icp test report certification packet/media/electronics...jul 28, 2011 · hitachi chemical dupont...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: TVS Array for ESD Protection Product #: SP1007-01WTG Issue Date: July 28, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

Global EHS Engineer

(1) Parts, sub-materials and unit parts

This document covers the TVS Array for ESD Protection RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 HD-4100 Polyimide 3-19 2 N/A Sputter Titanium 20-24 3 N/A Sputter Copper 25-30 4 N/A Plating Cu-Copper Sulfate 31-36 5 N/A Plating Sn 37-42

No. : CEnO11l24U3 Date : 2011/03/03 Page: I of 17

Validi nownFOr (JUePleas€ C ith scs

|lt[ta|||||rrrrIlHITACHI CHEMICAL DUPONT I/|ICROSYSTEMS250 CHEESEQUAKE ROAD-8LDG.424, PARLIN, NJ 08859-1241

Test Report

Sample DesciptionStyle/ltem No.Sample Receiving DateTesting Period

Thefollowing sample(s) was/werc submitted and identified by/on behalfofthe client a3:

POLYIIUIDEHD410020 t1toz24201 1 t0224 10 201 I t03t03

Tert Result(sl : Please refor to next page(s).

61t lered Ds red rcFn wid 6 GcomFry Fl!J;!::iit ' n.*f' )l il l; -ilrl,l . ii . r' |, i ' i*,.1 li - I lrr;+'il ' ',1: fU h'!iTh3fumdts6suedbvlh6comFn}su6]edbGcm€condltr3ois

d66, f 5ny Ihe Conp:ny s e e rsp.ilb ry ts ro 6 cr 6^r and Ii6 do@mrtu,'Lcibadd oaoGund6lbra mdbeBpdud.x6pr'niu.wrtuu

!hds rE rzo iqN f l . )E ro r ybwr / r r ] L . r : , : ; j r . $ r i ' r 14 r s610n2e t7e t+e l0 r )2e t i 7w@s!@n

Sgdfra||td

chdnLra L.bor.b.t- tllb.,

MembnorLh€scsG'o!p(5Gs5A1

scqTest Report No. I CE/2011/24843 Date: 2011/03/03 paae | 2of 17HITACHI CHEMICAL DUPONT MICROSYSTEMS250 CHEESEOUAKE ROAD-BLDG.424, PARLIN, NJ 08859-1241

Tost Resultls)PART NAME No.1 LT.BROWN LIQUID

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To€t ltem (s): Unit Method MDL ResultNo.1

(jadmrum (Cd) mg/(g with reference to lEc 62321: 2009€ndperformed by ICP-AES.

2 n.d.

Lead (Pb) mg/Kg With reference to IEC 62321: 2008 andperfomed by ICP-AES.

2 n.d.

Mercury (Hg) mg/Kg With reference to IEC 62321: 2008 andperformed by ICP.AES.

2 n.d.

HexavaEn gnromtum C(Vl) byalkaline extraction

mg/Kg With feference to IEC 62321: 2008 andperfomed by UV-VIS.

2 n.d.

Beryllium (Be) mgKg With reference to US EPA Method 3050tfor Beryllium Content. Analysis wasperformed by ICP-AES.

2 n-d.

Antimony (Sb) mg/Kg With refe.ence to US EPA lrelhod 3O5OBfor Antimony Content. Analysis wasperformed by |CPAES.

2 n.d.

Cobalt dichloride(CAS No. | 007646-79-9)

mg/kg SGS In-House method-RSTS-EE€VHG003, RSTS-EE-SVHC-004. Anatyzed byrcP-AES.

5 n .d .

Polychlorinated Biphenyls (PCBS)(CAS No.: 001336-3&3)

mgkg With reference to US EPA 3540C method.Analysis was performed by GC/[4S.

0.5 n.d.

Polychlorinated Naphthalene(PCN6)

mS/kg With reference to US EPA 3540C method.qnarysis was perlormed by cC/[rS.

n.d.

Polychlorinated Terphenyls(PCTs)

mdkg With reference to US EPA 3540C method.Analysis wa6 performed by cC/lMS.

0.5 n.d.

Alkanes, C1G.l3, chloro (ShodChain Chlo.inated Paraffins) (CASNo.:085$$44€)

o/o With reference to US EPA 3540C method.Anaiysis was performed by GC/IMS.

0.01 n.d.

PVC Analy6iswas performed by FTIR andFLAME Test.

Negative

Perfl uorooc'tane sulf onates(PFOS)PFOS -AcidPFOS - Metal SaltPFOS -Amide

mgikg With reference to US EPA 3540C: 1996method for PFOS Content. Analysiswa6performed by LC/IVS.

'10 n.d.

'n th s t6r rcpi der m, b ie s,hdcomtsry k:lFjj!i!!' rl|li rlr!rI:J'; rirlrll::lr f-i1++tr1.1./r\. 3$r;ri . , r" 111{q

ny 5uq6d b cceffi cdndrtrsoi s

on t , ndwrhn lb imGo ic r€ds i e p . i 3b r tE ronsos radbs ll b r r o h t s d d ] ' o d j o n s u n d s e k i i o l b e G p d u d d e p l n i u

Test Report No. I CEl2O11t24U3 Date:20t1l03i/03 page:3of17HITACHI CHEMICAL DUPONT MICROSYSTEIVS250 CHEESEQUAKE ROAD-BLDG. 424, PARLIN. NJ 08859-1241

|l flttttfltItt

Test ltem (s): Unit lr.thod MDL ResultNo.l

PFOA (CAS No.: 000335$7-1) mg/Kg With referenc€ to US EPA 35a0C: 1996method for PFOA Content. Analysiswaspedormed by LC/MS.

1 0 n.d.

Sum of PBBg

mg/Kg With reference to IEC 62321: 2008 andperfomed by GC/MS.

n .d .[4onobromobiphenyl n .d .Dibromobiphenyl n.d.Tribromobiphenyl n.d.Telrabromobiphenyl 5 n-d.Pentabromobiphenyl 5 n.d.Hexabromobiphenyl n.d.Heptabromobiphenyl 5 n,o.Octabromobiphenyl 5 n.o.Nonabromobiphenyl 5 n,o,Decabromobiphenyl 5 n.o.Sum of PBDES n,o.Ilronobromodiphenyl ether 5 n.o.Dibromodiphenyl elher 5 n.o.f ribromodiphenyl ether 5 n.d.fet€bromodiphenyl ether 5 n.o,PentabromodiDhenvl ether 5 n.d.HexabromodiDhenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.d.Octabromodiph€nyl ether 5 n.d.Non€bromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n,d,HalogenHalogen-Fluodne (F) (CAS No.:014762-94-8\

mg/Kg With reference to BS EN 1458212007.Analy6i6 was performed by lC.

50 92

Halogen-Chlorine (Cl) (CAS No.:022537 - t5-11

mg/Kg With reference to BS EN 1458212007.Analysis was performed by lC.

50 n.d.

Halogen-Brcmine (Br) (CAS No.:01 0097-32-2)

mg/Kg With reference to BS EN 1458212007 .Analysis was performed by lC.

50 n.d-

Halogen-lodine (l) (CAS No.:0'1436244-E)

mg/Kg With referenc€ to BS EN ft5A2:2OO7.Analysis '.vas perfomed by lC.

50 n.d.

O€anic-lin compound6TributylTin (TBT) (CAS No.:000688-73J)

mg/kg With reference to DIN 38407-13. Analysiswas performed by GC/FPD.

0.03 n.d.

cmFry 4 r ri{rii.r.. rlrl! 11,r-}J ilnrl:|:::r!,-liF^b!.1.1'.,*n+it, ^,:]rllsanys !q8drorsc '6ercod lonsd s

tu€.d6Etomd @mtu suB

n s i b i t y 6 l o i s c l e i l s d 6 € f u m e i

Test Report No.: CEl2011l24U3 Date r 2011/03/03 paae:4ofi7HITACHI CHEMICAL DUPONT MICROSYSTEMS250 CHEESEQUAKE ROAD.BLDG, 424, PARLIN, NJ 08859-1241

I][tttl[lrtt

T€st ltem (s): Unit Method MDL ResultNo.1

TriphenylTin (TphT) (CAS No.:000068-34-8)

mg/Kg With reference to DIN 38407-13. Analysiswas perforned by GC/FPD.

0.03 n.d.

AsbestosActinolite (CAS No.: 077536$6.4) oa With reference lo NIOSH 9000 method-

Analysis was performed by XRD.1 Negative

Amosite (CAS No.: 012172-73-5) % With reference to NTOSH 9000 method.Analysis was pertormed by XRD.

1 Negative

Anthophyllite (CAS No.: 077536-67-5)

o/o With reference to NIOSH 9000 method.Analysis was pertomed by XRD.

1 Negative

Chrysotile (CAS No.: 012001-29-1 % With reference to NIOSH 9000 method.Analysis w€s performed by XRD.

I Negative

Crocidolite (CAS No.: 012001-2&4)

With referenc€ to NIOSH 9000 method.An€lysis was performed by XRD.

1 Negative

fremolite {CAS No.: 07753668€) % With reference to NIOSH 9000 method.Analysis was perfomed by XRD.

1 Negative

AZO'1): 4-AMINODIPHENYL (CAS No.:000092s7-1)

mg/Kg With reference to LFcB 82.m-2. Analysiswas performed by cc/l\rs.

3 n.d.

2): BENZIDINE (CAS No.:000092-87-5)

mg/Kg With reference to LFGB 82.02-2. Analysi6was per{ormed by GC/l!tS.

3 n.d.

3): 4-CHLORO-o-TOLUIDINE(CAS No.: 000095€9-2)

mg/Kg With refe.enc€ to LFGB 82.02-2. Analysiswas performed by GC/l!lS.

3 n.d.

4): 2-MPHTHYLAI,IIlNE (CASNo.: 000091-59-8)

mg/Kg With reference to LFGB 82.02-2. Analysiswas performed by GC/MS.

3 n.d.

5): O-AMINOAZoToLUENE (CASNo.: 000097-56-3)

mg/kg With reference to LFGB 82.02-2. Analysiswas performed by GC/MS.

3 n.o.

6): 2-AMINO-4-NITROTOLUENE(CAS No.: 000099-55-8)

mg/Kg With reference to LFGB 82.02-2. Analysisu/as performed by GC/MS.

3 n.o.

7): P-CHLOROANILINE (CAS No.:00010647€)


3 n.d.

8)r 2,+DIAMINOANISOLE (cASNo.: 000615-054)

mg/kg Wilh reference to LFGB 82.02-2. Analysiswas performed by GC/[,S.

3 n.d.

9): 4,4'-DIAMINODIPHENYLI\4ETI-!qNE(CAS No.i 000101-77-9)

mg/K(l With reference to LFGB 82.02-2. Analysiswas perlormed by GC/lrS.

3 n.d-

pals)r8$d ThsBr+nennorbcnFny d"i ,i 1i}i !: . r ;t +:l'11$iri :ii 'rle: r.: r- . ,l-.1+*d11\ r =ir:il . 1.'11.,!li+.rh ' ddum-, B tssu€d by r€ c@r

suqd b rsms and condrois bf E rd rha rim#ld d 6bL I

po6b ' I s rd Gc r613nds3eumlhelfugh6aidobgd65undol|h.ta

r l l ! r = : 4 ! i i l+460r r r ! r r ,+s6 l . r r re r r ve4 , rm

Test Report No.: CEl2O11l24U3 Dale:2O11t03tO3 paqe: 5 of 17HITACHI CHEMICAL DUPONT MICROSYSTEIUS250 CHEESEOUAKE ROAD.BLDG. 424, PARLIN, NJ 08859.1241

I lllll|l Il]tIlt

Test llem (s); lJnit Method I'DL ResultNo.l'10): 3,3-DICHLOROBENZIDtNE

(CAS No.: 000091-94-1)mgikg With Gference to LFGB 82.02-2. Anatysis

was perfomed by GC/MS.3 n.d.

,I 1 ): 3,3'.DIMETHOXYBENZIDINE(CAS No.: 0001 19-90-4)

mg/Kg With reference to LFGB 82.02-2. Analysiswas performed by GC/IVS.

3 n.o.

'1 2): 3,3!DIMETHYLBENZIDINE(CAS No.: 0001 '19-93-7)

mg/K9 With referenc€ to LFGB 82.02-2. Anatysiswa6 performed by cc/lrs.

3 n . d .

1 3): 3,3'-DlMETHYL4,4'-DIA[,,IINODIPHENYLI\iIETHANE(CAS No.:000838-8&0)

mg/Kg With reference to LFGB 92.o--lnatysiswas perfomed by GC/MS.

3 n.d-

14): P-CRES|D|NE (2-ti]ETHOXY:s-ITETHYLANILINE) (CAS No.:000120-71€)

msag With reference to LFGB 82.02-2. Anatysisw€s perfomed by GC/MS.

3 n.d.

15): 4,4'-[TIETHYLENE-BlS- (2-CHLOROANILINE) (CAS No.:000101-144)

mg/Kg With reference to LFGB 82.02-2. Anatysis,,vas performed by GC/MS.

3 n,d.

16)No.

4,4',-OXYDTANTLTNE (CAS000101-804)

mg/Kg With referenc€ to LFGB 82.02-2. Anatysiswas performed by GC/l!lS.

3 n.d.

17)No.

4,4'-THtODTANTLTNE (CAS00013945-1)

mg/Kg With referenc€ to LFGB 82.02-2. Anatysiswas performed by GC/[,S.

3 n.d.

18): O-TOLUIDINE (CAS No.:000095-534)

mg/Kg Wjlh refe.ence to LFGB 82.02-2. Analysiswas performed by GC/MS.

3 n.d.

1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 000095-80-4

mg/kg With reference to LFGB 82_02-2. Anatysiswas performed by GC/MS.

3 n.d.

20): 2,4.s-TRIMETHYLANILINE(CAS No.: 00013717-7)

ngikg With reference to LFGB 82-02-2. AnalysiswBs perfomed by GC/MS.

3 n-d.

21): O.ANISIDINE (CAS No.:000090-04-0)


3 n.d.

22): P-AMINOAZOBENZENE(CAS No.: 000060-09-3)

mg/kg With reference to LFGB 82.02-2. Analysiswas peformed by GC/MS.

3 n.d.

23): 2,4-XYLIDINE (CAS No.:000095-68-1 )

mg/Kg With reference to LFGB 82.02-2. Analysiswas performed by GC/IVS.

3 n.d.

24): 2,6-XYLIDINE (CAS No.:00008762-7)

mg/Kg With reference to LFGB 82.02-2. Analysiswa6 performed by GC/lrS.

3 n.d.

rn rhE 16r €pd( d8r ody b rhe emproc)re*€n ThsBlr@d€nmrb€cmF iy ' t - f r - 1 : i 'N . r . ++ r ' t ! l { i r , r i i ' r i i r :E * . 1 . . 1++F r - t r d i t ' I l . a i t - . , 1€ .Ih 3 tuumd B csusd br rh6 cmps

po i3b ' l y s l occ i s l and lh3d6umlhe.'ghbaddga'msUndertbta

lL:rr,: =ur,lrf il r er (orrre ta t + s610rrr2s rr7 lww4j!ui

Test Report No. : CEl2011l24U3 Date : 2011/03/03 page j 6 of 17HITACHI CHEMICAL DUPONT I/|ICROSYSTEMS250 CHEESEOUAKE ROAD-BLDG. 424, PARLIN, NJ 08859-1241

Not€ :

|l flt fllrrl

'1. m94

Test Report No.: CEnorn4u3 Date:2011/0303 pase:7 of 17HITACHI CHEMICAL DUPONT I\/|ICROSYSTEMS250 CHEESEQUAKE ROAD-BLDG, 424, PARLIN, NJ 08859.1241

rr[tat][ttt]r

1) These samples were dissotved totally by pre-conditioning method according to below flow chan.(Cf- lest method excluded l

2) Name ofthe person who made measurement Climbg.eat yang3) Name ofthe person in chafge of measurement: Troy Chang

ICP-AES

Sample l\ratedal DigestionAcjdSteel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,Glass HNO/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic HrSO., HrOr, HNO3, HCIOthers Any acid to total digestion

'n{h3l6lB@nr€'arm|yloibsamp|e15)bseftsbnrepon€nidbd@dcomtsry h : l l r ,1 l1 r { . . .1* i " } ! ! : : r : r i1 r !$ 'n i ! ,1 - r i+ . }q1 . r \ - l t1 ; t , , . #J

iy suqed b b css€ condlbis d ssuq6d b rerns and ctu ro.s ior E

mm, dB ^d ddBde d, 6 b ai,6er .etu aid obrhs'trs ud ihe ft

rdn.i r!r ldJr- 1{ rMlorD rx r+ s6 (o?irrerrT w!!!dj

Cutling / Preparation

Acid digestion by suitable aciddepended on different samplematerial (as below table)

Add appopriate amount ofdigestion reagent

Heat to appropriate

temperature to extract

Cool, filter digestate

through filter1) Alkal iFusion2) HClto dissolve

Add diphenyl-carbazide forcolor development

measure the absorbance

at 540 nm by UV-VIS

TeSt RepOft No. : cEt2o11t24843 Date : 20.11/o3i/03 pase : I of .t7

HITACHI CHEMICAL DUPONT MICROSYSTEI,TS250 CHEESEQUAKE ROAD.BLDG. 424, PARLIN, NJ 08859.1241

L |lt||l||t t|l

'1) These samples were dissolvedchart.

2) Name dthe person who made measuement: Ctimbg|eatyang3) Name ofthe person in charge of measu€ment Troy Chang

totally by pre-conditioning method according to below ftow

Flow Chart ofdigestion for the elements analy6is pedormed by lCp-AES

Sleel, copper, aluminum, solder Aqua regia, HNO3, HCl, HE HrO,Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regiaSilver HNO]

Plastic H2SO1, H,O,, HNO3, HCI

Others Any acid to total digestion

ip6G)€dd Th€ r€d €tsn 6nd 6c6p.ny +.,,i!;ilrrr.I lltsrlx.r{ij,; -.irrr1ii'r i. !}1'lhi11,rir,;:+!l . I i:,9|i!1

slqed b rein6 md cddiroG ro. E

rhe, @is and ob 0a'd3lodsrbra

1) Alkal iFusion2) HClto dissolve

Test Report No. : CE12O11/248/3 Date : 2011/03/03 paaet 9of 17HITACHICHEMICAL250 CHEESEQUAKE

OUPONT MICROSYSTEIMSROAD.BLDG, 424, PARLIN, NJ 08859.1241

Analvtical flow chart of Cobalt dichtorido

1) Name ofthe person who made measurement: Climbgreat yang

2) Name of the person in charge of measurement Chenyu Kung

Ill l|[ttfltt]tl

€13) rdsd rhE bn rcpn 6nd b 'cmFry F r t l ! Je l . , r i i : : l : ' r : i r , ; l i r l t : : F * , . l l t r L+ t , 1 , r l ; , ' 1 r r 1 , 11 ,9& l l .

sqsd 'o r€ms 'd cmd{oB tor E

nnol be re!rcduced 6:c6d itur *iho!for$ryorfabfelo.dbeofun|d

rL,j:r ]JNarf it I s6 (0rrrs rr r 1s61.12e D t,w4j!di

Sample pretreated by acid digestjon andsolvent extraclion

Test Report No.'. CEl2011l24U3 Date : 2011/03i/03 page : .10 of 17HITACHICHEMICAL250 CHEESEQUAKE

DUPONT [/|ICROSYSTEMSROAD-BLDG, 424. PARLIN, NJ 08859-1241

Analysis flow chart for detemination of Asbestos'1) Name of the person who made measurement Victor Kao2) Name of the person in charge of measurement: Wendy Wd

|| t|trr|||l|t:[

Not containing AsbestodNegative

n h s r8r r€Fd d€r onry ro 1b sampr€tt ressd h s red re@d caiidr bd recompany N . ! l r , i i " i ! . r l i l i i i l r l rY l r ; ; l r l j r l l i i : 1 t r i l + i ! . l . ] . - I + - , r l j , r t t

ny 3uqed b 6668 condrtrs d s

ont,nd w thn lb imib d cr€d s Br.dbercoduedaceplLn,ui'lihod

r_ , r i l r l r i r ,

XRD Oualitative analysis by X-ray diffractionmethod

Diffraction peak ofasbestos is absent

Asbestos identifi cation byoptical microscopy

Asbestos fiber is Dresent

Test Report No. : CA2O11|24U3 Date: 2011l0t03 paae : 11 ot i7HITACHICHEMICAL250 CHEESEQUAKE

OUPONT MICROSYSTEMSROAD.BLDG, 424, PARLIN. NJ 08859.'1241

ll| ||[ tIl ]ll

Analytical flow chart of Organic-Tin content1) Name ofthe pe6on who made measurement: Ginny Chen2) Name of the person in charge of measurement: Troy Chang

uaEl

npek)Gdd Th s rd €Fn ennd bcmp5ny rL j l i r ; ' , . r r l . : l : r r i l . : \ r r t l : r l i " . + l : i i r i i l i a r l + , ' : j ' ! r . 1 . ! 1 " , , - j l i ! .f t sddn6 fossdby ' b6mpany9qedb i3Gs6€ | cdd {onsdSfu€sdMEbmd@manssd ]

Concentrate/Dilute Extracted solution

Analysis was perfomed by cCi/FPD

Test Report No.:CEnO11l24U3 Date:2011/03/03 Paae | 12 ot i7HITACHICHEMICAL250 CHEESEQUAKE

DUPONT MICROSYSTEMSROAD-BLDG. 424, PARLIN, NJ 08859.1241

Analytical flow chart of halogen content'1) Name of the person who made measurementt Rita chen2) Name of the person in charge of measurement Troy Ch€ng

llfl ll ttl l

n ' ^ 1 h 3 1 6 l l o p d l € f a r 6 | y l o 1 b s a m d q ' b s k T n 3 b d r e p o d € m d $cmFiy i:rr ,, !:ji ,. . .t -l+::;!1$i ! r!!r,rij: ts r 4i++14^/]\i 3r';1":.. r:.r11{4rh3 ddumdI6 6sd 6ylhe cmps

dkenAny]io]ddollhsdocumonp . i sb ' I yG lo6c |6 I ' dbs fu

rhe, d,b and ob oarmsundsrtbta

Sample pretreatmenl / Separation

Weighting and putting sample in c€ll

Orygen Bornb Combustion / Absorption

Dilution lo fxed volume

Analysis was performed by lC

Test Report No. I CU2O11|24U3 Date : 2011/03/03 page : 13 of 17HITACHI CHEMICAL DUPONT MICROSYSTEMS250 CHEESEOUAKE ROAD-BLDG. 424, PARLIN, NJ 08859.'1241

Analltical flow chart of Soxhlet extraction (LC/MS) procedure'1) Name of the person who made measuement: Lydia Fu

2) Name ofthe person in charge of measuremenl Shinjyh Chen

r Test ltems: PFOS/PFOA , Benzotriazole

Sample pretreatmenuseparation

Data

tI| |l tlrIlr[III

cm@iv *i: rl + ;iq, . r+rFrlilllirj ii!r,1lr e n . l.l++la^rrE i:;:4 . r'r-- 111{9; ,rhs d@hd ts 6s!.! bylh€cdr

sp .mb ' 9 t r o 6c ra l ad lhs&m

fu96lyollab'f€[email protected]|ol

tL r i: rit,!i? .rirerozrre

Test Report No.: CEl2011l24U3 Date:2011/0t03 page j4 ot 17HITACHI CHEMICAL DUPONT MICROSYSTEI/|S250 CHEESEQUAKE ROAD-BLDG, 424, PARLIN, NJ 08859-'1241

Analytical flow chart1) Name ofthe person who made measurement: Roman Wong2) Name of the person in cha€e of measurement: Troy Chang

r Test ltems: PBB/PBDE, TBBp-A-bis

Firsl testing process -----' Oplionalscr€en process ---, Confmation process -.>

t ]|lt[t ||t{l

. _ r : , . r + ! , b r l i , i r r I 46101 re

Screen analysis

vrv

Sample extraction method

ConcenkatdDilute Extracted solution

Analysis by GC/MS

lssue Report

nrh3rsrr€Fnd€ronryrolbsnpr€itbdd rh€radrcFd€nnorbrecomeanv F}r,E:i4 ..{llrir:rltlr: : iil1rf.t il1{,r-lr: itq., !i, r u : . . l {,I1{

.y suq.d b b GffiE condrEos or s

Test Report No. i CEl2O11t24U3 Date: 2011/03i/03 paoe: 15of 17HITACHICHEMICAL250 CHEESEQUAKE

DUPONT MICROSYSTEI,iSROAD-BLDG, 424, PARLIN, NJ 08859.1241

|l [ ! | | | | t I |

Analysis flow chart for determination of pVC in material1) Name ofthe person who made measurementt EvaChao2) Name of the person in charge of measurement Shinjyh Chen

or.Glr6dd rh s bsl @on.anid becm@y 4;i ri {ji}rri . .! J+ti!i$ir, ;il '.rttl.F r . ,ll4.1.,14r!\ f:i: 'n.ai: r'1r''kThs ddumd c $sn bys€ cmr

subled ro Tsms and CondboB irr E

8p .Bb ' i y s l o6c j s l and$3ded

; f r ' . , i r l b Q z w ! n r r s s b L

Sample pre{reatment

Sarnple analyzed by FTIR

Check wave-number of C-Cl bonding

Test Report No.: CEl20l1l24U3 Date:2011/0303 page: 16 of 17HITACHICHEMICAL250 CHEESEQUAKE

DUPONT MICROSYSTEMSROAD-BLDG. 424, PARLIN, NJ 08859.1241

Chlorinated Flame retardant analldical flow chart

1) Name ofthe person who made measurementi BarryTseng2) Name of the person in charge of measurement: Troy Changr Reference method: US EPA 8270D. US EpA 3540r Test ltems: PCBS, PCNS, PCTS, Mirex, Cp, lrccp

Data

lmlflI][tlttl!

n0eGrc{d rhs 161r@d €ind tcsFry *+ ,i !;i'!l . i rr tsil r:ifi;; ;ll!lt.:e * l.r+itlarrl, =iia f4.19Fnrd6 d@md € su€n by !r€ comPa

s l b ] d d b ] m s d d c 6 d i l ' 0 6 ' o r E

,dons { any fteh@r'ssdbrc

d!4orfahfelmdse6funlol

LA!.i ;nr'iirt ilre0zrlD

Test Report No. : CE/2011/24843 Date: 2011/0303 page: j7 ot 17HITACHI CHEMICAL250 CHEESEOUAKE

DUPONT MICROSYSTE[JSROAD-BLDG. 424, PARLIN. NJ 08859-1241

lllfltrl][t:tt|l

" End of Report "

r€pdu6derceplnfu|cm@iv ,i;:ri+tq . riilf;,'rl1{i ,J lit',lr-.E-;i,1.'tq+F.-rrr 'Jliiil. 1 ;',u{q ,Th3@m{1E6&3dbylfucqrysubidlohGa€€codiDBofs

i b ]edbT6 f r ssndcd id i | o66E

trrons. f any ftecm@tssoe€

T€st Report No. SHAEC1105702902 A01 Date: 04 May 2011

SOLAR CHEMICAL APPLIED IiIATERIALS TECHNOLOGY(KUNSHAN) CO.,LTDNO, 168 WUSONGJIANG S.ROAD,E.T.D,Z.,KUNSHAN,JIANGSU PROVINCE,CHINA

THIS REPORT IS TO STJPERSEDE TEST REPORT NO.SHAECI I 05702901 DATE zJl1I04T2g

The following sample(s) was/w€re submitted and identifed on behatf of the clienb €s : Ti

Pag€ 1of 5

sP11-012135 - SUZ

SOLAR CHEMICAL APPLIED IUATERIALS TECHNOLOGY(KUNSHAN)CO.,LTD

Ti

SOLAR CHEIIICAL APPLIED MATERIALS TECHNOLOGY(KUNSHAN)CO.,LTD

26 Apr 2011

26 Apr2011 - 03 Jan 2011

Selected test(s) as r€quested by client.

Please refer to next page(s).


Based on the performed tesh on submitted samples, the resulb comply with theRoHS Directive 200295/EC €nd its subsequent amendments.

' ibtub a'aninpnnblMrybtu|srrr{.}rnbd.

SGS Job No. :Buyer :

I\rodel No. :Supplier :

Date of Sample Rec€ived :Testing Pedod :Test Requested :

Test l elhod :

Test Resulb :

Concusion :

Signed for and on behalf ofSGgCSTC Ltd.

,aQr"-^Fan Jingjie, JJApproved Signatory

rih dsd f, b'd rr rh tuF,'y rld br. ond' c.'dtt!.. ot S.4to rni{.q opNd. dlrdr o rus.d 4@ -61!!g'* 6n &@.t- b rr.'. sr ffi b Ebffio h'ft ! ens*!,!|q .

Test Report No. SHAECl105702902 A0l Oate: 04 May 2011 Page 2 of 5Test Results :

Test Part Descdption :

Sp€cin|6n No. SGS Samd€ lD D€€cription1 SHA1 1-057029.001 Silver metal

Rema*€ :(1) 1 mg/kg= 1 PPm=0.0001%(2) irDL = l\4ethod Detection Limit(3) ND = Not Detected ( < [rDL )(4) '-" = Not Regulated

RoHS Dlr€.dw 2002/95/EC

Test llrethod : With reference to IEC 6232'1:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Determination of Merdry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimelric Method using uv-Vis.(5) Determination of PBBS / PBDES by GC-MS.

Test ltemls)

Cadmium (Cd)Lead (Pb)Mercury (Hg)Hexavalent Chroniun (C.Vl)

MonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexab.omobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenyloecabromobiphenylSum ol PBDESMonobromodiphenyl ether

ulx ud! MDt @110O mg/kg 2 ND

1,000 mg/kg 2 ND1,000 mgikg 2 ND

o Negative1 ,000 nglkg - ND

- mdkS 5 ND- mdks 5 NO- mg/kg 5 ND- mdks 5 ND- mg/kg 5 ND- mS/kS 5 ND- mg/kg 5 ND- mS/kS 5 ND- mg/kg 5 ND- mS/kS 5 ND

1,000 mg/kg - ND- mS/kS 5 ND

ftr ddn I en br rb enFry *!ld b rr os'.r c.dtor d 3.M*6dord3d4'di.dd'i. ' ' .bfu d.dfur rqc i rm! d *x,..6i6d r:.dmnrrTii-Ii6rli6in F ilhffitdr* judrehrd.tudftM 4r|*rdNrd.

Test ReportTest ltem(s)

Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl etherPentabromodiphenyl etherHerabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabronodiphenyl etherDecabromodiphenyl ether

No. SHAECl105702902 A01 Date: 04 May 2011 Page 3 of 5

tird! ud! MotmS/kg 5mdkg 5mdkS 5mdkS 5mdkg 5mg/kS 5mg/kg 5mS/kg 5ms/la 5

001NDNDNDNDNDNDNDNDN D

Notes :('1) The maximum pemissible limit is quoted from the document 2005/618/EC amending RoHS dhective2002gstEc(2) o spot-test:Negative = Absence of CrVl coating, Positive = Presence of CrVl coating;The tested sample should be further verified by boiling-wateFextraction method if the spot test result isNegative or c€nnot be confmed.o Boiling-water-e)dractionlNegetive = Abs€nce of CrVl coating; Posilive = Presence of CrVl coatingThe detect€d concenkation in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50cm" samole surfa@ area,For conosion proteclion coatings on metals: Information on storage @nditions and production date of thetested sample is unavailable and thus fesults of C(Vl) represent status of the sample at the time oftesting

.h dsrruru r.Dh.crd jdi|rrfrc.de.h.slahhidb i.'r!(rr..rr sEprt' M|.rtdM li..frbr.pred oahcomrb'!-rdkr{drd ot$.ofurd don e.;ryh FFehobrh.|ljririd.dcrtfi.r'.

rtu h * B {rd tr hrr b 'hr rnP .(.) !6!c

fi lhgn utrnhdxtitli4tudaor| 20@36+I -tl.;trql&L.et3{l ll: 2i@3

tEl€(s-ll)! @al tE E(F-?1)oWtt tw.6.!.m*(a.a)d4025a{ NLF-Z)aa&3 .€id'h.€{.6

M.mberolrh6 8OS GDur (8GSS )

Te6t R€port No. SHAECl105702902 A01 Oate: 04 May 2011 Page 4 of 5ATTACHMENT S

RoHS Testing Flow Chart

1) Name ofthe person who made testing: Jan Sha/Even Xu/Allen Xao/Gary Xl2) Nam€ ofthe person in charge oftesting: Jeff Zr an g/Georg e Xu/ Elim Lin3) These sampl€s were dissoh€d totially by pre +onditioning method according to betow fow chart_

(C 16+ and PBBS/PBDES test melhod €xcluded )

PbrcdrHg PBBSIPBDES

Samole Measurement

Acid digestion withmicrowale/ hotplate

Concentralion/Dilution of extraction

solution

Heating to 90-95cfor extraclion

1) Alkali Fusion /Dry Ashing

2) Acid to dissol\e Filtration and pHadjustment

Adding 1,5-diphenylcarbazide

for color


brcolorindic€te6 the

mfr&.GY||l|todrr$I||ttlnctah! 2O@3a+t -lt.*fqldrt€30+3tt ll: a@

r ErE {s-a}0r465ar rEEEt6?tt{59r9 q.6rcadHr{O-a)6fi@sa flLoCzl}sa5dE! ..gsCftOa.d

lronbor ot fio sca ODU9 (8Gg SA)

Test Report

Sample photo:

No. SHAEC1105702902 A01 Date: 04 [,lay 201 1 Page 5 of 5

sHA1l-057029.001

SGS authenticate the photo on original report only*'* End of Report *"

rh..smd. hd by h oiFry rq.d b d odrr c{naxrlor s.rrts tsnb. .yf,i.d, s!.!t. d &ub -.rgl!E:!e hn &ffi,*it-. riffi hd cdrs & t6m. D6h-r d h F. ..md..dd'|ii,i: adr6i-aM-8ffi;?lq:gff G(c.diF,,d.!ltdorhd!Ni..,"r+3f .rBtudrdsM6ffi l;ffi in,i.Ifu-tu6r.r,rir'F.rhho!EtEm rrat$cn h htrld ffi |rt\el rB. ftrc@sr. d. nMjbrnv i @ 6 crid $. ftj. enr.d ridffi. drsibrtudoIF".gr]..|5F!d.!I.!DruM rri{F, b..rrr *anrrhFr.6id'ori.rn6rddd6.r*iFnr {.r4flt66ffi fld .M - B ri qd rtr {'r b b.Fpr.l.r '-bd .

fl nEbaYarihdxc|ldfd$.ddorr [email protected].$r6ttlto0!6+l| ll:M

tE €{Ga)61@6! lE tFaFKn lrrs.4amHlj{&-e!}61{&sa'l |L(l!-21Fatadf,3 .s.dirergf,m

M6r$€r olrhescs Gro!9 €GgS )

Test Report No. SHAEC'1015856302 Date: 06 Nov 2010 Page 1 of6

SOLAR CHEMICAL APPLIED MATERIALS TECHNOLOGY(KUNSHAN) CO.,LTD

NO.16A WUSONGJIANG S-ROAD.E.T,D,Z.,KUNSHAN.JIANGSU PROVINCE,CHINA

The following sample(s) was^rere submitted and identified on beh€lf of the clients as : Copp€r

SGS Job No. :

Model No. :

Buyer:

Supplier :

Date of Sample Received :

Testing Period :Test Requested :

Test l\rethod :

Test Results :

Conclusion :

sP10-036695 - SUZCuSOLAR CHEMICAI

SOLAR CHEMICAL

04 Nov 2010

04 Nov 2010 - 06 Nov 2010

Selected test(s) as requested by client.



Based on the performed tesis on submitted samples, the results comply with theRoHS Directive 200295/EC and its subsequent amendments.

Signed for and on behalf ofscs-csTc Ltd.

,z?v"'^Fan Jingjie, JJApproved Signatory

fErndnerritodl,t,Dbqarurorr 2t@33+I -tl.*trAltftr}9fs+l ll.2!o?30

rE!E(S-?r)6!a!2550 tEtE{6-2rFffir9 *f_d4...Mf!(&.ell6l{&s1 Hlj{l6-21)6a@3 .lFdftOE.6

air€mbol or !n. scs o.oq lsos s4

Test Report No. SHAEC1015856302 Date: 06 Nov 2010 Page 2 of 6

Test Results :

Test P€rt Descriotion :

S@men No. SGS Sample lD D€e.ription1 SHA10-158563.002 Copper metal

R€marl6 :

(1) 1 m9/k9 = 1 PPm = 0 0001%(2) MDL = Method Detection Limit(3) ND = Not Deteded ( < MDL )(4) '-" = Not Regulated

RoHS Dir€divo 2002/igtEc

Test Method : With referenc€ to IEC 62321:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Dete.mination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis.(5) Determination ofPBBS / PBDES by GC-IjS.

Test ltem(s)Cadmium (Cd)Lead (Pb)Mercury (Hs)Hexaval€nt Chromium (CA/l)Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTelrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobaphenylSum of PBDESMonobrcmodiphenyl ether

luil Ud!100 mS/kS

1,000 mg/kg1,000 mg/kg

1,000 mg/kgmg/Kg- mg/Kg

m9Kg- mgKs- mdks- mg/Kg- mg/Kg- mg/Kg- ng/Kg- mg/Kg

1,000 mg/kg- mgKg

MDt pp22 N D2 72 N DO Negative

ND5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D

5 N D

lhL a@tudr hd brflt! Dr rb g@Frr dFd b rr o-.d cq!'ftdr d 3qr6 rnid d'nd,.

&n r.r!.h'bN bti. Lrhi.drds.rE5 dr m nr.nntu 'rrb1[ nhrr.{.,n.hr .

lbrl|nerl todx'r ulrttgr{riorr 20@33 rejiE|fi+t)6146'il 'tl.*icqltl€.F||dll l*Ms Hti tB-21r 6r.r&5..

tE|E (6-AFr6rO n6j{.6HL{S-?lF@l ..atdi.CFm

Msm!€r otfi€ SGS Cosp (9Og SA)

Test Report

Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl elherOclabromodiphenyl etherNonabromodiphenyl elherDecabromodiphenyl ether

Test ltem(s)Fluorine (F)Chlodne (Cl)Bromine (Br)lodine (l)

No. SHAEC1015856302 Date: 06 Nov 2010 Page 3 of 6

tltE|naYrs&ixn hndrc'Jc|li r!@3t!.ll.tE8ttll39rt3+t lr: 2@30

auNDNDNDNDN DN DN DN DN D

MOt 0u50 ND50 ND50 ND50 ND

lE&$-Q1)61@53 lA€6-AFa€St9 |,|rd.t!amHJF4l)61{E!L r{.:16aFml3 tlsd'ir€{.iqi

!!d! !d! uD!mg/kg 5mdkS 5mdkS 5mdkS 5mdkS 5mdkS 5mSikS 5mg/kg 5mg/kg 5

Notes :(1) The maximum permissible limit is quoted from the document 2005/618/EC amending RoHS di.ective

200?,95iEC(2) ' spot-testNegative = Absence of CrVl coating, Positive = Presence of CrVl coating;The tested sample should be further verified by boiling-waleFextraction method ifthe spot test result isNegative or cannot b€ confirmed.o Boiling-water-exiraction:Negative = Absence of CrVl coating; Positive = Presence of CrVl coatingThe detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with50 cm' sample surface area,Forcorrosion prolection coatings on metals: lnformation on stoEge conditions and production date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status ofthe sample atthe time oftesting

Haloo€n

Test l\rethod : With reference to EN 14582: 2007, analysis was performed by lon Chromatograph (lC).

ud!mg/Kgmg/kgms/Ksmg/Kg

tu d@-nd . ed !r tb c.nrdr rdd b r. or.r, o.nfltsr.t lrvteFtu Ml.n, srDb oi a.r o ffiffiEffi&ffiArl!.]{{ffi,ffi:;Jlfli$.SFil,i*#r3f;#,1,3*:ililiI.-li,:friitl$ittilffif"rf"i,tffitrfltr-r .tl|.t169tr uuE riw| h hr dnrd 6r +rr b h F pL(.' rdd

Moruer ol the SCS Oro{p (9OS SA)

Test Report No. SHAEC1015856302 Date: 06 Nov 2010 Page 4 of6ATTACHMENTS

RoHS Testing Flow Chart

1) Name ofthe pe6on who made teBting: Allen Xao/ Wesley Wei / Andy Zlao2) Name ofthe person in charge oftestingt Jeff Zl an g/ceo.g e Xu/Tracy Yue3) Thes€ samples were dissol\ed totally by pre ronditioning method according

end PB&/PBDES te6t method excluded)

/El'm Lin

to below fow chart.

Sample Preparalion

Sample Measurement

Acid digestion withmicrowa\ie/ hotplate

concentration/Dilution of extraclion

solutionAdding digestion

reagent

Heating to 90-95'Cbr extractaon

1) Alkali Fusion /DryAshing

2) Acid to dissol,€ Adding 1,5-diphenylcarbazide

brcolordel€lopment


for colordelelopment indicetes the

presence ofCr6',

Pb/cdrHg PBBs/PBDES

|rffi b B M nPd e drb ib r.hr .(.) ahc

lErphl8Ytbb&hrbt{tutllotr axES$t..tl.*EELdl|€3e|]3!lt a|:2@E

rErF(6{r)6r46rEt€(&-aF€5Sr9 ffi.rr..c.c!oliLoF,2rliqdsa NL@2tF€,}i!l .rFd'.r€F6

MemDor of ho AOS Go$ (SGS} SA)

Test Report No. SHAEC1015856302 Date: 06 Nov 2010

Halogen Testing Flow Chart

Page 5 of 6

1) Name ofthe person who made testing: Daisy cong2) Name ofthe per6on in charge oftesting: Alex Jiang

nr d6ld. tud br h orE ar'Fd b ||| onnr c.d r d s!d* rnM del.j..rrd.6 Eud dSE.,:Erryld hlr 9dmb,aqd b hr r. c@d. q Bdon. h4Dd d tusrrr,rm !

Test Report

Sample photo:

No. SHAEC1015856302 Dater 06 Nov 2010

sHA10-158563.002

Page 6 of6

raE(6-?r)6l402a50 tEt€l6-afi€5579 *r,qr{(6Hr(6-21)614@a H!lS-2r)!a5dE0 .€rd*ros8

SGS authenticate the photo on original report only

"' End of Report ""'

l-T:tEa. 99!. 9!: !!!1qt0.Erbi.hr.r6.L

irb tu 3.ipr.1r)6bd .

t'at!&.Dl|nft.d&tutlf.tsril otE 20@34!.-tl.*EAltftrols{ ll:Mo

Ma,nbgl ot fto AGS GrouD (S09 SAt

SGSJob No.Date of Sample ReceivedTesting Period

Test Requested

Test Method

Test Results

Concluslon

T€st Reporl No. CANEC1004388401 Date: 26 Oci 2010 Page 1of 6COOKSON ELECTRONICS LIMITEDBUILDING 9,SECTION 2,HONGHUALING INDUSTRIAL PARK,XILI,NANSHANDISTRICT,SHENZHEN,GUANGDONG,5l 8055,CHINA

The follo\,ving sample(s) was/were submitted and identified on behatf of the clients es :MICROFAB SC MAKE UP, I\'ICROFAB SG28 MAKE UP, MICROFAB SC I\4D, MICROFAB SC LO 7Ol30,MICROFAB SC COPPER SULFATE(MIXTURE)

127A4546 - SZ21oci2010210ct2010 -260Ct2010

Selected test(s) as requested by client.



ArBased on the p€rformed tests on submitted sample(s), the resutts cornplywtlh the RoHS Direclive 2002/95/EC and its subsequent amendments.

ry b th.3.npr.(r) r6r.d .


Silva ZhouApproved Signatory

B,e;.d b '.tu 'd codrrior 'q ., 'i6r!d rin iniil1;;L_infin-Gtiln_lEirfr tiLb lltGkq,nsdiu'ndbi6 rlrus d.rli.drhmin.^iyhold.' d drrdodr.ri tr rivhd 'hrin6nnb|dMn h.ff;fidah. conFiya fiid is. .rtuh or.u ltftitlr$iqtq{rhh b. nfr8rtl'frbi1! irliitsib rd ob 'Fnor! Jrd' d. hn'doi doon.{ hrooar.dclreri.Epdd

r$(dri.{sdidrP'lorEred idrdrytr{hlltllla,tur@r{ft 5l$63 I i!s.20)82159555 I ls2o)3d75113 lwcn.lqlBn+l l_# S;lfrrc4tE*!*tr**41$€ 5rl:5j0a63 I (6-r)321t{656 r @rq3207s111 s e96d@&.6

Momberorrh6 scsGroup (scs sa)

Test Report

Test Results:

lO for specimen 1Desc{iption for specimen 1

ARoHS Dil€dir,€ ZX'2/05/EC

Test ltem(s)Cadmium (Cd)Lead (Pb)Mercury (Hg)Hexavalent Chrornium (CrVl) byalkaline extraclionSum of PBBSI\ronobromobiphenylDibrohobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOc{abromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl elherDibromodiphenyl etherTribromodiph€nyl eiherTelrabromodiphenyl elherPentabromodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl elherNonabromodiphenyl etherDecabromodiphenyl ether

Note:1. mg/kg = ppm2. N.D. = Not Detectod (< MDL)3. [,!DL = Method Detedion Limit4. "-" = Not regulated

No. CANEC1004388401

:cAN'10-043884.001: Lfblue liquid

Date:26Od201O Page 2 of 6

UnitmgK9mgKgmgKgmg/ks

mslamsiksmg/KgmS/kSmS/kSmsikgmsikgmg/Kgmg/Kgmg/KgmS/kSmgKsmS/kSmS/kSmg/(9mg/Kgmg/Kgms/Kgmg/Kgmsftsmsftgmg/kg

N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D,N.D,N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.

Test l4ethod (Reference)IEC 62321:2008, ICPOESIEC 62321:2008, ICP-OESIEC 62321:2008, ICP-OESIEC 62321 :2008, UV,Vis

IEC 62321:2008, cc-ltlsIEC 62321:2008, GC-[,4SIEC 62321:2008, GC-IISIEC 62321:2008, GC-ltlSIEC 62321:2008, GC-MSIEC 62321:2008, GC-[4SIEC 62321:2008, GGMSIEC 62321:2008, GGII SIEC 62321:2008, ccMSIEC 62321:2008, GGMS

IEC 62321 :2008. GGMSIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, GGMSIEC 62321:2008, GCI! SIEC 62321:2008, GGIIISIEC 62321:2008, GC-[4SIEC 62321:2008, GC-IISIEC 62321:2008, GC-lt4SIEC 62321:2008, GC-[,4S

Result [,rDL LimitN.D. 2 100N.D. 2 1000N.D. 2 [email protected]. 2 1000

- 10005555555555- 10005555555555

.o,'!r dun.i.,.ubl.d 6 r.m. .i d ry4Es!4c!!-cJe!4!!.dlu'!dh{oiiru;d.nsd'ir.rn.^ .rl1birlr lrolff i

nhyL.b|kcn.dridhbdd.on,ddo*mIIdJi.Fddbseim|furh.conpary'isr.64o6|bl||tyL.b;ddm.nb triiBdocun.ii..iiori

tbs.3anc.(3)r.6rsd

mrcdlb,$|drrrrtucrtcs.lrdrro0 bFdoa(or'q4oir 510663 | (86"10)&156665 I (8&p0J82075113 M,ci.3tr,@li+l .r'rl .&*t**tq**lil*c193c t|: sioa r @20)3a55555 r (35-20)e0_/51$ 0 {r.drro|s'.a

Membor ol ths SGS Grou! (SGS SAI

Test Report No. CANEC1004388401 Date:26 Ocl2010 Page 3 of6

Test ltem(s) Unit

Perfluorooclanoicacid(PFOA) mS/kSPeafluorooctanesulfonates mg/kg(PFOS)PFOSAcidPFOS M€talSaltPFOSAmide

Note:'1 . mgi kg = ppm2. N.D. = Not Detecied (< IVDL)3. MDL = Method Detection Limit

Test Method (Reference)

EPA 355OC: 2007, LGMSEPA 35s0C:2007, LC-MS

Result MDLN . D .N , D ,

1 01 0

For refercnce: EnW 53 of Regulation (EC) No 55Z2OO9 amending Annex XV of REACH Regutation (EC) No19072006 (previously restricted under Directive 2006/122lEC):(1) May not be placed on the ma*et or used as a substance or constituent of prepa€tions in a concent€tionequal to or higherthan 0,005 % by mass.(2) l,Iay not be placed on the ma*et in semi-finished products or articles, or parts thereol if the concent€tion ofPFOS is equal to or higher than 0,1 % by mass calculated with reference to the mass of structurally ormicrostructurally distincl parts that contain PFOS or, for textites or other coated materials, if the amount of PFOSis equal to or higher than 1 Ug /m' of the coated mateial_

Rema* : The resultG) shown is/are of the total weight of wet sample.

rn. [email protected] rr b'u.d !' $. com raiy abl.lr r0 i. o.i.,r coid rd00t ot s.bh.nd ro,.dor. hn.' doNn.ddi{.d b r.ii! rd coxroir b {.m. ! o&-rdrriirh-;ir-i-iaffi-h;lFlEiitAr6' r!4tR{lr.d - r s'dEn B$.; d.rnd rh...r. ̂ ! rordd d h r do."n.a h ftv4s r i, -hltorfu:;;u-@

ryb rh "6n0 .G) r sd6d

l$(drtul6dbd'tur0d9lEcmhlltdnd$l.*9Bt0iiBcnde0n 510663 I {S-?0)32154656 I {36-20)32075113 'w,.n.4s,om4l .J_r{ &&f,,itrFt6fl+lNflltE1s3+ b!l: s1o683 r €&2!)32155555 r 6L20)32075113 o !ssd*@$M

Memborofths SGS 6b!p (565 SA)

Test Report

ATTACIIYENTSRoHs Tertng Flow Ch.rt

1) Name of the persm who made Estng. Be a WAng / CLtey yu / Ross Zhan2) Name of trte persm In chage d testing:Adams yt / Rya;yangJ) _r he-se samptes werB di6soh'/ed totelly by prB-conditionhg method accordirE to below flow chit(Cr8+ end PBBS/PBDES test method sxcluded.

-

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No. CANECt004388401 Date: 26 Ocr 2010 Page 4 of 6

ry6d,.t.npr.(tlr.d.d

ltr(d!id,sd.krhorErrdo|rldrdBhdqdrdd0lpllon 510663+E .Tiil .Etf,*tre8fl+!|fl*t1s8C N[!l: sjo663

IP6-e)e156666 I186-482@t113 M.d.arq.conl (36-20)!21s6555 t (85-o)320?s113 0 3!3..hiFots'm

M6mb6rofrh6 SGS Golp (SGS SA)

Sample Preparation

Sanple lvleasurement

Acld dlgesti0n $thmlcrl]waver' hotslate

ConcentraiorvDiluuon of extraction

solutlonAdding digestion

reagent

Solution Heating tog0-95'C foretaacton

Boiling,rreterBxtrac6on

l) Alkel i Fusion /Dry Ashing

2) Acid todissolv€

Filbation andpH adjwtmert

Adding 1,5-daph€rMcaftazide

develoFmentAdding 1,5-diphenylcalbazidefor colordevelopment

A red colorindicates thepresence of Cf..lf necessary

Pb,rcd/Hg PBET/PEDEt

Positive

Test Report

ATTACI{IIENTS

1) Name of the persm2) Name of the persm

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I (36-2qe$5555 l (36-20)320E113 Mm3!3$nI {36-20)32155555 I €6-20)32075n3 o !$cfrin €s$m

No. CANEC1004388401 Date: 26 Ocl2010 Page 5 of 6

PFOA t PFO6 Testing Ftow Chtrt

who made testlng: Cindy l-Langin chage dtesing: Ryan Yang

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Sampl€ cuting I Frepa.ation

Sample M€asuremert

Solvent extmctim

Concentatbrtoilution

Memberotrho sGS Ooup (SGS SA)

Test Report No. CANECl004388401 Date: 26 Oci 20 1 0 Page 6 of 6Sample photo:

cAN10-043884.001

SGS authenticate the photo on original report onty-' End of Report *.*

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M6Fb6rofth€ SGS Group (SGS 3A)

SGS Job No. :

Buyer:

Supplier :

Date of Sample Received :Testing Period :

Test Requested :

Test Method :

Test Results :

Conclusion :

T€st Report No. SHAEC'1012s81202 Date: 04 Sep 2010 Page 1 of6

SOLAR CHEI\4ICAL APPLIED MATERIALS TECHNOLOGY(KUNSHAN) CO.,LTDNO.168 WUSONGJIANG S.ROAD,E.T,D,Z.,KUNSHAN,JIANGSU PROVINCE,CHINA

The following sample(s) was/were submitted and identified on behatfofthe ctients as : SN

sP10-030305 - suzSOLAR CHEIJICAL APPLIED MATERIALS TECHNOLOGY(KUNSHAN)CO.,LTD

SOLAR CHEMICAL APPLIED MATERIALS TECHNOLOGY(KUNSHAN)CO.,LTD

31 Aug 2010

31 Aug 2010 - 04 Sep 2010Selected test(s) as requested by client.

Pleas€ refer to next page(s).

Pleas€ refer to next p€ge(s).

Based on the performed tests on submitted samples, the results comply with theRoHS Di.ective 200295/EC and its subsequent amendments.


7QvFan Jingjie, JJApproved Signatory

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M€hber or rho 3Og GDur (3OS SA)

SGSTest Report No. SHAEC10l2sa1202 Date: ()4 Sep 2010 Page 2 of6Test Results :

Test Part Description :

Sp€dmon No. SGS Sampt6 tO D66cdption1 SHA10-125812.002 Sitver metal

Remarks i

(1) 1 mg/kg = 1 ppm = 0.0001%(2) IVIDL = M€thod Detection Limit(3) ND = Not Detected ( < MDL )(4) "-" = Po1q"nr,","o

RoHS Dlr€div€ 2002/9dEC

Test Method :With refe.enc€ to IEC 62321:2008(1) Detemination ofCadmium by |CP-OES.(2) Detemination of L€ad by |CP-OES.(3) Detemination of l4ercury by tCP-OES.(4) Dotemination of Hexavatent Chromium by Spot test / Cotodmetdc Method using UV-Vis.(5) Detemination of PBBS / PBDES by GC-LilS.

Test ltem(s)

Cadmiun (Cd)Lead (Pb)Mercury (Hg)Hexavalent Chromium (CrVl)Sum of PBBSI\,{onobromobjphenylDibromobiphenylTribromobiphenylTet.abromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabrornobiphenylDecabromobiphenylSum of PBDESI\,lonobromodiphenyl ether

Limit Ud!100 mg/kg

1,000 mg/kg1,000 mg/kg

2 N D2 3 32 N DC Negative. N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D

5 N D

1.000

1,000

mg/KgmgKgmg/Kgmg/KgmgKgmgK9mg/Kgmg/KgmS/kSmg/Kgmg/K0mg/Kgmg/Kg

i by tb cqFry drd b lt ordr c.n rrsr.rtrttc pr'dd dri.d, .

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6m!or or !|o SGg Orolp (SgS SA)

tt-ri.AYft'btrftJeni$dJotu @Sl.-tl.tiEaltft80?3$t l|| 2@3

IE|E(Fa)flaffi IAEF-a)6affiI9 wr.cn.|{rdnlH!(6-21)n4@!Ea lt(i-zll!|{nBt ..$d*r€{r6

Test Report

Test lt€mfs)

Dibromodiphenyl etherTrjbrcmodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl etherDecabromodiphonyl ether

Test ltem(s)

Fluorine (F)Chlorine (Cl)Bromine (Br)lodine (l)

No. SHAEC1012581202 Date: 04 Sep 2010 Page 3 of 6

!Ei.t p!2N DN DN DN DN DN DN DN DN D

U-oi!msiksmg/kgmg/Kgmg/kg

MDt50505050

e92NDNDNDND

ud! MotmS/kg 5mg/kg 5mg/kg 5mg/kg 5mg/kg 5mg/kg 5ms/kg 5mS/kg 5mg/kg 5

Notes :(1) The maximum permissible timit is quoted froh the document 2005/61€/EC amending RoHS directive

2002t95tEC(2) o spot-testNegative = Absence of CrVl coating, Positive = presence of CrVl coating;The tested sample should be furth€r verified by boiting-water-extraction method ifthe spot test resutt jsNegative or cannot be confirmed.o Boiling-waterextraction:Negative = Absence of CrVl coating; Positive = pGsence of CrVl coatingThe detected concentration in boiling-water-e\"traction solution is equalor greaterthan O.O2 mg/kg with50 cm2 sample surfa@ area-For corrosion proteclion coatings on metals: Information on storage conditions and produc.tion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status ofthe sampl€ at the time oftesting

Halooon

Test Method : With referenc€ to EN 14582: 2007, analysis was performed by lon Chromatograph (lC).

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Menlor of ln€ SOS Orolp €Oa 84

Test Report No. SHAEC1012581202 Date: 04 Sep 2010 Page 4 of 6ATTACHMENTS

RoHS Testing Ftow Chart

1) Name of the pe6on wlto made testing: Allen Xiad Sping Zuo / Andy Zhao /Etim Lin2) N6me of the pe6on in charge of testing: Jeff Zhangiceorge Xu/Traci yuer) | nese_sampres were dtssotved tota y by preconditioning method according to below flow chart. (Cr6.

and PBBs,/PBDES test method exctud€d)

Pb/Cd/Hg PBB6/PBDEs

Sample Measurement

Acid digestion withmicrowav€/ hotplate

1) Alkali Fusion /DryAshing

2) Acid to dissolve

Heating to 90-9511for extraclion

Fiftration and pHadjustment


for colordevelopment

Adding 1,5-diphenylcarbazade

for colordevelopment

A red colorindicates the

presence of cf'.necessary,confirm with

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M.nler ot tt'. 9OS q|uD (Sos 6,{)

Test Report No. SHAEC1012581202 Date: 04 Sep 2010 Page 5 of 6Halogen Testing Flow Chart

1) Name of lhe person who made testing: D€isy Gong2) Name of the person in charge of testing:Alex Jiang

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Sample cutting/preparation

Combustion in orygen bomb

Dissolved in an absorptionsolution

Analyzed by ionchromatography- Double confim

by other instruments, ifnecessary

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M.nbor ol ino SOS Ollvr (SgS SA)

Test Report No. SHAEC1012581202 Date:04 Sep 2010 Page 6 of6Sample photo:

sHA10-125812.002

SGS €uthenticate the photo on odginal report only

"' End of Report .**

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