ILUNOIS ENVIRONMENTAL PROTECTIGN AGENCY

FACIUTY ANNUAL HAZARDOUS WAS1:E REPORT This rsport is for ths cslsndar year snding Oscsmbsr 31.1985 (COnL)

XVIII. COMMENTS

us EPA RECORDS CENTER REGION 5 »CiHty'S USEPA I.D. NO. Ii Li Di Oi Oi 51415 i6 i4 i3 191

527544 J aciiity's Illinois EPA I.D. No. j Oj 3j 1| 6| 5| 0| 0| 0| 0| 3|

05/JCor:>JO C ySMr(A//A. UJ/,

1) Page 2, Lines 1 and 2, T04 other thermal treatment is burning in boiler for recovery of heating value.

2) We did not do any ground water monitoring in 1985 because the Agnecy has determined that the wastewater equalization basins are not RCRA -regulated surface impoundments.

3) The Chemical Division of Sherwin-Williams was sold to PMC Specialties effective, July 1, 1985. Consequently, the figures»-on Page 2 reflect data for the first six (6) monthly only.

4) Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization certification under 3002 (b) of RCRA, I also certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and I have selected the method of treatment, storage or disposal currently available to me which minimizes the present and'future threat to human health and the environment. '

5) Our waste minimization plan includes the following:

(a) Reuse of overstock and return goods in the process. (b) Better Formulation. (c) Categorical documentation and follow-up on spoiled batches. (d) Distillation and Reclamation of Wash Solvents (1986 Program).

Page 10| 0| 3|

932644

/• •RCRA INSPECTION REPORT - INTERIM STATUS STANDARDS - TREATMENT^ STORAGE. AND DISPOSAL FACILITIES

.R)rm A General Facility Standards . . .

General Iriformatloh ^ "y -

USEPA Number: ^ ̂ LDP . Facility: YES>^ Notified As: Regulated As: A£:A): (A) :Facirity Nome: ^ •(Bystreet:^'

.. iTCi'pltV:^ ^ ' ; • (D) Stote: - (E) Zip Code: ••,(F); Phone: ' ^ (G) County:

Ope rotor: ;:

(I)StreeH ; XJlXX/ -X- ' A/JX : U) ' CI ty: ; YlX/X/)

(M) Phone:

(K) State: -r-L '(N) County:

• - (L) ZIP Code:

-

(0) Owner: . iS.^X^U/A) " LJ/XJ^I/?A%T

(P) Street: //>/

(Q) City:

(T) Phone:

(R).State: ,. /^X!' ' .(S) Zip Code"

_ (U) County: A'ujy/}AJ/>A/i

Region: /\J (V) Dote of Inspection: / / J7 / (W) Time: {?Tom)X'AAy/?ilo) XS^/n

Type of Inspection: Cl§D RECOPJD'REVIEW SAMPLING CITIZEN COMPLAINT

. CLOSED WITHDRAWAL OTHER . PARTE . ,

• . ..^ F/U / / (Dote of Initial Inspection)

(X) Vleother Conditions: SUA)/Jj/ ^

Area Section

/S7^ 7;2i-yM 7Jjr. 73)

-tj t

Class I

Class II

(AA) Preparer Information

Nome

Agency/Title

Telephone

<3J:3 - ^

TOTAL Class I's s Il's

RECEIVED

OCT 2 4 1986

IEPA-DLPO

1 PAGE REMOVEDNON-RESPONSIVE

C/1^

APPENDIX A-1 FAC LITY INSPECTION FORM FOR COMPLIANCE WITH INTERIM SIAIUS SIANDARUS COVERING GROUNDWAIbR MUNnORING~

General Information USEPA Number: lEPA Number:, Major Facility:' ̂ E^NO Notified As: r.sD Regulated As: Facility Nome: ^^

Street: ;

(•kr ex Ota City:

Phone: Aiz j fefeO'Holfe 9f State: J//.-^ <s»

County: CJOO k.

Facility Contact Official: Daryl RcvU.C'r Branch/Organization:

Title: gwvtVDrtrrtC.n4tt 1 5pf.r.f<vi»S'i^

Region: A/ Dote of Inspection: j /jjJAk. Time: (From)

Type of Inspection: @7 RR F/U / / (Date~of TnTTidrrnspectioh)

Zip Code:

(To)

Preparer Information: Nome:

Agency/Title:

XBFA- j £P<> Telephone:

^\-L j

Section

^/\/e4- iov.-|-e,4' by

7O>/'4

Type of facility: (check appropriately)

a) b) c) dl

surface impoundment landfill land treatment facility disposal waste pile*

Groundwater Monitoring Program 1. Was the groundwater monitoring program

reviewed prior to site visit? . if "NO". a) Was the groundwater program

reviewed at the facility prior to site inspection?

2. Has a groundwater monitoring program (capable of determining the facility's impact on the quality of groundwater in the uppermost aquifer underlying the facility) been Implemented? 725.190(a)

Sc>V?pe>.<"4- F

Class I

Class II

TOTAL Class I's & II's

YES NO UNKNOWN WAV I ED

'Listed separate from landfill for convenience of Identification.

IL 532-13liU IPC 195 lt/85

RECEIVED

APR . 7 1986

IEPA-DLPC

ILLINOIS ENVIRONMENTAL PROTECTION AGENCY • I

MEMORANDUM

DATE:

TO:

FROM:

March 4, 1986

Division File

Jeannine Balsamo

0316500003 - Cook County - Chicago/Sherwin-Williams SUBJECT: ILD0054565439 - Subpart F Inspection

An inspection was conducted on January 11, 1986 at the above referenced facility to inspect their groundwater monitoring program and-to further investigate the facility's contention . that they are not regulated by Subpart F Groundwater Monitoring Requirements. Present at the inspection were Gino Bruni, who also conducted an ISS inspection on this day, Caroline Panico, Cliff Gould and myself of lEPA, and Lily Herskovits of USEPA. Daryl Baker represented PMC and D.T. Rehor, Rob Martin, and Jim Baran represented Sherwin-Williams. Daryl Baker was previously employed by Sherwin-Williams and is still on contract to handle any matters^ concerning the surface impoundments. Sherwin-Williams manufacturers resins and generates such hazardous waste as wash solvent, paint waste, and still bottoms. All hazardous waste is sent for reclaiming or is sold as secondary fuel. In June, 1985, Sherwin-Williams sold 40 of their 123 acres to PMC Industries, Inc. PMC generates paracresol pitch (F004) which is used as secondary fuel, and spirit blue process residue (D002) which is landfilled.

Chemical sewers located throughout both facilities discharge caustic wastewater to the powerhouse, now located on PMC's property, where pH is adjusted. The effluent is then piped to two surface impoundments which are still located on Sherwin-Williams' property. Sherwin-Williams constructed the-impoundments, to satisfy MSD's regulations by allowing retention time for pH adjustment. The facility listed the impoundments on their initial Part A application in the belief that they would be disposing K081, wastewater treatment sludge from the production of paint, in the impoundment. K081 never became a listed waste under the RCRA regulations. There was also some concern as to whether -the impoundments received any other hazardous material as a result of spills. The facility also had been triggered into assessment on their first semi-annual sampling. The facility addressed this issue in a March 18, 1985 letter to the Agency explaining that raw materials, finished product nor other spill material had entered the sewer system or the impoundments. On June 4, 1985, Mark Haney notified the facility that the surface

RECEIVED

APR 7 1986

lEPA-DLPC IL 532-0570

EPA-90 (Rev. 6/75-20M)

Sherwin-Williams March 4, 1986 • Page 2

impoundments were not regulated, and thus the facility ceased monitoring the wells. USEPA, though, had not made a final determination regarding the sites status and monitoring was to have continued until such time. It appeared though, that Mark Haney's letter addressed only waste resulting from accidential spills at the Sherwin-Williams plant. Since these events, lEPA had discovered that other hazardous waste streams not previously mentioned, specifically, K083 and anniline, may have entered the impoundment from what is now PMC's facility. This inspection was conducted to evaluate these concerns. Upon lEPA receiving final authorization, USEPA has stopped investigating the case.

PMC is now producing alkali blue dye. Aniline, a starting material for the synthesis of many commercial dyes, is introduced to the process in the early stages. In a later stage, the alkali blue crystallizes and is filtered out for further processing. The remaining filtrate is allowed to settle, separating the lighter aniline from water. The aniline is recycled back into the process and the water is discharged to the impoundments. The facility states that any aniline that is discharged to the impoundments is a deminimus loss. By definition, the discharge of aniline would not be a deminimus loss since it is being discharged through a continuing process. PMC periodically samples the chemical drains to determine the amounts of aniline being discharged. Furthermore, MSB states that annually 8000 lbs. are discharged to the sewer after settling in the ponds. Aniline in this form, rthough, is not regulated by any RCRA or MSB regulations.

Buring the production of the alkali blue dye, a hot, blue residue is generated. The residue is quenched with water and allowed to dewater in rolloff boxes which--are placed over the chemical sewer drains. PMC refers to this residue as K083, still bottoms from the production of aniline. The facility claims that the waste is not actually K083 but is just called this for "lack of a better definition". The waste is landfilled as B002. There was some question as to whether the dewatering process was discharging K083 and/or aniline into the impoundments. Since the residue is not actually K083 and the aniline is not regulated, the dewatering process does not introduce any listed hazardous waste into the impoundments.

RECEIVED

APR "I 1986

lEPA-DLPC

Sherwin-Williams March 4, 19.86 Page 3

PMC intends on installing tanks in the future so their effluent is separate from Sherwin-Williams. Presently, Daryl Baker samples the effluent at the powerhouse daily and analyzes for BOD, pH and total solids. Seven times a month a sample is analyzed for COD and TOC. In the future, sampling stations will be installed for further analysis of the chemical sewers. The monitor wells were last sampled in February," 1985 but the results were never submitted to the Agency. Mr. Baker stated that the facility became "annoyed" with the Agency after its denial of their assessment plan and decided at that time to withdraw the impoundments. The impoundments were last emptied in 1981 and tlie sludge was landfilled as non-hazardous.

An old landfill is located on the southeast portion of the Sherwin-Williams property. Wells W-4, W-5, W-6 and W-7 monitor the landfill for non-RCRA purposes. One set of analytical data for these wells was submitted to the Agency on December 20, 1984 and shows above standard levels for many of the drinking water and groundwater quality parameters. In the future, the landfill may be a potential source of groundwater contamination.

In conclusion, the wastes generated by Sherwin-Williams and PMC which are treated and discharged into the surface impoundment are not regulated, therefore, the facilities are not subject to Subpart F requirements.

JB:pgb:2065P

cc: Northern Region Mark Haney Jeannine Balsamo

RECEIVED

APR V 1986

lEPA-DLPC

WAT^f^ \ R.efiTli£HT^ S CHICASO^ I i-i-.

YlclL UCC^TlOl^J V/f,

Tz-o^e/-

P/^C S'-rgcAVI ^ Qt.oMg

- (5.fe404 - 0.182.0 .1

G) - o.ns"9 " (2> - O.0 306. " eg) - 0.3041 " <5) - O ,Ol.HD "

1. 4 fa 1-"1-

«7CAi-ri l"v 590^

ruAOA^T-gg. o»= s-ragAM RECEIVED .

APR 7 1986 lEPA-DLPC '•

— S>MiTAg>< WAST.? i MOM-Process V*ASTCWAT.?«

— ^oepAC-^ &RA.MA6^

S-tr9^

•1 . m •

-i

n

• •"oSflsoafl

fdffia" CiD'k-'^;

liMtii' 1^''-'

v;^V:

HBi

r "Q[^v m i; H Li^, .LATD^

IsJ

-MpBr.

Q^Q

®

Vi^;i

(D

©

- o o »z

_J CM3

0>l'

.V

1

I i <

>« ..... n |n

V- ;

3M3a£3^

•• '•? ;^i

•ir

RECEIVED

;\PR 7 1986

IEPA-DLPO

4140 LITT DRIVE » Phone 312/544-3260 . HILLSIDE, ILLINOIS 60162 IMLF.

Shervin Williams Company Attn: Mr* R* Benson 11541 South Champlain Avenue Chicago, Illinois 606Z8

Sample Reed.. 6/20/80

/S>-D P.O. Mn C 58851

Source.

SAMPLE INFORMATION

#6173 - Pond Sludge Sample 83-1 6/20/80

_ Tests Completed

Comments.

Sampling Method: By Client. By Sub. Lab..

ANALYSIS Serco Auto-Sampler. Other.

6173 6173 Total Solids /O 37.87 ,CK> i>i>/ Nitrogen-Tot mg/l

Fix. Tot. Sol. mg/l Nitrogen-Amm mg/l

Vol. Tot. Sol. mg/l Nilrogen-Org mg/l

Diss. Solids mg/l Nitrite mg/l

Settle. Sol. ml/1 Nitrate mg/l - :• Tot. 5-js. Sol. mg/l Phosphotc (Total) mg/l

Fix. 5.,s. Sol. mg/l Phosphote (Drtho) mg/l ' Vol. S-js. Sol. mg/l Sulfate mg/l

33.3 . Sulfide mg/l

mg/l Sulfite mg/l

COD mg/l Aluminum mg/l

DO mg/l Antimony mg/l

Moisture % 62.13 Arseni c ppm XC^XX 0.129 /?>' Phenols og/l Borium ppm 32.0 ABS or LAS mg/l Beryllium mg/l

Oils & Greoses mg/l Boron mg/l

-r ppm xa$xx U.b> »•>- u Tot. Boct. Cells.'^lOO ml [ jAlcium mg/l

Tot. Coli. Cells/100 ml f sf/ f Chrom-Totol ppm XHsXX 27.6 -73 -iZ- r/;S

Fecal Coli. Cells/lOO ml r

Chrom-Hex. mg/l

Inorganic or /O 92.5 b' Chrom-Tri. mg/l •

pH lU.U Copper ppm WK 1.3U 3--fv f : 3».

Spec. Cond. Iron mg/l

Alholinity a 1U.30 Leod ppm mg/l 11.i 9 50 Acidity ppm O.U • Lithium mg/l

Tot. Herd, mg/l os CaC03 Magnesium mg/l

Resid. CI 2 mg/l Manganese mg/l

Bromide mg/l Mercury ppb X^XX f_ 1.0 Chloride mg/l Nickel ppm 10.3 J7 z'i f3 Fluoride mg/l Potassium mg/l

Cycnide- Totol ppm L 0.003 Silver ppm mg/l L D.IO <.>t^ •I-. « .J

Cyonide-Free mg/l Sodium mg/l

Selenium pom 0.514 /.5«. Strontium mg/l

Flash Point "F 212 Tin . mg/l • i rqanic % 7.5 Zinc ppm Xi^XX 2.24 />o . 4-

Our methods are in accordance^

ANALYSIS CERTIFIED BY:

th Association, Standard Methods 14th Edition. RECEIVED

Director n»t*- 7/2/80 den

DUPLICATE COPY

APR ? 1986

IEPA-DLPC

SALES COPE

A \oo^x SPECIAL WASTE ANALYSIS REPORT LABORATORY: Chsmical Waste Management of Ihinoio WASTE PROFILE SHEET CODE^

PROFILE SHEET RECEIVED ON: REPRESENTATIVE SAMPLE RECEIVED ON:

CERTIFICATE OF REP. SAMPLE RECEIVED: SAMPLE TAKEN: H

PROPOSED TREATMENT/DISPOSAL FACILITY: CH 1 C.^ lb i DATE OF ANALYSIS;

THE ANALYSES BELOW REPORTED WERE SELECTED BY ME. BASED UPON THE GENERATOR'S REPRESENTATIONS IN THE PROFILE SHEET AND ANY APPLICABLE WASTE ANALYSIS PLAN ESTAB­LISHED BY THE PROPOSED FACILITY FOR WASTE OF THIS TYPE. ANALYSE.? REQUIRED BY A WASTE ANALYSIS PLAN ARE INDICATED BY AN ASTERISK ( * ).

LAB MANAGER;. Ajsam^

Test As Received Cea^'ad Analyst

Initials

. If.-

Test As Received Leachate

Analyst Initials

Specific Gravity 1

PH T2 Acidity. ^ as Alkalinity. % as Phenols, mg/l

COD. mg/l Cyanides, as CN, Total, mg/l ^//xn B 0 Of. mg/l 1

Cyanides, as CN, Free, mg/l Total Solids @ 10S*C Total Dissolved Solids, mg/l Nitrogen, Ammonia, as N. mg/l / Total Suspended Solids, mg/l

1 z

8

1 O

z

Residue on Evaporation @ IBO'C Total Kjeldahl Nitrogen, as N. mg/l 1

Flash Point. F* TP Total Alkalinity (P). as CaCOi. mg/l Ash Content, on ignition -TP- Total Alkalinity (M). as CSCOJ, mg/l Heating Valve. BTU/lb Total Hardness, as CaCO^ mg/l -Acid Scrub." gNaOH/g Calcium Hardness, as CaCOi. mg/l

Magnesium Hardness, as CaCOi, mg.'l Arsenic, as AS. mg/l 1.0 Barium, as Ba. mg/l 90.Q Boron, as Bi. mg/l Oil and Grease; mg/l Cadmium, as Cd. mg/l f.Q Chromium. Total as Cr. mg/I I.O Hexavalent Chromium @ Cr. mg/l Aldrin. mg/l Copper, as Cu..mg/I /3.0 KK Chlordane. mg/l Iron. Total as Fe. mg/l DDTs. mg/l

Iron, dissolved, as Fe. mg/l Dieldrin. mg/l Lead, as Pb. mg/l /<!.0 RK Endrin. mg/l Manganese, as Mn. mg/l Heptachlor. mg/l Magnesium, as Mg, mg/l Lindane, mg/l

Mercury, as Hg. pP ft ^100. N Methoxychlor. mg/l Nickel, as Ni. mg/l WO.O < Toxaphene. mg/l r-ir-/-^r-i» /r n Selenium, as Se. mg/l ^I.O p Parathioa mg/l IvLULI i/t u Silver, as Ag. mg/l ZI.O 2. 4. D. mg/l Zinc, as Zn. mg/l 2. 4. S. TP (Silvex). mg/l 1 l\PR 7 1 386 "

PCB's. mg/l IhPA-DL :Q

Bicarbonates. as HCOi. mg/l Carbonates, as CO.i. mg/l Chlorides, as CI. mg/l Fluorides, as F. mg/l Nitrate, as NO ., mg/l TF

djbsnsfil :,qn:.jlio.n j.'efenssa

Nitrite, as NO.. mg/| ij rcpori TTTrrTZfic • *.0 :=v5 o:s ar djbsnsfil

:,qn:.jlio.n j.'efenssa

Phosphate, as P. mg/l or . i-'a repr: djbsnsfil :,qn:.jlio.n j.'efenssa Sulfate, as SO. mg. i J i-.x.p e V.,: jiiy cr un-: -C.'l 3ZCi. •-C/ or corr

djbsnsfil :,qn:.jlio.n j.'efenssa

Sulfides, as S. ma l/Bf^</)H/C^"^ Z/1 o -7-3- |ii«reby ir.acc la anu «•: a- -

CWM #5525

liw Appncation lenawaV _X_ iddltlonal Site

801672 ILLINOIS ENVIRONHEMTAL PROTECTION AGENCY DIVISION OF LAND/NOISE POLLUTION CONTROL

SPECIAL WASTE DISPOSAL APPLICATION

FOR AGENCY USE Log «_

THIS APPLICATION FOR HASTE: Treatment Disposal Storage

;ARD YPE DATE LPiiii AUTHORIZATION NUMBER ^

" i i • W HASTE HAULER

TRANS CODE

TT

DATE ENTERED (Agency Use)

14 HAULER REGISTRATION NUMBER _0_0J_9_ 21 24

ADDRESS R.R'. #1. Box 147

rniiMTY Will STATE II .

NAME Great Lake Disposal

COMMUNITY Crete

ZIP gfW7 AREA 312 TELEPHONE 758 7100

0

lASTE GENERATOR TBENEWmW

CODE ^ J. 1_6__0^^0_2_0__G NAME Sherviin Williams 25

ADDRESS

COUNTY

11541 Chgmplain COMMUNITY Chicago

Cook STATE II. _ ZIP 60628 AREA CODE 312 TELEPHONE 821 3028

GENERATOR CONTACT NAME ^tan Frvzel

DUNS NUMBER SIC CODE 2865 USEPA GEN. CODE

PROCESS NAME i i_t_l_i_n_g_&_E_g_u_a J. i. 2La_t_ijpjn _A_f_t_eTi_S_1_t^ _S_ejsf age Is treated.with-lime Ift^p&utraLlz^ed any acid prese "

GENERIC WASTE NAME ^ jB ̂ tl_ijl _g._P_OJl ̂ _S_1_U ̂ £.e_

lUPAC WASTE NAME 61 80

IT-TOTAL Am'AL HASTE VOLUME ;_5_p_o^

51 60

TRANSPORT FREQUENCY _3 WASTE CLASS 63 (Agency Use) 64 es

1 • ONE TIME 5 = MONTHLY 2 • DAILY 6 » BI-MONTHLY 3 • WEEKLY 7 - QUARTERLY 4 - BI-WEEKLY 8 ° SEMI-ANNUALLY

VOLUME UNITS 1_

1 = CUBIC YARDS' 2 = GALLONS

HASTE PHASE

1 =• SOLID 2 » SEMI-SOLID 3 - LIQUID 4 « GAS

SO

_2 S2

(Code either "1" for Low, "2" for Medium, or "B" for High as appropriate for columns 21 through 26):

INFECTIOUS INHAUTION , DERMAL TOXICITY TOXICITY /

FLASH POINT _ 27 30 .

IN6ESTIVE , TOXICITY I

a "ST ALPHA RADIATION (pC1/L)

"ST ^ 36

RECEIVED

7 1986-REACTIVITY EXPLOSIVE

35 - /3S"D COMPOSITION 2-

1 = ORGANIC 'EPA-DLPC ? = INORGANIC

PERCENT ACIDITY

PERCENT • TOTAL

40

PERCENT - ^ ^ TOTAL ^ ^ ̂ r ALKALINITY . pH Y SOLIDS J? C . S /

"Xi "XT "XX" — 46 XT •- — — tr •»-.

PERCENT KEY COMPONENT NAME "ITRCENT KEY COMPONENT NAME

Z?.-,! 4 ^LUi>.i.BssuiS 4 ^lietJOLic.s>. 4 ,

70 71

43 44 47 48 40 70 71

WEPA HAZARDOUS HASTE NO. (If Hazardous) '

)H udGce9>' .copIedr-loen^^^^^pSG^^dhrecNy or IndirecHy-iw-whole'-orirrporlrnoT'Ofed.^

CARD' nPE DATE L P S H C AUTHORIZATION NUMBER _

T 6 8

TRANS • CODE

IT 14

EP WASTE CHARACTERISTICS

• V'". • ;—«•> , DATE ENTERED ' . 'i -(Agency Use) / ;.

• .i.;.

EP • • -METAL KEY

cri 21

Ag

As ,

Ba ,

Cd.

Cr

PHENOL

23 .uTl .uo_ ie-^.

38

ENDRIN

LINDANE

METHOXYCHLOR

cu —Zt-Q 39 41 48 49 56

Hg __0.J

Ni .

Pb Ito Se _1 LQ zn ii.g s- 4,0 2-40 ^

2.4.5 - TP

TOXAPHENE

LABORATORY NAME j:h8mical>^st£.ManagemeilQLIEn5!l^ 81 40

CERTIFICATION NUMBER REVIEWED BY: / •1 ^ 50 61 I 83 64 56

J_ SITE CODE SITE NAME CLU.'i d «I-A\ / C. I i>» 21 22 29 or—I

DISPOSAL METHOD O J. NEUTRALIZATION METHOD 30 31 32 33

SIGNATURE SIGNATURE (SITE OWNER) (SITE

t-8'Slf 1 i •» 1 * S g g g-s ^° = Sz

STATUS 34

START DATE / _/ 35 36 37 38 39 40

EXPIRATION DATE / / 41 42 43 44 45 46

21

SITE CODE 22 w SITE NAME

« r- O ja n ^ o-

Q.^ T3 o O- ' p « s ̂ e -

J: — fii

II f .^ 3 "S e t &£ e E:^ =

DISPOSAL METHOD

SIGNATURE 30 31

NEUTRALIZATION METHOD. 32-33

SIGNATURE (SITE OWNER) TsiTE OPERATOR)

STATUS START DATE TS"SS ^ TTTTS"^ SIT'TO"

EXPIRATION DATE TI" ir ^ TT 7T ' TTW

_3^ 21 22

SITE CODE

DISPOSAL i-ETHOD

SIGNATURE

ilTE NAME 29

atr^r NEUTRALIZATION METHOD

^ST B3" SIGNATURE

(SITE OWNER) (SITE OPERATOR)

STATUS •ST

START DATE ST 36 ^ 37 38 ^ 39 40

EXPIRATION DATE / / __ 41 42 43 44 45 46

4 IT

SITE CODE 2r —

DISPOSAL METHOD • 29"

SITE NAME

SIGNATURE-. 30 31

NEUTRALIZATION METHOD 32 33

SIGNATURE :(SITE OWNER)

RECEIVED

"AFR TTO"

lEPA-DLPC (.SITE OPERATOR)

0» 41 — tn

.r >• r • ® o .2

f i' 5 111 Unii s. o -= «

•St- u f O /. L I

p ». C 4; t M J* • « -ii -5; N- u „

-T-s = - s 5 e* ?! .1 ^ t liili - S C ®- c fi? ^ ^ 3 S wl* S J '

s -

STATUS . ^ START DATE / / EXPIRATION DATE 34 35 36 37 38 39 40

/ / 41 49 49 •-

n E i5 > -S 5

La^^^ories, Inc. P.O. Box 686 Caton Farm Road

Joliet, Illinois 60434 Telephone 815 727-5436 312 454-0245

Telex 723421 OAR JOL

TABLE NO. 1

REVISED REPORT

Analysis of Monitor Wells for

Sherwin Williams Company

Parameter G102 GlOl G108 G109 91835 91836 91837 91838

Formaldehyde, mg/1 0.2 0.47 ,<0.1 0.35 Phenol, mg/1 0.024 0.012 0.014 0.612 Vanadium, mg/1 <0.2 <0.2 <0.2 <0.2 Acrylonitrile, mg/1 <0.005 <0.005 <0.005 <0.005 Aniline, mg/1 <0.01 <0.01 <0.01 <0.01 Benzonitrile, mg/1 <0.005 <0.005 <0.005 <0.005 Cresols, mg/1 <0.005 <0.005 <0.005 0.25 o-Dichlorobenzene, mg/1 <0.005 <0.005 <0.005 <0.005 Dibutylphthalate, mg/1 <0.01 <0.01 <0.01 <0.01 Phthalic Anhydride, mg/1 <0.01 <0.01 <0.01 <0.01 Toluene, mg/1 <0.01 <0.01 <0.01 <0.01 Xylene, mg/1 <0.01 <0.01 <0.01 <0.01 Diphenylamine, mg/1 <0.01 <0.01 <0.01 <0.01 Ethylbenzene, mg/1 <0.01 <0.01 <0.01 <0.01

Methods of Analysis

Formaldehyde - Distillation - Colorimetric Analysis Phenol - Disti^ation - Colorimetric Analysis Vanadium - Atomic Absorption Organics - GC/mass Spec. D. P

MAR 111985

RECEIVED

APR 7 1986 lEPA-DLPC