illinois environmental protection agency laboratory

31
INDIAN CREEK LANDFILL #2 Illinois Environmental Protection Agency Laboratory LABORATORY RESULTS 825 N. Rutledge Springfield, Illinois 62702 217.782.9780 Funding Code: LP43 Project/Facility Number: 1790305011 Name: Date Received : 02/13/18 Trip ID: Visit Number: Temperature C: 7.00 Date/Time Collected: Matrix: Water G18DT Client Sample ID: Lab Sample ID: 18B0280-01 Sample Type: 02/13/18 10:20 Sample Depth: Total Depth: JT Collected By: Cyanide by EPA Method 335.4 Analyte Result Reporting Limit Regulatory Level Qualifier Analyzed: Method: 335.4 Units: mg/L 02/15/18 09:11 Prepared: 02/15/18 14:49 ND Cyanide 0.005 pH Analyte Result Reporting Limit Regulatory Level Qualifier Analyzed: Method: SM 4500H+B Units: PH 02/15/18 12:13 Prepared: 02/15/18 12:17 7.4 Laboratory pH 0.1 Q Specific Conductance by Standard Method 2510B Analyte Result Reporting Limit Regulatory Level Qualifier Analyzed: Method: 2510B Units: µmho/cm @ 25.0 °C 02/27/18 09:56 Prepared: 02/27/18 10:57 678.00 Specific Conductance 10.00 Page 1 of 31 Reported: 03/06/18 12:56 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Test results meet all requirements of NELAC (accredited by Florida DOH #E37645). If you have any questions about this report, please contact Tom Weiss, Laboratory Manager, at 217.782.9780.

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INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DTClient Sample ID: Lab Sample ID: 18B0280-01

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Cyanide by EPA Method 335.4

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 335.4

Units: mg/L

02/15/18 09:11Prepared:

02/15/18 14:49

NDCyanide 0.005

pH

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SM 4500H+B

Units: PH

02/15/18 12:13Prepared:

02/15/18 12:17

7.4Laboratory pH 0.1Q

Specific Conductance by Standard Method 2510B

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2510B

Units: µmho/cm @ 25.0 °C

02/27/18 09:56Prepared:

02/27/18 10:57

678.00Specific Conductance 10.00

Page 1 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DTClient Sample ID: Lab Sample ID: 18B0280-01

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Total Dissolved Solids, Gravimetric, Dried at 180oC by Std. Method 2540C

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2540C

Units: mg/L

02/14/18 16:15Prepared:

02/14/18 16:15

362Total Dissolved Solids 10

Page 2 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DDClient Sample ID: Lab Sample ID: 18B0280-02

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Chloride by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: EPA 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 12:44

2.56Chloride 1.00

Mercury by EPA Method 7470

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 7470

Units: ug/L

02/20/18 15:26Prepared:

02/23/18 10:01

NDMercury 0.06

Metals by EPA 6000/7000 Series Methods

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 6020

Units: ug/L

02/20/18 10:32Prepared:

02/26/18 11:02

NDAntimony 2.00

118Arsenic 0.50

NDLead 5.00

NDSelenium 2.00

NDThallium 2.00

Page 3 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DDClient Sample ID: Lab Sample ID: 18B0280-02

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Metals (Minerals) by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: mg/L

02/20/18 15:21Prepared:

02/27/18 11:11

63.0Calcium 0.30 100000

312Hardness 1.98

37.5Magnesium 0.30 100000

1.98Potassium 1.40 100000

21.1Sodium 0.30

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:11

NDAluminum 60.0 40000

111Barium 5.00

NDBeryllium 1.00

197Boron 10.0

NDCadmium 3.00

NDChromium 5.00

NDCobalt 10.0

NDCopper 10.0

2690Iron 50.0 40000

NDManganese 15.0

NDNickel 5.00

Page 4 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DDClient Sample ID: Lab Sample ID: 18B0280-02

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:11

NDSilver 3.00

429Strontium 5.00

NDVanadium 5.00

NDZinc 25.0

Nitrate-Nitrite, Colorimetric, Automated Cadmium by EPA Method 353.2

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 353.2

Units: mg/L

02/15/18 11:01Prepared:

02/15/18 13:01

NDNitrogen, Nitrite (NO2) + Nitrate (NO3) as N 0.100

Nitrogen, Ammonia, Colorimetric, Automated Phenate by EPA Method 350.1

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 350.1

Units: mg/L

02/15/18 14:21Prepared:

02/15/18 14:21

5.15Ammonia as N 0.10

Page 5 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G18DDClient Sample ID: Lab Sample ID: 18B0280-02

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Sulfate by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 12:44

NDSulfate 10.0

Page 6 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DTClient Sample ID: Lab Sample ID: 18B0280-03

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Cyanide by EPA Method 335.4

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 335.4

Units: mg/L

02/15/18 09:11Prepared:

02/15/18 14:50

NDCyanide 0.005J3

pH

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SM 4500H+B

Units: PH

02/15/18 12:13Prepared:

02/15/18 12:17

7.3Laboratory pH 0.1Q

Specific Conductance by Standard Method 2510B

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2510B

Units: µmho/cm @ 25.0 °C

02/27/18 09:56Prepared:

02/27/18 10:57

761.00Specific Conductance 10.00

Page 7 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DTClient Sample ID: Lab Sample ID: 18B0280-03

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Total Dissolved Solids, Gravimetric, Dried at 180oC by Std. Method 2540C

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2540C

Units: mg/L

02/14/18 16:15Prepared:

02/14/18 16:15

412Total Dissolved Solids 10

Page 8 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DDClient Sample ID: Lab Sample ID: 18B0280-04

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Chloride by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: EPA 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 12:54

2.73Chloride 1.00

Mercury by EPA Method 7470

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 7470

Units: ug/L

02/20/18 15:26Prepared:

02/23/18 10:01

NDMercury 0.06

Metals by EPA 6000/7000 Series Methods

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 6020

Units: ug/L

02/20/18 10:32Prepared:

02/26/18 11:06

NDAntimony 2.00

36.9Arsenic 0.50

NDLead 5.00

NDSelenium 2.00

NDThallium 2.00

Page 9 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DDClient Sample ID: Lab Sample ID: 18B0280-04

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Metals (Minerals) by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: mg/L

02/20/18 15:21Prepared:

02/27/18 11:14

74.1Calcium 0.30 100000

354Hardness 1.98

41.1Magnesium 0.30 100000

1.70Potassium 1.40 100000

22.1Sodium 0.30

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:14

NDAluminum 60.0 40000

118Barium 5.00

NDBeryllium 1.00

186Boron 10.0

NDCadmium 3.00

NDChromium 5.00

NDCobalt 10.0

NDCopper 10.0

3090Iron 50.0 40000

19.1Manganese 15.0

NDNickel 5.00

Page 10 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DDClient Sample ID: Lab Sample ID: 18B0280-04

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:14

NDSilver 3.00

470Strontium 5.00

NDVanadium 5.00

NDZinc 25.0

Nitrate-Nitrite, Colorimetric, Automated Cadmium by EPA Method 353.2

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 353.2

Units: mg/L

02/15/18 11:01Prepared:

02/15/18 13:02

NDNitrogen, Nitrite (NO2) + Nitrate (NO3) as N 0.100

Nitrogen, Ammonia, Colorimetric, Automated Phenate by EPA Method 350.1

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 350.1

Units: mg/L

02/15/18 14:25Prepared:

02/15/18 14:25

3.76Ammonia as N 0.10

Page 11 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G30DDClient Sample ID: Lab Sample ID: 18B0280-04

Sample Type:

02/13/18 11:15

Sample Depth: Total Depth:

JT Collected By:

Sulfate by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 12:54

NDSulfate 10.0

Page 12 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DTClient Sample ID: Lab Sample ID: 18B0280-05

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Cyanide by EPA Method 335.4

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 335.4

Units: mg/L

02/15/18 09:11Prepared:

02/15/18 14:52

NDCyanide 0.005

pH

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SM 4500H+B

Units: PH

02/15/18 12:13Prepared:

02/15/18 12:17

7.2Laboratory pH 0.1Q

Specific Conductance by Standard Method 2510B

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2510B

Units: µmho/cm @ 25.0 °C

02/27/18 09:56Prepared:

02/27/18 10:57

842.00Specific Conductance 10.00

Page 13 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DTClient Sample ID: Lab Sample ID: 18B0280-05

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Total Dissolved Solids, Gravimetric, Dried at 180oC by Std. Method 2540C

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2540C

Units: mg/L

02/14/18 16:15Prepared:

02/14/18 16:15

476Total Dissolved Solids 10

Page 14 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DDClient Sample ID: Lab Sample ID: 18B0280-06

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Chloride by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: EPA 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:04

1.90Chloride 1.00

Mercury by EPA Method 7470

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 7470

Units: ug/L

02/20/18 15:26Prepared:

02/23/18 10:01

NDMercury 0.06

Metals by EPA 6000/7000 Series Methods

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 6020

Units: ug/L

02/20/18 10:32Prepared:

02/26/18 11:09

NDAntimony 2.00

2.33Arsenic 0.50

NDLead 5.00

NDSelenium 2.00

NDThallium 2.00

Page 15 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DDClient Sample ID: Lab Sample ID: 18B0280-06

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Metals (Minerals) by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: mg/L

02/20/18 15:21Prepared:

02/27/18 11:17

93.2Calcium 0.30 100000

424Hardness 1.98

46.4Magnesium 0.30 100000

1.86Potassium 1.40 100000J3

22.4Sodium 0.30

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:17

NDAluminum 60.0 40000

178Barium 5.00

NDBeryllium 1.00

195Boron 10.0

NDCadmium 3.00

NDChromium 5.00

NDCobalt 10.0

NDCopper 10.0

4260Iron 50.0 40000

30.1Manganese 15.0

NDNickel 5.00

Page 16 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DDClient Sample ID: Lab Sample ID: 18B0280-06

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:17

NDSilver 3.00

522Strontium 5.00

NDVanadium 5.00

NDZinc 25.0

Nitrate-Nitrite, Colorimetric, Automated Cadmium by EPA Method 353.2

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 353.2

Units: mg/L

02/15/18 11:01Prepared:

02/15/18 13:03

NDNitrogen, Nitrite (NO2) + Nitrate (NO3) as N 0.100

Nitrogen, Ammonia, Colorimetric, Automated Phenate by EPA Method 350.1

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 350.1

Units: mg/L

02/15/18 14:28Prepared:

02/15/18 14:28

2.36Ammonia as N 0.10

Page 17 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

R31DDClient Sample ID: Lab Sample ID: 18B0280-06

Sample Type:

02/13/18 11:55

Sample Depth: Total Depth:

JT Collected By:

Sulfate by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:04

NDSulfate 10.0

Page 18 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DTClient Sample ID: Lab Sample ID: 18B0280-07

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Cyanide by EPA Method 335.4

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 335.4

Units: mg/L

02/15/18 09:11Prepared:

02/15/18 14:53

NDCyanide 0.005

pH

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SM 4500H+B

Units: PH

02/15/18 12:13Prepared:

02/15/18 12:17

7.0Laboratory pH 0.1Q

Specific Conductance by Standard Method 2510B

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2510B

Units: µmho/cm @ 25.0 °C

02/27/18 09:56Prepared:

02/27/18 10:57

886.00Specific Conductance 10.00

Page 19 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DTClient Sample ID: Lab Sample ID: 18B0280-07

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Total Dissolved Solids, Gravimetric, Dried at 180oC by Std. Method 2540C

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2540C

Units: mg/L

02/14/18 16:15Prepared:

02/14/18 16:15

496Total Dissolved Solids 10

Page 20 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DDClient Sample ID: Lab Sample ID: 18B0280-08

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Chloride by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: EPA 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:13

1.62Chloride 1.00

Mercury by EPA Method 7470

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 7470

Units: ug/L

02/20/18 15:26Prepared:

02/23/18 10:01

NDMercury 0.06

Metals by EPA 6000/7000 Series Methods

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 6020

Units: ug/L

02/20/18 10:32Prepared:

02/26/18 11:12

NDAntimony 2.00

16.1Arsenic 0.50

NDLead 5.00

NDSelenium 2.00

NDThallium 2.00

Page 21 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DDClient Sample ID: Lab Sample ID: 18B0280-08

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Metals (Minerals) by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: mg/L

02/20/18 15:21Prepared:

02/27/18 11:20

107Calcium 0.30 100000

443Hardness 1.98

42.3Magnesium 0.30 100000

1.44Potassium 1.40 100000I

20.7Sodium 0.30I

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:20

NDAluminum 60.0 40000

200Barium 5.00

NDBeryllium 1.00

199Boron 10.0

NDCadmium 3.00

NDChromium 5.00

NDCobalt 10.0

NDCopper 10.0

4190Iron 50.0 40000

50.0Manganese 15.0

NDNickel 5.00

Page 22 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DDClient Sample ID: Lab Sample ID: 18B0280-08

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:20

NDSilver 3.00

444Strontium 5.00

NDVanadium 5.00

NDZinc 25.0

Nitrate-Nitrite, Colorimetric, Automated Cadmium by EPA Method 353.2

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 353.2

Units: mg/L

02/15/18 11:01Prepared:

02/15/18 13:04

NDNitrogen, Nitrite (NO2) + Nitrate (NO3) as N 0.100

Nitrogen, Ammonia, Colorimetric, Automated Phenate by EPA Method 350.1

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 350.1

Units: mg/L

02/15/18 14:32Prepared:

02/15/18 14:32

2.15Ammonia as N 0.10

Page 23 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G32DDClient Sample ID: Lab Sample ID: 18B0280-08

Sample Type:

02/13/18 12:25

Sample Depth: Total Depth:

JT Collected By:

Sulfate by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:13

NDSulfate 10.0

Page 24 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DTClient Sample ID: Lab Sample ID: 18B0280-09

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Cyanide by EPA Method 335.4

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 335.4

Units: mg/L

02/15/18 09:11Prepared:

02/15/18 14:54

NDCyanide 0.005

pH

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SM 4500H+B

Units: PH

02/15/18 12:13Prepared:

02/15/18 12:17

7.4Laboratory pH 0.1Q

Specific Conductance by Standard Method 2510B

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2510B

Units: µmho/cm @ 25.0 °C

02/27/18 09:56Prepared:

02/27/18 10:57

683.00Specific Conductance 10.00

Page 25 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DTClient Sample ID: Lab Sample ID: 18B0280-09

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Total Dissolved Solids, Gravimetric, Dried at 180oC by Std. Method 2540C

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 2540C

Units: mg/L

02/14/18 16:15Prepared:

02/14/18 16:15

366Total Dissolved Solids 10

Page 26 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DDClient Sample ID: Lab Sample ID: 18B0280-10

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Chloride by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: EPA 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:42

2.57Chloride 1.00

Mercury by EPA Method 7470

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 7470

Units: ug/L

02/20/18 15:26Prepared:

02/23/18 10:01

NDMercury 0.06

Metals by EPA 6000/7000 Series Methods

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 6020

Units: ug/L

02/20/18 10:32Prepared:

02/26/18 11:15

NDAntimony 2.00

120Arsenic 0.50

NDLead 5.00

NDSelenium 2.00

NDThallium 2.00

Page 27 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DDClient Sample ID: Lab Sample ID: 18B0280-10

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Metals (Minerals) by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: mg/L

02/20/18 15:21Prepared:

02/27/18 11:23

64.5Calcium 0.30 100000

319Hardness 1.98

38.5Magnesium 0.30 100000

1.99Potassium 1.40 100000

21.4Sodium 0.30

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:23

132Aluminum 60.0 40000

113Barium 5.00

NDBeryllium 1.00

202Boron 10.0

NDCadmium 3.00

NDChromium 5.00

NDCobalt 10.0

NDCopper 10.0

2730Iron 50.0 40000

NDManganese 15.0

NDNickel 5.00

Page 28 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DDClient Sample ID: Lab Sample ID: 18B0280-10

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Metals by EPA Method 6010 - ICP

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: SW-846 6010

Units: ug/L

02/20/18 15:21Prepared:

02/27/18 11:23

NDSilver 3.00

437Strontium 5.00

NDVanadium 5.00

NDZinc 25.0

Nitrate-Nitrite, Colorimetric, Automated Cadmium by EPA Method 353.2

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 353.2

Units: mg/L

02/15/18 11:01Prepared:

02/15/18 13:06

NDNitrogen, Nitrite (NO2) + Nitrate (NO3) as N 0.100

Nitrogen, Ammonia, Colorimetric, Automated Phenate by EPA Method 350.1

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 350.1

Units: mg/L

02/15/18 14:35Prepared:

02/15/18 14:35

5.38Ammonia as N 0.10

Page 29 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Date/Time Collected:Matrix: Water

G90DDClient Sample ID: Lab Sample ID: 18B0280-10

Sample Type:

02/13/18 10:20

Sample Depth: Total Depth:

JT Collected By:

Sulfate by Ion Chromatography 300.0

Analyte Result Reporting Limit Regulatory LevelQualifier

Analyzed:

Method: 300.0

Units: mg/L

02/14/18 07:44Prepared:

02/14/18 13:42

NDSulfate 10.0

Page 30 of 31

Reported:

03/06/18 12:56

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.

INDIAN CREEK LANDFILL #2

Illinois Environmental Protection Agency Laboratory

LABORATORY RESULTS

825 N. Rutledge Springfield, Illinois 62702 217.782.9780

Funding Code: LP43

Project/Facility Number: 1790305011

Name:

Date Received : 02/13/18

Trip ID:

Visit Number:

Temperature C: 7.00

Notes and Definitions

Q Maximum holding time exceeded.

J3 The reported value failed to meet the established quality control criteria for either precision or accuracy possibly due to matrix

effects.

I See Case Narrative for more information.

Analyte NOT DETECTED at or above the reporting limitND

* Non-NELAP accredited

Metals: 18B0280-08 Client Matrix Assessment- sample failed method dilution test for Sodium and post spike test for Potassium, indicating

probable matrix interference.

Page 31 of 31

Reported:

03/06/18 12:56

Report Authorized by:

The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety. Test results meet all requirements of NELAC (accredited by Florida

DOH #E37645). If you have any questions about this report, please contact

Tom Weiss, Laboratory Manager, at 217.782.9780.