remediation general permit notice of intent: proposed ... · 980 harrison avenue . boston , ma...
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Geotechnical Engineers 3' 20
US Environmental Protection Agency RGP - NOC Processing Municipal Assistance Unit One Congress Street, Suite 1100 Boston , MA 02114
Attention: Mr. Victor Alvarez
Boston Water and Sewer Commission 980 Harrison Avenue Boston , MA 02119
Attention: Mr. Francis M. McLaughlin
Reference: Proposed Boston Renaissance Charter Public School 1415 Hyde Park Avenue; Hyde Park , Massachusetts Temporary Construction Dewatering Discharge Permit Application Under Massachusetts General Permit No. MAG910000
This letter report was prepared by McPhail Associates , Inc. on behalf of Boston Renaissance Charter Public School in support of an application for permission from the US Environmental Protection Agency (EPA) and the Boston Water and Sewer Commission (BWSC) for the temporary discharge of groundwater into storm drain lines which outfall into Mother Brook and ultimately into the Neponset River , for the purpose of construction dewatering at the above referenced location. Refer to 1 for the generalFigure
site locus.
These services were performed and this permit application was prepared in accordance with our proposal dated March 24, 2009 and the subsequent authorization of Boston Renaissance Charter Public School.
Appendix A.These services are subject to the limitations contained in
The required US EPA Notice of Intent (NOI) and the BWSC Dewatering Discharge Permit Application are Appendix B.included in
APPLICANT
Boston Renaissance Charter Public School 250 Stuart Street Boston , MA 02116
Contact: Mr. Kevin D. Cherry, Chief Financial Offcer Telephone: 617-357-0900 x1212
EXISTING SITE CONDITIONS
Fronting onto Hyde Park Avenue to the east , the subject site is bounded by railroad tracks to the west , the Mother Brook to the north , and Dacy Street to the south. The site is presently occupied by a three-story
2269 Massachusetts Avenue
Cambridge , Massachusetts 02140
6171868. 1420
617/868. 1423 (Fax)
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brick former mill structure which occupies an approximate 20, 376 square-foot plan area , a one-story warehouse structure which occupies an approximate 21 371 square-foot plan area , and a shed occupying approximately 1 500 square-foot plan area.
2. The ground surface across the site consists of bituminousFigureExisting site conditions are shown in
concrete paved areas and gravel surfaces. Areas in the north and south portions of the property appear to be vegetated with brush or trees. In general , existing ground surface across the site slopes gradually downward from south to north from about Elevation +56 along the southern end of the site to about Elevation +49 along the northern end of the site. Elevations as indicated herein refer to the Boston City Base (BCB) datum which is 5.65 feet below the National Geodetic Vertical Datum (NGVD).
SITE ENVIRONMENTAL SETTING
The site is located in a mixed commercial and residential area along Hyde Park Avenue. A multi-unit residential building abuts the site to the northeast. Mother Brook , a Class B surface water, is located to the north of the site. Based on the DEP site scoring map, a 1 OO-year flood plain and open water associated with Mother Brook are located to the north of the site. Protected open space and open water associated with the Neponset River, a Class B Surface Water, are located approximately 500 feet to the east of the site. No other sensitive environmental receptors have been identified on the site. Information contained in the current Massachusetts DEP Priority Resources Map for Boston indicates that the site is not located within a Zone II of a public water supply, an Interim Wellhead Protection Area, a Potentially Productive Aquifer or a Zone A of a Class A surface water supply reservoir.
The subject site and the surrounding area are serviced by public utilities including water , electricity, surface drainage and sanitary sewer.
Polynuclear aromatic hydrocarbons (PAHs), petroleum-related hydrocarbons , metals , and volatie organic compounds (VOCs) at concentrations that require notification of the DEP were detected in the site soil and groundwater during performance of several environmental investigations that were completed at the site. Response actions will be performed pursuant to relevant provisions contained in the Massachusetts Contingency Plan (MCP), 310 CMR 40.0000. Further details regarding the results of soil and groundwater chemical analyses are presented below.
SITE HISTORY AND USAGE
The project area has a history of industrial manufacturing over the last century and was the location of machine shops, brass and iron foundries , and petroleum storage tanks. Our research into the site history of 1415 Hyde Park Avenue included a review of Sanborn Maps from 1917 , 1930 , 1950 , and 1990.
It is understood that Boston Fire Prevention Bureau records contain permits for storage of both gasoline and fuel. oil in three underground storage tanks, all of which have reportedly been removed. Based on our review of previous reports , a release of an unknown amount of NO. 4 fuel oil was identified during a tank removal in 1987 and was assigned State Spill Site N87-0823.
Based on our review of DEP information available online and reports prepared by others , PAHs and metals (lead , arsenic, antimony, cadmium , copper , chromium , nickel) were found to exceed MCP reportable concentrations and were reported to DEP , who assigned Release Tracking Number (RTN) 3
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27791 to the release in June 2008. Petroleum hydrocarbons and chlorinated volatie organics vinyl chloride (VC) and trichloroethene (TCE) in the central area of the site were found to exceed MCP reportable concentrations and were reported to DEP . who assigned RTN 3-28336 in March 2009.
Concentrations of chlorinated volatile organic compounds (VOCs) detected in soil and groundwater were reported on the northern portion of the site and reported to DEP, who assigned RTN 3-27790 in June
2008. A Class B-1 Response Action Outcome (RAO) statement was submitted in September 2008 which indicated that there was a condition of no significant risk related to the presence of VOCs in the northern portion of the site and that VOCs had not been cleaned up to background conditions.
In addition , PCBs were detected in Mother Brook sediments and bank soils to the north of the site by other parties performing remediation of Mother Brook. The finding of PCBs in the Mother Brook sediments and bank soils to the north of the site was deemed to be an Imminent Hazard as defined by the MCP and was
reported to DEP and assigned RTN 3-27168 in October 2007. An Immediate Response Action is being performed by Thomas and Betts Corporation and by New Albertsons , Inc.
PROPOSED SCOPE OF NEW CONSTRUCTION
The proposed development is understood to consist of the renovation of the existing mill and warehouse structures , and the construction of three building additions. It is understood that the redeveloped buildings
and grounds are to be used for a school.
In general , one addition will be located on the west side of the existing mill building and will abut the entire south side of the existing warehouse. The second addition wil be located on the east side of the warehouse. The third addition consists of an entrance addition on the north side of the warehouse. It is understood that the lowest levels of. the proposed additions will approximate the lowest floor level of the existing warehouse and will not contain any below grade space. The proposed renovation to the existing mill building is understood to include the construction of two stair structures and the lowering of the elevated wood floor located in the northeast wing down to the existing concrete floor level located at about Elevation +52.
The approximate locations of the proposed building additions, stair structures and the approximate Figure 2. Construction of
location of existing elevated wood floW level are indicated on the enclosed
below-grade space is not anticipated Proposed foundation support for the additions and stair foundations consists of piers and grade beams. Support for pier footings will require over-excavation of the existing fill
to the top of the alluvial or glacial outwash deposits located at depths of up to 10.5 feet below existing
ground surface , and backfilling the excavation. Prior to placement of gravel fil for the support of slabs-ongrade, all soft and/or compressible areas detected by proof-rolling will be removed and replaced with suitable materials. In addition , below-grade remains of former structures may be removed if they interfere with new construction.
A playing field is proposed for a portion of the site , and play and parking areas are proposed around the existing and proposed structures.
Excavation requiring dewatering is expected to be incidental in nature and would be related to excavations for pier footing supports , to remove unsuitable soils or below grade remains , to construct elevator pits
stair structures within the building footprint and/or utility structures within the property.
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PREVIOUS SITE INVESTIGATIONS
A Preliminary Site Assessment was conducted and reported by IES , Inc. in 2001. IES reported that drums of cutting oil , lubricants , wastes generated by furniture restoration business , parts cleaner, and
dichloromethane were observed. IES conducted a subsurface investigation including test borings monitoring well installation , soil screening, and laboratory analysis of soil and gro ndwater samples. IES performed six soil borings and four monitoring well installations to the west, south , and north of the existing buildings. The results of sampling and analysis indicated that PAHs indicative of fill containing ash and cinders were detected in the soil samples. The results of groundwater analyses indicated that dissolved barium was detected at concentrations well below reportable concentrations and that EPH VOCs , and the remaining RCRA metals were not detected. IES concluded that a reportable release had not occurred at the site.
GEC conducted a Phase I Environmental Site Assessment followed by two Phase II investigations in 2008. The investigations consisted of installation of borings , soil screening, sampling and analysis of soil samples in exterior areas of the site, monitoring well installation and groundwater sampling, as well as subslab soil vapor samples. GEC also conducted a soil precharacterization program in the area to the west of the mill building and south of the warehouse to assess soil characteristics for the purpose of off-site disposal. TPH , Metals , and VOCs were found to exceed MCP reportable concentrations.
In 2008 , CDW conducted two limited subsurface investigations focused on the portion of the property between the warehouse and Mother Brook. Investigations consisted of borings , soil sampling and analysis, indoor air sampling and analysis , monitoring well installation , and groundwater sampling. VOCs were found to exceed MCP reportable concentrations.
In 2007 through 2009, Shaw Environmental Inc. conducted remediation of PCB-contaminated soil on the banks of Mother Brook to the north of the site. Based on our review of site maps provided to us remediation on the south bank is located within the limits of the site property lines. Remediation is intended to remediate and stabilize the bank between the railroad bridge and Hyde Park Avenue bridge by excavating six feet into the north and south banks to remove PCB-contaminated soil , placement of a direct contact barrier on the north bank and stabilization of the south bank with a minimum of 1 foot clean soil
topped by 8- inch riprap. This work is ongoing as of the date of this report.
SUBSURFACE INVESTIGATION PERFORMED BY MCPHAIL ASSOCIATES, INC.
Between October 7 , 2008 and October 10, 2008, eleven (11) borings were conducted at the site by Carr-Dee Corp. The approximate exploration locations are indicated on the enclosed Subsurface Exploration Plan Figure 2. Boring and soil sampling locations were selected based on the proposed concept plan of the intended renovations; historical evidence of foundries , machine shops , and petroleum storage; and chemical test results reported by other consultants performing evaluations at the site.
The borings were performed to depths of 10 to 18 feet below surface grade over most portions of the site with five of the borings performed within the footprint of the proposed building additions and the existing warehouse to assess the chemical nature of subsurface soil at the site. Standard 2-inch O. D. split-spoon samples and standard penetration test results were obtained continuously from the surface to the depth of the boring. The borings were terminated in natural soil deposits at depths of approximately seven (7) feet
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below the observed groundwater table corresponding to approximately 11 to 18 below ground surface. Seven (7) of the borings were completed as 2-inch diameter monitoring wells. Boring logs and well details prepared by Carr- Dee Corp. are presented in Appendix C and approximate locations are shown in Figure
Soil samples were screened for the presence of total VOCs (TVOCs) using a photoionization detector and visual and olfactory observation and a sample each was generally selected for analysis from the fill and the natural soils. Headspace screening results are provided in 1. The results of chemical testing ofTable
soil are provided in Table 2.
Groundwater samples were collected for chemical testing on October 29 2008 from the recently installed monitoring wells MAI-1 OW , MAI-4 OW , MAI-5 OW , MAI-8 OW , MAI-9 OW , MAI-10 OW , and MAIOW. In addition , groundwater samples were collected for chemical testing from monitoring wells GECGEC- , GEC-3 installed by GEC and MW-2 installed by CDW (CDW-MW-2). Monitoring well MAI-5 OW . was resampled on November 5, 2008. Monitoring wells MAI-1 OW and CDW-MW-2 were resampled on December 2 , 2008. The results of chemical testing are summarized in Table 3.
On March 30 , 2009 , McPhail Associates obtained groundwater samples from monitoring wells MAI-1 and MAI-8. The approximate locations of the sampled wells are shown on the enclosed 2. The resultsFigure
4. The samples were tested for total suspended solids (TSS), pH , total cyanide , total residual chlorine (TRC), total phenolics hexavalent chromium , total and dissolved Priority Pollutants (PP-13) metals (antimony, arsenic , cadmium chromium , copper, iron, lead , mercury, nickel , selenium , silver and zinc), TPH , pesticides , VOCs , SVOCs and polychlorinated biphenyls (PCBs).
E and summarized inof the chemical testing are included in Appendix Table
SUBSURFACE CONDITIONS
A detailed description of the subsurface conditions encountered at the exploration locations are C. The generalized subsurface conditions across the site
were inferred primarily from these explorations , but also from our general knowledge of the local geology. The subsurface conditions encountered in the exploration are described below.
documented on the logs contained in Appendix
The results of our subsurface investigation indicates that the ground surface is underlain by a 4 to 10-foot thickness of fill material. In the area of the addition to be located to the south of the existing mill building the fill material was directly underlain by a compact to dense sand and gravel deposit. In the area of the two additions to be located to the north of the existing mill building and in the area of Mother Brook, the explorations indicate that thefill material was underlain by a 1.5 to 2-foot thickness of organics consisting of peat. The existing fill material and organics were underlain by a natural sand and gravel deposit the surface of which was present at depths ranging from 4 to 10.5 below existing ground surface.
South and west of the existing buildings, the existing fill material was encountered to depths of approximately 6. 5 to 8 feet below ground surface. North of the existing buildings , the fill material was encountered to depths of approximately 10.5 feet diminishing to 3 feet below ground surface near Mother Brook. North of the existing buildings, fill material was underlain by up to a 3-foot thickness of organics consisting of peat in some borings.
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Wood , brick , coal , ash and cinder were noted by the field engineer in the fill deposit in borings across the property. Materials described as slag or metal shavings were described in the area between the existing
buildings and Mother Brook.
AppendixGroundwater level information is provided in D. Groundwater was observed within the
completed borings at a depths of between 4.5 to 9 feet below the existing ground surface, corresponding to Elevations +42.9 to +44. Based on the groundwater elevations noted , the groundwater gradient is likely relatively low. The apparent flow direction is to the northeast toward Mother Brook. Flow direction may also be influenced by local features such as underground utilities and foundations. It is anticipated that future groundwater levels across the site may vary from those reported herein due to factors such as normal seasonal changes, periods of heavy precipitation , and alterations of existing drainage patterns.
RESULTS OF CHEMICAL TESTING BY MCPHAIL ASSOCIATES- SOIL SAMPLES
All samples of the fill material and natural soils were screened utilizing a Photoionization detector for the presence of volatile organic compounds (TVOCs). The results generally indicated no visual or olfactory evidence of a release in the majority of the samples screened. Six (6) of the 68 samples screened exhibited moderate PID readings (between 10 and 50 ppm) and one sample from boring MAI-10 (OW)
had a reading of 99.9 ppm (2. 5 to 4. 5 feet below ground surface). Natural soils typically had very low heads pace readings.
Soil samples were collected for chemical analysis from both fill materials and natural soils. Samples were typically grab samples collected from a single location. Samples were selected from surface fill materials and subsurface natural soils. Samples were analyzed for extractable petroleum hydrocarbons (EPH), polychlorinated biphenyls (PCBs), polynuclear aromatic hydrocarbons (PAHs), metals (antimony, arsenic cadmium , chromium , copper , lead , nickel , silver , and zinc), and/or volatile organic compounds (VOCs).
Table 2. In general , elevated chemicalA summary of the results for soil is presented on the enclosed
concentrations in soil were typically associated with fill materials and not with underlying natural soils.
Fill soils
Extractable petroleum hydrocarbons were detected in fill soils at concentrations consistent with previous investigations
Concentrations of PAHs in fill materials typically were consistent with or less than published Background concentrations for fill soils and are consistent with previous investigations. Samples from MAI-2 (0.5 to
5 feet below ground) and MAI-10 (0. 5 to 2.5 feet below ground) exceeded published Background concentrations for fill soils.
Concentrations of metals in fill materials typically exceeded published Background concentrations for fil soils, reflecting the potential disposal of foundry sand or other materials on site. Cadmium , total
chromium , nickel , zinc , antimony and lead appeared to be elevated. One sample with elevated chromium concentrations was analyzed for hexavalent chromium , which was reported as non-detect. Metals
concentrations wer generally consistent with or less than those reported in previous investigations.
VOCs were detected at trace concentrations in three (3) samples in fill soils. VOCs detections
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corresponded to elevated headspace readings reported by the field engineer at two locations. Concentrations of VOCs are generally consistent with or less than those documented in previous reports by GEC and CDW.
Natural Soils
Concentrations of PAHs in natural soils were typically not detected at laboratory reporting limits or were consistent with published Background concentrations for natural soils.
Concentrations of metals in natural soils were typically consistent with published Background1 (OW) (3 to 6 feetconcentrations for natural soils with the exception of a sample collected from MAI-below ground) where metals concentrations exceeded background concentrations for natural soil. It is possible that this sample contained some fill materials, resulting in this result.
PCBs were not detected on-site. Findings of PCBs as non-detect are generally consistent with those
documented in previous reports by GEC and CDW , who reported infrequent detects of PCBs below the
Risk-based criteria.
The concentration of naphthalene was found to exceed the published Background concentration forsoil samples.natural soils in one natural soil sample. VOCs were not detected in other natural
Concentrations of VOCs are generally consistent with or less than those documented in previous reportsGEC and CDWby GEC and CDW. Concentrations of chlorinated VOCs in several samples collected by and reported to exceed reportable concentration RCS-1 were not confirmed by these results.
RESULTS OF CHEMICAL TESTING BY MCPHAIL ASSOCIATES- 2008 GROUNDWATER SAMPLES
Groundwater samples were analyzed for extractable petroleum hydrocarbons (EPH), polynuclear aromatic, lead , nickel , silver , and
hydrocarbons (PAHs), metals (antimony, arsenic, cadmium, chromium, copperzinc), and/or volatile organic compounds (VOCs). Each analytical method was selected based on the
locations of the monitoring wells relative to previously reported results by others and potential historical sources (machine shops, foundries), and the proposed future uses as either indoor space parking/roadways, or outdoor play areas.
Table 3. A summary of the results for samples collected in 2008 is presented on the enclosed
Concentrations reported by our laboratory for EPH and PAHs (not detected), metals, and VOCs are generally consistent with or less than those documented in previous reports by GEC and CDW and with those previously reported to DEP.
EPH. One (1) groundwater sample obtained from MAI-10 (OW)was analyzed for EPH. EPHnondetectedconcentrations in the sample were not detected. This finding is consistent with
concentrations of EPH fractions in groundwater samples documented in previous reports by GEC and CDW.
PAHs . Four (4) groundwater samples were analyzed for PAHs. Concentrations of PAHs in groundwater samples were not detected. This finding is consistent with nondetected concentrations of PAHs in
groundwater samples documented in previous reports by GEC and CDW.
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Metals . Three (3) groundwater samples were collected using low flow methods and analyzed for total metals. Two samples were also analyzed for dissolved copper and lead. Total arsenic , copper , lead , and zinc were detected in groundwater samples at concentrations exceeding RGP effluent limits. Dissolved lead was not detected , indicating that the detectable lead levels were likely due to the presence of suspended solids in the water. Dissolved copper concentrations were similar to or greater than total copper concentrations , indicating that copper was present in the dissolved form. Both samples with elevated copper concentrations are located in the north portion of the property.
The presence of detected metals are generally consistent with those documented in previous reports by CDW for monitoring wells MW-1 and MW-2. The concentrations of detected metals are somewhat higher than those documented in previous reports by CDW; this difference is attributed to the presence of turbidity in the unfiltered samples collected by McPhail.
VOCs . VOCs were detected at trace concentrations in six (6) samples, none of which exceeded RGP effuent limits. Previous investigations ' reported similar results as well as trace concentrations of Naphthalene and 1 , 1-trichloroethane (1 , 1-TCA).
RESULTS OF CHEMICAL TESTING BY MCPHAIL ASSOCIATES - 2009 GROUNDWATER SAMPLES
A summary of results for samples collected in 2009 specifically for this permit application is presented in Table Table4. As shown in the enclosed , the results of the groundwater chemical analyses indicate that none of the tested samples exhibited the presence of detectable concentrations of total cyanide , TRC total phenolics , TPH , pesticides , or PCBs.
Trace concentrations of VOCs were detected at levels below RGP effluent limits.
Total copper was detected at a maximum concentration of 104,6 milligrams per liter (mg/l) which is in excess of the RGP effuent limit of 5.2 mg/l (with no dilution). Hexavalent chromium was detected at a maximum concentration of 21 milligrams per liter (mg/l) which is in excess of the RGP effuent limit of 11.4 mg/l (with no dilution). Dissolved concentrations of copper as reported in the laboratory report indicate that elevated concentrations of copper are in the dissolved form. Total antimony, arsenic, chromium , iron lead , nickel , selenium , and zinc were detected at concentrations well below the RGP effluent limits. None of the other PP- 13 metals were detected at concentrations in xcess of the MDLs which are well below the RGP effuent limits.
pH Was measured at 11. , which is in excess of the Class B surface water discharge limit of 8. , therefore pH adjustment will be necessary during discharge.
In summary, the results of the chemical testing performed on samples of the groundwater at the site indicate exceedences of the RGP limits for copper, hexavalent chromium , and pH.
All other analytes that were tested for were not detected at levels that require implementation of special treatment of the effluent prior to discharge. Calculation of the mass of each of the detected chemicals is5.provided in Table
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DILUTION FACTOR for METALS
A Dilution Factor (DF) was calculated in order to identify the RGP limits for total metals. The DF calculations were performed in accordance with the procedure contained in MAG910000 , Appendix VCalculation of Dilution Factor for Applications in Massachusetts . The purpose of the DF calculation is to
establish Total Recoverable Limitsfor metals , taking into consideration the anticipated dilution of the detected analytes upon discharge of the effuent into the Mother Brook.
The calculated DF was then used to find the appropriate Dilution Range Concentrations (DRCs) contained in MAG910000 , Appendix IV.
The DF that was utilized in finding the appropriate DRCs was calculated as follows:
DF = (Od + Os)/Od
Where: Od is the maximum discharge flow rate of 15 GPM = 0.03 cubic feet per second (cfs),(1 GPM = 0. 00223 cfs)
Os is the receiving water flow rate (minimum for 7 consecutive days with a recurrence interval of 10 years)
The value for Os used for identifying the DRCs contained in MAG 910000 Appendix IV is based on information provided by the US Geological Survey (USGS) at "Streamstats for Massachusetts" web application (http://water.usqs.qOv/osw/streamstats/massachusetts. html) . Since there was no streamflow gage in the vicinity of the anticipated discharge , the Os was estimated using the regression equations provided at the web application. The point of estimation used was at the approximate point of entry of the outfall to Mother Brook. A printout of the Streamflow parameters and statistics are provided in AppendixF. The Minimum Flow Rate estimated for 7 consecutive days with a recurrence interval of 10 years (7010flow) is 0. 15 cfs.
The resulting DF is 6.
Based on the DF value of 6, the applicable DRCs contained in MAG910000 , Appendix IV, are equal to those shown for DF between 5 and 10 (provided in Table 4). The maximum value of hexavalent chromium detected on the site meets the DRC limit. The maximum value of total copper detected on the site does not meet the DRC limit. As noted abqve , the presence of copper is likely to be in the dissolved form , therefore additional treatment in addition to settling may be required. As a result of these exceeded levels, a system designed to treat copper contaminated water, which may include but is not limited to ion exchange, precipitation , coagulation , and flocculation , adsorption , and absorption will be implemented prior to discharge.
PROPOSED TEMPORARY DEWATERING DURING CONSTRUCTION
Based upon the configuration of the proposed construction and the conditions encountered in the subsurface explorations , excavation below the observed groundwater elevation will be required for the construction of foundation structures , elevator pit , and site utilities. Hence , construction dewatering isanticipated to be required within localized areas of the site.
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In general , it is anticipated that intermittent dewatering by means of strategically located sumps and trenches should suffce during construction operations. In addition , trapped surface water is anticipated toaccumulate within localized depressions in the ground surface across the site after periods of heavy precipitation and will most likely necessitate localized pumping. It is estimated that the typical continuousgroundwater discharge required during the proposed excavation will be on the order of 15 gallons per minute (GPM). The influent will be pumped from localized sumps that will be situated across the footprint of the area subject to excavation into a 10 OOO-galion sedimentation tank in order to allow the settementof particulate matter. Alternatively, the contractor may elect the utilization of two (2) sedimentation tanks
000-galions each installed in- line. pH adjustment would be performed by the contractor in the sedimenttanks to achieve the required limits.
The approximate locations of proposed discharge points on-site are provided in Figure 3. A review of a
100-scale drawing provided to McPhail by Boston Water and Sewer Commission (BWSC) indicates the presence of a storm drain line beneath Hyde Park Avenue which discharges into Mother Brook at Outfall No. SD0244. The storm drain line expands from 15 inches at the south end of the site to 24 inches at thenorth end of the site. The approximate locations of the above referenced storm drain line and outfall are shown on the enclosed Figure 4.
Based on the results of the chemical analyses performed on groundwater samples obtained from the subject site , it is concluded that the effluent will require treatment for total copper prior to discharge into Mother Brook. A system designed to treat copper-contaminated water, which may include but is notlimited to ion exchange , precipitation , coagulation and flocculation , adsorption , and absorption will beimplemented prior to discharge. Finally, the effluent will pass through a bag-filter prior to discharge inorder to further reduce the concentration of TSS. A schematic of the proposed discharge system is presented in Figure 5.
It is anticipated that the proposed dewatering will commence on May 1 , 2009 and will be completed on or before September 1 2010.
SUMMARY AND CONCLUSIONS
The proposed development includes renovation of the existing mill and warehouse structures , and theconstruction of three building additions. Excavation will be required for an elevator pit and to install utilitiesand foundation structures and will require the implemetation of a temporary construction dewatering system and discharge of the effluent off-site.
Based on information provided to McPhail Associates by the BSWC , it is anticipated that the temporarydischarge of the dewatering effluent from the subject construction site will utilize a storm drain line that is situated beneath Hyde Park Avenue that discharges into an outfall located on Mother Brook and ultimately into the Neponset River. It is anticipated that the discharge will be intermittent during the constructionperiod with an average discharge rate of about 15 GPM.
Based on the groundwater chemical test results , it is concluded that treatment of the effuent would berequired in order to meet the MAG91 0000 Discharge Limits. The effluent will be treated for copper. Inaddition , the influent will be pumped through a sedimentation tank and the effluent will be pumped through bag filters prior to discharge in order to meet the TSS Limits contained in MAG910000.
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Sampling and chemical testing of the influent and effuent will be performed in accordance with the requirements contained in the US EPA's Authorization to Discharge. Should the results of the initial
monitoring indicate the presence of evidence of contamination in the effuent at levels that exceed the RGP limits, appropriate corrective measures will be implemented and additional confirmatory monitoring will be performed.
We trust that the above satisfies your present requirements. Please do not hesitate to contact us should you have any questions or require additional information.
Very truly yours
Enclosures
cc: Boston Renaissance Charter Public School (Mr. Kevin Cherry)
F:\WP5\REPORTS\4860-RGP Application rev 1.wpd MLZ/ajd
Geotechnical Engineers
APPENDIX B
US EPA Notice of Intent and
Boston Water and Sewer Commission Dewatering Permit Application
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of o
pera
tor
(if d
iffer
ent f
rom
ow
ner)
: St
reet
:
Tow
n:
Stat
e:
Zip
: C
ount
y:
d) C
heck
"ye
s" or "
" fo
r th
e fo
llow
ing:
I.
Has
a p
rior
NPD
ES
perm
it ex
clus
ion
been
gra
nted
for
the
disc
harg
e? Y
es
NoL
, if "
yes
" nu
mbe
r:
2. H
as a
pri
or N
PDE
S ap
plic
atio
n (F
orm
1 &
2C
) ev
er b
een
file
d fo
r th
e di
scha
rge?
Yes
N
o
, if "ye
s "
date
and
trac
king
#:
3. I
s th
e di
scha
rge
a "n
ew d
isch
arge
as
def
ined
by
40 C
FR 1
22.2? Yes ';
No
4. F
or s
ites
in M
assa
chus
etts
, is
the
disc
harg
e co
vere
d un
der
the
MA
Co
ti-;g
ency
Plan (MCP) and exempt from state permitting?
Yes
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
_-
---
___
___
___
___
___
__
e) I
s si
te/f
acili
ty s
ubje
ct to
any
Sta
te p
erm
ittin
g or
oth
er a
ctio
n w
hich
is c
ausi
ng th
e f)
Is
the
site
/fac
ility
cov
ered
by
any
othe
r E
P A
per
mit
, inc
ludi
ng:
gene
ratio
n of
dis
char
ge?
Yes_- No
\. m
ulti-
sect
or s
torm
wat
er g
ener
al p
erm
it? Y
N
L,
ifY
, num
ber:
If "ye
s "
plea
se li
st:
2. p
hase
I or
II c
onst
ruct
ion
stor
m w
ater
gen
eral
per
mit?
Y
\. si
te id
entif
icat
ion
# as
sign
ed b
y th
e st
ate
of N
H o
r M
A:
if Y
, num
ber:
2.
per
mit
or li
cens
e #
assi
gned
: 3.
indi
vidu
al N
PDE
S pe
rmit?
Y
N-.
_ if
Y, n
umbe
r:
3. s
tate
age
ncy
cont
act i
nfor
mat
ion:
nam
e , lo
catio
n, a
nd te
leph
one
num
ber:
4.
any
oth
er w
ater
qua
lity
rela
ted
perm
it? Y
N
-", i
fY, n
umbe
r:
2. D
isch
arge
info
rmat
ion.
Ple
ase
prov
ide
info
rmat
ion
abou
t the
dis
char
ge, (
atta
chin
g ad
ditio
nal s
heet
s as
nee
ded)
incl
udin
g:
a) D
escr
ibe
the
disc
harg
e ac
tiviti
es f
or w
hich
the
owne
r/ap
plic
ant i
s se
ekin
g co
vera
ge:
Tem
pora
ry in
term
itten
t con
stru
ctio
n de
wat
erin
g fo
r ex
cava
tion
for
pier
foot
ings
sup
port
, ele
vato
r pi
t, ut
ilitie
s, a
nd r
emov
al o
f uns
uita
ble
fill s
oils
b) P
rovi
de th
e 1)
Num
ber
of
2) W
hat i
s th
e m
axim
um a
nd a
vera
ge f
low
rat
e of
dis
char
ge (
in c
ubic
fee
t per
sec
ond
, ft3
/s)?
M
ax. f
low
.03
3
follo
win
g di
scha
rge
Ave
rage
flow
.01
7 Is
max
imum
flo
w a
des
ign
valu
e?
info
rmat
ion
poin
ts:
For average flow
, inc
lude
the
units
and
app
ropr
iate
not
atio
n if
this
val
ue is
a d
esig
n va
lue
or e
stim
ate
if n
ot a
vaila
ble.
ab
out e
ach
di
scha
rge:
3) Latitude and longitude of each discharge within 100 feet: pt. :long.
42.
lat.
; pt.2: long.
lat.
; pt. 3: long,
lat.
pt.4
:long
. la
t. ; pt.5: long.
lat.
; pt.6
:long
. la
t. ; pt.: long.
lat.
; pt.8
:long
. la
t. ; e
tc.
4) I
f hy
dros
tatic
test
ing,
tota
l vol
ume
of.th
e di
scha
rge
(gal
s):
5) I
s th
e di
scha
rge
inte
rmitt
ent
or s
easo
nal
Is d
isch
arge
ong
oing
Y
es
c) E
xpec
ted
date
s of
dis
char
ge (
mm
/dd/
yy):
sta
rt 0
5/01
/09
end
08/3
0/10
d) P
leas
e at
tach
a li
ne d
raw
ing
or f
low
sch
emat
ic s
how
ing
wat
er f
low
thro
ugh
the
faci
lity
incl
udin
g:
\. so
urce
s of
inta
ke w
ater
, 2. c
ontr
ibut
ing
flow
fro
m th
e op
erat
ion
, 3. t
reat
men
t uni
ts, a
nd 4
. dis
char
ge p
oint
s an
d re
ceiv
ing
wat
ers(
s).
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
3. C
onta
min
ant i
nfor
mat
ion.
In
orde
r to
com
plet
e th
is s
ectio
n, t
he a
pplic
ant w
il ne
ed to
take
a m
inim
um o
f on
e sa
mpl
e of
the
untr
eate
d w
ater
and
hav
e it
anal
yzed
for
all
of th
e pa
ram
eter
s lis
ted
in A
ppen
dix
III.
His
tori
cal d
ata,
(i.
, dat
a ta
ken
no m
ore
than
2 y
ears
pri
or to
the
effe
ctiv
e da
te o
f th
e pe
rmit)
may
be
used
if o
btai
ned
purs
uant
to:
i. M
assa
chus
etts
' re
gula
tions
310
CM
R 4
0. 0
000
, the
Mas
sach
uset
ts C
ontin
genc
y Pl
an (
"Chapter 21 E"
); ii
. New
Ham
pshi
re s
Titl
e 50
RSA
485
-A: W
ater
Pol
lutio
n an
d
Was
te D
ispo
sal o
r T
itle
50 R
SA 4
85-C
: Gro
undw
ater
Pro
tect
ion
Act
; or
iii. a
n E
P A
per
mit
excl
usio
n le
tter
issu
ed p
ursu
ant t
o 40
CFR
122
. , p
rovi
ded
the
data
was
anal
yzed
with
test
met
hods
that
mee
t the
req
uire
men
ts o
f th
is p
erm
it. O
ther
wis
e, a
new
sam
ple
shal
l be
take
n an
d an
alyz
ed.
a) B
ased
on
the
anal
ysis
of
the
sam
ple(
s) o
f th
e un
trea
ted
infl
uent
, the
app
lican
t mus
t che
ck th
e bo
x of
the
sub-
cate
gori
es th
at th
e po
tent
ial d
isch
arge
fal
ls w
ithin
.
Gas
olin
e O
nly
VO
C O
nly
Prim
arily
Met
als
Site
s C
onta
min
ated
Sum
ps
Mix
ed C
onta
min
ants
Aquifer Testing
Urban Fill
Fuel Oils (and
VO
C w
ith O
ther
Pe
trol
eum
with
Oth
er
Lis
ted
Con
tam
inat
ed
Con
tam
inat
ed
Hyd
rost
atic
Tes
ting
of
Wel
l Dev
elop
men
t
Oth
er O
ils)
only
C
onta
min
ants
C
onta
min
ants
Si
tes
Dredge Condensates
Pipe
lines
/Tan
ks
or R
ehab
ilita
tion
b) B
ased
on
the
anal
ysis
of
the
untr
eate
d in
flue
nt, t
he a
pplic
ant m
ust i
ndic
ate
whe
ther
eac
h lis
ted
chem
ical
is b
elie
ved
pres
ent o
r be
lieve
d ab
sent
in th
e po
tent
ial
disc
harg
e. A
ttach
add
ition
al s
heet
s as
nee
ded.
Ana
lytic
al
Min
imum
M
axim
um d
aily
val
ue
Avg
. dai
ly v
alue
PAR
AM
ET
ER
B
elie
ve
Bel
ieve
#
of
Typ
e of
A
bsen
t Pr
esen
t Sa
mpl
es
Sam
ple
Met
hod
Lev
el (
ML
) of
(1
min
-(e
.g.,
grab
) U
sed
Tes
t Met
hod
conc
entr
atio
n m
ass
(kg)
co
ncen
trat
ion
mas
s (k
g)
imum
) (m
etho
d #)
(u
g/l)
(u
g/l)
1. T
otal
Sus
pend
ed S
olid
s
grab
25
40
5 mg/I
8500
42
50
348
2. T
otal
Res
idua
l gr
ab
4500
CL
-02 mg/I
Chl
orin
e
3. T
otal
Pet
role
um
grab
16
64A
4 mg/I
Hyd
roca
rbon
s
4. C
yani
de
grab
45
00C
N-
005
mg/
I
5. B
enze
ne
grab
62
4
6. Toluene
grab
62
4
7. Ethylbenzene
grab
62
4
8. (
m
o) X
ylen
es
grab
62
4
9. T
otal
BT
EX
'
BT
EX
= S
um o
f B
enze
ne, T
olue
ne, E
thyl
benz
ene,
tota
l Xyl
enes
.
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
#of
Typ
e of
A
naly
tical
M
inim
um
Max
imum
dai
ly v
alue
A
vg. d
aily
val
uePA
RA
ME
TE
R
Bel
ieve
B
elie
ve
Abs
ent
Pres
ent
Sam
ples
S
ampl
e (e
.g.,
Met
hod
Lev
el (
ML
) of
(1
min
-gr
ab)
Use
d T
est M
etho
d co
ncen
trat
ion
mas
s (k
g)
conc
entr
atio
n m
ass
(kg)
(m
etho
d #)
(u
g/I)
imum
) (u
g/I)
10. Ethylene Dibromide
020
grab
50
4.
(1,2
- D
ibro
mo-
met
hane
)
11.
Met
hyl-
tert
-But
yl
grab
62
4 E
ther
(M
tBE
)
12. tert-
But
yl
Alc
ohol
gr
ab
624
100
(TB
A)
13. tert-
Am
yl
Met
hyl
grab
62
4 E
ther
(T
AM
E)
14. N
apht
hale
ne
grab
82
70C
15. Carbon
Tet
ra-
grab
62
4 ch
lori
de
16. 1
, D
ichl
orob
enze
ne
grab
62
4
grab
62
417. 1
Dic
hlor
oben
zene
grab
62
418. 1
Dic
hlor
oben
zene
19. 1
, D
ichl
oroe
than
e gr
ab
624
20. 1
, D
ichl
oroe
than
e gr
ab
624
grab
62
421. 1
Dic
hlor
oeth
ylen
e
22. c
is-
2 D
ichl
oro-
0003
0gr
ab
624
ethy
lene
23.
Dic
hlor
omet
hane
gr
ab
624
(Met
hyle
ne C
hlor
ide)
24. T
etra
chlo
roet
hyle
ne
grab
62
4
ED
B is
a g
roun
dwat
er c
onta
min
ant a
t file
l spi
l and
pes
ticid
e ap
plic
atio
n si
tes
in N
ew E
ngla
nd.
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
0001
5
PAR
AM
ET
ER
B
elie
ve
Bel
ieve
#
of
Type of
Abs
ent
Pres
ent
Sam
ples
Sa
mpl
e (e
. gr
ab)
(1 m
in
imum
)
25. 1
, 1
Tri
chlo
roet
hane
gr
ab
grab
26. 1
Tri
chlo
roet
hane
27. T
rich
loro
ethy
lene
gr
ab
28. V
inyl
Chl
orid
e
. gra
b
29. A
ceto
ne
grab
30. 1
, 4 D
ioxa
ne
grab
31. T
otal
Phe
nols
gr
ab
grab
32.
Pent
achl
orop
heno
l
33. Total Phthalates
grab
(Pht
hala
te e
sthe
rs)
34. B
is (
2-E
thyl
hexy
l)
Pht
hala
te (
Di-
grab
(e
thyl
hexy
l) P
htha
late
)
35. T
otal
Gro
up I
grab
Pol
ycyc
lic A
rom
atic
H
ydro
carb
ons
(P A
H)
a. B
enzo
(a)
Ant
hrac
ene
gr
ab
b. B
enzo
(a)
Pyr
ene
gr
ab
c. B
enzo
(b)F
luor
anth
ene
gr
ab
d. B
enzo
(k)
Flu
oran
then
e
grab
e. C
hrys
ene
gr
ab
The
sum
ofi
ndiv
idl1
al p
htha
late
com
poun
ds.
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
Ana
lytic
al
Met
hod
Use
d (m
etho
d #)
624
624
624
624
624
624
420.
8270
C
8270
C
8270
C
8270
C
8270
C
8270
C
8270
C
8270
C
8270
C
Min
imum
Lev
el
Max
imum
dai
ly v
alue
A
vg. d
aily
Val
ue
(ML)
ofT
est
Met
hod
co
ncen
trat
ion
mas
s (k
g)
conc
entr
atio
n m
ass
(kg)
(ug/
l)
(ug/
l)
0001
5
0001
2
0027
16
. 00
013
2000
03 r
ig/I
5 m
g/.
PAR
AM
ET
ER
B
elie
ve
Bel
ieve
#
of
Type of
Ana
lytic
al
Min
imum
M
axim
um d
aily
val
ue
Ave
rage
dai
ly v
alue
Abs
ent
Pres
ent
Sam
ples
Sa
mpl
e (e
. M
etho
d U
sed
Lev
el (
ML
) of
gr
ab)
(met
hod
#)
Tes
t Met
hod
(1 m
in-
conc
entr
atio
n m
ass
(kg)
co
ncen
trat
ion
mas
s (k
g)
imum
) (u
g/l)
(u
g/l)
f. D
iben
zo(a
gr
ab
8270
Can
thra
cene
g. I
nden
o(1,
3-
cd)
grab
82
70C
Pyre
ne
36. T
otal
Gro
up I
I 00
0017
10
5 00
0008
6P
olyc
yclic
Aro
mat
ic
grab
.2
1
Hyd
roca
rbon
s (P
AH
)
h. A
cena
phth
ene
gr
ab
8270
C
i. A
cena
phth
ylen
e
grab
82
70C
j. A
nthr
acen
e
grab
82
70C
k. Benzo(ghi) Perylene
grab
82
70C
I. F
luor
anth
ene
gr
ab
8270
C
m. Fluorene
grab
82
70C
n. N
apht
hale
ne-
grab
82
70C
.2
1 00
0017
10
5 00
0008
6o.
Phe
nant
hren
e
grab
82
70C
p. P
yren
e
grab
82
70C
37. T
otal
Pol
ychl
orin
ated
gr
ab
.258
608
Bip
heny
ls (
PCB
s)
0000
74
0.45
00
0037
38. A
ntim
ony
gr
ab
6020
grab
60
20
0002
2 00
011
39. Arsenic
40. C
adm
ium
gr
ab
6020
III
grab
60
20
3500
CR
-01
0 m
g/I
0017
10
. 00
086
41. Chromium
42. C
hrom
ium
VI
gr
ab
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
----
-g.
,
PAR
AM
ET
ER
B
elie
ve
Bel
ieve
#
of
Typ
e of
A
naly
tical
M
inim
um
Max
imum
dai
ly v
alue
A
vg. d
aily
val
ue
Abs
ent
Pres
ent
Sam
ples
Sa
mpl
e (e
. M
etho
d L
evel
(M
L)
of
(I m
in-
grab
) U
sed
Tes
t Met
hod
mas
s (k
g)
conc
entr
atio
n m
ass
(kg)
co
ncen
trat
ion
imum
) (m
etho
d #)
(u
gll)
(u
g/l)
52.
0043
243
. Cop
per
gr
ab
6020
10
4.
0085
0000
9 00
0045
44. L
ead
gr
ab
6020
45. M
ercu
ry
grab
24
5.
14.
0011
9 8.
75
0007
2 46. Nickel
grab
60
20
0002
45
0001
647
. Sel
eniu
m
grab
60
20
48. S
ilver
gr
ab
6020
grab
60
20
20.2
00
165
10.
0008
349
. Zin
c
110
0090
00
4550
. Iro
n gr
ab
200.
Oth
er (
desc
ribe
):
c) F
or d
isch
arge
s w
here
met
als
are
belie
ved
pres
ent,
ple
ase
fill
out t
he f
ollo
win
g:
If y
es, w
hich
met
als?
Step 1:
Do
any
of th
e m
etal
s in
the
influ
ent h
ave
a re
ason
able
potential to exceed the
Cop
per,
Hex
aval
ent C
hrom
e Y
L, the limits set atzero to five dilutions)?
effu
ent l
imits
in A
ppen
dix
II (
i.
III
limits
L
ook
up th
e lim
it ca
lcul
ated
at t
he c
orre
spon
ding
dilu
tion
fact
or in
Step
2:
For
any
met
als
whi
ch h
ave
reas
onab
le potential to exceed the Appendix
App
endi
x IV
. Do
any
of th
e m
etal
s in
the
infl
uent
hav
e th
e po
tent
ial t
oca
lcul
ate
the
dilu
tion
fact
or (
DF)
usi
ng th
e fo
rmul
a in
Par
t LA
. c)
(st
ep 2
) of
the
NO
I , i
s th
eex
ceed
the
corr
espo
ndin
g ef
flue
nt li
mits
in A
ppen
dix
IV (
i.in
stru
ctio
ns o
r as
det
erm
ined
by
the
Stat
e pr
ior
to th
e su
bmis
sion
of
this
NO
r.
infl
uent
con
cent
ratio
n ab
ove
the
limit
set a
t the
cal
cula
ted
dilu
tion
Wha
t is
the
dilu
tion
fact
or f
or a
pplic
able
met
als?
M
etal
s: C
oppe
r, H
exav
alen
t Chr
ome
fact
or)?
If "Y
es "
list
whi
ch m
etal
s: C
oppe
rD
F:
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
-"'''-
--'._
'''''''-
'-""
"''
----
-__
___
__
4. T
reat
men
t sys
tem
info
rmat
ion.
Ple
ase
desc
ribe
the
trea
tmen
t sys
tem
usi
ng s
epar
ate
shee
ts a
s ne
cess
ary,
incl
udin
g:
a) A
des
crip
tion
ofth
e tr
eatm
ent s
yste
m, i
nclu
ding
a s
chem
atic
of
the
prop
osed
or
exis
ting
trea
tmen
t sys
tem
: Sed
imen
tatio
n ta
nk a
nd b
ag fi
lers
-see
text
for
deta
ils
b) Identify each app licable
Frac
. ta
nk
Air
str
ippe
r Oil/water separator
I E
qual
izat
ion
tank
s I
Bag
filt
er
I G
AC
filt
er
trea
tmen
t uni
t (ch
eck
all
that
app
ly):
C
hlor
inat
ion
Dec
hlor
inat
ion
Oth
er (
plea
se d
escr
ibe)
: M
etal
s re
mov
al ,
incl
udin
g bu
t not
lim
ited
to c
oppe
r
c) P
ropo
sed
aver
age
and
max
imum
flo
w r
ates
(ga
llons
per
min
ute)
for
the
disc
harg
e an
d th
e de
sign
flo
w r
ate
(s)
(gal
lons
per
min
ute)
of
the
trea
tmen
t sys
tem
: A
vera
ge fl
ow r
ate
of d
isch
arge
l: Maximum flow rate of treatment system
Q.-
----
Des
ign
flow
rat
e of
trea
tmen
t sys
tem
d) A
des
crip
tion
of c
hem
ical
add
itive
s be
ing
used
or
plan
ned
to b
e us
ed (
atta
ch M
SDS
shee
ts):
Non
e
5. R
ecei
ving
sur
face
wat
er(s
). P
leas
e pr
ovid
e in
form
atio
n ab
out t
he r
ecei
ving
wat
er(s
) us
ing
sepa
rate
she
ets
as n
eces
sary
'
a) I
dent
ify
the
disc
harg
e pa
thw
ay:
I D
irec
t I W
ithin
faci
lity
I St
orm
dra
in
I R
iver
/bro
ok
I W
etla
nds
I O
ther
(de
scri
be):
b) P
rovi
de a
nar
rativ
e de
scrip
tion
of th
e di
scha
rge
path
way
, inc
ludi
ng th
e na
me(
s) o
fthe
rece
ivin
g w
ater
s:
Sto
rm d
rain
into
Mot
her
Bro
ok. S
ee F
igur
e 4
c) A
ttach
a d
etai
led
map
(s)
indi
catin
g th
e si
te lo
catio
n an
d lo
catio
n of
the
outf
all t
o th
e re
ceiv
ing
wat
er:
1. F
or m
ultip
le d
isch
arge
s , n
umbe
r th
e di
scha
rges
seq
uent
ially
. 2.
For
indi
rect
dis
char
gers
, in
dica
te th
e lo
catio
n of
the
disc
harg
e to
the
indi
rect
con
veya
nce
and
the
disc
harg
e to
sur
face
wat
er
The
map
sho
uld
also
incl
ude
the
loca
tion
and
dist
ance
to th
e ne
ares
t san
itary
sew
er a
s w
ell a
s th
e lo
cus
of n
earb
y se
nsiti
ve r
ecep
tors
(ba
sed
on U
SGS
topo
grap
hica
l m
appi
ng),
suc
h as
sur
face
wat
ers ,
dri
nkin
g w
ater
sup
plie
s, a
nd w
etla
nd a
reas
.
d) P
rovi
de th
e st
ate
wat
er q
ualit
y cl
assi
fica
tion
of th
e re
ceiv
ing
wat
er
e) P
rovi
de th
e re
port
ed o
r ca
lcul
ated
sev
en d
ay- t
en y
ear
low
flow
(7Q
10)
of t
he r
ecei
ving
wat
er..
cfs
Pl
ease
atta
ch a
ny c
alcu
latio
n sh
eets
use
d to
sup
port
str
eam
flo
w a
nd d
ilutio
n ca
lcul
atio
ns.
f) I
s th
e re
ceiv
ing
wat
er a
list
ed 3
03(d
) w
ater
qua
lity
impa
ired
or
limite
d w
ater
? Y
es
_- If yes
, for
whi
ch p
ollu
tant
(s)?
nut
rient
s, l
ow D
. , p
atho
gens
Is
ther
e a
TM
DL
? Y
es
If y
es, f
or w
hich
pol
luta
nt(s
)?
No
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
. ,,-
-./
_-
6. R
esul
ts o
f C
onsu
ltatio
n w
ith F
eder
al S
ervi
ces:
Ple
ase
prov
ide
the
follo
win
g info=ation according to requirements of
Par
t LB
A a
nd A
ppen
dice
s II
and
VIL
a) A
re a
ny li
sted
thre
aten
ed o
r en
dang
ered
spe
cies
, or
desi
gnat
ed c
ritic
al h
abita
t , in
pro
xim
ity to
the
disc
harg
e? Y
es
Has
any
con
sulta
tion
with
the
fede
ral s
ervi
ces
been
com
plet
ed?
Yes- N01
or is
con
sulta
tion
unde
rway
? Y
es - No
Wha
t wer
e th
e re
sults
of t
he c
onsu
ltatio
n w
ith th
e U
. S. F
ish
and
Wild
life
Serv
ice
andl
or N
atio
nal M
arin
e Fi
sher
ies
Serv
ice
(che
ck o
ne):
a "no
jeop
ardy
" op
inio
n? _
_or written concurrence
on a
fin
ding
that
the
disc
harg
es a
re n
ot li
kely
to a
dver
sely
aff
ect a
ny e
ndan
gere
d sp
ecie
s or
cri
tical
hab
itat?
b) A
re a
ny h
isto
ric
prop
ertie
s lis
ted
or e
ligib
le f
or li
stin
g on
the
Nat
iona
l Reg
iste
r of
His
tori
c Pl
aces
loca
ted
on th
e fa
cilit
y or
site
or
in p
roxi
mity
to th
e di
scha
rge?
Yes No
Hav
e an
y st
ate
or tr
ibal
his
tori
c pr
eser
vatio
n of
fcer
bee
n co
nsul
ted
in th
is d
eter
min
atio
n (M
assa
chus
etts
onl
y)?
Yes
7. S
uppl
emen
tal i
nfor
mat
ion.
:
Plea
se p
rovi
de a
ny s
uppl
emen
tal i
nfon
natio
n. A
ttach
any
ana
lytic
al d
ata
used
to s
uppo
rt th
e ap
plic
atio
n. A
ttach
any
cer
tific
atio
n(s)
req
uire
d by
the
gene
ral p
erm
it.
8. Signa ture R
equi
rem
ents
: The
Not
ice
of In
tent
mus
t be
sign
ed b
y th
e op
erat
or in
acc
orda
nce
with
the
sign
ator
y re
quir
emen
ts o
f 40
CFR
Sec
tion
122.
, i
nclu
ding
the
follo
win
g ce
rtfi
catio
n:
1 ce
rtify
und
er p
enal
ty o
f law
that
this
doc
umen
t and
all
atta
chm
ents
wer
e pr
epar
ed u
nder
my
dire
ctio
n or
sup
ervi
sion
in a
ccor
danc
e w
ith a
sys
tem
des
igne
d to
ass
ure
that
qua
lifed
per
sonn
el p
rope
rly
gath
er a
nd e
valu
ate
the
info
rm a
tion
subm
ited.
Bas
ed o
n m
y in
quiry
of
the
pers
on o
r pe
rson
s w
ho m
anag
e th
e sy
stem
, or
thos
epe
rson
s di
rect
(v r
espo
nsib
le f
or g
athe
ring
the
info
rmat
ion ,
I ce
rtify
that
the
info
rmat
ion
subm
ited
is, t
o th
e be
st o
f my
know
ledg
e an
d be
lief,
true
, acc
urat
e , a
ndco
mpl
ete.
1 c
ertif
y th
at 1
am
aw
are
that
ther
e ar
e signifcant penaltiesfor submittingfalse information, i
nclu
ding
the
poss
ibilt
y af
fine
and
impr
ison
men
t for
kno
win
gvi
olat
ions
.
Faci
lity/
Site
Nam
e:
futu
re s
ite- B
osto
n R
enai
ssan
ce C
hart
er P
ublic
Sch
ool
Opm
toe,
ign,
ture
o
Titl
e:
dFO
C
Dat
e:
Rem
edia
tion
Gen
eral
Per
mit
- N
otic
e of
Int
ent
Boston Water and Sewer Commission s Dewatering Discharge Permit Application
Facilty/Business Name: Boston Renaissance Charter Public School
Mailng Address: 250 Stuart Street, Boston, MA 02116
Authorized Representative concerning information provided herein:
Name: Mr. Kevin Cherry Title: Chief Financial Officer
617- 357-0900 x1212 Beeper#:Phone #: Fax#: 617-357- 0949
Owner of propert being dewatered: Boston Renaissance Charter Public School
Location of Discharge:
Street Hyde Park Avenue Neighborhood Hyde Park Phone# N/A
Discharge is to a: Sanitary Sewer
BWSC Outfall #: SD0244
Combined Sewer
Receiving Waters:
(Sorm D;V Mother Brook
(Circle One)
Temporary Discharges: 6/1/0 To 9/1/10 (provide anticipated dates of discharge)
Groundwater Remediation Tank Removallstallation J: Foundation Excavation Utilty/Manhole Pumping Test Pit Trench Excavation
JS Accum. Surface Water Hydrogeologic Testing Other
Permanent Discharges:
Foundation Dndnage Crawl SpacelFooting Drain.
Accumulated Surface Water Non-contactJncontaminated Cooling
Non-contactJncontaminated Process Other
Attach a Site Plan showing the source of the discharge and the location of the point of discharge (i. the sewer pipe or catch basin). Include meter tye, meter number, size, make and start reading. All discharges are assessed current sewer charges.
If discharging to a sanitary or combined sewer, attach a copy of MWRA' s Sewer Use Discharge permit or application.
If discharging to a separate storm drain attached a copy of EP A' s NPDES Permit or NOI application, or NPDES Permit exclusion letter for the discharge, as wen as other relevant information.
Dewatering Drainage Permit wil be denied or revoked if applicant fails to obtain the necessary permits from MW or EP A.
Submit to: Mr. Francis M. McLaughlin Phone: 617-989-7000 Manager, Engineerig Customer Services Fax: 617-989-7716 Boston Water and Sewer Commission 980 Harrison Ave.
Boston, MA 02119 :BWSC Use Only
Date Received: Comments:
Geotechnical Engineers
APPENDIX E
Groundwater Chemical Test Results
ALPHA ANALYTICAL
Eight Walkup Drive Westborough, Massachusetts 01581- 1019 (508) 898-9220 ww. alpha1ab. com
MA:M-MA086 NH:2003 CT:PH- 0574 ME:MA0086 RI:LA000065 NY:11148 NJ:MA935 Army:USACE
CERTIFICATE OF ANALYSIS
Client: McPhail Associates Laboratory Job Numer: L0903860
Address: 2269 Massachusetts Avenue Date Received: 30- MA- 2009
Cambridge, MA 02140 Date Reported: 06 - APR-2 00 9
Attn: Mr. Ambrose Donovan Delivery Method: Al pha
Project Number: 4860. Si te: BOSTON RENAISSANCE CHATER
ALPHA SAMPLE NUER CLIENT IDENTIFICATION SAMPLE LOCATION
L0903860- MAl - I 15 HYDE PARK AVE. L0903 8 60 - 02 MAl - 8 IS HYDE PARK AVE. L0903860- TRIP BLAK IS HYDE PARK AVE.
, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible
for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and
complete. This certificate of analysis is not complete unless this page accompanies any and all pages f this report.
Author;,ed by, .t yt.
Tech al RepresentatIve
04060916: 03 Page 1 of 24
ALPHA ANALYTICAL NARRATIVE REPORT
Laboratory Job Numer: L0903860
The samples were received in accordance with the chain of custody and no significant deviations were encountered during preparation or analysis unless otherwise noted below.
Volatile organics
The WG357153- 4 LCS recovery associated with L0903860- 01 and - 02 was above the acceptance criteria for Carbon tetrachloride (1 52%) however, the associated samples were non-detect for this target compound. The results of the original analysis are reported.
04060916: 03 page 2 of 24
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
MA:M-MA086 NH: 2003 CT: PH- 0574 ME :MA0086 RI: LA000065 NY: 11148 NJ:MA935 Army:USACE
-Date Collected: 30- MA-2009 11: 00Laboratory Sample Number: L0903860-01
MAl - 1 ample Matrix: WATER
Condition of Sample: Satisfactory
Number & Type of Containers: Amber
PARATER RESULT
General Chemistry Westborough Lab
Solids Total Suspended Cyanide, Total Chlorine, Total Residual TPH Phenolics, Total Chromi urn, Hexavalent 021
Total Metals Westborough Lab
Antimony, Total 0009 Arseni c, Total 0027 Cadmium, Total Chromium, Total 0120 Copper Total 0 . 1043 Iron, Total Lead, Total 0011 Mercury, Total Nickel Total 0145 Selenium, Total 003 Silver Total zinc, Total
Dissolved Metals Wes tboroughLab
Antimony , Dissolved 0011 Arsenic, Dissolved 0025 Cadmium, Dissolved Chromi urn, Dissolved 0114 Copper, Dissolved 0983 Iron, Dissolved Lead, Dissolved Mercury, Dissolved Nickel Dissolved 0138 Selenium, Dissolved 002 Silver , Dissolved Zinc, Dissolved
Date Received Date Reported
Field Prep:
Plastic, 4-Vial
UNITS RDL
mg/l mg/l 005 mg/l mg/l mg/l mg/l 010
mg/l 0005 mg/l 0005 mg/l 0002 mg/l 0005 mg/l 0005 mg/l mg/l 0005 mg/l 0002 mg/l 0005 mg/l 001 mg/l 0004 mg/l 0050
mg/l 0005 mg/l 0005 mg/l 0002 mg/l 0005 mg/l 0005 mg/l mg/l 0005 mg/l 0002 mg/l 0005 mg/l 001 mg/l 0004 mg/l 0050
REF METHOD
30 2540D
30 4500CN
30 4500CL
74 1664A
420. 30 3500CR
6020
6020
6020
6020
6020
19 200.
6020
245. 6020
6020
6020
6020
6020
6020
6020
6020
6020
6010B
6020
7470A
6020
6020
6020
6020
30-MA-2009 06 - APR- 2 009
None
DATE PREP ANAL
0402 10: 40 DW
0403 11: 00 0403 16:51 DD
0330 20:00 JO
0401 18: 00 0402 00:30 JO
0402 16:08 TH
0331 01: 30 0331 01: 30 JT
0401 11:20 0402 16:18 BM
0401 11:20 0402 16: 18 BM
0401 11: 20 0402 16:18 BM
0401 11:20 0402 16: 18 BM
0401 11:20 0402 16:18 BM 0401 11:20 0402 13:35 MG
0401 11:20 0402 16:18 BM 0331 12: 30 0401 10: 33 EZ
0401 11:20 0402 16: 18 BM
0401 11: 20 0402 16: 18 BM
0401 11:20 0402 16:18 BM 0401 11: 20 0402 16:18 BM
0401 11: 20 0402 18:41 BM
0401 11:20 0402 18:41 BM
0401 11: 20 0402 18: 41 BM
0401 11:20 0402 18:41 BM
0401 11: 20 0402 18:41 BM
0403 11:20 0406 10:04 MG 0401 11:20 0402 18:41 BM
0331 12: 30 0401 11:42 EZ 0401 11: 20 0402 18:41 BM
0401 11:20 0402 18:41 BM
0401 11:20 0402 18:41 BM
0401 11:20 0402 18:41 BM
Comments: Complete list of References and Glossary of Terms found in Addendum
04060916: 03 Page 3 of 24
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L0903860MAI - 1
PARATER RESULT UNITS RDL REF METHOD DATE
PREP ANAL
14 504. 0406 09:30 0406 13:03 JIJPesticides by GC Westborough Lab
I, 2 - Dibromoethane ug/l 020
624 033120:20 TTVolatile organics by GC /MB Westborougb Lab Methylene chloride ug/l
Dichloroethane ug/l 1. 5
1. 5 Chloroform ug/l 1. 0 Carbon tetrachloride ug/l
2 - Dichloropropane ug/l 1. 0 Dibromochlorometbane ug/l
1, I, 2 -Tricbloroetbane ug/l 1. 5
2 - Chloroethyl vinyl ether ug/l 10. 1. 5 Tetracbloroethene ug/l
Chlorobenzene ug/l Tr i chI oro f I uoromethane ug/l
2 - Dicbloroethane ug/l 1.5 , l, Trichloroethane ug/l
1. 0 Bromodichloromethane ug/l 1. 5 trans- I, 3-Dichloropropene ug/l 1. 5 cis- I, 3 -Dichloropropene ug/l 1. 0 Bromoform ug/l 1. 0 I, I, 2, 2 - Tetrachloroethane ug/l 1. 0 Benzene ug/l 1. 0 Toluene ug/l 1. 0 Ethylbenzene ug/l
Chloromethane ug/l 10. Bromomethane ug/l vinyl chloride ug/l Chloroethane ug/l
1. 0 I, 1-Dichloroethene ug/l trans- , 2-Dichloroethene ug/l' 1. 5
1. 0 cis- I, 2 - Dichloroethene ug/l 1. 0 1. 8 Trichloroethene ug/l
I, 2-Dichlorobenzene ug/l 3 - Dichlorobenzene ug/l
I, 4- Dichlorobenzene ug/l p/m-Xylene ug/l
1. 0 xylene ug/l Xylene (Total) ug/l
1. 0 Styrene ug/l Acetone ug/l Carbon disulfide ug/l
B1.tanone ug/l 10. Vinyl acetate ug/l 20. 4 -Methyl- 2 -pentanone ug/l 10. 2 - Hexanone ug/l 10. Acrolein ug/l Acryloni trile ug/l 10. Methyl tert butyl ether ug/l 20. 1, 4- Dioxane ug/l 2000
Comments: Complete list of References and Glossary of Terms found in Addendum I
04060916: 03 Page 4 of 24
Laboratory Sample Numer:
PARATER
Volatile Organics by GC/MSTert-Butyl Alcohol Tertiary-Amyl Methyl Ether
Surrogate (s) Pentaf luorobenzene FI uorobenzene 4 - Bromofluorobenzene
Recovery 83. 88. 109
PARs by GC/MS-SIM - Westborough Lab
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
L0903860MAl - 1
RESULT UNITS RDL REF METHOD DATE PREP ANAL
- Westborough Lab cont' 100NDND ug/lug/l 20.
624 0331 10:20 TT
Acenaphthene 2 - ChloronaphthaleneFluoranthene Naphthalene Benzo (a) anthracene Benzo (a) pyrene Benzo (b) fluoranthene Benzo (k) fluoranthene Chrysene Acenaphthylene Anthracene Benzo (ghi) perylene FI uorene Phenanthrene Dibenzo (a, h) anthracene lndeno (1, 2, 3 - cd) Pyrene Pyrene
Methylnaphthalene 2 - Methylnaphthalene
Surrogate (s) Ni trobenzene -
Fluorobiphenyl Terphenyl- d14
Polychlorinated Biphenyls by Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260
Surrogate (s) Tetrachloro- xylene
Decachlorobiphenyl
ug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l
Recovery 56. 49. 60.
GC - Westborough Lab ug/lug/lug/lug/lug/lug/lug/l
Recovery 84. 114
QCCri teria 80 -12 0
80- 120 80- 120
8270C 0403 01:39 0405 08:42 HL
QC Criteria 23- 120 43- 120 33 - 12 0
608 0402 03:03 0403 15:54 JB
258 258 258 258 258 258 258
QC Criteria 30- 150 30-150
Comments: Complete list of References and Glossary of Terms found in Addendum
04060916: 03 Page 5 of 24
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
MA:M- MA086 NH: 2003 CT: PH- 0574 ME:MA0086 RI :LA000065 NY: 11148 NJ:MA935 Army:USACE
Laboratory Sample Number: L0903860MAl - 8
Sample Matrix: WATER
Condition of Sample: Satisfactory
Number & Type of Containers: Amber
PARATER RESULT
General Chemistry - Westborough Lab
Solids, Total SuspendedCyanide, Total Chlorine, Total Residual TPH Phenolics, Total Chromium, Hexavalent
Total Metals - westporough Lab
Antimony, Total Arsenic, Total Cadmium, Total Chromium, Total Copper, Total 0014 Iron, Total Lead, Total Mercury, Total Nickel, Total 0030 Selenium, Total 001 Silver, Total Zinc, Total 0202
Dissolved Metals - Westborough Lab
Antimony , Dissolved Arsenic , Dissolved Cadmium, Dissolved Chromium, Dissolved Copper, Dissolved 0013 Iron, Dissolved Lead, Dissolved Mercury, Dissolved Nickel, Dissolved 0028 Selenium, Dissolved Silver, Dissolved Zinc, Dissolved 0193
plastic,
UNITS
mg/l mg/l mg/l mg/l mg/l mg/l
mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l
mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l
Date Collected: Date Received Date Reported
Field Prep:
Vial
RDL REF METHOD
30 2540D
005 30 4500CN
30 4500CL
74 1664A
420.
010 30 3500CR
0005 6020
0005 6020
0002 6020
0005 6020
0005 6020
19 200.
0005 6020
0002 245.
0005 6020
001 6020
0004 6020
0050 6020
0005 6020
0005 6020
0002 6020
0005 6020
0005 6020
601 DE
0005 6020
0002 7470A
0005 6020
001 6020
0004 6020
0050 6020
30- MA- 2009 13: 00
30- MA- 2009 06 - APR - 2 0 0 9
None
DATE PREP ANAL
0402 10: 40 DW
0403 11:00 0403 16:53 DD
0330 20:00 JO
0401 18:00 0402 00:30 JO
0402 16: 09 TH
0331 01: 30 0331 01: 30 . JT
0401 11:20 0402 16:26 EM
0401 11:20 0402 16:26 EM
0401 11: 20 0402 16: 26 EM
0401 11: 20 0402 16: 26 EM
0401 11: 20 0402 16: 26 EM
0401 11:20 0402 13:38 MG
0401 11: 20 0402 16: 26 EM
0331 12: 30 0401 10: 35 EZ
0401 11:20 0402 16:26 EM
0401 11:20 0402 16:26 EM
0401 11:20 0402 16:26 EM
0401 11:20 0402 16:26 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0403 11:20 0406 10:07 MG
0401 11:20 0402 18:47 EM
0331 12: 30 0401 11: 44 EZ
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
0401 11:20 0402 18:47 EM
Comments: Complete list of References and Glossary of Terms found in Addendum I
04060916: 03 Page 6 of 24
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
Laboratory sample Number: L0903860MAl - 8
PARATER RESULT UNITS
Pesticides by GC - Westborough LabDibromoethane ug/l
Volatile Organics by GC/MS - Westborough Lab Methylene chloride ug/l
Dichloroethane ug/lChloroform ug/lCarbon tetrachloride ug/l
2 -Dichloropropane ug/libromochl orome thane ug/l
Trichloroethane ug/l2 - Chloroethyl vinyl ether ug/lTe t r achl oroe thene ug/lChlorobenzene ug/lTrichlorof I uoromethane ug/l
Dichloroethane ug/lTrichloroethane ug/l
Bromodichloromethane ug/ltrans- , 3 - Dichloropropene ug/lcis- Dichloropropene ug/lBromoform ug/l1, 1, 2, 2 - Tetrachloroethane ug/lBenzene ug/lTol uene ug/lEthylbenzene ug/lChloromethane ug/lBromomethane ug/lVinyl chloride ug/lChloroethane ug/l
Dichloroethene ug/ltrans- Dichloroethene ug/lcis- Dichloroethene ug/lTr i chI oroe thene 1. 2 ug/l
2 - Dichlorobenzene ug/lDichlorobenzene ug/lDichlorobenzene ug/l
p/m-Xylene ug/lxylene ug/l
Xylene (Total) ug/lStyrene ug/lAcetone ug/lCarbon disulfide ug/l2 - Bu tanone ug/lVinyl acetate ug/l4 - Methyl- 2 - pentanone ug/l2 - Hexanone ug/lAcrolein ug/lAcryloni trile ug/lMethyl tert butyl ether ug/l
Dioxane ug/l
RDL REF METHOD DATE PREP ANAL
14 504. 0406 09:30 0406 13:16 JB
020
624 0331 10:54 TT
1. 5
1. 5
1. 0
1. 0
1. 5
10. 1. 5
1. 5
1. 0
1.5 1. 5
1. 0
1. 0
1. 0
1. 0
1. 0
10.
1. 0
1. 5
1. 0
1. 0
1. 0
1. 0
10.
10. 20. 10. 10.
10. 20. 2000
Comments: Complete list of References and Glossary of Terms found in Addendum I
04060916: 03 Page 7 of 24
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
Laboratory Sample Number: L0903860MAl - 8
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
Volatile Organics by GC/MS - westborough Lab cont' 624 0331. 10:54 TT
Tert-Butyl Alcohol 100 Tertiary-Amyl Methyl Ether
NONO ug/lug/l 20.
Surrogate (s) Recovery Pentaf 1 uorobenzene 81. 0
Fl uorobenzene 88. 4 - Bromof 1 uorobenzene 113
PAHs by GC/MS-SlM - Westborough Lab Acenaphthene 2 - ChloronaphthaleneFluoranthene Naphthalene Benzo (a) anthracene Benzo (a) pyrene Benzo (b) fluoranthene Benzo (k) fluoranthene Chrysene Acenaphthylene Anthracene Benzo (ghi) perylene Fluorene Phenanthrene Dibenzo (a, h) anthracene lndeno (1 2, 3 - cd) Pyrene Pyrene
Methylnaphthalene 2 - Methylnaphthalene
Surrogate (s) Ni trobenzene2 - Fl uorobiphenyl 4 - Terphenyl- d14
Polychlorinated Biphenyls by Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260
Surrogate (s) 6 - Tetrachloro-m- xylene
Decachlorobiphenyl
ug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l
Recovery 55. 43. 66.
GC - westborough Labug/lug/lug/lug/lug/lug/lug/l
Recovery 75. 119
QC Criteria 80- 120 80- 120 80 - 12 0
8270C 0403 01: 3 0405 O : 11 HL
QC Criteria 23- 120 43- 120 33 - 12 0
608 0402 03: 03 0403 15: 41 JB
258 258 258 258 258 258 258
QC Criteria 30- 150 30- 150
Comments: Complete list of References and Glossary of Terms found in Addendum I
04060 16: 03 Page 8 of 24
******* *******
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
MA:M-MA086 NH: 2003 CT: PH- 0574 ME :MA0086 RI: LA000065 NY: 11148 NJ:MA935 Army:USACE
Laboratory Sample Number: L0903860 Date Collected: 30- MA- 2009 00: 00 TRIP BLAK Date Received 30-MA- 2009
Sample Matrix: WATER Date Reported 06-APR- 2009
Condition of Sample: Satisfactory Field Prep: None
Number & Type of Containers: 3 - Vial
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
THIS SAMPLE IS ON HOLD
Comments: Complete list of References and Glossary of Terms found in Addendum
04060916: 03 Page 9 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH DUPLICATE ANALYSIS
Laboratory Job Numer: L0903860
Parameter Val ue 1 Value 2 Units RPD RPD Limits
General Chemistry - Westborough Lab for sample (s) 01- 02 (L0903928- 01, WG357511
Solids, Total Suspended 41 44 mg/l General Chemistry - Westborough Lab for sample (s) 01- 02 (L0903860-01, WG357788
Cyanide, Total ND NO mg/l NC General Chemistry - Westborough Lab for sample(s) 01- 02 (L0903860- 02, WG357226
Chlorine, Total Residual ND NO mg/l General Chemistry - westborough Lab for sample (s) 01- 02 (L0903860- 01, WG357485-4)ND NO mg/l NCTPH
Gene:tal Chemistry - westborough Lab for sample (s) 01- 02 (L0903857- 0l, WG357624Phenolics, Total ND NO mg/l NC
General Chemistry - Westborough Lab for sample(s) 01- 02 (L0903860- 01, WG357230
Chromium, Hexavalent 0.021 0. 021 mg/l Total Metals - Westborough Lab for sampleNO(8) 01-02
mg /1
(L0903 857 - 01, WG357535- 3)
Antimony, Total NC Arseni c , Total 0118 NO0112 mg/l
mg /lCadmi urn, Total NC Chromium, Total 0007 0007 mg/l Copper, Total 0042 NO0044 mg/l
mg /1Lead, Total NC Nickel, Total 0053 Selenium, Total 026 NO
0054028 mg/lmg/l mg /1 NCSilver, Total
Zinc, Total 0219 o . 021 7 mg /l
Total Metals - westborough Lab for sample (s) 01- 02 (L0903857-'01, WG357534Iron, Total 21 23 mg/l
Total Metals - Westborough Lab for sample (s) 01- 02 (L0903857- 01, WG357308
Mercury, Total ND NO mg/l Dissolved Metals - westborough Lab for sample(s) 01- 02 (L0903887-06, WG357536
Cadmium, Dissolved NCLead, Dissolved NDND NONO mg/lmg/l NC Dissolved Metals - Westborough Lab for sample(s) 01- 02 (L0903860- 02, WG357758-3)Dissolved ND NO mg/l NCIron,
Dissolved Metals - Westborough Lab for sample(s) 01- 02 (L0903887- 01, WG357310
Mercury, Dissolved ND NO mg/l NC
04060916: 03 Page 10 of 24
ALPHA ANALYTICAL QUALITY ASSURACE BATCH DUPLICATE ANALYSIS
Laboratory Job Numer: L0903860 Continued
Parameter Val ue 1 Value 2 Units RPD RPD Limits
volatile Organi9s by GCfMS Methylene chloride
Dichloroethane Chloroform Carbon tetrachloride
Dichloropropane Dibromochloromethane
1, 2- Trichloroethane Chloroethylvinyl ether
Te t rachl oroe thene Chlorobenzene Tr i chlorof 1 uoromethane
2 - Dichloroethane , I- Trichloroethane
Bromodichloromethane trans- I, 3 - Dichloropropenecis- Dichloropropene Bromoform
2 -Tetrachloroethane Benz ene Tol uene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane
Dichloroethene trans- I, 2 -Dichloroethene cis- Dichloroethene Tr i chI oroe thene
2 - Dichlorobenzene 3 - Dichlorobenzene
Dichlorobenzene pfm- Xylene o-xyleneXylene (Total) Styrene Acetone Carbon disulfide 2 - Bu tanone Vinyl acetate 4 -Methyl- 2 -pentanone 2 - Hexanone Acrolein Acrylonitrile Methyl tert butyl ether
Dioxane Tert-Butyl AlcoholTertiary-Amyl Methyl Ether
- Westborough Lab for sample (s)ugflugflugflugflugflugflugflug/lugflugflug/lugflugflugflugflugflugflugflugflugflugflugflugflugfl
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND ugfl
7 3. ugfl
1.8 1.9
ugflugflugflugflugflugflugfl
NDNDNDNDNDNDND ugflugflug/l33 ug/lugflugflugflug/lug/lugflugflugfl
NDNDNDNDNDNDNDNDNDNDND ugflugflugfl
01- 02 (L0903 860- 01, WG357153
04060916: 03 Page 11 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH DUPLICATE ANALYSIS
Laboratory Job Numer: L0903860 Continued
RPD Limi tsParameter Val ue 1 Val ue 2 uni ts RPD
Volatile organics by GC/MS - Westborough Lab for sample (s) 01- 02 (L0903860-01, WG357153
Surrogate (s) Recovery QC Criteria 83. 80. 80- 120Pen taf 1 uorobenzene
80 - 12 0Fl uorobenzene 88. 85. 80 - 12 04 - Bromof 1 uorobenzene 109 109
Polychlorinated Biphenyls by GC - Westborougl1 Lab for sample (s) 01- (L0903857 01, WG357506
Aroclor 1016 ug/lAroclor 1221 ug/lAroclor 1232 ug/lAroclor 1242 ug/lAroclor 1248 ug/lAroclor 1254 ug/lAroclor 1260 ug/l
Surrogate (s) Recovery QC Criteria
Tetrachloro-m- xylene 58. 82. 30 - 15 0
30- 150Decachlorobiphenyl 84. 84.
04060916: 03 Page 12 of 24
ALPHA ANALYTICAL QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0903860
Parameter % Recovery QC Cri teria
General Chemistry - Westborough Lab LCS for sample (s) 01- 02 (WG357788Cyanide, Total 103 80- 120
General Chemistry - Westborough Lab LCS for sample (s) 01- 02 (WG357226Chlorine / Total Residual 101
General Chemistry - Westborough Lab LCS for sample (s) 01-02 (WG357485TPH 80 64- 132
General Chemistry - Westborough Lab LCS for sample (s) 01-02 (WG357624-2)Phenolics, Total 94 82 - 111
General Chemistry - Westborough Lab LCS for sample (s) 01-02 (WG357230-2)Chromium, Hexavalent 98 85- 115
Total Metals - Westborough LabLCS for sample (s) 01- 02 (WG357535Antimony / Total 80 - 12 0 Arseni c , Total 80 -12 0
Cadmium, ' Total 102 80- 120 Chromium, Total 102 80- 120 Copper , Total 101 80 - 12 0 Lead , Total 101 80-120 Nickel Total 100 80 - 120 Selenium, Total 80- 120 Silver Total 104 80- 120 zinc , Total 106 80 - 12 0
Total Metals - Westborough Lab LCS for saTDple (s) 01- 02 (WG357534TotalIron 98 85- 115
Total Metals - WestboroughLab LCS for sample (s) 01- 02 (WG357308Mercury, Total 103
Dissolved Metals - Westborough Lab LCS for sample (s) 01- 02 (WG357536-2 )Antimony, Dissolved Arsenic / Dissolved Cadmium, Dissolved Chromium, Dissolved Copper , Dissolved
109 80-114 80-117 80-
119 80-118 80-116 80-115 80-115 80-
108 80-107 80-
120
120120
120120120
120120120120
Lead, Dissolved Nickel, Dissolved Selenium, Dissolved Silver, Dissolved Zinc / Dissolved
Dissolved Metals - Westborough Lab LCS for sample (s) 01- 02 (WG357758Iron, Dissolved 96 80- 120
04060916: 03 Page 13 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0903860 Continued
Parameter % Recovery QC Cri teria
Dissolved Metals -' westborough Lab LCS for sample ($) 01- 02 (WG357310-2)Mercury, Dissolved 111 70- 130
Pesticides by GC - Westborough Lab LCS for sample (s) 01- 02 (WG357920Dibromoethane 86 70- 130 Dibromo-3-chloropropane 100 70- 130
Volatile organics by GC/MS Westborough Lab LCS for sample (s) 01- 02 (WG357153Methylene chloride 119 221
Dichloroethane 128 59- 155 Chloroform 125 51- 138 Carbon tetrachloride 152 70- 140
Dichloropropane 124 210 ibromochl oromethane 141 53- 149
1, 1 , 2- Trichloroethane 121 52 - 150 2 - Chloroethyl vinyl ether 305 Tetrachloroethene 113 64 - 148 Chlorobenzene 37- 160 Tri chlorof 1 uoromethane 131 17- 181
Dichloroethane . 154 49- 155 Trichloroethane 157 52 - 162
Bromodi chloromethane 152 35- 155 trans - 3 -Dichloropropene 124 17- 183 cis- Dichloropropene 118 227 Bromoform 145 45- 169
Tetrachloroethane 108 46- 157 Benzene 121 37- 151 Toluene 114 47- 150 Ethylbenzene 112 37- 162 Chloromethane 132 273 Bromomethane 242 Vinyl chloride 121 251 Chloroethane 108 14 - 230
Dichloroethene 117 234 trans- 1, 2 - Dichloroethene 113 54 - 156 cis- Dichloroethene 60- 140 Trichloroethene 106 71- 157
Dichlorobenzene 109 18 - 190 3 -Dichlorobenzene 102 59- 156 4 -Dichlorobenzene 113 18- 190
p/m- Xylene 116 40- 160 Xylene 114 40- 160
XYLENE (TOTAL) 116 40- 160 Styrene 105 40- 160 Acetone 145 40- 160
40- 160Carbon disulfide 40- 160Butanone 105
Vinyl acetate 40- 160 4 - Methyl- 2 -pentanone 113 40- 160
04060916: 03 Page 14 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0903860 Continued
Parameter % Recovery QC Criteria
Volatile Organics by GC!MS - Westborough Lab LCS for sample (s) 02 (WG357153
2 - Hexanone 134 40- 160 Acrolein 40- 160 Acryloni trile 106 40- 160
Surrogate (s) Pentaf I uorobenzene 80- 120 FI uorobenzene 80- 120 4 - Bromof I uorobenzene 102 80- 120
Polychlorinateq Biphenyls by GC - Westborough Lab LCS for sample (s) 01- 02 (WG357506Aroclor 1016 79 40- 126Aroclor 1260 89 40- 127
Surrogate (s)Tetrachloro-m-xylene 30- 150
Deca chI orobi pheny I 110 30- 150
General Chemistry - Westborough Lab SPIKE fo+ s mple (s) 01-02 (L0903860- 01, WG357788Cyanide, Total 106 80- 120
General Chemist+y - Westborough Lab SPIKE for sample (s) 01-02 (L0903860- 02, WG357485TPH 83 64 - 13 2
General Chemistry - Westborough Lab SPIKE for sample (s) 01-02 (L0903857- , WG357624~
Phenolics, Total 96 77- 124
General Chemistry - westborough Lab SPIKE for sample(s) 01- 02 (L0903860- 02, WG357230
Chromium, Hexavalent 100 85- 115
Total Metals - westborougn Lab SPIKE for sample (s) 01- 02 (L0903857 - 01, WG357535Antimony, Total 108 80- 120 Arseni c / Total 115 80- 120 Cadmium, Total 118 80- 120 Chromium, Total 107 80- 120 Lead, Total 112 80- 120 Nickel/ Total 100 80- 120 Selenium, Total 106 80 - 12 0
Silver, Total 104 80- 120 Zinc / Total 103 80- 120
Total Metals - Westborough Lab SPIKE for sample (s) 01- 02 (L0903857- 01, WG357534Iron, Total 200 75- 125
Total Metals, - Westborough Lab SPIKE for sample (s) 01-02 (L0903857-01, WG357308-4)Mercury, Total
04060916: 03 Page 15 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0903860 Continued
Parameter % Recovery QC Criteria
Dissol ved Metals - Westborough Lab SPIKE. for sample (s) 01- 02 (L0903887-06, WG357536-4) Antimony, Dissolved Arsenic, Dissolved 104
80- 120 80- 120
Cadmium , Dissolved 111 80- 120 Chromium, Dissolved 105 80- 120 Copper, Dissolved 105 80- 120 Lead, Dissolved 104 80 - 12 0
Nickel , Dissolved 103 80- 120 Selenium, Dissolved Silver , Dissolved
104 104
80- 120 80- 120
Zinc, Dissolved 110 80- 120
Dissolved Metals - Westborough Lab SPIKE: for sample(s) 01- 02 (L0903860- 02, WG357758Iron, Dissolved 94 75- 125
ab SPIKE for sample (s) 01-02 (L0903887-01, WG357310Dissolved Metals - WestboroughMercury, Dissolved 124 70- 130
Pesticides by GC - Westborough Lab SPIKE for sample(s) 01-02 (L0903857-01, WG357920
Dibromoethane 87 70- 130 Dibromo- 3-chloropropane' 96 70- 130
Volatile Qrganics by GC/MS - Westborough Lab SPIKE Methylene chloride 111
Dichloroethane 118 Chloroform 121 Carbon tetrachloride 152
2 - Dichloropropane 117 Dibromochloromethane 134
2 - Trichloroethane 119 2 - Chloroethyl vinyl ether Tetrachloroethene 126 Chlorobenzene Trichlorof I uoromethane 147
, 1 , 2 - Di chloroethane 151 Trichloroethane 160
Bromodi chI orome thane 147 trans- Dichloropropene 128 cis- 1, 3 - Dichloropropene 114 Bromoform 142
2 - Tetrachloroethane 104 Benzene 120 Toluene 113 Ethylbenzene 113 Chloromethane 127 Bromomethane Vinyl chloride 121 Chloroethane 100
Dichloroethene 123
for sample (s) 221
59 - 155 51- 138 70- 140
210 53- 149 52- 150
305 64- 148 37- 160 17- 181 49- 155 52 - 162 35- 155 17- 183
227 45- 169 46- 157 35- 151 47- 150 37- 162
273 242 251
14- 230 234
01- 02 (L0903755- 01, WG357153
04060916: 03 Page 16 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0903860
Parameter
Volatile Organics by GCjMS trans- Dichloroethene 119 54- 156 cis- I, 2 -Dichloroethene 104 60- 140 Trichloroethene 121 71- 157
2 - Dichlorobenzene 3 -Dichlorobenzene 109 59- 156
Dichlorobenzene 118 18- 190 pjm- xylene
Xylene 109 40- 160 114 40- 160XYLENE (TOTAL)
Styrene 106 40- 160 40- 160Acetone 142
Carbon disulfide 110 40- 160 2 - Bu tanone
2 - Hexanone 123 40- 160 Acrolein Acrylonitrile 101 40- 160
Surrogate (s) Pen t a f 1 uorobenzene Fl uorobenzene 4 - Bromof 1 uorobenzene
Continued
% Recovery QC Cri teria
- Wes tborough Lab SPIKE for sample (s) 01- 02 (L0903 755 - 01, WG3 57153
116 18 - 190
116 40- 160
40- 160 40- 160
40- 160
Vinyl acetate 4 - Methyl- 2 -pentanone 102 40- 160
80- 120 80- 120 80- 120
Polychlorinated Biphenyls by GC - westborough Lab SPAroclor 1016 76Aroclor 1260 88 IKE for sample (s) 01- 02 (L0903857- 01, WG35'
40- 12640- 127
Surrogate (s)Tetrachloro-m-xylene 30- 150
Decachlorobiphenyl 30- 150
04060916,03 Page 17 of 24
ALPHA ANALYTICAL QUALITY ASSURACE BATCH LCS/LCSD ANALYSIS
Laboratory Job Numer: L0903860.
Parameter LCS LCSD RPD RPD Limi t Limits
PAHs by GCjMS- SIM Westborough Lab for sample (s) 01- (WG357679- WG357679Acenaphthene 40- 140
Fluoranthene 40 - 14 0 Anthracene 40 - 14 0
2 - Chloronaphthalene 40- 140
Pyrene 40- 140
Surrogate (s) Nitrobenzene- 23- 120 2 - Fl uorobiphenyl 43- 120
Terphenyl- d14 33 - 12 0
04060916: 03 Page 18 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0903860
DATEPARATER RESULT UNITS RDL REF METHOD PREP ANAL
Blank Analysis for sample (s) 01- 02 (WG357511
General Chemistry - Westborough Lab
0402 10: 40 DWmg/l 30 2540DSolids, Total Suspended
Slank Analysis for sample (s) 01- 02 (WG357788
General Chemistry - westborough Lab
mg/l 005 30 4500CN- 040311:00040316,41 DDCyanide, Total
Blank Analysi$ for sample(s) 01- 02 (WG357226
General Chemistry - westborough Lab
30 4500CL- 0330 20,00 JOChlorine, Total Residual mg/l
Blank Analysis for sample (s) 01- 02 (WG357485
General Chemistry - westborough Lab
TPH mg/l 74 1664A 0401 18:00 0402 00,30 JO
Blank Analysis for sample (s) 01- 02 (WG357624
General Chemistry - Westborough Lab
4 420. 0402 16: 04 THPhenol i c s , Total mg/l
Blank Analysis for sample(s) 01- 02 (WG357230
General Chemistry - westborough Lab
mg/l 010 30 3500CR- 0331 01:30 0331 01,30 JTChromi urn, Hexavalent
Blank Analysis for sample (s) 01- 02 (WG357535
Total Metals - westborough Lab
0401 11: 20 0402 15: 48 BMAntimony, Total mg/l 0005 6020
mg/l 0005 6020 0401 11:20 0402 15:48 BMArsenic, Total mg/l 0002 6020 0401 11:20 0402 15:48 BMCadmium, Total
0005 6020 0401 11: 20 0402 15:48 BMChromium, Total mg/l mg/l 0005 6020 0401 11,20 0402 15:48 BMCopper, Total
0401 11: 20 0402 15:48 BMLead, Total mg/l 0005 6020
mg/l 0005 6020 0401 11:20 0402 15:48 BMNickel, Total 6020 0401 11: 20 0402 15:48 BMSelenium, Total mg/l 001
mg/l 0004 6020 0401 11:20 0402 15:48 BMSilver, Total 0050 6020 0401 11:20 0402 15,48 BMzinc, Total mg/l
04060916: 03 Page 19 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0903860 Continued
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
Blank Analysis for sample(s) 01-02 (WG357534Total Metals - Westborough Lab 19 200.
Iron, Total mg/l 19 200. 0401 11:20 0402 13:18 MG
Blank Analysis for sample (s) 01- 02 (WG357308Total Metals - Westborough Lab
Mercury, Total mg/l 0002 3 245. 0331 12: 30 0401 10: 21 EZ
Blank A,alysis for sample(s) 01-02 (WG357536-1) Dissol ved Metals - westborough Lab
Antimony , Dissolved mg/l 0005 6020 0401 11:20 0402 18,30 BM
Arsenic , Dissolved mg/l 0005 6020 0401 11: 20 0402 18:30 BM
Cadmium, Dissolved mg/l 0002 6020 0401 11:20 0402 18,30 BM
Chromi urn, Dissolved mg/l 0005 6020 0401 11:20 0402 18:30 BM
Copper , Dissolved mg/l 0005 6020 0401 11: 20 0402 18,30 BM
Lead, Dissolved mg/l 0005 6020 0401 11:20 0402 18:30 BM
Nickel , Dissolved mg/l 0005 6020 0401 11:20 0402 18:30 BM
Selenium, Dissolved mg/l 001 6020 0401 11:20 0402 18:30 BM
Silver , Dissolved mg/l 0004 6020 0401 11:20 0402 18:30 BM
zinc, Dissolved mg/l 0050 6020 0401 11,20 0402 18:30 BM
Blank Analysis for sample (s) 01- 02 (WG35775B-1) Dissolved Metals - WestboroughLab
Iron, Dissolved mg/l 6010B 0403 11:20 0406 09,58 MG
Blank Analysis for sample ($) 01- 02 (WG357310Dissolved Metals Westborough Lab
Mercury, Dissolved mg/l 0002 7470A 0331 12: 30 0401 11: 31 EZ
Blank Analysis for sample(s) Oh02 (WG357920Pesticides by GC - Westborough Lab 14 504. 0406 09: 30 0406 12: 12 JB
020 2 - Dibromo- 3 - chloropropane ND ug/l 020 Dibromoethane ug/l
Blank Analysis for sample (s) 01- (WG357153Volatile Organics by GC/MS - Westborough Lab 624 0331 08:14 TT
Methylene chloride ug/l 1. 5 Dichloroethane ug/l 1. 5 Chloroform ug/l
Carbon tetrachloride ug/lDichloropropane ug/l 1. 0
1. 0 Dibromochloromethane ug /1
1. 5 TriChloroethane
NDNDNDNDNDNDND ug/l
04060916: 03 Page 20 of 24
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0903860 Continued
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
Blank Analysis for sample (s) 01-02 (WG357153 I d 624Volatile Organics by GC/MS - Westborough Lab contug/l 10.Chloroethylvinyl etherTetrachloroethene ug/l 1.Chlorobenzene ug/l 3.Trichlorofluoromethane ug/l 5.Dichloroethane ug/l 1.
Trichloroethane ug/l 2.Bromodichloromethane ug/l 1. trans- Dichloropropene ug/l 1.cis- Dichloropropene ug/l 1.Bromoform ug/l 1.
Tetrachloroethane ug/l 1.ug/l 1.Benzene ug/l 1.TolueneEthylbenzene ug/l 1.Chloromethane ug/l 10.Bromomethane ug/l 5.Vinyl chloride ug/l 2.Chloroethane ug/l 2.Dichloroethene ug/l 1.
trans- Dichloroethene ug/l 1.cis- Dichloroethene ug/l 1.Trichloroethene ug/l 1.
Dichlorobenzene ug/l 5.Dichlorobenzene ug/l 5.Dichlorobenzene ug/l 5.
ug/l 2.p/m-Xylene ug/l 1.o-xylene
Xylene (Total) ug/l 2.ug/l 1.StyreneAcetone ug/l 10.
Carbon disulfide ug/l 5.Butanone ug/l 10.Vinyl acetate ug /1 20. Methyl- 2 -pentanoneHexanone ug/lug/l 10.
ug/l 8.Acrolein 10.
AcrylonitrileMethyl tert butyl ether 20.Dioxane
10.
100Tert-Butyl Alcohol 2000
Tertiary-Amyl Methyl Ether
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND ug/lug/lug/lug/lug/l 20.
Surrogate (s) Recovery QC Criteria
Pentaf 1 uorobenzene 89. 80 - 12 0
Fl uorobenzene 89. 80- 120 4 - Bromof 1 uorobenzene 107 80 - 12 0
04060916 :03 Page 21 of 24
0331 08:14 TT
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0903860 Continued
PARATER RESULT UNITS
Blank Analysis for sample (s) 01PAHs by $C/MS- SIM - Westborough LabAcenaphthene ug/l2 - Chloronaphthalene ug/lFluoranthene ug/lNaphthalene ug/lBenzo (a) anthracene ug/lBenzo (a) pyrene ug/lBenzo (b) fluoranthene ug/lBenzo (k) fluoranthene ug/l
ug/lChryseneAcenaphthylene ug/lAnthracene ug/lBenzo (ghi) perylene ug/lFluorenePhenan threne ug/lDibenzo (a, h) anthracene ug/lIndeno ( 1 , 2 , 3 - cd) Pyrene ug/l
ug/lPyrene ug/l
Methylnaphthalene ug/lMethylnaphthalene ug/l
Surroga te ( Recovery Ni trobenzene - 82. 2 - Fluorobiphenyl 62.
Terphenyl- d14 73.
Blank Analysis for sample(s) 01Polychlorinated Biphenyls by GC - Westborough Lab Aroclor 1016 ug /1
Aroclor 1221 ug /1
Aroclor 1232 ug /1
Aroclor 1242 ug /1
Aroclor 1248 ug /1
Aroclor 1254
NDNDNDNDNDNDND ug /1
ug/lAroclor 1260
Surrogate (s) Recovery 6 - Tetrachloro-m-xylene 65.
Decachlorobiphenyl 102
RDL REF METHOD DATE
PREP ANAL
(WG3576798270C 0403 01: 39 0405 07: 14 HL
QC Criteria 23- 120 43- 120 33- 120
(WG357506-1) 608 0402 03: 03 0403 14: 36 JB
250 250 250 250 250 250 250
QC Criteria 30- 150 30- 150
04060916: 03 Page 22 of 24
ALPHA ANALYTICAL ADDENDUM I
REFERENCES
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW
846. Third Edition. Updates I - IlIA, 1997.
Methods for the Determination of Metals in Environmental Samples, Supplement
I. EPA/600/R- 94/111. May 1994.
Methods for Chemical Analysis of Water and Wastes. EPA 600/4- 79- 020. Revised March 1983.
Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater. Appendix A, Part 136, 40 CFR (Code of Federal Regulations)
14. Methods for the Determination of organic Compounds in Finished Drinking Water and Raw Source Water. EPA/600/4- 88/039, Revised July 1991.
19. Inductively Coupled Plasma Atomic Emission Spectrometric Method for Trace Element Analysis of Water and Wastes. Appendix C, Part 136, 40 CFR (Code of Federal Regulations). July 1, 1999 edition.
30. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF.
18th Edition. 1992.
74. Method 1664, Revision A: N-Hexane Extractable Material (HEM; Oil & Grease) and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material) by Extraction and Gravimetry, EPA- 821- 98- 002, February 1999.
04060916: 03 Page 23 of 24
ALPHA ANALYTICAL ADDENDUM I
REFERENCES
GLOSSARY OF TERMS AN SYMBOLS
REF Reference number in which test method may be found. METHOD Method number by which analysis was performed.
Initials of the analyst. Not detected in comparison to the reported detection limit. Not Igni table.
ug / cart Micrograms per Cartridge. The analysis of pH was performed beyond the regulatory- required holding
time of 15 minutes from the time of sample collect ion.
LIMITATION OF LIABILITIES
Alpha Analytical, Inc. performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the . event of an error, the sole and exclusive responsibility of Alpha Analytical, Inc., shall be to re-perform the work at it I S own expense. In no event shall Alpha Analytical, Inc. be held liable for any incidental consequential or special damages, including but not
limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical, Inc.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding times and splitting of samples in the field.
04060916: 03 Page 24 of 24
Certificate/Approval Program Summary Last revised February 18, 2009 - Westboro Facility
The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Certificate/Lab ID : PH-0574.Connecticut Department of Public Health
Inorqanic Parameters : Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Drinking Water
Chlorine , Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium , Beryllium,
Cadmium , Calcium , Chromium , Copper, Iron , Lead, Magnesium, Manganese, Mercury, Molybdenum , Nickel
Potassium , Selenium, Silver, Sodium, Thallium, Vanadium , Zinc, Total Dissolved Solids, Total Organic Carbon, Orqanic Parameters: Haloacetic Acids, Volatile Organics 524.2, TotalTotal Cyanide, Perchlorate.
Trihalomethanes 524.2, 1 , Dibromo-3-chloropropane (DBCP), Ethylene Dibromide (EDB). Wastewater/Non-Potable Water Inorqanic Parameters : Color, pH , Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness , Calcium Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl
Nitrogen , Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium,
Boron , Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium,
Manganese, Mercury, Molybdenum, Nickel , Potassium, Selenium, Silver, Sodium , Strontium , Thallium , Tin,
Titanium , Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids , Total Suspended Solids (non-filterable),
BOD , CBOD, COD , TOC, Total Cyanide , Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Orqanic
Parameters : PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, 2,4-D, 2,4, , 2,4,
TP(Silvex), Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone , Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics.
Inorqanic Parameters : Lead in Paint, pH, Aluminum, Antimony, Arsenic, Barium , Beryllium,Solid Waste/Soil
Boron , Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead ,. Magnesium,
. Manganese, Mercury, Molybdenum , Nickel , Potassium , Selenium, Silver, Sodium, Thallium, Tin , Vanadium , Zinc,
Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), Reactivity. Orqanic Parameters : PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Extractable Petroleum Hydrocarbons (ETPH), Dicamba, 2,4-D, 2,4, T, 2,4, TP(Silvex), Volatile Organics, Acid Extractables (Phenols), 3. Dichlorobenzidine,
Phthalates, Nitrosamines, Nitroaromatics & Cyclic Ketones, PAHs, Haloethers , Chlorinated Hydrocarbons. )
Certificate/Lab ID : MA0086.Maine Department of Human Services
Inorqanic Parameters: SM9215B , 9221 E, 9222B, 9222D , 9223B , EPA 150. , 180. , 300.0, 353.
SM2130B , 2320B, 4500CI- , 4500CN-C, 4500CN-E, 4500F- , 4500H+B,4500N03- , EPA 200.7, EPA 200.Drinking Water
245. 1. Orqanic Parameters : 504. , 524. 2, SM 6251 B. Wastewater/Non-Potable Water Inorqanic Parameters : EPA 120. , 1664A , 350. , 351. , 353. , 410.4, 420.
, 4500CI- , 4500CNLachat 10-107-06- B, SM2320B, 2340B, 2510B, 2540C, 2540D, 426C, 4500CI
, 4500F- , 4500F-C, 4500H+B , 4500Norg- , 4500Norg- , 4500NH3-B, 4500NH3- , 4500NH34500CN4500N03- , 4500P- 5, 4500P-E, 5210B, 5220D , 5310C , EPA 200. 200. 245. 1. Orqanic Parameters: 608,
624.
Certificate/Lab ID : M-MA086. Massachusetts Department of Environmental Protection
Drinking Water Se,TI)Inorqanic Parameters: (EPA 200.8 for: Sb As, Ba, Be, Cd,Cr,Cu, Pb,
(EPA 200.7 for: Ba, Be, Ca,Cd, Cu, Na, Ni) 245. , (300.0 for: Nitrate-N, Nitrite- , Fluoride , Sulfate) , EPA 180. 1, SM2130B , SM4500CI353. 2 for: Nitrate-N, Nitrite-N; SM4500N03-F, 4500F-C, 4500CN
2320B , SM2540C, EPA 150. , SM4500HOrqanic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics) (504. 1 for: 1, Dibromoethane , 1 , Dibromo- Chloropropane), SM6251 B, 314.
Non-Potab/e Water Pb, Se,Ag, TI,Zn)Inorqanic Parameters , (EPA 200. 8 for: AI Sb,As, Be, Cd,
(EPA 200. 7 for: AI Cd, Co, Fe, Mn, Mo, Se,Ag,Sr, Ca, Mg, Na, , SM2510B, 2540C , 2540B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3245. 1, SM4500H, , EPA 120.
BH, (EPA 350. 1 for: Ammonia-N), LACHAT 10-107-06- B for Nitrate- , SM4500N03- , 353.2 for Nitrate
SM4500NH3- Titr, SM4500NH3-BC-NES, EPA 351. , SM4500P-E, 4500P- , 5220D , EPA 410.4, SM
5210B , 5310C, 4500CN-CE, 2540D , 4500CL- , EPA 1664 , SM14 510AC , EPA 420.
Orqanic Parameters : (EPA 624 for Volatile Halocarbons, Volatile Aromatics) (608 for: Chlordane, Aldrin , Dieldrin , DDD , DDE, DDT, Heptachlor, Heptachlor Epoxide , PCB-Water)
600/4-81-045-PCB-Oil
Massachusetts Department of Environmental Protection Certificate/Lab 10 : M-MA086. Drinking Water Microbioloqy Parameters : SM9215B; MF-SM9222B; ENZ. SUB. SM9223; EC-SM9221 E; MF-SM92220; ENZ. SUB. SM9223;
New Hampshire Department of Environmental Services Certificate/Lab 10 : 200307. Drinking Water Inorqanic Parameters : SM6215B, 9222B , 9223B Colilert, EPA 200. , 200.8, 245. , 110. 2, 120. 150. , 300.0, 325. , 314.0, SM4500CN-E, 4500H+B, 4500N03- , 2320B, 2510B, 2540C , 4500F- , 5310C,
2120B, EPA 331.0. Orqanic Parameters : 504. , 524. , SM6251 B. Non-Potab/e Water Inorqanic Parameters : SM92220, 9221B , 9222B , 9221E-EC, EPA 200. , 200. , 245.
245. 2, SW-846 6010B , 6020 , 7196A, 7470A, SM3500-CR-0, EPA 120. , 150. 1, 300.0, 305. 1, 310. , 325.
340. 350. 350. 351. 353. 354. 365. 375.4 , 376. , 405. , 415. , 420. , 425. , 1664A, SW-846 9010, 9030 , 9040B , EPA 160. 160. 160. 3, SM426C, SM2310B, 2540B, 25400 , 4500H+B, 4500NH3-H, 4500NH34500N02- , 4500P- , 4500-S2- , 5210B , 2320B, 2540C, 4500F-C, 5310C , 5540C, LAC HAT 10-117-07LACHAT 10-107-06- , LAC HAT 10-107-04- C, LAC HAT 10-107-04- J, LAC HAT 10-117-07- , SM4500CLE, LACHAT 10-204-00- A, LAC HAT 10-107-06- 0. Orqanic Parameters : SW-846 3005A , 3015A, 3510C,
5030B , 8021B, 8260B, 8270C, 8330 , EPA 624, 625, 608, SW-846 8082, 8081A.) Solid Chemical Materia/s Inorqanic Parameters : SW-846 6010B , 7196A, 7471A, 7. 2, 7.3.4. , 1010, 1030, 9010 , 9012A , 9014, 9030B, 9040, 9045C , 9050C, 1311 , 3005A, 3050B , 3051A. Orqanic Parameters : SW-846 3540C, 3545, 3580A 5030B, 5035 8021B, 8260B, 8270C, 8330, 8151A, 8082, 8081A.
New Jersey Department of Environmental Protection Certificate/Lab 10: MA935. Inorqanic Parameters : SM9222B, 9221 E , 9223B, 9215B, 4500N03-F, 4500F-C, EPA 300.Drinking Water
200. , 2540C, 2320B, 314.0, 331.0, 110. , SM2120B , 2510B, 5310C , EPA 150. , SM4500H- , EPA 200. 245. 2. Orqanic Parameters: 504. , SM6251 B, 524. Non-Potab/e Water Inorqanic Parameters : SM5210B , EPA 410. , SM52200, 4500CI- , EPA 300. , SM2120B SM4500F-BC, EPA 200. 351. , LACHAT 10-107-06- , EPA 353. 2, SM4500N03- , 4500N02-B, EPA 1664A, SM5310B, C or 0, 4500- , EPA 420. , SM4500P-B5+E , 2540B, 2540C, 25400 , EPA 120. 1, SM2510B, SM15 426C, SM9221 CE, 92220, 92218, 9222B, 9215B , 2310B, 2320B, 4500NH3-H, EPA 350.2/. , SM5210B, SW-846 3015 , 6020, 74 70A, 5540C , 4500H- , EPA 200.8, SM3500Cr- , EPA 245. , 245. , SW-846 9040B, 3005A, EPA 6010B , 7196A, SW-846 901 OB , 9030B. Orqanic Parameters : SW-846 8260B, 8270C, 3510C , EPA 608, 624, 625 SW-846 5030B , 8021 B, 8081A, 8082 , 8151A , 8330.
Inorqanic Parameters: SW-846 9040B, 3005A, 6010B, 7196A , 5030B , 9010B 9030B , 1030, 1311 , 3050B, 3051, 7471 A , 9014 , 9012A, 9045C, 9050A , 9065. Orqanic Parameters : SW-846 8021 B, 8081A , 8082 , 8151A , 8330, 8260B , 8270C, 1311 , 3540C, 3545, 3550B, 3580A , 5035L, 5035H.
Solid Chemical Materials
New York Department of Health Certificate/Lab 10: 11148. Inorqanic Parameters: SM9223B , 9222B, 8215B , EPA 200.8, 200. , 245. , SM5310C, EPADrinking Water
314. 331. 0, SM2320B , EPA 300. 325. , 110. , SM2120B, 4500CN- , 4500F-C, EPA 150. , SM4500H4500N03- , 2540C, EPA 120. , SM 251 OB. Orqanic Parameters : EPA 524. , 504. , SM6251 B. Non-Potab/e Water Inorqanic Parameters : SM9221 E, 92220 , 9221 B, 9222B, 9215B, EPA 405. , SM5210B , EPA 410.4, SM52200 , EPA 305. , SM2310B-4a, .EPA 310. , SM2320B , EPA 200. , 300.0, 325.2, LAC HAT 10-11707-1A or B , SM4500CI- , EPA 340. , SM4500F-C, EPA 375.4, SM15 426C, EPA 350. 350. , LAC HAT 10-10706- , SM4500NH3- , EPA 351. , LAC HAT 10-107-06- , EPA 353. , LACHAT 10-107-041-C, SM4500-N030F, EPA 354. 1, SM4500-N02- , EPA 365. , SM4500P-E, EPA 160. 3, SM2540B , EPA 160. , SM2540C , EPA 160. SM25400 , EPA 200.8, EPA 6010B , 6020, EPA 7196A, S\M3500Cr-0, EPA 245. 245. , 7470A, 110. SM2120B, 335. , LACHAT 10-204-00- A, EPA 150. 1, 9040B, SM4500-HB, EPA 1664A, EPA 415. , SM5310C, EPA 420. , SM14 510C , EPA 120. , SM2510B , EPA 376. , SM4500S- , EPA 425. , SM5540C, EPA 3005A,
Orqanic Parameters : EPA 624 , 8260B , 8270C, 625 608, 8081A, 8151A , 8330 , 8082, 8021B, EPA 3510C, 5030B, 9010B, 9030B. 3015.
Inorqanic Parameters : EPA 9040B, 9045C, 1010 , 1 030, SW 846 Ch 7 Sec 7.3, EPA 6010B , 7196A, 7471A, 9012A , 9014 , 9040B , 9045C, 9065, 9050, EPA 1311 , 3005A, 3050B, 3051, 9010B Solid Hazardous Waste
Orqanic Parameters : EPA 8260B , 8270C , 8081A, 8151A, 8330, 8082 , 8021B , 3540C , 3545, 3580, 5030B 5035. 9030B.
CLP Volatile Organics , CLP Inorganics, CLP PCB/Pesticides.Ana/ytical Services Protocol:
Rhode Island Department of Health Certificate/Lab 10 : LA000065. Refer to MA-OEP Certificate for Potable and Non-Potable Water. Refer to NY-OOH Certificate for Potable and Non-Potable Water.
Certificate/Lab 10 : 68-03671. Registered Laboratory.Pennsylvania Department of Environmental Protection
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ALPHA ANALYTICAL
Eight Walkup Drive Westborough, Massachusetts 01581- 1019 (508) 898- 9220 ww. alphalab. com
Army: USACENH:2003 CT:PH- 0574 ME:MA0086 RI:LA000065 NY:11148 NJ: MA9 3 5
CERTIFICATE OF ANALYSIS
MA:M- MA086
L0904364Client: McPhail Associates Laboratory Job Numer:
Address: 2269 Massachusetts Avenue Date Received: 09-APR-2009
Cambridge, MA 02140 Date Reported: 14 - APR- 2 009
Attn: Mr. Ambrose Donovan Delivery Method: Al pha
Project Number: 4860. site: BOSTON RENN CHARTER
SAMPLE LOCATIONCLIENT IDENTIFICATIONALPHA SAMPLE NUER
15 HYDE PARK AVE.MAI- (OW)L090436415 HYDE PARK AVE.MAI- (OW)L0904364
that, based upon my personal inquiry of those responsibleI, the undersigned, attest under the pains and penalties of perjury
is, to the best of my knowledge and belief, accurate andfor obtaining the information, the material contained in this report
complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.
Author"ed by, if/.
Tech al Representatlve
page 1 of 1004140917: 53
ALPHA ANALYTICAL NARRATIVE REPORT
Laboratory Job Numer: L0904364
The samples were received in accordance with the chain of custody and no significant deviations were encountered during preparation or analysis unless otherwise noted below.
04140917,53 Page 2 of 10
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
11148 NJ:MA935 Army:USACEMA:M- MA086 NH: 2003 CT: PH- 0574 ME:MA0086 RI: LA000065 NY:
09: 00 Date Collected: 09 - APR- 200 9 Laboratory Sample Number: L0904364
Date Received 09 - APR- 2 00 9MAl - 1 (OW)
Date Reported 14 - APR- 2 009WATERSample Matrix:
Condition of Sample: Satisfactory Field Prep: None
Amber, Plastic Number & Type of Containers:
DATEUNITS RDL REF METHODRESULTPARATER PREP ANAL
General Chemistry - westborough Lab
0409 23:00 JO30 4500H+11.(H)'
8270C 0410 11:25 0411 14:26 NOwestborough LabSemi volatile organics by GC/MS -Bis (2- Ethylhexyl) phthalate ug/lButyl benzyl phthalate ug/lDi -n-butylphthalate ug/lDi -n-octylphthalate ug/lDiethyl phthalate ug/l
ug/lDimethyl phthalatePentachlorophenol ug/l
Recovery QC CriteriaSurrogate (s) 21- 120
2 - Fl uorophenol 37. 10- 12026.Phenol23- 12061. 0 Ni trobenzene - 43- 120Fluorobiphenyl 62. 10- 12082.2, 4, 6 - Tr ibromophenol
75. 33 - 12 0Terphenyl- d14
Comments: Complete list of References and Glossary of Terms found in Addendum
Page 3 of 1004140917 :.
ALPHA ANALYTICAL CERTIFICATE OF ANALYSIS
MA:M-MA086 NH: 2003 CT: PH- 0574 ME :MA0086 RI: LA000065 NY: 11148 NJ:MA935 Army:USACE
Laboratory Sample Number:
Sample Matrix:
Condi tion Sample:
Number & Type of Containers:
L0904364MAl - 8 (OW)
WATER
Satisfactory
Amber Plastic
Date Collected: 09 - APR-2 009 Date Received 0 9 - APR - 2 0 0 9
Date Reported 14 - APR - 2 0 0 9
Field Prep: None
09: 30
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
General Chemistry - Westborough Lab
(H) 30 4500H+ 0409 23: 00 JO
Semi volatile Organics by GC/MS Bis (2- Ethylhexyl)phthalate NDButyl benzyl phthalateDi -n-butylphthalateDi -n-octylphthalateDiethyl phthalateDimethyl phthalatePentachlorophenol
Westborough Labug/lug/lug/lug/lug/lug/lug/l 10.
8270C 0410 11:25 0411 15:59 NO
Surrogate (s) 2 - Fl uorophenol Phenol-
Recovery 37. 25.
QC Criteria 21- 120 10- 120
Ni trobenzene 61. 0 23- 120 2 - Fl uorobiphenyl 2 , 4, 6 - Tr ibromophenol
60. 74.
43- 120 10- 120
4 - Terphenyl- d14 77. 33- 120
Comments: Complete list of References and Glossary of Terms found in Addendum I
04140917:53 Page 4 of 10
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH DUPLICATE ANALYSIS
Laboratory Job Numer: L0904364
Uni ts RPD RPD Limi tsParameter Val ue 1 Val ue 2
General Chemistry - Westborough Lab for sample(s) 01-02 (L0904359- 05, WG358417(H) 7.1 7. SU
04140917:53 Page 5 of 10
ALPHA ANALYTICAL QUALITY ASSURACE BATCH SPIKE ANALYSES
Laboratory Job Numer: L0904364
Parameter % Recovery QC Cri teria
General Chemistry - Westborough Lab LCS for sample (s) 01-02 (WG358417-1)100 99-101
04140917: 53 Page 6 of 10
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH LCS/LCSD ANALYSIS
Laboratory Job Numer: L0904364
RPD Limit QC LimitsLCS % LCSD % RPDParameter
semi volatile Organics by GC/MS Acenaphthene
4 - Trichlorobenzene 2 - Chloronaphthalene
Dichlorobenzene Dichlorobenzene
4 - Dini trotol uene
2, 6 - Dini trotol uene Fluoranthene 4 - Chlorophenyl phenyl ether n - Ni trosodi -n -propylamine Butyl benzyl phthalate Anthracene Pyrene
Chloro- Cresol 2 - Chlorophenol 2 - Ni trophenol
NitrophenolDinitrophenol
pentachlorophenol Phenol
surrogate (s) 2 - Fl uorophenol Phenol-Nitrobenzene2 - Fl uorobiphenyl
Tribromophenol Terphenyl- d14
- Westborough Lab for sample (s) 017973806865948199867999959578677144507833
(WG358473- 2, WG35847330 46- 11830 39. 40- 14030 40- 14030 36- 97
30 2430 40- 14030 40- 14030 40- 14030 41- 11630 40- 14030 40- 14030 26- 12730 2330 27- 12330 30- 13030 1030 30-30 9- 103
130
30 12- 110
21- 120 10 - 12 0
23 - 12 0 43- 120 10- 120 33 - 120
04140917,53 page 7 of 10
ALPHA ANALYTICAL QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0904364
PARATER RESULT UNITS RDL REF METHOD DATE PREP ANAL
Blank Analysis for sample(s) 01Semivolatile Organics :by GC/MS - Westborough LabAcenaphthene ug /1Benz idine ug /1
Trichlorobenzene ug/lHexachlorobenzene ug/lBis (2- chloroethyl) ether ug/lChloronaphthalene ug/lDichlorobenzene ug/lDichlorobenzene ug/lDichlorobenzene ug/l
3 I -Dichlorobenzidine ug/lDinitrotoluene ug/lDinitrotoluene ug/lAzobenzene ug /1Fluoranthene ug/l Chlorophenyl phenyl ether ug/l Bromophenyl phenyl ether ug/l
. Bis (2-chloroisopropyl) ether ug/lBis (2-chloroethoxy) methane ug/lHexachlorobutadiene
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND ug/lHexachlorocyclopentadiene ND ug/lHexachloroethane ug/lIsophoroneNaphthalene ug/l
ug/lNitrobenzene NDNDNDND ug/l
NitrosoDiPhenylAmine (NDPA) /DPA ND ug/lBis (2- Ethylhexyl) phthalate ug/lButyl benzyl phthalate ug/lDi- butylphthalate ug/lDi-n-octylphthalate ug/lDiethyl phthalate
NDNDNDNDND ug/lDimethyl phthalate Nq ug/l Benzo (a) anthracene ug/lBenzo (a) pyrene ug/l Benzo (b) fluoranthene ug/l Benzo (k) fluoranthene ug/lChrysene ug /1Acenaphthylene ug/lAnthracene ug/l Benzo (ghi) perylene ug/lFluorene ug/lPhenanthrene ug/lDibenzo (a, h) anthracene ug/lIndeno(1, cd)Pyrene ug/lPyrene
ug/l ug /1AnilineChloroaniline
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND ug/l
(WG358473 -1) 8270C 0410 11:25 0411 14:49 ND
50.
50.
10. 30.
15.
20.
04140917: 53 Page 8 of 10
ALPHA ANALYTICAL
QUALITY ASSURACE BATCH BLANK ANALYSIS
Laboratory Job Numer: L0904364 Continued
RESULT UNITS RDL REF METHOD DATEPARATER PREP ANAL
Blank Analysis for sample(s) 01- 02 (WG3584738270C 0410 ,1:25 0411 14:49 NDby GC/MS - Westborough Lab cont I d
Semivolatile Organic$ 1- Methylnaphthalene ug /1 5 . 0
Nitroaniline ug/l 5.3 - Ni troaniline ug /1 5 . 0
Nitroaniline ug /1 7 . 0
Dibenzofuran ug /1 5 . 0
2 - Methylnaphthalene ug /1ug/l 5 . 0 50.n - Ni trosodimethylamine
Trichlorophenol ug / 1 5 . 0
Chloro- Cresol ug /1 5 . 0
2 - Chlorophenol ug /1 6 . 0 10.
4 - Dichlorophenol 10.Dimethylphenol
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND 20.Nitrophenol 10.Nitrophenol 30.4 - Dini trophenol
Dinitro-o-cresol
ug/lug/lug/lug/lug/lug/lug/l 20.10.pentachlorophenol
Phenol ug /1 7 . 0
2 - Methylphenol ug /1 6 . 0
3 - Methylphenol/ 4 -Methylphenol ug /1 6 . 0
Trichlorophenol ug /1 5 . 0
Benzoic Acid ug/lug/l 50.10.Benzyl Alcohol
Carbazole ug /1 5 . 0
NDNDNDNDNDNDNDNDNDND ug/l 50.pyridine
Surrogate (s) Recovery Criteria 21- 120Fluorophenol 33.
22. 10- 120Phenol52. 23- 120Nitrobenzene
43- 1202 - Fl uorobiphenyl 53. 6 -Tribromophenol 60. 10- 120
33 - 120Terphenyl- d14 66.
04140917: 53 Page 9 of 10
ALPHA ANALYTICAL ADDENDUM I
REFERENCES
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW846. Third Edition. Updates I - IlIA, 1997.
30. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992.
GLOSSARY OF TERMS AN SYMBOLS REF Reference number in which test method may be found. METHOD Method number by which analysis was performed.
Initials of the analyst. Not detected in comparison to the reported detection limit. Not Igni table.
ug / cart Micrograms per Cartridge. The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
LIMITATION OF LIABILITIES
Alpha Analytical, Inc. performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical , Inc., shall be to re-perform the work at it I S own expense. In no event shall Alpha Analytical , Inc. be held liable for any incidental consequential or special damages, including but not limited to, damages in any way connected with the use of , interpretation of information or analysis provided by Alpha Analytical, Inc.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation , cooling, containers, sampling procedures, holding times and splitting of samples in the field.
04140917,53 Page 10 of 10
Certificate/Approval Program Summary Last revised February 18, 2009 - Westboro Facility
The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Certificate/Lab ID : PH-0574. Connecticut Department of Public Health
Inorqanic Parameters : Color, pH , Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Drinking Water
Chlorine , Fluoride, Calcium Hardness , Sulfate, Nitrate, Nitrite, Aluminum , Antimony, Arsenic, Barium, Beryllium,
Cadmium , Calcium , Chromium, Copper, Iron , Lead, Magnesium, Manganese, Mercury, Molybdenum , Nickel
Potassium , Selenium, Silver, Sodium , Thallium , Vanadium, Zinc, Total Dissolved Solids, Total Organic Carbon, Haloacetic Acids, Volatile Organics 524. Total
Total Cyanide, Perchlorate. Orqanic Parameters: Dibromo-3-chloropropane (DBCP), Ethylene Dibromide (EDB).Trihalomethanes 524.2, 1 ,
Wastewater/Non-Potable Water Inorqanic Parameters : Color, pH, Conductivity, Acidity, Alkalinity, Chloride , Total
Residual Chlorine, Fluoride, Total Hardness, Calcium Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl
Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium , Beryllium,
Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium
Manganese, Mercury, Molybdenum, Nickel , Potassium, Selenium, Silver, Sodium, Strontium , Thallium , Tin,
filterable),Titanium , Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non- Orqanic BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease.
, 2,4,Parameters: PCBs, Organochlorine Pesticides , Technical Chlordane, Toxaphene, 2,4-D, 2,4,
TP(Silvex), Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics &
Isophorone, Polynuclear Aromatic Hydrocarbons , Haloethers, Chlorinated Hydrocarbons , Volatile Organics.
Inorqanic Parameters : Lead in Paint, pH, Aluminum , Antimony, Arsenic , Barium , Beryllium, Solid Waste/Soil
Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium , Cobalt, Copper, Iron , Lead, Magnesium,
Manganese, Mercury, Molybdenum, Nickel , Potassium, Selenium , Silver, Sodium, Thallium, Tin, Vanadium , Zinc, Orqanic Parameters : PCBs,
Total Cyanide , Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), Reactivity.
Organochlorine Pesticides, Technical Chlordane, Toxaphene, Extractable Petroleum Hydrocarbons (ETPH), Dichlorobenzidine
Dicamba, 2,4-D, 2,4, , 2,4, TP(Silvex), Volatile Organics, Acid Extractables (Phenols), 3. Phthalates, Nitrosamines, Nitroaromatics & Cyclic Ketones, PAHs, Haloethers, Chlorinated Hydrocarbons. )
Certificate/Lab ID : MA0086. Maine Department of Human Services
InorQanic Parameters : SM9215B, 9221 E, 9222B, 9222D, 9223B , EPA 150. , 180. 1, 300.0, 353. Drinking Water
, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B,4500N03-F, EPA 200.7, EPA 200.SM2130B, 2320B , 4500CI245. 1. OrQanic Parameters : 504. , 524. , SM 6251 B.
, 1664A, 350. 1, 351. , 353.2, 410.4 , 420.Wastewater/Non-Potable Water Inorqanic Parameters : EPA 120. Lachat 10-107-06- , SM2320B, 2340B, 2510B, 2540C, 2540D, 426C, 4500CI-D, 4500CI-E, 4500CN
4500CN- , 4500F-B, 4500F-C, 4500H+B , 4500Norg- , 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NH3
, 5210B, 5220D, 5310C, EPA 200. , 200. , 245. 1. Orqanic Parameters: 6084500N03-F, 4500P- 5, 4500P624.
Certificate/Lab ID : M-MA086. Massachusetts Department of Environmental Protection
Drinking Water Be,Cd,Cr, Cu, Pb, Ni, TI)InorQanic Parameters: (EPA 200.8 for: Sb,As,
(EPA 200. 7 for: Ba, Be, Ca,Cd, Cr, Cu, Na, Ni) 245. 1, (300.0 for: Nitrate- , Nitrite-N, Fluoride, Sulfate) , 4500CN- , EPA 180. , SM2130B, SM4500CI353.2 for: Nitrate- , Nitrite-N; SM4500N03- , 4500F
2320B, SM2540C, EPA 150. , SM4500HOrQanic Parameters : (EPA 524.2 for: Trihalomethanes, Volatile Organics) (504. 1 for: 1, Dibromoethane, 1, Dibromo- Chloropropane), SM6251 B , 314.
Non-Potable Water Cd, Cu, Pb, Mn, Se,Ag, Zn)
Inorqanic Parameters , (EPA 200. 8 for: AI Sb,As, Ca, Mg, Na,
(EPA 200. 7 for: AI,Sb,As, Be, Cr,Co, Se,Ag,
245. , SM4500H, , EPA 120. 1, SM2510B, 2540C , 2540B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3B for Nitrate-N, SM4500N03- , 353.2 for Nitrate
, (EPA 350. 1 for: Ammonia-N), LAC HAT 10-107-06, SM4500P-E, 4500P- , 5220D , EPA 410.4 , SM
SM4500NH3- Titr, SM4500NH3-BC-NES, EPA 351. , 2540D, 4500CL- , EPA 1664, SM14 510AC, EPA 420.5210B, 5310C, 4500CN
OrQanic Parameters : (EPA 624 for Volatile Halocarbons, Volatile Aromatics) (608 for: Chlordane, Aldrin , Dieldrin , DDD, DDE , DDT, Heptachlor, Heptachlor Epoxide, PCB-Water)
600/4-81-045-PCB-Oil
Massachusetts Department of Environmental Protection Certificate/Lab ID : M-MA086. Drinking Water Microbioloqy Parameters : SM9215B; MF-SM9222B; ENZ. SUB. SM9223; EC-SM9221 E; MF-SM92220; ENZ. SUB. SM9223;
New Hampshire Department of Environmental Services Certificate/Lab 10 : 200307. Drinking Water Inorqanic Parameters : SM6215B, 9222B , 9223B Colilert, EPA 200. , 200.8, 245. , 110. , 120. 150. , 300. , 325. , 314. , SM4500CN- , 4500H+B, 4500N03- , 2320B, 2510B , 2540C, 4500F- , 5310C, 2120B , EPA 331.0. Orqanic Parameters : 504. , 524. , SM6251 B. Non-Potab/e Water Inorqanic Parameters : SM92220 , 9221B , 9222B, 9221E- , EPA 200. , 200. , 245.
245. , SW-846 6010B , 6020, 7196A, 7470A, SM3500-CR- , EPA 120. , 150. , 300. , 305. 1, 310. , 325.
340. 350. 350. 351. 353. 354. 365. 375.4 , 376. 405. 415. 420. 425. , 1664A, SW-846 9010 9030 , 9040B, EPA 160. 1, 160. , 160. 3, SM426C, SM2310B , 2540B , 25400 , 4500H+B, 4500NH3- , 4500NH34500N02- , 4500P-E, 4500-S2- , 5210B, 2320B, 2540C, 4500F-C, 5310C, 5540C , LAC HAT 10-117-07LAC HAT 10-107-06- , LAC HAT 10-107-04- C, LAC HAT 10-107-04- J, LACHAT 10-117-07-1-A, SM4500CL, LAC HAT 10-204-00- LACHAT 10-107-06- 0. Orqanic Parameters : SW-846 3005A, 3015A, 3510C
5030B , 8021 B , 8260B, 8270C , 8330, EPA 624 , 625 , 608 , SW-846 8082 8081 A. Solid Chemical Materia/s Inorqanic Parameters : SW-846 6010B, 7196A, 7471A, 7. , 7.3.4. , 1010, 1030, 9010, 9012A, 9014 , 9030B , 9040, 9045C, 9050C , 1311 , 3005A, 3050B , 3051 A. Orqanic Parameters : SW-846 3540C, 3545, 3580A 5030B, 5035, 8021B, 8260B, 8270C 8330, 8151A, 8082, 8081A.
New Jersey Department of Environmental Protection Certificate/Lab 10 : MA935. Drinking Water Inorqanic Parameters : SM9222B, 9221 E , 9223B, 9215B, 4500N03- , 4500F- , EPA 300. 200. , 2540C, 2320B, 314. , 331.0, 110. , SM2120B, 2510B , 5310C , EPA 150. , SM4500H- , EPA 200. 245. 2. Orqanic Parameters : 504. , SM6251 B , 524. Non-Potable Water Inorqanic Parameters : SM5210B, EPA 410. , SM52200, 4500CI- , EPA 300.0, SM2120B SM4500F- , EPA 200. 351. , LAC HAT 10-107-06- , EPA 353. , SM4500N03- , 4500N02- , EPA 1664A SM5310B, Cor 0 , 4500- , EPA 420. , SM4500P-B5+E , 2540B, 2540C , 25400, EPA 120. , SM2510B, SM15 426C , SM9221CE, 92220 , 9221B, 9222B, 9215B , 2310B, 23208, 4500NH3- , EPA350.2/. , SM5210B, SW-846 3015 6020 , 7470A, 5540C, 4500H- , EPA 200. , SM3500Cr- , EPA 245. 245. , SW-846 9040B, 3005A, EPA 6010B , 7196A , SW-846 901 OB , 9030B. Orqanic Parameters : SW-846 8260B, 8270C, 3510C , EPA 608 , 624 , 625 SW-846 5030B, 8021 B , 8081A , 8082 , 8151A , 8330. Solid Chemica/ Materia/s Inorqanic Parameters : SW-846 9040B, 3005A, 6010B, 7196A , 5030B, 9010B 9030B, 1030, 1311 , 3050B , 3051, 7471 A, 9014 , 9012A, 9045C , 9050A , 9065. Orqanic Parameters : SW-846 8021B, 8081A , 8082 , 8151A, 8330 , 8260B, 8270C, 1311 , 3540C , 3545 , 3550B , 3580A, 5035L , 5035H.
New York Department of Health Certificate/Lab 10 : 11148. Inorqanic Parameters : SM9223B , 9222B, 8215B , EPA 200.8, 200. , 245. , SM5310C , EPADrinking Water
314. 331. 0, SM2320B , EPA 300. 325. , 110. , SM2120B, 4500CN- , 4500F- , EPA 150. , SM4500H4500N03- , 2540C , EPA 120. , SM 2510B. Orqanic Parameters : EPA 524. 504. , SM6251 B. Non-Potab/e Water Inorqanic Parameters : SM9221 E, 92220 , 9221 B, 9222B , 9215B, EPA 405. , SM5210B , EPA 410.4, SM52200 , EPA 305. , SM2310B-4a, EPA 310. , SM2320B , EPA 200. , 300. , 325. , LAC HAT 10-11707-1A or B , SM4500CI- , EPA 340. 2, SM4500F-C, EPA 375.4 , SM15 426C, EPA 350. 350. , LAC HAT 10-10706- , SM4500NH3- , EPA 351. , LAC HAT 10-107-06- , EPA 353. , LACHAT 10-107-041- , SM4500-N030F EPA 354. , SM4500-N02- , EPA 365. , SM4500P- , EPA 160. , SM2540B , EPA 160. , SM2540C , EPA 160. SM25400, EPA 200. , EPA 6010B, 6020, EPA 7196A, S\M3500Cr- , EPA 245. , 245. , 7470A, 110. SM2120B, 335. , LACHA T 10-204-00- , EPA 150. , 9040B, SM4500- , EPA 1664A , EPA 415. , SM5310C, EPA 420. , SM14 510C , EPA 120. , SM2510B , EPA 376. , SM4500S- , EPA 425. , SM5540C , EPA 3005A 3015. Orqanic Parameters : EPA 624 , 8260B, 8270C , 625 , 608 , 8081A, 8151A , 8330, 8082 , 8021B, EPA 3510C 5030B, 9010B, 9030B. Solid Hazardous Waste Inorganic Parameters : EPA 9040B, 9045C, 1010 , 1030, SW-846 Ch 7 See 7. , EPA 6010B , 7196A, 7471A , 9012A, 9014 , 9040B , 9045C, 9065, 9050, EPA 1311 , 3005A, 3050B , 3051 , 9010B 9030B. Orqanic Parameters:EPA 8260B , 8270C, 8081A, 8151A, 8330 , 8082 , 8021B , 3540C , 3545 , 3580 , 5030B 5035. Ana/ytica/ Services Protocol: CLP Volatile Organics, CLP Inorganics, CLP PCB/Pesticides.
Rhode Island Department of Health Certificate/Lab 10 : LA000065. Refer to MA-OEP Certificate for Potable and Non-Potable Water. Refer to NY-OOH Certificate for Potable and Non-Potable Water.
Pennsylvania Department of Environmental Protection Certificate/Lab 10 : 68-03671. Registered Laboratory.
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