memo containing purgeable organic analysis · 0000526 m/ef *•p>
TRANSCRIPT
0000526
PgtMef bull ltn
JUH14RECD
6-15-87
US EivViRQWiENYfiL PROTECTION ftGENCY60 msEtview StreetLexington MA Opound173
Superfund Records CenterSITEBREAK OTHER
SUBJECT Nutmeg Valley CTmdashPurgeable Organic AnalysisSamples finalyzee by GLhiS 67 38 446 44pound 445 4pound1 440 433 4pound7 4poundi=Be 5s Screening data for samples 67444 and 443
Ofl
i i i 1 e anc Bcot t C1 i f fora^ bull r [r^t iv i i 1 e anc Scot t C1 i f fora Chern i st s
rC Do- Eerrer Chief 0 H and raquo
THKU Dr W i J l i a r n f indradeC h i e f Chemis t ry Sertio
PROJECT NUMBER 87Ol7pound
DArEltS) SO--PLES RECEIVED BY THE LflBD^ATORY S-3O-67
rea-al -s let or volume 49 =poundO9 Occ izS
H laboratory blank was analyzed prior to sample analysis
Each sample was saiked witn several surrcoate coriic-onnos ataciprox irnatej y 3O DOD concent ra ion Tne results for- toesurrogate recoveries are reported for eacrs sarnole
jar-icle SrEE W^B ariaiysed Ln ciupiiacat^ toanaiyrirai D^ec a sion end aver ace concentrations werereoortea
c Rich haworth
C000527
liS7rti_gt ~
bullURGE co-
ftixfl_YTICfiL PftRAMETERS PURGErtbi_E ORGANIC ftNftLYSIS
7e Kmar PlLS 7ei-ltmar LSCmdashpound
Firim uar Oigta SOB
gtbullbullbull DC Tire and Flow
iztL shy ci 3 c- shy r--f Fi ow-
I-a -e out cycle-
i prroer-ctire
1 - ~ II
eci-r-on c-
r^^ss Range
tear Rate
Hel i urn
i 1 mi ft f 40 rn i rnin
S5 cm stairiles steel (16 i n O D ) packed w i t n 15 cn 6OSO rntvs- Te^ax-GC p lus 8 crn 35SO I 6V 3 lt--or tyrgte i5 O a T Ge-L
bullr r-in poundbullgt t n j ^ u 4
7 f r-1 n
S i--ter ty pound n i ID D cc-1 unii-i oarneri w r t i ^ 1 -bull- mdash j OOO ori oOo us---
3 ilaquo bull 1 1 v bullbull lt=- nr-oD r-a bull- r=r e 8 Cv tc SiC C rrd no ci bullbullraquo t 7e tr-^
H e I 11 i f 3O rn I m bull rlt
7O V
3S S6O
3 secorics
OOOO528
FACILITY SftttPLED Nutmeg Valley
US EiWlRQNXENTftL PROTECTION AGENCY REGION I LPBORflTORY ECrS PuRSEflELE ORGANIC ANALYSIS - WATER
DATE OF ANPilY3SS-3-87 RTE C-- CC EC O N - ^Kfc^^ REFERENCE BODK 8 Itt 0- C _ _ - C cr
AM-~gt_F A7CLiTSi
Det CAS STORE Con pound Cone L imi t Comments NO NJ ( u c L ) ( u g L )
4-87-3 34^pound C~- loro^ii-t iare ND 1 3O 4-83-S bull 3 ircf bullbull-bull rc ngtTiVipound fvD 30 5-01-4 2S75 V 3 r-yl Cn lor icie NL1 4O 5-OC- 2-T C^ A bullbull-bull r - J hane KD pound0 Jmdash OS-pound 3-r 1 3 IV-G--- -y bull enr C~ 1 or i ce ND j 0 I-6S-4 3445pound Trich lorof 1 uororre-chane ND poundO 5trade5raquoj~i v^ bullbull oO j i 1 mdash D i en 1 or-oet hy I ens ND pound0 5-34-3 3lt9pound 1 j -Die iCroF-trare gtVD 10
_r | Tgt 5amp-60--5 -^5-i- c-Dich bull ii--cc-t-ry lEripound isornev cO 7-66-2 31-vE C i oro c bullbullbullbull ND 10 07-o6-pound s --bull 2mdash D i en bull oroe- 1 h ane 10 bullND
iV 1-55-C I-~-L 1 _- T- ic- i i i - f roct he 1O 6mdash pound3-5 3 - T Ia r bullo T ~ poundgtt r-ac i or idc IND 0 5-pound7-4 Z^ 0 r-r-orrorj x ch 1 ororret narre ND poundO a-raquo7 ---= bull v - -bull ic- O-C -r-ciieriegt gtD 0 OO61-0pound-pound r---f-BS r - 3 mdash D i cL I o r o p r o p lt ne ND X O 9-Oi-B ~vgt 80 Tgt i ch 1 0c-e t hy 1 ene bull- 0
103
pound4-4pound-I - bull- 2 bullbull L claquo r- o - h 1 c v c K e -i -i a n egt M Elt1
OOSl -Oi- 3^70^ cmdash 3-D i cn - orc-prosene iVD laquo O g-00-fi gt5 i bull J- r- ch oroet h ane ND iO l_i -_- i)3gt H = gt - bull r-l rsifi 0 10-75- T-f~o c- mdash C r i o r o s- c rt y i v i n y i et n er lv D 1 5O 5-pound5-P r-= 0 rr-c-ficf or- D IO pound7-16-4 24475 T et r ach I or oet h y 1 ene fTTo IO 9-34-c 245 pound l 1 i^ 2-exracrTioroet hane D IO O6-poundpound-i 2 ^ 0 i O To I LI ene ND 10 06-30-7 34301 Cn 1 orobenzene ND IO pO-4l-ltgt 24371 Ethy l berisene ND IO 07-O2-S 34210 Pero He in ND 50 O )7-13-J 34515 Aery Ion it r i le ND poundOO
D i ch 1 cro bens ene i sorners ND poundO 1 pound-Tr i ch I oro- poundpoundshy i
t r i f 1 uoroet hane ND 50 -6^-1 SI 552 Acetone ND 43O i-15-0 770tl C a r bo ri D i e i I f i d e ND 4O
( con t )
COO0529 US FNVIRO-vrcENTOL PROTECTION fiGENCY Flt--ICN I
ampEftB^E Of lof iNIC flNftLYSIS shy WftTER
c Det
Cr~ G t i ~pound i Corr DOund Cone Limit Comments ^ r shy ~~ (LDL) (ugL)
gM- mdash mdashmdash mdash _ _
8 S3-J C ~~-~Z J--3 17 ef ne ND pound4O O6mdash O- 7 bull ^ 7 V j r iy ] Pco-cate ND 90 91-1 ~ cshy Jmdash - shy c- -i - -i _- ND 50
K 1 TiND 3O of- = shy 5 Kr shy ^--p ^ tamre ND 10 SS-IM1-7 bull X v c - ^ c (To~al) n 80
shy gti ~-r -5 nanrr ND 10
v ND tgt0
c i- r cr vc A y c c nt i f i
ugt~rc-r Recv sr i es _ i r n j s are cK 36 77-J17
11O 35-1^ 1O1 87-ti3
3 4-rircviCf 1 uorcoeri^ene 106 89-113
lt =bull- 1 e bull
OOOOS3O
SAMPLED Nutmeg Valley
gt= EvIROvpoundMTpL PROTECTION P3ENCY RfSlGN I LfiBDRftTORY Cw C PjrLrTOE_E Q^GftMC ftVJfi-YSTS - WfiTER
P7446 DQTE Or fiNPlLYSISamp-3-e7 RLFERECE BDOK- 87
1- _bull _ __ mdashr f - v
jJoLuorT ^o s net Cfib pound Z - Z L3Durio Coric L i m i t Comments
l U D _ ) ( U D L )
4--7 r - bdquobdquo- ^uir -ei-- -- - bull _ bull j - ~ ft i i I j 1 5-01-4 bdquobull r j y ~ i E xD ishy5-0 u -2 1 r f i -ir c t- v h fr fe fN ~ c 3j-c=gt-r - _ t - bull bull gt c F lt5 $ Li 2 l
^_CC mdashi i2 o -raquo w ^ _ i v iCf a o^o uc ronei nar-e K c 1-35-4 25i i j mdash Di ci t u royt ry I SV-JB ^D c 5-34-2 -- =bull 1 1 -D - c i _ -lt r- - - - - c I) 1 SS-SO-5 = --pound f -D- r - _ - - or- V^e^e iccrrc^= ^D E 7-pound6-2 1- t c - - _ ^ to f-l |5 A - - _ _ _ ^ ^ f^mdash -O7-U6-E- -- bull_ bull bull ic^is $ ~ 1-5E-C _ - - c - r bdquo r gt e Zoa L_J 5
S-iST-1 I raquo - gt gt - s r r - i cc lt r- I 5_1pound7_i __ _ pound c - ~ c - 0 r- fr - n e ^ t j D =bull
_ _ - _ - _ - shya-eshyoofci-vc-r 2-t r - T - -Li cr c iiov-lt- Fne ^^ 3 9-Qj --_ -~ c- - c ^ -amp- v -bull=bull- e ^ fTdJ 5 gL-4c - J I ^ bull o bull-- i r n c -ve- N D 1 OOpound - _gt_ -pound - lt ^ --bull ~lu - 0 or - -CDe-- -p= ltD i y (i mdash _ bull laquo _ - mdash bull bull C i T1 r ipound h SiS1 P
1-4 - - - 3 r^S I egt16- - _ O
10-7S-- r -gt bull- i_ bull- e- - y x bull gt tr n e- ^ -J i-r-- r rgt i^O-^i 1 N1
S7-1C- _-pound -bdquo-_ H v _ amp c r v tn(_ ^ PTT21 L
9-3^ -r - 1 1 1 Imdash i e r -bull- ~ -c r~~ltei l~fgtiis M 1 OB-6fe- I A- _bull Tc 3vt-r-G ^D i O8-1 )-7 ^ bull -UI Z- ic t-erser-e iD 3 00-4- 2^271 E t T v l b r mdash ne^-p- NO j 07-upound~tgt 2^210 flc^olein r ND 5O O7-13-1 J4poundi5 Ac --y 1 o fgt 1 1 r i i e N D ampO
Dirh lore us-iZErie a sorters D c 1 c poundmdash Tr ic h I rlaquor omdash c c Lsect_J ^
bull5v 1 ucvcet -ane bullraquoamp 5 A3fmdash poundpoundmdash 3 pound ^5S Ptcptov-pi ND
5-lS-G rv -)i - Cci-^i D i lt - j 3 f i c e ^J 4 (cor t )
-
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
C000527
liS7rti_gt ~
bullURGE co-
ftixfl_YTICfiL PftRAMETERS PURGErtbi_E ORGANIC ftNftLYSIS
7e Kmar PlLS 7ei-ltmar LSCmdashpound
Firim uar Oigta SOB
gtbullbullbull DC Tire and Flow
iztL shy ci 3 c- shy r--f Fi ow-
I-a -e out cycle-
i prroer-ctire
1 - ~ II
eci-r-on c-
r^^ss Range
tear Rate
Hel i urn
i 1 mi ft f 40 rn i rnin
S5 cm stairiles steel (16 i n O D ) packed w i t n 15 cn 6OSO rntvs- Te^ax-GC p lus 8 crn 35SO I 6V 3 lt--or tyrgte i5 O a T Ge-L
bullr r-in poundbullgt t n j ^ u 4
7 f r-1 n
S i--ter ty pound n i ID D cc-1 unii-i oarneri w r t i ^ 1 -bull- mdash j OOO ori oOo us---
3 ilaquo bull 1 1 v bullbull lt=- nr-oD r-a bull- r=r e 8 Cv tc SiC C rrd no ci bullbullraquo t 7e tr-^
H e I 11 i f 3O rn I m bull rlt
7O V
3S S6O
3 secorics
OOOO528
FACILITY SftttPLED Nutmeg Valley
US EiWlRQNXENTftL PROTECTION AGENCY REGION I LPBORflTORY ECrS PuRSEflELE ORGANIC ANALYSIS - WATER
DATE OF ANPilY3SS-3-87 RTE C-- CC EC O N - ^Kfc^^ REFERENCE BODK 8 Itt 0- C _ _ - C cr
AM-~gt_F A7CLiTSi
Det CAS STORE Con pound Cone L imi t Comments NO NJ ( u c L ) ( u g L )
4-87-3 34^pound C~- loro^ii-t iare ND 1 3O 4-83-S bull 3 ircf bullbull-bull rc ngtTiVipound fvD 30 5-01-4 2S75 V 3 r-yl Cn lor icie NL1 4O 5-OC- 2-T C^ A bullbull-bull r - J hane KD pound0 Jmdash OS-pound 3-r 1 3 IV-G--- -y bull enr C~ 1 or i ce ND j 0 I-6S-4 3445pound Trich lorof 1 uororre-chane ND poundO 5trade5raquoj~i v^ bullbull oO j i 1 mdash D i en 1 or-oet hy I ens ND pound0 5-34-3 3lt9pound 1 j -Die iCroF-trare gtVD 10
_r | Tgt 5amp-60--5 -^5-i- c-Dich bull ii--cc-t-ry lEripound isornev cO 7-66-2 31-vE C i oro c bullbullbullbull ND 10 07-o6-pound s --bull 2mdash D i en bull oroe- 1 h ane 10 bullND
iV 1-55-C I-~-L 1 _- T- ic- i i i - f roct he 1O 6mdash pound3-5 3 - T Ia r bullo T ~ poundgtt r-ac i or idc IND 0 5-pound7-4 Z^ 0 r-r-orrorj x ch 1 ororret narre ND poundO a-raquo7 ---= bull v - -bull ic- O-C -r-ciieriegt gtD 0 OO61-0pound-pound r---f-BS r - 3 mdash D i cL I o r o p r o p lt ne ND X O 9-Oi-B ~vgt 80 Tgt i ch 1 0c-e t hy 1 ene bull- 0
103
pound4-4pound-I - bull- 2 bullbull L claquo r- o - h 1 c v c K e -i -i a n egt M Elt1
OOSl -Oi- 3^70^ cmdash 3-D i cn - orc-prosene iVD laquo O g-00-fi gt5 i bull J- r- ch oroet h ane ND iO l_i -_- i)3gt H = gt - bull r-l rsifi 0 10-75- T-f~o c- mdash C r i o r o s- c rt y i v i n y i et n er lv D 1 5O 5-pound5-P r-= 0 rr-c-ficf or- D IO pound7-16-4 24475 T et r ach I or oet h y 1 ene fTTo IO 9-34-c 245 pound l 1 i^ 2-exracrTioroet hane D IO O6-poundpound-i 2 ^ 0 i O To I LI ene ND 10 06-30-7 34301 Cn 1 orobenzene ND IO pO-4l-ltgt 24371 Ethy l berisene ND IO 07-O2-S 34210 Pero He in ND 50 O )7-13-J 34515 Aery Ion it r i le ND poundOO
D i ch 1 cro bens ene i sorners ND poundO 1 pound-Tr i ch I oro- poundpoundshy i
t r i f 1 uoroet hane ND 50 -6^-1 SI 552 Acetone ND 43O i-15-0 770tl C a r bo ri D i e i I f i d e ND 4O
( con t )
COO0529 US FNVIRO-vrcENTOL PROTECTION fiGENCY Flt--ICN I
ampEftB^E Of lof iNIC flNftLYSIS shy WftTER
c Det
Cr~ G t i ~pound i Corr DOund Cone Limit Comments ^ r shy ~~ (LDL) (ugL)
gM- mdash mdashmdash mdash _ _
8 S3-J C ~~-~Z J--3 17 ef ne ND pound4O O6mdash O- 7 bull ^ 7 V j r iy ] Pco-cate ND 90 91-1 ~ cshy Jmdash - shy c- -i - -i _- ND 50
K 1 TiND 3O of- = shy 5 Kr shy ^--p ^ tamre ND 10 SS-IM1-7 bull X v c - ^ c (To~al) n 80
shy gti ~-r -5 nanrr ND 10
v ND tgt0
c i- r cr vc A y c c nt i f i
ugt~rc-r Recv sr i es _ i r n j s are cK 36 77-J17
11O 35-1^ 1O1 87-ti3
3 4-rircviCf 1 uorcoeri^ene 106 89-113
lt =bull- 1 e bull
OOOOS3O
SAMPLED Nutmeg Valley
gt= EvIROvpoundMTpL PROTECTION P3ENCY RfSlGN I LfiBDRftTORY Cw C PjrLrTOE_E Q^GftMC ftVJfi-YSTS - WfiTER
P7446 DQTE Or fiNPlLYSISamp-3-e7 RLFERECE BDOK- 87
1- _bull _ __ mdashr f - v
jJoLuorT ^o s net Cfib pound Z - Z L3Durio Coric L i m i t Comments
l U D _ ) ( U D L )
4--7 r - bdquobdquo- ^uir -ei-- -- - bull _ bull j - ~ ft i i I j 1 5-01-4 bdquobull r j y ~ i E xD ishy5-0 u -2 1 r f i -ir c t- v h fr fe fN ~ c 3j-c=gt-r - _ t - bull bull gt c F lt5 $ Li 2 l
^_CC mdashi i2 o -raquo w ^ _ i v iCf a o^o uc ronei nar-e K c 1-35-4 25i i j mdash Di ci t u royt ry I SV-JB ^D c 5-34-2 -- =bull 1 1 -D - c i _ -lt r- - - - - c I) 1 SS-SO-5 = --pound f -D- r - _ - - or- V^e^e iccrrc^= ^D E 7-pound6-2 1- t c - - _ ^ to f-l |5 A - - _ _ _ ^ ^ f^mdash -O7-U6-E- -- bull_ bull bull ic^is $ ~ 1-5E-C _ - - c - r bdquo r gt e Zoa L_J 5
S-iST-1 I raquo - gt gt - s r r - i cc lt r- I 5_1pound7_i __ _ pound c - ~ c - 0 r- fr - n e ^ t j D =bull
_ _ - _ - _ - shya-eshyoofci-vc-r 2-t r - T - -Li cr c iiov-lt- Fne ^^ 3 9-Qj --_ -~ c- - c ^ -amp- v -bull=bull- e ^ fTdJ 5 gL-4c - J I ^ bull o bull-- i r n c -ve- N D 1 OOpound - _gt_ -pound - lt ^ --bull ~lu - 0 or - -CDe-- -p= ltD i y (i mdash _ bull laquo _ - mdash bull bull C i T1 r ipound h SiS1 P
1-4 - - - 3 r^S I egt16- - _ O
10-7S-- r -gt bull- i_ bull- e- - y x bull gt tr n e- ^ -J i-r-- r rgt i^O-^i 1 N1
S7-1C- _-pound -bdquo-_ H v _ amp c r v tn(_ ^ PTT21 L
9-3^ -r - 1 1 1 Imdash i e r -bull- ~ -c r~~ltei l~fgtiis M 1 OB-6fe- I A- _bull Tc 3vt-r-G ^D i O8-1 )-7 ^ bull -UI Z- ic t-erser-e iD 3 00-4- 2^271 E t T v l b r mdash ne^-p- NO j 07-upound~tgt 2^210 flc^olein r ND 5O O7-13-1 J4poundi5 Ac --y 1 o fgt 1 1 r i i e N D ampO
Dirh lore us-iZErie a sorters D c 1 c poundmdash Tr ic h I rlaquor omdash c c Lsect_J ^
bull5v 1 ucvcet -ane bullraquoamp 5 A3fmdash poundpoundmdash 3 pound ^5S Ptcptov-pi ND
5-lS-G rv -)i - Cci-^i D i lt - j 3 f i c e ^J 4 (cor t )
-
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOOO528
FACILITY SftttPLED Nutmeg Valley
US EiWlRQNXENTftL PROTECTION AGENCY REGION I LPBORflTORY ECrS PuRSEflELE ORGANIC ANALYSIS - WATER
DATE OF ANPilY3SS-3-87 RTE C-- CC EC O N - ^Kfc^^ REFERENCE BODK 8 Itt 0- C _ _ - C cr
AM-~gt_F A7CLiTSi
Det CAS STORE Con pound Cone L imi t Comments NO NJ ( u c L ) ( u g L )
4-87-3 34^pound C~- loro^ii-t iare ND 1 3O 4-83-S bull 3 ircf bullbull-bull rc ngtTiVipound fvD 30 5-01-4 2S75 V 3 r-yl Cn lor icie NL1 4O 5-OC- 2-T C^ A bullbull-bull r - J hane KD pound0 Jmdash OS-pound 3-r 1 3 IV-G--- -y bull enr C~ 1 or i ce ND j 0 I-6S-4 3445pound Trich lorof 1 uororre-chane ND poundO 5trade5raquoj~i v^ bullbull oO j i 1 mdash D i en 1 or-oet hy I ens ND pound0 5-34-3 3lt9pound 1 j -Die iCroF-trare gtVD 10
_r | Tgt 5amp-60--5 -^5-i- c-Dich bull ii--cc-t-ry lEripound isornev cO 7-66-2 31-vE C i oro c bullbullbullbull ND 10 07-o6-pound s --bull 2mdash D i en bull oroe- 1 h ane 10 bullND
iV 1-55-C I-~-L 1 _- T- ic- i i i - f roct he 1O 6mdash pound3-5 3 - T Ia r bullo T ~ poundgtt r-ac i or idc IND 0 5-pound7-4 Z^ 0 r-r-orrorj x ch 1 ororret narre ND poundO a-raquo7 ---= bull v - -bull ic- O-C -r-ciieriegt gtD 0 OO61-0pound-pound r---f-BS r - 3 mdash D i cL I o r o p r o p lt ne ND X O 9-Oi-B ~vgt 80 Tgt i ch 1 0c-e t hy 1 ene bull- 0
103
pound4-4pound-I - bull- 2 bullbull L claquo r- o - h 1 c v c K e -i -i a n egt M Elt1
OOSl -Oi- 3^70^ cmdash 3-D i cn - orc-prosene iVD laquo O g-00-fi gt5 i bull J- r- ch oroet h ane ND iO l_i -_- i)3gt H = gt - bull r-l rsifi 0 10-75- T-f~o c- mdash C r i o r o s- c rt y i v i n y i et n er lv D 1 5O 5-pound5-P r-= 0 rr-c-ficf or- D IO pound7-16-4 24475 T et r ach I or oet h y 1 ene fTTo IO 9-34-c 245 pound l 1 i^ 2-exracrTioroet hane D IO O6-poundpound-i 2 ^ 0 i O To I LI ene ND 10 06-30-7 34301 Cn 1 orobenzene ND IO pO-4l-ltgt 24371 Ethy l berisene ND IO 07-O2-S 34210 Pero He in ND 50 O )7-13-J 34515 Aery Ion it r i le ND poundOO
D i ch 1 cro bens ene i sorners ND poundO 1 pound-Tr i ch I oro- poundpoundshy i
t r i f 1 uoroet hane ND 50 -6^-1 SI 552 Acetone ND 43O i-15-0 770tl C a r bo ri D i e i I f i d e ND 4O
( con t )
COO0529 US FNVIRO-vrcENTOL PROTECTION fiGENCY Flt--ICN I
ampEftB^E Of lof iNIC flNftLYSIS shy WftTER
c Det
Cr~ G t i ~pound i Corr DOund Cone Limit Comments ^ r shy ~~ (LDL) (ugL)
gM- mdash mdashmdash mdash _ _
8 S3-J C ~~-~Z J--3 17 ef ne ND pound4O O6mdash O- 7 bull ^ 7 V j r iy ] Pco-cate ND 90 91-1 ~ cshy Jmdash - shy c- -i - -i _- ND 50
K 1 TiND 3O of- = shy 5 Kr shy ^--p ^ tamre ND 10 SS-IM1-7 bull X v c - ^ c (To~al) n 80
shy gti ~-r -5 nanrr ND 10
v ND tgt0
c i- r cr vc A y c c nt i f i
ugt~rc-r Recv sr i es _ i r n j s are cK 36 77-J17
11O 35-1^ 1O1 87-ti3
3 4-rircviCf 1 uorcoeri^ene 106 89-113
lt =bull- 1 e bull
OOOOS3O
SAMPLED Nutmeg Valley
gt= EvIROvpoundMTpL PROTECTION P3ENCY RfSlGN I LfiBDRftTORY Cw C PjrLrTOE_E Q^GftMC ftVJfi-YSTS - WfiTER
P7446 DQTE Or fiNPlLYSISamp-3-e7 RLFERECE BDOK- 87
1- _bull _ __ mdashr f - v
jJoLuorT ^o s net Cfib pound Z - Z L3Durio Coric L i m i t Comments
l U D _ ) ( U D L )
4--7 r - bdquobdquo- ^uir -ei-- -- - bull _ bull j - ~ ft i i I j 1 5-01-4 bdquobull r j y ~ i E xD ishy5-0 u -2 1 r f i -ir c t- v h fr fe fN ~ c 3j-c=gt-r - _ t - bull bull gt c F lt5 $ Li 2 l
^_CC mdashi i2 o -raquo w ^ _ i v iCf a o^o uc ronei nar-e K c 1-35-4 25i i j mdash Di ci t u royt ry I SV-JB ^D c 5-34-2 -- =bull 1 1 -D - c i _ -lt r- - - - - c I) 1 SS-SO-5 = --pound f -D- r - _ - - or- V^e^e iccrrc^= ^D E 7-pound6-2 1- t c - - _ ^ to f-l |5 A - - _ _ _ ^ ^ f^mdash -O7-U6-E- -- bull_ bull bull ic^is $ ~ 1-5E-C _ - - c - r bdquo r gt e Zoa L_J 5
S-iST-1 I raquo - gt gt - s r r - i cc lt r- I 5_1pound7_i __ _ pound c - ~ c - 0 r- fr - n e ^ t j D =bull
_ _ - _ - _ - shya-eshyoofci-vc-r 2-t r - T - -Li cr c iiov-lt- Fne ^^ 3 9-Qj --_ -~ c- - c ^ -amp- v -bull=bull- e ^ fTdJ 5 gL-4c - J I ^ bull o bull-- i r n c -ve- N D 1 OOpound - _gt_ -pound - lt ^ --bull ~lu - 0 or - -CDe-- -p= ltD i y (i mdash _ bull laquo _ - mdash bull bull C i T1 r ipound h SiS1 P
1-4 - - - 3 r^S I egt16- - _ O
10-7S-- r -gt bull- i_ bull- e- - y x bull gt tr n e- ^ -J i-r-- r rgt i^O-^i 1 N1
S7-1C- _-pound -bdquo-_ H v _ amp c r v tn(_ ^ PTT21 L
9-3^ -r - 1 1 1 Imdash i e r -bull- ~ -c r~~ltei l~fgtiis M 1 OB-6fe- I A- _bull Tc 3vt-r-G ^D i O8-1 )-7 ^ bull -UI Z- ic t-erser-e iD 3 00-4- 2^271 E t T v l b r mdash ne^-p- NO j 07-upound~tgt 2^210 flc^olein r ND 5O O7-13-1 J4poundi5 Ac --y 1 o fgt 1 1 r i i e N D ampO
Dirh lore us-iZErie a sorters D c 1 c poundmdash Tr ic h I rlaquor omdash c c Lsect_J ^
bull5v 1 ucvcet -ane bullraquoamp 5 A3fmdash poundpoundmdash 3 pound ^5S Ptcptov-pi ND
5-lS-G rv -)i - Cci-^i D i lt - j 3 f i c e ^J 4 (cor t )
-
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
COO0529 US FNVIRO-vrcENTOL PROTECTION fiGENCY Flt--ICN I
ampEftB^E Of lof iNIC flNftLYSIS shy WftTER
c Det
Cr~ G t i ~pound i Corr DOund Cone Limit Comments ^ r shy ~~ (LDL) (ugL)
gM- mdash mdashmdash mdash _ _
8 S3-J C ~~-~Z J--3 17 ef ne ND pound4O O6mdash O- 7 bull ^ 7 V j r iy ] Pco-cate ND 90 91-1 ~ cshy Jmdash - shy c- -i - -i _- ND 50
K 1 TiND 3O of- = shy 5 Kr shy ^--p ^ tamre ND 10 SS-IM1-7 bull X v c - ^ c (To~al) n 80
shy gti ~-r -5 nanrr ND 10
v ND tgt0
c i- r cr vc A y c c nt i f i
ugt~rc-r Recv sr i es _ i r n j s are cK 36 77-J17
11O 35-1^ 1O1 87-ti3
3 4-rircviCf 1 uorcoeri^ene 106 89-113
lt =bull- 1 e bull
OOOOS3O
SAMPLED Nutmeg Valley
gt= EvIROvpoundMTpL PROTECTION P3ENCY RfSlGN I LfiBDRftTORY Cw C PjrLrTOE_E Q^GftMC ftVJfi-YSTS - WfiTER
P7446 DQTE Or fiNPlLYSISamp-3-e7 RLFERECE BDOK- 87
1- _bull _ __ mdashr f - v
jJoLuorT ^o s net Cfib pound Z - Z L3Durio Coric L i m i t Comments
l U D _ ) ( U D L )
4--7 r - bdquobdquo- ^uir -ei-- -- - bull _ bull j - ~ ft i i I j 1 5-01-4 bdquobull r j y ~ i E xD ishy5-0 u -2 1 r f i -ir c t- v h fr fe fN ~ c 3j-c=gt-r - _ t - bull bull gt c F lt5 $ Li 2 l
^_CC mdashi i2 o -raquo w ^ _ i v iCf a o^o uc ronei nar-e K c 1-35-4 25i i j mdash Di ci t u royt ry I SV-JB ^D c 5-34-2 -- =bull 1 1 -D - c i _ -lt r- - - - - c I) 1 SS-SO-5 = --pound f -D- r - _ - - or- V^e^e iccrrc^= ^D E 7-pound6-2 1- t c - - _ ^ to f-l |5 A - - _ _ _ ^ ^ f^mdash -O7-U6-E- -- bull_ bull bull ic^is $ ~ 1-5E-C _ - - c - r bdquo r gt e Zoa L_J 5
S-iST-1 I raquo - gt gt - s r r - i cc lt r- I 5_1pound7_i __ _ pound c - ~ c - 0 r- fr - n e ^ t j D =bull
_ _ - _ - _ - shya-eshyoofci-vc-r 2-t r - T - -Li cr c iiov-lt- Fne ^^ 3 9-Qj --_ -~ c- - c ^ -amp- v -bull=bull- e ^ fTdJ 5 gL-4c - J I ^ bull o bull-- i r n c -ve- N D 1 OOpound - _gt_ -pound - lt ^ --bull ~lu - 0 or - -CDe-- -p= ltD i y (i mdash _ bull laquo _ - mdash bull bull C i T1 r ipound h SiS1 P
1-4 - - - 3 r^S I egt16- - _ O
10-7S-- r -gt bull- i_ bull- e- - y x bull gt tr n e- ^ -J i-r-- r rgt i^O-^i 1 N1
S7-1C- _-pound -bdquo-_ H v _ amp c r v tn(_ ^ PTT21 L
9-3^ -r - 1 1 1 Imdash i e r -bull- ~ -c r~~ltei l~fgtiis M 1 OB-6fe- I A- _bull Tc 3vt-r-G ^D i O8-1 )-7 ^ bull -UI Z- ic t-erser-e iD 3 00-4- 2^271 E t T v l b r mdash ne^-p- NO j 07-upound~tgt 2^210 flc^olein r ND 5O O7-13-1 J4poundi5 Ac --y 1 o fgt 1 1 r i i e N D ampO
Dirh lore us-iZErie a sorters D c 1 c poundmdash Tr ic h I rlaquor omdash c c Lsect_J ^
bull5v 1 ucvcet -ane bullraquoamp 5 A3fmdash poundpoundmdash 3 pound ^5S Ptcptov-pi ND
5-lS-G rv -)i - Cci-^i D i lt - j 3 f i c e ^J 4 (cor t )
-
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOOOS3O
SAMPLED Nutmeg Valley
gt= EvIROvpoundMTpL PROTECTION P3ENCY RfSlGN I LfiBDRftTORY Cw C PjrLrTOE_E Q^GftMC ftVJfi-YSTS - WfiTER
P7446 DQTE Or fiNPlLYSISamp-3-e7 RLFERECE BDOK- 87
1- _bull _ __ mdashr f - v
jJoLuorT ^o s net Cfib pound Z - Z L3Durio Coric L i m i t Comments
l U D _ ) ( U D L )
4--7 r - bdquobdquo- ^uir -ei-- -- - bull _ bull j - ~ ft i i I j 1 5-01-4 bdquobull r j y ~ i E xD ishy5-0 u -2 1 r f i -ir c t- v h fr fe fN ~ c 3j-c=gt-r - _ t - bull bull gt c F lt5 $ Li 2 l
^_CC mdashi i2 o -raquo w ^ _ i v iCf a o^o uc ronei nar-e K c 1-35-4 25i i j mdash Di ci t u royt ry I SV-JB ^D c 5-34-2 -- =bull 1 1 -D - c i _ -lt r- - - - - c I) 1 SS-SO-5 = --pound f -D- r - _ - - or- V^e^e iccrrc^= ^D E 7-pound6-2 1- t c - - _ ^ to f-l |5 A - - _ _ _ ^ ^ f^mdash -O7-U6-E- -- bull_ bull bull ic^is $ ~ 1-5E-C _ - - c - r bdquo r gt e Zoa L_J 5
S-iST-1 I raquo - gt gt - s r r - i cc lt r- I 5_1pound7_i __ _ pound c - ~ c - 0 r- fr - n e ^ t j D =bull
_ _ - _ - _ - shya-eshyoofci-vc-r 2-t r - T - -Li cr c iiov-lt- Fne ^^ 3 9-Qj --_ -~ c- - c ^ -amp- v -bull=bull- e ^ fTdJ 5 gL-4c - J I ^ bull o bull-- i r n c -ve- N D 1 OOpound - _gt_ -pound - lt ^ --bull ~lu - 0 or - -CDe-- -p= ltD i y (i mdash _ bull laquo _ - mdash bull bull C i T1 r ipound h SiS1 P
1-4 - - - 3 r^S I egt16- - _ O
10-7S-- r -gt bull- i_ bull- e- - y x bull gt tr n e- ^ -J i-r-- r rgt i^O-^i 1 N1
S7-1C- _-pound -bdquo-_ H v _ amp c r v tn(_ ^ PTT21 L
9-3^ -r - 1 1 1 Imdash i e r -bull- ~ -c r~~ltei l~fgtiis M 1 OB-6fe- I A- _bull Tc 3vt-r-G ^D i O8-1 )-7 ^ bull -UI Z- ic t-erser-e iD 3 00-4- 2^271 E t T v l b r mdash ne^-p- NO j 07-upound~tgt 2^210 flc^olein r ND 5O O7-13-1 J4poundi5 Ac --y 1 o fgt 1 1 r i i e N D ampO
Dirh lore us-iZErie a sorters D c 1 c poundmdash Tr ic h I rlaquor omdash c c Lsect_J ^
bull5v 1 ucvcet -ane bullraquoamp 5 A3fmdash poundpoundmdash 3 pound ^5S Ptcptov-pi ND
5-lS-G rv -)i - Cci-^i D i lt - j 3 f i c e ^J 4 (cor t )
-
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOO0531
US ENVIRONMENTAL PROTECTION AGENCY RIGIO I LABORATORY GChS PURGEAPLE ORGANIC ANALYSIS - WATER
gta no muea Det
CPS t UK^T Corraound Cone L i m i t Comments t r-3 bullbull (ug L) ( u g L )
8-33-2 ri^-5 a-Pi-anore ND pound4 O6-05-4i91-0-t
77-gt-57 7 7 v gt w J
V i ry l Acetate pound--^xar line
ND ND
9 5
06- i O-i F ^Spound 4-^ et ny l-c-Pe^tanone ND 3 OOmdash -pound-5 fshy 70S Sty --pne ND 1 33-Opound-7 K Sib Xyleries ( r o t p l ) ND pound
-Pi-gt-oM-5t^poundraquorie c bull P1-- i^c f-r s-gt
(EDB) ND N-D
1 14
l-ti iyl etner D 8
EL 0 T bull bull CO Ti D bull- 11 bullO 5
pound Terit a~c i veiy I d e n t i f i e d
Qaant i t a ted
i Z--D i c- I oroet hane d4 Flt5 Sf^^1 Ci6 To 1 L^^if-1 rS 1 4-Promof 1 uoro_benzene
Gbltserved Recovs1- I
100 111 99
104
SSjiConf idence i_ i rn 11 s 77-117 92-lpoundpound 87-109 83-113
tes -ovpound Detected ciopr- -ir-iate ess than cr t aier than
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOOO532
FftCTLITY SflMPLED Nutmeg Valley
t L S t VVI KUiV^fM i Hl_ HKU tL iUN HbtlNUY
R C S T Q N I LPBCRft-QRY h GCV3 PURBZ^F 1 =pound O R G A N I C fiMfiLYSIS - UflTER
ift^PLI ^C 87445 fcfeampDampNltT DqTE QF AMflLYSIS6-3-87
iflTE O ~ r~ t T 1 D1- ^n^1^ REFERENCE BOOK 8 [IKE G- r- 1-1Z UH^OA laquoMP_E FiEampV^~S to ~rcgtS^ HO
VyO ^^CQ r O67 pound Det bull CfiS STORZT Corioound Cone Limit Cofiime nt s
NO NZi ( u g L ) ( u g L )
bull-r iov vi y Pgt~lt 1 1 gt i t ant ^
v4-67-3 3 - i - ^ ^ ~ c vraquo t ND 13 4-63-S Z-j r bullbull bull i n iPt hc-ne ND 3 5-01-4 bdquo - _ v iy 1 Cn icr ioe ND ^ p-00-3 3^31 CM Ic-roet a^e ND pound
1 ir ~ _bullpoundbull _ i C v 1 C S i ^ r j CP Lorof uor-c methane ND CL
ir-35-4 34501 i 1-Dichloroethylene ND pound $-34-3 ~lt 43pound 1 1 - D -bull ru 1 ore et ^re ND 1
mdash56-60-5 3-f^pound 1 -~ bullgt cr bullgt ) Dmet ~iy I e^e i sonprs ND c7-GE-3 r Ceuro 1 ~ -ltrgt- clt T-gt N D 1
07-os-E -lt-- i pound -Dznlc ^t7-5re ND 1 1-55-6 2ltJi bull- 3 mdash r 3 CM or r-ct Mcie ND 1
46-23-5 3- I a - r r - n T e r r a c h l c ^ i d e bullvD 1
5-pound7~^ 3_ _ Pr r T icr l r c-f -ethane ND 1
48-S7-r --r- - -^ --bull bull- 3^-laquo ND oopoundi-oji-pound 3-t^j- c mdash L 3-D i eh 1 oroorooerie ND 1
9-0 3 -C videgTgt0 ~v- - bull ] - rlt c f y 1 erie lt1 1
pound4-4S - I T r r r ir rrh ioroinrt hene ND 1
OO6-o - Z - 7 0 ^ - c- 3mdash rgt2 c 1 o- O^^roer e D 1
9-OC-5 Z4r i i J-richlor_Rthane ND 1
l-4r-_ ~4C3u ^- gt - ~a bull cgt ND 1 j cr 1G-7C-E bull ~ -r- - -frt -y v i r y ethev- Zshy
5trade c Iz1 trade c raquo trade ltbull_ -f raquoraquo c 13^0^ iv ND i pound7-lS-^ 3^ 7 Tel roc1 - or e^hy lere ND i 9-3i-E 345 IS 1 l L 5-et re r i 1 or Det hane ND i 08-26-2 3lt- i lO To_ ufgtrn=gt ND i 08-30-7 34301 C bullbull ] o bull C aen r e oe ND i pO-4-4 34371 Et Myi benzene ND i 07-OE-S 34pound10 fie re 1 em ND so 07-13- i 34=15 fiery loii tr i le ND pound0 t Dicn 1 oro benzene i sorters ND pound
11 pound-Trichloro-l pound poundshytr i f I uoroet hane ND 5 laquoI
|-64-l 6J55S Acetone ND 43 B-15-0 77041 Carbon Dilt3Ul f ide ND 4
(con t)
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
L
0000533
US ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY GCPpound PURBt-ABLE ORGANIC ANALYSIS - WATER
3aTiobull lte sc11s Cont i nued
S-QRET Compound NiO vo
08-05-4 770Z7 Vinyl Acetatejraquo9l-0~e 77] C-r-exanone08-10-1 6l5Spound 4-hictnyi-c-PentarioneOO-4pound-f ol7vpound BtyrerE33-Opound-7 amp-15 Xylenes (total)
bull = -Diororf-pinane ltEDB)f t ragtgtycgtof ursfi L c -v 1 poundgtt-er
j C ~amp i l3(~ HO u rjGS
Tentatively Identifieo
raquo
C^-iE Com^-i-jnos Cuant itated
j
ample Recoveric~ oshyiurrocar-r- Co -bullro -bullbull cc
1 c-Dich loroebnane d4r-e-nsne d6ToluenedG14-Bromofluorobenzene
tes D-none cetected
i mate~an - than
Det Cone Limit Comments (unL) ltuoL)
ND 9 ND 5
ND 3 ND 1
ND pound ND 1
ND 14 ND 8
Observed 95^Confidence Recoveries Limits
99 77-117 115 92-lpoundpound 99 67-109
104 89-113
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
0000534 FPCIi_ITY SAILED Nutmeg Valley
US EXVIROlNAiENTftL PROTECTION P6ENCY REGION i LfiBORPTORY C-CbullI nu^GZHE^S ORampflJIC flNfli_YSIS - WflTER
87421 flMPLE L CC^D DfiTE 0~ RNftLYSI36-3-87 ftTF C-c t I -_T REFERENCE BOOK 87 IttE D^ wJ_ _
AMPLE RFFJ -T= Det
COS 5~ gt-=7 CoiDouna Coric L imi t Comrnents NO I lt u r L ) (uo L)
~ io r i tgt ol 1 irar rs
fc-87-3 laquo-bull a CT or c -e t r ^rs 13 (h-83-5 3- ^ Z t ronr f-f=w1-ic- rt ND 3 5-01-^ -r 71 v-1 1 riy 1 C raquo i or ice D 5-00-3 3-- C~ ] ore P v -( re NT) c J-0- --- iS^ ~gt v 1 ampx -r u i O - 4 C S L 1 S-6S-4 Jn^Et 7 i c^ I oro^ raquo uoromfet hane ND 2 |mdash 35mdash4 j^aOi 1 l mdash DicTloroet iy lene ND e 1-34-3 3-45fe 1 mdashD i c~ j orr_ B hs^ie ND i 5amp-60-5 3-- ^0 l f mdash L CT oropt UV] e^ip IEO^IS^S ND 2 7-66-3 3 J- C- 0 bullxirfiv rn ND l 07-O6-2 bull - 1 I - i c bull I o Cp t r ane D 1 1-55-6 - r c i i bull- i- ei ha^-e ND J
6-23-5 31 -^ L C - J I - I bull st ampc-i Icr ice D l 5-27-4 3J C r r c ( c1- - or iToe c havie N D 17
3~~o7~rlt bull r - 4 - bullbull -t^r^s- ND bulli
006-Oc-G 341~ - ( - bdquo w-T w w-hi c c-oroDene D 1 9-0 -6 r^ _ bullbull U bullbullbullraquo OefVlPME ND i 24-Aamp-1 2 v-- I1 ^ i r^ rr C C t i C f ^ Oi1 pound I ~i S i^ ND j ooampi-o-C r-r )bull+ c mdash r mdash D 3 r f~i I o OE 11 t re rvD 1 9-OO -b 3-f I c-~i- ic ^ --eti-ane ND i 1-43-J ~r C t_ reraquorgt- ND bullt
mdash10-7^-t 3^ c poundmdash lrt ci^~t-iU v -v i y4 etne-- i 5-25-ir 3- oi poundlt-- frr-if ogtri F i 27-lbmdash 34^7t- ~e-claquo-acn J orr-e--hyieiie ND i 9~mdash 7 laquo_ T bullbull i~ ^^ w r k raquo n _ i t L- r i-~5T rac-iiCrop-charis tD I oe-es-3 ilt -0 lt_ T -i erse ND X
r~ mdashi mdash bull mdash mdash e ^ ^ trade I T ^- j~ 08-90-7 7i j l i l ltD 1 30-4^mdash^- 3^371 E t n y a bennene D 1 07-O2-6 342 1O ftcro I ei n ND 50 07-13-j 34215 fiery i ogt 1 1 r r 11 e ND 2O
D i en j or-ODSTisene i sorners ND 2 1 i gt 2-Tncn ioro-1 pound 2
bullcr i f 1 uoroetharie ND 5 -64 -i 61552 Rceione ND 43 5-15-O 77i^J Car so D i s u j l f i d e ND 4
(conraquo t )
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
0000535
US ENVIRONMENTAL PROTECTIONREGION I LttBORflTORY
AGENCY
GCfcS PUtfGEflBLE ORGANIC ANALYSIS shy WATER
LE N~ 674pound1 1e -S Irs Cont i nued
CR3 STCRET tvQ ND
Compound Cone (unL)
Det L i m i t
( u g L ) Comment
8-33-3 ND pound4 OS-05-4 770S7 Viny l ftcetate ND 9 i91-10--amp 7703 ci--exanone ND 5 08-10-1 6i5SG 4- Xoti-tyl-2-Pentanone ND 3 OO-42-5 f-705 Styrene ND 1 33-Opound-7 o55 Xylenes ( t o t a l ) ND pound
i pound-D i bromoet hane ( poundDB ) ND 1 drof uv-an ND 14
rthy1 ether- ND e
Tenta t ive ly Iden t i f i ed
DoTieishy CornpouncH Quant itated
arnoie Rampcove-ieishy for Observed SS^-Conf idence cc~fr CoroouriCsr Recoveries L imi t s
1 pound-Dicnioroethane d4 97 77-117 Benzene dpound 114 9pound-lpoundpound Toluene 08 99 87-109 1 4-Bromof 1 uoroiDenzene 112 89mdash113
ptes ND-none Detected
t-an gt - c- r-eat er than
nn 1
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
0000536 FACILITY SAMPLED Nutmeg Valley
US ENVJRCJNhrZNTfiL PROTECTION ftGENCY RESIGN I LftBO^ftTGRY GCXS PjRGifiBi_E ORGANIC PCMflLYSIS shy
67440
DATE OF ANALYSIS6-3-87 ATE CF CD-- eC~ 3N (VJRTampKJ REFERENCE BOOK 8 1Mb Gr CJiJ_
AMPLE R-SJ LTS r
Det CAS Compound Cone Limit Comments N-3 (ugL) (ugL)
obull--bull i o gt- i t y Po bullbulli u t s r t s
T ~ _~ 4-87-3 C i ov-iori5i ana ND 13 4-S3-S 3 bull+ - 3 Bromornet Mane ND 3 5-01-4 li-- i Ti Vi ryl Cnloricje1 ND 4 5-OO-3 3^3 A C^lo^oe-thene ND f j-09-pound i^Z3 fgt t-t v - e n s Cr ]t or bull i o e ii) 1 S-6S-4 3^-466 Trie ~i ior C f 1 uorometh ane ND iS
|-35-4 34501 11 -D i c-h 1 oroet hy1 ene ND pound 5-34-3 3^- pound 1 -D i cn - or-oet nlaquone ND 1 56-60-5 ----bull^6 ^ cmdashD i en i or-OE-gtt h y I ene i sorrerE ND c
7-66-3 w- bdquo 1 Oci ir loro-Forrn 1m07-06-3 - lt J P-I bull- i oroet i~gt snp ND 1 1-55-fc bull-bull pound ^ i mdash -r- 1 cfi j oroet nane JpoundQ 1 6-S3-b 3T Oil Car-bor T e fc ram i or j de (3J 1 5_--7mdashi mdash - - x- - Ki~t c f i raquoii_ j bull- EI^CTHOC i en ororrBi hane iVlJ c
1
OOfcx-OS-b J-tJ-^S -1 3-Di ch1 oroor opene ND 1 19-0 i -6 -i -bull -bull bull bull V c -bull - oroer ny I er-e ND
bull -bull r~ vshypound4- 46-gt raquomdashbull -- - -~t D a b r o moc1 1 o o r-i e t n a n e ND 1
OOSl-Ol-L 3^ bull+ c -1 3-L 3 c-~i 1 or o pro gene ND i 9-oo-s 3^51 i - ci-Trich ioroethane ND i 1mdash43 -it 34O30 poundbullbullbull 2 ene ND i 10-7- 8 vi T I r bull i- mdash C~ i _bullbullbullbullgt jpoundt gt- vi ny i et her ND 15 5-pound5-pound 3pound- 04 Br-of oTii ND 1 pound7-18-4 3-r7t Tet rac-n i oroet hy 1 ene ND 1 9-34-6 3- J r U- 5 I pound r- Tetr-c-c orce thane ND 1 O6-6poundmdash3 3^010 TOJ Mene ND 1 O8-90-7 3430 j T bull-bull J o r o D e n z e n e ND 1 OO-41-4 34371 Et hy i benzene ND i
O7-OS-8 3421O Acrolein ND 50 O7-13-1 34pound15 fiery i on i t ri 1 e ND SO
Di en I orobenzene i somers ND pound 11 pound-Tr i ch1 oro- 1 pound poundshy
t ri f I uor oet h ane 4
P-64-1 ei55pound Acetone (46J 43 5-15-0 77041 Carbon Disulfide ND 4
(cont)
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
0000537
LS EWIRONNiENTftL PROTECTION AGENCY Rpound3ZON I LABORATORY
Pu^BEfiBlE ORGANIC flNOLYSISshy WflTER
laquoa rn 3 f bull shy poundbull 2 bull_ - T o f-7440 Cont inued
CPL j K C gtbull
Compound Cone ( u r u )
Det L imi t
( uc L ) Comments
8-92-3O8-05-4raquo91-10-608-10-i
e-Sr-S 770^7 771 OS amp15S6
i-i-baT anone V i n y l ft^etate c---texanone 4-i^ethyi~pound-Pentanone
bull
ND ND
ND ND
pound4 9 5 3
33-05-7 eE5 Xyienps ( to t a l )i r-rib-onoethane
T f t t r aHyc^o^u renr-i yshy r-ie-
(EDtO ND
ND ND
ND
pound 1
14 8
Tpr ta t iveiy i d e n t i f i e d
C shy=shy COT-T -bull r-r = taD gtt 11 at pd
iarncle - lec_-vr i et forJur-rbullbull cpoundbullbull bull - bull _ bull bull gt - =
Or-se^-vecj Recover ies
95iConf irie _i r i i tH
l pound-Dicnioroethane c4 99 77-H7 ^enrt= r dfo 114 9ll-lpoundpound
I To^-e oG 99 67-109 f 1 A-ri^cr^cif luorooer-zene lOS 89-113
ND=r-C-e (detected =-ap D gtbull xi iv s t e lt~ eF5 t -ltan gt=c re= c t than
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
87
0000538
FOCI LI TV SP^iPLED Nutmeg Valley
US ENVIRONMENTAL PROTECTION flGENCY REGION I LABORATORY GcX5 PLJRGECraquoB_E ORGANIC ANALYSIS - WOTER
NT 87423 flMP_E LCI-Cltgt TDM DflTE OF ONOLYSIS6-3-87
REFERENCE BOOKIME OF
RpoundSw_TS Det
COS amp Gpound i Compound Cone Limit Comments MO (ugLgt (ucL)
bull-r i or i t y Po i 1 ut ant s
amp-S7-3 3 4 tf C- c-rcnet-ane ND 13 -S3-9 344 3 Pr cgt roo ramp1h bullnB ND 3 5-01-4 3S i 7 i vi r y i Cn i o r IDS ND 4 5-OO-3 3 31 2 Cn Iorolt5t hane ND pound
l f- ~ ~- plusmn f-1pv i_~4 1mdashiV- S (1 TA ^ w w A W H5-03-c- J - mdash t iD 1 5-63-4 34453 Trien lorof1 uorornethane ND pound 1-35-4 345O1 1 1 -D i en 1 oroet hylene ND pound 3-34-3 -r-i C5pound i -D i ch 1 or oc i- h -ne ND 1 56-60-5 345 ~pound 3 E-Diehloroernylene isorners ND pound 7-66-3 3 L 0 pound C~i lore form ND 1 07-06-S vl1 -~ mdash I pound-Di en I oroet hane ND 1I
1-55-6 3450pound i i 1mdash rich 1 oroet hane ND 1 B-pound3-5 3c bull 0pound Ha^Dovt Te- rachlor ide ND 1 5-pound7-4 Oraquo ~ O u t^-ornoc i ch I oroinethane ND pound 3-87-5 bull-- I pound-1 --1 ororrooss NB 1 0061-02-6 34-655 t- 1 3-D i eh 1 oraquoODropene ND 1 9-01-6 3 I- J SO ~r i c- bull- oroet ny i ampne ND 1 24-48-1 3_= 05 D i c^oivoeh i oronet hane ND 1
bulli ooei-oi-5 347 CM e~ a 3-D i c~i 1 oroproDpoundne ND 9-00-5 345 1 11 poundmdash Tr i ch I oroet hane ND 1 1-43-E 3 030 Be-rampiie ND 1 1O-75- c 3AD7pound pound-Ch Io roe thy 1 vir yI ether ND 15 5-S5-S 3pound1 04 BroMof orm ND J pound7-18-4 34475 Tet raeh J oroet hyI ene ND 1 9-34-5 345 bullpound 1 1raquo poundpoundmdash etraeh i oroet hane ND 1 08-86-3 340 i 0 To uene ND 1 08-30-7 34301 Ch I ore be -2 ene ND 1 DO-41-4 34371 Etny loenzene ND 1 D7-0pound-S 34pound10 ND 50 07-13-1 34S15 fiery J oni tri ie ND SO
Dicni orobenzene isomers ND pound li pound-Tr ichloromdash 1 pound poundmdash
tr i f i uoroet hane gt -64-1 Si55pound fleet one ND 43 -15-0 770 -1 Carbon Disulfide ND 4
lteontgt
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOOO539
Llt= EMVISQNttENTftL PROTECTION flBENCY
GCi-S PuRGeLfttLE GRGftNIC flNflLYSIS shy WflTER
iftfcPLE Jamo amp
CPI -VJ
67433 Corit inued
S ORpoundT VJ
Coin pound Cone ltugl_)
Det Limit
lt L t g L gt Comments
fs-93-3J08-05mdash4gt91 mdash 1 0 mdash pound0poundmdashiO-ioO-4-533-0pound-7
l
C- i 770-37 ~ t ~ 7 ~ i s pound- = pound fgt 71gt3 pound a i f _
c-Jtjra^oris V i n y l Restate 2mdashsxano-ie 4-l^iet ny i-5-Per-tanone Ptv-e^e Xy loses ( t o t a l )
3 poundmdashDi Dgtcroet Tans ltpoundDE)Tet rayr ^gt_ rtraquoran
E i y ec -poundr i
ND ND
ND ND
ND _ ND
ND ND
ND
pound4 9 5 3 1 pound 1
14 8
en ta t ive ly loen t i f i eo
C ~ 5 shy riTtc U-DS C-ja^t it atesd
f c ^ e z - - v p - _ shy _ f- Goserveo 95Corf ic ence bull gt r r v s C bullbullbullgt_bullbull r ~ pound Fecoveries t - i rn i ts
tpound-Di en ioroefcnane o4 iOO 77-^1
Tc - e re cS iUO 87-XO3
oebected
~c renter than
nn 1
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
OOOO54O Nutmeg Valley
US ENVlRDNMENTf tL PROTECTION ftGENCY REISICM I LftbORHTORY
o PLMGCQL-i-E OrtoflNIC PNflLYSIS - WrtTER
flfci_E NC 674pound7 ISC NsC DOTE OF fiNfiLYSIS 6-3-87
VTE Of- L CL-L EC I0 REFERENCE BOCK 8 IME 0- uO_ i- -----
WPLE E5u gt_ J C Det
CfiS E uRET Con pound Cone Limit Comments NO mdash bull (ugL) (ugL)
fr bullbull i T y Po 1 1 ut ant s
i-87-3 C11 o^or-ie-wiane ND 13 -83-3 Bgt- orn imetha ne ND 3 3-01-4 3 = _ b V i ny i C ~i i or i oe ND 4 J-OO-3 Cn loroethane ND pound t f v traderaquo 1jlaquo i _j_mdash pound 3 13 i ampbull ri 1e ns C ~s I orj c e ND 1 1-69-4 3ii4SS Tri ch 1 orof 1 uoromet hane ND pound fr-35-4 3r5Ol 1 1 -Di chl oroet hyl ene ND pound Sr-34-3 S-496 1 imdashDich loroethane ND 1 56-60-5 34546 1 poundmdashDi ch 1 oroet ny1 ene i somers ND pound 7-66-3 31 06 Chloroform ND 1 37-06-2 3nZ31 1 2-Dich loroethane ND 1 1-55-6 3 506 13 1mdash Tri ch loroethane ND 1 5-23-5 3T 102 Caroon Tetrach lor ide ND 1 5-pound7-4 32i0 1 Brornocl i ch 1 oromet hane ND pound 3-87-5 ZA-f 41 1 pound-D i ch J oroorooane ND 1 306 1-02-6 34G9S t- 1 3-Di ch 1 orooropene ND 1 3-01-6 331 6 J Tri ch 1 or oet ny i ene ND 1 24-48-1 3 BIOS D i brornoch 1 oromet hane ND 1 OO61-01-5 34 04 c-1 3-D i ch 1 orooropene ND 1 3-00-5 3^511 11 pound-Tr i ch 1 oroet hane ND 1 1-43-2 3403O Benzene ND 1 10-75-8 34576 pound-Ch 1 oroet hyl vinyl ether ND 15 5-pound5-pound 321 04 Brornof orrn ND 1 S7-18-4 34475 Tet rach i oroet hy 1 ene ND 1 9-34-5 34516 1 1 pound 2-Tetrach loroethane ND 1 08-88-3 3- U 1 0 Tol uene ND 1 08-90-7 34301 Ch lorobenzene ND 1 00-41-4 34371 Ethyl benzene ND 1 07-O2-8 34pound1O ficroiein ND SO 07-13-1 34215 fiery lonitri le ND 2O r Dichlorobensene isorners ND 2
11 E-Tr i ch 1 oro-poundpoundshyt r i f 1 uoroeth ane ND 5
-64-1 61552 fleet one ND 43 J-15-O 77041 Carbon Disulfide ND 4
ltcont)
i-ii- 1 7
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
US ENVIRONMENTAL PROTECTION AGENCY OOOOS41 RHGIQN I LABORATORY GCfrS PURGEPBLE ORGANIC ANALYSIS - WATER
ifiKPLE ND 874pound7 Re suit s Cont i
CPS S70RET (VD
8-33-3 a 15--5 08-05-4 77057
7 703 08-10-i OO-4S--5 33-0pound-7
n ued
Compound
pound-B-rtanorie Vinyl Acetate pound-Hexanone 4-^et hy i -pound-Pe-nt anone
Xylenes (total) j c-Di br-c-fnoethcrne (EDB) e ranyd^of uran Ethyl ether
t iveiy Identifiea
Cone (ugL)
ND ND ND ND ND ND ND ND ND
Det Limit ltugL)
pound4 9 5 3 1 pound 1
14 8
Comments
arn p i amp Pe^ c-ve laquobull_ amp bullbull f c-r
1 pound- D i en i oroet hane d4 ecover es
5Cori fid ence
i 4-Eltr-cirnofi uorobenzene
ND=rone detected
lt=IeEs than te^ than
nn
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
FACILITY SfMPLEDl Nut meg Va11ey
115 ENVIRONMENTAL PROTECTION AGENCY REGION I LABORATORY
PU96EABLE ORGANIC ANALYSIS - WATER
AMP -c NT bdquo fl^Pi-E i_rv-t~] DATE OF ANALYSIS 6-3-87 ATE D- _ f ^ laquo bv 1 mdash 1 gt i~f mdash - W87 W Uf I m
IME C- L3_ _-irM QJfVTER)
c bullBMPLE RES_ Det
CAS poundj~LR_7 uornpouna Cone L imi t Continents xND -r (UD i_) (ugL)
^ - lori ty aoi I utarits
gtbull- 1 mdash- - - _ mdash bdquo - -_ mdash-87-3 4 m ND 13 V- -fc S~
4mdash82-3 z 4 raquo z Erc i D t- na re N D 3 p-ui-4 3 J 75 V i n y l C-Icn ide ND 4 5-OO-3 3-fZ Z i ] ci r i-e bull h a rie ND CL 5-09-2 v c r v - v i f e Z - n jne vD jw ~ ~ lt _~1
3-6S-4 3r^-oC- i r icr lor-oiraquo uoroneLhane N D c 1-35-4 3A501 1 l-Dicnloroethy lene ND c 5-34-3 ZT-T^S 1 mdash Dei ior _iCl h -gtr t ND 1 56-60-5 Z-3tS l 2 - D 3 c - I r - i oetgt-gtlsgtr e x sorters ND III
7-66-3 ^ - L- _c- -c - bulllaquo ND 1 07-06-2 3^+32 1 2-D 3 c ~i ] o --oe c IT a bull e ND 1
trer C JwJI O 3--- t - _ -Vr ich - crcetnar e NT 1
6-23-5 3= 102 Caoori Te-crfic1) lor ioamp ND H
5-27-4 3Jo B ^i^oc _c~ ioronej hane ND mdashr
8-37-r raquo i raquo Z - D i e - io^DDrcoanr ND 3 OO61-Ot-f Z-^= - t- j 3-D ici Ici- oprope-ne ND i
Dr9-0 -k r ~f n cniorclaquoeuro3t Ty Icne ND 1
i - ^ iE x fcraquojf mdash i mdash t^ t iin _ llfr u t raquo iS
OO6-oi f ~ bull ^ _ -t c mdash 3- T 1 _ I i o - o o o oe f f S 1 9-oc-s _ mdash ^ - pound-Tr-ic~t i or ethane ND i
4l-43-pound i4 3gt^ Es re-e ND J
10-pound-fc Z -s 7 Z Z-Zr crocfiy 1 v i ny 1 ether ND 15 5mdash25-2 zz 0 Er onifclt^^ ND 1
TS7-1G-4 34^- bull= et racn 1 oi-oebhy jene ND 9-34-5 345 c 11 2 2- et rach ^ oroet nano ND 1 06-6S-2 3r jC Tol uene ND 1 oe-go-7 3r301 C-i I ore oenzena ND 1 OO-41-4 34371 Et lt ~ gt i berrene ND 1 07-02-8 3421O Ac ro i ei n ND 5O 07-13-i 34215 Aery I on 1 1 r i ie ND 20
Dic^ lorobpnzene A sowers ND 2 11 2-Tr ich loro-1 2 poundshy
t r i f 1 u Ci^oet h ane ND 5 -6mdashI 81552 Acetone ND 43 J-15-O 77041 Caroon P i s u l f i d e ND 4
(eon t )
nn 1 lt3
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334
0000543
US ENVIRONMENTAL PROTECTION RGENCY REGION I LABORATORY GCM3 PURGEfiBLE ORBONIC flNOLYSIS - WATER
fc AM PL E NO i 674poundpound Jamp 1 e rce-sbull 11s Cont inued
Det CPE S-QRET Cornpourid Cone L i m i t V3 NC ( u r L ) ( u g L )
SI 595 poundmdashButanone ND 06-O5-4 77057 Vinyl fleetate ND 91-10-6 77103 ND O8-1O-1 61536 4mdashMethylmdashpoundmdashPentanone ND OO-4pound-5 El 703 Styrene ND 33-02-7 pound- bull 55 Xylenes (total) ND
1 K-Di brornc ltt hc-nc (EDBgt ND ~e i- ratydroFiiran ND ETMyl ether ND
pound4 9 5 3 1 pound 1 14 3
Comments
Tentatively Icentifies
Gf-er Compounds Quant it at ed
ample Recoveries for Observed urrocate Cirnsurd5 Recoveries Limits
1pound-Dichloroethaned4 1OO 77-317 Benzene dS 114 3pound-lpoundpound
[ ToluenedS 99 67-109 f 14-Bromof1 uorobenzene 1O8 89-113
tes ND-none detected
lt=less than gt=arfater than
- barcode 41334
- barcodetext SEMS Doc ID 41334