j45537-1 nj full package final report
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ANALYTICAL REPORT
Job Number 460-45537-1
Job Description 17338-TO4-2012 RACER GM Wilmington
ForConestoga-Rovers amp Associates Inc
2055 Niagara Falls Blvd Suite 3Niagara Falls NY 14304
Attention Ms Sue Scrocchi
_____________________________________________
Approved for releaseJanet MosleyProject Mgmt Assistant10162012 243 PM
Designee forJamie Capaci
Project Manager Ijamiecapacitestamericainccom
10162012
cc Chris Barton
The test results in this report meet all NELAP requirements unless specified within the case narrative Pursuant toNELAP this report may not be reproduced except in full without the written approval of the laboratory All questionsregarding this report should be directed to the TestAmerica Edison Project Manager
TestAmerica Edison Certifications and Approvals Connecticut CTDOH PH-0200 New Jersey NJDEP (NELAP)12028 New York NYDOH (NELAP) 11452 NYDOH (ELAP) 11452 Pennsylvania PADEP (NELAP) 68-00522 andRhode Island RIDOH LAO00132
TestAmerica Laboratories Inc
TestAmerica Edison 777 New Durham Road Edison NJ 08817
Tel (732) 549-3900 Fax (732) 549-3679 wwwtestamericainccom
10162012Page 1 of 323
Table of ContentsCover Title Page 1
Data Summaries 4
Report Narrative 4
Sample Summary 5
Executive Summary 6
Method Summary 7
Method Analyst Summary 8
Sample Datasheets 9
Surrogate Summary 22
QC Data Summary 24
Data Qualifiers 35
QC Association Summary 36
Lab Chronicle 37
Organic Sample Data 39
GCMS VOA 39
Method 8260 DEL 39Method 8260 DEL QC Summary 40Method 8260 DEL Sample Data 51Standards Data 72
Method 8260 DEL ICAL Data 72Method 8260 DEL CCAL Data 96
Raw QC Data 106Method 8260 DEL Tune Data 106Method 8260 DEL Blank Data 114Method 8260 DEL LCSLCSD Data 119Method 8260 DEL MSMSD Data 124
10162012Page 2 of 323
Table of ContentsMethod 8260 DEL Run Logs 134Method 8260 DEL Prep Data 136
GC Semi VOA 140
Method 8082 - Delaware 140Method 8082 - Delaware QC Summary 141Method 8082 - Delaware Sample Data 151Standards Data 163
Method 8082 - Delaware ICAL Data 163Method 8082 - Delaware CCAL Data 256
Raw QC Data 276Method 8082 - Delaware Blank Data 276Method 8082 - Delaware LCSLCSD Data 294
Method 8082 - Delaware Run Logs 314Method 8082 - Delaware Prep Data 316
Shipping and Receiving Documents 321
Client Chain of Custody 322
Sample Receipt Checklist 323
10162012Page 3 of 323
CASE NARRATIVE
Client Conestoga-Rovers amp Associates Inc
Project 17338-TO4-2012 RACER GM Wilmington
Report Number 460-45537-1
This case narrative is in the form of an exception report where only the anomalies related to this report method specific performance
andor QAQC issues are discussed If there are no issues to report this narrative will include a statement that documents that there are
no relevant data issues
It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting
limits in some cases Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables
quantification of target analytes or interferences which exceed the calibration range of the instrument
Calculations are performed before rounding to avoid round-off errors in calculated results
All holding times were met and proper preservation noted for the methods performed on these samples unless otherwise detailed in the
individual sections below
RECEIPT
The samples were received on 10052012 710 PM the samples arrived in good condition properly preserved and on ice The
temperature of the coolers at receipt was 32 C
Note All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required
temperature or method specified range For samples with a specified temperature of 4C samples with a temperature ranging from just
above freezing temperature of water to 6C shall be acceptable Samples that are hand delivered immediately following collection may not
meet these criteria however they will be deemed acceptable according to NELAC standards if there is evidence that the chilling process
has begun such as arrival on ice etc
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 460-45537-1 and 460-45537-2 were analyzed for polychlorinated biphenyls (PCBs) in accordance with EPA SW-846 Method
8082DEL The samples were prepared on 10082012 and analyzed on 10092012
No difficulties were encountered during the PCBs analyses
All quality control parameters were within the acceptance limits
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 460-45537-1 through 460-45537-3 were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846
Method 8260B The samples were analyzed on 10112012 and 10122012
The matrix spike matrix spike duplicate (MSMSD) recoveries for batch 131656 were outside control limits 12-Dibromo-3-chloropropane
The MSD recoveries were also outside control limits for trans-13-Dichloropropene and Methyl tert-butyl ether The associated laboratory
control sample (LCS) recoveries met acceptance criteria
12-Dibromo-3-Chloropropane failed the recovery criteria high for the MS of sample 460-45537-2 in batch 460-131656
12-Dibromo-3-Chloropropane Methyl tert-butyl ether and trans-13-Dichloropropene failed the recovery criteria high for the MSD of
sample 460-45537-2 in batch 460-131656
Refer to the QC report for details
No other difficulties were encountered during the volatiles analyses
All other quality control parameters were within the acceptance limits
10162012Page 4 of 323
SAMPLE SUMMARY
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
DateTime DateTime
460-45537-1 WC-17338-100512-MW14-MM-2
51
Water 10052012 1000 10052012 1910
460-45537-2 WC-17338-100512-MW101-MM-
252
Water 10052012 1230 10052012 1910
460-45537-3TB TB-17338-100512-253 Water 10052012 0000 10052012 1910
TestAmerica Edison 10162012Page 5 of 323
EXECUTIVE SUMMARY - Detections
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
460-45537-1 WC-17338-100512-MW14-MM-251
10 ugL 8260B017 JMethyl tert-butyl ether
10 ugL 8260B017 JToluene
10 ugL 8260B028 JTetrachloroethene
460-45537-2 WC-17338-100512-MW101-MM-252
10 ugL 8260B020 JMethyl tert-butyl ether
460-45537-3TB TB-17338-100512-253
10 ugL 8260B074 JMethylene Chloride
10 ugL 8260B0096 JChloroform
TestAmerica Edison 10162012Page 6 of 323
METHOD SUMMARY
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Preparation MethodMethodLab LocationDescription
Matrix Water
Volatile Organics (GCMS) TAL EDI SW846 8260B
Purge and Trap TAL EDI SW846 5030B
Polychlorinated Biphenyls (PCBs) (GC) TAL EDI SW846 8082
Liquid-Liquid Extraction (Separatory Funnel) TAL EDI SW846 3510C
Lab References
TAL EDI = TestAmerica Edison
Method References
SW846 = Test Methods For Evaluating Solid Waste PhysicalChemical Methods Third Edition November 1986 And Its Updates
TestAmerica Edison 10162012Page 7 of 323
METHOD ANALYST SUMMARY
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Method Analyst Analyst ID
Boykin Kenneth KBSW846 8260B
Boykin Carol B CBBSW846 8082
TestAmerica Edison
10162012Page 8 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW14-MM-251
Client Matrix
460-45537-1
Water
Date Sampled 10052012 1000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2341
10112012 2341
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08983d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
0060 U 100060111-Trichloroethane
022 U 10022Dichlorodifluoromethane
010 U 10010Chloromethane
014 U 10014Vinyl chloride
018 U 10018Bromomethane
040 U 1004012-Dibromo-3-Chloropropane
021 U 1002112-Dichlorobenzene
015 U 10015Trichlorofluoromethane
0090 U 10009011-Dichloroethene
0090 U 10009012-Dichloropropane
0080 U 100080112-Trichloro-122-trifluoroethane
27 U 5027Acetone
013 U 10013Carbon disulfide
034 U 20034Methyl acetate
018 U 10018Methylene Chloride
013 U 10013trans-12-Dichloroethene
020 U 10020Chlorodibromomethane
017 J 10014Methyl tert-butyl ether
017 U 10017Chloroethane
013 U 1001311-Dichloroethane
018 U 10018cis-12-Dichloroethene
23 U 50232-Butanone (MEK)
0080 U 100080Chloroform
010 U 10010Ethylbenzene
016 U 10016Cyclohexane
0060 U 100060Carbon tetrachloride
0080 U 100080Benzene
019 U 1001912-Dichloroethane
0090 U 100090Trichloroethene
014 U 10014Methylcyclohexane
012 U 10012Dichlorobromomethane
018 U 10018cis-13-Dichloropropene
099 U 500994-Methyl-2-pentanone (MIBK)
017 J 10015Toluene
024 U 10024trans-13-Dichloropropene
019 U 10019112-Trichloroethane
028 J 10010Tetrachloroethene
050 U 500502-Hexanone
028 U 1002812-Dibromoethane
011 U 10011Chlorobenzene
036 U 30036Xylenes Total
012 U 10012Styrene
019 U 10019Bromoform
0080 U 100080Isopropylbenzene
016 U 100161122-Tetrachloroethane
014 U 1001413-Dichlorobenzene
TestAmerica Edison 10162012Page 9 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW14-MM-251
Client Matrix
460-45537-1
Water
Date Sampled 10052012 1000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2341
10112012 2341
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08983d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
023 U 1002314-Dichlorobenzene
034 U 10034124-Trichlorobenzene
Surrogate Rec Acceptance LimitsQualifier
97 70 - 13012-Dichloroethane-d4 (Surr)
99 70 - 1304-Bromofluorobenzene
96 70 - 130Toluene-d8 (Surr)
TestAmerica Edison 10162012Page 10 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW14-MM-251
Client Matrix
460-45537-1
Water
Date Sampled 10052012 1000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2341
10112012 2341
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08983d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Tentatively Identified Compounds
QualifierEst Result (ugL)RTAnalyteCas Number
0Number TICs Found
NoneTentatively Identified Compound
TestAmerica Edison 10162012Page 11 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW101-MM-252
Client Matrix
460-45537-2
Water
Date Sampled 10052012 1230
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10122012 0004
10122012 0004
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08984d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
0060 U 100060111-Trichloroethane
022 U 10022Dichlorodifluoromethane
010 U 10010Chloromethane
014 U 10014Vinyl chloride
018 U 10018Bromomethane
040 U 1004012-Dibromo-3-Chloropropane
021 U 1002112-Dichlorobenzene
015 U 10015Trichlorofluoromethane
0090 U 10009011-Dichloroethene
0090 U 10009012-Dichloropropane
0080 U 100080112-Trichloro-122-trifluoroethane
27 U 5027Acetone
013 U 10013Carbon disulfide
034 U 20034Methyl acetate
018 U 10018Methylene Chloride
013 U 10013trans-12-Dichloroethene
020 U 10020Chlorodibromomethane
020 J 10014Methyl tert-butyl ether
017 U 10017Chloroethane
013 U 1001311-Dichloroethane
018 U 10018cis-12-Dichloroethene
23 U 50232-Butanone (MEK)
0080 U 100080Chloroform
010 U 10010Ethylbenzene
016 U 10016Cyclohexane
0060 U 100060Carbon tetrachloride
0080 U 100080Benzene
019 U 1001912-Dichloroethane
0090 U 100090Trichloroethene
014 U 10014Methylcyclohexane
012 U 10012Dichlorobromomethane
018 U 10018cis-13-Dichloropropene
099 U 500994-Methyl-2-pentanone (MIBK)
015 U 10015Toluene
024 U 10024trans-13-Dichloropropene
019 U 10019112-Trichloroethane
010 U 10010Tetrachloroethene
050 U 500502-Hexanone
028 U 1002812-Dibromoethane
011 U 10011Chlorobenzene
036 U 30036Xylenes Total
012 U 10012Styrene
019 U 10019Bromoform
0080 U 100080Isopropylbenzene
016 U 100161122-Tetrachloroethane
014 U 1001413-Dichlorobenzene
TestAmerica Edison 10162012Page 12 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW101-MM-252
Client Matrix
460-45537-2
Water
Date Sampled 10052012 1230
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10122012 0004
10122012 0004
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08984d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
023 U 1002314-Dichlorobenzene
034 U 10034124-Trichlorobenzene
Surrogate Rec Acceptance LimitsQualifier
97 70 - 13012-Dichloroethane-d4 (Surr)
98 70 - 1304-Bromofluorobenzene
97 70 - 130Toluene-d8 (Surr)
TestAmerica Edison 10162012Page 13 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW101-MM-252
Client Matrix
460-45537-2
Water
Date Sampled 10052012 1230
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10122012 0004
10122012 0004
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08984d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Tentatively Identified Compounds
QualifierEst Result (ugL)RTAnalyteCas Number
0Number TICs Found
NoneTentatively Identified Compound
TestAmerica Edison 10162012Page 14 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
TB-17338-100512-253
Client Matrix
460-45537-3TB
Water
Date Sampled 10052012 0000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2317
10112012 2317
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08982d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
0060 U 100060111-Trichloroethane
022 U 10022Dichlorodifluoromethane
010 U 10010Chloromethane
014 U 10014Vinyl chloride
018 U 10018Bromomethane
040 U 1004012-Dibromo-3-Chloropropane
021 U 1002112-Dichlorobenzene
015 U 10015Trichlorofluoromethane
0090 U 10009011-Dichloroethene
0090 U 10009012-Dichloropropane
0080 U 100080112-Trichloro-122-trifluoroethane
27 U 5027Acetone
013 U 10013Carbon disulfide
034 U 20034Methyl acetate
074 J 10018Methylene Chloride
013 U 10013trans-12-Dichloroethene
020 U 10020Chlorodibromomethane
014 U 10014Methyl tert-butyl ether
017 U 10017Chloroethane
013 U 1001311-Dichloroethane
018 U 10018cis-12-Dichloroethene
23 U 50232-Butanone (MEK)
0096 J 100080Chloroform
010 U 10010Ethylbenzene
016 U 10016Cyclohexane
0060 U 100060Carbon tetrachloride
0080 U 100080Benzene
019 U 1001912-Dichloroethane
0090 U 100090Trichloroethene
014 U 10014Methylcyclohexane
012 U 10012Dichlorobromomethane
018 U 10018cis-13-Dichloropropene
099 U 500994-Methyl-2-pentanone (MIBK)
015 U 10015Toluene
024 U 10024trans-13-Dichloropropene
019 U 10019112-Trichloroethane
010 U 10010Tetrachloroethene
050 U 500502-Hexanone
028 U 1002812-Dibromoethane
011 U 10011Chlorobenzene
036 U 30036Xylenes Total
012 U 10012Styrene
019 U 10019Bromoform
0080 U 100080Isopropylbenzene
016 U 100161122-Tetrachloroethane
014 U 1001413-Dichlorobenzene
TestAmerica Edison 10162012Page 15 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
TB-17338-100512-253
Client Matrix
460-45537-3TB
Water
Date Sampled 10052012 0000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2317
10112012 2317
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08982d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
023 U 1002314-Dichlorobenzene
034 U 10034124-Trichlorobenzene
Surrogate Rec Acceptance LimitsQualifier
97 70 - 13012-Dichloroethane-d4 (Surr)
99 70 - 1304-Bromofluorobenzene
97 70 - 130Toluene-d8 (Surr)
TestAmerica Edison 10162012Page 16 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
TB-17338-100512-253
Client Matrix
460-45537-3TB
Water
Date Sampled 10052012 0000
Date Received 10052012 1910
8260B Volatile Organics (GCMS)
Dilution
10112012 2317
10112012 2317
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
e08982d
5 mL
5 mL
5030B
VOAMS5
Analysis Date
Prep Date
Analysis Batch
Prep Batch
460-131656
NA
Analysis Method
Prep Method
Tentatively Identified Compounds
QualifierEst Result (ugL)RTAnalyteCas Number
0Number TICs Found
NoneTentatively Identified Compound
TestAmerica Edison 10162012Page 17 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW14-MM-251
Client Matrix
460-45537-1
Water
Date Sampled 10052012 1000
Date Received 10052012 1910
8082 Polychlorinated Biphenyls (PCBs) (GC)
Dilution
8082
3510C
10
10092012 0029
10082012 0755
Instrument ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Result Type PRIMARY
980 mL
5 mL
PESTGC9
Analysis Date
Prep Date
Analysis Batch 460-131137
460-130997Prep Batch
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
013 U 051013PCB-1016
029 U 051029PCB-1221
012 U 051012PCB-1232
012 U 051012PCB-1242
024 U 051024PCB-1248
017 U 051017PCB-1254
015 U 051015PCB-1260
Surrogate Rec Acceptance LimitsQualifier
83 37 - 150DCB Decachlorobiphenyl
TestAmerica Edison 10162012Page 18 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW14-MM-251
Client Matrix
460-45537-1
Water
Date Sampled 10052012 1000
Date Received 10052012 1910
8082 Polychlorinated Biphenyls (PCBs) (GC)
Dilution
8082
3510C
10
10092012 0029
10082012 0755
Instrument ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Result Type SECONDARY
980 mL
5 mL
PESTGC9
Analysis Date
Prep Date
Analysis Batch 460-131137
460-130997Prep Batch
Analysis Method
Prep Method
Surrogate Rec Acceptance LimitsQualifier
82 37 - 150DCB Decachlorobiphenyl
TestAmerica Edison 10162012Page 19 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW101-MM-252
Client Matrix
460-45537-2
Water
Date Sampled 10052012 1230
Date Received 10052012 1910
8082 Polychlorinated Biphenyls (PCBs) (GC)
Dilution
8082
3510C
10
10092012 0045
10082012 0755
Instrument ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Result Type PRIMARY
990 mL
5 mL
PESTGC9
Analysis Date
Prep Date
Analysis Batch 460-131137
460-130997Prep Batch
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
013 U 051013PCB-1016
028 U 051028PCB-1221
012 U 051012PCB-1232
012 U 051012PCB-1242
024 U 051024PCB-1248
017 U 051017PCB-1254
015 U 051015PCB-1260
Surrogate Rec Acceptance LimitsQualifier
52 37 - 150DCB Decachlorobiphenyl
TestAmerica Edison 10162012Page 20 of 323
Analytical Data
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Client Sample ID
Lab Sample ID
WC-17338-100512-MW101-MM-252
Client Matrix
460-45537-2
Water
Date Sampled 10052012 1230
Date Received 10052012 1910
8082 Polychlorinated Biphenyls (PCBs) (GC)
Dilution
8082
3510C
10
10092012 0045
10082012 0755
Instrument ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Result Type SECONDARY
990 mL
5 mL
PESTGC9
Analysis Date
Prep Date
Analysis Batch 460-131137
460-130997Prep Batch
Analysis Method
Prep Method
Surrogate Rec Acceptance LimitsQualifier
50 37 - 150DCB Decachlorobiphenyl
TestAmerica Edison 10162012Page 21 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Surrogate Recovery Report
8260B Volatile Organics (GCMS)
Client Matrix Water
Lab Sample ID Client Sample ID
DCA TOL BFB
Rec Rec Rec
460-45537-1 WC-17338-100512-M
W14-MM-251
97 96 99
460-45537-2 WC-17338-100512-M
W101-MM-252
97 97 98
460-45537-3 TB-17338-100512-25
3
97 97 99
MB 460-1316564 99 96 95
LCS 460-1316563 96 99 97
460-45537-2 MS WC-17338-100512-M
W101-MM-252 MS
96 99 99
460-45537-2 MSD WC-17338-100512-M
W101-MM-252 MSD
96 99 97
Surrogate Acceptance Limits
DCA = 12-Dichloroethane-d4 (Surr) 70-130
TOL = Toluene-d8 (Surr) 70-130
BFB = 4-Bromofluorobenzene 70-130
TestAmerica Edison
10162012Page 22 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Surrogate Recovery Report
8082 Polychlorinated Biphenyls (PCBs) (GC)
Client Matrix Water
Lab Sample ID Client Sample ID
DCB1 DCB2
Rec Rec
460-45537-1 WC-17338-100512-M
W14-MM-251
82 83
460-45537-2 WC-17338-100512-M
W101-MM-252
52 50
MB 460-1309971-A 97 88
LCS 460-1309972-A 91 84
LCSD
460-1309973-A
108 99
Surrogate Acceptance Limits
DCB = DCB Decachlorobiphenyl 37-150
TestAmerica Edison
10162012Page 23 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 460-131656
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
e08981d
5 mL
5 mLUnits ugL
Method 8260B
Preparation 5030B
VOAMS5MB 460-1316564
Analysis Date 10112012 2247
Analysis Batch
Prep Batch
Leach Batch
NA
NA
460-131656
Prep Date
Leach Date
10112012 2247
NA
Analyte RLMDLQualResult
0060 U 100060111-Trichloroethane
022 U 10022Dichlorodifluoromethane
010 U 10010Chloromethane
014 U 10014Vinyl chloride
018 U 10018Bromomethane
040 U 1004012-Dibromo-3-Chloropropane
021 U 1002112-Dichlorobenzene
015 U 10015Trichlorofluoromethane
0090 U 10009011-Dichloroethene
0090 U 10009012-Dichloropropane
0080 U 100080112-Trichloro-122-trifluoroethane
27 U 5027Acetone
013 U 10013Carbon disulfide
034 U 20034Methyl acetate
018 U 10018Methylene Chloride
013 U 10013trans-12-Dichloroethene
020 U 10020Chlorodibromomethane
014 U 10014Methyl tert-butyl ether
017 U 10017Chloroethane
013 U 1001311-Dichloroethane
018 U 10018cis-12-Dichloroethene
23 U 50232-Butanone (MEK)
0080 U 100080Chloroform
010 U 10010Ethylbenzene
016 U 10016Cyclohexane
0060 U 100060Carbon tetrachloride
0080 U 100080Benzene
019 U 1001912-Dichloroethane
0090 U 100090Trichloroethene
014 U 10014Methylcyclohexane
012 U 10012Dichlorobromomethane
018 U 10018cis-13-Dichloropropene
099 U 500994-Methyl-2-pentanone (MIBK)
015 U 10015Toluene
024 U 10024trans-13-Dichloropropene
019 U 10019112-Trichloroethane
010 U 10010Tetrachloroethene
050 U 500502-Hexanone
028 U 1002812-Dibromoethane
011 U 10011Chlorobenzene
036 U 30036Xylenes Total
012 U 10012Styrene
019 U 10019Bromoform
0080 U 100080Isopropylbenzene
016 U 100161122-Tetrachloroethane
TestAmerica Edison 10162012Page 24 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 460-131656
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
e08981d
5 mL
5 mLUnits ugL
Method 8260B
Preparation 5030B
VOAMS5MB 460-1316564
Analysis Date 10112012 2247
Analysis Batch
Prep Batch
Leach Batch
NA
NA
460-131656
Prep Date
Leach Date
10112012 2247
NA
Analyte RLMDLQualResult
014 U 1001413-Dichlorobenzene
023 U 1002314-Dichlorobenzene
034 U 10034124-Trichlorobenzene
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 99 70 - 130
4-Bromofluorobenzene 95 70 - 130
Toluene-d8 (Surr) 96 70 - 130
Method Blank TICs- Batch 460-131656
Cas Number Analyte RT Est Result Qual
Tentatively Identified Compound None
TestAmerica Edison 10162012Page 25 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Water
10
Lab Control Sample - Batch 460-131656
Client Matrix
Lab Sample ID
Dilution
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
e08977d
5 mL
5 mLUnits ugL
Method 8260B
Preparation 5030B
VOAMS5LCS 460-1316563
Analysis Date 10112012 2113
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
Prep Date
Leach Date
10112012 2113
NA
Analyte QualLimit RecResultSpike Amount
200 210 105 74 - 128111-Trichloroethane
200 181 90 46 - 145Dichlorodifluoromethane
200 210 105 58 - 146Chloromethane
200 203 101 61 - 144Vinyl chloride
200 211 105 55 - 153Bromomethane
200 222 111 70 - 11612-Dibromo-3-Chloropropane
200 209 104 82 - 12212-Dichlorobenzene
200 190 95 69 - 147Trichlorofluoromethane
200 223 112 56 - 13911-Dichloroethene
200 211 106 80 - 12012-Dichloropropane
200 203 102 47 - 139112-Trichloro-122-trifluoroethane
200 250 125 45 - 156Acetone
200 218 109 58 - 139Carbon disulfide
200 220 110 50 - 151Methyl acetate
200 200 100 79 - 119Methylene Chloride
200 216 108 75 - 122trans-12-Dichloroethene
200 217 109 80 - 120Chlorodibromomethane
200 207 104 71 - 115Methyl tert-butyl ether
200 201 101 69 - 145Chloroethane
200 204 102 78 - 12211-Dichloroethane
200 211 106 80 - 120cis-12-Dichloroethene
200 214 107 65 - 1142-Butanone (MEK)
200 205 103 82 - 123Chloroform
200 206 103 79 - 126Ethylbenzene
200 208 104 58 - 133Cyclohexane
200 211 105 73 - 120Carbon tetrachloride
200 212 106 83 - 124Benzene
200 204 102 74 - 11812-Dichloroethane
200 212 106 78 - 119Trichloroethene
200 215 107 61 - 129Methylcyclohexane
200 214 107 79 - 119Dichlorobromomethane
200 216 108 80 - 120cis-13-Dichloropropene
200 214 107 53 - 1204-Methyl-2-pentanone (MIBK)
200 205 103 80 - 120Toluene
200 215 108 78 - 118trans-13-Dichloropropene
200 217 109 79 - 119112-Trichloroethane
200 210 105 68 - 139Tetrachloroethene
200 201 100 53 - 1212-Hexanone
200 215 107 78 - 11812-Dibromoethane
200 206 103 81 - 121Chlorobenzene
600 612 102 76 - 121Xylenes Total
200 207 104 69 - 112Styrene
200 217 109 73 - 123Bromoform
200 207 104 80 - 125Isopropylbenzene
200 210 105 74 - 1261122-Tetrachloroethane
200 204 102 81 - 12613-Dichlorobenzene
TestAmerica Edison 10162012Page 26 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Water
10
Lab Control Sample - Batch 460-131656
Client Matrix
Lab Sample ID
Dilution
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
e08977d
5 mL
5 mLUnits ugL
Method 8260B
Preparation 5030B
VOAMS5LCS 460-1316563
Analysis Date 10112012 2113
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
Prep Date
Leach Date
10112012 2113
NA
Analyte QualLimit RecResultSpike Amount
200 204 102 83 - 12314-Dichlorobenzene
200 220 110 66 - 120124-Trichlorobenzene
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 96 70 - 130
4-Bromofluorobenzene 97 70 - 130
Toluene-d8 (Surr) 99 70 - 130
TestAmerica Edison 10162012Page 27 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Dilution
Dilution
Water
50
50
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
e08985d
5 mL
5 mL
e08986d
5 mL
5 mL
Method 8260B
Preparation 5030B
VOAMS5
VOAMS5
460-45537-2
460-45537-2
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 460-131656
10122012 0027
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
Analysis Date
Prep Date
Leach Date
10122012 0051
10122012 0051
NA
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
10122012 0027
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
103 106 74 - 128 3 30111-Trichloroethane
87 90 46 - 145 4 30Dichlorodifluoromethane
102 101 58 - 146 0 30Chloromethane
104 105 61 - 144 0 30Vinyl chloride
107 105 55 - 153 2 30Bromomethane
121 121 70 - 116 0 30 F F12-Dibromo-3-Chloropropane
107 111 82 - 122 3 3012-Dichlorobenzene
121 100 69 - 147 19 30Trichlorofluoromethane
108 119 56 - 139 9 3011-Dichloroethene
111 110 80 - 120 0 3012-Dichloropropane
102 111 47 - 139 8 30112-Trichloro-122-trifluoroethane
99 101 45 - 156 2 30Acetone
113 119 58 - 139 5 30Carbon disulfide
100 101 50 - 151 1 30Methyl acetate
106 106 79 - 119 0 30Methylene Chloride
106 108 75 - 122 2 30trans-12-Dichloroethene
116 118 80 - 120 2 30Chlorodibromomethane
114 116 71 - 115 1 30 FMethyl tert-butyl ether
116 105 69 - 145 10 30Chloroethane
104 111 78 - 122 7 3011-Dichloroethane
105 109 80 - 120 4 30cis-12-Dichloroethene
111 114 65 - 114 3 302-Butanone (MEK)
108 113 82 - 123 4 30Chloroform
107 111 79 - 126 3 30Ethylbenzene
108 117 58 - 133 7 30Cyclohexane
105 110 73 - 120 5 30Carbon tetrachloride
106 114 83 - 124 7 30Benzene
107 109 74 - 118 2 3012-Dichloroethane
107 113 78 - 119 5 30Trichloroethene
115 121 61 - 129 5 30Methylcyclohexane
113 116 79 - 119 3 30Dichlorobromomethane
109 115 80 - 120 5 30cis-13-Dichloropropene
111 114 53 - 120 3 304-Methyl-2-pentanone (MIBK)
TestAmerica Edison 10162012Page 28 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Dilution
Dilution
Water
50
50
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
e08985d
5 mL
5 mL
e08986d
5 mL
5 mL
Method 8260B
Preparation 5030B
VOAMS5
VOAMS5
460-45537-2
460-45537-2
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 460-131656
10122012 0027
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
Analysis Date
Prep Date
Leach Date
10122012 0051
10122012 0051
NA
Analysis Batch
Prep Batch
Leach Batch
460-131656
NA
NA
10122012 0027
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
106 111 80 - 120 5 30Toluene
113 119 78 - 118 5 30 Ftrans-13-Dichloropropene
112 116 79 - 119 3 30112-Trichloroethane
110 116 68 - 139 5 30Tetrachloroethene
109 111 53 - 121 2 302-Hexanone
116 117 78 - 118 1 3012-Dibromoethane
107 111 81 - 121 3 30Chlorobenzene
106 110 76 - 121 3 30Xylenes Total
107 110 69 - 112 3 30Styrene
115 114 73 - 123 1 30Bromoform
107 111 80 - 125 4 30Isopropylbenzene
115 116 74 - 126 0 301122-Tetrachloroethane
106 110 81 - 126 4 3013-Dichlorobenzene
106 110 83 - 123 4 3014-Dichlorobenzene
110 119 66 - 120 8 30124-Trichlorobenzene
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 96 96 70 - 130
4-Bromofluorobenzene 99 97 70 - 130
Toluene-d8 (Surr) 99 99 70 - 130
TestAmerica Edison 10162012Page 29 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Water
10122012 0027 10122012 0051
Dilution Dilution50 50
Client Matrix Client Matrix Water
Method 8260B
Preparation 5030B
Units ugL460-45537-2 460-45537-2MS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 460-131656
Analysis Date
Prep Date
Leach Date
10122012 0027
NA
Analysis Date
Prep Date
Leach Date
10122012 0051
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
0060 U 100 100 103 106111-Trichloroethane
022 U 100 100 865 896Dichlorodifluoromethane
010 U 100 100 102 101Chloromethane
014 U 100 100 104 105Vinyl chloride
018 U 100 100 107 105Bromomethane
040 U 100 100 121 121F F12-Dibromo-3-Chloropropane
021 U 100 100 107 11112-Dichlorobenzene
015 U 100 100 121 997Trichlorofluoromethane
0090 U 100 100 108 11911-Dichloroethene
0090 U 100 100 111 11012-Dichloropropane
0080 U 100 100 102 111112-Trichloro-122-trifluoroethane
27 U 100 100 986 101Acetone
013 U 100 100 113 119Carbon disulfide
034 U 100 100 100 101Methyl acetate
018 U 100 100 106 106Methylene Chloride
013 U 100 100 106 108trans-12-Dichloroethene
020 U 100 100 116 118Chlorodibromomethane
020 J 100 100 114 116 FMethyl tert-butyl ether
017 U 100 100 116 105Chloroethane
013 U 100 100 104 11111-Dichloroethane
018 U 100 100 105 109cis-12-Dichloroethene
23 U 100 100 111 1142-Butanone (MEK)
0080 U 100 100 108 113Chloroform
010 U 100 100 107 111Ethylbenzene
016 U 100 100 108 117Cyclohexane
0060 U 100 100 105 110Carbon tetrachloride
0080 U 100 100 106 114Benzene
019 U 100 100 107 10912-Dichloroethane
0090 U 100 100 107 113Trichloroethene
014 U 100 100 115 121Methylcyclohexane
012 U 100 100 113 116Dichlorobromomethane
018 U 100 100 109 115cis-13-Dichloropropene
099 U 100 100 111 1144-Methyl-2-pentanone (MIBK)
015 U 100 100 106 111Toluene
024 U 100 100 113 119 Ftrans-13-Dichloropropene
019 U 100 100 112 116112-Trichloroethane
010 U 100 100 110 116Tetrachloroethene
050 U 100 100 109 1112-Hexanone
028 U 100 100 116 11712-Dibromoethane
011 U 100 100 107 111Chlorobenzene
036 U 300 300 318 329Xylenes Total
012 U 100 100 107 110Styrene
019 U 100 100 115 114Bromoform
TestAmerica Edison 10162012Page 30 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Water
10122012 0027 10122012 0051
Dilution Dilution50 50
Client Matrix Client Matrix Water
Method 8260B
Preparation 5030B
Units ugL460-45537-2 460-45537-2MS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 460-131656
Analysis Date
Prep Date
Leach Date
10122012 0027
NA
Analysis Date
Prep Date
Leach Date
10122012 0051
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
0080 U 100 100 107 111Isopropylbenzene
016 U 100 100 115 1161122-Tetrachloroethane
014 U 100 100 106 11013-Dichlorobenzene
023 U 100 100 106 11014-Dichlorobenzene
034 U 100 100 110 119124-Trichlorobenzene
TestAmerica Edison 10162012Page 31 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 460-130997
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
vr479496d
1000 mL
5 mLUnits ugL
Method 8082
Preparation 3510C
PESTGC9MB 460-1309971-A
Analysis Date 10082012 2208
Analysis Batch
Prep Batch
Leach Batch NA
460-131137
460-130997
Prep Date Injection Volume
Leach Date
10082012 0755
NA PRIMARYColumn ID
Analyte RLMDLQualResult
013 U 050013PCB-1016
028 U 050028PCB-1221
012 U 050012PCB-1232
012 U 050012PCB-1242
024 U 050024PCB-1248
017 U 050017PCB-1254
015 U 050015PCB-1260
Surrogate Rec Acceptance Limits
DCB Decachlorobiphenyl 97 37 - 150
Surrogate Rec Acceptance Limits
DCB Decachlorobiphenyl 88 37 - 150
TestAmerica Edison 10162012Page 32 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 460-130997
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Column ID
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Column ID
ugL
vf479497d
1000 mL
5 mL
PRIMARY
vf479498d
1000 mL
5 mL
PRIMARY
ugL
Method 8082
Preparation 3510C
PESTGC9
PESTGC9
LCS 460-1309972-A
LCSD 460-1309973-A
Analysis Date
Prep Date
Leach Date
10082012 2224
10082012 0755
NA
Analysis Batch
Prep Batch
Leach Batch
460-131137
460-130997
NA
Analysis Date
Prep Date
Leach Date
10082012 2239
10082012 0755
NA
Analysis Batch
Prep Batch
Leach Batch
460-131137
460-130997
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
103101 71 - 126 2 30PCB-1016
119115 73 - 130 4 30PCB-1260
Surrogate LCS Rec LCSD Rec Acceptance Limits
DCB Decachlorobiphenyl 91 108 37 - 150
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 460-130997
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Column ID
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Injection Volume
Column ID
ugL
vr479497d
1000 mL
5 mL
SECONDARY
vr479498d
1000 mL
5 mL
SECONDARY
ugL
Method 8082
Preparation 3510C
PESTGC9
PESTGC9
LCS 460-1309972-A
LCSD 460-1309973-A
Analysis Date
Prep Date
Leach Date
10082012 2224
10082012 0755
NA
Analysis Batch
Prep Batch
Leach Batch
460-131137
460-130997
NA
Analysis Date
Prep Date
Leach Date
10082012 2239
10082012 0755
NA
Analysis Batch
Prep Batch
Leach Batch
460-131137
460-130997
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
9997 71 - 126 3 30PCB-1016
117111 73 - 130 5 30PCB-1260
Surrogate LCS Rec LCSD Rec Acceptance Limits
DCB Decachlorobiphenyl 84 99 37 - 150
TestAmerica Edison 10162012Page 33 of 323
Quality Control Results
Job Number 460-45537-1Client Conestoga-Rovers amp Associates Inc
Water
10082012 2224
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 460-130997
Method 8082
Preparation 3510C
Units ugLLCS 460-1309972-A LCSD 460-1309973-ALCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
10082012 0755
Analysis Date
Prep Date
Leach Date
10082012 2239
10082012 0755
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
516507500 500PCB-1016
595573500 500PCB-1260
Water
10082012 2224
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 460-130997
Method 8082
Preparation 3510C
Units ugLLCS 460-1309972-A LCSD 460-1309973-ALCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
10082012 0755
Analysis Date
Prep Date
Leach Date
10082012 2239
10082012 0755
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
497483500 500PCB-1016
583557500 500PCB-1260
TestAmerica Edison 10162012Page 34 of 323
DATA REPORTING QUALIFIERS
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Lab Section Qualifier Description
GCMS VOA
Indicates the analyte was analyzed for but not detectedU
MSMSD Recovery or RPD exceeds the control limitsF
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value
J
GC Semi VOA
Indicates the analyte was analyzed for but not detectedU
TestAmerica Edison 10162012Page 35 of 323
Quality Control Results
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GCMS VOA
Analysis Batch460-131656
Lab Control Sample Water 8260BLCS 460-1316563 T
Method Blank Water 8260BMB 460-1316564 T
WaterWC-17338-100512-MW14-MM-251 8260B460-45537-1 T
WaterWC-17338-100512-MW101-MM-252 8260B460-45537-2 T
Matrix Spike Water 8260B460-45537-2MS T
Matrix Spike Duplicate Water 8260B460-45537-2MSD T
WaterTB-17338-100512-253 8260B460-45537-3TB T
Report Basis
T = Total
GC Semi VOA
Prep Batch 460-130997
Lab Control Sample Water 3510CLCS 460-1309972-A T
Lab Control Sample Duplicate Water 3510CLCSD 460-1309973-A T
Method Blank Water 3510CMB 460-1309971-A T
WaterWC-17338-100512-MW14-MM-251 3510C460-45537-1 T
WaterWC-17338-100512-MW101-MM-252 3510C460-45537-2 T
Analysis Batch460-131137
Lab Control Sample Water 460-1309978082LCS 460-1309972-A T
Lab Control Sample Duplicate Water 460-1309978082LCSD 460-1309973-A T
Method Blank Water 460-1309978082MB 460-1309971-A T
Water 460-130997WC-17338-100512-MW14-MM-251 8082460-45537-1 T
Water 460-130997WC-17338-100512-MW101-MM-252 8082460-45537-2 T
Report Basis
T = Total
TestAmerica Edison
10162012Page 36 of 323
Quality Control Results
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Laboratory Chronicle
10052012 1910
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime Received DateTime10052012 1000
460-45537-1 WC-17338-100512-MW14-MM-251
P5030B 460-45537-A-1 460-131656 10112012 2341 KBTAL EDI1
A8260B 460-45537-A-1 460-131656 10112012 2341 KBTAL EDI1
P3510C 460-45537-E-1-B 460-131137 460-130997 10082012 0755 HWTAL EDI1
A8082 460-45537-E-1-B 460-131137 460-130997 10092012 0029 CBBTAL EDI1
10052012 1910
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime Received DateTime10052012 1230
460-45537-2 WC-17338-100512-MW101-MM-252
P5030B 460-45537-A-2 460-131656 10122012 0004 KBTAL EDI1
A8260B 460-45537-A-2 460-131656 10122012 0004 KBTAL EDI1
P3510C 460-45537-E-2-A 460-131137 460-130997 10082012 0755 HWTAL EDI1
A8082 460-45537-E-2-A 460-131137 460-130997 10092012 0045 CBBTAL EDI1
10052012 1910
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime Received DateTime10052012 1230
460-45537-2 MS WC-17338-100512-MW101-MM-252
P5030B 460-45537-C-2 MS 460-131656 10122012 0027 KBTAL EDI5
A8260B 460-45537-C-2 MS 460-131656 10122012 0027 KBTAL EDI5
10052012 1910
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime Received DateTime10052012 1230
460-45537-2 MSD WC-17338-100512-MW101-MM-252
P5030B 460-45537-C-2 MSD 460-131656 10122012 0051 KBTAL EDI5
A8260B 460-45537-C-2 MSD 460-131656 10122012 0051 KBTAL EDI5
10052012 1910
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime Received DateTime10052012 0000
460-45537-3 TB-17338-100512-253
P5030B 460-45537-A-3 460-131656 10112012 2317 KBTAL EDI1
A8260B 460-45537-A-3 460-131656 10112012 2317 KBTAL EDI1
A = Analytical Method P = Prep Method TestAmerica Edison
10162012Page 37 of 323
Quality Control Results
Client Conestoga-Rovers amp Associates Inc Job Number 460-45537-1
Laboratory Chronicle
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime NA Received DateTime NA
MB NA
P5030B MB 460-1316564 460-131656 10112012 2247 KBTAL EDI1
A8260B MB 460-1316564 460-131656 10112012 2247 KBTAL EDI1
P3510C MB 460-1309971-A 460-131137 460-130997 10082012 0755 HWTAL EDI1
A8082 MB 460-1309971-A 460-131137 460-130997 10082012 2208 CBBTAL EDI1
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime NA Received DateTime NA
LCS NA
P5030B LCS 460-1316563 460-131656 10112012 2113 KBTAL EDI1
A8260B LCS 460-1316563 460-131656 10112012 2113 KBTAL EDI1
P3510C LCS 460-1309972-A 460-131137 460-130997 10082012 0755 HWTAL EDI1
A8082 LCS 460-1309972-A 460-131137 460-130997 10082012 2224 CBBTAL EDI1
Lab ID
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared
Analyzed Dil Lab Analyst
Client ID
Sample DateTime NA Received DateTime NA
LCSD NA
P3510C LCSD
460-1309973-A
460-131137 460-130997 10082012 0755 HWTAL EDI1
A8082 LCSD
460-1309973-A
460-131137 460-130997 10082012 2239 CBBTAL EDI1
Lab ReferencesTAL EDI = TestAmerica Edison
A = Analytical Method P = Prep Method TestAmerica Edison
10162012Page 38 of 323
Method 8260 DELVolatile Organics (GCMS) by Method
8260 (Delaware)
10162012Page 39 of 323
FORM II
GCMS VOA SURROGATE RECOVERY
Lab Name Job No 460-45537-1
SDG No
Matrix Water Level Low
TestAmerica Edison
GC Column (1) Rtx-VMS ID 018(mm)
Lab Sample IDClient Sample ID DCA TOL BFB
460-45537-1WC-17338-100512-MW14-MM-251
97 96 99
460-45537-2WC-17338-100512-MW101-MM-252
97 97 98
460-45537-3TB-17338-100512-253
97 97 99
MB 460-1316564 99 96 95
LCS 460-1316563 96 99 97
460-45537-2 MSWC-17338-100512-MW101-MM-252 MS
96 99 99
460-45537-2 MSDWC-17338-100512-MW101-MM-252 MSD
96 99 97
QC LIMITSQC LIMITSDCA = 12-Dichloroethane-d4 (Surr) 70-130
TOL = Toluene-d8 (Surr) 70-130
BFB = 4-Bromofluorobenzene 70-130
FORM II 8260B
Column to be used to flag recovery values
10162012Page 40 of 323
GCMS VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08977dWater
Lab ID LCS 460-1316563 Client ID
TestAmerica Edison
REC
REC
QC
LIMITSCONCENTRATION
(ugL)
SPIKE
ADDED
(ugL)
LCS LCS
COMPOUND
111-Trichloroethane 200 210 74-128105
Dichlorodifluoromethane 200 181 46-14590
Chloromethane 200 210 58-146105
Vinyl chloride 200 203 61-144101
Bromomethane 200 211 55-153105
12-Dibromo-3-Chloropropane 200 222 70-116111
12-Dichlorobenzene 200 209 82-122104
Trichlorofluoromethane 200 190 69-14795
11-Dichloroethene 200 223 56-139112
12-Dichloropropane 200 211 80-120106
112-Trichloro-122-trifluoroethane
200 203 47-139102
Acetone 200 250 45-156125
Carbon disulfide 200 218 58-139109
Methyl acetate 200 220 50-151110
Methylene Chloride 200 200 79-119100
trans-12-Dichloroethene 200 216 75-122108
Chlorodibromomethane 200 217 80-120109
Methyl tert-butyl ether 200 207 71-115104
Chloroethane 200 201 69-145101
11-Dichloroethane 200 204 78-122102
cis-12-Dichloroethene 200 211 80-120106
2-Butanone (MEK) 200 214 65-114107
Chloroform 200 205 82-123103
Ethylbenzene 200 206 79-126103
Cyclohexane 200 208 58-133104
Carbon tetrachloride 200 211 73-120105
Benzene 200 212 83-124106
12-Dichloroethane 200 204 74-118102
Trichloroethene 200 212 78-119106
Methylcyclohexane 200 215 61-129107
Dichlorobromomethane 200 214 79-119107
cis-13-Dichloropropene 200 216 80-120108
4-Methyl-2-pentanone (MIBK) 200 214 53-120107
Toluene 200 205 80-120103
trans-13-Dichloropropene 200 215 78-118108
112-Trichloroethane 200 217 79-119109
Tetrachloroethene 200 210 68-139105
2-Hexanone 200 201 53-121100
12-Dibromoethane 200 215 78-118107
Chlorobenzene 200 206 81-121103
Xylenes Total 600 612 76-121102
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 41 of 323
GCMS VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08977dWater
Lab ID LCS 460-1316563 Client ID
TestAmerica Edison
REC
REC
QC
LIMITSCONCENTRATION
(ugL)
SPIKE
ADDED
(ugL)
LCS LCS
COMPOUND
Styrene 200 207 69-112104
Bromoform 200 217 73-123109
Isopropylbenzene 200 207 80-125104
1122-Tetrachloroethane 200 210 74-126105
13-Dichlorobenzene 200 204 81-126102
14-Dichlorobenzene 200 204 83-123102
124-Trichlorobenzene 200 220 66-120110
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 42 of 323
GCMS VOA MATRIX SPIKE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08985dWater
Lab ID 460-45537-2 MS Client ID WC-17338-100512-MW101-MM-252 MS
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ugL) (ugL) (ugL)
MS MS
100 103 74-128111-Trichloroethane 1030060 U
100 865 46-145Dichlorodifluoromethane 87022 U
100 102 58-146Chloromethane 102010 U
100 104 61-144Vinyl chloride 104014 U
100 107 55-153Bromomethane 107018 U
100 121 70-11612-Dibromo-3-Chloropropane 121040 U F
100 107 82-12212-Dichlorobenzene 107021 U
100 121 69-147Trichlorofluoromethane 121015 U
100 108 56-13911-Dichloroethene 1080090 U
100 111 80-12012-Dichloropropane 1110090 U
100 102 47-139112-Trichloro-122-trifluoroethane
1020080 U
100 986 45-156Acetone 9927 U
100 113 58-139Carbon disulfide 113013 U
100 100 50-151Methyl acetate 100034 U
100 106 79-119Methylene Chloride 106018 U
100 106 75-122trans-12-Dichloroethene 106013 U
100 116 80-120Chlorodibromomethane 116020 U
100 114 71-115Methyl tert-butyl ether 114020 J
100 116 69-145Chloroethane 116017 U
100 104 78-12211-Dichloroethane 104013 U
100 105 80-120cis-12-Dichloroethene 105018 U
100 111 65-1142-Butanone (MEK) 11123 U
100 108 82-123Chloroform 1080080 U
100 107 79-126Ethylbenzene 107010 U
100 108 58-133Cyclohexane 108016 U
100 105 73-120Carbon tetrachloride 1050060 U
100 106 83-124Benzene 1060080 U
100 107 74-11812-Dichloroethane 107019 U
100 107 78-119Trichloroethene 1070090 U
100 115 61-129Methylcyclohexane 115014 U
100 113 79-119Dichlorobromomethane 113012 U
100 109 80-120cis-13-Dichloropropene 109018 U
100 111 53-1204-Methyl-2-pentanone (MIBK) 111099 U
100 106 80-120Toluene 106015 U
100 113 78-118trans-13-Dichloropropene 113024 U
100 112 79-119112-Trichloroethane 112019 U
100 110 68-139Tetrachloroethene 110010 U
100 109 53-1212-Hexanone 109050 U
100 116 78-11812-Dibromoethane 116028 U
100 107 81-121Chlorobenzene 107011 U
300 318 76-121Xylenes Total 106036 U
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 43 of 323
GCMS VOA MATRIX SPIKE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08985dWater
Lab ID 460-45537-2 MS Client ID WC-17338-100512-MW101-MM-252 MS
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ugL) (ugL) (ugL)
MS MS
100 107 69-112Styrene 107012 U
100 115 73-123Bromoform 115019 U
100 107 80-125Isopropylbenzene 1070080 U
100 115 74-1261122-Tetrachloroethane 115016 U
100 106 81-12613-Dichlorobenzene 106014 U
100 106 83-12314-Dichlorobenzene 106023 U
100 110 66-120124-Trichlorobenzene 110034 U
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 44 of 323
GCMS VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08986dWater
Lab ID 460-45537-2 MSD Client ID WC-17338-100512-MW101-MM-252
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION
REC
RPD
QC LIMITS
RPD REC (ugL) (ugL)
MSD MSD
100 106 30 74-128111-Trichloroethane 3106
100 896 30 46-145Dichlorodifluoromethane 490
100 101 30 58-146Chloromethane 0101
100 105 30 61-144Vinyl chloride 0105
100 105 30 55-153Bromomethane 2105
100 121 30 70-11612-Dibromo-3-Chloropropane 0121 F
100 111 30 82-12212-Dichlorobenzene 3111
100 997 30 69-147Trichlorofluoromethane 19100
100 119 30 56-13911-Dichloroethene 9119
100 110 30 80-12012-Dichloropropane 0110
100 111 30 47-139112-Trichloro-122-trifluoroethane
8111
100 101 30 45-156Acetone 2101
100 119 30 58-139Carbon disulfide 5119
100 101 30 50-151Methyl acetate 1101
100 106 30 79-119Methylene Chloride 0106
100 108 30 75-122trans-12-Dichloroethene 2108
100 118 30 80-120Chlorodibromomethane 2118
100 116 30 71-115Methyl tert-butyl ether 1116 F
100 105 30 69-145Chloroethane 10105
100 111 30 78-12211-Dichloroethane 7111
100 109 30 80-120cis-12-Dichloroethene 4109
100 114 30 65-1142-Butanone (MEK) 3114
100 113 30 82-123Chloroform 4113
100 111 30 79-126Ethylbenzene 3111
100 117 30 58-133Cyclohexane 7117
100 110 30 73-120Carbon tetrachloride 5110
100 114 30 83-124Benzene 7114
100 109 30 74-11812-Dichloroethane 2109
100 113 30 78-119Trichloroethene 5113
100 121 30 61-129Methylcyclohexane 5121
100 116 30 79-119Dichlorobromomethane 3116
100 115 30 80-120cis-13-Dichloropropene 5115
100 114 30 53-1204-Methyl-2-pentanone (MIBK) 3114
100 111 30 80-120Toluene 5111
100 119 30 78-118trans-13-Dichloropropene 5119 F
100 116 30 79-119112-Trichloroethane 3116
100 116 30 68-139Tetrachloroethene 5116
100 111 30 53-1212-Hexanone 2111
100 117 30 78-11812-Dibromoethane 1117
100 111 30 81-121Chlorobenzene 3111
300 329 30 76-121Xylenes Total 3110
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 45 of 323
GCMS VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID e08986dWater
Lab ID 460-45537-2 MSD Client ID WC-17338-100512-MW101-MM-252
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION
REC
RPD
QC LIMITS
RPD REC (ugL) (ugL)
MSD MSD
100 110 30 69-112Styrene 3110
100 114 30 73-123Bromoform 1114
100 111 30 80-125Isopropylbenzene 4111
100 116 30 74-1261122-Tetrachloroethane 0116
100 110 30 81-12613-Dichlorobenzene 4110
100 110 30 83-12314-Dichlorobenzene 4110
100 119 30 66-120124-Trichlorobenzene 8119
FORM III 8260B
Column to be used to flag recovery and RPD values
10162012Page 46 of 323
FORM IV
GCMS VOA METHOD BLANK SUMMARY
Lab Name
SDG No
Job No 460-45537-1TestAmerica Edison
Date Analyzed
GC Column ID
Instrument ID 10112012 2247
Rtx-VMS
NHeated Purge(YN)
VOAMS5
e08981dLab File ID Lab Sample ID MB 460-1316564
WaterMatrix
018(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES
LAB SAMPLE ID
LAB
FILE ID DATE ANALYZEDCLIENT SAMPLE ID
10112012 2113e08977dLCS 460-1316563
10112012 2317e08982d460-45537-3TB-17338-100512-253
10112012 2341e08983d460-45537-1WC-17338-100512-MW14-MM-251
10122012 0004e08984d460-45537-2WC-17338-100512-MW101-MM-252
10122012 0027e08985d460-45537-2 MSWC-17338-100512-MW101-MM-252 MS
10122012 0051e08986d460-45537-2 MSDWC-17338-100512-MW101-MM-252 MSD
FORM IV 8260B
10162012Page 47 of 323
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name
SDG No
Job No 460-45537-1
Lab File ID
Instrument ID
e07834d
VOAMS5
09172012
0324
BFB Injection Date
BFB Injection Time
ME ION ABUNDANCE CRITERIA RELATIVEABUNDANCE
Analysis Batch No 128076
50 150 - 400 of mass 95 219
75 300 - 600 of mass 95 525
95 Base Peak 100 relative abundance 1000
96 50 - 90 of mass 95 64
173 Less than 20 of mass 174 00 (00)1
174 500 - 12000 of mass 95 796
175 50 - 90 of mass 174 66 (83)1
176 950 - 1010 of mass 174 761 (957)1
177 50 - 90 of mass 176 48 (63)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
GCMS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
e07836d 09172012 0449IC 460-1280762
e07838d 09172012 0536IC 460-1280763
e07839d 09172012 0600ICIS 460-1280764
e07840d 09172012 0623IC 460-1280765
e07841d 09172012 0646IC 460-1280766
e07842d 09172012 0710IC 460-1280767
FORM V 8260B 10162012Page 48 of 323
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name
SDG No
Job No 460-45537-1
Lab File ID
Instrument ID
e08975d
VOAMS5
10112012
2008
BFB Injection Date
BFB Injection Time
ME ION ABUNDANCE CRITERIA RELATIVEABUNDANCE
Analysis Batch No 131656
50 150 - 400 of mass 95 218
75 300 - 600 of mass 95 518
95 Base Peak 100 relative abundance 1000
96 50 - 90 of mass 95 65
173 Less than 20 of mass 174 07 (07)1
174 500 - 12000 of mass 95 896
175 50 - 90 of mass 174 72 (80)1
176 950 - 1010 of mass 174 872 (973)1
177 50 - 90 of mass 176 53 (61)2
1-Value is mass 174 2-Value is mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES MS MSD BLANKS AND STANDARDS
GCMS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
e08976d 10112012 2050CCVIS 460-1316562
e08977d 10112012 2113LCS 460-1316563
e08981d 10112012 2247MB 460-1316564
TB-17338-100512-253 e08982d 10112012 2317460-45537-3
WC-17338-100512-MW14-MM-251
e08983d 10112012 2341460-45537-1
WC-17338-100512-MW101-MM-252
e08984d 10122012 0004460-45537-2
WC-17338-100512-MW101-MM-252 MS
e08985d 10122012 0027460-45537-2 MS
WC-17338-100512-MW101-MM-252 MSD
e08986d 10122012 0051460-45537-2 MSD
e08987d 10122012 0114CCV 460-13165610
FORM V 8260B 10162012Page 49 of 323
GCMS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name Job No
SDG No
FORM VIII
TestAmerica Edison 460-45537-1
Sample No CCVIS 460-1316562 Date Analyzed 10112012 2050
Lab File ID (Standard) e08976d
Instrument ID VOAMS5 GC Column Rtx-VMS ID 018(mm)
Heated Purge (YN) N
Calibration ID 17515
AREA RT AREA RT AREA RT
FB CBZ DCB
UPPER LIMIT
LOWER LIMIT
2625312
656328 578671
2314682
333917
1335668
360 695 10471224 HOUR STD
410
310
745
645
1097
997
1312656 1157341 667834
LAB SAMPLE ID CLIENT SAMPLE ID
LCS 460-1316563 1318918 1146590 683882 360 695 1047
MB 460-1316564 1238441 1084553 638826 360 695 1047
460-45537-3 TB-17338-100512-253 1280000 1135339 646856 359 695 1047
460-45537-1 WC-17338-100512-MW14-MM-251
1242225 1119807 641810 359 695 1047
460-45537-2 WC-17338-100512-MW101-MM-252
1247617 1105330 633816 360 695 1047
460-45537-2 MS WC-17338-100512-MW101-MM-252 MS
1234975 1102789 642491 359 695 1047
460-45537-2 MSD WC-17338-100512-MW101-MM-252 MSD
1296388 1119645 654839 360 695 1047
CCV 460-13165610 1274024 1125053 665092 359 695 1047
FB = Fluorobenzene
CBZ = Chlorobenzene-d5
DCB = 14-Dichlorobenzene-d4
Area Limit = 50-200 of internal standard area
RT Limit = plusmn 05 minutes of internal standard RT
Column used to flag values outside QC limits
FORM VIII 8260B
10162012Page 50 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW14-MM-2
SDG No
460-45537-1
Lab Sample ID 460-45537-1
Matrix e08983dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2341
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 0060U71-55-6 111-Trichloroethane 0060
10 022U75-71-8 Dichlorodifluoromethane 022
10 010U74-87-3 Chloromethane 010
10 014U75-01-4 Vinyl chloride 014
10 018U74-83-9 Bromomethane 018
10 040U96-12-8 12-Dibromo-3-Chloropropane 040
10 021U95-50-1 12-Dichlorobenzene 021
10 015U75-69-4 Trichlorofluoromethane 015
10 0090U75-35-4 11-Dichloroethene 0090
10 0090U78-87-5 12-Dichloropropane 0090
10 0080U76-13-1 112-Trichloro-122-trifluoroethane
0080
50 27U67-64-1 Acetone 27
10 013U75-15-0 Carbon disulfide 013
20 034U79-20-9 Methyl acetate 034
10 018U75-09-2 Methylene Chloride 018
10 013U156-60-5 trans-12-Dichloroethene 013
10 020U124-48-1 Chlorodibromomethane 020
10 014J1634-04-4 Methyl tert-butyl ether 017
10 017U75-00-3 Chloroethane 017
10 013U75-34-3 11-Dichloroethane 013
10 018U156-59-2 cis-12-Dichloroethene 018
50 23U78-93-3 2-Butanone (MEK) 23
10 0080U67-66-3 Chloroform 0080
10 010U100-41-4 Ethylbenzene 010
10 016U110-82-7 Cyclohexane 016
10 0060U56-23-5 Carbon tetrachloride 0060
10 0080U71-43-2 Benzene 0080
10 019U107-06-2 12-Dichloroethane 019
10 0090U79-01-6 Trichloroethene 0090
10 014U108-87-2 Methylcyclohexane 014
10 012U75-27-4 Dichlorobromomethane 012
10 018U10061-01-5 cis-13-Dichloropropene 018
50 099U108-10-1 4-Methyl-2-pentanone (MIBK) 099
10 015J108-88-3 Toluene 017
10 024U10061-02-6 trans-13-Dichloropropene 024
FORM I 8260B
10162012Page 51 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW14-MM-2
SDG No
460-45537-1
Lab Sample ID 460-45537-1
Matrix e08983dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2341
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 019U79-00-5 112-Trichloroethane 019
10 010J127-18-4 Tetrachloroethene 028
50 050U591-78-6 2-Hexanone 050
10 028U106-93-4 12-Dibromoethane 028
10 011U108-90-7 Chlorobenzene 011
30 036U1330-20-7 Xylenes Total 036
10 012U100-42-5 Styrene 012
10 019U75-25-2 Bromoform 019
10 0080U98-82-8 Isopropylbenzene 0080
10 016U79-34-5 1122-Tetrachloroethane 016
10 014U541-73-1 13-Dichlorobenzene 014
10 023U106-46-7 14-Dichlorobenzene 023
10 034U120-82-1 124-Trichlorobenzene 034
RECCAS NO LIMITSQSURROGATE
97 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
99 70-130460-00-4 4-Bromofluorobenzene
96 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 52 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID
Lab Name Job No
WC-17338-100512-MW14-MM-2
SDG No
460-45537-1
Lab Sample ID 460-45537-1
Matrix e08983dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2341
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
Number TICs Found TIC Result Total 00
QRTCOMPOUND NAME RESULTCAS NO
Tentatively Identified Compound None
FORM I-TIC 8260B
10162012Page 53 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08983d Report Date 12-Oct-2012 0041
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08983dLab Smp Id 460-45537-A-1 Client Smp ID WC-17338-100512-MW1Inj Date 11-OCT-2012 2341 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info 460-45537-A-1Misc Info 460-45537-A-1Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 8 Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
28 MTBE 73 2016 2022 (0561) 2797 016909 017(a)
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 375883 486598 49
52 Fluorobenzene 96 3595 3601 (1000) 1242225 500000
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1240232 479413 48
66 Toluene 91 5162 5162 (0742) 4639 017041 017(a)
71 Tetrachloroethene 166 5582 5582 (0803) 1902 028047 028(a)
78 Chlorobenzene-d5 117 6954 6954 (1000) 1119807 500000
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 516081 495668 50
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 641810 500000
QC Flag Legend
a - Target compound detected but quantitated amountBelow Limit Of Quantitation(BLOQ)
10162012Page 54 of 323
Data File e08983d
Date 11-OCT-2012 2341
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-1 Operator GCMS VOAMS5
10162012Page 55 of 323
Data File e08983d
Date 11-OCT-2012 2341
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-1 Operator GCMS VOAMS5
28 MTBE
10162012Page 56 of 323
Data File e08983d
Date 11-OCT-2012 2341
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-1 Operator GCMS VOAMS5
66 Toluene
10162012Page 57 of 323
Data File e08983d
Date 11-OCT-2012 2341
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-1 Operator GCMS VOAMS5
71 Tetrachloroethene
10162012Page 58 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2
Matrix e08984dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0004
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 0060U71-55-6 111-Trichloroethane 0060
10 022U75-71-8 Dichlorodifluoromethane 022
10 010U74-87-3 Chloromethane 010
10 014U75-01-4 Vinyl chloride 014
10 018U74-83-9 Bromomethane 018
10 040U96-12-8 12-Dibromo-3-Chloropropane 040
10 021U95-50-1 12-Dichlorobenzene 021
10 015U75-69-4 Trichlorofluoromethane 015
10 0090U75-35-4 11-Dichloroethene 0090
10 0090U78-87-5 12-Dichloropropane 0090
10 0080U76-13-1 112-Trichloro-122-trifluoroethane
0080
50 27U67-64-1 Acetone 27
10 013U75-15-0 Carbon disulfide 013
20 034U79-20-9 Methyl acetate 034
10 018U75-09-2 Methylene Chloride 018
10 013U156-60-5 trans-12-Dichloroethene 013
10 020U124-48-1 Chlorodibromomethane 020
10 014J1634-04-4 Methyl tert-butyl ether 020
10 017U75-00-3 Chloroethane 017
10 013U75-34-3 11-Dichloroethane 013
10 018U156-59-2 cis-12-Dichloroethene 018
50 23U78-93-3 2-Butanone (MEK) 23
10 0080U67-66-3 Chloroform 0080
10 010U100-41-4 Ethylbenzene 010
10 016U110-82-7 Cyclohexane 016
10 0060U56-23-5 Carbon tetrachloride 0060
10 0080U71-43-2 Benzene 0080
10 019U107-06-2 12-Dichloroethane 019
10 0090U79-01-6 Trichloroethene 0090
10 014U108-87-2 Methylcyclohexane 014
10 012U75-27-4 Dichlorobromomethane 012
10 018U10061-01-5 cis-13-Dichloropropene 018
50 099U108-10-1 4-Methyl-2-pentanone (MIBK) 099
10 015U108-88-3 Toluene 015
10 024U10061-02-6 trans-13-Dichloropropene 024
FORM I 8260B
10162012Page 59 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2
Matrix e08984dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0004
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 019U79-00-5 112-Trichloroethane 019
10 010U127-18-4 Tetrachloroethene 010
50 050U591-78-6 2-Hexanone 050
10 028U106-93-4 12-Dibromoethane 028
10 011U108-90-7 Chlorobenzene 011
30 036U1330-20-7 Xylenes Total 036
10 012U100-42-5 Styrene 012
10 019U75-25-2 Bromoform 019
10 0080U98-82-8 Isopropylbenzene 0080
10 016U79-34-5 1122-Tetrachloroethane 016
10 014U541-73-1 13-Dichlorobenzene 014
10 023U106-46-7 14-Dichlorobenzene 023
10 034U120-82-1 124-Trichlorobenzene 034
RECCAS NO LIMITSQSURROGATE
97 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
98 70-130460-00-4 4-Bromofluorobenzene
97 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 60 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2
Matrix e08984dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0004
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
Number TICs Found TIC Result Total 00
QRTCOMPOUND NAME RESULTCAS NO
Tentatively Identified Compound None
FORM I-TIC 8260B
10162012Page 61 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08984d Report Date 12-Oct-2012 1126
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08984dLab Smp Id 460-45537-A-2 Client Smp ID WC-17338-100512-MW1Inj Date 12-OCT-2012 0004 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info 460-45537-A-2Misc Info 460-45537-A-2Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 9 Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
28 MTBE 73 2016 2022 (0561) 3378 020333 020(a)
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 375158 483561 48
52 Fluorobenzene 96 3595 3601 (1000) 1247617 500000
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1243750 487069 49
78 Chlorobenzene-d5 117 6954 6954 (1000) 1105330 500000
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 506189 492299 49
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 633816 500000
QC Flag Legend
a - Target compound detected but quantitated amountBelow Limit Of Quantitation(BLOQ)
10162012Page 62 of 323
Data File e08984d
Date 12-OCT-2012 0004
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-2 Operator GCMS VOAMS5
10162012Page 63 of 323
Data File e08984d
Date 12-OCT-2012 0004
Client ID WC-17338-100512-MW1 Instrument VOAMS5i
Sample Info 460-45537-A-2 Operator GCMS VOAMS5
28 MTBE
10162012Page 64 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
TB-17338-100512-253
SDG No
460-45537-1
Lab Sample ID 460-45537-3
Matrix e08982dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 0000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2317
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 0060U71-55-6 111-Trichloroethane 0060
10 022U75-71-8 Dichlorodifluoromethane 022
10 010U74-87-3 Chloromethane 010
10 014U75-01-4 Vinyl chloride 014
10 018U74-83-9 Bromomethane 018
10 040U96-12-8 12-Dibromo-3-Chloropropane 040
10 021U95-50-1 12-Dichlorobenzene 021
10 015U75-69-4 Trichlorofluoromethane 015
10 0090U75-35-4 11-Dichloroethene 0090
10 0090U78-87-5 12-Dichloropropane 0090
10 0080U76-13-1 112-Trichloro-122-trifluoroethane
0080
50 27U67-64-1 Acetone 27
10 013U75-15-0 Carbon disulfide 013
20 034U79-20-9 Methyl acetate 034
10 018J75-09-2 Methylene Chloride 074
10 013U156-60-5 trans-12-Dichloroethene 013
10 020U124-48-1 Chlorodibromomethane 020
10 014U1634-04-4 Methyl tert-butyl ether 014
10 017U75-00-3 Chloroethane 017
10 013U75-34-3 11-Dichloroethane 013
10 018U156-59-2 cis-12-Dichloroethene 018
50 23U78-93-3 2-Butanone (MEK) 23
10 0080J67-66-3 Chloroform 0096
10 010U100-41-4 Ethylbenzene 010
10 016U110-82-7 Cyclohexane 016
10 0060U56-23-5 Carbon tetrachloride 0060
10 0080U71-43-2 Benzene 0080
10 019U107-06-2 12-Dichloroethane 019
10 0090U79-01-6 Trichloroethene 0090
10 014U108-87-2 Methylcyclohexane 014
10 012U75-27-4 Dichlorobromomethane 012
10 018U10061-01-5 cis-13-Dichloropropene 018
50 099U108-10-1 4-Methyl-2-pentanone (MIBK) 099
10 015U108-88-3 Toluene 015
10 024U10061-02-6 trans-13-Dichloropropene 024
FORM I 8260B
10162012Page 65 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
TB-17338-100512-253
SDG No
460-45537-1
Lab Sample ID 460-45537-3
Matrix e08982dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 0000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2317
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 019U79-00-5 112-Trichloroethane 019
10 010U127-18-4 Tetrachloroethene 010
50 050U591-78-6 2-Hexanone 050
10 028U106-93-4 12-Dibromoethane 028
10 011U108-90-7 Chlorobenzene 011
30 036U1330-20-7 Xylenes Total 036
10 012U100-42-5 Styrene 012
10 019U75-25-2 Bromoform 019
10 0080U98-82-8 Isopropylbenzene 0080
10 016U79-34-5 1122-Tetrachloroethane 016
10 014U541-73-1 13-Dichlorobenzene 014
10 023U106-46-7 14-Dichlorobenzene 023
10 034U120-82-1 124-Trichlorobenzene 034
RECCAS NO LIMITSQSURROGATE
97 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
99 70-130460-00-4 4-Bromofluorobenzene
97 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 66 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID
Lab Name Job No
TB-17338-100512-253
SDG No
460-45537-1
Lab Sample ID 460-45537-3
Matrix e08982dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 0000
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2317
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
Number TICs Found TIC Result Total 00
QRTCOMPOUND NAME RESULTCAS NO
Tentatively Identified Compound None
FORM I-TIC 8260B
10162012Page 67 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08982d Report Date 12-Oct-2012 1126
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08982dLab Smp Id 460-45537-A-3 Client Smp ID TB-17338-100512-253Inj Date 11-OCT-2012 2317 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info 460-45537-A-3Misc Info 460-45537-A-3Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 7 Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
22 Methylene Chloride 49 1864 1864 (0518) 6426 073512 074(a)
42 Chloroform 83 2839 2845 (0790) 973 009557 0096(aH)
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 385354 484137 48
52 Fluorobenzene 96 3595 3601 (1000) 1280000 500000
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1266759 482968 48
78 Chlorobenzene-d5 117 6954 6954 (1000) 1135339 500000
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 518232 493851 49
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 646856 500000
QC Flag Legend
a - Target compound detected but quantitated amountBelow Limit Of Quantitation(BLOQ)
H - Operator selected an alternate compound hit
10162012Page 68 of 323
Data File e08982d
Date 11-OCT-2012 2317
Client ID TB-17338-100512-253 Instrument VOAMS5i
Sample Info 460-45537-A-3 Operator GCMS VOAMS5
10162012Page 69 of 323
Data File e08982d
Date 11-OCT-2012 2317
Client ID TB-17338-100512-253 Instrument VOAMS5i
Sample Info 460-45537-A-3 Operator GCMS VOAMS5
22 Methylene Chloride
10162012Page 70 of 323
Data File e08982d
Date 11-OCT-2012 2317
Client ID TB-17338-100512-253 Instrument VOAMS5i
Sample Info 460-45537-A-3 Operator GCMS VOAMS5
42 Chloroform
10162012Page 71 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
018(mm)Rtx-VMS ID
INTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-1280762 e07836d2Level IC 460-1280763 e07838d3Level ICIS 460-1280764 e07839d4Level IC 460-1280765 e07840d5Level IC 460-1280766 e07841d6Level IC 460-1280767 e07842d
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
RSD MAXRSD
R^2OR COD
MIN R^2OR COD
MIN RRF
LVL 6
Dichlorodifluoromethane 01877 01710 01761 01874 01774 Ave 6501572
01000 30001761
Chloromethane 04585 03624 03717 03896 03503 Ave 13403074
01000 30003733
Vinyl chloride 03440 02904 02965 03157 02914 Ave 10102532
01000 30002985
Bromomethane 01457 01433 01250 01279 01268 Ave 8301184
01000 30001312
Chloroethane 01177 01273 01133 01184 00992 Ave 14300838
01000 30001099
Trichlorofluoromethane 02861 02160 02403 02359 02461 Ave 9902285
01000 30002422
11-Dichloroethene 01607 01355 01549 01479 01528 Ave 5801456
01000 30001496
Carbon disulfide 07031 06470 06825 07347 07283 Ave 5906366
01000 30006887
112-Trichloro-122-trifluoroethane 01346 01631 01661 01849 01887 Ave 11601772
01000 30001691
Methylene Chloride 04479 03769 03581 03500 03182 Ave 14802947
01000 30003576
Acetone 00225 00193 00188 00182 00162 Ave 13800153
01000 30000184
trans-12-Dichloroethene 02047 01989 02141 02174 02016 Ave 4301946
01000 30002052
Methyl acetate 00482 00463 00420 00421 00402 Ave 9400371
01000 30000426
Methyl tert-butyl ether 07109 07281 06924 06817 06907 Ave 6505992
01000 30006838
11-Dichloroethane 04650 04524 04893 04673 04494 Ave 4604257
01000 30004582
FORM VI 8260B
Note The m1 coefficient is the same as Ave RRF for an Ave curve type
10162012Page 72 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
018(mm)Rtx-VMS ID
INTERNAL STANDARD CURVE EVALUATION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
RSD MAXRSD
R^2OR COD
MIN R^2OR COD
MIN RRF
LVL 6
cis-12-Dichloroethene 02536 02396 02453 02363 02237 Ave 5602184
01000 30002361
Cyclohexane 03116 04199 04030 04447 04640 Ave 13204438
01000 30004145
Chloroform 03895 04109 04030 04060 03948 Ave 2503851
01000 30003982
Carbon tetrachloride 02420 02373 02793 02813 02930 Ave 9102903
01000 30002705
111-Trichloroethane 03091 03114 03513 03424 03583 Ave 6403522
01000 30003375
2-Butanone (MEK) 00273 00279 00385 00372 00372 Ave 14900364
01000 30000341
Benzene 12012 12533 12592 12117 12284 Ave 8709836
01000 30011896
12-Dichloroethane 03398 03425 03293 03270 03193 Ave 3503124
01000 30003284
Methylcyclohexane 02272 03440 03287 03727 03690 Ave 16303532
01000 30003325
Trichloroethene 02571 02192 02414 02341 02365 Ave 5202426
01000 30002385
12-Dichloropropane 02758 02786 02804 02730 02724 Ave 1202733
01000 30002756
Dichlorobromomethane 03209 03160 03185 03141 03239 Ave 1303237
01000 30003195
cis-13-Dichloropropene 05043 05293 05370 05217 05393 Ave 3105530
01000 30005308
Toluene 13662 13454 14250 13844 13425 Ave 9510731
01000 30013228
Tetrachloroethene 02730 02844 03369 03253 03225 Ave 8303255
01000 30003113
4-Methyl-2-pentanone (MIBK) 03587 03603 03526 03550 03603 Ave 1603692
01000 30003593
trans-13-Dichloropropene 04563 04743 04806 04779 04910 Ave 3805114
01000 30004819
112-Trichloroethane 02303 02327 02287 02201 02185 Ave 2502280
01000 30002264
Chlorodibromomethane 03013 02986 03088 03052 03111 Ave 3003249
01000 30003083
12-Dibromoethane 02596 02708 02743 02671 02629 Ave 2002676
01000 30002670
FORM VI 8260B
Note The m1 coefficient is the same as Ave RRF for an Ave curve type
10162012Page 73 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
018(mm)Rtx-VMS ID
INTERNAL STANDARD CURVE EVALUATION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
RSD MAXRSD
R^2OR COD
MIN R^2OR COD
MIN RRF
LVL 6
2-Hexanone 02652 02737 02670 02679 02755 Ave 3202514
01000 30002668
Chlorobenzene 08958 08985 09292 09070 08727 Ave 4008261
01000 30008882
Ethylbenzene 04549 04523 04953 04866 04834 Ave 3704808
01000 30004756
m-Xylene amp p-Xylene 05967 05752 06297 06168 06094 Ave 6505224
01000 30005917
o-Xylene 05732 05675 06142 06014 05989 Ave 3205765
01000 30005886
Bromoform 02053 01991 02150 02194 02258 Ave 4902237
01000 30002147
Styrene 09657 09899 10525 10511 10477 Ave 6408917
01000 30009998
Isopropylbenzene 13314 13509 15606 15346 15340 Ave 10811764
01000 30014146
1122-Tetrachloroethane 06545 06405 06616 06489 06390 Ave 1706330
01000 30006462
13-Dichlorobenzene 12616 12687 13292 13133 12758 Ave 3012242
01000 30012788
14-Dichlorobenzene 13636 13114 13708 13534 13010 Ave 3412550
01000 30013259
12-Dichlorobenzene 12298 12143 12601 12232 11746 Ave 3211521
01000 30012090
12-Dibromo-3-Chloropropane 01290 01163 01082 01109 01042 Ave 7801095
01000 30001130
124-Trichlorobenzene 06538 06139 06311 06265 05725 Ave 5405732
01000 30006118
12-Dichloroethane-d4 (Surr) 02599 02736 02573 02553 02667 Ave 2802702
01000 30002638
Toluene-d8 (Surr) 11377 12027 11720 11573 11645 Ave 1811690
01000 30011672
4-Bromofluorobenzene 07799 08146 08086 08044 08193 Ave 1908206
01000 30008079
FORM VI 8260B
Note The m1 coefficient is the same as Ave RRF for an Ave curve type
10162012Page 74 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
GC Column Rtx-VMS ID 018(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-1280762 e07836dLevel 2 IC 460-1280763 e07838dLevel 3 ICIS 460-1280764 e07839dLevel 4 IC 460-1280765 e07840dLevel 5 IC 460-1280766 e07841dLevel 6 IC 460-1280767 e07842d
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UGL)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Dichlorodifluoromethane AveFB 8660 39416 167418 450014 17982634551928
100 500 200 500 200500
Chloromethane AveFB 21155 83523 353287 935453 35519068902969
100 500 200 500 200500
Vinyl chloride AveFB 15876 66919 281874 757876 29543837332518
100 500 200 500 200500
Bromomethane AveFB 6723 33032 118799 307121 12855673429373
100 500 200 500 200500
Chloroethane AveFB 5433 29332 107678 284219 10059762426216
100 500 200 500 200500
Trichlorofluoromethane AveFB 13203 49780 228376 566305 24953266618134
100 500 200 500 200500
11-Dichloroethene AveFB 7415 31234 147259 355088 15491024214942
100 500 200 500 200500
Carbon disulfide AveFB 32446 149121 648801 1763903 738404918433408
100 500 200 500 200500
112-Trichloro-122-trifluoroethane
AveFB 6213 37580 157867 443949 19130255130629
100 500 200 500 200500
Methylene Chloride AveFB 20667 86862 340378 840419 32256318533685
100 500 200 500 200500
Acetone AveFB 5188 13342 17849 43750 164598441742
500 150 200 500 200500
trans-12-Dichloroethene AveFB 9445 45844 203500 521911 20443355633771
100 500 200 500 200500
Methyl acetate AveFB 2222 10660 39926 101112 4077131074355
100 500 200 500 200500
Methyl tert-butyl ether AveFB 32806 167790 658123 1636664 700252217351574
100 500 200 500 200500
11-Dichloroethane AveFB 21457 104265 465144 1121930 455634112326764
100 500 200 500 200500
cis-12-Dichloroethene AveFB 11702 55218 233129 567238 22679686324299
100 500 200 500 200500
FORM VI 8260B 10162012Page 75 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
GC Column Rtx-VMS ID 018(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UGL)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Cyclohexane AveFB 14380 96765 383104 1067735 470410312852489
100 500 200 500 200500
Chloroform AveFB 17974 94697 383084 974788 400250611152231
100 500 200 500 200500
Carbon tetrachloride AveFB 11168 54679 265527 675330 29705928405131
100 500 200 500 200500
111-Trichloroethane AveFB 14264 71766 333961 821993 363312510199723
100 500 200 500 200500
2-Butanone (MEK) AveFB 6291 19260 36552 89217 3773171055008
500 150 200 500 200500
Benzene AveCBZ 45050 227079 968083 2380099 986355721876514
100 500 200 500 200500
12-Dichloroethane AveFB 15679 78926 312991 785178 32368389046377
100 500 200 500 200500
Methylcyclohexane AveFB 10486 79279 312424 894738 374094710227785
100 500 200 500 200500
Trichloroethene AveFB 11865 50527 229465 562086 23978387026524
100 500 200 500 200500
12-Dichloropropane AveFB 12728 64209 266559 655380 27621167913672
100 500 200 500 200500
Dichlorobromomethane AveFB 14807 72835 302742 754124 32836079374106
100 500 200 500 200500
cis-13-Dichloropropene AveCBZ 18914 95905 412847 1024782 433022112299317
100 500 200 500 200500
Toluene AveCBZ 51238 243768 1095520 2719268 1077972123868197
100 500 200 500 200500
Tetrachloroethene AveCBZ 10238 51530 258990 639002 25895417239654
100 500 200 500 200500
4-Methyl-2-pentanone (MIBK) AveCBZ 67258 195851 271059 697282 28927468212153
500 150 200 500 200500
trans-13-Dichloropropene AveCBZ 17115 85943 369516 938808 394242511373599
100 500 200 500 200500
112-Trichloroethane AveCBZ 8636 42154 175853 432262 17543015071317
100 500 200 500 200500
Chlorodibromomethane AveCBZ 11301 54107 237421 599464 24982697227226
100 500 200 500 200500
12-Dibromoethane AveCBZ 9735 49066 210900 524614 21107665952425
100 500 200 500 200500
2-Hexanone AveCBZ 49729 148758 205286 526223 22117155590902
500 150 200 500 200500
Chlorobenzene AveCBZ 33596 162793 714336 1781568 700752018374405
100 500 200 500 200500
FORM VI 8260B 10162012Page 76 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GCMS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
VOAMS5
Analy Batch No 128076
17515Calibration Start Date Calibration End Date09172012 0449
N
09172012 0710
GC Column Rtx-VMS ID 018(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UGL)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Ethylbenzene AveCBZ 17061 81955 380762 955894 388164310693410
100 500 200 500 200500
m-Xylene amp p-Xylene AveCBZ 44761 208423 968280 2423002 978688223238078
200 100 400 100 4001000
o-Xylene AveCBZ 21499 102832 472158 1181273 480921512821590
100 500 200 500 200500
Bromoform AveCBZ 7698 36074 165267 430943 18127954974461
100 500 200 500 200500
Styrene AveCBZ 36217 179367 809158 2064560 841264519831782
100 500 200 500 200500
Isopropylbenzene AveCBZ 49933 244766 1199765 3014281 1231710326165908
100 500 200 500 200500
1122-Tetrachloroethane AveDCB 13823 63947 277413 702309 28987687365342
100 500 200 500 200500
13-Dichlorobenzene AveDCB 26644 126663 557342 1421450 578731414243841
100 500 200 500 200500
14-Dichlorobenzene AveDCB 28798 130929 574816 1464915 590189114602396
100 500 200 500 200500
12-Dichlorobenzene AveDCB 25972 121236 528396 1324016 532862113405399
100 500 200 500 200500
12-Dibromo-3-Chloropropane AveDCB 2725 11615 45388 120062 4727441274610
100 500 200 500 200500
124-Trichlorobenzene AveDCB 13808 61295 264648 678119 25969596669727
100 500 200 500 200500
12-Dichloroethane-d4 (Surr) AveFB 599539 630441 611357 613057 676105782507
500 500 500 500 500500
Toluene-d8 (Surr) AveCBZ 2133452 2179204 2252606 2273339 23375152600040
500 500 500 500 500500
4-Bromofluorobenzene AveDCB 823604 813301 847619 870646 929176954872
500 500 500 500 500500
Curve Type LegendAve = Average ISTD
FORM VI 8260B 10162012Page 77 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07836d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07836dLab Smp Id IC-VMCAL1 Inj Date 17-SEP-2012 0449 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info IC-VMCAL1Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 2 Calibration Sample Level 1Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 8660 100000 11
3 Chloromethane 50 1004 1004 (0280) 21155 100000 12
4 Vinyl Chloride 62 1016 1016 (0283) 15876 100000 12
6 Bromomethane 94 1169 1169 (0326) 6723 100000 11
5 Chloroethane 64 1230 1230 (0343) 5433 100000 11
7 Trichlorofluoromethane 101 1291 1291 (0360) 13203 100000 12
14 Freon TF 101 1565 1565 (0436) 6213 100000 080(a)
15 11-Dichloroethene 96 1547 1547 (0431) 7415 100000 11
16 Acetone 58 1882 1882 (0524) 5188 500000 61
18 Carbon Disulfide 76 1559 1559 (0434) 32446 100000 10
27 Methyl Acetate 74 1955 1955 (0545) 2222 100000 11
22 Methylene Chloride 49 1851 1851 (0516) 20667 100000 12
28 MTBE 73 2016 2016 (0562) 32806 100000 10
25 trans-12-Dichloroethene 96 1937 1937 (0540) 9445 100000 100
30 11-Dichloroethane 63 2303 2303 (0642) 21457 100000 10
36 cis-12-Dichloroethene 96 2644 2644 (0737) 11702 100000 11
10162012Page 78 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07836d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3071 (0856) 6291 500000 40(a)
42 Chloroform 83 2839 2839 (0791) 17974 100000 098(a)
44 Cyclohexane 56 2778 2778 (0774) 14380 100000 075(a)
43 111-Trichloroethane 97 2973 2973 (0828) 14264 100000 092(a)
45 Carbon Tetrachloride 117 2924 2924 (0815) 11168 100000 089(a)
48 Benzene 78 3254 3254 (0468) 45050 100000 10
$ 47 12-Dichloroethane-d4 (SUR) 65 3357 3357 (0935) 599539 500000 49
49 12-Dichloroethane 62 3412 3412 (0951) 15679 100000 10
52 Fluorobenzene 96 3589 3589 (1000) 2307227 500000
54 Trichloroethene 95 3735 3735 (1041) 11865 100000 11
56 Methyl cyclohexane 83 3723 3723 (1037) 10486 100000 068(a)
57 12-Dichloropropane 63 4192 4192 (1168) 12728 100000 10
68 Bromodichloromethane 83 4266 4266 (1189) 14807 100000 10
67 cis-13-Dichloropropene 75 4906 4906 (0706) 18914 100000 095(a)
70 4-Methyl-2-Pentanone 43 5625 5625 (0810) 67258 500000 50
$ 65 Toluene-d8 (SUR) 98 5101 5101 (0734) 2133452 500000 49
66 Toluene 91 5156 5156 (0742) 51238 100000 10
64 trans-13-Dichloropropene 75 5650 5650 (0813) 17115 100000 095(a)
69 112-Trichloroethane 83 5826 5826 (0839) 8636 100000 10
71 Tetrachloroethene 166 5582 5582 (0803) 10238 100000 088(a)
73 2-Hexanone 43 6674 6674 (0960) 49729 500000 50
74 Dibromochloromethane 129 6015 6015 (0866) 11301 100000 098(a)
77 12-Dibromoethane 107 6265 6265 (0902) 9735 100000 097(a)
78 Chlorobenzene-d5 117 6948 6948 (1000) 1875221 500000
79 Chlorobenzene 112 6972 6972 (1004) 33596 100000 10
81 Ethylbenzene 106 7064 7064 (1017) 17061 100000 096(a)
82 m+p-Xylene 106 7271 7271 (1046) 44761 200000 20
84 o-Xylene 106 7856 7856 (1131) 21499 100000 097(a)
85 Styrene 104 7942 7942 (1143) 36217 100000 096(a)
86 Bromoform 173 7911 7911 (1139) 7698 100000 096(a)
88 Isopropylbenzene 105 8344 8344 (1201) 49933 100000 094(a)
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 823604 500000 48
92 1122-Tetrachloroethane 83 9112 9112 (0871) 13823 100000 10
105 13-Dichlorobenzene 146 10332 10332 (0987) 26644 100000 099(a)
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 1055978 500000
109 14-Dichlorobenzene 146 10484 10484 (1002) 28798 100000 10
111 12-Dichlorobenzene 146 11148 11148 (1065) 25972 100000 10(H)
112 12-Dibromo-3-chloropropane 75 12234 12234 (1169) 2725 100000 11
114 124-Trichlorobenzene 180 12971 12971 (1239) 13808 100000 11
M 120 12-Dichloroethene (Total) 100 21147 200000 21
M 121 Xylene (Total) 100 66260 300000 30
QC Flag Legend
a - Target compound detected but quantitated amountBelow Limit Of Quantitation(BLOQ)
H - Operator selected an alternate compound hit
10162012Page 79 of 323
Data File e07836d
Date 17-SEP-2012 0449
Client ID Instrument VOAMS5i
Sample Info IC-VMCAL1 Operator GCMS VOAMS5
10162012Page 80 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07838d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07838dLab Smp Id IC-VMCAL2 Inj Date 17-SEP-2012 0536 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info IC-VMCAL2Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 4 Calibration Sample Level 2Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 39416 500000 48
3 Chloromethane 50 1016 1016 (0283) 83523 500000 48
4 Vinyl Chloride 62 1022 1022 (0285) 66919 500000 49
6 Bromomethane 94 1169 1169 (0326) 33032 500000 55
5 Chloroethane 64 1230 1230 (0343) 29332 500000 58
7 Trichlorofluoromethane 101 1291 1291 (0360) 49780 500000 45
14 Freon TF 101 1559 1559 (0434) 37580 500000 48
15 11-Dichloroethene 96 1541 1541 (0429) 31234 500000 45
16 Acetone 58 1894 1894 (0528) 13342 150000 16
18 Carbon Disulfide 76 1553 1553 (0433) 149121 500000 47
27 Methyl Acetate 74 1961 1961 (0546) 10660 500000 54
22 Methylene Chloride 49 1851 1851 (0516) 86862 500000 53
28 MTBE 73 2016 2016 (0562) 167790 500000 53
25 trans-12-Dichloroethene 96 1937 1937 (0540) 45844 500000 48
30 11-Dichloroethane 63 2296 2296 (0640) 104265 500000 49
36 cis-12-Dichloroethene 96 2644 2644 (0737) 55218 500000 51
10162012Page 81 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07838d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3077 3077 (0857) 19260 150000 12
42 Chloroform 83 2839 2839 (0791) 94697 500000 52
44 Cyclohexane 56 2772 2772 (0772) 96765 500000 51
43 111-Trichloroethane 97 2973 2973 (0828) 71766 500000 46
45 Carbon Tetrachloride 117 2924 2924 (0815) 54679 500000 44
48 Benzene 78 3254 3254 (0468) 227079 500000 53
$ 47 12-Dichloroethane-d4 (SUR) 65 3357 3357 (0935) 630441 500000 52
49 12-Dichloroethane 62 3412 3412 (0951) 78926 500000 52
52 Fluorobenzene 96 3589 3589 (1000) 2304638 500000
54 Trichloroethene 95 3735 3735 (1041) 50527 500000 46
56 Methyl cyclohexane 83 3717 3717 (1036) 79279 500000 52
57 12-Dichloropropane 63 4192 4192 (1168) 64209 500000 50
68 Bromodichloromethane 83 4272 4272 (1190) 72835 500000 49
67 cis-13-Dichloropropene 75 4906 4906 (0706) 95905 500000 50
70 4-Methyl-2-Pentanone 43 5625 5625 (0810) 195851 150000 15
$ 65 Toluene-d8 (SUR) 98 5101 5101 (0734) 2179204 500000 52
66 Toluene 91 5156 5156 (0742) 243768 500000 51
64 trans-13-Dichloropropene 75 5643 5643 (0812) 85943 500000 49
69 112-Trichloroethane 83 5820 5820 (0838) 42154 500000 51
71 Tetrachloroethene 166 5576 5576 (0803) 51530 500000 46
73 2-Hexanone 43 6680 6680 (0961) 148758 150000 15
74 Dibromochloromethane 129 6015 6015 (0866) 54107 500000 48
77 12-Dibromoethane 107 6259 6259 (0901) 49066 500000 51
78 Chlorobenzene-d5 117 6948 6948 (1000) 1811885 500000
79 Chlorobenzene 112 6972 6972 (1004) 162793 500000 50
81 Ethylbenzene 106 7058 7058 (1016) 81955 500000 48
82 m+p-Xylene 106 7271 7271 (1046) 208423 100000 97
84 o-Xylene 106 7856 7856 (1131) 102832 500000 48
85 Styrene 104 7942 7942 (1143) 179367 500000 50
86 Bromoform 173 7911 7911 (1139) 36074 500000 46
88 Isopropylbenzene 105 8344 8344 (1201) 244766 500000 48
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 813301 500000 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 63947 500000 50
105 13-Dichlorobenzene 146 10325 10325 (0987) 126663 500000 50
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 998386 500000
109 14-Dichlorobenzene 146 10484 10484 (1002) 130929 500000 49
111 12-Dichlorobenzene 146 11148 11148 (1065) 121236 500000 50
112 12-Dibromo-3-chloropropane 75 12234 12234 (1169) 11615 500000 51
114 124-Trichlorobenzene 180 12965 12965 (1239) 61295 500000 50
M 120 12-Dichloroethene (Total) 100 101062 100000 99
M 121 Xylene (Total) 100 311255 150000 14
10162012Page 82 of 323
Data File e07838d
Date 17-SEP-2012 0536
Client ID Instrument VOAMS5i
Sample Info IC-VMCAL2 Operator GCMS VOAMS5
10162012Page 83 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07839d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07839dLab Smp Id ICIS-VMCAL3 Inj Date 17-SEP-2012 0600 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info ICIS-VMCAL3Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 5 Calibration Sample Level 3Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 167418 200000 20
3 Chloromethane 50 1016 1016 (0283) 353287 200000 20
4 Vinyl Chloride 62 1016 1016 (0283) 281874 200000 20
6 Bromomethane 94 1175 1175 (0327) 118799 200000 19
5 Chloroethane 64 1230 1230 (0343) 107678 200000 21
7 Trichlorofluoromethane 101 1291 1291 (0360) 228376 200000 20
14 Freon TF 101 1559 1559 (0434) 157867 200000 20
15 11-Dichloroethene 96 1540 1540 (0429) 147259 200000 21
16 Acetone 58 1888 1888 (0526) 17849 200000 20
18 Carbon Disulfide 76 1559 1559 (0434) 648801 200000 20
27 Methyl Acetate 74 1955 1955 (0545) 39926 200000 20
22 Methylene Chloride 49 1851 1851 (0516) 340378 200000 20
28 MTBE 73 2016 2016 (0562) 658123 200000 20
25 trans-12-Dichloroethene 96 1943 1943 (0541) 203500 200000 21
30 11-Dichloroethane 63 2303 2303 (0642) 465144 200000 21
36 cis-12-Dichloroethene 96 2644 2644 (0737) 233129 200000 21
10162012Page 84 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07839d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3071 (0856) 36552 200000 22
42 Chloroform 83 2839 2839 (0791) 383084 200000 20
44 Cyclohexane 56 2778 2778 (0774) 383104 200000 19
43 111-Trichloroethane 97 2973 2973 (0828) 333961 200000 21
45 Carbon Tetrachloride 117 2924 2924 (0815) 265527 200000 21
48 Benzene 78 3254 3254 (0468) 968083 200000 21
$ 47 12-Dichloroethane-d4 (SUR) 65 3357 3357 (0935) 611357 500000 49
49 12-Dichloroethane 62 3412 3412 (0951) 312991 200000 20
52 Fluorobenzene 96 3589 3589 (1000) 2376396 500000
54 Trichloroethene 95 3735 3735 (1041) 229465 200000 20
56 Methyl cyclohexane 83 3723 3723 (1037) 312424 200000 20
57 12-Dichloropropane 63 4192 4192 (1168) 266559 200000 20
68 Bromodichloromethane 83 4266 4266 (1189) 302742 200000 20
67 cis-13-Dichloropropene 75 4906 4906 (0705) 412847 200000 20
70 4-Methyl-2-Pentanone 43 5625 5625 (0809) 271059 200000 20
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 2252606 500000 50
66 Toluene 91 5156 5156 (0741) 1095520 200000 22
64 trans-13-Dichloropropene 75 5643 5643 (0812) 369516 200000 20
69 112-Trichloroethane 83 5820 5820 (0837) 175853 200000 20
71 Tetrachloroethene 166 5576 5576 (0802) 258990 200000 22
73 2-Hexanone 43 6680 6680 (0961) 205286 200000 20
74 Dibromochloromethane 129 6015 6015 (0865) 237421 200000 20
77 12-Dibromoethane 107 6259 6259 (0900) 210900 200000 20
78 Chlorobenzene-d5 117 6954 6954 (1000) 1921967 500000
79 Chlorobenzene 112 6972 6972 (1003) 714336 200000 21
81 Ethylbenzene 106 7064 7064 (1016) 380762 200000 21
82 m+p-Xylene 106 7277 7277 (1046) 968280 400000 42
84 o-Xylene 106 7856 7856 (1130) 472158 200000 21
85 Styrene 104 7942 7942 (1142) 809158 200000 21
86 Bromoform 173 7911 7911 (1138) 165267 200000 20
88 Isopropylbenzene 105 8344 8344 (1200) 1199765 200000 22
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 847619 500000 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 277413 200000 20
105 13-Dichlorobenzene 146 10325 10325 (0987) 557342 200000 21
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 1048295 500000
109 14-Dichlorobenzene 146 10484 10484 (1002) 574816 200000 21
111 12-Dichlorobenzene 146 11148 11148 (1065) 528396 200000 21
112 12-Dibromo-3-chloropropane 75 12233 12233 (1169) 45388 200000 19
114 124-Trichlorobenzene 180 12965 12965 (1239) 264648 200000 21
M 120 12-Dichloroethene (Total) 100 436629 400000 42
M 121 Xylene (Total) 100 1440438 600000 63
10162012Page 85 of 323
Data File e07839d
Date 17-SEP-2012 0600
Client ID Instrument VOAMS5i
Sample Info ICIS-VMCAL3 Operator GCMS VOAMS5
10162012Page 86 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07840d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07840dLab Smp Id IC-VMCAL4 Inj Date 17-SEP-2012 0623 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info IC-VMCAL4Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 6 Calibration Sample Level 4Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 450014 500000 53
3 Chloromethane 50 1010 1010 (0281) 935453 500000 52
4 Vinyl Chloride 62 1016 1016 (0283) 757876 500000 53
6 Bromomethane 94 1175 1175 (0327) 307121 500000 49
5 Chloroethane 64 1230 1230 (0342) 284219 500000 54
7 Trichlorofluoromethane 101 1290 1290 (0359) 566305 500000 49
14 Freon TF 101 1565 1565 (0435) 443949 500000 55
15 11-Dichloroethene 96 1540 1540 (0428) 355088 500000 49
16 Acetone 58 1888 1888 (0525) 43750 500000 50
18 Carbon Disulfide 76 1559 1559 (0434) 1763903 500000 53
27 Methyl Acetate 74 1961 1961 (0546) 101112 500000 49
22 Methylene Chloride 49 1851 1851 (0515) 840419 500000 49
28 MTBE 73 2016 2016 (0561) 1636664 500000 50
25 trans-12-Dichloroethene 96 1943 1943 (0540) 521911 500000 53
30 11-Dichloroethane 63 2302 2302 (0640) 1121930 500000 51
36 cis-12-Dichloroethene 96 2644 2644 (0735) 567238 500000 50
10162012Page 87 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07840d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3071 (0854) 89217 500000 54
42 Chloroform 83 2839 2839 (0790) 974788 500000 51
44 Cyclohexane 56 2778 2778 (0773) 1067735 500000 54
43 111-Trichloroethane 97 2973 2973 (0827) 821993 500000 51
45 Carbon Tetrachloride 117 2924 2924 (0813) 675330 500000 52
48 Benzene 78 3254 3254 (0468) 2380099 500000 51
$ 47 12-Dichloroethane-d4 (SUR) 65 3357 3357 (0934) 613057 500000 48
49 12-Dichloroethane 62 3412 3412 (0949) 785178 500000 50
52 Fluorobenzene 96 3595 3595 (1000) 2400971 500000
54 Trichloroethene 95 3735 3735 (1039) 562086 500000 49
56 Methyl cyclohexane 83 3723 3723 (1036) 894738 500000 56
57 12-Dichloropropane 63 4192 4192 (1166) 655380 500000 50
68 Bromodichloromethane 83 4272 4272 (1188) 754124 500000 49
67 cis-13-Dichloropropene 75 4906 4906 (0705) 1024782 500000 49
70 4-Methyl-2-Pentanone 43 5625 5625 (0809) 697282 500000 49
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 2273339 500000 50
66 Toluene 91 5162 5162 (0742) 2719268 500000 52
64 trans-13-Dichloropropene 75 5649 5649 (0812) 938808 500000 50
69 112-Trichloroethane 83 5820 5820 (0837) 432262 500000 49
71 Tetrachloroethene 166 5576 5576 (0802) 639002 500000 52
73 2-Hexanone 43 6680 6680 (0961) 526223 500000 50
74 Dibromochloromethane 129 6015 6015 (0865) 599464 500000 49
77 12-Dibromoethane 107 6259 6259 (0900) 524614 500000 50
78 Chlorobenzene-d5 117 6954 6954 (1000) 1964266 500000
79 Chlorobenzene 112 6972 6972 (1003) 1781568 500000 51
81 Ethylbenzene 106 7064 7064 (1016) 955894 500000 51
82 m+p-Xylene 106 7277 7277 (1046) 2423002 100000 100
84 o-Xylene 106 7862 7862 (1131) 1181273 500000 51
85 Styrene 104 7942 7942 (1142) 2064560 500000 52
86 Bromoform 173 7911 7911 (1138) 430943 500000 51
88 Isopropylbenzene 105 8350 8350 (1201) 3014281 500000 54
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 870646 500000 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 702309 500000 50
105 13-Dichlorobenzene 146 10331 10331 (0987) 1421450 500000 51
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 1082388 500000
109 14-Dichlorobenzene 146 10490 10490 (1002) 1464915 500000 51
111 12-Dichlorobenzene 146 11154 11154 (1066) 1324016 500000 50
112 12-Dibromo-3-chloropropane 75 12233 12233 (1169) 120062 500000 49
114 124-Trichlorobenzene 180 12971 12971 (1239) 678119 500000 51
M 120 12-Dichloroethene (Total) 100 1089149 100000 100
M 121 Xylene (Total) 100 3604275 150000 160
10162012Page 88 of 323
Data File e07840d
Date 17-SEP-2012 0623
Client ID Instrument VOAMS5i
Sample Info IC-VMCAL4 Operator GCMS VOAMS5
10162012Page 89 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07841d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07841dLab Smp Id IC-VMCAL5 Inj Date 17-SEP-2012 0646 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info IC-VMCAL5Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 7 Calibration Sample Level 5Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 1798263 200000 200
3 Chloromethane 50 1010 1010 (0281) 3551906 200000 190
4 Vinyl Chloride 62 1016 1016 (0283) 2954383 200000 200
6 Bromomethane 94 1175 1175 (0327) 1285567 200000 190
5 Chloroethane 64 1230 1230 (0342) 1005976 200000 180
7 Trichlorofluoromethane 101 1291 1291 (0359) 2495326 200000 200
14 Freon TF 101 1565 1565 (0435) 1913025 200000 220
15 11-Dichloroethene 96 1541 1541 (0429) 1549102 200000 200
16 Acetone 58 1894 1894 (0527) 164598 200000 180
18 Carbon Disulfide 76 1559 1559 (0434) 7384049 200000 210
27 Methyl Acetate 74 1961 1961 (0546) 407713 200000 190
22 Methylene Chloride 49 1851 1851 (0515) 3225631 200000 180
28 MTBE 73 2016 2016 (0561) 7002522 200000 200
25 trans-12-Dichloroethene 96 1943 1943 (0540) 2044335 200000 200
30 11-Dichloroethane 63 2303 2303 (0640) 4556341 200000 200
36 cis-12-Dichloroethene 96 2650 2650 (0737) 2267968 200000 190
10162012Page 90 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07841d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3071 (0854) 377317 200000 220
42 Chloroform 83 2839 2839 (0790) 4002506 200000 200
44 Cyclohexane 56 2784 2784 (0774) 4704103 200000 220
43 111-Trichloroethane 97 2979 2979 (0829) 3633125 200000 210
45 Carbon Tetrachloride 117 2930 2930 (0815) 2970592 200000 220
48 Benzene 78 3260 3260 (0468) 9863557 200000 210
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 676105 500000 50
49 12-Dichloroethane 62 3418 3418 (0951) 3236838 200000 190
52 Fluorobenzene 96 3595 3595 (1000) 2534623 500000
54 Trichloroethene 95 3741 3741 (1041) 2397838 200000 200
56 Methyl cyclohexane 83 3729 3729 (1037) 3740947 200000 220
57 12-Dichloropropane 63 4199 4199 (1168) 2762116 200000 200
68 Bromodichloromethane 83 4272 4272 (1188) 3283607 200000 200
67 cis-13-Dichloropropene 75 4912 4912 (0706) 4330221 200000 200
70 4-Methyl-2-Pentanone 43 5631 5631 (0809) 2892746 200000 200
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 2337515 500000 50
66 Toluene 91 5162 5162 (0742) 10779721 200000 200
64 trans-13-Dichloropropene 75 5656 5656 (0813) 3942425 200000 200
69 112-Trichloroethane 83 5826 5826 (0837) 1754301 200000 190
71 Tetrachloroethene 166 5582 5582 (0802) 2589541 200000 210
73 2-Hexanone 43 6686 6686 (0961) 2211715 200000 210
74 Dibromochloromethane 129 6021 6021 (0865) 2498269 200000 200
77 12-Dibromoethane 107 6265 6265 (0900) 2110766 200000 200
78 Chlorobenzene-d5 117 6960 6960 (1000) 2007362 500000
79 Chlorobenzene 112 6978 6978 (1003) 7007520 200000 200
81 Ethylbenzene 106 7076 7076 (1017) 3881643 200000 200
82 m+p-Xylene 106 7289 7289 (1047) 9786882 400000 410
84 o-Xylene 106 7869 7869 (1131) 4809215 200000 200
85 Styrene 104 7954 7954 (1143) 8412645 200000 210
86 Bromoform 173 7923 7923 (1138) 1812795 200000 210
88 Isopropylbenzene 105 8356 8356 (1201) 12317103 200000 220(A)
$ 89 Bromofluorobenzene (SUR) 174 8716 8716 (0832) 929176 500000 51
92 1122-Tetrachloroethane 83 9124 9124 (0871) 2898768 200000 200
105 13-Dichlorobenzene 146 10344 10344 (0987) 5787314 200000 200
108 14-Dichlorobenzene-d4 152 10478 10478 (1000) 1134091 500000
109 14-Dichlorobenzene 146 10502 10502 (1002) 5901891 200000 200
111 12-Dichlorobenzene 146 11167 11167 (1066) 5328621 200000 190
112 12-Dibromo-3-chloropropane 75 12240 12240 (1168) 472744 200000 180
114 124-Trichlorobenzene 180 12971 12971 (1238) 2596959 200000 190
M 120 12-Dichloroethene (Total) 100 4312303 400000 380
M 121 Xylene (Total) 100 14596097 600000 620
QC Flag Legend
A - Target compound detected but quantitated amountexceeded maximum amount
10162012Page 91 of 323
Data File e07841d
Date 17-SEP-2012 0646
Client ID Instrument VOAMS5i
Sample Info IC-VMCAL5 Operator GCMS VOAMS5
10162012Page 92 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07842d Report Date 17-Sep-2012 1317
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1217sep12be07842dLab Smp Id IC-VMCAL6 Inj Date 17-SEP-2012 0710 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info IC-VMCAL6Misc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12b8260DE_09mMeth Date 17-Sep-2012 1317 vibha Quant Type ISTDCal Date 17-SEP-2012 0600 Cal File e07839dAls bottle 8 Calibration Sample Level 6Dil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0888 0888 (0247) 4551928 500000 450
3 Chloromethane 50 1010 1010 (0280) 8902969 500000 410
4 Vinyl Chloride 62 1016 1016 (0282) 7332518 500000 420
6 Bromomethane 94 1175 1175 (0326) 3429373 500000 450
5 Chloroethane 64 1230 1230 (0341) 2426216 500000 380
7 Trichlorofluoromethane 101 1297 1297 (0360) 6618134 500000 470
14 Freon TF 101 1571 1571 (0436) 5130629 500000 520(A)
15 11-Dichloroethene 96 1547 1547 (0429) 4214942 500000 490
16 Acetone 58 1894 1894 (0526) 441742 500000 420
18 Carbon Disulfide 76 1559 1559 (0433) 18433408 500000 460
27 Methyl Acetate 74 1961 1961 (0545) 1074355 500000 440
22 Methylene Chloride 49 1851 1851 (0514) 8533685 500000 410
28 MTBE 73 2022 2022 (0562) 17351574 500000 440
25 trans-12-Dichloroethene 96 1943 1943 (0540) 5633771 500000 470
30 11-Dichloroethane 63 2302 2302 (0639) 12326764 500000 460
36 cis-12-Dichloroethene 96 2650 2650 (0736) 6324299 500000 460
10162012Page 93 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07842d Report Date 17-Sep-2012 1317
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3083 3083 (0856) 1055008 500000 530(A)
42 Chloroform 83 2845 2845 (0790) 11152231 500000 480
44 Cyclohexane 56 2790 2790 (0775) 12852489 500000 540(A)
43 111-Trichloroethane 97 2985 2985 (0829) 10199723 500000 520(A)
45 Carbon Tetrachloride 117 2936 2936 (0815) 8405131 500000 540(A)
48 Benzene 78 3260 3260 (0468) 21876514 500000 410
$ 47 12-Dichloroethane-d4 (SUR) 65 3369 3369 (0936) 782507 500000 51
49 12-Dichloroethane 62 3424 3424 (0951) 9046377 500000 480
52 Fluorobenzene 96 3601 3601 (1000) 2895790 500000
54 Trichloroethene 95 3753 3753 (1042) 7026524 500000 510(A)
56 Methyl cyclohexane 83 3741 3741 (1039) 10227785 500000 530(A)
57 12-Dichloropropane 63 4205 4205 (1168) 7913672 500000 500
68 Bromodichloromethane 83 4284 4284 (1190) 9374106 500000 510(A)
67 cis-13-Dichloropropene 75 4924 4924 (0706) 12299317 500000 520(A)
70 4-Methyl-2-Pentanone 43 5649 5649 (0810) 8212153 500000 510(A)
$ 65 Toluene-d8 (SUR) 98 5113 5113 (0733) 2600040 500000 50
66 Toluene 91 5168 5168 (0741) 23868197 500000 400
64 trans-13-Dichloropropene 75 5668 5668 (0813) 11373599 500000 530(A)
69 112-Trichloroethane 83 5838 5838 (0837) 5071317 500000 500(A)
71 Tetrachloroethene 166 5594 5594 (0802) 7239654 500000 520(A)
73 2-Hexanone 43 6698 6698 (0961) 5590902 500000 470
74 Dibromochloromethane 129 6033 6033 (0865) 7227226 500000 530(A)
77 12-Dibromoethane 107 6277 6277 (0900) 5952425 500000 500(A)
78 Chlorobenzene-d5 117 6972 6972 (1000) 2224153 500000
79 Chlorobenzene 112 6997 6997 (1003) 18374405 500000 460
81 Ethylbenzene 106 7094 7094 (1017) 10693410 500000 500(A)
82 m+p-Xylene 106 7308 7308 (1048) 23238078 100000 880
84 o-Xylene 106 7887 7887 (1131) 12821590 500000 490
85 Styrene 104 7966 7966 (1143) 19831782 500000 440
86 Bromoform 173 7942 7942 (1139) 4974461 500000 520(A)
88 Isopropylbenzene 105 8368 8368 (1200) 26165908 500000 420(A)
$ 89 Bromofluorobenzene (SUR) 174 8728 8728 (0832) 954872 500000 51
92 1122-Tetrachloroethane 83 9143 9143 (0871) 7365342 500000 490
105 13-Dichlorobenzene 146 10362 10362 (0987) 14243841 500000 480
108 14-Dichlorobenzene-d4 152 10496 10496 (1000) 1163568 500000
109 14-Dichlorobenzene 146 10526 10526 (1003) 14602396 500000 470
111 12-Dichlorobenzene 146 11185 11185 (1066) 13405399 500000 480
112 12-Dibromo-3-chloropropane 75 12246 12246 (1167) 1274610 500000 480
114 124-Trichlorobenzene 180 12977 12977 (1236) 6669727 500000 470
M 120 12-Dichloroethene (Total) 100 11958070 100000 940
M 121 Xylene (Total) 100 36059668 150000 1400
QC Flag Legend
A - Target compound detected but quantitated amountexceeded maximum amount
10162012Page 94 of 323
Data File e07842d
Date 17-SEP-2012 0710
Client ID Instrument VOAMS5i
Sample Info IC-VMCAL6 Operator GCMS VOAMS5
10162012Page 95 of 323
FORM VII
Lab Name Job No
SDG No
Instrument ID
Calibration Date
Calib Start Date
Lab Sample ID
Calib End DateGC Column ID
GCMS VOA CONTINUING CALIBRATION DATA
018(mm)
460-45537-1
VOAMS5
10112012 2050
09172012 0449
09172012 0710
CCVIS 460-1316562
Rtx-VMS
TestAmerica Edison
Lab File ID e08976d Heated Purge (YN) NConc Units ugL
ANALYTE CURVE CALC SPIKE D MAX
TYPE AMOUNT AMOUNT D
AVE RRF RRF MIN RRF
Dichlorodifluoromethane 0194701761 01000 221 200 105 250Ave
Chloromethane 0322303733 01000 173 200 -137 250Ave
Vinyl chloride 0274402985 01000 184 200 -81 250Ave
Bromomethane 0159401312 01000 243 200 215 250Ave
Chloroethane 0127501099 01000 232 200 160 250Ave
Trichlorofluoromethane 0296002422 01000 244 200 222 250Ave
11-Dichloroethene 0161001496 01000 215 200 76 250Ave
Carbon disulfide 0655806887 01000 190 200 -48 250Ave
112-Trichloro-122-trifluoroethane
0198901691 01000 235 200 176 250Ave
Methylene Chloride 0341503576 01000 191 200 -45 250Ave
Acetone 0021400184 01000 233 200 164 250Ave
trans-12-Dichloroethene 0208902052 01000 204 200 18 250Ave
Methyl acetate 0037700426 01000 177 200 -115 250Ave
Methyl tert-butyl ether 0665806838 01000 195 200 -26 250Ave
11-Dichloroethane 0443404582 01000 194 200 -32 250Ave
cis-12-Dichloroethene 0227602361 01000 193 200 -36 250Ave
Cyclohexane 0338904145 01000 163 200 -183 250Ave
Chloroform 0397703982 01000 200 200 -01 250Ave
Carbon tetrachloride 0281602705 01000 208 200 41 250Ave
111-Trichloroethane 0352303375 01000 209 200 44 250Ave
2-Butanone (MEK) 0035400341 01000 208 200 40 250Ave
Benzene 10301190 01000 173 200 -134 250Ave
12-Dichloroethane 0331603284 01000 202 200 10 250Ave
Methylcyclohexane 0280603325 01000 169 200 -156 250Ave
Trichloroethene 0228602385 01000 192 200 -41 250Ave
12-Dichloropropane 0242002756 01000 176 200 -122 250Ave
Dichlorobromomethane 0303603195 01000 190 200 -50 250Ave
cis-13-Dichloropropene 0438605308 01000 165 200 -174 250Ave
Toluene 12151323 01000 184 200 -81 250Ave
Tetrachloroethene 0302803113 01000 195 200 -27 250Ave
4-Methyl-2-pentanone (MIBK) 0273203593 01000 152 200 -240 250Ave
trans-13-Dichloropropene 0396604819 01000 165 200 -177 250Ave
112-Trichloroethane 0185102264 01000 164 200 -182 250Ave
Chlorodibromomethane 0265003083 01000 172 200 -141 250Ave
12-Dibromoethane 0231002670 01000 173 200 -135 250Ave
2-Hexanone 0209702668 01000 157 200 -214 250Ave
Chlorobenzene 0830208882 01000 187 200 -65 250Ave
Ethylbenzene 0437104756 01000 184 200 -81 250Ave
m-Xylene amp p-Xylene 0555805917 01000 376 400 -61 250Ave
o-Xylene 0545405886 01000 185 200 -73 250Ave
FORM VII 8260B
10162012Page 96 of 323
FORM VII
Lab Name Job No
SDG No
Instrument ID
Calibration Date
Calib Start Date
Lab Sample ID
Calib End DateGC Column ID
GCMS VOA CONTINUING CALIBRATION DATA
018(mm)
460-45537-1
VOAMS5
10112012 2050
09172012 0449
09172012 0710
CCVIS 460-1316562
Rtx-VMS
TestAmerica Edison
Lab File ID e08976d Heated Purge (YN) NConc Units ugL
ANALYTE CURVE CALC SPIKE D MAX
TYPE AMOUNT AMOUNT D
AVE RRF RRF MIN RRF
Bromoform 0188102147 01000 175 200 -124 250Ave
Styrene 092181000 01000 184 200 -78 250Ave
Isopropylbenzene 13421415 01000 190 200 -52 250Ave
1122-Tetrachloroethane 0512306462 01000 159 200 -207 250Ave
13-Dichlorobenzene 11861279 01000 186 200 -72 250Ave
14-Dichlorobenzene 12311326 01000 186 200 -72 250Ave
12-Dichlorobenzene 11211209 01000 185 200 -73 250Ave
12-Dibromo-3-Chloropropane 0086101130 01000 152 200 -238 250Ave
124-Trichlorobenzene 0630306118 01000 206 200 30 250Ave
12-Dichloroethane-d4 (Surr) 0310902638 01000 589 500 178 250Ave
Toluene-d8 (Surr) 11551167 01000 495 500 -11 250Ave
4-Bromofluorobenzene 0811108079 01000 502 500 04 250Ave
FORM VII 8260B
10162012Page 97 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08976d Report Date 11-Oct-2012 2130
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08976dLab Smp Id CCVIS Inj Date 11-OCT-2012 2050 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info CCVISMisc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 1 Continuing Calibration SampleDil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0900 0900 (0250) 102235 200000 22
3 Chloromethane 50 1016 1016 (0282) 169224 200000 17
4 Vinyl Chloride 62 1028 1028 (0286) 144069 200000 18
6 Bromomethane 94 1181 1181 (0328) 83687 200000 24
5 Chloroethane 64 1242 1242 (0345) 66969 200000 23
7 Trichlorofluoromethane 101 1303 1303 (0362) 155393 200000 24
14 Freon TF 101 1577 1577 (0438) 104446 200000 24
15 11-Dichloroethene 96 1553 1553 (0431) 84531 200000 22
16 Acetone 58 1894 1894 (0526) 11228 200000 23
18 Carbon Disulfide 76 1571 1571 (0436) 344348 200000 19
27 Methyl Acetate 74 1967 1967 (0546) 19813 200000 18
22 Methylene Chloride 49 1864 1864 (0518) 179288 200000 19
28 MTBE 73 2022 2022 (0562) 349596 200000 19
25 trans-12-Dichloroethene 96 1949 1949 (0541) 109681 200000 20
30 11-Dichloroethane 63 2309 2309 (0641) 232818 200000 19
36 cis-12-Dichloroethene 96 2656 2656 (0738) 119502 200000 19
10162012Page 98 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08976d Report Date 11-Oct-2012 2130
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3077 3077 (0854) 18598 200000 21
42 Chloroform 83 2845 2845 (0790) 208815 200000 20
44 Cyclohexane 56 2784 2784 (0773) 177923 200000 16
43 111-Trichloroethane 97 2985 2985 (0829) 185002 200000 21
45 Carbon Tetrachloride 117 2937 2937 (0815) 147853 200000 21
48 Benzene 78 3260 3260 (0469) 476925 200000 17
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0934) 408134 500000 59
49 12-Dichloroethane 62 3418 3418 (0949) 174132 200000 20
52 Fluorobenzene 96 3601 3601 (1000) 1312656 500000
54 Trichloroethene 95 3741 3741 (1039) 120041 200000 19
56 Methyl cyclohexane 83 3729 3729 (1036) 147336 200000 17
57 12-Dichloropropane 63 4199 4199 (1166) 127078 200000 18
68 Bromodichloromethane 83 4272 4272 (1186) 159386 200000 19
67 cis-13-Dichloropropene 75 4912 4912 (0706) 203059 200000 16
70 4-Methyl-2-Pentanone 43 5625 5625 (0809) 126467 200000 15
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1336847 500000 49
66 Toluene 91 5162 5162 (0742) 562689 200000 18
64 trans-13-Dichloropropene 75 5649 5649 (0812) 183587 200000 16
69 112-Trichloroethane 83 5820 5820 (0837) 85707 200000 16
71 Tetrachloroethene 166 5582 5582 (0803) 140177 200000 19
73 2-Hexanone 43 6680 6680 (0961) 97080 200000 16
74 Dibromochloromethane 129 6021 6021 (0866) 122657 200000 17
77 12-Dibromoethane 107 6265 6265 (0901) 106920 200000 17
78 Chlorobenzene-d5 117 6954 6954 (1000) 1157341 500000
79 Chlorobenzene 112 6972 6972 (1003) 384334 200000 19
81 Ethylbenzene 106 7064 7064 (1016) 202362 200000 18
82 m+p-Xylene 106 7277 7277 (1046) 514606 400000 38
84 o-Xylene 106 7862 7862 (1131) 252476 200000 18
85 Styrene 104 7942 7942 (1142) 426740 200000 18
86 Bromoform 173 7911 7911 (1138) 87078 200000 18
88 Isopropylbenzene 105 8350 8350 (1201) 621124 200000 19
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 541700 500000 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 136860 200000 16
105 13-Dichlorobenzene 146 10331 10331 (0987) 316835 200000 18
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 667834 500000
109 14-Dichlorobenzene 146 10490 10490 (1002) 328709 200000 18
111 12-Dichlorobenzene 146 11148 11148 (1065) 299393 200000 18
112 12-Dibromo-3-chloropropane 75 12234 12234 (1169) 23001 200000 15
114 124-Trichlorobenzene 180 12977 12977 (1240) 168371 200000 21
M 120 12-Dichloroethene (Total) 100 229183 400000 40
M 121 Xylene (Total) 100 767082 600000 56
10162012Page 99 of 323
Data File e08976d
Date 11-OCT-2012 2050
Client ID Instrument VOAMS5i
Sample Info CCVIS Operator GCMS VOAMS5
10162012Page 100 of 323
FORM VII
Lab Name Job No
SDG No
Instrument ID
Calibration Date
Calib Start Date
Lab Sample ID
Calib End DateGC Column ID
GCMS VOA CONTINUING CALIBRATION DATA
018(mm)
460-45537-1
VOAMS5
10122012 0114
09172012 0449
09172012 0710
CCV 460-13165610
Rtx-VMS
TestAmerica Edison
Lab File ID e08987d Heated Purge (YN) NConc Units ugL
ANALYTE CURVE CALC SPIKE D MAX
TYPE AMOUNT AMOUNT D
AVE RRF RRF MIN RRF
Dichlorodifluoromethane 0166601761 01000 189 200 -54 250Ave
Chloromethane 0311403733 01000 167 200 -166 250Ave
Vinyl chloride 0256002985 01000 172 200 -142 250Ave
Bromomethane 0162301312 01000 247 200 237 250Ave
Chloroethane 0127201099 01000 231 200 157 250Ave
Trichlorofluoromethane 0257102422 01000 212 200 62 250Ave
11-Dichloroethene 0184901496 01000 247 200 236 250Ave
112-Trichloro-122-trifluoroethane
0225501691 01000 267 200 334 250Ave
Carbon disulfide 0788506887 01000 229 200 145 250Ave
Methylene Chloride 0351303576 01000 196 200 -18 250Ave
Acetone 0022000184 01000 239 200 197 250Ave
trans-12-Dichloroethene 0232002052 01000 226 200 130 250Ave
Methyl acetate 0048700426 01000 228 200 141 250Ave
Methyl tert-butyl ether 0769506838 01000 225 200 125 250Ave
11-Dichloroethane 0469804582 01000 205 200 25 250Ave
cis-12-Dichloroethene 0240902361 01000 204 200 20 250Ave
Cyclohexane 0384004145 01000 185 200 -74 250Ave
Chloroform 0438203982 01000 220 200 100 250Ave
Carbon tetrachloride 0291802705 01000 216 200 79 250Ave
111-Trichloroethane 0362803375 01000 215 200 75 250Ave
2-Butanone (MEK) 0042500341 01000 250 200 248 250Ave
Benzene 11151190 01000 188 200 -62 250Ave
12-Dichloroethane 0359603284 01000 219 200 95 250Ave
Methylcyclohexane 0344803325 01000 207 200 37 250Ave
Trichloroethene 0248302385 01000 208 200 41 250Ave
12-Dichloropropane 0265202756 01000 192 200 -38 250Ave
Dichlorobromomethane 0339803195 01000 213 200 63 250Ave
cis-13-Dichloropropene 0490405308 01000 185 200 -76 250Ave
Toluene 12801323 01000 194 200 -32 250Ave
Tetrachloroethene 0323103113 01000 208 200 38 250Ave
4-Methyl-2-pentanone (MIBK) 0319703593 01000 178 200 -110 250Ave
trans-13-Dichloropropene 0454104819 01000 188 200 -58 250Ave
112-Trichloroethane 0212502264 01000 188 200 -61 250Ave
Chlorodibromomethane 0306403083 01000 199 200 -06 250Ave
12-Dibromoethane 0261302670 01000 196 200 -22 250Ave
2-Hexanone 0243802668 01000 183 200 -86 250Ave
Chlorobenzene 0879308882 01000 198 200 -10 250Ave
Ethylbenzene 0463104756 01000 195 200 -26 250Ave
m-Xylene amp p-Xylene 0587505917 01000 397 400 -07 250Ave
o-Xylene 0578505886 01000 197 200 -17 250Ave
FORM VII 8260B
10162012Page 101 of 323
FORM VII
Lab Name Job No
SDG No
Instrument ID
Calibration Date
Calib Start Date
Lab Sample ID
Calib End DateGC Column ID
GCMS VOA CONTINUING CALIBRATION DATA
018(mm)
460-45537-1
VOAMS5
10122012 0114
09172012 0449
09172012 0710
CCV 460-13165610
Rtx-VMS
TestAmerica Edison
Lab File ID e08987d Heated Purge (YN) NConc Units ugL
ANALYTE CURVE CALC SPIKE D MAX
TYPE AMOUNT AMOUNT D
AVE RRF RRF MIN RRF
Bromoform 0223102147 01000 208 200 39 250Ave
Styrene 099051000 01000 198 200 -09 250Ave
Isopropylbenzene 14391415 01000 203 200 17 250Ave
1122-Tetrachloroethane 0579606462 01000 179 200 -103 250Ave
13-Dichlorobenzene 12591279 01000 197 200 -15 250Ave
14-Dichlorobenzene 13061326 01000 197 200 -15 250Ave
12-Dichlorobenzene 12151209 01000 201 200 05 250Ave
12-Dibromo-3-Chloropropane 0102901130 01000 182 200 -90 250Ave
124-Trichlorobenzene 0743906118 01000 243 200 216 250Ave
12-Dichloroethane-d4 (Surr) 0320902638 01000 608 500 216 250Ave
Toluene-d8 (Surr) 11471167 01000 491 500 -18 250Ave
4-Bromofluorobenzene 0806308079 01000 499 500 -02 250Ave
FORM VII 8260B
10162012Page 102 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12abe08987d Report Date 12-Oct-2012 0132
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12abe08987dLab Smp Id CCV Inj Date 12-OCT-2012 0114 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info CCVMisc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12ab8260DE_09mMeth Date 12-Oct-2012 0132 ken Quant Type ISTDCal Date 12-OCT-2012 0114 Cal File e08987dAls bottle 12 Continuing Calibration SampleDil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0894 0894 (0249) 84911 200000 19
3 Chloromethane 50 1016 1016 (0283) 158694 200000 17
4 Vinyl Chloride 62 1022 1022 (0284) 130464 200000 17
6 Bromomethane 94 1181 1181 (0328) 82695 200000 25
5 Chloroethane 64 1236 1236 (0344) 64840 200000 23
7 Trichlorofluoromethane 101 1297 1297 (0361) 131020 200000 21
14 Freon TF 101 1565 1565 (0435) 114931 200000 27
15 11-Dichloroethene 96 1547 1547 (0430) 94244 200000 25
16 Acetone 58 1894 1894 (0527) 11208 200000 24
18 Carbon Disulfide 76 1565 1565 (0435) 401807 200000 23
27 Methyl Acetate 74 1961 1961 (0546) 24794 200000 23
22 Methylene Chloride 49 1857 1857 (0517) 179010 200000 20
28 MTBE 73 2022 2022 (0562) 392131 200000 22
25 trans-12-Dichloroethene 96 1943 1943 (0540) 118223 200000 23
30 11-Dichloroethane 63 2302 2302 (0640) 239419 200000 20
36 cis-12-Dichloroethene 96 2650 2650 (0737) 122782 200000 20
10162012Page 103 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12abe08987d Report Date 12-Oct-2012 0132
AMOUNTS
QUANT SIG CAL-AMT ON-COL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3077 3077 (0856) 21666 200000 25
42 Chloroform 83 2845 2845 (0791) 223324 200000 22
44 Cyclohexane 56 2784 2784 (0774) 195679 200000 18
43 111-Trichloroethane 97 2979 2979 (0829) 184861 200000 21
45 Carbon Tetrachloride 117 2930 2930 (0815) 148689 200000 22
48 Benzene 78 3260 3260 (0469) 501947 200000 19
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 408924 500000 61
49 12-Dichloroethane 62 3418 3418 (0951) 183231 200000 22
52 Fluorobenzene 96 3595 3595 (1000) 1274024 500000
54 Trichloroethene 95 3741 3741 (1041) 126518 200000 21
56 Methyl cyclohexane 83 3723 3723 (1036) 175700 200000 21
57 12-Dichloropropane 63 4192 4192 (1166) 135130 200000 19
68 Bromodichloromethane 83 4272 4272 (1188) 173147 200000 21
67 cis-13-Dichloropropene 75 4906 4906 (0705) 220680 200000 18
70 4-Methyl-2-Pentanone 43 5631 5631 (0810) 143892 200000 18
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1290179 500000 49
66 Toluene 91 5162 5162 (0742) 576151 200000 19
64 trans-13-Dichloropropene 75 5649 5649 (0812) 204342 200000 19
69 112-Trichloroethane 83 5820 5820 (0837) 95620 200000 19
71 Tetrachloroethene 166 5582 5582 (0803) 145404 200000 21
73 2-Hexanone 43 6680 6680 (0961) 109697 200000 18
74 Dibromochloromethane 129 6015 6015 (0865) 137888 200000 20
77 12-Dibromoethane 107 6265 6265 (0901) 117575 200000 20
78 Chlorobenzene-d5 117 6954 6954 (1000) 1125053 500000
79 Chlorobenzene 112 6972 6972 (1003) 395719 200000 20
81 Ethylbenzene 106 7064 7064 (1016) 208414 200000 19
82 m+p-Xylene 106 7277 7277 (1046) 528781 400000 40
84 o-Xylene 106 7856 7856 (1130) 260320 200000 20
85 Styrene 104 7942 7942 (1142) 445737 200000 20
86 Bromoform 173 7917 7917 (1139) 100375 200000 21
88 Isopropylbenzene 105 8344 8344 (1200) 647568 200000 20
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 536325 500000 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 154190 200000 18
105 13-Dichlorobenzene 146 10331 10331 (0987) 335032 200000 20
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 665092 500000
109 14-Dichlorobenzene 146 10490 10490 (1002) 347387 200000 20
111 12-Dichlorobenzene 146 11148 11148 (1065) 323155 200000 20
112 12-Dibromo-3-chloropropane 75 12233 12233 (1169) 27376 200000 18
114 124-Trichlorobenzene 180 12977 12977 (1240) 197894 200000 24
M 120 12-Dichloroethene (Total) 100 241005 400000 43
M 121 Xylene (Total) 100 789101 600000 59
10162012Page 104 of 323
Data File e08987d
Date 12-OCT-2012 0114
Client ID Instrument VOAMS5i
Sample Info CCV Operator GCMS VOAMS5
10162012Page 105 of 323
Data File chemVOAMS5i8260DE09-17-1217sep12be07834d Report Date 17-Sep-2012 0605
TestAmerica
Data file chemVOAMS5i8260DE09-17-1217sep12be07834dLab Smp Id BFB Inj Date 17-SEP-2012 0324 Operator VOAMS 1 Inst ID VOAMS5iSmp Info BFBMisc Info Comment Method chemVOAMS5i8260DE09-17-1217sep12bBFBDELmMeth Date 27-Feb-2012 1508 sylvanus Quant Type ISTDCal Date Cal File Als bottle 2 QC Sample BFBDil Factor 100000 Integrator HP RTE Compound Sublist allsubTarget Version 350 Sample Matrix WATERProcessing Host hpd2
Concentration Formula Amt DF Uf Vf VI CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorUf 100000 ng unit correction factorVf 100000 Volumetric correction factorVI 100000 Injection Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT (REL RT) MASS RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 BFB CAS 460-00-4
2352 2600 (0000) 95 195072 000- 10000 10000
2352 2600 (0000) 50 42624 1500- 4000 2185
2352 2600 (0000) 75 102376 3000- 6000 5248
2352 2600 (0000) 96 12530 500- 900 642
2352 2600 (0000) 173 0 000- 200 000
2352 2600 (0000) 174 155200 5000- 10000 7956
2352 2600 (0000) 175 12902 500- 900 831
2352 2600 (0000) 176 148480 9500- 10100 9567
2352 2600 (0000) 177 9343 500- 900 629
-------------------------------------------------------------------------------
10162012Page 106 of 323
Data File e07834d
Date 17-SEP-2012 0324
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
10162012Page 107 of 323
Data File e07834d
Date 17-SEP-2012 0324
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
1 BFB
RELATIVE me ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak 100 relative abundance | 10000 || 50 | 1500 - 4000 of mass 95 | 2185 || 75 | 3000 - 6000 of mass 95 | 5248 || 96 | 500 - 900 of mass 95 | 642 || 173 | Less than 200 of mass 174 | 000 ( 000) || 174 | 5000 - 10000 of mass 95 | 7956 || 175 | 500 - 900 of mass 174 | 661 ( 831) || 176 | 9500 - 10100 of mass 174 | 7612 ( 9567) || 177 | 500 - 900 of mass 176 | 479 ( 629) |+-----+------------------------------------------+---------------------+
10162012Page 108 of 323
Data File e07834d
Date 17-SEP-2012 0324
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
Data File chemVOAMS5i8260DE09-17-1217sep12be07834dSpectrum Avg Scans 50-52 ( 235) Background Scan 46
Location of Maximum 9500Number of points 151
mz Y mz Y mz Y mz Y+------------------+------------------+------------------+------------------+| 3500 53 | 7700 1350 | 12300 88 | 17700 9343 || 3600 1914 | 7800 695 | 12400 252 | 17800 381 || 3700 12535 | 7900 5782 | 12500 148 | 18000 35 || 3800 10760 | 8000 1455 | 12700 282 | 18300 181 || 3900 3962 | 8100 5745 | 12800 338 | 18600 248 |+------------------+------------------+------------------+------------------+| 4100 387 | 8200 905 | 12900 75 | 18700 80 || 4400 707 | 8300 42 | 13000 926 | 18800 162 || 4500 1464 | 8500 229 | 13100 166 | 18900 142 || 4600 281 | 8600 239 | 13200 7 | 19100 151 || 4700 3334 | 8700 7427 | 13400 27 | 19200 54 |+------------------+------------------+------------------+------------------+| 4800 1491 | 8800 7774 | 13700 332 | 19300 44 || 4900 8401 | 9100 1022 | 13800 172 | 19400 110 || 5000 42624 | 9200 5845 | 14000 185 | 19600 46 || 5100 13346 | 9300 8046 | 14100 1957 | 19800 171 || 5200 539 | 9400 21672 | 14200 53 | 20000 162 |+------------------+------------------+------------------+------------------+| 5300 13 | 9500 195072 | 14300 1698 | 20200 62 || 5400 14 | 9600 12530 | 14400 295 | 20300 48 || 5500 230 | 9700 551 | 14500 186 | 20400 104 || 5600 3600 | 9900 79 | 14600 115 | 20500 34 || 5700 5500 | 10000 36 | 14700 156 | 20700 223 |+------------------+------------------+------------------+------------------+| 5800 113 | 10100 136 | 14800 465 | 20900 81 || 5900 106 | 10200 36 | 14900 118 | 21500 80 || 6000 1861 | 10300 237 | 15000 105 | 21900 89 || 6100 10125 | 10400 905 | 15300 459 | 22000 60 || 6200 9219 | 10500 514 | 15400 192 | 22600 84 |+------------------+------------------+------------------+------------------+| 6300 7541 | 10600 1054 | 15700 390 | 23000 188 || 6400 270 | 10700 304 | 16000 378 | 23100 74 || 6500 625 | 11000 398 | 16100 530 | 23500 107 || 6600 51 | 11100 151 | 16400 54 | 23900 43 || 6700 378 | 11200 121 | 16700 172 | 24600 123 |+------------------+------------------+------------------+------------------+| 6800 20496 | 11300 247 | 16800 205 | 24700 37 || 6900 19976 | 11500 421 | 16900 243 | 25000 57 || 7000 1570 | 11600 358 | 17000 351 | 25200 33 || 7200 740 | 11700 1343 | 17100 439 | 25500 46 || 7300 9006 | 11800 855 | 17200 227 | 26200 43 |+------------------+------------------+------------------+------------------+| 7400 34320 | 11900 733 | 17400 155200 | 26400 63 || 7500 102376 | 12100 68 | 17500 12902 | 26500 45 || 7600 8204 | 12200 77 | 17600 148480 | |+------------------+------------------+------------------+------------------+
10162012Page 109 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08975d Report Date 11-Oct-2012 2012
TestAmerica
Data file chemVOAMS5i8260DE09-17-1211oct12be08975dLab Smp Id BFB Inj Date 11-OCT-2012 2008 Operator VOAMS 1 Inst ID VOAMS5iSmp Info BFBMisc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12bBFBDELmMeth Date 27-Feb-2012 1508 sylvanus Quant Type ISTDCal Date Cal File Als bottle 2 QC Sample BFBDil Factor 100000 Integrator HP RTE Compound Sublist allsubTarget Version 350 Sample Matrix WATERProcessing Host hpd2
Concentration Formula Amt DF Uf Vf VI CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorUf 100000 ng unit correction factorVf 100000 Volumetric correction factorVI 100000 Injection Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT (REL RT) MASS RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 BFB CAS 460-00-4
2352 2600 (0000) 95 135522 000- 10000 10000
2352 2600 (0000) 50 29541 1500- 4000 2180
2352 2600 (0000) 75 70179 3000- 6000 5178
2352 2600 (0000) 96 8846 500- 900 653
2352 2600 (0000) 173 896 000- 200 074
2352 2600 (0000) 174 121433 5000- 10000 8960
2352 2600 (0000) 175 9704 500- 900 799
2352 2600 (0000) 176 118148 9500- 10100 9729
2352 2600 (0000) 177 7241 500- 900 613
-------------------------------------------------------------------------------
10162012Page 110 of 323
Data File e08975d
Date 11-OCT-2012 2008
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
10162012Page 111 of 323
Data File e08975d
Date 11-OCT-2012 2008
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
1 BFB
RELATIVE me ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak 100 relative abundance | 10000 || 50 | 1500 - 4000 of mass 95 | 2180 || 75 | 3000 - 6000 of mass 95 | 5178 || 96 | 500 - 900 of mass 95 | 653 || 173 | Less than 200 of mass 174 | 066 ( 074) || 174 | 5000 - 10000 of mass 95 | 8960 || 175 | 500 - 900 of mass 174 | 716 ( 799) || 176 | 9500 - 10100 of mass 174 | 8718 ( 9729) || 177 | 500 - 900 of mass 176 | 534 ( 613) |+-----+------------------------------------------+---------------------+
10162012Page 112 of 323
Data File e08975d
Date 11-OCT-2012 2008
Client ID Instrument VOAMS5i
Sample Info BFB Operator VOAMS 1
Data File chemVOAMS5i8260DE09-17-1211oct12be08975dSpectrum Avg Scans 50-52 ( 235) Background Scan 46
Location of Maximum 9500Number of points 149
mz Y mz Y mz Y mz Y+------------------+------------------+------------------+------------------+| 3600 1294 | 7800 45 | 13100 382 | 18200 69 || 3700 8431 | 7900 4274 | 13200 84 | 18300 115 || 3800 6991 | 8000 1313 | 13400 26 | 18600 116 || 3900 2548 | 8100 3602 | 13500 465 | 18700 340 || 4000 550 | 8200 868 | 13600 63 | 18800 34 |+------------------+------------------+------------------+------------------+| 4100 253 | 8300 128 | 13700 225 | 18900 18 || 4200 100 | 8400 171 | 13900 69 | 19900 265 || 4400 553 | 8500 53 | 14000 115 | 20100 29 || 4500 1283 | 8700 5211 | 14100 1442 | 20400 84 || 4700 1587 | 8800 4550 | 14200 269 | 20500 33 |+------------------+------------------+------------------+------------------+| 4800 651 | 9100 642 | 14300 1465 | 20600 138 || 4900 5880 | 9200 3657 | 14400 23 | 20700 20 || 5000 29536 | 9300 6715 | 14500 103 | 20900 79 || 5100 8612 | 9400 15687 | 14700 151 | 21000 74 || 5200 396 | 9500 135488 | 14800 365 | 21100 1 |+------------------+------------------+------------------+------------------+| 5300 107 | 9600 8846 | 14900 429 | 21200 140 || 5500 726 | 9700 271 | 15100 54 | 21300 52 || 5600 1691 | 9800 1 | 15300 430 | 21400 189 || 5700 4463 | 10000 110 | 15400 385 | 22100 72 || 5800 245 | 10300 207 | 15500 1021 | 22200 35 |+------------------+------------------+------------------+------------------+| 5900 116 | 10400 668 | 15600 236 | 22400 188 || 6000 1281 | 10600 562 | 15700 473 | 22600 79 || 6100 6975 | 10700 159 | 15800 3 | 22800 39 || 6200 7260 | 11000 145 | 15900 410 | 23000 95 || 6300 5465 | 11100 68 | 16100 441 | 23300 189 |+------------------+------------------+------------------+------------------+| 6400 672 | 11200 80 | 16400 208 | 23400 42 || 6500 144 | 11300 261 | 16500 57 | 23500 36 || 6600 201 | 11600 813 | 17000 641 | 23600 58 || 6700 729 | 11700 882 | 17100 38 | 24100 103 || 6800 14333 | 11800 446 | 17200 338 | 24700 36 |+------------------+------------------+------------------+------------------+| 6900 14506 | 11900 1049 | 17300 896 | 25100 40 || 7000 1361 | 12000 38 | 17400 121432 | 25500 61 || 7200 782 | 12100 249 | 17500 9704 | 25600 33 || 7300 6586 | 12400 108 | 17600 118144 | 26000 59 || 7400 24016 | 12600 138 | 17700 7241 | 26500 78 |+------------------+------------------+------------------+------------------+| 7500 70176 | 12700 39 | 17900 19 | || 7600 5444 | 12900 479 | 18000 29 | || 7700 507 | 13000 702 | 18100 322 | |+------------------+------------------+------------------+------------------+
10162012Page 113 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
SDG No
460-45537-1
Lab Sample ID MB 460-1316564
Matrix e08981dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2247
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 0060U71-55-6 111-Trichloroethane 0060
10 022U75-71-8 Dichlorodifluoromethane 022
10 010U74-87-3 Chloromethane 010
10 014U75-01-4 Vinyl chloride 014
10 018U74-83-9 Bromomethane 018
10 040U96-12-8 12-Dibromo-3-Chloropropane 040
10 021U95-50-1 12-Dichlorobenzene 021
10 015U75-69-4 Trichlorofluoromethane 015
10 0090U75-35-4 11-Dichloroethene 0090
10 0090U78-87-5 12-Dichloropropane 0090
10 0080U76-13-1 112-Trichloro-122-trifluoroethane
0080
50 27U67-64-1 Acetone 27
10 013U75-15-0 Carbon disulfide 013
20 034U79-20-9 Methyl acetate 034
10 018U75-09-2 Methylene Chloride 018
10 013U156-60-5 trans-12-Dichloroethene 013
10 020U124-48-1 Chlorodibromomethane 020
10 014U1634-04-4 Methyl tert-butyl ether 014
10 017U75-00-3 Chloroethane 017
10 013U75-34-3 11-Dichloroethane 013
10 018U156-59-2 cis-12-Dichloroethene 018
50 23U78-93-3 2-Butanone (MEK) 23
10 0080U67-66-3 Chloroform 0080
10 010U100-41-4 Ethylbenzene 010
10 016U110-82-7 Cyclohexane 016
10 0060U56-23-5 Carbon tetrachloride 0060
10 0080U71-43-2 Benzene 0080
10 019U107-06-2 12-Dichloroethane 019
10 0090U79-01-6 Trichloroethene 0090
10 014U108-87-2 Methylcyclohexane 014
10 012U75-27-4 Dichlorobromomethane 012
10 018U10061-01-5 cis-13-Dichloropropene 018
50 099U108-10-1 4-Methyl-2-pentanone (MIBK) 099
10 015U108-88-3 Toluene 015
10 024U10061-02-6 trans-13-Dichloropropene 024
FORM I 8260B
10162012Page 114 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
SDG No
460-45537-1
Lab Sample ID MB 460-1316564
Matrix e08981dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2247
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 019U79-00-5 112-Trichloroethane 019
10 010U127-18-4 Tetrachloroethene 010
50 050U591-78-6 2-Hexanone 050
10 028U106-93-4 12-Dibromoethane 028
10 011U108-90-7 Chlorobenzene 011
30 036U1330-20-7 Xylenes Total 036
10 012U100-42-5 Styrene 012
10 019U75-25-2 Bromoform 019
10 0080U98-82-8 Isopropylbenzene 0080
10 016U79-34-5 1122-Tetrachloroethane 016
10 014U541-73-1 13-Dichlorobenzene 014
10 023U106-46-7 14-Dichlorobenzene 023
10 034U120-82-1 124-Trichlorobenzene 034
RECCAS NO LIMITSQSURROGATE
99 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
95 70-130460-00-4 4-Bromofluorobenzene
96 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 115 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID
Lab Name Job No
SDG No
460-45537-1
Lab Sample ID MB 460-1316564
Matrix e08981dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2247
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
Number TICs Found TIC Result Total 00
QRTCOMPOUND NAME RESULTCAS NO
Tentatively Identified Compound None
FORM I-TIC 8260B
10162012Page 116 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08981d Report Date 12-Oct-2012 0041
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08981dLab Smp Id MB Inj Date 11-OCT-2012 2247 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info MBMisc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 6 QC Sample BLANKDil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 381607 495518 50
52 Fluorobenzene 96 3595 3601 (1000) 1238441 500000
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1209056 482553 48
78 Chlorobenzene-d5 117 6954 6954 (1000) 1084553 500000
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 494380 477044 48
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 638826 500000
10162012Page 117 of 323
Data File e08981d
Date 11-OCT-2012 2247
Client ID Instrument VOAMS5i
Sample Info MB Operator GCMS VOAMS5
10162012Page 118 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
SDG No
460-45537-1
Lab Sample ID LCS 460-1316563
Matrix e08977dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2113
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 006071-55-6 111-Trichloroethane 210
10 02275-71-8 Dichlorodifluoromethane 181
10 01074-87-3 Chloromethane 210
10 01475-01-4 Vinyl chloride 203
10 01874-83-9 Bromomethane 211
10 04096-12-8 12-Dibromo-3-Chloropropane 222
10 02195-50-1 12-Dichlorobenzene 209
10 01575-69-4 Trichlorofluoromethane 190
10 009075-35-4 11-Dichloroethene 223
10 009078-87-5 12-Dichloropropane 211
10 008076-13-1 112-Trichloro-122-trifluoroethane
203
50 2767-64-1 Acetone 250
10 01375-15-0 Carbon disulfide 218
20 03479-20-9 Methyl acetate 220
10 01875-09-2 Methylene Chloride 200
10 013156-60-5 trans-12-Dichloroethene 216
10 020124-48-1 Chlorodibromomethane 217
10 0141634-04-4 Methyl tert-butyl ether 207
10 01775-00-3 Chloroethane 201
10 01375-34-3 11-Dichloroethane 204
10 018156-59-2 cis-12-Dichloroethene 211
50 2378-93-3 2-Butanone (MEK) 214
10 008067-66-3 Chloroform 205
10 010100-41-4 Ethylbenzene 206
10 016110-82-7 Cyclohexane 208
10 006056-23-5 Carbon tetrachloride 211
10 008071-43-2 Benzene 212
10 019107-06-2 12-Dichloroethane 204
10 009079-01-6 Trichloroethene 212
10 014108-87-2 Methylcyclohexane 215
10 01275-27-4 Dichlorobromomethane 214
10 01810061-01-5 cis-13-Dichloropropene 216
50 099108-10-1 4-Methyl-2-pentanone (MIBK) 214
10 015108-88-3 Toluene 205
10 02410061-02-6 trans-13-Dichloropropene 215
FORM I 8260B
10162012Page 119 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
SDG No
460-45537-1
Lab Sample ID LCS 460-1316563
Matrix e08977dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 1
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10112012 2113
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
10 01979-00-5 112-Trichloroethane 217
10 010127-18-4 Tetrachloroethene 210
50 050591-78-6 2-Hexanone 201
10 028106-93-4 12-Dibromoethane 215
10 011108-90-7 Chlorobenzene 206
30 0361330-20-7 Xylenes Total 612
10 012100-42-5 Styrene 207
10 01975-25-2 Bromoform 217
10 008098-82-8 Isopropylbenzene 207
10 01679-34-5 1122-Tetrachloroethane 210
10 014541-73-1 13-Dichlorobenzene 204
10 023106-46-7 14-Dichlorobenzene 204
10 034120-82-1 124-Trichlorobenzene 220
RECCAS NO LIMITSQSURROGATE
96 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
97 70-130460-00-4 4-Bromofluorobenzene
99 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 120 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08977d Report Date 11-Oct-2012 2301
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08977dLab Smp Id LCS Inj Date 11-OCT-2012 2113 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info LCSMisc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 2 QC Sample BSDil Factor 100000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0894 0900 (0249) 92905 180886 18
3 Chloromethane 50 1016 1016 (0283) 178821 210339 21
4 Vinyl Chloride 62 1022 1028 (0284) 146748 202753 20
6 Bromomethane 94 1181 1181 (0328) 88580 210689 21
5 Chloroethane 64 1236 1242 (0344) 67759 201399 20
7 Trichlorofluoromethane 101 1297 1303 (0361) 148657 190423 19
14 Freon TF 101 1565 1577 (0435) 106548 203057 20
15 11-Dichloroethene 96 1547 1553 (0430) 94737 223085 22
16 Acetone 58 1900 1894 (0529) 14083 249674 25
18 Carbon Disulfide 76 1565 1571 (0435) 377236 218062 22
27 Methyl Acetate 74 1961 1967 (0546) 21873 219755 22
22 Methylene Chloride 49 1858 1864 (0517) 180593 200499 20
28 MTBE 73 2022 2022 (0562) 363998 207251 21
25 trans-12-Dichloroethene 96 1943 1949 (0540) 119022 216004 22
30 11-Dichloroethane 63 2303 2309 (0640) 238759 204130 20
36 cis-12-Dichloroethene 96 2650 2656 (0737) 126688 211021 21
10162012Page 121 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08977d Report Date 11-Oct-2012 2301
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3077 (0854) 20020 214276 21
42 Chloroform 83 2845 2845 (0791) 215227 205163 20
44 Cyclohexane 56 2778 2784 (0773) 186275 208395 21
43 111-Trichloroethane 97 2979 2985 (0829) 195599 210453 21
45 Carbon Tetrachloride 117 2931 2937 (0815) 156464 210644 21
48 Benzene 78 3260 3260 (0469) 500200 211727 21
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 391700 477589 48
49 12-Dichloroethane 62 3412 3418 (0949) 178793 204379 20
52 Fluorobenzene 96 3595 3601 (1000) 1318918 500000
54 Trichloroethene 95 3735 3741 (1039) 127803 211922 21
56 Methyl cyclohexane 83 3723 3729 (1036) 159134 214991 21
57 12-Dichloropropane 63 4192 4199 (1166) 134808 211159 21
68 Bromodichloromethane 83 4272 4272 (1188) 171399 214054 21
67 cis-13-Dichloropropene 75 4906 4912 (0705) 217526 216258 22
70 4-Methyl-2-Pentanone 43 5631 5625 (0810) 134218 214248 21
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1312817 495616 50
66 Toluene 91 5162 5162 (0742) 572353 205343 20
64 trans-13-Dichloropropene 75 5650 5649 (0812) 195539 215018 22
69 112-Trichloroethane 83 5820 5820 (0837) 92220 217218 22
71 Tetrachloroethene 166 5582 5582 (0803) 145712 209847 21
73 2-Hexanone 43 6680 6680 (0961) 96649 200980 20
74 Dibromochloromethane 129 6015 6021 (0865) 132048 217333 22
77 12-Dibromoethane 107 6259 6265 (0900) 113742 214758 21
78 Chlorobenzene-d5 117 6954 6954 (1000) 1146590 500000
79 Chlorobenzene 112 6972 6972 (1003) 392243 206030 21
81 Ethylbenzene 106 7064 7064 (1016) 206211 205716 20
82 m+p-Xylene 106 7277 7277 (1046) 519872 407882 41
84 o-Xylene 106 7856 7862 (1130) 254939 203845 20
85 Styrene 104 7942 7942 (1142) 437977 207191 21
86 Bromoform 173 7911 7911 (1138) 93696 217219 22
88 Isopropylbenzene 105 8344 8350 (1200) 637526 207206 21
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 538047 484974 48
92 1122-Tetrachloroethane 83 9112 9112 (0871) 147339 210261 21
105 13-Dichlorobenzene 146 10325 10331 (0987) 330263 203584 20
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 683882 500000
109 14-Dichlorobenzene 146 10484 10490 (1002) 343961 204369 20
111 12-Dichlorobenzene 146 11148 11148 (1065) 320073 208797 21
112 12-Dibromo-3-chloropropane 75 12234 12234 (1169) 26198 222454 22
114 124-Trichlorobenzene 180 12977 12977 (1240) 189475 219787 22
M 120 12-Dichloroethene (Total) 100 245711 427025 43
M 121 Xylene (Total) 100 774811 611727 61
10162012Page 122 of 323
Data File e08977d
Date 11-OCT-2012 2113
Client ID Instrument VOAMS5i
Sample Info LCS Operator GCMS VOAMS5
10162012Page 123 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2 MS
Matrix e08985dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 5
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0027
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
50 03071-55-6 111-Trichloroethane 103
50 1175-71-8 Dichlorodifluoromethane 865
50 05074-87-3 Chloromethane 102
50 07075-01-4 Vinyl chloride 104
50 09074-83-9 Bromomethane 107
50 2096-12-8 12-Dibromo-3-Chloropropane 121
50 1195-50-1 12-Dichlorobenzene 107
50 07575-69-4 Trichlorofluoromethane 121
50 04575-35-4 11-Dichloroethene 108
50 04578-87-5 12-Dichloropropane 111
50 04076-13-1 112-Trichloro-122-trifluoroethane
102
25 1367-64-1 Acetone 986
50 06575-15-0 Carbon disulfide 113
10 1779-20-9 Methyl acetate 100
50 09075-09-2 Methylene Chloride 106
50 065156-60-5 trans-12-Dichloroethene 106
50 10124-48-1 Chlorodibromomethane 116
50 0701634-04-4 Methyl tert-butyl ether 114
50 08575-00-3 Chloroethane 116
50 06575-34-3 11-Dichloroethane 104
50 090156-59-2 cis-12-Dichloroethene 105
25 1278-93-3 2-Butanone (MEK) 111
50 04067-66-3 Chloroform 108
50 050100-41-4 Ethylbenzene 107
50 080110-82-7 Cyclohexane 108
50 03056-23-5 Carbon tetrachloride 105
50 04071-43-2 Benzene 106
50 095107-06-2 12-Dichloroethane 107
50 04579-01-6 Trichloroethene 107
50 070108-87-2 Methylcyclohexane 115
50 06075-27-4 Dichlorobromomethane 113
50 09010061-01-5 cis-13-Dichloropropene 109
25 50108-10-1 4-Methyl-2-pentanone (MIBK) 111
50 075108-88-3 Toluene 106
50 1210061-02-6 trans-13-Dichloropropene 113
FORM I 8260B
10162012Page 124 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2 MS
Matrix e08985dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 5
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0027
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
50 09579-00-5 112-Trichloroethane 112
50 050127-18-4 Tetrachloroethene 110
25 25591-78-6 2-Hexanone 109
50 14106-93-4 12-Dibromoethane 116
50 055108-90-7 Chlorobenzene 107
15 181330-20-7 Xylenes Total 318
50 060100-42-5 Styrene 107
50 09575-25-2 Bromoform 115
50 04098-82-8 Isopropylbenzene 107
50 08079-34-5 1122-Tetrachloroethane 115
50 070541-73-1 13-Dichlorobenzene 106
50 12106-46-7 14-Dichlorobenzene 106
50 17120-82-1 124-Trichlorobenzene 110
RECCAS NO LIMITSQSURROGATE
96 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
99 70-130460-00-4 4-Bromofluorobenzene
99 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 125 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08985d Report Date 12-Oct-2012 0117
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08985dLab Smp Id 460-45537-C-2 MS Inj Date 12-OCT-2012 0027 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info 460-45537-C-2 MS5Misc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 10 QC Sample MSDil Factor 500000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 500000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0894 0900 (0249) 83204 173010 86
3 Chloromethane 50 1016 1016 (0283) 161645 203059 100
4 Vinyl Chloride 62 1022 1028 (0284) 141501 208792 100
6 Bromomethane 94 1181 1181 (0328) 84568 214819 110
5 Chloroethane 64 1236 1242 (0344) 73104 232055 120
7 Trichlorofluoromethane 101 1297 1303 (0361) 177163 242363 120
14 Freon TF 101 1571 1577 (0437) 100496 204542 100
15 11-Dichloroethene 96 1553 1553 (0432) 86070 216451 110
16 Acetone 58 1894 1894 (0527) 10416 197218 99
18 Carbon Disulfide 76 1565 1571 (0435) 366514 226264 110
27 Methyl Acetate 74 1961 1967 (0546) 18655 200164 100
22 Methylene Chloride 49 1857 1864 (0517) 178536 211689 100
28 MTBE 73 2016 2022 (0561) 376182 228747 110
25 trans-12-Dichloroethene 96 1949 1949 (0542) 109215 211677 100
30 11-Dichloroethane 63 2309 2309 (0642) 226749 207039 100
36 cis-12-Dichloroethene 96 2650 2656 (0737) 118569 210921 100
10162012Page 126 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08985d Report Date 12-Oct-2012 0117
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3077 (0854) 19396 221710 110
42 Chloroform 83 2845 2845 (0791) 213034 216876 110
44 Cyclohexane 56 2784 2784 (0774) 180984 216238 110
43 111-Trichloroethane 97 2979 2985 (0829) 179996 206829 100
45 Carbon Tetrachloride 117 2930 2937 (0815) 145570 209299 100
48 Benzene 78 3260 3260 (0469) 482493 212344 110
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 369860 481613 48
49 12-Dichloroethane 62 3418 3418 (0951) 175178 213858 110
52 Fluorobenzene 96 3595 3601 (1000) 1234975 500000
54 Trichloroethene 95 3741 3741 (1041) 121196 214627 110
56 Methyl cyclohexane 83 3729 3729 (1037) 158792 229110 110
57 12-Dichloropropane 63 4192 4199 (1166) 132380 221450 110
68 Bromodichloromethane 83 4272 4272 (1188) 168703 225007 110
67 cis-13-Dichloropropene 75 4906 4912 (0705) 211819 218949 110
70 4-Methyl-2-Pentanone 43 5625 5625 (0809) 133223 221106 110
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1260222 494657 49
66 Toluene 91 5162 5162 (0742) 566751 211409 100
64 trans-13-Dichloropropene 75 5649 5649 (0812) 197737 226072 110
69 112-Trichloroethane 83 5820 5820 (0837) 91872 224994 110
71 Tetrachloroethene 166 5582 5582 (0803) 147320 220590 110
73 2-Hexanone 43 6674 6680 (0960) 100809 217957 110
74 Dibromochloromethane 129 6015 6021 (0865) 135240 231427 120
77 12-Dibromoethane 107 6259 6265 (0900) 117784 231222 120
78 Chlorobenzene-d5 117 6954 6954 (1000) 1102789 500000
79 Chlorobenzene 112 6972 6972 (1003) 391979 214069 110
81 Ethylbenzene 106 7064 7064 (1016) 207079 214786 110
82 m+p-Xylene 106 7277 7277 (1046) 521861 425705 210
84 o-Xylene 106 7856 7862 (1130) 254032 211187 100
85 Styrene 104 7942 7942 (1142) 433507 213222 110
86 Bromoform 173 7911 7911 (1138) 95433 230033 120
88 Isopropylbenzene 105 8350 8350 (1201) 635772 214844 110
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 518047 497030 50
92 1122-Tetrachloroethane 83 9112 9112 (0871) 151817 230609 120
105 13-Dichlorobenzene 146 10325 10331 (0987) 322106 211348 100
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 642491 500000
109 14-Dichlorobenzene 146 10490 10490 (1002) 334190 211356 100
111 12-Dichlorobenzene 146 11148 11148 (1065) 308704 214355 110
112 12-Dibromo-3-chloropropane 75 12233 12234 (1169) 26873 242889 120(R)
114 124-Trichlorobenzene 180 12977 12977 (1240) 177853 219597 110
M 120 12-Dichloroethene (Total) 100 227784 422599 210
M 121 Xylene (Total) 100 775893 636892 320
QC Flag Legend
R - SpikeSurrogate failed recovery limits
10162012Page 127 of 323
Data File e08985d
Date 12-OCT-2012 0027
Client ID Instrument VOAMS5i
Sample Info 460-45537-C-2 MS5 Operator GCMS VOAMS5
10162012Page 128 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2 MSD
Matrix e08986dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 5
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0051
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
50 03071-55-6 111-Trichloroethane 106
50 1175-71-8 Dichlorodifluoromethane 896
50 05074-87-3 Chloromethane 101
50 07075-01-4 Vinyl chloride 105
50 09074-83-9 Bromomethane 105
50 2096-12-8 12-Dibromo-3-Chloropropane 121
50 1195-50-1 12-Dichlorobenzene 111
50 07575-69-4 Trichlorofluoromethane 997
50 04575-35-4 11-Dichloroethene 119
50 04578-87-5 12-Dichloropropane 110
50 04076-13-1 112-Trichloro-122-trifluoroethane
111
25 1367-64-1 Acetone 101
50 06575-15-0 Carbon disulfide 119
10 1779-20-9 Methyl acetate 101
50 09075-09-2 Methylene Chloride 106
50 065156-60-5 trans-12-Dichloroethene 108
50 10124-48-1 Chlorodibromomethane 118
50 0701634-04-4 Methyl tert-butyl ether 116
50 08575-00-3 Chloroethane 105
50 06575-34-3 11-Dichloroethane 111
50 090156-59-2 cis-12-Dichloroethene 109
25 1278-93-3 2-Butanone (MEK) 114
50 04067-66-3 Chloroform 113
50 050100-41-4 Ethylbenzene 111
50 080110-82-7 Cyclohexane 117
50 03056-23-5 Carbon tetrachloride 110
50 04071-43-2 Benzene 114
50 095107-06-2 12-Dichloroethane 109
50 04579-01-6 Trichloroethene 113
50 070108-87-2 Methylcyclohexane 121
50 06075-27-4 Dichlorobromomethane 116
50 09010061-01-5 cis-13-Dichloropropene 115
25 50108-10-1 4-Methyl-2-pentanone (MIBK) 114
50 075108-88-3 Toluene 111
50 1210061-02-6 trans-13-Dichloropropene 119
FORM I 8260B
10162012Page 129 of 323
FORM IForm 1GCMS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2 MSD
Matrix e08986dLab File ID
Date Collected8260BAnalysis Method
Water
TestAmerica Edison
10052012 1230
Sample wtvol
Moisture
GC ColumnSoil Extract Vol
Dilution FactorSoil Aliquot Vol 5
Level (lowmed) Low
5(mL)
018(mm)
Date Analyzed 10122012 0051
IDRtx-VMS
Analysis Batch No 131656 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
50 09579-00-5 112-Trichloroethane 116
50 050127-18-4 Tetrachloroethene 116
25 25591-78-6 2-Hexanone 111
50 14106-93-4 12-Dibromoethane 117
50 055108-90-7 Chlorobenzene 111
15 181330-20-7 Xylenes Total 329
50 060100-42-5 Styrene 110
50 09575-25-2 Bromoform 114
50 04098-82-8 Isopropylbenzene 111
50 08079-34-5 1122-Tetrachloroethane 116
50 070541-73-1 13-Dichlorobenzene 110
50 12106-46-7 14-Dichlorobenzene 110
50 17120-82-1 124-Trichlorobenzene 119
RECCAS NO LIMITSQSURROGATE
96 70-13017060-07-0 12-Dichloroethane-d4 (Surr)
97 70-130460-00-4 4-Bromofluorobenzene
99 70-1302037-26-5 Toluene-d8 (Surr)
FORM I 8260B
10162012Page 130 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08986d Report Date 12-Oct-2012 0118
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file chemVOAMS5i8260DE09-17-1211oct12be08986dLab Smp Id 460-45537-C-2 MSD Inj Date 12-OCT-2012 0051 Operator GCMS VOAMS5 Inst ID VOAMS5iSmp Info 460-45537-C-2 MSD5Misc Info Comment Method chemVOAMS5i8260DE09-17-1211oct12b8260DE_09mMeth Date 11-Oct-2012 2130 ken Quant Type ISTDCal Date 11-OCT-2012 2050 Cal File e08976dAls bottle 11 QC Sample MSDDil Factor 500000 Integrator HP RTE Compound Sublist HSLDELsubTarget Version 350 Processing Host hpd2
Concentration Formula Amt DF 5Vo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 500000 Dilution FactorVo 500000 Sample Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
2 Dichlorodifluoromethane 85 0894 0900 (0249) 90471 179208 90
3 Chloromethane 50 1016 1016 (0283) 169425 202751 100
4 Vinyl Chloride 62 1022 1028 (0284) 149176 209689 100
6 Bromomethane 94 1181 1181 (0328) 86595 209548 100
5 Chloroethane 64 1236 1242 (0344) 69668 210673 100
7 Trichlorofluoromethane 101 1297 1303 (0361) 152935 199307 100
14 Freon TF 101 1565 1577 (0435) 114134 221294 110
15 11-Dichloroethene 96 1547 1553 (0430) 98966 237094 120
16 Acetone 58 1900 1894 (0529) 11165 201386 100
18 Carbon Disulfide 76 1565 1571 (0435) 405349 238385 120
27 Methyl Acetate 74 1961 1967 (0546) 19684 201192 100
22 Methylene Chloride 49 1858 1864 (0517) 187993 212342 110
28 MTBE 73 2022 2022 (0562) 399850 231621 120(R)
25 trans-12-Dichloroethene 96 1943 1949 (0540) 117162 216323 110
30 11-Dichloroethane 63 2309 2309 (0642) 255983 222660 110
36 cis-12-Dichloroethene 96 2650 2656 (0737) 129220 218978 110
10162012Page 131 of 323
Data File chemVOAMS5i8260DE09-17-1211oct12be08986d Report Date 12-Oct-2012 0118
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ugL) ( ugL)
========================== ==== == ====== ====== ======== ======= =======
38 2-Butanone 72 3071 3077 (0854) 20938 227991 110
42 Chloroform 83 2845 2845 (0791) 233404 226357 110
44 Cyclohexane 56 2778 2784 (0773) 204751 233046 120
43 111-Trichloroethane 97 2979 2985 (0829) 194508 212915 110
45 Carbon Tetrachloride 117 2931 2937 (0815) 161111 220670 110
48 Benzene 78 3260 3260 (0469) 525066 227601 110
$ 47 12-Dichloroethane-d4 (SUR) 65 3363 3363 (0936) 386156 479012 48
49 12-Dichloroethane 62 3412 3418 (0949) 188223 218898 110
52 Fluorobenzene 96 3595 3601 (1000) 1296388 500000
54 Trichloroethene 95 3741 3741 (1041) 133629 225434 110
56 Methyl cyclohexane 83 3723 3729 (1036) 175741 241553 120
57 12-Dichloropropane 63 4192 4199 (1166) 138376 220515 110
68 Bromodichloromethane 83 4272 4272 (1188) 182026 231276 120
67 cis-13-Dichloropropene 75 4906 4912 (0705) 226245 230339 120
70 4-Methyl-2-Pentanone 43 5625 5625 (0809) 139423 227913 110
$ 65 Toluene-d8 (SUR) 98 5107 5107 (0734) 1279885 494812 49
66 Toluene 91 5162 5162 (0742) 602122 221221 110
64 trans-13-Dichloropropene 75 5650 5649 (0812) 211878 238592 120(R)
69 112-Trichloroethane 83 5820 5820 (0837) 95786 231047 120
71 Tetrachloroethene 166 5582 5582 (0803) 157152 231769 120
73 2-Hexanone 43 6680 6680 (0961) 103997 221464 110
74 Dibromochloromethane 129 6015 6021 (0865) 140562 236912 120
77 12-Dibromoethane 107 6259 6265 (0900) 120913 233791 120
78 Chlorobenzene-d5 117 6954 6954 (1000) 1119645 500000
79 Chlorobenzene 112 6972 6972 (1003) 411739 221475 110
81 Ethylbenzene 106 7064 7064 (1016) 216984 221672 110
82 m+p-Xylene 106 7277 7277 (1046) 549474 441482 220
84 o-Xylene 106 7856 7862 (1130) 265488 217389 110
85 Styrene 104 7942 7942 (1142) 452927 219420 110
86 Bromoform 173 7911 7911 (1138) 96039 228008 110
88 Isopropylbenzene 105 8344 8350 (1200) 668990 222665 110
$ 89 Bromofluorobenzene (SUR) 174 8710 8710 (0832) 517679 487311 49
92 1122-Tetrachloroethane 83 9112 9112 (0871) 155509 231763 120
105 13-Dichlorobenzene 146 10325 10331 (0987) 342279 220349 110
108 14-Dichlorobenzene-d4 152 10466 10466 (1000) 654839 500000
109 14-Dichlorobenzene 146 10490 10490 (1002) 355256 220442 110
111 12-Dichlorobenzene 146 11148 11148 (1065) 324646 221173 110
112 12-Dibromo-3-chloropropane 75 12234 12234 (1169) 27355 242581 120(R)
114 124-Trichlorobenzene 180 12977 12977 (1240) 196651 238228 120
M 120 12-Dichloroethene (Total) 100 246382 435302 220
M 121 Xylene (Total) 100 814963 658871 330
QC Flag Legend
R - SpikeSurrogate failed recovery limits
10162012Page 132 of 323
Data File e08986d
Date 12-OCT-2012 0051
Client ID Instrument VOAMS5i
Sample Info 460-45537-C-2 MSD5 Operator GCMS VOAMS5
10162012Page 133 of 323
Lab Name Job No
SDG No
Instrument ID
Analysis Batch Number
GCMS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-45537-1
VOAMS5
128076
Start Date
End Date 09172012 1616
09172012 0324
BFB 460-1280761 Rtx-VMS 018(mm)109172012 0324 e07834d
IC 460-1280762 Rtx-VMS 018(mm)109172012 0449 e07836d
IC 460-1280763 Rtx-VMS 018(mm)109172012 0536 e07838d
ICIS 460-1280764 Rtx-VMS 018(mm)109172012 0600 e07839d
IC 460-1280765 Rtx-VMS 018(mm)109172012 0623 e07840d
IC 460-1280766 Rtx-VMS 018(mm)109172012 0646 e07841d
IC 460-1280767 Rtx-VMS 018(mm)109172012 0710 e07842d
ZZZZZ Rtx-VMS 018(mm)109172012 0937
ZZZZZ Rtx-VMS 018(mm)109172012 1047
ZZZZZ Rtx-VMS 018(mm)109172012 1111
ZZZZZ Rtx-VMS 018(mm)109172012 1134
ZZZZZ Rtx-VMS 018(mm)109172012 1157
ZZZZZ Rtx-VMS 018(mm)509172012 1221
ZZZZZ Rtx-VMS 018(mm)509172012 1244
ZZZZZ Rtx-VMS 018(mm)109172012 1307
ZZZZZ Rtx-VMS 018(mm)109172012 1331
ZZZZZ Rtx-VMS 018(mm)109172012 1354
ZZZZZ Rtx-VMS 018(mm)109172012 1417
ZZZZZ Rtx-VMS 018(mm)109172012 1441
CCV 460-12807620 Rtx-VMS 018(mm)109172012 1616
8260B
10162012Page 134 of 323
Lab Name Job No
SDG No
Instrument ID
Analysis Batch Number
GCMS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-45537-1
VOAMS5
131656
Start Date
End Date 10122012 0114
10112012 2008
BFB 460-1316561 Rtx-VMS 018(mm)110112012 2008 e08975d
CCVIS 460-1316562 Rtx-VMS 018(mm)110112012 2050 e08976d
LCS 460-1316563 Rtx-VMS 018(mm)110112012 2113 e08977d
MB 460-1316564 Rtx-VMS 018(mm)110112012 2247 e08981d
460-45537-3 TB-17338-100512-253 Rtx-VMS 018(mm)110112012 2317 e08982d
460-45537-1 WC-17338-100512-MW14-MM-251
Rtx-VMS 018(mm)110112012 2341 e08983d
460-45537-2 WC-17338-100512-MW101-MM-252
Rtx-VMS 018(mm)110122012 0004 e08984d
460-45537-2 MS WC-17338-100512-MW101-MM-252 MS
Rtx-VMS 018(mm)510122012 0027 e08985d
460-45537-2 MSD WC-17338-100512-MW101-MM-252 MSD
Rtx-VMS 018(mm)510122012 0051 e08986d
CCV 460-13165610 Rtx-VMS 018(mm)110122012 0114 e08987d
8260B
10162012Page 135 of 323
10162012Page 136 of 323
10162012Page 137 of 323
10162012Page 138 of 323
10162012Page 139 of 323
Method 8082 -
DelawarePolychlorinated Biphenyls (PCBs)
(GC) by Method 8082 (Delaware)
10162012Page 140 of 323
FORM II
GC SEMI VOA SURROGATE RECOVERY
Lab Name Job No 460-45537-1
SDG No
Matrix Water Level Low
TestAmerica Edison
GC Column (1) ID (mm) GC Column (2) ID (mm)CLP-1 053 CLP-2 053
Lab Sample IDClient Sample ID DCB1 DCB2
460-45537-1WC-17338-100512-MW14-MM-251
82 83
460-45537-2WC-17338-100512-MW101-MM-252
52 50
MB 460-1309971-A
97 88
LCS 460-1309972-A
91 84
LCSD 460-1309973-A
108 99
QC LIMITSQC LIMITSDCB = DCB Decachlorobiphenyl 37-150
FORM II 8082
Column to be used to flag recovery values
10162012Page 141 of 323
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID vf479497dWater
Lab ID LCS 460-1309972-A Client ID
TestAmerica Edison
REC
REC
QC
LIMITSCONCENTRATION
(ugL)
SPIKE
ADDED
(ugL)
LCS LCS
COMPOUND
PCB-1016 500 507 71-126101
PCB-1260 500 557 73-130111
FORM III 8082
Column to be used to flag recovery and RPD values
10162012Page 142 of 323
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID vr479497dWater
Lab ID LCS 460-1309972-A Client ID
TestAmerica Edison
REC
REC
QC
LIMITSCONCENTRATION
(ugL)
SPIKE
ADDED
(ugL)
LCS LCS
COMPOUND
PCB-1016 500 483 71-12697
PCB-1260 500 573 73-130115
FORM III 8082
Column to be used to flag recovery and RPD values
10162012Page 143 of 323
GC SEMI VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID vf479498dWater
Lab ID LCSD 460-1309973-A Client ID
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION
REC
RPD
QC LIMITS
RPD REC (ugL) (ugL)
LCSD LCSD
500 516 30 71-126PCB-1016 2103
500 583 30 73-130PCB-1260 5117
FORM III 8082
Column to be used to flag recovery and RPD values
10162012Page 144 of 323
GC SEMI VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job NoLab Name
SDG No
LevelMatrixMatrix
Low
460-45537-1
Lab File ID vr479498dWater
Lab ID LCSD 460-1309973-A Client ID
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION
REC
RPD
QC LIMITS
RPD REC (ugL) (ugL)
LCSD LCSD
500 497 30 71-126PCB-1016 399
500 595 30 73-130PCB-1260 4119
FORM III 8082
Column to be used to flag recovery and RPD values
10162012Page 145 of 323
FORM IV
GC SEMI VOA METHOD BLANK SUMMARY
Lab Name
SDG No
Job No 460-45537-1TestAmerica Edison
Date Analyzed(1)
Instrument ID(1)
GC Column(1) ID
Instrument ID(2)
Date Extracted 10082012 0755
Date Analyzed(2)
GC Column(2) IDCLP-2053(mm) 053(mm)
PESTGC9
10082012 2208
Lab File ID(1) Lab File ID(2)
Matrix Water
vf479496d
Lab Sample ID MB 460-1309971-A
vr479496d
10082012 2208
PESTGC9
CLP-1
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES
ANALYZED 2
DATEDATE
ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID
LCS 460-1309972-A 10082012 2224 10082012 2224
LCSD 460-1309973-A 10082012 2239 10082012 2239
460-45537-1WC-17338-100512-MW14-MM-251
10092012 0029 10092012 0029
460-45537-2WC-17338-100512-MW101-MM-252
10092012 0045 10092012 0045
FORM IV 8082
10162012Page 146 of 323
GC SEMI VOA ANALYTICAL SEQUENCE
Lab Name Job No
SDG No
FORM VIII
TestAmerica Edison 460-45537-1
Sample No CCVRT 460-1311372 Date Analyzed 10082012 1830
Lab File ID (Standard) vf479493d
Instrument ID PESTGC9 GC Column CLP-2 ID 053(mm)
Heated Purge (YN) N
Calibration ID 17840
THE ANALYTICAL SEQUENCE OF BLANKS SAMPLES STANDARDS MSMSDs AND LCSs IS GIVEN BELOW
RT
DCB
UPPER LIMIT
LOWER LIMIT
1159
1139
CONTINUING CALIBRATION SURROGATE 1149
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-1311372 10082012 1830 1149vf479493d
MB 460-1309971-A 10082012 2208 1148vf479496d
LCS 460-1309972-A 10082012 2224 1148vf479497d
LCSD 460-1309973-A 10082012 2239 1148vf479498d
460-45537-1 10092012 0029 1149WC-17338-100512-MW14-MM-251
vf479505d
460-45537-2 10092012 0045 1149WC-17338-100512-MW101-MM-252
vf479506d
PIBLK 460-13113718 10092012 0131 1149vf479509d
CCV 460-13113719 10092012 0147 1149vf479510d
DCB = DCB Decachlorobiphenyl
DCB RT Limit = plusmn 01 minutes of surrogate RT
Column used to flag values outside QC limits
FORM VIII 8082
10162012Page 147 of 323
GC SEMI VOA ANALYTICAL SEQUENCE
Lab Name Job No
SDG No
FORM VIII
TestAmerica Edison 460-45537-1
Sample No CCVRT 460-1311372 Date Analyzed 10082012 1830
Lab File ID (Standard) vr479493d
Instrument ID PESTGC9 GC Column CLP-1 ID 053(mm)
Heated Purge (YN) N
Calibration ID 17839
THE ANALYTICAL SEQUENCE OF BLANKS SAMPLES STANDARDS MSMSDs AND LCSs IS GIVEN BELOW
RT
DCB
UPPER LIMIT
LOWER LIMIT
1071
1051
CONTINUING CALIBRATION SURROGATE 1061
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-1311372 10082012 1830 1061vr479493d
MB 460-1309971-A 10082012 2208 1061vr479496d
LCS 460-1309972-A 10082012 2224 1061vr479497d
LCSD 460-1309973-A 10082012 2239 1061vr479498d
460-45537-1 10092012 0029 1061WC-17338-100512-MW14-MM-251
vr479505d
460-45537-2 10092012 0045 1061WC-17338-100512-MW101-MM-252
vr479506d
PIBLK 460-13113718 10092012 0131 1061vr479509d
CCV 460-13113719 10092012 0147 1061vr479510d
DCB = DCB Decachlorobiphenyl
DCB RT Limit = plusmn 01 minutes of surrogate RT
Column used to flag values outside QC limits
FORM VIII 8082
10162012Page 148 of 323
FORM XForm 1
Client Sample ID
Lab Name Job No
SDG No
Lab Sample ID LCS 460-1309972-A
Instrument ID (1) Instrument ID (2)
Date Analyzed (1) Date Analyzed (2)
GC Column (1) ID GC Column (2) ID
TestAmerica Edison 460-45537-1
IDENTIFICATION SUMMARYForm 1
053(mm) 053(mm)
10082012 2224 10082012 2224
PESTGC9 PESTGC9
CLP-1 CLP-2
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEAN
CONCENTRATIONRPD
PCB-1016 1 1 206 201 215 473 483 47
2 250 246 260 494
3 275 271 285 530
4 310 306 320 501
5 330 326 340 520
6 369 361 375 302
7 401 397 411 541
8 419 412 426 505
2 1 293 289 303 525 507
2 360 357 371 562
3 404 401 415 567
4 444 441 455 558
5 468 465 479 594
6 518 509 523 402
7 557 547 561 259
8 571 568 582 584
PCB-1260 1 1 605 600 614 554 573 28
2 650 645 659 558
3 694 689 703 581
4 714 709 723 548
5 758 753 767 565
6 886 882 896 559
7 908 904 918 619
8 1014 1008 1022 600
2 1 771 769 783 600 557
2 817 814 828 594
3 903 901 915 625
4 928 926 940 622
5 941 938 952 643
6 986 983 997 612
7 1062 1055 1069 212
8 1106 1102 1116 550
FORM X 8082
10162012Page 149 of 323
FORM XForm 1
Client Sample ID
Lab Name Job No
SDG No
Lab Sample ID LCSD 460-1309973-A
Instrument ID (1) Instrument ID (2)
Date Analyzed (1) Date Analyzed (2)
GC Column (1) ID GC Column (2) ID
TestAmerica Edison 460-45537-1
IDENTIFICATION SUMMARYForm 1
053(mm) 053(mm)
10082012 2239 10082012 2239
PESTGC9 PESTGC9
CLP-1 CLP-2
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEAN
CONCENTRATIONRPD
PCB-1016 1 1 206 201 215 483 497 38
2 250 246 260 505
3 275 271 285 542
4 310 306 320 510
5 330 326 340 529
6 368 361 375 369
7 401 397 411 549
8 419 412 426 491
2 1 292 289 303 535 516
2 359 357 371 574
3 404 401 415 572
4 443 441 455 572
5 468 465 479 606
6 518 509 523 407
7 557 547 561 267
8 571 568 582 599
PCB-1260 1 1 605 600 614 565 595 19
2 650 645 659 571
3 694 689 703 595
4 714 709 723 563
5 757 753 767 585
6 886 882 896 582
7 908 904 918 656
8 1014 1008 1022 639
2 1 771 769 783 615 583
2 816 814 828 610
3 902 901 915 645
4 928 926 940 648
5 940 938 952 669
6 986 983 997 637
7 1062 1055 1069 253
8 1106 1102 1116 590
FORM X 8082
10162012Page 150 of 323
FORM IForm 1GC SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW14-MM-2
SDG No
460-45537-1
Lab Sample ID 460-45537-1
Matrix vf479505dLab File ID
Date Collected8082Analysis Method
Water
TestAmerica Edison
10052012 1000
Con Extract VolVolumeInjection Volume
GPC Cleanup(YN)
Date Extracted
Date Analyzed
Dilution Factor 1
Extraction Method 3510C 10082012 0755
10092012 0029
5(mL)
Sample wtvol 980(mL)
Moisture
GC Column ID 053(mm)CLP-2
N
Analysis Batch No 131137 ugLUnits
RECCAS NO LIMITSQSURROGATE
83 37-1502051-24-3 DCB Decachlorobiphenyl
FORM I 8082
10162012Page 151 of 323
Data File vf479505d Report Date 09-Oct-2012 0313
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontoct1210-08-1208oct12bbvf479505dLab Smp Id 460-45537-E-1-B Client Smp ID WC-17338-100512-MW1Inj Date 09-OCT-2012 0029 Operator Inst ID PESTGC9iSmp Info 460-45537-E-1-BMisc Info 460-45537-E-1-BComment Method chem1PESTGC9i8082frontoct1210-08-1208oct12bb08Vf8082mMeth Date 01-Oct-2012 0847 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 35 Dil Factor 100000 Integrator Falcon Compound Sublist AllPCBsubTarget Version 350 Sample Matrix WATERProcessing Host hpd3
Concentration Formula Amt DF VtVo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 500000 Volume of final extract (mL)Vo 98000000 Volume of sample extracted (mL)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11489 11515 -0026 22061081 829479 042 8000- 12000 10000
-------------------------------------------------------------------------------
10162012Page 152 of 323
Data File vf479505d
Date 09-OCT-2012 0029
Client ID WC-17338-100512-MW1 Instrument PESTGC9i
Sample Info 460-45537-E-1-B Operator
10162012Page 153 of 323
FORM IForm 1GC SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW14-MM-2
SDG No
460-45537-1
Lab Sample ID 460-45537-1
Matrix vr479505dLab File ID
Date Collected8082Analysis Method
Water
TestAmerica Edison
10052012 1000
Con Extract VolVolumeInjection Volume
GPC Cleanup(YN)
Date Extracted
Date Analyzed
Dilution Factor 1
Extraction Method 3510C 10082012 0755
10092012 0029
5(mL)
Sample wtvol 980(mL)
Moisture
GC Column ID 053(mm)CLP-1
N
Analysis Batch No 131137 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
051 013U12674-11-2 PCB-1016 013
051 029U11104-28-2 PCB-1221 029
051 012U11141-16-5 PCB-1232 012
051 012U53469-21-9 PCB-1242 012
051 024U12672-29-6 PCB-1248 024
051 017U11097-69-1 PCB-1254 017
051 015U11096-82-5 PCB-1260 015
RECCAS NO LIMITSQSURROGATE
82 37-1502051-24-3 DCB Decachlorobiphenyl
FORM I 8082
10162012Page 154 of 323
Data File vr479505d Report Date 09-Oct-2012 0303
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearoct1210-08-1208oct12bbvr479505dLab Smp Id 460-45537-E-1-B Client Smp ID WC-17338-100512-MW1Inj Date 09-OCT-2012 0029 Operator Inst ID PESTGC9iSmp Info 460-45537-E-1-BMisc Info 460-45537-E-1-BComment Method chem1PESTGC9i8082rearoct1210-08-1208oct12bb08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 35 Dil Factor 100000 Integrator Falcon Compound Sublist AllPCBsubTarget Version 350 Sample Matrix WATERProcessing Host hpd3
Concentration Formula Amt DF VtVo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 500000 Volume of final extract (mL)Vo 98000000 Volume of sample extracted (mL)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10611 10624 -0013 38407031 815954 042 8000- 12000 10000
-------------------------------------------------------------------------------
10162012Page 155 of 323
Data File vr479505d
Date 09-OCT-2012 0029
Client ID WC-17338-100512-MW1 Instrument PESTGC9i
Sample Info 460-45537-E-1-B Operator
10162012Page 156 of 323
FORM IForm 1GC SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2
Matrix vf479506dLab File ID
Date Collected8082Analysis Method
Water
TestAmerica Edison
10052012 1230
Con Extract VolVolumeInjection Volume
GPC Cleanup(YN)
Date Extracted
Date Analyzed
Dilution Factor 1
Extraction Method 3510C 10082012 0755
10092012 0045
5(mL)
Sample wtvol 990(mL)
Moisture
GC Column ID 053(mm)CLP-2
N
Analysis Batch No 131137 ugLUnits
RECCAS NO LIMITSQSURROGATE
50 37-1502051-24-3 DCB Decachlorobiphenyl
FORM I 8082
10162012Page 157 of 323
Data File vf479506d Report Date 09-Oct-2012 0322
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontoct1210-08-1208oct12bbvf479506dLab Smp Id 460-45537-E-2-A Client Smp ID WC-17338-100512-MW1Inj Date 09-OCT-2012 0045 Operator Inst ID PESTGC9iSmp Info 460-45537-E-2-AMisc Info 460-45537-E-2-AComment Method chem1PESTGC9i8082frontoct1210-08-1208oct12bb08Vf8082mMeth Date 01-Oct-2012 0847 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 36 Dil Factor 100000 Integrator Falcon Compound Sublist AllPCBsubTarget Version 350 Sample Matrix WATERProcessing Host hpd3
Concentration Formula Amt DF VtVo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 500000 Volume of final extract (mL)Vo 99000000 Volume of sample extracted (mL)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11487 11515 -0028 13346591 501821 025 8000- 12000 10000
-------------------------------------------------------------------------------
10162012Page 158 of 323
Data File vf479506d
Date 09-OCT-2012 0045
Client ID WC-17338-100512-MW1 Instrument PESTGC9i
Sample Info 460-45537-E-2-A Operator
10162012Page 159 of 323
FORM IForm 1GC SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID
Lab Name Job No
WC-17338-100512-MW101-MM-
SDG No
460-45537-1
Lab Sample ID 460-45537-2
Matrix vr479506dLab File ID
Date Collected8082Analysis Method
Water
TestAmerica Edison
10052012 1230
Con Extract VolVolumeInjection Volume
GPC Cleanup(YN)
Date Extracted
Date Analyzed
Dilution Factor 1
Extraction Method 3510C 10082012 0755
10092012 0045
5(mL)
Sample wtvol 990(mL)
Moisture
GC Column ID 053(mm)CLP-1
N
Analysis Batch No 131137 ugLUnits
CAS NO COMPOUND NAME RESULT Q MDLRL
051 013U12674-11-2 PCB-1016 013
051 028U11104-28-2 PCB-1221 028
051 012U11141-16-5 PCB-1232 012
051 012U53469-21-9 PCB-1242 012
051 024U12672-29-6 PCB-1248 024
051 017U11097-69-1 PCB-1254 017
051 015U11096-82-5 PCB-1260 015
RECCAS NO LIMITSQSURROGATE
52 37-1502051-24-3 DCB Decachlorobiphenyl
FORM I 8082
10162012Page 160 of 323
Data File vr479506d Page 1 Report Date 09-Oct-2012 0322
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearoct1210-08-1208oct12bbvr479506dLab Smp Id 460-45537-E-2-A Client Smp ID WC-17338-100512-MW1Inj Date 09-OCT-2012 0045 Operator Inst ID PESTGC9iSmp Info 460-45537-E-2-AMisc Info 460-45537-E-2-AComment Method chem1PESTGC9i8082rearoct1210-08-1208oct12bb08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 36 Dil Factor 100000 Integrator Falcon Compound Sublist AllPCBsubTarget Version 350 Sample Matrix WATERProcessing Host hpd3
Concentration Formula Amt DF VtVo CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 500000 Volume of final extract (mL)Vo 99000000 Volume of sample extracted (mL)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10611 10624 -0013 24675227 524223 026 8000- 12000 10000
-------------------------------------------------------------------------------
10162012Page 161 of 323
Data File vr479506d
Date 09-OCT-2012 0045
Client ID WC-17338-100512-MW1 Instrument PESTGC9i
Sample Info 460-45537-E-2-A Operator
10162012Page 162 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17840Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-1299267 vf479200dLevel 2 IC 460-1299268 vf479201dLevel 3 IC 460-1299269 vf479202dLevel 4 IC 460-12992610 vf479203dLevel 5 IC 460-12992611 vf479204d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
PCB-1016 Peak 1 29602891 - 30312960 2960 2961 2959 2959PCB-1016 Peak 2 36403571 - 37113640 3640 3641 3639 3640PCB-1016 Peak 3 40844015 - 41554084 4084 4085 4083 4083PCB-1016 Peak 4 44774409 - 45494477 4477 4479 4477 4476PCB-1016 Peak 5 47224652 - 47924722 4722 4722 4722 4722PCB-1016 Peak 6 51575088 - 52285157 5158 5158 5157 5157PCB-1016 Peak 7 55425472 - 56125542 5543 5542 5542 5542PCB-1016 Peak 8 57515682 - 58225751 5751 5752 5751 5751PCB-1260 Peak 1 77567686 - 78267756 7756 7756 7756 7755PCB-1260 Peak 2 82158145 - 82858216 8215 8215 8215 8215PCB-1260 Peak 3 90839014 - 91549084 9084 9084 9083 9082PCB-1260 Peak 4 93329262 - 94029332 9332 9332 9332 9331PCB-1260 Peak 5 94549384 - 95249454 9454 9454 9454 9453PCB-1260 Peak 6 99019831 - 99719901 9901 9901 9901 9901PCB-1260 Peak 7 1061710546 - 1068610617 10617 10616 10617 10616PCB-1260 Peak 8 1108611016 - 1115611087 11087 11086 11084 11085DCB Decachlorobiphenyl 1151511415 - 1161511518 11520 11515 11510 11512
FORM VI 8082 10162012Page 163 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17840Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-1299267 vf479200d2Level IC 460-1299268 vf479201d3Level IC 460-1299269 vf479202d4Level IC 460-12992610 vf479203d5Level IC 460-12992611 vf479204d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
LVL 5
PCB-1016 Peak 1 Ave 155 20012858 10484 96475 9762186122
102726535
PCB-1016 Peak 2 Ave 122 20025248 21181 20808 2014318185
211130015
PCB-1016 Peak 3 Ave 124 20010359 90007 83526 8441074163
871400841
PCB-1016 Peak 4 Ave 130 20045579 38951 35291 3591632814
377100165
PCB-1016 Peak 5 Ave 129 20019485 17677 14821 1595214340
164548979
PCB-1016 Peak 6 Ave 171 20012410 10306 89543 9039281426
977025128
PCB-1016 Peak 7 Ave 161 20015097 12427 11165 1121510046
119900052
PCB-1016 Peak 8 Ave 121 20014456 12522 11609 1161310532
121463746
PCB-1260 Peak 1 Ave 165 20028165 22320 20852 2059718598
221063931
PCB-1260 Peak 2 Ave 173 20032398 25230 23518 2315121164
250922627
PCB-1260 Peak 3 Ave 101 20042792 37584 35706 3549332757
368665853
PCB-1260 Peak 4 Ave 114 20019125 16727 15681 1547514194
162405856
PCB-1260 Peak 5 Ave 71 20097407 90339 86445 8609680436
881445133
PCB-1260 Peak 6 Ave 116 20020218 16837 16387 1620514980
169255417
PCB-1260 Peak 7 Ave 115 20025044 20516 20530 2080218426
210635761
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 164 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17840Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
LVL 5
PCB-1260 Peak 8 Ave 114 20092729 80982 75320 7482969000
785718832
DCB Decachlorobiphenyl Ave 104 200306013 281530 257456 246481238335
265963086
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 165 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17840Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
GC Column CLP-2 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-1299267 vf479200dLevel 2 IC 460-1299268 vf479201dLevel 3 IC 460-1299269 vf479202dLevel 4 IC 460-12992610 vf479203dLevel 5 IC 460-12992611 vf479204d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
PCB-1016 Peak 1 Ave 1285777 5241842 9647477 14643185 21530533 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 2524804 10590544 20808307 30213965 45462323 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 1035943 4500373 8352607 12661468 18540701 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 4557926 19475271 35290615 53874092 82034010 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 1948484 8838480 14821328 23927783 35848765 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 1240957 5152808 8954270 13558761 20356566 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 1509707 6213265 11165134 16822458 25115800 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 1445572 6260864 11609452 17418946 26330856 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 2816529 11159859 20851674 30895442 46495806 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 3239811 12615093 23518487 34726449 52908911 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 4279245 18792136 35705636 53240044 81893015 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 1912505 8363664 15681452 23213228 35484032 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 974074 4516956 8644462 12914338 20108960 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 2021814 8418625 16386843 24307809 37450674 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 2504445 10257895 20530020 31202581 46064749 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 927285 4049088 7531982 11224374 17250044 100 500 1000 1500 2500DCB Decachlorobiphenyl Ave 7650320 14076513 25745578 36972164 47667099 250 500 100 150 200
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 166 of 323
Data File vf479200d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479200dLab Smp Id IC-SG1660L1_00013 Inj Date 30-SEP-2012 1704 Operator Inst ID PESTGC9iSmp Info ic-SG1660L1_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1704 Cal File vf479200dAls bottle 7 Calibration Sample Level 1Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2960 2961 -0001 1285777 100000 120 8000- 12000 10000
3640 3641 -0001 2524804 100000 120 15709- 23564 19636
4084 4085 -0001 1035943 100000 120 6446- 9668 8057
4477 4479 -0002 4557926 100000 120 28359- 42539 35449
4722 4722 0000 1948484 100000 120 12123- 18185 15154
5157 5158 -0001 1240957 100000 130 7721- 11582 9651
5542 5542 0000 1509707 100000 120 9393- 14090 11742
5751 5752 -0001 1445572 100000 120 8994- 13491 11243
Average of Peak Amounts = 122
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
7756 7756 0000 2816529 100000 130 8000- 12000 10000(M)
10162012Page 167 of 323
Data File vf479200d Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
8216 8215 0001 3239811 100000 130 9202- 13803 11503
9084 9084 0000 4279245 100000 120 12155- 18232 15193
9332 9332 0000 1912505 100000 120 5432- 8148 6790
9454 9454 0000 974074 100000 110 2767- 4150 3458
9901 9901 0000 2021814 100000 120 5743- 8614 7178
10617 10616 0001 2504445 100000 120 7114- 10670 8892
11087 11086 0001 927285 100000 120 2634- 3951 3292
Average of Peak Amounts = 120
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11518 11515 0003 7650320 250000 29 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 168 of 323
Data File vf479200d
Date 30-SEP-2012 1704
Client ID Instrument PESTGC9i
Sample Info ic-SG1660L1_00013 Operator
10162012Page 169 of 323
Data File vf479201d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479201dLab Smp Id IC-SG1660L2_00013 Inj Date 30-SEP-2012 1720 Operator Inst ID PESTGC9iSmp Info SG1660L2_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1720 Cal File vf479201dAls bottle 8 Calibration Sample Level 2Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2960 2961 -0001 5241842 500000 510 8000- 12000 10000
3640 3641 -0001 10590544 500000 500 16163- 24245 20204
4084 4085 -0001 4500373 500000 520 6868- 10303 8585
4477 4479 -0002 19475271 500000 520 29723- 44584 37153
4722 4722 0000 8838480 500000 540 13489- 20234 16861
5158 5158 0000 5152808 500000 530 7864- 11796 9830
5543 5542 0001 6213265 500000 520 9483- 14224 11853
5751 5752 -0001 6260864 500000 520 9555- 14333 11944
Average of Peak Amounts = 518
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
7756 7756 0000 11159859 500000 500 8000- 12000 10000(M)
10162012Page 170 of 323
Data File vf479201d Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
8215 8215 0000 12615093 500000 500 9043- 13565 11304
9084 9084 0000 18792136 500000 510 13471- 20207 16839
9332 9332 0000 8363664 500000 510 5996- 8993 7494
9454 9454 0000 4516956 500000 510 3238- 4857 4048
9901 9901 0000 8418625 500000 500 6035- 9052 7544
10617 10616 0001 10257895 500000 490 7353- 11030 9192
11087 11086 0001 4049088 500000 520 2903- 4354 3628
Average of Peak Amounts = 506
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11520 11515 0005 14076513 500000 53 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 171 of 323
Data File vf479201d
Date 30-SEP-2012 1720
Client ID Instrument PESTGC9i
Sample Info SG1660L2_00013 Operator
10162012Page 172 of 323
Data File vf479202d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479202dLab Smp Id IC-SG1660L3_00019 Inj Date 30-SEP-2012 1735 Operator Inst ID PESTGC9iSmp Info SG1660L3_00019Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 9 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2961 2961 0000 9647477 100000 940 8000- 12000 10000
3641 3641 0000 20808307 100000 980 17255- 25882 21569
4085 4085 0000 8352607 100000 960 6926- 10389 8658
4479 4479 0000 35290615 100000 940 29264- 43896 36580
4722 4722 0000 14821328 100000 900 12290- 18435 15363
5158 5158 0000 8954270 100000 920 7425- 11138 9281
5542 5542 0000 11165134 100000 930 9258- 13888 11573
5752 5752 0000 11609452 100000 960 9627- 14440 12034
Average of Peak Amounts = 940
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
7756 7756 0000 20851674 100000 940 8000- 12000 10000(M)
10162012Page 173 of 323
Data File vf479202d Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
8215 8215 0000 23518487 100000 940 9023- 13535 11279
9084 9084 0000 35705636 100000 970 13699- 20548 17124
9332 9332 0000 15681452 100000 960 6016- 9025 7520
9454 9454 0000 8644462 100000 980 3317- 4975 4146
9901 9901 0000 16386843 100000 970 6287- 9431 7859
10616 10616 0000 20530020 100000 970 7877- 11815 9846
11086 11086 0000 7531982 100000 960 2890- 4335 3612
Average of Peak Amounts = 962
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11515 11515 0000 25745578 100000 97 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 174 of 323
Data File vf479202d
Date 30-SEP-2012 1735
Client ID Instrument PESTGC9i
Sample Info SG1660L3_00019 Operator
10162012Page 175 of 323
Data File vf479203d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479203dLab Smp Id IC-SG1660L4_00013 Inj Date 30-SEP-2012 1751 Operator Inst ID PESTGC9iSmp Info SG1660L4_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1751 Cal File vf479203dAls bottle 10 Calibration Sample Level 4Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2959 2961 -0002 14643185 150000 1400 8000- 12000 10000
3639 3641 -0002 30213965 150000 1400 16507- 24760 20633
4083 4085 -0002 12661468 150000 1400 6917- 10376 8647
4477 4479 -0002 53874092 150000 1400 29433- 44149 36791
4722 4722 0000 23927783 150000 1400 13072- 19609 16341
5157 5158 -0001 13558761 150000 1400 7408- 11111 9259
5542 5542 0000 16822458 150000 1400 9191- 13786 11488
5751 5752 -0001 17418946 150000 1400 9516- 14275 11896
Average of Peak Amounts = 143e+03
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
7756 7756 0000 30895442 150000 1400 8000- 12000 10000(M)
10162012Page 176 of 323
Data File vf479203d Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
8215 8215 0000 34726449 150000 1400 8992- 13488 11240
9083 9084 -0001 53240044 150000 1400 13786- 20679 17232
9332 9332 0000 23213228 150000 1400 6011- 9016 7513
9454 9454 0000 12914338 150000 1500 3344- 5016 4180
9901 9901 0000 24307809 150000 1400 6294- 9441 7868
10617 10616 0001 31202581 150000 1500 8080- 12119 10099
11084 11086 -0002 11224374 150000 1400 2906- 4360 3633
Average of Peak Amounts = 143e+03
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11510 11515 -0005 36972164 150000 140 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 177 of 323
Data File vf479203d
Date 30-SEP-2012 1751
Client ID Instrument PESTGC9i
Sample Info SG1660L4_00013 Operator
10162012Page 178 of 323
Data File vf479204d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479204dLab Smp Id IC-SG1660L5_00013 Inj Date 30-SEP-2012 1807 Operator Inst ID PESTGC9iSmp Info SG1660L5_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1807 Cal File vf479204dAls bottle 11 Calibration Sample Level 5Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2959 2961 -0002 21530533 250000 2100 8000- 12000 10000
3640 3641 -0001 45462323 250000 2200 16892- 25338 21115
4083 4085 -0002 18540701 250000 2100 6889- 10334 8611
4476 4479 -0003 82034010 250000 2200 30481- 45721 38101
4722 4722 0000 35848765 250000 2200 13320- 19980 16650
5157 5158 -0001 20356566 250000 2100 7564- 11346 9455
5542 5542 0000 25115800 250000 2100 9332- 13998 11665
5751 5752 -0001 26330856 250000 2200 9784- 14675 12230
Average of Peak Amounts = 213e+03
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
7755 7756 -0001 46495806 250000 2100 8000- 12000 10000(M)
10162012Page 179 of 323
Data File vf479204d Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
8215 8215 0000 52908911 250000 2100 9103- 13655 11379
9082 9084 -0002 81893015 250000 2200 14090- 21136 17613
9331 9332 -0001 35484032 250000 2200 6105- 9158 7632
9453 9454 -0001 20108960 250000 2300 3460- 5190 4325
9901 9901 0000 37450674 250000 2200 6444- 9666 8055
10616 10616 0000 46064749 250000 2200 7926- 11889 9907
11085 11086 -0001 17250044 250000 2200 2968- 4452 3710
Average of Peak Amounts = 219e+03
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
11512 11515 -0003 47667099 200000 180 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 180 of 323
Data File vf479204d
Date 30-SEP-2012 1807
Client ID Instrument PESTGC9i
Sample Info SG1660L5_00013 Operator
10162012Page 181 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17839Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)GC Column CLP-1 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-1299267 vr479200dLevel 2 IC 460-1299268 vr479201dLevel 3 IC 460-1299269 vr479202dLevel 4 IC 460-12992610 vr479203dLevel 5 IC 460-12992611 vr479204d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
PCB-1016 Peak 1 20842015 - 21552085 2084 2085 2083 2084PCB-1016 Peak 2 25272457 - 25972527 2526 2527 2527 2526PCB-1016 Peak 3 27762707 - 28472777 2776 2777 2775 2775PCB-1016 Peak 4 31283060 - 32003128 3128 3130 3128 3127PCB-1016 Peak 5 33293260 - 34003329 3329 3330 3328 3328PCB-1016 Peak 6 36823615 - 37553682 3682 3685 3683 3681PCB-1016 Peak 7 40433973 - 41134042 4043 4043 4042 4043PCB-1016 Peak 8 41904121 - 42614190 4190 4191 4188 4190PCB-1260 Peak 1 60716002 - 61426072 6072 6072 6071 6071PCB-1260 Peak 2 65226452 - 65926522 6523 6522 6522 6521PCB-1260 Peak 3 69646894 - 70346964 6965 6964 6963 6964PCB-1260 Peak 4 71647095 - 72357165 7165 7165 7164 7164PCB-1260 Peak 5 76027532 - 76727602 7603 7602 7602 7601PCB-1260 Peak 6 88938823 - 89638893 8894 8893 8893 8892PCB-1260 Peak 7 91159045 - 91859115 9115 9115 9115 9114PCB-1260 Peak 8 1015310083 - 1022310153 10154 10153 10153 10153DCB Decachlorobiphenyl 1062410524 - 1072410625 10625 10624 10624 10624
FORM VI 8082 10162012Page 182 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17839Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-1299267 vr479200d2Level IC 460-1299268 vr479201d3Level IC 460-1299269 vr479202d4Level IC 460-12992610 vr479203d5Level IC 460-12992611 vr479204d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
LVL 5
PCB-1016 Peak 1 Ave 197 20021391 15827 14690 1421213626
159493236
PCB-1016 Peak 2 Ave 165 20034434 28377 25503 2514722693
272309984
PCB-1016 Peak 3 Ave 77 20020149 18502 16986 1713716990
179529604
PCB-1016 Peak 4 Ave 163 20075334 61344 55787 5498850020
594947119
PCB-1016 Peak 5 Ave 111 20026774 23733 21963 2197020028
228936643
PCB-1016 Peak 6 Ave 186 20030865 24479 22517 2109919526
236972316
PCB-1016 Peak 7 Ave 97 20025842 23012 21540 2153920131
224127747
PCB-1016 Peak 8 Ave 151 20012619 94689 86303 1057294995
101578271
PCB-1260 Peak 1 Ave 163 20041532 33110 31025 3015327565
326771001
PCB-1260 Peak 2 Ave 177 20078411 60909 57128 5539650491
604671657
PCB-1260 Peak 3 Ave 138 20068452 55082 53236 5187948612
554520757
PCB-1260 Peak 4 Ave 154 20037971 30462 28586 2772626073
301638112
PCB-1260 Peak 5 Ave 148 20034082 26592 25567 2477624302
270637128
PCB-1260 Peak 6 Ave 81 20038982 34673 33173 3331131697
343672090
PCB-1260 Peak 7 Ave 66 20023297 21847 20031 2012320512
211620048
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 183 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17839Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
LVL 5
PCB-1260 Peak 8 Ave 59 20018824 17382 16914 1709216013
172450198
DCB Decachlorobiphenyl Ave 109 200544588 499440 455074 438703415700
470701073
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 184 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17839Calibration Start Date Calibration End Date09302012 1704
N
09302012 1807
GC Column CLP-1 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-1299267 vr479200dLevel 2 IC 460-1299268 vr479201dLevel 3 IC 460-1299269 vr479202dLevel 4 IC 460-12992610 vr479203dLevel 5 IC 460-12992611 vr479204d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
PCB-1016 Peak 1 Ave 2139086 7913738 14690255 21317999 34065069 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 3443416 14188692 25503333 37720095 56733462 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 2014938 9251204 16986172 25705034 42475382 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 7533379 30672168 55786970 82482485 125050351 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 2677413 11866731 21962918 32955239 50069130 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 3086462 12239557 22517485 31648230 48815297 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 2584175 11505820 21540272 32309208 50326849 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 1261883 4734436 8630325 15857466 23748661 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 4153239 16554914 31025367 45229464 68912349 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 7841143 30454619 57128111 83094008 126227611 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 6845178 27541094 53235986 77818190 121529078 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 3797116 15230911 28586487 41589423 65183263 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 3408191 13295973 25567248 37163734 60754093 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 3898216 17336408 33172625 49966572 79243490 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 2329661 10923449 20031237 30184937 51279969 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 1882356 8691093 16914378 25637846 40032694 100 500 1000 1500 2500DCB Decachlorobiphenyl Ave 13614701 24972013 45507407 65805444 83140007 250 500 100 150 200
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 185 of 323
Data File vr479200d Page 1 Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479200dLab Smp Id IC-SG1660L1_00013 Inj Date 30-SEP-2012 1704 Operator Inst ID PESTGC9iSmp Info ic-SG1660L1_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 7 Calibration Sample Level 1Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2085 2085 0000 2139086 100000 130 8000- 12000 10000(M)
2527 2527 0000 3443416 100000 130 13324- 19985 16098
2777 2777 0000 2014938 100000 110 9975- 14963 9420
3128 3130 -0002 7533379 100000 130 29367- 44051 35218
3329 3330 -0001 2677413 100000 120 11758- 17638 12517
3682 3685 -0003 3086462 100000 130 11464- 17196 14429
4042 4043 -0001 2584175 100000 120 11819- 17728 12081
4190 4191 -0001 1261883 100000 120 5577- 8366 5899
Average of Peak Amounts = 123
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
6072 6072 0000 4153239 100000 130 8000- 12000 10000
10162012Page 186 of 323
Data File vr479200d Page 2 Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6522 6522 0000 7841143 100000 130 14654- 21981 18880
6964 6964 0000 6845178 100000 120 14108- 21162 16482
7165 7165 0000 3797116 100000 120 7567- 11351 9143
7602 7602 0000 3408191 100000 120 7053- 10579 8206
8893 8893 0000 3898216 100000 110 9199- 13799 9386
9115 9115 0000 2329661 100000 110 5953- 8930 5609
10153 10153 0000 1882356 100000 110 4647- 6971 4532
Average of Peak Amounts = 121
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10625 10624 0001 13614701 250000 29 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 187 of 323
Data File vr479200d
Date 30-SEP-2012 1704
Client ID Instrument PESTGC9i
Sample Info ic-SG1660L1_00013 Operator
10162012Page 188 of 323
Data File vr479201d Page 1 Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479201dLab Smp Id IC-SG1660L2_00013 Inj Date 30-SEP-2012 1720 Operator Inst ID PESTGC9iSmp Info SG1660L2_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 8 Calibration Sample Level 2Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2084 2085 -0001 7913738 500000 500 8000- 12000 10000(M)
2526 2527 -0001 14188692 500000 520 13324- 19985 17929
2776 2777 -0001 9251204 500000 520 9975- 14963 11690
3128 3130 -0002 30672168 500000 520 29367- 44051 38758
3329 3330 -0001 11866731 500000 520 11758- 17638 14995
3682 3685 -0003 12239557 500000 520 11464- 17196 15466
4043 4043 0000 11505820 500000 510 11819- 17728 14539
4190 4191 -0001 4734436 500000 470 5577- 8366 5983
Average of Peak Amounts = 508
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
6072 6072 0000 16554914 500000 510 8000- 12000 10000
10162012Page 189 of 323
Data File vr479201d Page 2 Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6523 6522 0001 30454619 500000 500 14654- 21981 18396
6965 6964 0001 27541094 500000 500 14108- 21162 16636
7165 7165 0000 15230911 500000 500 7567- 11351 9200
7603 7602 0001 13295973 500000 490 7053- 10579 8031
8894 8893 0001 17336408 500000 500 9199- 13799 10472
9115 9115 0000 10923449 500000 520 5953- 8930 6598
10154 10153 0001 8691093 500000 500 4647- 6971 5250
Average of Peak Amounts = 503
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10625 10624 0001 24972013 500000 53 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 190 of 323
Data File vr479201d
Date 30-SEP-2012 1720
Client ID Instrument PESTGC9i
Sample Info SG1660L2_00013 Operator
10162012Page 191 of 323
Data File vr479202d Page 1 Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479202dLab Smp Id IC-SG1660L3_00019 Inj Date 30-SEP-2012 1735 Operator Inst ID PESTGC9iSmp Info SG1660L3_00019Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 9 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2085 2085 0000 14690255 100000 920 8000- 12000 10000(M)
2527 2527 0000 25503333 100000 940 13324- 19985 17361
2777 2777 0000 16986172 100000 950 9975- 14963 11563
3130 3130 0000 55786970 100000 940 29367- 44051 37975
3330 3330 0000 21962918 100000 960 11758- 17638 14951
3685 3685 0000 22517485 100000 950 11464- 17196 15328
4043 4043 0000 21540272 100000 960 11819- 17728 14663
4191 4191 0000 8630325 100000 850 5577- 8366 5875
Average of Peak Amounts = 933
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
6072 6072 0000 31025367 100000 950 8000- 12000 10000
10162012Page 192 of 323
Data File vr479202d Page 2 Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6522 6522 0000 57128111 100000 940 14654- 21981 18413
6964 6964 0000 53235986 100000 960 14108- 21162 17159
7165 7165 0000 28586487 100000 950 7567- 11351 9214
7602 7602 0000 25567248 100000 940 7053- 10579 8241
8893 8893 0000 33172625 100000 960 9199- 13799 10692
9115 9115 0000 20031237 100000 950 5953- 8930 6456
10153 10153 0000 16914378 100000 980 4647- 6971 5452
Average of Peak Amounts = 955
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10624 10624 0000 45507407 100000 97 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 193 of 323
Data File vr479202d
Date 30-SEP-2012 1735
Client ID Instrument PESTGC9i
Sample Info SG1660L3_00019 Operator
10162012Page 194 of 323
Data File vr479203d Page 1 Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479203dLab Smp Id IC-SG1660L4_00013 Inj Date 30-SEP-2012 1751 Operator Inst ID PESTGC9iSmp Info SG1660L4_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 10 Calibration Sample Level 4Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2083 2085 -0002 21317999 150000 1300 8000- 12000 10000(M)
2527 2527 0000 37720095 150000 1400 13324- 19985 17694
2775 2777 -0002 25705034 150000 1400 9975- 14963 12058
3128 3130 -0002 82482485 150000 1400 29367- 44051 38691
3328 3330 -0002 32955239 150000 1400 11758- 17638 15459
3683 3685 -0002 31648230 150000 1300 11464- 17196 14846
4042 4043 -0001 32309208 150000 1400 11819- 17728 15156
4188 4191 -0003 15857466 150000 1600 5577- 8366 7439
Average of Peak Amounts = 141e+03
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
6071 6072 -0001 45229464 150000 1400 8000- 12000 10000
10162012Page 195 of 323
Data File vr479203d Page 2 Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6522 6522 0000 83094008 150000 1400 14654- 21981 18372
6963 6964 -0001 77818190 150000 1400 14108- 21162 17205
7164 7165 -0001 41589423 150000 1400 7567- 11351 9195
7602 7602 0000 37163734 150000 1400 7053- 10579 8217
8893 8893 0000 49966572 150000 1400 9199- 13799 11047
9115 9115 0000 30184937 150000 1400 5953- 8930 6674
10153 10153 0000 25637846 150000 1500 4647- 6971 5668
Average of Peak Amounts = 141e+03
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10624 10624 0000 65805444 150000 140 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 196 of 323
Data File vr479203d
Date 30-SEP-2012 1751
Client ID Instrument PESTGC9i
Sample Info SG1660L4_00013 Operator
10162012Page 197 of 323
Data File vr479204d Page 1 Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479204dLab Smp Id IC-SG1660L5_00013 Inj Date 30-SEP-2012 1807 Operator Inst ID PESTGC9iSmp Info SG1660L5_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 11 Calibration Sample Level 5Dil Factor 100000 Integrator Falcon Compound Sublist AR16600SsubTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS 12674-11-2
2084 2085 -0001 34065069 250000 2100 8000- 12000 10000(M)
2526 2527 -0001 56733462 250000 2100 13324- 19985 16654
2775 2777 -0002 42475382 250000 2400 9975- 14963 12469
3127 3130 -0003 125050351 250000 2100 29367- 44051 36709
3328 3330 -0002 50069130 250000 2200 11758- 17638 14698
3681 3685 -0004 48815297 250000 2000 11464- 17196 14330
4043 4043 0000 50326849 250000 2200 11819- 17728 14774
4190 4191 -0001 23748661 250000 2300 5577- 8366 6972
Average of Peak Amounts = 219e+03
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS 11096-82-5
6071 6072 -0001 68912349 250000 2100 8000- 12000 10000
10162012Page 198 of 323
Data File vr479204d Page 2 Report Date 01-Oct-2012 0846
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6521 6522 -0001 126227611 250000 2100 14654- 21981 18317
6964 6964 0000 121529078 250000 2200 14108- 21162 17635
7164 7165 -0001 65183263 250000 2200 7567- 11351 9459
7601 7602 -0001 60754093 250000 2200 7053- 10579 8816
8892 8893 -0001 79243490 250000 2300 9199- 13799 11499
9114 9115 -0001 51279969 250000 2400 5953- 8930 7441
10153 10153 0000 40032694 250000 2300 4647- 6971 5809
Average of Peak Amounts = 223e+03
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS 2051-24-3
10624 10624 0000 83140007 200000 180 8000- 12000 10000
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated
10162012Page 199 of 323
Data File vr479204d
Date 30-SEP-2012 1807
Client ID Instrument PESTGC9i
Sample Info SG1660L5_00013 Operator
10162012Page 200 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17848Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992612 vf479205d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1221 Peak 1 16651595 - 17351665PCB-1221 Peak 2 21352065 - 22052135PCB-1221 Peak 3 26722602 - 27422672PCB-1221 Peak 4 28732803 - 29432873PCB-1221 Peak 5 29612891 - 30312961PCB-1221 Peak 6 37393669 - 38093739PCB-1221 Peak 7 40834013 - 41534083PCB-1221 Peak 8 44774407 - 45474477
FORM VI 8082 10162012Page 201 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17848Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992612 vf479205d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
47106PCB-1221 Peak 1 Ave 20047106130012961PCB-1221 Peak 2 Ave 20012960750058524PCB-1221 Peak 3 Ave 20058523710040015PCB-1221 Peak 4 Ave 20040015420013789PCB-1221 Peak 5 Ave 20013788908018488PCB-1221 Peak 6 Ave 20018488040061501PCB-1221 Peak 7 Ave 20061500800024165PCB-1221 Peak 8 Ave 200241652800
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 202 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17848Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
GC Column CLP-2 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992612 vf479205d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1221 Peak 1 Ave 4710613 1000PCB-1221 Peak 2 Ave 1296075 1000PCB-1221 Peak 3 Ave 5852371 1000PCB-1221 Peak 4 Ave 4001542 1000PCB-1221 Peak 5 Ave 13788908 1000PCB-1221 Peak 6 Ave 1848804 1000PCB-1221 Peak 7 Ave 615008 1000PCB-1221 Peak 8 Ave 2416528 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 203 of 323
Data File vf479205d Report Date 01-Oct-2012 0846
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479205dLab Smp Id IC-SG1221L3_00014 Inj Date 30-SEP-2012 1822 Operator Inst ID PESTGC9iSmp Info ic SG1221L3_00014Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0846 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 12 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12210subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
22 Aroclor-1221 CAS 11104-28-2
1665 1665 0000 4710613 100000 1000 8000- 12000 10000
2135 2135 0000 1296075 100000 1000 2201- 3302 2751
2672 2672 0000 5852371 100000 1000 9939- 14909 12424
2873 2873 0000 4001542 100000 1000 6796- 10194 8495
2961 2961 0000 13788908 100000 1000 23418- 35126 29272
3739 3739 0000 1848804 100000 1000 3140- 4710 3925
4083 4083 0000 615008 100000 1000 1044- 1567 1306
4477 4477 0000 2416528 100000 1000 4104- 6156 5130
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 204 of 323
Data File vf479205d
Date 30-SEP-2012 1822
Client ID Instrument PESTGC9i
Sample Info ic SG1221L3_00014 Operator
10162012Page 205 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17841Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
053(mm)GC Column CLP-1 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992612 vr479205d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1221 Peak 1 11111041 - 11811111PCB-1221 Peak 2 15111441 - 15811511PCB-1221 Peak 3 18601790 - 19301860PCB-1221 Peak 4 20822012 - 21522082PCB-1221 Peak 5 25282458 - 25982528PCB-1221 Peak 6 26022532 - 26722602PCB-1221 Peak 7 26852615 - 27552685PCB-1221 Peak 8 31303060 - 32003130
FORM VI 8082 10162012Page 206 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17841Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992612 vr479205d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
64024PCB-1221 Peak 1 Ave 20064024020030571PCB-1221 Peak 2 Ave 20030571000095270PCB-1221 Peak 3 Ave 20095269770024981PCB-1221 Peak 4 Ave 20024981158027336PCB-1221 Peak 5 Ave 20027336400022123PCB-1221 Peak 6 Ave 20022122590041633PCB-1221 Peak 7 Ave 20041632790048909PCB-1221 Peak 8 Ave 200489094700
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 207 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17841Calibration Start Date Calibration End Date09302012 1822
N
09302012 1822
GC Column CLP-1 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992612 vr479205d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1221 Peak 1 Ave 6402402 1000PCB-1221 Peak 2 Ave 3057100 1000PCB-1221 Peak 3 Ave 9526977 1000PCB-1221 Peak 4 Ave 24981158 1000PCB-1221 Peak 5 Ave 2733640 1000PCB-1221 Peak 6 Ave 2212259 1000PCB-1221 Peak 7 Ave 4163279 1000PCB-1221 Peak 8 Ave 4890947 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 208 of 323
Data File vr479205d Page 1 Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479205dLab Smp Id IC-SG1221L3_00014 Inj Date 30-SEP-2012 1822 Operator Inst ID PESTGC9iSmp Info ic SG1221L3_00014Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 12 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12210subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
22 Aroclor-1221 CAS 11104-28-2
1111 1111 0000 6402402 100000 1000 8000- 12000 10000(M)
1511 1511 0000 3057100 100000 1000 3820- 5730 4775
1860 1860 0000 9526977 100000 1000 11904- 17856 14880
2082 2082 0000 24981158 100000 1000 31215- 46822 39018
2528 2528 0000 2733640 100000 1000 3416- 5124 4270
2602 2602 0000 2212259 100000 1000 2764- 4146 3455
2685 2685 0000 4163279 100000 1000 5202- 7803 6503
3130 3130 0000 4890947 100000 1000 6111- 9167 7639
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 209 of 323
Data File vr479205d Page 2 Report Date 01-Oct-2012 0847
QC Flag Legend
M - Compound response manually integrated
10162012Page 210 of 323
Data File vr479205d
Date 30-SEP-2012 1822
Client ID Instrument PESTGC9i
Sample Info ic SG1221L3_00014 Operator
10162012Page 211 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17849Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992613 vf479206d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1232 Peak 1 29612891 - 30312961PCB-1232 Peak 2 36403570 - 37103640PCB-1232 Peak 3 40854015 - 41554085PCB-1232 Peak 4 47224652 - 47924722PCB-1232 Peak 5 49024832 - 49724902PCB-1232 Peak 6 50875017 - 51575087PCB-1232 Peak 7 55425472 - 56125542PCB-1232 Peak 8 57515681 - 58215751
FORM VI 8082 10162012Page 212 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17849Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992613 vf479206d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
97711PCB-1232 Peak 1 Ave 20097710620094688PCB-1232 Peak 2 Ave 20094688030035761PCB-1232 Peak 3 Ave 20035761260066995PCB-1232 Peak 4 Ave 20066994820050607PCB-1232 Peak 5 Ave 20050607280041053PCB-1232 Peak 6 Ave 20041053380057396PCB-1232 Peak 7 Ave 20057395890062677PCB-1232 Peak 8 Ave 200626765000
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 213 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17849Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
GC Column CLP-2 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992613 vf479206d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1232 Peak 1 Ave 9771062 1000PCB-1232 Peak 2 Ave 9468803 1000PCB-1232 Peak 3 Ave 3576126 1000PCB-1232 Peak 4 Ave 6699482 1000PCB-1232 Peak 5 Ave 5060728 1000PCB-1232 Peak 6 Ave 4105338 1000PCB-1232 Peak 7 Ave 5739589 1000PCB-1232 Peak 8 Ave 6267650 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 214 of 323
Data File vf479206d Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479206dLab Smp Id ic SG1232L3_00013 Inj Date 30-SEP-2012 1838 Operator Inst ID PESTGC9iSmp Info ic SG1232L3_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0847 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 13 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12320subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
23 Aroclor-1232 CAS 11141-16-5
2961 2961 0000 9771062 100000 1000 8000- 12000 10000
3640 3640 0000 9468803 100000 1000 7753- 11629 9691
4085 4085 0000 3576126 100000 1000 2928- 4392 3660
4722 4722 0000 6699482 100000 1000 5485- 8228 6856
4902 4902 0000 5060728 100000 1000 4143- 6215 5179
5087 5087 0000 4105338 100000 1000 3361- 5042 4202
5542 5542 0000 5739589 100000 1000 4699- 7049 5874
5751 5751 0000 6267650 100000 1000 5132- 7697 6415
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 215 of 323
Data File vf479206d
Date 30-SEP-2012 1838
Client ID Instrument PESTGC9i
Sample Info ic SG1232L3_00013 Operator
10162012Page 216 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17842Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
053(mm)GC Column CLP-1 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992613 vr479206d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1232 Peak 1 20822012 - 21522082PCB-1232 Peak 2 25262456 - 25962526PCB-1232 Peak 3 27762706 - 28462776PCB-1232 Peak 4 31283058 - 31983128PCB-1232 Peak 5 33293259 - 33993329PCB-1232 Peak 6 34243354 - 34943424PCB-1232 Peak 7 40423972 - 41124042PCB-1232 Peak 8 46144544 - 46844614
FORM VI 8082 10162012Page 217 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17842Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992613 vr479206d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
18402PCB-1232 Peak 1 Ave 20018402354014182PCB-1232 Peak 2 Ave 20014181613010089PCB-1232 Peak 3 Ave 20010089309027669PCB-1232 Peak 4 Ave 20027669356010841PCB-1232 Peak 5 Ave 20010840936085833PCB-1232 Peak 6 Ave 20085833230011581PCB-1232 Peak 7 Ave 20011580551048393PCB-1232 Peak 8 Ave 200483934800
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 218 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17842Calibration Start Date Calibration End Date09302012 1838
N
09302012 1838
GC Column CLP-1 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992613 vr479206d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1232 Peak 1 Ave 18402354 1000PCB-1232 Peak 2 Ave 14181613 1000PCB-1232 Peak 3 Ave 10089309 1000PCB-1232 Peak 4 Ave 27669356 1000PCB-1232 Peak 5 Ave 10840936 1000PCB-1232 Peak 6 Ave 8583323 1000PCB-1232 Peak 7 Ave 11580551 1000PCB-1232 Peak 8 Ave 4839348 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 219 of 323
Data File vr479206d Page 1 Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479206dLab Smp Id ic SG1232L3_00013 Inj Date 30-SEP-2012 1838 Operator Inst ID PESTGC9iSmp Info ic SG1232L3_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 13 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12320subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
23 Aroclor-1232 CAS 11141-16-5
2082 2082 0000 18402354 100000 1000 8000- 12000 10000
2526 2526 0000 14181613 100000 1000 6165- 9248 7706
2776 2776 0000 10089309 100000 1000 4386- 6579 5483
3128 3128 0000 27669356 100000 1000 12029- 18043 15036
3329 3329 0000 10840936 100000 1000 4713- 7069 5891
3424 3424 0000 8583323 100000 1000 3731- 5597 4664
4042 4042 0000 11580551 100000 1000 5034- 7552 6293
4614 4614 0000 4839348 100000 1000 2104- 3156 2630
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 220 of 323
Data File vr479206d
Date 30-SEP-2012 1838
Client ID Instrument PESTGC9i
Sample Info ic SG1232L3_00013 Operator
10162012Page 221 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17850Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992614 vf479207d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1242 Peak 1 29612891 - 30312961PCB-1242 Peak 2 36413571 - 37113641PCB-1242 Peak 3 40864016 - 41564086PCB-1242 Peak 4 44794409 - 45494479PCB-1242 Peak 5 47234653 - 47934723PCB-1242 Peak 6 51585088 - 52285158PCB-1242 Peak 7 57525682 - 58225752PCB-1242 Peak 8 62656195 - 63356265
FORM VI 8082 10162012Page 222 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17850Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992614 vf479207d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
81414PCB-1242 Peak 1 Ave 20081414290015365PCB-1242 Peak 2 Ave 20015365311065982PCB-1242 Peak 3 Ave 20065981950028106PCB-1242 Peak 4 Ave 20028106459012209PCB-1242 Peak 5 Ave 20012208628069961PCB-1242 Peak 6 Ave 20069960990010615PCB-1242 Peak 7 Ave 20010615499010283PCB-1242 Peak 8 Ave 200102828980
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 223 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17850Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
GC Column CLP-2 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992614 vf479207d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1242 Peak 1 Ave 8141429 1000PCB-1242 Peak 2 Ave 15365311 1000PCB-1242 Peak 3 Ave 6598195 1000PCB-1242 Peak 4 Ave 28106459 1000PCB-1242 Peak 5 Ave 12208628 1000PCB-1242 Peak 6 Ave 6996099 1000PCB-1242 Peak 7 Ave 10615499 1000PCB-1242 Peak 8 Ave 10282898 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 224 of 323
Data File vf479207d Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479207dLab Smp Id ic SG1242L3_00013 Inj Date 30-SEP-2012 1854 Operator Inst ID PESTGC9iSmp Info ic SG1242L3_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0847 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 14 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12420subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
24 Aroclor-1242 CAS 53469-21-9
2961 2961 0000 8141429 100000 1000 8000- 12000 10000(M)
3641 3641 0000 15365311 100000 1000 15098- 22648 18873
4086 4086 0000 6598195 100000 1000 6484- 9725 8104
4479 4479 0000 28106459 100000 1000 27618- 41427 34523
4723 4723 0000 12208628 100000 1000 11997- 17995 14996
5158 5158 0000 6996099 100000 1000 6875- 10312 8593
5752 5752 0000 10615499 100000 1000 10431- 15647 13039
6265 6265 0000 10282898 100000 1000 10104- 15156 12630
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 225 of 323
Data File vf479207d Report Date 01-Oct-2012 0847
QC Flag Legend
M - Compound response manually integrated
10162012Page 226 of 323
Data File vf479207d
Date 30-SEP-2012 1854
Client ID Instrument PESTGC9i
Sample Info ic SG1242L3_00013 Operator
10162012Page 227 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17843Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
053(mm)GC Column CLP-1 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992614 vr479207d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1242 Peak 1 20832013 - 21532083PCB-1242 Peak 2 25272457 - 25972527PCB-1242 Peak 3 27772707 - 28472777PCB-1242 Peak 4 31293059 - 31993129PCB-1242 Peak 5 33293259 - 33993329PCB-1242 Peak 6 36853615 - 37553685PCB-1242 Peak 7 40443974 - 41144044PCB-1242 Peak 8 51265056 - 51965126
FORM VI 8082 10162012Page 228 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17843Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992614 vr479207d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
13527PCB-1242 Peak 1 Ave 20013526845020219PCB-1242 Peak 2 Ave 20020218998014340PCB-1242 Peak 3 Ave 20014339987044262PCB-1242 Peak 4 Ave 20044261735017388PCB-1242 Peak 5 Ave 20017387684018314PCB-1242 Peak 6 Ave 20018314121017750PCB-1242 Peak 7 Ave 20017749733015393PCB-1242 Peak 8 Ave 200153932670
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 229 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17843Calibration Start Date Calibration End Date09302012 1854
N
09302012 1854
GC Column CLP-1 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992614 vr479207d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1242 Peak 1 Ave 13526845 1000PCB-1242 Peak 2 Ave 20218998 1000PCB-1242 Peak 3 Ave 14339987 1000PCB-1242 Peak 4 Ave 44261735 1000PCB-1242 Peak 5 Ave 17387684 1000PCB-1242 Peak 6 Ave 18314121 1000PCB-1242 Peak 7 Ave 17749733 1000PCB-1242 Peak 8 Ave 15393267 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 230 of 323
Data File vr479207d Page 1 Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479207dLab Smp Id ic SG1242L3_00013 Inj Date 30-SEP-2012 1854 Operator Inst ID PESTGC9iSmp Info ic SG1242L3_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 14 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12420subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
24 Aroclor-1242 CAS 53469-21-9
2083 2083 0000 13526845 100000 1000 8000- 12000 10000(M)
2527 2527 0000 20218998 100000 1000 11958- 17937 14947
2777 2777 0000 14339987 100000 1000 8481- 12721 10601
3129 3129 0000 44261735 100000 1000 26177- 39266 32721
3329 3329 0000 17387684 100000 1000 10283- 15425 12854
3685 3685 0000 18314121 100000 1000 10831- 16247 13539
4044 4044 0000 17749733 100000 1000 10497- 15746 13122
5126 5126 0000 15393267 100000 1000 9104- 13656 11380
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 231 of 323
Data File vr479207d Page 2 Report Date 01-Oct-2012 0847
QC Flag Legend
M - Compound response manually integrated
10162012Page 232 of 323
Data File vr479207d
Date 30-SEP-2012 1854
Client ID Instrument PESTGC9i
Sample Info ic SG1242L3_00013 Operator
10162012Page 233 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17851Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992615 vf479208d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1248 Peak 1 36373567 - 37073637PCB-1248 Peak 2 44734403 - 45434473PCB-1248 Peak 3 49514881 - 50214951PCB-1248 Peak 4 50865016 - 51565086PCB-1248 Peak 5 55415471 - 56115541PCB-1248 Peak 6 57505680 - 58205750PCB-1248 Peak 7 61916121 - 62616191PCB-1248 Peak 8 62626192 - 63326262
FORM VI 8082 10162012Page 234 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17851Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992615 vf479208d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
89356PCB-1248 Peak 1 Ave 20089355610020760PCB-1248 Peak 2 Ave 20020759623031559PCB-1248 Peak 3 Ave 20031559070012341PCB-1248 Peak 4 Ave 20012341389015809PCB-1248 Peak 5 Ave 20015808884017466PCB-1248 Peak 6 Ave 20017465791016624PCB-1248 Peak 7 Ave 20016623508019431PCB-1248 Peak 8 Ave 200194311040
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 235 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17851Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
GC Column CLP-2 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992615 vf479208d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1248 Peak 1 Ave 8935561 1000PCB-1248 Peak 2 Ave 20759623 1000PCB-1248 Peak 3 Ave 3155907 1000PCB-1248 Peak 4 Ave 12341389 1000PCB-1248 Peak 5 Ave 15808884 1000PCB-1248 Peak 6 Ave 17465791 1000PCB-1248 Peak 7 Ave 16623508 1000PCB-1248 Peak 8 Ave 19431104 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 236 of 323
Data File vf479208d Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082frontSep1209-30-12ical30sep12abvf479208dLab Smp Id ic SG1248L3_00013 Inj Date 30-SEP-2012 1909 Operator Inst ID PESTGC9iSmp Info ic SG1248L3_00013Misc Info Comment Method chem1PESTGC9i8082frontSep1209-30-12ical30sep12ab08Vf8082mMeth Date 01-Oct-2012 0847 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vf479211dAls bottle 15 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12480subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
25 Aroclor-1248 CAS 12672-29-6
3637 3637 0000 8935561 100000 1000 8000- 12000 10000
4473 4473 0000 20759623 100000 1000 18586- 27879 23233
4951 4951 0000 3155907 100000 1000 2825- 4238 3532
5086 5086 0000 12341389 100000 1000 11049- 16574 13812
5541 5541 0000 15808884 100000 1000 14154- 21231 17692
5750 5750 0000 17465791 100000 1000 15637- 23456 19546
6191 6191 0000 16623508 100000 1000 14883- 22325 18604
6262 6262 0000 19431104 100000 1000 17397- 26095 21746
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 237 of 323
Data File vf479208d
Date 30-SEP-2012 1909
Client ID Instrument PESTGC9i
Sample Info ic SG1248L3_00013 Operator
10162012Page 238 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17844Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
053(mm)GC Column CLP-1 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992615 vr479208d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1248 Peak 1 25252455 - 25952525PCB-1248 Peak 2 31243054 - 31943124PCB-1248 Peak 3 34233353 - 34933423PCB-1248 Peak 4 36783608 - 37483678PCB-1248 Peak 5 40413971 - 41114041PCB-1248 Peak 6 41864116 - 42564186PCB-1248 Peak 7 46154545 - 46854615PCB-1248 Peak 8 51245054 - 51945124
FORM VI 8082 10162012Page 239 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17844Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
053(mm)CLP-1 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992615 vr479208d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
11417PCB-1248 Peak 1 Ave 20011416682034274PCB-1248 Peak 2 Ave 20034273988063635PCB-1248 Peak 3 Ave 20063635020034030PCB-1248 Peak 4 Ave 20034030097030220PCB-1248 Peak 5 Ave 20030220358018203PCB-1248 Peak 6 Ave 20018202681015611PCB-1248 Peak 7 Ave 20015610993034370PCB-1248 Peak 8 Ave 200343696460
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 240 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17844Calibration Start Date Calibration End Date09302012 1909
N
09302012 1909
GC Column CLP-1 ID 053(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992615 vr479208d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UGL)
LVL 1 LVL 1
PCB-1248 Peak 1 Ave 11416682 1000PCB-1248 Peak 2 Ave 34273988 1000PCB-1248 Peak 3 Ave 6363502 1000PCB-1248 Peak 4 Ave 34030097 1000PCB-1248 Peak 5 Ave 30220358 1000PCB-1248 Peak 6 Ave 18202681 1000PCB-1248 Peak 7 Ave 15610993 1000PCB-1248 Peak 8 Ave 34369646 1000
Curve Type LegendAve = Average
FORM VI 8082 10162012Page 241 of 323
Data File vr479208d Page 1 Report Date 01-Oct-2012 0847
TestAmerica
GC ORGANICS QUANTITATION REPORTData file chem1PESTGC9i8082rearSep1209-30-12ical30sep12abvr479208dLab Smp Id ic SG1248L3_00013 Inj Date 30-SEP-2012 1909 Operator Inst ID PESTGC9iSmp Info ic SG1248L3_00013Misc Info Comment Method chem1PESTGC9i8082rearSep1209-30-12ical30sep12ab08Vr8082mMeth Date 01-Oct-2012 0828 sita Quant Type ESTDCal Date 30-SEP-2012 1956 Cal File vr479211dAls bottle 15 Calibration Sample Level 3Dil Factor 100000 Integrator Falcon Compound Sublist AR12480subTarget Version 350 Sample Matrix SOILProcessing Host hpd3
Concentration Formula Amt DF Vt(Ws(100-M)100) CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 100000 Dilution FactorVt 1000000 Volume of final extract (mL)Ws 1500000 Weight of sample extracted (g)M 000000 Moisture
Cpnd Variable Local Compound Variable
AMOUNTS
CAL-AMT ON-COL
RT EXP RT DLT RT RESPONSE ( ugL) ( ugL) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
25 Aroclor-1248 CAS 12672-29-6
2525 2525 0000 11416682 100000 1000 8000- 12000 10000(M)
3124 3124 0000 34273988 100000 1000 24017- 36025 30021
3423 3423 0000 6363502 100000 1000 4459- 6689 5574
3678 3678 0000 34030097 100000 1000 23846- 35769 29807
4041 4041 0000 30220358 100000 1000 21176- 31764 26470
4186 4186 0000 18202681 100000 1000 12755- 19133 15944
4615 4615 0000 15610993 100000 1000 10939- 16409 13674
5124 5124 0000 34369646 100000 1000 24084- 36126 30105
Average of Peak Amounts = 1e+03
-------------------------------------------------------------------------------
10162012Page 242 of 323
Data File vr479208d Page 2 Report Date 01-Oct-2012 0847
QC Flag Legend
M - Compound response manually integrated
10162012Page 243 of 323
Data File vr479208d
Date 30-SEP-2012 1909
Client ID Instrument PESTGC9i
Sample Info ic SG1248L3_00013 Operator
10162012Page 244 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17852Calibration Start Date Calibration End Date09302012 1925
N
09302012 1925
053(mm)GC Column CLP-2 ID
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE IDLevel 1 IC 460-12992616 vf479209d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1254 Peak 1 50855015 - 51555085PCB-1254 Peak 2 62536183 - 63236253PCB-1254 Peak 3 65806510 - 66506580PCB-1254 Peak 4 71577087 - 72277157PCB-1254 Peak 5 73717301 - 74417371PCB-1254 Peak 6 85968526 - 86668596PCB-1254 Peak 7 90869016 - 91569086PCB-1254 Peak 8 98439773 - 99139843
FORM VI 8082 10162012Page 245 of 323
FORM VI
Lab Name Job No
Calibration ID
SDG No
Instrument ID GC Column Heated Purge (YN)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-45537-1
PESTGC9
Analy Batch No 129926
17852Calibration Start Date Calibration End Date09302012 1925
N
09302012 1925
053(mm)CLP-2 ID
EXTERNAL STANDARD CURVE EVALUATION
Calibration Files
LEVEL LAB SAMPLE ID LAB FILE ID1Level IC 460-12992616 vf479209d
MIN R^2OR COD
R^2OR COD
MAXRSD
RSDCOEFFICIENT
M2M1B
CURVETYPE
LVL 1
CFANALYTE MIN CF
97124PCB-1254 Peak 1 Ave 20097124230016374PCB-1254 Peak 2 Ave 20016373834017590PCB-1254 Peak 3 Ave 20017589776013684PCB-1254 Peak 4 Ave 20013683949027505PCB-1254 Peak 5 Ave 20027504947017262PCB-1254 Peak 6 Ave 20017261880028714PCB-1254 Peak 7 Ave 20028713900074774PCB-1254 Peak 8 Ave 200747739500
FORM VI 8082
Note The m1 coefficient is the same as Ave CF for an Ave curve type
10162012Page 246 of 323