B-5, B-6) from a depth of 0 to 2 feet bgs and in 3 soil borings (B-2, B-5, B-6) from a depth of 2 to 4 feet bgs for TPH (ERO). No VOC concentration encountered exceeded industrial cleanup objectives. VOC and TPH analytical results have been depicted on Figure 4a and shown on Table 1.

3.3.2 Carcinogenic Polyaromatic Hydrocarbons

Soil impacts exceeding IDEM RISC IDCLs were encountered in 2 soil borings advanced (B-5, B-6) from a depth of 0 to 2 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. Additionally, soil boring B-5 had a chemical concentration for benzo(a)pyrene and dibenzo(a,h)anthracene exceeding IDEM RISC IDCLs from 2 to 4 feet bgs. Soil boring B-6 also had chemical impacts exceeding IDEM RISC IDCLs from 2 to 4 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. Soil boring B-1 had chemical impacts exceeding IDEM RISC IDCLs from a depth of 0 to 2 feet bgs for benzo(a)pyrene and dibenzo(a,h)anthracene. Soil boring B-2 had chemical impacts exceeding IDEM RISC IDCLs from 0 to 2 feet bgs for benzo(a)pyrene and from 2 to 4 feet bgs for benzo(a)pyrene, benzo(b)fluroanthene and dibenzo(a,h)anthracene. Chemical impacts exceeding IDEM RISC IDCLs for phenathrene were found in soil boring B-6 from 0 to 2 feet bgs and 2 to 4 feet bgs. CPAH analytical results are depicted on Figure 4b and shown on Table 2. 3.3.3 Polychlorinated Biphenyls No soil impacts were encountered exceeding IDEM RISC Residential or IDEM RISC Industrial Cleanup objectives for PCBs. PCBs do not appear to be of concern for soils in the assessment area. PCB analytical results are depicted on Figure 4c and shown on Table 3.

3.0 Summary of Findings (Continued)



3.3.4 Metals Soil impacts exceeding IDEM RISC IDCLs were encountered in 1 soil boring advanced (B-1) from a depth of 0 to 2 feet bgs. Additionally, 2 soil borings advanced (B-6 and B-8) exhibited arsenic concentrations above IDEM RISC IDCLs from 0 to 2 feet bgs and 1 soil boring advanced (B-7) exhibited an arsenic concentration exceeding IDEM RISC IDCLs from 2 to 4 feet bgs. No other metal concentration encountered exceeding industrial cleanup objectives. Metal analytical results are depicted on Figure 4d and shown on Table 4.

3.4 Groundwater Analytical Results 3.4.1 Volatile Organics Compounds/Total Petroleum Hydrocarbons Groundwater impacts exceeding IDEM RISC IDCLs were encountered in 3 of the 6 groundwater monitoring wells installed (MW-1, MW-3, MW-5) for TPH (ERO) with the highest concentration (6,600 ppb) located at MW-1 and MW-5. VOC concentrations encountered did not exceed industrial cleanup objectives. VOC and TPH analytical results are depicted on Figure 5a and shown on Table 5.

3.4.2 Carcinogenic Polyaromatic Hydrocarbons

Groundwater impacts were not encountered exceeding IDEM RISC Residential or IDEM RISC Industrial Cleanup objectives. CPAHs do not appear to be of concern for groundwater in the assessment area. CPAH analytical results are depicted on Figures 5b and shown on Table 6. 3.4.4 Metals Groundwater impacts exceeding IDEM RISC IDCLs were encountered for arsenic in monitoring well MW – 3. No additional metals concentrations encountered exceeded IDEM RISC industrial cleanup objectives. Metals analytical results are depicted on Figure 5c and shown on Table 7.



4.0 Conclusions & Recommendations Qepi has performed this Phase II ESA as outlined in the proposed scope of work for the NBD Bank Trust/Zaleski property located to the east of Cline Avenue between Chicago Avenue and Gary Avenue in Gary, Indiana. This assessment revealed the following results:

• 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding RISC IDCLs for total TPH (GRO) from a depth of 0 to 2 feet bgs. Additionally 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding RISC Default Industrial cleanup objectives for TPH (GRO) from a depth of 2 to 4 feet bgs.

• 4 of the 10 soil borings advanced exhibited chemical concentrations exceeding IDEM RISC IDCLs for hydrocarbons TPH (ERO) from a depth of 0 to 2 feet bgs. Additionally 3 of the 10 soil borings advanced exhibited chemical concentrations exceeding RISC Default Industrial cleanup objectives for TPH (ERO) from a depth of 2 to 4 feet bgs.

• 2 of the 10 soil borings advanced exhibited chemical concentrations above IDEM RISC IDCLS from a depth of 0 to 2 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. Additionally, one of these soil borings had a chemical concentration for benzo(a)pyrene and dibenzo(a,h)anthracene exceeding IDEM RISC IDCLs from 2 to 4 feet bgs and one of these soil borings also had chemical impacts exceeding IDEM RISC IDCLs from 2 to 4 feet bgs for benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene and dibenzo(a,h)anthracene. One soil boring advanced had chemical impacts exceeding IDEM RISC IDCLs from a depth of 0 to 2 feet bgs for benzo(a)pyrene and dibenzo(a,h)anthracene. An additional soil boring advanced had chemical impacts exceeding IDEM RISC IDCLs from 0 to 2 feet bgs for benzo(a)pyrene and from 2 to 4 feet bgs for benzo(a)pyrene, benzo(b)fluroanthene and dibenzo(a,h)anthracene. Chemical impacts exceeding IDEM RISC IDCLs for phenathrene were also found in one soil boring from 0 to 2 feet bgs and 2 to 4 feet bgs.

• 1 of the 10 soil borings advanced exhibited chemical concentrations exceeding IDEM RISC

IDCLs for lead from a depth of 0 to 2 feet bgs. Additionally, 2 of the 10 soil borings exhibited arsenic concentrations above IDEM RISC IDCLs from 0 to 2 feet bgs. One soil borings (B-7) exhibited concentrations exceeding IDEM RISC IDCLs for arsenic from 2 to 4 feet bgs.

• 3 of the 6 groundwater monitoring wells installed exhibited chemical concentrations

above IDEM RISC IDCLs for TPH (ERO). Additionally, one of the monitoring wells exhibited chemical concentrations above IDEM RISC IDCLs for arsenic.

Based on the findings of this assessment, chemical impacts exceeding IDEM RISC IDCLs were present in both soil and groundwater for portions of the subject site. Qepi was provided with previously completed Phase II Environmental Site Assessments for the northern parcels of the site. Qepi will utilize data obtained from this assessment in concert with previously collected data to

4.0 Conclusions & Recommendation (Continued)



provide the GCIAA with remedial alternatives for both soil and groundwater. Qepi will provide a Corrective Action Plan report to the GCIAA under separate cover.



5.0 Report Disclaimer This Phase II ESA report was prepared in accordance with generally accepted principles and practices in the environmental consulting field. Conclusions and recommendations expressed herein were developed from site evaluation and limited research, and we are not responsible for unrecorded data pertaining to this site. Qepi makes no warranties, expressed or implied, as to the fitness or merchantability of said property for any particular purpose, and we are not responsible for independent conclusions or opinions made by others based on this report. This assessment was limited to the areas specified on the figures of this report. Qepi is not responsible for the identification of recognized environmental conditions that may be present outside this evaluated area, chemical parameters other than those specified by the GCIAA, or at depths greater than that to which soil borings were advanced. Any opinions and/or recommendations presented apply to site conditions existing at the time of performance of services. We are unable to report on or accurately predict events, which may impact the site, following performance of the described services, whether occurring naturally or caused by external forces. We assume no responsibility for conditions we are not authorized to investigate, or conditions not generally recognized as predictable at the time services are performed. Qepi makes no recommendations in regards to the sale, purchase, lease, construction, or other improvements on the subject property. We are not responsible for changes in applicable regulatory standards, practices, or regulations following performance of services.



6.0 References Cited Fenelon, Joseph M., Keith E. Bobay, et al., 1994. Hydrogeologic Atlas of Aquifers in Indiana.

United States Geological Survey, Water-Resources Investigations Report 92-4142. Gray, Henry H., 1983, Map of Indiana Showing Thickness of Unconsolidated Deposits,

Department of Natural Resources, Geological Survey, Miscellaneous Map 37.

Gray, Henry H., Curtis H. Ault, and Stanley J. Keller, 1987, Bedrock Geologic Map of Indiana, Department of Natural Resources, Geological Survey, Miscellaneous Map 48.

Shaver, Robert H., Curtis H. Ault, Ann M. Burger, Donald D. Carr, John B. Droste, Donald L. Eggert, Henry H. Gray, Denver Harper, Nancy R. Hasenmueller, Walter A. Hasenmueller, Alan S. Horowitz, Harold C. Hutchison, Brian D. Keith, Stanley J. Keller, John B. Patton, Carl B. Rexroad, and Charles E. Weir, 1986, Compendium of Paleozoic Rock-Unit Stratigraphy in Indiana - A Revision, Indiana Geological Survey, Bulletin 59

Shineldecker, Chris L. Handbook of Environmental Contaminants: A Guide for Site Assessment. Lewis Publishers, Inc. 1992.

United States Department of Agriculture, Soil Conservation Service, 1979. Soil Survey of Lake County, Indiana.

United States Geological Survey, Highland, Indiana Quadrangle, Indiana, 7.5 Minute Series Topographic Map.

7.0 Signature Page

This Phase II Environmental Site Assessment report was prepared by Mr. Nivas R. Vijay, Project Manager, and reviewed by Mr. Philip N. Ward, Director of Geology Services. Nivas R. Vijay Project Manager

Philip N. Ward, LPG Director of Geology Services



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FIGURE 1SITE LOCATION MAP

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Site Location MapHighland Quadrangle

Section 35, Township 37N, Range 9W

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Sample LocationDate SampledSample Depth (feet)BenzeneCarbon DisulfideEthylbenzenecis-1,2-DichloroetheneMethylene ChlorideTolueneTrichloroetheneXylenesTPH-GROTPH-ERO

3806,800

18.8<5.54.3<22

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Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Benzene <5.7 <7.6Carbon Disulfide <11 19Ethylbenzene 8.6 13cis-1,2-Dichloroethene <5.7 <7.6Methylene Chloride <23 <30Toluene 6.0 9.6Trichloroethene <5.7 <7.6Xylenes 30 65TPH-GRO 720 2,000TPH-ERO 4,400 28,000

08/07/07B-2

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Benzene <5.6 <6.3Carbon Disulfide <11 <13Ethylbenzene <5.6 1cis-1,2-Dichloroethene <5.6 <6.3Methylene Chloride <22 <25Toluene <5.6 <6.3Trichloroethene <5.6 <6.3Xylenes 3.7 2.4TPH-GRO <560 <630TPH-ERO <9.6 <9.9

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Sample LocationDate SampledSample Depth (feet) 0'-2 2'-4'Benzene <5.3 <6.2Carbon Disulfide <11 <12Ethylbenzene 2.1 1.3cis-1,2-Dichloroethene <5.3 <6.2Methylene Chloride <21 <25Toluene <5.3 <6.2Trichloroethene <5.3 <6.2Xylenes 14.1 3.9TPH-GRO <530 <620TPH-ERO 27 <9.9

08/08/07B-4

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Benzene 21 <67Carbon Disulfide <110 <130Ethylbenzene 55 81cis-1,2-Dichloroethene <57 <67Methylene Chloride <230 <270Toluene 180 12Trichloroethene <57 <67Xylenes 630 340TPH-GRO 26,000 27,000TPH-ERO 69,000 9,900

08/08/07B-5

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Benzene 48 60Carbon Disulfide <160 <120Ethylbenzene 220 <60cis-1,2-Dichloroethene <79 <60Methylene Chloride <79 <240Toluene 90 46Trichloroethene <79 <60Xylenes 1,000 720TPH-GRO 160,000 250,000TPH-ERO 14,000 11,000

08/08/07B-6

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Benzene <5.8 <8.1Carbon Disulfide <12 <16Ethylbenzene <5.8 1.9cis-1,2-Dichloroethene <5.8 <8.1Methylene Chloride <23 <32Toluene <5.8 <8.1Trichloroethene <5.8 <8.1Xylenes 2.7 9.2TPH-GRO <580 460TPH-ERO <9.7 <9.5

08/08/07B-7

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4' 8'-10'Benzene <5.9 1.3 <530Carbon Disulfide 2.4 <10 <1100Ethylbenzene 2.7 <5.2 290cis-1,2-Dichloroethene <5.9 <5.2 86Methylene Chloride 33 20 930Toluene 1.3 <5.2 <530Trichloroethene 3.6 <5.2 <530Xylenes 8.5 2.1 430TPH-GRO 300 <260 410,000TPH-ERO <12 <9.8 4,000

08/09/07B-8


<650<12

3.1<6.5<6.538

1.3<6.5

<6.5<13

08/09/070'-2'

B-9


<53017

8.1<5.3<5.323

2.5<5.3

<5.3<11

08/09/070'-2'

B-10

NRV

FIGURE 4BPAH IN SOIL


Clin

e A

ve

State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

e A

veC

line

Av e


Clin

e A

veC

line

Av e

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:



³

Legend

Soil Boring

Site Boundary

Sample LocationDate SampledSample Depth (feet)AcenaptheneAcenapthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenzo(a,h)anthraceneFluorantheneFluoreneIndeno(1,2,3-cd)pyreneNaphthalenePhenanthrenePyrene

B-108/07/07

0'-2'8521

2803,3004,4002,8005,500950

6,8003,600350100

1,600400

1,2003,100

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Acenapthene 88 3,100Acenapthylene <580 370Anthracene 260 1,200Benzo(a)anthracene 3,100 9,600Benzo(a)pyrene 3,000 6,100Benzo(b)fluoranthene 4,000 8,200Benzo(g,h,i)perylene 4,200 3,200Benzo(k)fluoranthene 840 2,500Chrysene 6,000 34,000Dibenzo(a,h)anthracene 1,100 1,700Fluoranthene 670 3,600Fluorene 210 5,600Indeno(1,2,3-cd)pyrene 670 930Naphthalene 390 170Phenanthrene 3,500 16,000Pyrene 9,200 28,000

B-208/07/07

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Acenapthene <56 <63Acenapthylene <56 <63Anthracene 10 <63Benzo(a)anthracene 120 <63Benzo(a)pyrene 290 25Benzo(b)fluoranthene 150 18Benzo(g,h,i)perylene 270 21Benzo(k)fluoranthene 34 <63Chrysene 320 <63Dibenzo(a,h)anthracene 79 <63Fluoranthene 69 <63Fluorene 7.9 <63Indeno(1,2,3-cd)pyrene 77 <63Naphthalene 13 <63Phenanthrene 270 22Pyrene 300 44

B-308/07/07

Sample LocationDate SampledSample Depth (feet) 0'-2 2'-4'Acenapthene 6.4 <62Acenapthylene <53 <62Anthracene 29 <62Benzo(a)anthracene 240 <62Benzo(a)pyrene 190 <62Benzo(b)fluoranthene 220 <62Benzo(g,h,i)perylene 330 9.5Benzo(k)fluoranthene 51 <62Chrysene 600 30Dibenzo(a,h)anthracene 70 <62Fluoranthene 150 <62Fluorene 24 <62Indeno(1,2,3-cd)pyrene 93 <62Naphthalene 58 <62Phenanthrene 840 <62Pyrene 630 20

B-408/08/07

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Acenapthene 8,800 3,900Acenapthylene 1,600 630Anthracene 5,000 1,300Benzo(a)anthracene 40,000 14,000Benzo(a)pyrene 25,000 8,800Benzo(b)fluoranthene 30,000 9,500Benzo(g,h,i)perylene 16,000 5,300Benzo(k)fluoranthene 7,900 2,100Chrysene 130,000 44,000Dibenzo(a,h)anthracene 8,500 3,100Fluoranthene 15,000 4,500Fluorene 16,000 6,700Indeno(1,2,3-cd)pyrene 4,400 1,700Naphthalene 4,100 440Phenanthrene 92,000 36,000Pyrene 110,000 34,000

B-508/08/07

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Acenapthene 3,700 4,000Acenapthylene 620 430Anthracene 8,100 10,000Benzo(a)anthracene 64,000 52,000Benzo(a)pyrene 23,000 16,000Benzo(b)fluoranthene 25,000 16,000Benzo(g,h,i)perylene 14,000 7,600Benzo(k)fluoranthene 6,900 4,600Chrysene 180,000 87,000Dibenzo(a,h)anthracene 9,800 4,000Fluoranthene 39,000 44,000Fluorene 16,000 36,000Indeno(1,2,3-cd)pyrene 5,700 3,400Naphthalene 2,900 450Phenanthrene 200,000 740,000Pyrene 150,000 130,000

B-608/08/07

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4'Acenapthene <58 <81Acenapthylene <58 <81Anthracene 34 110Benzo(a)anthracene 330 59Benzo(a)pyrene 490 27Benzo(b)fluoranthene 310 35Benzo(g,h,i)perylene 450 42Benzo(k)fluoranthene 67 <81Chrysene 530 97Dibenzo(a,h)anthracene 330 <81Fluoranthene 72 35Fluorene 8.1 12Indeno(1,2,3-cd)pyrene 180 13Naphthalene 24 9.1Phenanthrene 300 120Pyrene 320 130

B-708/08/07

Sample LocationDate SampledSample Depth (feet) 0'-2' 2'-4' 8'-10'Acenapthene - - -Acenapthylene - - -Anthracene - - -Benzo(a)anthracene <59 <52 150Benzo(a)pyrene <59 <52 <640Benzo(b)fluoranthene <59 <52 <640Benzo(g,h,i)perylene - - -Benzo(k)fluoranthene <59 <52 <640Chrysene 8.2 7.6 160Dibenzo(a,h)anthracene <59 <52 <640Fluoranthene - - -Fluorene - - -Indeno(1,2,3-cd)pyrene <59 <52 <640Naphthalene <59 <52 270Phenanthrene - - -Pyrene - - -

B-808/09/07

Sample LocationDate SampledSample Depth (feet)Acenapthene - -Acenapthylene - -Anthracene - -Benzo(a)anthracene 12 -Benzo(a)pyrene <65 -Benzo(b)fluoranthene <65 -Benzo(g,h,i)perylene - -Benzo(k)fluoranthene <65 -Chrysene 12 -Dibenzo(a,h)anthracene <65 -Fluoranthene - -Fluorene - -Indeno(1,2,3-cd)pyrene <65 -Naphthalene <65 -Phenanthrene - -Pyrene - -

B-908/09/07

0'-2'

Sample Location B-10Date Sampled 08/09/07Sample Depth (feet) 0'-2'Acenapthene -Acenapthylene -Anthracene -Benzo(a)anthracene 140Benzo(a)pyrene 190Benzo(b)fluoranthene 100Benzo(g,h,i)perylene -Benzo(k)fluoranthene 54Chrysene 180Dibenzo(a,h)anthracene 26Fluoranthene -Fluorene -Indeno(1,2,3-cd)pyrene 66Naphthalene 11Phenanthrene -Pyrene -

NRV

FIGURE 4CPCBs IN SOIL


Clin

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State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

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veC

line

Av e


Clin

e A

veC

line

Av e

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:



³

Legend

Soil Boring

Site Boundary

Sample Location B-1 Date Sampled 08/07/07 Sample Depth (feet) 0'-2' PCB-1254 (Aroclor 1254) 180

Sample Location Date Sampled Sample Depth (feet) 0'-2' 2'-4' PCB-1254 (Aroclor 1254) 100 <500

B-208/07/07

Sample Location Date Sampled Sample Depth (feet) 0'-2' 2'-4' PCB-1254 (Aroclor 1254) 190 180

B-508/08/07

Sample Location Date Sampled Sample Depth (feet) 0'-2' 2'-4' PCB-1254 (Aroclor 1254) 410 78

B-608/08/07

NRV

FIGURE 4DMETALS IN SOIL


Clin

e A

ve

State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

e A

veC

line

Av e


Clin

e A

veC

line

Av e

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:



³

Legend

Soil Boring

Site Boundary

Sample Location B-1Date Sampled 08/07/07Sample Depth 0'-2'Arsenic 3.0Barium 22Cadmium 0.16Chromium 9.7Lead 1,700Mercury 0.27Selenium <1.6Silver <0.54

Sample LocationDate SampledSample Depth 0'-2' 2'-4'Arsenic 2.8 5.2Barium 40 12Cadmium 0.35 <0.14Chromium 7.1 3.8Lead 65 9.9Mercury 0.85 0.052Selenium <1.4 <2.0Silver <0.48 <0.68

B-208/07/07

Sample LocationDate SampledSample Depth 0'-2' 2'-4'Arsenic 2.1 2.7Barium 20 8.7Cadmium 0.15 <0.12Chromium 3.8 3.3Lead 44 9.9Mercury 0.04 0.01Selenium <1.5 <1.9Silver <0.50 <0.62

B-308/07/07

Sample LocationDate SampledSample Depth 0'-2 2'-4'Arsenic 2.2 2.1Barium 9.9 4.5Cadmium 0.062 <0.12Chromium 3.7 2.6Lead 17 2.2Mercury 0.64 0.0035Selenium <1.5 <1.7Silver <0.54 <0.58

B-408/08/07

Sample LocationDate SampledSample Depth 0'-2' 2'-4'Arsenic 5.1 4.3Barium 48 20Cadmium 0.65 <0.13Chromium 3.8 3.7Lead 130 52Mercury 0.062 0.014Selenium <1.5 <2.0Silver <0.51 <0.67

08/08/07B-5

Sample LocationDate SampledSample Depth 0'-2' 2'-4'Arsenic 5.9 1.6Barium 52 4.8Cadmium 0.89 <0.11Chromium 6.2 2.8Lead 190 3.9Mercury 0.29 0.0038Selenium <2.4 <1.7Silver <0.79 <0.58

B-608/08/07

Sample LocationDate SampledSample Depth 0'-2' 2'-4'Arsenic 2.0 9.5Barium 15 18Cadmium 0.017 0.13Chromium 4.5 3.5Lead 17 18Mercury 0.070 0.016Selenium <1.7 <2.2Silver <0.56 <0.72

B-708/08/07

Sample LocationDate SampledSample Depth 0'-2' 2'-4' 8'-10'Arsenic 8.5 0.98 2.3Barium 100 6.9 12Cadmium 1.2 <0.10 <0.20Chromium 410 2.3 410Lead 60 4.0 5.9Mercury 0.10 0.0031 0.041Selenium <1.8 <1.5 <3.0Silver <0.59 <0.52 <0.99

B-808/09/07

Sample LocationDate SampledSample DepthArsenicBariumCadmiumChromiumLeadMercurySeleniumSilver

B-908/09/07

4.8<0.12

0'-2'0.83

<0.61

0.00161

2.36.4

Sample Location B-10Date Sampled 08/09/07Sample Depth 0'-2'Arsenic 1.3Barium 560Cadmium 0.19Chromium 11Lead 22Mercury <0.043Selenium 9.2Silver <0.52

NRV

FIGURE 6AVOCs IN WATER


Clin

e A

ve

State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

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veC

line

Av e


Clin

e A

veC

line

Av e

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:


6001 WEST INDUSTRIAL HIGHWAYGARY, INDIANA

³

Legend

Soil Boring

Site Boundary

Sample Location MW-1Date Sampled 08/26/07Benzene 0.93Chloromethane 1.81,2-Dichloroethane <5.01,1-Dichloroethene <5.0cis-1,2-Dichloroethene <5.0trans-1,2-Dichloroethene <5.0Ehtylbenzene <5.0Toluene 1.11,1,1-Trichloroethane <5.0Trichloroethene <5.0Xylenes 0.92Vinyl Chloride <10 TPH-ERO 6,600

Sample Location MW-3Date Sampled 08/26/07Benzene 2Chloromethane 1.51,2-Dichloroethane <5.01,1-Dichloroethene <5.0cis-1,2-Dichloroethene <5.0trans-1,2-Dichloroethene <5.0Ehtylbenzene 1.9Toluene 1.21,1,1-Trichloroethane <5.0Trichloroethene <5.0Xylenes 4.2Vinyl Chloride <10 TPH-ERO 4,700

Sample Location MW-4Date Sampled 08/26/07Benzene <5.0Chloromethane 1.21,2-Dichloroethane <5.01,1-Dichloroethene <5.0cis-1,2-Dichloroethene <5.0trans-1,2-Dichloroethene <5.0Ehtylbenzene <5.0Toluene <5.01,1,1-Trichloroethane <5.0Trichloroethene <5.0Xylenes <5.0Vinyl Chloride <10 TPH-ERO <100

Sample Location MW-5Date Sampled 08/26/07Benzene 6.1Chloromethane 2.81,2-Dichloroethane 4.41,1-Dichloroethene 80cis-1,2-Dichloroethene 310trans-1,2-Dichloroethene 3.1Ehtylbenzene 2.9Toluene <5.01,1,1-Trichloroethane 1.3Trichloroethene 10Xylenes 2.3Vinyl Chloride 20 TPH-ERO 6,600

Sample Location MW-6Date Sampled 08/26/07Benzene <5.0Chloromethane 1.61,2-Dichloroethane <5.01,1-Dichloroethene <5.0cis-1,2-Dichloroethene 0.87trans-1,2-Dichloroethene <5.0Ehtylbenzene <5.0Toluene <5.01,1,1-Trichloroethane <5.0Trichloroethene <5.0Xylenes <5.0Vinyl Chloride <10 TPH-ERO 200

NRV

FIGURE 6BcPAHs IN WATER

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Clin

e A

ve

State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

e A

veC

line

Av e


Clin

e A

veC

line

Av e


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:



³

Legend

Soil Boring

Site Boundary

Sample Location MW-1Date Sampled 08/26/07Acenapthene 0.58Anthracene <1.0Benzo(a)anthracene <1.0Benzo(a)pyrene <1.0Benzo(b)fluoranthene <1.0Benzo(g,h,i)perylene <1.0Benzo(k)fluoranthene <1.0Chrysene <1.0Dibenzo(a,h)anthracene <1.0Fluoranthene <1.0Fluorene 0.42Indeno(1,2,3-cd)pyrene <1.0Naphthalene 0.23Phenanthrene <1.0Pyrene 0.34

Sample Location MW-3Date Sampled 08/26/07Acenapthene 0.58Anthracene 0.88Benzo(a)anthracene 1.3Benzo(a)pyrene 0.57Benzo(b)fluoranthene 0.84Benzo(g,h,i)perylene 0.58Benzo(k)fluoranthene <1.0Chrysene 1.7Dibenzo(a,h)anthracene <1.0Fluoranthene 1.9Fluorene 4.0Indeno(1,2,3-cd)pyrene <1.0Naphthalene 0.66Phenanthrene 41Pyrene 4.1

Sample Location MW-5Date Sampled 08/26/07Acenapthene <1.0Anthracene <1.0Benzo(a)anthracene <1.0Benzo(a)pyrene <1.0Benzo(b)fluoranthene <1.0Benzo(g,h,i)perylene <1.0Benzo(k)fluoranthene <1.0Chrysene <1.0Dibenzo(a,h)anthracene <1.0Fluoranthene <1.0Fluorene <1.0Indeno(1,2,3-cd)pyrene <1.0Naphthalene 0.39Phenanthrene <1.0Pyrene <1.0

Sample Location MW-6Date Sampled 08/26/07Acenapthene <0.99Anthracene <0.99Benzo(a)anthracene 0.27Benzo(a)pyrene 0.46Benzo(b)fluoranthene 0.56Benzo(g,h,i)perylene 1.1Benzo(k)fluoranthene <0.99Chrysene <0.99Dibenzo(a,h)anthracene 0.8Fluoranthene <0.99Fluorene <0.99Indeno(1,2,3-cd)pyrene 0.92Naphthalene <0.99Phenanthrene 1.2Pyrene <0.99

NRV

FIGURE 6CMETALS IN WATER


Clin

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ve

State Road 312

Gary Ave

145th St

Chicago Ave

Columbus Dr

Dearborn St

Clin

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veC

line

Av e


Clin

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veC

line

Av e

B-9

B-5

B-3

B-1

B-8/MW-5

B-7/MW-4

B-6/MW-3

B-4/MW-2

B-2/MW-1

B-10/MW-6


Checked By:

07-05-024

CWH

Drawn By:


9/14/07

1"=1000'

1Sheet:



³

Legend

Soil Boring

Site Boundary

Sample Location MW-1Date Sampled 08/26/07Arsenic 0.0027Barium 0.056Chromium 0.002Lead <0.0075Silver <0.010

Sample Location MW-2Date Sampled 08/26/07Arsenic <0.010Barium 0.013Chromium 0.0019Lead 0.0031Silver <0.010

Sample Location MW-3Date Sampled 08/26/07Arsenic 0.018Barium 0.029Chromium 0.0021Lead 0.040Silver 0.0026

Sample Location MW-4Date Sampled 08/26/07Arsenic <0.010Barium 0.066Chromium 0.0016Lead <0.0075Silver <0.010



Table

s

Sam

ple

Loc

atio

n

Dat

e Sa

mpl

ed

Sam

ple

Dep

th (f

eet)

Ben

zene

Car

bon

Dis

ulfid

e

Car

bon

Tet

rach

lori

de

1,1

-Dic

hlor

oeth

ane

1,2

-Dic

hlor

oeth

ane

1,1

-Dic

hlor

oeth

ene

Eth

ylbe

nzen

e

cis

-1,2

-Dic

hlor

oeth

ene

tran

s-1,

2- D

ichl

oroe

then

e

Met

hyle

ne C

hlor

ide

Tet

rach

loro

ethe

ne

Tol

uene

1,1

,1-T

rich

loro

etha

ne

Tri

chlo

roet

hene

Vin

yl C

hlor

ide

Xyl

enes

TPH

-GR

O

TPH

-ER

O

34 10,000 66 5,600 24 58 13,000 400 680 23 58 12,000 1,900 57 13 210,000 25 80

350 82,000 290 58,000 150 42,000 200,000 5,800 14,000 1,800 640 96,000 280,000 350 27 430,000 330 1,000

0'-2' <5.7 <11 <5.7 <5.7 <5.7 <5.7 8.6 <5.7 <5.7 <23 <5.7 6.0 <5.7 <5.7 <11 30 720 4,4002'-4' <7.6 19 <7.6 <7.6 <7.6 <7.6 13 <7.6 <7.6 <30 <7.6 9.6 <7.6 <7.6 <15 65 2,000 28,0000'-2' <5.6 <11 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <5.6 <22 <5.6 <5.6 <5.6 <5.6 <11 3.7 <560 <9.62'-4' <6.3 <13 <6.3 <6.3 <6.3 <6.3 1 <6.3 <6.3 <25 <6.3 <6.3 <6.3 <6.3 <13 2.4 <630 <9.90'-2 <5.3 <11 <5.3 <5.3 <5.3 <5.3 2.1 <5.3 <5.3 <21 <5.3 <5.3 <5.3 <5.3 <11 14.1 <530 272'-4' <6.2 <12 <6.2 <6.2 <6.2 <6.2 1.3 <6.2 <6.2 <25 <6.2 <6.2 <6.2 <6.2 <12 3.9 <620 <9.90'-2' 21 <110 <57 <57 <57 <57 55 <57 <57 <230 <57 180 <57 <57 <110 630 26,000 69,0002'-4' <67 <130 <67 <67 <67 <67 81 <67 <67 <270 <67 12 <67 <67 <130 340 27,000 9,9000'-2' 48 <160 <79 <79 <79 <79 220 <79 <79 <79 <79 90 <79 <79 <160 1,000 160,000 14,0002'-4' 60 <120 <60 <60 <60 <60 <60 <60 <60 <240 <60 46 <60 <60 <120 720 250,000 11,0000' 2' <5 8 <12 <5 8 <5 8 <5 8 <5 8 <5 8 <5 8 <5 8 <23 <5 8 <5 8 <5 8 <5 8 <12 2 7 <580 <9 7

<5.5

08/08/07

B-3 08/07/07

B-4 08/08/07

B-6

<5.5

Table 1TPH and VOCs in Soil

NBD Trust/Zaleski Property

Gary, IndianaEast of Cline Avenue between Gary and Chicago Avenue

RISC Default Residential closure levels

RISC Default Industrial closure levels

<22 18.8B-1 08/07/07

B-2 08/07/07

B-5 08/08/07

0'-2' <5.5 <5.5 <5.5 <5.5 <5.51.9 <11 <11 380 6,8002.3 4.3 <5.5 <5.5

0'-2' <5.8 <12 <5.8 <5.8 <5.8 <5.8 <5.8 <5.8 <5.8 <23 <5.8 <5.8 <5.8 <5.8 <12 2.7 <580 <9.72'-4' <8.1 <16 <8.1 <8.1 <8.1 <8.1 1.9 <8.1 <8.1 <32 <8.1 <8.1 <8.1 <8.1 <16 9.2 460 <9.50'-2' <5.9 2.4 <5.9 <5.9 <5.9 <5.9 2.7 <5.9 <5.9 33 <5.9 1.3 <5.9 3.6 <12 8.5 300 <122'-4' 1.3 <10 <5.2 <5.2 <5.2 <5.2 <5.2 <5.2 <5.2 20 <5.2 <5.2 <5.2 <5.2 <5.2 2.1 <260 <9.8

8'-10' <530 <1100 <530 <530 <530 <530 290 86 <530 930 <530 <530 <530 <530 <1100 430 410,000 4,000

Notes: Values presented in parts per billion (ppb) or ug/kgConstituents not listed were below the laboratory detection limitDefault Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 8260 and 8015 Bold cell denotes value exceeds RISC Default Residential closure level

Shaded cell denotes value exceeds RISC Default Industrial closure level

B-9 08/09/07

B-10 08/09/07

B-7 08/08/07

B-8 08/09/07

1.3

2.5 8.1

<6.5 38 <6.5 <6.50'-2'

0'-2'

<6.5 <6.5 <6.5 <6.5 <13 <650 <123.1

<5.3 <5.3 <5.3 <5.3 <5.3

<6.5

<11 <530 17<5.3<5.3 <11 <5.323 <5.3 <5.3 <5.3

<6.5<6.5 <13 <6.5

Page 1 of 7

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9,500,000 1,100,000 2,000,000 5,000 500 5,000 16,000 50,000 500,000 500 2,000,000 6,300,000 5,000 700 13,000 2,000,000

24,000,000 2,800,000 37,000,000 15,000 1,500 15,000 16,000 150,000 1,500,000 1,500 2,000,000 16,000,000 15,000 170,000 170,000 2,000,000

3 6002 800210'-2' 1 600 3 100400280 5 500 950 6 80085

RISC Default Industrial Closure Levels

3 300 4 400B-1 08/07/07

Table 2cPAHs in Soil

NBD Trust/Zaleski PropertyEast of Cline Avenue between Gary and Chicago Avenue

RISC Default Residential Closure Levels

Gary, Indiana

350 100 1 200

0'-2' 88 <580 260 3,100 3,000 4,000 4,200 840 6,000 1,100 670 210 670 390 3,500 9,2002'-4' 3,100 370 1,200 9,600 6,100 8,200 3,200 2,500 34,000 1,700 3,600 5,600 930 170 16,000 28,0000'-2' <56 <56 10 120 290 150 270 34 320 79 69 7.9 77 13 270 3002'-4' <63 <63 <63 <63 25 18 21 <63 <63 <63 <63 <63 <63 <63 22 440'-2 6.4 <53 29 240 190 220 330 51 600 70 150 24 93 58 840 6302'-4' <62 <62 <62 <62 <62 <62 9.5 <62 30 <62 <62 <62 <62 <62 <62 200'-2' 8,800 1,600 5,000 40,000 25,000 30,000 16,000 7,900 130,000 8,500 15,000 16,000 4,400 4,100 92,000 110,0002'-4' 3,900 630 1,300 14,000 8,800 9,500 5,300 2,100 44,000 3,100 4,500 6,700 1,700 440 36,000 34,0000'-2' 3,700 620 8,100 64,000 23,000 25,000 14,000 6,900 180,000 9,800 39,000 16,000 5,700 2,900 200,000 150,0002'-4' 4,000 430 10,000 52,000 16,000 16,000 7,600 4,600 87,000 4,000 44,000 36,000 3,400 450 740,000 130,0000'-2' <58 <58 34 330 490 310 450 67 530 330 72 8.1 180 24 300 3202'-4' <81 <81 110 59 27 35 42 <81 97 <81 35 12 13 9.1 120 1300'-2' - - - <59 <59 <59 - <59 8.2 <59 - - <59 <59 - -2'-4' - - - <52 <52 <52 - <52 7.6 <52 - - <52 <52 - -

8'-10' - - - 150 <640 <640 - <640 160 <640 - - <640 270 - -

3,600

- - - - -<65

08/07/07

B-4 08/08/07

B-7 08/08/07

B-5

2,800210 2 1,600 3,100400280 5,500 950 6,800

<65 <65

85

08/08/07

B-6 08/08/07

B-3

3,300 4,400B 1 08/07/07

B-2 08/07/07

0'-2' <65 12 <65-

B-8 08/09/07

B-9 08/09/07 12

350 100 1,200

<65- -

B-10 08/09/07 0'-2' - - - 140 190 100 - 54 180 26 - - 66 11-

-

Notes: Values presented in parts per billion (ppb) or ug/kgDefault Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 8270SIM-: Not analyzed

Bold cell denotes value exceeds RISC Default Residential closure levelShaded cell denotes value exceeds RISC Default Industrial closure level

Page 2 of 7

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PC

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101

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PC

B-1

221

(Aro

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122

1)

PC

B-1

232

(Aro

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123

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B-1

242

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248

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B-1

254

(Aro

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B-1

260

(Aro

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126

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PC

B-1

262

(Aro

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126

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PC

B-1

268

(Aro

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126

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1,800 1,800 1,800 1,800 1,800 1,800 1,800 1,800 1,800

5,300 5,300 5,300 5,300 5,300 5,300 5,300 5,300 5,300

0'-2' <38 <38 <38 <38 <38 100 <38 <38 <382'-4' <500 <500 <500 <500 <500 <500 <500 <500 <5000'-2' <37 <37 <37 <37 <37 <37 <37 <37 <372'-4' <42 <42 <42 <42 <42 <42 <42 <42 <420'-2 <35 <35 <35 <35 <35 <35 <35 <35 <352'-4' <41 <41 <41 <41 <41 <41 <41 <41 <410'-2' <38 <38 <38 <38 <38 190 <38 <38 <382'-4' <44 <44 <44 <44 <44 180 <44 <44 <440'-2' <52 <52 <52 <52 <52 410 <52 <52 <522'-4' <39 <39 <39 <39 <39 78 <39 <39 <390'-2' <38 <38 <38 <38 <38 <38 <38 <38 <382' 4' <53 <53 <53 <53 <53 <53 <53 <53 <53

Gary, Indiana

Table 3PCBs in Soil


B-3 08/07/07



B-1 08/07/07

B-2 08/07/07

B-4 08/08/07

B-5 08/08/07

B-6 08/08/07

B-7 08/08/07

0'-2' <37 <37 <37 <37 <37<37 180 <37 <37

2 -4 <53 <53 <53 <53 <53 <53 <53 <53 <530'-2' <39 <39 <39 <39 <39 <39 <39 <39 <392'-4' <34 <34 <34 <34 <34 <34 <34 <34 <348'-10' <210 <210 <210 <210 <210 <210 <210 <210 <210

B-10 08/09/07 0'-2' <35 <35 <35 <35 <35 <35 <35 <35 <35

Default Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Ammended Aug-06.Notes: Values presented in parts per billion (ppb) or ug/kg

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 8082Bold cell denotes value exceeds RISC Default Residential closure level


B-8 08/09/07

B-9 08/09/07 <430'-2' <43 <43 <43 <43 <43 <43 <43 <43

Page 3 of 7

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3.9 1,600 7.5 10,000 81 2 5 31

5.8 10,000 77 10,000 230 32 53 87

0'-2' 2.8 40 0.35 7.1 65 0.85 <1.4 <0.482'-4' 5.2 12 <0.14 3.8 9.9 0.052 <2.0 <0.680'-2' 2.1 20 0.15 3.8 44 0.04 <1.5 <0.502'-4' 2.7 8.7 <0.12 3.3 9.9 0.01 <1.9 <0.620'-2 2.2 9.9 0.062 3.7 17 0.64 <1.5 <0.542'-4' 2.1 4.5 <0.12 2.6 2.2 0.0035 <1.7 <0.580'-2' 5.1 48 0.65 3.8 130 0.062 <1.5 <0.512'-4' 4.3 20 <0.13 3.7 52 0.014 <2.0 <0.670'-2' 5.9 52 0.89 6.2 190 0.29 <2.4 <0.79



Gary, Indiana

Table 4Metals in Soil


B-1

B-2

B-3

B-4

B-5

B-6

0'-2'08/07/07

08/07/07

08/07/07

08/08/07

08/08/07

08/08/07

0.16 9.7 1,700 0.273.0 22 <1.6 <0.54

2'-4' 1.6 4.8 <0.11 2.8 3.9 0.0038 <1.7 <0.580'-2' 2.0 15 0.017 4.5 17 0.070 <1.7 <0.562'-4' 9.5 18 0.13 3.5 18 0.016 <2.2 <0.720'-2' 8.5 100 1.2 410 60 0.10 <1.8 <0.592'-4' 0.98 6.9 <0.10 2.3 4.0 0.0031 <1.5 <0.52

8'-10' 2.3 12 <0.20 410 5.9 0.041 <3.0 <0.99

B-10 08/09/07 0'-2' 1.3 560 0.19 11 22 <0.043 9.2 <0.52

Default Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.Notes: Values presented in parts per million (ppm) or mg/kg

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 6010B/7471ABold cell denotes value exceeds RISC Default Residential closure level


B-9 08/09/07 0'-2'

B-6

B-7

B-8 08/09/07

08/08/07

08/08/07

1 <0.610.83 4.8 <0.12 2.3 6.4 0.0016

Page 4 of 7

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5 990 5 - 5 7 70 100 5 700.0 5 1,000 200 5 10,000 2 100

22 10,000 52 - 31 5,100 1,000 2,000 380 10,000 55 8,200 29,000 31.0 20,000 4 1,100

MW-1 08/26/07 <5.0 <5.0 0.93 1.8 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 1.1 <5.0 <5.0 0.92 <10 6,600MW-2 08/26/07 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 250MW-3 08/26/07 <5.0 <5.0 2 1.5 <5.0 <5.0 <5.0 <5.0 <10 1.9 <5.0 1.2 <5.0 <5.0 4.2 <10 4,700MW-4 08/26/07 <5.0 <5.0 <5.0 1.2 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <100MW-5 08/26/07 <5.0 <5.0 6.1 2.8 4.4 80 310 3.1 <10 2.9 <5.0 <5.0 1.3 10 2.3 2 6,600MW-6 08/26/07 <5.0 <5.0 <5.0 1.6 <5.0 <5.0 0.87 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 200

N V l d i billi ( b) /l



Table 5VOCs in Groundwater

East of Cline Avenue between Gary and Chicago AvenueGary, Indiana

NBD Trust/Zaleski Property

Notes: Values presented in parts per billion (ppb) or ug/lDefault Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 8260 and 8015 Bold cell denotes value exceeds RISC Default Residential closure level


Page 5 of 7

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460 71 2,000,000 5,000 500 5,000 16,000 50,000 500,000 500 2,000,000 310 5,000 700 13,000 2,000,000

4,200 730 37,000,000 15,000 1,500 15,000 16,000 150,000 1,500,000 1,500 2,000,000 2,000 15,000 170,000 170,000 2,000,000

MW-1 08/26/07 0.58 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.42 <1.0 0.23 <1.0 0.34MW-2 08/26/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0MW-3 08/26/07 0.58 <1.0 0.88 1.3 0.57 0.84 0.58 <1.0 1.7 <1.0 1.9 4.0 <1.0 0.66 41 4.1MW-4 08/26/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0MW-5 08/26/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.39 <1.0 <1.0MW-6 08/26/07 <0.99 <0.99 <0.99 0.27 0.46 0.56 1.1 <0.99 <0.99 0.8 <0.99 <0.99 0.92 1.2 <0.99 <0.99

Notes: Values presented in parts per billion (ppb) or ug/lDefault Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 8270d l d f l id i l l l l

Gary, Indiana

RISC Default Residential Closure Levels

RISC Default Industrial Closure Levels

Table 6cPAHs in Water


Bold cell denotes value exceeds RISC Default Residential closure levelShaded cell denotes value exceeds RISC Default Industrial closure level

Page 6 of 7

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0.01 2 0.005 0.1 0.015 0.002 0.05 0.18

0.01 20 0.051 150 0.042 0.031 0.51 0.51

MW-1 08/26/07 0.0027 0.056 <0.002 0.002 <0.0075 <0.0002 <0.030 <0.010MW-2 08/26/07 <0.010 0.013 <0.002 0.0019 0.0031 <0.0002 <0.030 <0.010MW-3 08/26/07 0.018 0.029 <0.002 0.0021 0.040 <0.0002 <0.030 0.0026MW-4 08/26/07 <0.010 0.066 <0.002 0.0016 <0.0075 <0.0002 <0.030 <0.010MW-5 08/26/07 0.0066 0.038 <0.002 0.11 <0.0075 <0.0002 <0.030 <0.010MW-6 08/26/07 0.003 0.073 <0.002 0.0024 <0.0075 <0.0002 <0.030 <0.010



Gary, Indiana

Table 7Metals in Groundwater

East of Cline Avenue between Gary and Chicago AvenueNBD Trust/Zaleski Property

Notes: Values presented in parts per million (ppm) or mg/lDefault Closure levels based on RISC Technical Users Guide, Updated 01/31/06. Amended August 2006.

Analytical: Samples analyzed at MicroBac Laboratories, Inc. using US EPA SW-846 Method 6010B/7471ABold Cell denotes value exceeds RISC Default Residential closure level

Shaded Cell denotes value exceeds RISC Default Industrial closure level

Page 7 of 7

Appendix A

Appendix B

of 48

Page 1 of 48

August 27, 2007

Quality Environmental Professionals, Inc.Nivas Vijay

Dear Nivas Vijay:RE: NBD - Gary Airport

Work Order No.: ME07083491611 S. Franklin RoadIndianapolis, IN 46239

The enclosed results were obtained from and are applicable to the sample(s) as received at the laboratory. All sample results are reported on an "as received" basis unless otherwise noted.

All data included in this report have been reviewed and meet the applicable project specific and certification specific requirements, unless otherwise noted. A qualifications page is included in this report and lists the programs under which Microbac maintains certification.

This report has been paginated in its entirety and shall not be reproduced except in full, without the written approval of Microbac Laboratories.

We appreciate the opportunity to service your analytical needs. If you have any questions, please feel free to contact us.

Sincerely,Microbac Laboratories, Inc.

Deborah GriffithsSenior Project Manager

Enclosures

Microbac Laboratories, Inc. received 14 samples on 8/8/2007 4:30:00 PM for the analyses presented in the following report.

5713 West 85th Street, Indianapolis, IN 46278 TEL.800.466.5577 TEL.317.872.1375 FAX.317.872.1379Page 1 of 48

of 48

Page 2 of 48

Project: NBD - Gary Airport

CLIENT: Quality Environmental Professionals, Inc.

Lab Order: ME0708349

Lab Sample ID Client Sample ID Collection DateTag Number Date Received

WORK ORDER SAMPLE SUMMARY Date: Monday, August 27, 2007

ME0708349-01A B-1 8/7/2007 10:02:00 AM0-2’ 8/8/2007

ME0708349-02A B-2 8/7/2007 12:03:00 PM0-2’ 8/8/2007

ME0708349-03A B-2 8/7/2007 12:11:00 PM2-4’ 8/8/2007

ME0708349-04A B-3 8/7/2007 2:42:00 PM0-2’ 8/8/2007

ME0708349-05A B-3 8/7/2007 2:45:00 PM2-4’ 8/8/2007

ME0708349-06A B-4 8/8/2007 8:02:00 AM0-2’ 8/8/2007

ME0708349-07A B-4 8/8/2007 8:04:00 AM2-4’ 8/8/2007

ME0708349-08A B-5 8/8/2007 10:46:00 AM0-2’ 8/8/2007

ME0708349-09A B-5 8/8/2007 10:51:00 AM2-4’ 8/8/2007

ME0708349-10A B-6 8/8/2007 11:10:00 AM0-2’ 8/8/2007

ME0708349-11A B-6 8/8/2007 11:13:00 AM2-4’ 8/8/2007

ME0708349-12A B-7 8/8/2007 2:12:00 PM0-2’ 8/8/2007

ME0708349-13A B-7 8/8/2007 2:19:00 PM2-4’ 8/8/2007

ME0708349-14A DUP 8/8/2007


of 48

Page 3 of 48

RLMDLSTAnalyses Result Qual Units AnalyzedDF

ANALYTICAL RESULTS

Client Project: NBD - Gary AirportClient Sample ID: B-1

Collection Date: 08/07/07 10:02Sample Matrix: Soil

Client: Quality Environmental Professionals, Inc.

Work Order / ID: ME0708349-01

Date: Monday, August 27, 2007

Sample Description: 0-2’Date Received: 08/08/07 16:30

PCB’S SW8082 Analyst: ALSMethod: Prep Date/Time: 08/15/07 08:30

Aroclor 1016 08/17/07 18:5137 µg/Kg-dry 1A ND 3.3

Aroclor 1221 08/17/07 18:5137 µg/Kg-dry 1A ND 37




Aroclor 1254 08/17/07 18:5137 µg/Kg-dry 1A 180 3.7




Total PCB’s 08/17/07 18:5137 µg/Kg-dry 1A 180 2.3

Surr: Tetrachloro-m-xylene S 08/17/07 18:515-165 %REC 1S 265 0

Surr: Decachlorobiphenyl 08/17/07 18:515-222 %REC 1S 30.0 0

EXTENDED RANGE ORGANICS SW8015BMOD Analyst: ALSMethod: Prep Date/Time: 08/10/07 01:30

Extended Range Organics 08/12/07 02:33470 mg/Kg 50A 6800 470

Surr: Decafluorobiphenyl SD 08/12/07 02:3350-150 %REC 50S 0 0

TOTAL METALS SW6010B Analyst: AVCMethod: Prep Date/Time: 08/10/07 10:30

Arsenic 08/13/07 16:210.54 mg/Kg-dry 1A 3.0 0.11

Barium 08/10/07 16:300.11 mg/Kg-dry 1A 22 0.021

Cadmium 08/10/07 16:300.11 mg/Kg-dry 1A 0.16 0.0065

Chromium 08/10/07 16:300.16 mg/Kg-dry 1A 9.7 0.02

Lead 08/10/07 16:300.41 mg/Kg-dry 1A 1700 0.064

Selenium 08/10/07 16:301.6 mg/Kg-dry 1A ND 0.081

Silver 08/10/07 16:300.54 mg/Kg-dry 1A ND 0.086

TOTAL METALS SW7471A Analyst: AVCMethod: Prep Date/Time: 08/10/07 10:00

Mercury 08/10/07 13:060.037 mg/Kg-dry 1A 0.27 0.00081

PAH BY GC/MS-SIM SW8270C Analyst: BEMMethod: Prep Date/Time: 08/14/07 14:44

Acenaphthene J 08/14/07 19:30110 µg/Kg-dry 2A 85 12

Acenaphthylene J 08/14/07 19:30110 µg/Kg-dry 2A 21 12

Anthracene 08/14/07 19:30110 µg/Kg-dry 2A 280 17

Benzo[a]anthracene 08/14/07 19:30110 µg/Kg-dry 2A 3300 15

Benzo[a]pyrene 08/15/07 00:54550 µg/Kg-dry 10A 4400 79

Benzo[b]fluoranthene 08/14/07 19:30110 µg/Kg-dry 2A 2800 24

Benzo[g,h,i]perylene 08/15/07 00:54550 µg/Kg-dry 10A 5500 79

5713 West 85th Street, Indianapolis, IN 46278 TEL.800.466.5577 TEL.317.872.1375 FAX.317.872.1379

Page 3 of 48

of 48

Page 4 of 48


ANALYTICAL RESULTS








Benzo[k]fluoranthene 08/14/07 19:30110 µg/Kg-dry 2A 950 21

Chrysene 08/15/07 00:54550 µg/Kg-dry 10A 6800 69

Dibenz[a,h]anthracene 08/14/07 19:30110 µg/Kg-dry 2A 3600 16

Fluoranthene 08/14/07 19:30110 µg/Kg-dry 2A 350 21

Fluorene J 08/14/07 19:30110 µg/Kg-dry 2A 100 13

Indeno[1,2,3cd]pyrene 08/14/07 19:30110 µg/Kg-dry 2A 1600 15

Naphthalene 08/14/07 19:30110 µg/Kg-dry 2A 400 12

Phenanthrene 08/14/07 19:30110 µg/Kg-dry 2A 1200 18

Pyrene 08/15/07 00:54550 µg/Kg-dry 10A 3100 68

Surr: Nitrobenzene-d5 08/14/07 19:3014.2-125 %REC 2S 43.2 0

Surr: 2-Fluorobiphenyl 08/14/07 19:3021.6-112 %REC 2S 41.0 0

Surr: Terphenyl-d14 08/14/07 19:3010-139 %REC 2S 82.9 0

VOLATILE ORGANICS SW8260B Analyst: NLTMethod: Prep Date/Time:

Acetone 08/15/07 16:5955 µg/Kg-dry 1A ND 11

Acrolein 08/15/07 16:59110 µg/Kg-dry 1A ND 17

Acrylonitrile 08/15/07 16:59110 µg/Kg-dry 1A ND 14

Benzene J 08/15/07 16:595.5 µg/Kg-dry 1A 1.9 1.3

Bromodichloromethane 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.55

Bromoform 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.78

Bromomethane 08/15/07 16:5911 µg/Kg-dry 1A ND 4

2-Butanone 08/15/07 16:5911 µg/Kg-dry 1A ND 4

Carbon Disulfide 08/15/07 16:5911 µg/Kg-dry 1A ND 1.9

Carbon tetrachloride 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.3

Chlorobenzene 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.66

Chloroethane 08/15/07 16:5911 µg/Kg-dry 1A ND 2.7

Chloroform 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.66

Chloromethane 08/15/07 16:5911 µg/Kg-dry 1A ND 1.7

Dibromochloromethane 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.89

1,1-Dichloroethane 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.78


1,1-Dichloroethene 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.3

cis-1,2-Dichloroethene 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.89

trans-1,2-Dichloroethene 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.1

1,2-Dichloropropane 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.1

cis-1,3-Dichloropropene 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.89

trans-1,3-Dichloropropene 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.78

Ethylbenzene J 08/15/07 16:595.5 µg/Kg-dry 1A 2.3 0.78


Page 4 of 48

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Page 5 of 48


ANALYTICAL RESULTS








2-Hexanone 08/15/07 16:5911 µg/Kg-dry 1A ND 2.7

4-Methyl-2-Pentanone 08/15/07 16:5911 µg/Kg-dry 1A ND 1.9

Methyl-t-Butyl Ether 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.66

Methylene chloride 08/15/07 16:5922 µg/Kg-dry 1A ND 9.6

Styrene 08/15/07 16:595.5 µg/Kg-dry 1A ND 0.89

1,1,1,2-Tetrachloroethane 08/15/07 16:5911 µg/Kg-dry 1A ND 0.66

1,1,2,2-Tetrachloroethane 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.6

Tetrachloroethene 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.8

Toluene J 08/15/07 16:595.5 µg/Kg-dry 1A 4.3 0.78

1,1,1-Trichloroethane 08/15/07 16:595.5 µg/Kg-dry 1A ND 1.1


Trichloroethene 08/15/07 16:595.5 µg/Kg-dry 1A ND 1

Trichlorofluoromethane 08/15/07 16:5911 µg/Kg-dry 1A ND 3.8

Vinyl Acetate 08/15/07 16:5911 µg/Kg-dry 1A ND 1.7

Vinyl chloride 08/15/07 16:5911 µg/Kg-dry 1A ND 1.9

m,p-Xylene 08/15/07 16:595.5 µg/Kg-dry 1A 8.8 1.8

o-Xylene 08/15/07 16:595.5 µg/Kg-dry 1A 10 1

Total Xylenes 08/15/07 16:595.5 µg/Kg-dry 1A 19 1

Surr: 4-Bromofluorobenzene 08/15/07 16:5948.6-134 %REC 1S 84.3 0

Surr: Dibromofluoromethane 08/15/07 16:5970-136 %REC 1S 99.0 0

Surr: 1,2-Dichloroethane-d4 08/15/07 16:5968.6-148 %REC 1S 107 0

Surr: Toluene-d8 08/15/07 16:5959.4-155 %REC 1S 115 0

GASOLINE RANGE ORGANICS SW8260BMOD Analyst: NLTMethod: Prep Date/Time:

Gasoline Range Organics J 08/15/07 16:59550 µg/Kg-dry 1A 380 280


PERCENT MOISTURE 2540B_18ED Analyst: ALLMethod: Prep Date/Time:

Percent Moisture 08/12/07 12:230.10 WT% 1A 9.7 0.1


Page 5 of 48

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Page 6 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 16:580.097 mg/Kg-dry 1A 40 0.018



Lead 08/10/07 16:580.36 mg/Kg-dry 1A 65 0.057






Acenaphthene J 08/15/07 01:19580 µg/Kg-dry 10A 88 64

Acenaphthylene 08/15/07 01:19580 µg/Kg-dry 10A ND 62

Anthracene J 08/15/07 01:19580 µg/Kg-dry 10A 260 90






Page 6 of 48

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Page 7 of 48


ANALYTICAL RESULTS












Fluorene J 08/15/07 01:19580 µg/Kg-dry 10A 210 67


Naphthalene J 08/15/07 01:19580 µg/Kg-dry 10A 390 61


Pyrene 08/15/07 01:19580 µg/Kg-dry 10A 9200 70








Benzene 08/15/07 17:335.7 µg/Kg-dry 1A ND 1.4



Bromomethane 08/15/07 17:3311 µg/Kg-dry 1A ND 4.1

2-Butanone 08/15/07 17:3311 µg/Kg-dry 1A ND 4.1

Carbon Disulfide 08/15/07 17:3311 µg/Kg-dry 1A ND 2















Ethylbenzene 08/15/07 17:335.7 µg/Kg-dry 1A 8.6 0.8


Page 7 of 48

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Page 8 of 48


ANALYTICAL RESULTS









4-Methyl-2-Pentanone 08/15/07 17:3311 µg/Kg-dry 1A ND 2


Methylene chloride 08/15/07 17:3323 µg/Kg-dry 1A ND 10





Toluene 08/15/07 17:335.7 µg/Kg-dry 1A 6.0 0.8






Vinyl chloride 08/15/07 17:3311 µg/Kg-dry 1A ND 2

m,p-Xylene 08/15/07 17:335.7 µg/Kg-dry 1A 16 1.8

o-Xylene 08/15/07 17:335.7 µg/Kg-dry 1A 14 1

Total Xylenes 08/15/07 17:335.7 µg/Kg-dry 1A 30 1


Surr: Dibromofluoromethane 08/15/07 17:3370-136 %REC 1S 104 0




Gasoline Range Organics 08/15/07 17:33570 µg/Kg-dry 1A 720 290



Percent Moisture 08/12/07 12:230.10 WT% 1A 13 0.1


Page 8 of 48

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Page 9 of 48


ANALYTICAL RESULTS

















Total PCB’s 08/20/07 15:30500 µg/Kg-dry 10A ND 32

Surr: Tetrachloro-m-xylene 08/20/07 15:305-165 %REC 10S 50.1 0

Surr: Decachlorobiphenyl 08/20/07 15:305-222 %REC 10S 100 0

EXTENDED RANGE ORGANICS SW8015BMOD Analyst: MLTMethod: Prep Date/Time: 08/10/07 01:30

Extended Range Organics 08/14/07 15:11750 mg/Kg-dry 50A 28000 750




Barium 08/10/07 17:030.14 mg/Kg-dry 1A 12 0.026

Cadmium 08/10/07 17:030.14 mg/Kg-dry 1A ND 0.0082


Lead 08/10/07 17:030.51 mg/Kg-dry 1A 9.9 0.081




Mercury J 08/10/07 13:150.062 mg/Kg-dry 1A 0.052 0.0013


Acenaphthene 08/15/07 01:44760 µg/Kg-dry 10A 3100 85








Page 9 of 48

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Page 10 of 48


ANALYTICAL RESULTS












Fluorene 08/15/07 01:44760 µg/Kg-dry 10A 5600 88




Pyrene 08/15/07 14:241500 µg/Kg-dry 20A 28000 180



Surr: Terphenyl-d14 08/15/07 01:4410-139 %REC 10S 125 0

VOLATILE ORGANICS SW8260B Analyst: JLNMethod: Prep Date/Time:

Acetone 08/15/07 23:29760 µg/Kg-dry 10A 1500 150







2-Butanone 08/15/07 23:29150 µg/Kg-dry 10A 360 55

Carbon Disulfide 08/15/07 18:0615 µg/Kg-dry 1A 19 2.6















Ethylbenzene 08/15/07 18:067.6 µg/Kg-dry 1A 13 1.1


Page 10 of 48

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Page 11 of 48


ANALYTICAL RESULTS
















Toluene 08/15/07 18:067.6 µg/Kg-dry 1A 9.6 1.1



Trichloroethene 08/15/07 18:067.6 µg/Kg-dry 1A ND 1.4




m,p-Xylene 08/15/07 18:067.6 µg/Kg-dry 1A 30 2.4

o-Xylene 08/15/07 18:067.6 µg/Kg-dry 1A 35 1.4

Total Xylenes 08/15/07 18:067.6 µg/Kg-dry 1A 65 1.4











Page 11 of 48

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Page 12 of 48


ANALYTICAL RESULTS

















Total PCB’s 08/17/07 19:5637 µg/Kg-dry 1A ND 2.4




Extended Range Organics 08/11/07 05:499.6 mg/Kg 1A ND 9.6

Surr: Decafluorobiphenyl 08/11/07 05:4950-150 %REC 1S 89.6 0



Barium 08/10/07 17:090.10 mg/Kg-dry 1A 20 0.019



Lead 08/10/07 17:090.38 mg/Kg-dry 1A 44 0.059






Acenaphthene 08/14/07 20:2056 µg/Kg-dry 1A ND 6.3

Acenaphthylene 08/14/07 20:2056 µg/Kg-dry 1A ND 6.1

Anthracene J 08/14/07 20:2056 µg/Kg-dry 1A 10 8.8

Benzo[a]anthracene 08/14/07 20:2056 µg/Kg-dry 1A 120 7.5





Page 12 of 48

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Page 13 of 48


ANALYTICAL RESULTS








Benzo[k]fluoranthene J 08/14/07 20:2056 µg/Kg-dry 1A 34 10


Dibenz[a,h]anthracene 08/14/07 20:2056 µg/Kg-dry 1A 79 8.3


Fluorene J 08/14/07 20:2056 µg/Kg-dry 1A 7.9 6.5

Indeno[1,2,3cd]pyrene 08/14/07 20:2056 µg/Kg-dry 1A 77 7.6


Phenanthrene 08/14/07 20:2056 µg/Kg-dry 1A 270 9.3

Pyrene 08/14/07 20:2056 µg/Kg-dry 1A 300 6.9




























Ethylbenzene 08/15/07 18:405.6 µg/Kg-dry 1A ND 0.79


Page 13 of 48

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Page 14 of 48


ANALYTICAL RESULTS
















Toluene 08/15/07 18:405.6 µg/Kg-dry 1A ND 0.79







m,p-Xylene J 08/15/07 18:405.6 µg/Kg-dry 1A 2.2 1.8

o-Xylene J 08/15/07 18:405.6 µg/Kg-dry 1A 1.5 1

Total Xylenes 08/15/07 18:405.6 µg/Kg-dry 1A ND 1






Gasoline Range Organics 08/15/07 18:40560 µg/Kg-dry 1A ND 280





Page 14 of 48

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Page 15 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 17:360.12 mg/Kg-dry 1A 8.7 0.024



Lead 08/10/07 17:360.47 mg/Kg-dry 1A 9.9 0.073








Anthracene 08/14/07 20:4663 µg/Kg-dry 1A ND 9.9

Benzo[a]anthracene 08/14/07 20:4663 µg/Kg-dry 1A ND 8.5

Benzo[a]pyrene J 08/14/07 20:4663 µg/Kg-dry 1A 25 9

Benzo[b]fluoranthene J 08/14/07 20:4663 µg/Kg-dry 1A 18 14

Benzo[g,h,i]perylene J 08/14/07 20:4663 µg/Kg-dry 1A 21 9


Page 15 of 48

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Page 16 of 48


ANALYTICAL RESULTS








Benzo[k]fluoranthene 08/14/07 20:4663 µg/Kg-dry 1A ND 12

Chrysene 08/14/07 20:4663 µg/Kg-dry 1A ND 7.8

Dibenz[a,h]anthracene 08/14/07 20:4663 µg/Kg-dry 1A ND 9.4

Fluoranthene 08/14/07 20:4663 µg/Kg-dry 1A ND 12

Fluorene 08/14/07 20:4663 µg/Kg-dry 1A ND 7.3

Indeno[1,2,3cd]pyrene 08/14/07 20:4663 µg/Kg-dry 1A ND 8.6

Naphthalene 08/14/07 20:4663 µg/Kg-dry 1A ND 6.7

Phenanthrene J 08/14/07 20:4663 µg/Kg-dry 1A 22 11

Pyrene J 08/14/07 20:4663 µg/Kg-dry 1A 44 7.7
















Chloroethane 08/16/07 00:0313 µg/Kg-dry 1A ND 3



Dibromochloromethane 08/16/07 00:036.3 µg/Kg-dry 1A ND 1




cis-1,2-Dichloroethene 08/16/07 00:036.3 µg/Kg-dry 1A ND 1



cis-1,3-Dichloropropene 08/16/07 00:036.3 µg/Kg-dry 1A ND 1


Ethylbenzene J 08/16/07 00:036.3 µg/Kg-dry 1A 1 0.89


Page 16 of 48

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Page 17 of 48


ANALYTICAL RESULTS








2-Hexanone 08/16/07 00:0313 µg/Kg-dry 1A ND 3




Styrene 08/16/07 00:036.3 µg/Kg-dry 1A ND 1



Tetrachloroethene 08/16/07 00:036.3 µg/Kg-dry 1A ND 2



1,1,2-Trichloroethane 08/16/07 00:036.3 µg/Kg-dry 1A ND 1





m,p-Xylene J 08/16/07 00:036.3 µg/Kg-dry 1A 2.4 2

o-Xylene 08/16/07 00:036.3 µg/Kg-dry 1A ND 1.1

Total Xylenes 08/16/07 00:036.3 µg/Kg-dry 1A ND 1.1





GASOLINE RANGE ORGANICS SW8260BMOD Analyst: JLNMethod: Prep Date/Time:






Page 17 of 48

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Page 18 of 48


ANALYTICAL RESULTS


















Surr: Tetrachloro-m-xylene 08/17/07 21:015-165 %REC 1S 100 0



Extended Range Organics 08/11/07 07:109.8 mg/Kg 1A 27 9.8




Barium 08/10/07 17:410.10 mg/Kg-dry 1A 9.9 0.02

Cadmium J 08/10/07 17:410.10 mg/Kg-dry 1A 0.062 0.0062


Lead 08/10/07 17:410.39 mg/Kg-dry 1A 17 0.061






Acenaphthene J 08/14/07 21:1153 µg/Kg-dry 1A 6.4 5.9




Benzo[a]pyrene 08/14/07 21:1153 µg/Kg-dry 1A 190 7.5


Benzo[g,h,i]perylene 08/14/07 21:1153 µg/Kg-dry 1A 330 7.5


Page 18 of 48

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Page 19 of 48


ANALYTICAL RESULTS








Benzo[k]fluoranthene J 08/14/07 21:1153 µg/Kg-dry 1A 51 9.9

Chrysene 08/14/07 21:1153 µg/Kg-dry 1A 600 6.6



Fluorene J 08/14/07 21:1153 µg/Kg-dry 1A 24 6.2


Naphthalene 08/14/07 21:1153 µg/Kg-dry 1A 58 5.6


Pyrene 08/14/07 21:1153 µg/Kg-dry 1A 630 6.5






























Page 19 of 48

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Page 20 of 48


ANALYTICAL RESULTS
























o-Xylene J 08/16/07 01:435.3 µg/Kg-dry 1A 4.8 0.95

Total Xylenes 08/16/07 01:435.3 µg/Kg-dry 1A 9.3 0.95











Page 20 of 48

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Page 21 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 17:470.12 mg/Kg-dry 1A 4.5 0.022



Lead 08/10/07 17:470.44 mg/Kg-dry 1A 2.2 0.069








Anthracene 08/14/07 21:3662 µg/Kg-dry 1A ND 9.6


Benzo[a]pyrene 08/14/07 21:3662 µg/Kg-dry 1A ND 8.8

Benzo[b]fluoranthene 08/14/07 21:3662 µg/Kg-dry 1A ND 14

Benzo[g,h,i]perylene J 08/14/07 21:3662 µg/Kg-dry 1A 9.5 8.8


Page 21 of 48

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Page 22 of 48


ANALYTICAL RESULTS









Chrysene J 08/14/07 21:3662 µg/Kg-dry 1A 30 7.7


Fluoranthene 08/14/07 21:3662 µg/Kg-dry 1A ND 12

Fluorene 08/14/07 21:3662 µg/Kg-dry 1A ND 7.2



Phenanthrene 08/14/07 21:3662 µg/Kg-dry 1A ND 10

Pyrene J 08/14/07 21:3662 µg/Kg-dry 1A 20 7.5






























Page 22 of 48

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Page 23 of 48


ANALYTICAL RESULTS















Tetrachloroethene 08/16/07 02:176.2 µg/Kg-dry 1A ND 2








m,p-Xylene J 08/16/07 02:176.2 µg/Kg-dry 1A 3.9 2













Page 23 of 48

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Page 24 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 17:520.10 mg/Kg-dry 1A 48 0.019



Lead 08/10/07 17:520.38 mg/Kg-dry 1A 130 0.06







Acenaphthylene 08/14/07 22:011400 µg/Kg-dry 10A 1600 150







Page 24 of 48

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Page 25 of 48


ANALYTICAL RESULTS
















Pyrene 08/15/07 02:096800 µg/Kg-dry 50A 110000 830

Surr: Nitrobenzene-d5 SI 08/14/07 22:0114.2-125 %REC 10S 149 0


Surr: Terphenyl-d14 SI 08/14/07 22:0110-139 %REC 10S 142 0


Acetone J 08/16/07 03:57570 µg/Kg-dry 10A 220 110



Benzene J 08/16/07 03:5757 µg/Kg-dry 10A 21 14

Bromodichloromethane 08/16/07 03:5757 µg/Kg-dry 10A ND 5.7

Bromoform 08/16/07 03:5757 µg/Kg-dry 10A ND 8




Carbon tetrachloride 08/16/07 03:5757 µg/Kg-dry 10A ND 14

Chlorobenzene 08/16/07 03:5757 µg/Kg-dry 10A ND 6.8


Chloroform 08/16/07 03:5757 µg/Kg-dry 10A ND 6.8

Chloromethane 08/16/07 03:57110 µg/Kg-dry 10A ND 17

Dibromochloromethane 08/16/07 03:5757 µg/Kg-dry 10A ND 9.1

1,1-Dichloroethane 08/16/07 03:5757 µg/Kg-dry 10A ND 8


1,1-Dichloroethene 08/16/07 03:5757 µg/Kg-dry 10A ND 14

cis-1,2-Dichloroethene 08/16/07 03:5757 µg/Kg-dry 10A ND 9.1

trans-1,2-Dichloroethene 08/16/07 03:5757 µg/Kg-dry 10A ND 11

1,2-Dichloropropane 08/16/07 03:5757 µg/Kg-dry 10A ND 11

cis-1,3-Dichloropropene 08/16/07 03:5757 µg/Kg-dry 10A ND 9.1

trans-1,3-Dichloropropene 08/16/07 03:5757 µg/Kg-dry 10A ND 8

Ethylbenzene J 08/16/07 03:5757 µg/Kg-dry 10A 55 8


Page 25 of 48

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Page 26 of 48


ANALYTICAL RESULTS










Methyl-t-Butyl Ether 08/16/07 03:5757 µg/Kg-dry 10A ND 6.8


Styrene 08/16/07 03:5757 µg/Kg-dry 10A ND 9.1


1,1,2,2-Tetrachloroethane 08/16/07 03:5757 µg/Kg-dry 10A ND 16

Tetrachloroethene 08/16/07 03:5757 µg/Kg-dry 10A ND 18

Toluene 08/16/07 03:5757 µg/Kg-dry 10A 180 8

1,1,1-Trichloroethane 08/16/07 03:5757 µg/Kg-dry 10A ND 11

1,1,2-Trichloroethane 08/16/07 03:5757 µg/Kg-dry 10A ND 9.1

Trichloroethene 08/16/07 03:5757 µg/Kg-dry 10A ND 10

Trichlorofluoromethane 08/16/07 03:57110 µg/Kg-dry 10A ND 39

Vinyl Acetate 08/16/07 03:57110 µg/Kg-dry 10A ND 17


m,p-Xylene 08/16/07 03:5757 µg/Kg-dry 10A 280 18

o-Xylene 08/16/07 03:5757 µg/Kg-dry 10A 350 10

Total Xylenes 08/16/07 03:5757 µg/Kg-dry 10A 630 10

Surr: 4-Bromofluorobenzene 08/16/07 03:5748.6-134 %REC 10S 103 0




GASOLINE RANGE ORGANICS SW8260BMOD Analyst: MLTMethod: Prep Date/Time:






Page 26 of 48

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Page 27 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 17:580.13 mg/Kg-dry 1A 20 0.025



Lead 08/10/07 17:580.50 mg/Kg-dry 1A 52 0.079














Page 27 of 48

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Page 28 of 48


ANALYTICAL RESULTS
















Pyrene 08/15/07 14:503300 µg/Kg-dry 50A 34000 410








Benzene 08/16/07 04:3167 µg/Kg-dry 10A ND 16


Bromoform 08/16/07 04:3167 µg/Kg-dry 10A ND 9.3





Chlorobenzene 08/16/07 04:3167 µg/Kg-dry 10A ND 8


Chloroform 08/16/07 04:3167 µg/Kg-dry 10A ND 8


Dibromochloromethane 08/16/07 04:3167 µg/Kg-dry 10A ND 11

1,1-Dichloroethane 08/16/07 04:3167 µg/Kg-dry 10A ND 9.3



cis-1,2-Dichloroethene 08/16/07 04:3167 µg/Kg-dry 10A ND 11



cis-1,3-Dichloropropene 08/16/07 04:3167 µg/Kg-dry 10A ND 11

trans-1,3-Dichloropropene 08/16/07 04:3167 µg/Kg-dry 10A ND 9.3

Ethylbenzene 08/16/07 04:3167 µg/Kg-dry 10A 81 9.3


Page 28 of 48

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Page 29 of 48


ANALYTICAL RESULTS










Methyl-t-Butyl Ether 08/16/07 04:3167 µg/Kg-dry 10A ND 8


Styrene 08/16/07 04:3167 µg/Kg-dry 10A ND 11




Toluene J 08/16/07 04:3167 µg/Kg-dry 10A 12 9.3












Surr: 1,2-Dichloroethane-d4 08/16/07 04:3168.6-148 %REC 10S 99.6 0








Page 29 of 48

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Page 30 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 18:030.16 mg/Kg-dry 1A 52 0.03


Chromium b 08/10/07 18:030.24 mg/Kg-dry 1A 6.2 0.028

Lead 08/10/07 18:030.59 mg/Kg-dry 1A 190 0.093














Page 30 of 48

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Page 31 of 48


ANALYTICAL RESULTS
















Pyrene 08/15/07 15:157900 µg/Kg-dry 100A 150000 970























cis-1,2-Dichloroethene 08/16/07 05:0479 µg/Kg-dry 10A ND 13





Ethylbenzene 08/16/07 05:0479 µg/Kg-dry 10A 220 11


Page 31 of 48

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Page 32 of 48


ANALYTICAL RESULTS


























Surr: 4-Bromofluorobenzene SI 08/16/07 05:0448.6-134 %REC 10S 174 0










Page 32 of 48

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Page 33 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 18:080.11 mg/Kg-dry 1A 4.8 0.021



Lead 08/10/07 18:080.42 mg/Kg-dry 1A 3.9 0.066














Page 33 of 48

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Page 34 of 48


ANALYTICAL RESULTS
















Pyrene 08/15/07 15:417100 µg/Kg-dry 100A 130000 870

Surr: Nitrobenzene-d5 SI 08/14/07 23:1514.2-125 %REC 10S 166 0


Surr: Terphenyl-d14 SI 08/14/07 23:1510-139 %REC 10S 252 0






Bromodichloromethane 08/16/07 05:3760 µg/Kg-dry 10A ND 6

Bromoform 08/16/07 05:3760 µg/Kg-dry 10A ND 8.3










1,1-Dichloroethane 08/16/07 05:3760 µg/Kg-dry 10A ND 8.3







trans-1,3-Dichloropropene 08/16/07 05:3760 µg/Kg-dry 10A ND 8.3

Ethylbenzene 08/16/07 05:3760 µg/Kg-dry 10A 210 8.3


Page 34 of 48

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Page 35 of 48


ANALYTICAL RESULTS
















Toluene J 08/16/07 05:3760 µg/Kg-dry 10A 46 8.3










Surr: 4-Bromofluorobenzene SI 08/16/07 05:3748.6-134 %REC 10S 255 0










Page 35 of 48

of 48

Page 36 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 18:140.11 mg/Kg-dry 1A 15 0.021



Lead 08/10/07 18:140.42 mg/Kg-dry 1A 17 0.067












Benzo[g,h,i]perylene 08/14/07 23:4058 µg/Kg-dry 1A 450 8.3


Page 36 of 48

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Page 37 of 48


ANALYTICAL RESULTS









Chrysene 08/14/07 23:4058 µg/Kg-dry 1A 530 7.2



Fluorene J 08/14/07 23:4058 µg/Kg-dry 1A 8.1 6.7


Naphthalene J 08/14/07 23:4058 µg/Kg-dry 1A 24 6.2


Pyrene 08/14/07 23:4058 µg/Kg-dry 1A 320 7.1






























Page 37 of 48

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Page 38 of 48


ANALYTICAL RESULTS
























o-Xylene 08/16/07 02:505.8 µg/Kg-dry 1A ND 1

Total Xylenes 08/16/07 02:505.8 µg/Kg-dry 1A ND 1











Page 38 of 48

of 48

Page 39 of 48


ANALYTICAL RESULTS

























Barium 08/10/07 18:190.14 mg/Kg-dry 1A 18 0.027



Lead 08/10/07 18:190.54 mg/Kg-dry 1A 18 0.085






Acenaphthene 08/15/07 00:0481 µg/Kg-dry 1A ND 9



Benzo[a]anthracene J 08/15/07 00:0481 µg/Kg-dry 1A 59 11

Benzo[a]pyrene J 08/15/07 00:0481 µg/Kg-dry 1A 27 11

Benzo[b]fluoranthene J 08/15/07 00:0481 µg/Kg-dry 1A 35 18

Benzo[g,h,i]perylene J 08/15/07 00:0481 µg/Kg-dry 1A 42 11


Page 39 of 48

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Page 40 of 48


ANALYTICAL RESULTS










Dibenz[a,h]anthracene 08/15/07 00:0481 µg/Kg-dry 1A ND 12

Fluoranthene J 08/15/07 00:0481 µg/Kg-dry 1A 35 15

Fluorene J 08/15/07 00:0481 µg/Kg-dry 1A 12 9.4

Indeno[1,2,3cd]pyrene J 08/15/07 00:0481 µg/Kg-dry 1A 13 11

Naphthalene J 08/15/07 00:0481 µg/Kg-dry 1A 9.1 8.5


Pyrene 08/15/07 00:0481 µg/Kg-dry 1A 130 9.8





Acetone 08/16/07 03:2481 µg/Kg-dry 1A 130 15

























Page 40 of 48

of 48

Page 41 of 48


ANALYTICAL RESULTS




































Page 41 of 48

of 48

Page 42 of 48


ANALYTICAL RESULTS

Client Project: NBD - Gary AirportClient Sample ID: DUP

Collection Date:Sample Matrix: Soil




Sample Description:Date Received: 08/08/07 16:30



















Barium 08/10/07 18:250.11 mg/Kg-dry 1A 20 0.021



Lead 08/10/07 18:250.41 mg/Kg-dry 1A 960 0.065














Page 42 of 48

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Page 43 of 48


ANALYTICAL RESULTS
















Pyrene 08/15/07 02:335700 µg/Kg-dry 50A 77000 690


Surr: 2-Fluorobiphenyl S 08/15/07 00:3021.6-112 %REC 10S 20.0 0




























Page 43 of 48

of 48

Page 44 of 48


ANALYTICAL RESULTS




























Surr: 1,2-Dichloroethane-d4 08/16/07 06:1168.6-148 %REC 10S 99.5 0








Page 44 of 48

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Page 45 of 48

FLAGS, FOOTNOTES AND ABBREVIATIONS (as needed)

NA N/A

ug/L

ug/Kg

U

J

B

D

ND

= =

=

=

=

=

=

=

=

mg/L

mg/Kg

=

=

Not Analyzed Not Applicable

Micrograms per Liter (ppb)

Micrograms per Kilogram (ppb)

Undetected

Analyte concentration detected between RL and MDL (Metals / Organics)

Detected in the associated Method Blank at a concentration above the routine PQL/RL

Surrogate recoveries are not calculated due to sample dilution

Not Detected at the Reporting Limit (or the Method Detection Limit, if listed)

Milligrams per Liter (ppm)

Milligrams per Kilogram (ppm)

QC SAMPLE IDENTIFICATIONS

MBLK

DUP

LCS

MS

ICB

ICV

PDS

ICSA=

=

=

=

=

=

=

=Method Blank

Method Duplicate

Laboratory Control Sample

Matrix Spike

Initial Calibration Blank

Initial Calibration Verification

Post Digestion Spike

Interference Check Standard "A"

ICSAB

LCSD

MSD

=

=

=

Interference Check Standard "AB"

Laboratory Control Sample Duplicate

Matrix Spike Duplicate

CCB

CCV

SD

=

=

=

Continuing Calibration Blank

Continuing Calibration Verification

Serial Dilution

E = Value above quantitation range

H = Analyte was prepared and/or analyzed outside of the analytical method holding time

I = Matrix Interference

R = RPD outside accepted recovery limits

S = Spike recovery outside recovery limits

SAMPLE TYPES

A = Analyte

I = Internal Standard

S = Surrogate

T = Tentatively Identified Compound (TIC, concentration estimated)

DF = Dilution Factor

Surr = Surrogate

cfu = Colony Forming Unit

ng/L = Nanograms per Liter (ppt)

CERTIFICATIONS

MICROBAC LOCATIONS, SERVICE CENTERS (SC) AND SATELLITE OFFICES (Sat)

Below is a list of certifications maintained by the Microbac Merrillville Laboratory. All data included in this report has been reviewed for and meets all project specific and quality control requirements of the applicable accreditation, unless otherwise noted. Complete lists of individual analytes pursuant to each certification below are available upon request.

- Illinois EPA for the analysis wastewater and solid waste in accordance with the requirements of the National Environmental Laboratory Accreditation Program [NELAP] (accreditation #100435)

- Indiana DEM approved support laboratory for solid waste and wastewater analyses

- Indiana SDH for the chemical analysis of drinking water (lab #C-45-02)

- Indiana SDH for the microbiological analysis of drinking water (lab #M-45-08)

- Kentucky EPPC for the analysis of samples applicable to the Underground Storage Tank program (lab #0061)

- North Carolina DENR for the environmental analysis for NPDES effluent, surface water, groundwater, and pretreatment regulations (certificate #597)

- Wisconsin DNR for the chemical analysis of wastewater and solid waste (lab #998036710)

RL = Reporting Limit ST = Sample Type MDL = Method Detection Limit

- Illinois Department of Public Health for the microbiological analysis of drinking water (registry #175458)

OPR = Ongoing Precision and Recovery Standard

b = Detected in the associated Method Blank at a concentration above the Method Detection Limit but less than the routine PQL/RL

Baltimore DivisionCamp Hill Division

Camp Hill Division (SC)Chicagoland Division

Chicagoland Division (SC)Corona Division

Erie DivisionFayetteville Division

Hauser Division

- Baltimore, MD - Camp Hill, PA - Pittston, PA - Merrillville, IN - Indianapolis, IN - Corona, CA - Erie, PA - Fayetteville, NC - Boulder, CO

Kentucky DivisionKentucky Division (Sat)Kentucky Division (Sat)Kentucky Division (Sat)

Knoxville DivisionMassachusetts Division

Microbac Corporate OfficeMicrobac NY - Cortland OfficeMicrobac NY - Waverly Office

- Louisville, KY - Evansville, IN - Lexington, KY - Paducah, KY - Maryville, TN - Marlborough, MA - Wexford, PA - Cortland, NY - Waverly, NY

New Castle DivisionPittsburgh DivisionRichmond Division

South Carolina DivisionSouth Jersey Division

Southern HeadquartersSouthern Testing Division

Southern Testing Division (Sat)Venice Division

- New Castle, PA - Warrendale, PA - Richmond, VA - New Ellenton, SC - Turnersville, NJ - Poquoson, VA - Wilson, NC - Greensboro, NC - Venice, FL


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Page 46 of 48

Client Name Quality Environmental Professi

Work Order Number ME0708349

Date / Time Received: 8/8/2007 4:30:00 PM

Received by: SPM

Checklist completed by Reviewed by

Carrier name: Microbac

Shipping container/cooler in good condition? Yes No Not PresentCustody seals intact on shippping container/cooler? Yes No Not Present

Custody seals intact on sample bottles? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Yes No

Container/Temp Blank temperatures

No VOA vials submitted Yes NoVOA vials for aqueous samples have zero headspace?

ANY "NO" EVALUATION (excluding After-Hour Receipt) REQUIRES CLIENT NOTIFICATION.

COOLER INSPECTION Monday, August 27, 2007

General Comments:Sample identified as DUP was not listed on the COC. Dhg8/9/07

Samples received on ice?

After-Hour Arrival? Yes No

Chain of custody included sufficient client identification? Yes No

Chain of custody included sufficient sample collector information? Yes No

Chain of custody included a sample description? Yes No

Chain of custody identified the appropriate matrix? Yes No

Chain of custody included date of collection? Yes No

Chain of custody included time of collection? Yes No

Chain of custody identified the appropriate number of containers? Yes No

Chain of custody identified the appropriate preservatives (if preserved)? Yes No

Samples properly preserved? Yes No

If No, adjusted by? Date/Time

Chain of custody included the requested analyses? Yes No

SPM 8/8/2007 5:46:11 PM DDG 8/9/2007 4:22:05 PM

Date:

Sample ID CommentsClient Sample ID

Cooler Temp1 1 ºC

ME0708349-01A REPORT IN DRY WEIGHT/ICOC REQUIREDB-1













ME0708349-14A REPORT IN DRY WEIGHT/ICOC REQUIREDDUP


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Page 47 of 48Page 47 of 48

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of 21

Page 1 of 21

August 22, 2007


Dear Nivas Vijay:RE: Gary Airport








Enclosures

Microbac Laboratories, Inc. received 5 samples on 8/10/2007 12:40:00 PM for the analyses presented in the following report.


of 21

Page 2 of 21

Project: Gary Airport




WORK ORDER SAMPLE SUMMARY Date: Wednesday, August 22, 2007

ME0708434-01A B-8 (0-2’) 8/9/2007 10:10:00 AM 8/10/2007

ME0708434-02A B-8 (2-4’) 8/9/2007 10:20:00 AM 8/10/2007

ME0708434-03A B-8 (8-10’) 8/9/2007 10:40:00 AM 8/10/2007

ME0708434-04A B-9 (0-2’) 8/9/2007 12:35:00 PM 8/10/2007

ME0708434-05A B-10 (0-2’) 8/9/2007 12:45:00 PM 8/10/2007


of 21

Page 3 of 21

Project: Gary Airport



CASE NARRATIVE Date: Wednesday, August 22, 2007

Volatile Organics Analysis:Sample ME0708434-03 was analyzed at a 1:50 dilution due to the large fuel like pattern in the chromatigram.


of 21

Page 4 of 21


ANALYTICAL RESULTS

Client Project: Gary AirportClient Sample ID: B-8 (0-2’)




Date: Wednesday, August 22, 2007
















Extended Range Organics 08/15/07 04:3212 mg/Kg-dry 1A ND 12




Barium b 08/15/07 18:000.12 mg/Kg-dry 1A 100 0.022


Chromium b 08/15/07 18:000.18 mg/Kg-dry 1A 410 0.021

Lead b 08/15/07 18:000.44 mg/Kg-dry 1A 60 0.069










Chrysene Jb 08/16/07 20:4359 µg/Kg-dry 1A 8.2 7.3


Indeno[1,2,3cd]pyrene 08/16/07 20:4359 µg/Kg-dry 1A ND 8


Page 4 of 21

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Page 5 of 21


ANALYTICAL RESULTS












VOLATILE ORGANICS SW8260B Analyst: MLTMethod: Prep Date/Time:









Carbon Disulfide J 08/17/07 13:4912 µg/Kg-dry 1A 2.4 2



















Methylene chloride J 08/17/07 13:4959 µg/Kg-dry 1A 33 10






Page 5 of 21

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Page 6 of 21


ANALYTICAL RESULTS








Toluene J 08/17/07 13:495.9 µg/Kg-dry 1A 1.3 0.82



Trichloroethene J 08/17/07 13:495.9 µg/Kg-dry 1A 3.6 1.1










Surr: Toluene-d8 08/17/07 13:4959.4-155 %REC 1S 98.5 0







Page 6 of 21

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Page 7 of 21


ANALYTICAL RESULTS





















Extended Range Organics 08/15/07 05:129.8 mg/Kg-dry 1A ND 9.8




Barium b 08/15/07 18:060.10 mg/Kg-dry 1A 6.9 0.02



Lead 08/16/07 13:460.39 mg/Kg-dry 1A 4.0 0.061









Benzo[k]fluoranthene 08/16/07 21:0852 µg/Kg-dry 1A ND 9.6

Chrysene Jb 08/16/07 21:0852 µg/Kg-dry 1A 7.6 6.4




Page 7 of 21

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Page 8 of 21


ANALYTICAL RESULTS













Acetone 08/17/07 14:2252 µg/Kg-dry 1A ND 9.9



Benzene J 08/17/07 14:225.2 µg/Kg-dry 1A 1.3 1.2
















trans-1,2-Dichloroethene 08/17/07 14:225.2 µg/Kg-dry 1A ND 1

1,2-Dichloropropane 08/17/07 14:225.2 µg/Kg-dry 1A ND 1













Page 8 of 21

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Page 9 of 21


ANALYTICAL RESULTS




























Page 9 of 21

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Page 10 of 21


ANALYTICAL RESULTS

















Total PCB’s 08/17/07 16:07210 µg/Kg-dry 1A ND 13





Surr: Decafluorobiphenyl SD 08/16/07 08:4250-150 %REC 20S 8.85 0






Lead 08/16/07 14:080.74 mg/Kg-dry 1A 5.9 0.12






Benzo[a]anthracene J 08/16/07 21:33640 µg/Kg-dry 1A 150 86

Benzo[a]pyrene 08/16/07 21:33640 µg/Kg-dry 1A ND 91



Chrysene J 08/16/07 21:33640 µg/Kg-dry 1A 160 79

Dibenz[a,h]anthracene 08/16/07 21:33640 µg/Kg-dry 1A ND 94



Page 10 of 21

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Page 11 of 21


ANALYTICAL RESULTS
















Benzene 08/17/07 16:21530 µg/Kg-dry 50A ND 130

Bromodichloromethane 08/17/07 16:21530 µg/Kg-dry 50A ND 53






Chlorobenzene 08/17/07 16:21530 µg/Kg-dry 50A ND 64


Chloroform 08/17/07 16:21530 µg/Kg-dry 50A ND 64






cis-1,2-Dichloroethene J 08/17/07 16:21530 µg/Kg-dry 50A 86 85








Methyl-t-Butyl Ether 08/17/07 16:21530 µg/Kg-dry 50A ND 64







Page 11 of 21

of 21

Page 12 of 21


ANALYTICAL RESULTS








Toluene 08/17/07 16:21530 µg/Kg-dry 50A ND 74







m,p-Xylene J 08/17/07 16:21530 µg/Kg-dry 50A 320 170

o-Xylene J 08/17/07 16:21530 µg/Kg-dry 50A 110 96

Total Xylenes 08/17/07 16:21530 µg/Kg-dry 50A ND 96











Page 12 of 21

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Page 13 of 21


ANALYTICAL RESULTS





















Extended Range Organics 08/16/07 06:4212 mg/Kg-dry 1A ND 12




Barium b 08/15/07 19:000.12 mg/Kg-dry 1A 4.8 0.023



Lead b 08/15/07 19:000.46 mg/Kg-dry 1A 6.4 0.072

Selenium J 08/15/07 19:001.8 mg/Kg-dry 1A 1 0.091





Benzo[a]anthracene J 08/16/07 21:5765 µg/Kg-dry 1A 12 8.7




Chrysene Jb 08/16/07 21:5765 µg/Kg-dry 1A 12 8.1




Page 13 of 21

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Page 14 of 21


ANALYTICAL RESULTS



























Dibromochloromethane 08/17/07 14:566.5 µg/Kg-dry 1A ND 1




cis-1,2-Dichloroethene 08/17/07 14:566.5 µg/Kg-dry 1A ND 1



cis-1,3-Dichloropropene 08/17/07 14:566.5 µg/Kg-dry 1A ND 1







Styrene 08/17/07 14:566.5 µg/Kg-dry 1A ND 1





Page 14 of 21

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Page 15 of 21


ANALYTICAL RESULTS




























Page 15 of 21

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Page 16 of 21


ANALYTICAL RESULTS




























Lead b 08/15/07 19:050.39 mg/Kg-dry 1A 22 0.062

Selenium 08/15/07 19:051.6 mg/Kg-dry 1A 9.2 0.078



Mercury 08/13/07 14:290.043 mg/Kg-dry 1A ND 0.00093





Benzo[k]fluoranthene 08/16/07 22:2253 µg/Kg-dry 1A 54 9.9

Chrysene b 08/16/07 22:2253 µg/Kg-dry 1A 180 6.6

Dibenz[a,h]anthracene J 08/16/07 22:2253 µg/Kg-dry 1A 26 7.9



Page 16 of 21

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Page 17 of 21


ANALYTICAL RESULTS








Naphthalene J 08/16/07 22:2253 µg/Kg-dry 1A 11 5.6
































Methylene chloride J 08/17/07 15:2953 µg/Kg-dry 1A 23 9.3






Page 17 of 21

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Page 18 of 21


ANALYTICAL RESULTS
















o-Xylene J 08/17/07 15:295.3 µg/Kg-dry 1A 2 0.96












Page 18 of 21

of 21

Page 19 of 21


NA N/A

ug/L

ug/Kg

U

J

B

D

ND

= =

=

=

=

=

=

=

=

mg/L

mg/Kg

=

=




Undetected








MBLK

DUP

LCS

MS

ICB

ICV

PDS

ICSA=

=

=

=

=

=

=

=Method Blank

Method Duplicate


Matrix Spike





ICSAB

LCSD

MSD

=

=

=




CCB

CCV

SD

=

=

=



Serial Dilution






SAMPLE TYPES

A = Analyte


S = Surrogate



Surr = Surrogate



CERTIFICATIONS


















Hauser Division












of 21

Page 20 of 21

Client Name QEPI



Received by: SPM


Carrier name: Microbac










Yes No




COOLER INSPECTION Wednesday, August 22, 2007

General Comments:














SPM 8/10/2007 12:49:18 PM DDG 8/13/2007 10:46:12 AM

Date:


Cooler Temp1 2 ºC

ME0708434-01A REPORT IN DRY WEIGHTB-8 (0-2')






of 21


of 27

Page 1 of 27

September 10, 2007


Dear Nivas Vijay:RE: NBD Trust

Work Order No.: ME0708B071611 S. Franklin RoadIndianapolis, IN 46239







Enclosures

Microbac Laboratories, Inc. received 7 samples on 8/27/2007 10:00:00 AM for the analyses presented in the following report.


of 27

Page 2 of 27

Project: NBD Trust


Lab Order: ME0708B07


WORK ORDER SAMPLE SUMMARY Date: Monday, September 10, 2007

ME0708B07-01A MW-1 8/26/2007 12:40:00 PM 8/27/2007

ME0708B07-01B MW-1 8/26/2007 12:40:00 PM 8/27/2007

ME0708B07-01C MW-1 8/26/2007 12:40:00 PM 8/27/2007

ME0708B07-02A MW-2 8/26/2007 9:39:00 AM 8/27/2007

ME0708B07-02B MW-2 8/26/2007 9:39:00 AM 8/27/2007

ME0708B07-02C MW-2 8/26/2007 9:39:00 AM 8/27/2007

ME0708B07-03A MW-3 8/26/2007 2:16:00 PM 8/27/2007

ME0708B07-03B MW-3 8/26/2007 2:16:00 PM 8/27/2007

ME0708B07-03C MW-3 8/26/2007 2:16:00 PM 8/27/2007

ME0708B07-04A MW-4 8/26/2007 11:53:00 AM 8/27/2007

ME0708B07-04B MW-4 8/26/2007 11:53:00 AM 8/27/2007

ME0708B07-04C MW-4 8/26/2007 11:53:00 AM 8/27/2007

ME0708B07-05A MW-5 8/26/2007 11:11:00 AM 8/27/2007

ME0708B07-05B MW-5 8/26/2007 11:11:00 AM 8/27/2007

ME0708B07-05C MW-5 8/26/2007 11:11:00 AM 8/27/2007

ME0708B07-06A MW-6 8/26/2007 1:25:00 PM 8/27/2007

ME0708B07-06B MW-6 8/26/2007 1:25:00 PM 8/27/2007

ME0708B07-06C MW-6 8/26/2007 1:25:00 PM 8/27/2007

ME0708B07-07A Duplicate 8/27/2007

ME0708B07-07B Duplicate 8/27/2007

ME0708B07-07C Duplicate 8/27/2007


of 27

Page 3 of 27

Project: NBD Trust


Lab Order: ME0708B07

CASE NARRATIVE Date: Monday, September 10, 2007

Volatile Organics Analysis:The ’J’ flagged concentration of Cis-1,2-Dichloroethene in sample ME0708B07-06, may be due to carryover.


of 27

Page 4 of 27


ANALYTICAL RESULTS

Client Project: NBD TrustClient Sample ID: MW-1

Collection Date: 08/26/07 12:40Sample Matrix: Aqueous


Work Order / ID: ME0708B07-01

Date: Monday, September 10, 2007



Extended Range Organics 09/01/07 01:4391 µg/L 1A 6600 91



Arsenic Jb 08/31/07 08:460.010 mg/L 1A 0.0027 0.0025

Barium 08/31/07 08:460.0020 mg/L 1A 0.056 0.0003

Cadmium 08/31/07 08:460.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 08:460.0030 mg/L 1A 0.002 0.0006

Lead 08/31/07 08:460.0075 mg/L 1A ND 0.0025

Selenium 08/31/07 08:460.030 mg/L 1A ND 0.0053

Silver 08/31/07 08:460.010 mg/L 1A ND 0.0013

TOTAL METALS SW7470A Analyst: SAAMethod: Prep Date/Time: 08/28/07 07:25

Mercury 08/28/07 11:060.00020 mg/L 1A ND 0.000043


Acenaphthene J 09/07/07 19:481.0 µg/L 1A 0.58 0.15

Acenaphthylene 09/07/07 19:481.0 µg/L 1A ND 0.18

Anthracene 09/07/07 19:481.0 µg/L 1A ND 0.16

Benzo[a]anthracene 09/07/07 19:481.0 µg/L 1A ND 0.21

Benzo[a]pyrene 09/07/07 19:481.0 µg/L 1A ND 0.35

Benzo[b]fluoranthene 09/07/07 19:481.0 µg/L 1A ND 0.25

Benzo[g,h,i]perylene 09/07/07 19:481.0 µg/L 1A ND 0.22

Benzo[k]fluoranthene 09/07/07 19:481.0 µg/L 1A ND 0.25

Chrysene 09/07/07 19:481.0 µg/L 1A ND 0.19

Dibenz[a,h]anthracene 09/07/07 19:481.0 µg/L 1A ND 0.21

Fluoranthene 09/07/07 19:481.0 µg/L 1A ND 0.18

Fluorene J 09/07/07 19:481.0 µg/L 1A 0.42 0.15

Indeno[1,2,3cd]pyrene 09/07/07 19:481.0 µg/L 1A ND 0.21

Naphthalene J 09/07/07 19:481.0 µg/L 1A 0.23 0.12

Phenanthrene 09/07/07 19:481.0 µg/L 1A ND 0.18

Pyrene J 09/07/07 19:481.0 µg/L 1A 0.34 0.15

Surr: Decafluorobiphenyl 09/07/07 19:4813.8-106 %REC 1S 41.3 0

VOLATILE ORGANICS SW8260B Analyst: BRRMethod: Prep Date/Time:

Acetone J 09/03/07 14:0450 µg/L 1A 6.9 5.8

Acrolein 09/03/07 14:04100 µg/L 1A ND 16


Page 4 of 27

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Page 5 of 27


ANALYTICAL RESULTS








Acrylonitrile 09/03/07 14:04100 µg/L 1A ND 13

Benzene J 09/03/07 14:045.0 µg/L 1A 0.93 0.8

Bromodichloromethane 09/03/07 14:045.0 µg/L 1A ND 0.7

Bromoform 09/03/07 14:045.0 µg/L 1A ND 0.8

Bromomethane 09/03/07 14:0410 µg/L 1A ND 1.8

2-Butanone 09/03/07 14:0410 µg/L 1A ND 3.6

Carbon Disulfide 09/03/07 14:0410 µg/L 1A ND 1.7

Carbon tetrachloride 09/03/07 14:045.0 µg/L 1A ND 1.7

Chlorobenzene 09/03/07 14:045.0 µg/L 1A ND 0.8

Chloroethane 09/03/07 14:0410 µg/L 1A ND 2.3

Chloroform 09/03/07 14:045.0 µg/L 1A ND 0.9

Chloromethane J 09/03/07 14:0410 µg/L 1A 1.8 1

Dibromochloromethane 09/03/07 14:045.0 µg/L 1A ND 0.8

1,1-Dichloroethane 09/03/07 14:045.0 µg/L 1A ND 0.8


1,1-Dichloroethene 09/03/07 14:045.0 µg/L 1A ND 1.7

cis-1,2-Dichloroethene 09/03/07 14:045.0 µg/L 1A ND 0.8

trans-1,2-Dichloroethene 09/03/07 14:045.0 µg/L 1A ND 1.1

1,2-Dichloropropane 09/03/07 14:045.0 µg/L 1A ND 1

cis-1,3-Dichloropropene 09/03/07 14:045.0 µg/L 1A ND 0.8

trans-1,3-Dichloropropene 09/03/07 14:045.0 µg/L 1A ND 0.7

Ethylbenzene 09/03/07 14:045.0 µg/L 1A ND 0.9

2-Hexanone 09/03/07 14:0410 µg/L 1A ND 2.4

4-Methyl-2-Pentanone 09/03/07 14:0410 µg/L 1A ND 1.7

Methyl-t-Butyl Ether 09/03/07 14:045.0 µg/L 1A ND 0.8

Methylene chloride 09/03/07 14:0410 µg/L 1A ND 3.1

Styrene 09/03/07 14:045.0 µg/L 1A ND 0.7

1,1,1,2-Tetrachloroethane 09/03/07 14:0410 µg/L 1A ND 1.1

1,1,2,2-Tetrachloroethane 09/03/07 14:045.0 µg/L 1A ND 1.4

Tetrachloroethene 09/03/07 14:045.0 µg/L 1A ND 1.3

Toluene J 09/03/07 14:045.0 µg/L 1A 1.1 0.9

1,1,1-Trichloroethane 09/03/07 14:045.0 µg/L 1A ND 0.9


Trichloroethene 09/03/07 14:045.0 µg/L 1A ND 0.9

Vinyl Acetate 09/03/07 14:0410 µg/L 1A ND 1.5

Vinyl chloride 09/03/07 14:0410 µg/L 1A ND 0.9

m,p-Xylene 09/03/07 14:045.0 µg/L 1A ND 1.7

o-Xylene J 09/03/07 14:045.0 µg/L 1A 0.92 0.9

Trichlorofluoromethane 09/03/07 14:0410 µg/L 1A ND 1.1


Page 5 of 27

of 27

Page 6 of 27


ANALYTICAL RESULTS








Total Xylenes 09/03/07 14:045.0 µg/L 1A ND 0.9



Surr: Dibromofluoromethane 09/03/07 14:0480.2-126 %REC 1S 112 0



Page 6 of 27

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Page 7 of 27


ANALYTICAL RESULTS











Arsenic 08/31/07 08:510.010 mg/L 1A ND 0.0025

Barium 08/31/07 08:510.0020 mg/L 1A 0.013 0.0003

Cadmium 08/31/07 08:510.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 08:510.0030 mg/L 1A 0.0019 0.0006

Lead Jb 08/31/07 12:580.0075 mg/L 1A 0.0031 0.0025

Selenium 08/31/07 08:510.030 mg/L 1A ND 0.0053

Silver 08/31/07 08:510.010 mg/L 1A ND 0.0013


Mercury 08/28/07 11:070.00020 mg/L 1A ND 0.000043


Acenaphthene 09/07/07 20:141.0 µg/L 1A ND 0.15








Chrysene 09/07/07 20:141.0 µg/L 1A ND 0.19



Fluorene 09/07/07 20:141.0 µg/L 1A ND 0.15


Naphthalene 09/07/07 20:141.0 µg/L 1A ND 0.12


Pyrene 09/07/07 20:141.0 µg/L 1A ND 0.15



Acetone 09/03/07 14:4150 µg/L 1A ND 5.8

Acrolein 09/03/07 14:41100 µg/L 1A ND 16


Page 7 of 27

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Page 8 of 27


ANALYTICAL RESULTS









Benzene 09/03/07 14:415.0 µg/L 1A ND 0.8




2-Butanone 09/03/07 14:4110 µg/L 1A ND 3.6






Chloromethane 09/03/07 14:4110 µg/L 1A ND 1











2-Hexanone 09/03/07 14:4110 µg/L 1A ND 2.4




Styrene 09/03/07 14:415.0 µg/L 1A ND 0.7




Toluene 09/03/07 14:415.0 µg/L 1A ND 0.9






m,p-Xylene 09/03/07 14:415.0 µg/L 1A ND 1.7

o-Xylene 09/03/07 14:415.0 µg/L 1A ND 0.9



Page 8 of 27

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Page 9 of 27


ANALYTICAL RESULTS














Page 9 of 27

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Page 10 of 27


ANALYTICAL RESULTS











Arsenic b 08/31/07 08:560.010 mg/L 1A 0.018 0.0025

Barium 08/31/07 08:560.0020 mg/L 1A 0.029 0.0003

Cadmium 08/31/07 08:560.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 08:560.0030 mg/L 1A 0.0021 0.0006

Lead b 08/31/07 08:560.0075 mg/L 1A 0.040 0.0025

Selenium 08/31/07 08:560.030 mg/L 1A ND 0.0053

Silver J 08/31/07 08:560.010 mg/L 1A 0.0026 0.0013


Mercury 08/28/07 11:080.00020 mg/L 1A ND 0.000043




Anthracene J 09/07/07 21:301.0 µg/L 1A 0.88 0.16

Benzo[a]anthracene 09/07/07 21:301.0 µg/L 1A 1.3 0.21

Benzo[a]pyrene J 09/07/07 21:301.0 µg/L 1A 0.57 0.35

Benzo[b]fluoranthene J 09/07/07 21:301.0 µg/L 1A 0.84 0.25

Benzo[g,h,i]perylene J 09/07/07 21:301.0 µg/L 1A 0.58 0.22


Chrysene 09/07/07 21:301.0 µg/L 1A 1.7 0.19


Fluoranthene 09/07/07 21:301.0 µg/L 1A 1.9 0.18

Fluorene 09/07/07 21:301.0 µg/L 1A 4.0 0.15



Phenanthrene 09/07/07 21:301.0 µg/L 1A 41 0.18

Pyrene 09/07/07 21:301.0 µg/L 1A 4.1 0.15



Acetone 09/03/07 15:1750 µg/L 1A ND 5.8

Acrolein 09/03/07 15:17100 µg/L 1A ND 16


Page 10 of 27

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Page 11 of 27


ANALYTICAL RESULTS









Benzene J 09/03/07 15:175.0 µg/L 1A 2 0.8




2-Butanone 09/03/07 15:1710 µg/L 1A ND 3.6
















Ethylbenzene J 09/03/07 15:175.0 µg/L 1A 1.9 0.9

2-Hexanone 09/03/07 15:1710 µg/L 1A ND 2.4




Styrene 09/03/07 15:175.0 µg/L 1A ND 0.7




Toluene J 09/03/07 15:175.0 µg/L 1A 1.2 0.9






m,p-Xylene J 09/03/07 15:175.0 µg/L 1A 3.1 1.7

o-Xylene J 09/03/07 15:175.0 µg/L 1A 1.1 0.9



Page 11 of 27

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Page 12 of 27


ANALYTICAL RESULTS














Page 12 of 27

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ANALYTICAL RESULTS








Extended Range Organics 09/01/07 05:03100 µg/L 1A ND 100



Arsenic 08/31/07 09:020.010 mg/L 1A ND 0.0025

Barium 08/31/07 09:020.0020 mg/L 1A 0.066 0.0003

Cadmium 08/31/07 09:020.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 09:020.0030 mg/L 1A 0.0016 0.0006

Lead 08/31/07 09:020.0075 mg/L 1A ND 0.0025

Selenium 08/31/07 09:020.030 mg/L 1A ND 0.0053

Silver 08/31/07 09:020.010 mg/L 1A ND 0.0013


Mercury 08/28/07 11:100.00020 mg/L 1A ND 0.000043










Chrysene 09/07/07 20:391.0 µg/L 1A ND 0.19



Fluorene 09/07/07 20:391.0 µg/L 1A ND 0.15


Naphthalene 09/07/07 20:391.0 µg/L 1A ND 0.12


Pyrene 09/07/07 20:391.0 µg/L 1A ND 0.15



Acetone 09/03/07 15:5450 µg/L 1A ND 5.8

Acrolein 09/03/07 15:54100 µg/L 1A ND 16


Page 13 of 27

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Page 14 of 27


ANALYTICAL RESULTS









Benzene 09/03/07 15:545.0 µg/L 1A ND 0.8




2-Butanone 09/03/07 15:5410 µg/L 1A ND 3.6

















2-Hexanone 09/03/07 15:5410 µg/L 1A ND 2.4




Styrene 09/03/07 15:545.0 µg/L 1A ND 0.7




Toluene 09/03/07 15:545.0 µg/L 1A ND 0.9






m,p-Xylene 09/03/07 15:545.0 µg/L 1A ND 1.7

o-Xylene 09/03/07 15:545.0 µg/L 1A ND 0.9



Page 14 of 27

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Page 15 of 27


ANALYTICAL RESULTS














Page 15 of 27

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Page 16 of 27


ANALYTICAL RESULTS











Arsenic Jb 08/31/07 09:230.010 mg/L 1A 0.0066 0.0025

Barium 08/31/07 09:230.0020 mg/L 1A 0.038 0.0003

Cadmium 08/31/07 09:230.0020 mg/L 1A ND 0.0003

Chromium 08/31/07 09:230.0030 mg/L 1A 0.11 0.0006

Lead 08/31/07 13:030.0075 mg/L 1A ND 0.0025

Selenium 08/31/07 09:230.030 mg/L 1A ND 0.0053

Silver 08/31/07 09:230.010 mg/L 1A ND 0.0013


Mercury 08/28/07 11:110.00020 mg/L 1A ND 0.000043










Chrysene 09/07/07 21:051.0 µg/L 1A ND 0.19



Fluorene 09/07/07 21:051.0 µg/L 1A ND 0.15




Pyrene 09/07/07 21:051.0 µg/L 1A ND 0.15



Acetone J 09/03/07 16:3050 µg/L 1A 15 5.8

Acrolein 09/03/07 16:30100 µg/L 1A ND 16


Page 16 of 27

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Page 17 of 27


ANALYTICAL RESULTS









Benzene 09/03/07 16:305.0 µg/L 1A 6.1 0.8




2-Butanone 09/03/07 16:3010 µg/L 1A ND 3.6




Chloroethane J 09/03/07 16:3010 µg/L 1A 2.8 2.3


Chloromethane 09/03/07 16:3010 µg/L 1A ND 1


1,1-Dichloroethane 09/03/07 16:305.0 µg/L 1A 80 0.8

1,2-Dichloroethane J 09/03/07 16:305.0 µg/L 1A 4.4 1.2


cis-1,2-Dichloroethene 09/04/07 12:2350 µg/L 10A 310 8

trans-1,2-Dichloroethene J 09/03/07 16:305.0 µg/L 1A 3.1 1.1





2-Hexanone 09/03/07 16:3010 µg/L 1A ND 2.4




Styrene 09/03/07 16:305.0 µg/L 1A ND 0.7




Toluene 09/03/07 16:305.0 µg/L 1A ND 0.9

1,1,1-Trichloroethane J 09/03/07 16:305.0 µg/L 1A 1.3 0.9


Trichloroethene 09/03/07 16:305.0 µg/L 1A 10 0.9


Vinyl chloride 09/03/07 16:3010 µg/L 1A 20 0.9

m,p-Xylene J 09/03/07 16:305.0 µg/L 1A 2.3 1.7

o-Xylene 09/03/07 16:305.0 µg/L 1A ND 0.9



Page 17 of 27

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Page 18 of 27


ANALYTICAL RESULTS














Page 18 of 27

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Page 19 of 27


ANALYTICAL RESULTS








Arsenic Jb 08/31/07 09:280.010 mg/L 1A 0.003 0.0025

Barium 08/31/07 09:280.0020 mg/L 1A 0.073 0.0003

Cadmium 08/31/07 09:280.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 09:280.0030 mg/L 1A 0.0024 0.0006

Lead 08/31/07 11:480.0075 mg/L 1A ND 0.0025

Selenium 08/31/07 09:280.030 mg/L 1A ND 0.0053

Silver 08/31/07 09:280.010 mg/L 1A ND 0.0013


Mercury 08/28/07 11:150.00020 mg/L 1A ND 0.000043


Acetone 09/03/07 17:0750 µg/L 1A ND 5.8

Acrolein 09/03/07 17:07100 µg/L 1A ND 16


Benzene 09/03/07 17:075.0 µg/L 1A ND 0.8




2-Butanone 09/03/07 17:0710 µg/L 1A ND 3.6











cis-1,2-Dichloroethene J 09/03/07 17:075.0 µg/L 1A 0.87 0.8






2-Hexanone 09/03/07 17:0710 µg/L 1A ND 2.4



Page 19 of 27

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Page 20 of 27


ANALYTICAL RESULTS










Styrene 09/03/07 17:075.0 µg/L 1A ND 0.7




Toluene 09/03/07 17:075.0 µg/L 1A ND 0.9






m,p-Xylene 09/03/07 17:075.0 µg/L 1A ND 1.7

o-Xylene 09/03/07 17:075.0 µg/L 1A ND 0.9








Page 20 of 27

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Page 21 of 27


ANALYTICAL RESULTS

Client Project: NBD TrustClient Sample ID: Duplicate

Collection Date:Sample Matrix: Aqueous









Arsenic b 08/31/07 09:340.010 mg/L 1A 0.011 0.0025

Barium 08/31/07 09:340.0020 mg/L 1A 0.030 0.0003

Cadmium 08/31/07 09:340.0020 mg/L 1A ND 0.0003

Chromium J 08/31/07 09:340.0030 mg/L 1A 0.0017 0.0006

Lead b 08/31/07 09:340.0075 mg/L 1A 0.034 0.0025

Selenium 08/31/07 09:340.030 mg/L 1A ND 0.0053

Silver 08/31/07 09:340.010 mg/L 1A ND 0.0013


Mercury Jb 08/28/07 11:170.00020 mg/L 1A 0.000058 0.000043




Anthracene J 09/07/07 21:551.0 µg/L 1A 0.84 0.16

Benzo[a]anthracene 09/07/07 21:551.0 µg/L 1A 1.6 0.21


Benzo[b]fluoranthene 09/07/07 21:551.0 µg/L 1A 1.1 0.25

Benzo[g,h,i]perylene J 09/07/07 21:551.0 µg/L 1A 0.75 0.22


Chrysene 09/07/07 21:551.0 µg/L 1A 2.7 0.19

Dibenz[a,h]anthracene J 09/07/07 21:551.0 µg/L 1A 0.23 0.21

Fluoranthene 09/07/07 21:551.0 µg/L 1A 2.2 0.18

Fluorene 09/07/07 21:551.0 µg/L 1A 3.7 0.15

Indeno[1,2,3cd]pyrene J 09/07/07 21:551.0 µg/L 1A 0.23 0.21


Phenanthrene 09/07/07 21:551.0 µg/L 1A 32 0.18

Pyrene 09/07/07 21:551.0 µg/L 1A 5.7 0.15



Acetone 09/03/07 17:4350 µg/L 1A ND 5.8

Acrolein 09/03/07 17:43100 µg/L 1A ND 16


Page 21 of 27

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ANALYTICAL RESULTS









Benzene J 09/03/07 17:435.0 µg/L 1A 1.9 0.8




2-Butanone 09/03/07 17:4310 µg/L 1A ND 3.6

















2-Hexanone 09/03/07 17:4310 µg/L 1A ND 2.4




Styrene 09/03/07 17:435.0 µg/L 1A ND 0.7




Toluene J 09/03/07 17:435.0 µg/L 1A 1 0.9






m,p-Xylene J 09/03/07 17:435.0 µg/L 1A 2.8 1.7

o-Xylene J 09/03/07 17:435.0 µg/L 1A 1.3 0.9



Page 22 of 27

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Page 23 of 27


ANALYTICAL RESULTS














Page 23 of 27

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Page 24 of 27


NA N/A

ug/L

ug/Kg

U

J

B

D

ND

= =

=

=

=

=

=

=

=

mg/L

mg/Kg

=

=




Undetected








MBLK

DUP

LCS

MS

ICB

ICV

PDS

ICSA=

=

=

=

=

=

=

=Method Blank

Method Duplicate


Matrix Spike





ICSAB

LCSD

MSD

=

=

=




CCB

CCV

SD

=

=

=



Serial Dilution






SAMPLE TYPES

A = Analyte


S = Surrogate



Surr = Surrogate



CERTIFICATIONS


















Hauser Division












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Page 25 of 27


Work Order Number ME0708B07

Date / Time Received: 8/27/2007 10:00:00 AM

Received by: KRS


Carrier name: Client Delivered










Yes No




COOLER INSPECTION Monday, September 10, 2007

General Comments:














DPP 8/27/2007 11:24:49 AM DDG 8/29/2007 7:29:57 AM

Date:


Cooler Temp1 3 ºC

ME0708B07-01A MW-1

ME0708B07-01B MW-1

ME0708B07-01C MW-1

ME0708B07-02A MW-2

ME0708B07-02B MW-2

ME0708B07-02C MW-2

ME0708B07-03A MW-3

ME0708B07-03B MW-3

ME0708B07-03C MW-3

ME0708B07-04A MW-4

ME0708B07-04B MW-4

ME0708B07-04C MW-4

ME0708B07-05A MW-5

ME0708B07-05B MW-5


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Page 26 of 27


ME0708B07-05C MW-5

ME0708B07-06A MW-6

ME0708B07-06B MW-6

ME0708B07-06C MW-6

ME0708B07-07A Duplicate

ME0708B07-07B Duplicate

ME0708B07-07C Duplicate


of 27


of 6

Page 1 of 6

September 21, 2007


Dear Nivas Vijay:RE: NBD/07-05-024








Enclosures

Microbac Laboratories, Inc. received 1 sample on 9/19/2007 2:45:00 PM for the analyses presented in the following report.


of 6

Page 2 of 6

Project: NBD/07-05-024




WORK ORDER SAMPLE SUMMARY Date: Friday, September 21, 2007

ME0709763-01A MW-6 9/19/2007 12:35:00 PM 9/19/2007


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Page 3 of 6


ANALYTICAL RESULTS

Client Project: NBD/07-05-024Client Sample ID: MW-6




Date: Friday, September 21, 2007









Benzo[a]anthracene J 09/19/07 20:250.99 µg/L 1A 0.27 0.21


Benzo[b]fluoranthene J 09/19/07 20:250.99 µg/L 1A 0.56 0.25

Benzo[g,h,i]perylene b 09/19/07 20:250.99 µg/L 1A 1.1 0.22


Chrysene 09/19/07 20:250.99 µg/L 1A ND 0.19

Dibenz[a,h]anthracene Jb 09/19/07 20:250.99 µg/L 1A 0.8 0.21


Fluorene 09/19/07 20:250.99 µg/L 1A ND 0.15

Indeno[1,2,3cd]pyrene J 09/19/07 20:250.99 µg/L 1A 0.92 0.21

Naphthalene 09/19/07 20:250.99 µg/L 1A 1.2 0.12


Pyrene 09/19/07 20:250.99 µg/L 1A ND 0.15

Surr: Nitrobenzene-d5 09/19/07 20:2510-121 %REC 1S 66.0 0




Page 3 of 6

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Page 4 of 6


NA N/A

ug/L

ug/Kg

U

J

B

D

ND

= =

=

=

=

=

=

=

=

mg/L

mg/Kg

=

=




Undetected








MBLK

DUP

LCS

MS

ICB

ICV

PDS

ICSA=

=

=

=

=

=

=

=Method Blank

Method Duplicate


Matrix Spike





ICSAB

LCSD

MSD

=

=

=




CCB

CCV

SD

=

=

=



Serial Dilution






SAMPLE TYPES

A = Analyte


S = Surrogate



Surr = Surrogate



CERTIFICATIONS


















Hauser Division












of 6

Page 5 of 6




Received by: DPP


Carrier name: Client Delivered










Yes No




COOLER INSPECTION Friday, September 21, 2007

General Comments:














DPP 9/19/2007 3:21:58 PM DDG 9/20/2007 8:16:25 AM

Date:


Cooler Temp1 3 ºC

ME0709763-01A MW-6


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site assessment report phase ii...chemical impacts exceeding idem risc idcls from 0 to 2 feet bgs...

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