formulience - sandro ballariano cosmeticlove · 2019. 4. 25. · wet wipes lotion cp 17-18-26d inci...
TRANSCRIPT
FORMULIENCE™
PALM OIL
FREE
PolyAquol™ LW
Key features
Our Technology*
Naturally-derived “naturally emulsifying™” – PEG-free – Non-ionic
Perfect for low-energy emulsification
Compatible with “one-pot” emulsions
Ideal for low viscosity lotions and sprayable emulsions
Cold process – Energy saving – Cost&Time effective – Friendly use - allowing the use of ingredients heating sensitive – Environmentally friendly
Bio sustainability – Palm free – Cosmos approved
25ºC
PALM OIL
FREE
Polyglyceryl-4 Laurate
Polyglyceryl-6 Laurate
– Chemical integrity of polyglycerol and fatty acid components
– Know-how in reacting those components and assembling them to create a O/W emulsion matrix
OH OH
OH OH OH OH
OH OHOH OH
HO O
HO O O O O
O O O O O
O
O
OH OH
OH OH OH OH
OH OHOH OH
HO O
HO O O O O
O O O O O
O
O
* patent pending technology
PolyAquol™-LW can be added to the oil phase or in the water phase in a cold-process environment
0
1200
1000
800
600
400
200
PolyAquol™-LWin oil phase
PolyAquol™-LWin water phase
Vis
cosi
ty (c
Ps)
25ºC
Cold processemulsion
Low energy emulsions
One-pot formulation
25ºC
PolyAquol™-LW is compatible with “one-pot” emulsion systems where all components are added in one single container
5 Oryza Sativa Bran Oil
6 Gossypium Herbaceum Seed Oil
7 Octyldodecyl Oleate (and) Octyldodecyl Stearoyl Stearate (and) Polyhydroxystearic Acid (and) Octyldodecanol
8 Caprylic/Capric Triglyceride
D
9 PreservativeE
Water 1
Glycerin 2
PolyAquol™-LW 3
Xanthan gum 4
A
B
C
Prepare phase A;
Add phase B to phase A and homogenize for a few minutes;
Add phase C to phase A+B and homogenize for a few minutes;
Add one by one the ingredients of phase D in the given order and continue to homogenize for a few minutes;
Add phase D under gentle agitation.
Homogenizer-free emulsification method
80ºC
25ºC25ºC
80ºC 80ºC
PolyAquol™-LW + oil O/W emulsion PolyAquol™-LW + oil Water dilution O/W emulsionCoarse W/Oemulsion
O/Wemulsion
Single step process P.I.T. (Phase Inversion Temperature) process
First stepPrepare oil phase (PolyAquol™-LW + oil) and warm it to 75-80˚C;
Add a small amount of water phase to oil phase, very slowly, under agitation;Cool down to 25˚C under gentle stirring.
Second stepDilute the O/W emulsion concentrate with the
remaining water, under gentle stirring.
EmulsifierOil
Phase*Stability
(1 month at 50°C)
A Polyglyceryl-4 Laurate/Succinate, Aqua
5% 1%
Unstable
B Polyglyceryl-3 Cocoate, Polyglyceryl-6 Oleate, Propanediol Unstable
C Sorbitan Laurate, Polyglyceryl-4 Laurate, Dilauryl Citrate Unstable
D Polyglyceryl-4 Laurate (commercial 1) Unstable
E Polyglyceryl-4 Laurate (commercial 2) Unstable
F PolyAquol™–LW 3Stable
Water Phase: Water, preservative* Oil Phase: Dicaprylyl Ether
No need of homogenizer
A, B and C D and E
Comparison with liquid polyglycerol-based O/W emulsifiers
EmulsifierOil
Phase*Viscosity (cPs)**
Stability(1 month at 50°C)
A Polyglyceryl-4 Laurate/Succinate, Aqua
5% 10%
1025 Unstable
BPolyglyceryl-3 Cocoate, Polyglyceryl-6 Oleate, Propanediol
n.a. Unstable
C Sorbitan Laurate, Polyglyceryl-4 Laurate, Dilauryl Citrate 1200 Unstable
D Polyglyceryl-4 Laurate (commercial 1) 1000 Unstable
E Polyglyceryl-4 Laurate (commercial 2) 1565 Unstable
F PolyAquol™–LW 1000 3Stable
Water Phase: Water, Xanthan Gum, preservative* Oil Phase: Prunus Amigdalus Dulcis (Sweet Almond) Oil, Caprylic/Capric Triglyceride, Paraffinum Liquidum** Brookfield, RVDV-i Prime, Sp 03, 20 rpm
25ºC
Cold process emulsion
Superior stability
More homogeneous emulsion
Fine particle size distribution
PolyAquol™-LW
Optical microscopy analysis 600x
A
C
D
F
E
Compatibilty with different lipid phases
Vis
cosi
ty (c
Ps)
0
800
600
200
400
100
1200
1400
Prunus AmigdalusDulcis (SweetAlmond) Oil
Caprylic/CapricTriglyceride
innollient™LO ParaffinumLiquidum
PolyAquol™-LW forms stable emulsions and low viscosity regardless of the lipid phase polarity
Compatibility with rheological modifiers/thickeners
PolyAquol™-LW is compatible with various synthetic thickeners
Synthetic thickeners
P-LWOil
Phase*Thickener %
Viscosity (cPs)**
Stability(1 month at 50°C)
5% 10%
A Carbomer 0.10 1600 3Stable
BAcrylates/C10-30 Alkyl Acrylate Crosspolymer
0.10 1080 3Stable
CAmmonium Acryloyldimethyltaurate/Beheneth-25 Methacrylate Crosspolymer
0.15 950 3Stable
DAmmonium Acryloyldimethyltaurate/VP Copolymer
0.30 2500 3Stable
E Sodium Polyacrylate 0.30 2100 3Stable
F Polyacrylate Crosspolymer-11 0.30 2500 3Stable
* Oil Phase: Prunus Amigdalus Dulcis (Sweet Almond) Oil, Caprylic/Capric Triglyceride, Paraffinum Liquidum** Brookfield, RVDV-i Prime, Sp 03, 20 rpm
25ºC
PolyAquol™-LW Thickeners
Vis
cosi
ty (c
Ps)
0
2000
1500
1000
500
2500
3000
A B C D E F
Naturally derived thickeners
P-LWOil
Phase*Thickener %
Viscosity (cPs)**
Stability(1 month at 50°C)
5% 10%
A Dehydroxanthan Gum 0.30 2100 3Stable
B Xanthan Gum 0.50 1000 3Stable
C Sclerotium Gum 0.50 750 3Stable
DMicrocrystalline Cellulose (and) Cellulose Gum
1.20 700 3Stable
E Magnesium Aluminum Silicate 2.00 890 3Stable
F Hydroxypropyl Starch Phosphate 3.00 820 3Stable
* Oil Phase: Prunus Amigdalus Dulcis (Sweet Almond) Oil, Caprylic/Capric Triglyceride, Paraffinum Liquidum** Brookfield, RVDV-i Prime, Sp 03, 20 rpm
Vis
cosi
ty (c
Ps)
0
1500
1000
500
2000
2500
A B C D E F
Vis
cosi
ty (c
Ps)
0
1500
1000
500
2000
A B C D
PolyAquol™-LW is compatible with various naturally derived thickeners
A 0.3% Xanthan Gum + 1.0% Hydroxypropyl Starch Phosphate
B 0.3% Xanthan Gum + 1.2% Microcrystalline Cellulose (and) Cellulose Gum
C 0.3% Xanthan Gum + 0.4% Sclerotium Gum
D 0.5% Xanthan Gum + 1.0% Tapioca Starch
Formulations with PolyAquol™-LW
Cold process Lotion TR 52-09
INCI Name % Function
Phase A
Water (Aqua) up to 100.00
Glycerin 3.00 Humectant
Phase B
Sodium Polyacrylate 0.30 Thickener
Phase D
PolyAquol™-LW 3.00 Emulsifier
Prunus Amigdalus Dulcis (Sweet Almond) Oil 5.00 Emollient
Caprylic/Capric Triglyceride 3.00 Emollient
Parafinum Liquidum 2.00 Emollient
Phase E
Preservative a.n. Preservative
Parfum a.n. Parfum
VISCOSITY after 24h Brk, RVDV-I Prime, Sp 03, 20 rpm pH (100%) 1500 - 2000 cps 5.0 - 7.0
Cold process
Low viscosity
Light and fresh texture
25ºC
Cold process emulsion
PolyAquol™-LW
Wet Wipes Lotion CP 17-18-26D
INCI Name % Function
Phase A
Water (Aqua) up to 100.00
Phase A1
Water (Aqua) 20.00
Phase B
PolyAquol™-LW 5.00 Emulsifier
Dicaprylyl Ether 1.00 Emollient
Preservative a.n. Preservative
Phase C
Polysorbate 20 a.n. Solubilizer
Parfum a.n. Parfum
VISCOSITY after 24h Brk, RVDV-I Prime, Sp 03, 20 rpm pH (100%) 200 - 300 cps 5.0 - 7.0
Low energy emulsion
No need for homogenization
Super low viscosity
PolyAquol™-LW
PolyAquol™–LWThe selection of highly purified polyglyceryl and fatty acid building blocks coupled to a molecular engineering know-how led to the creation of PolyAquol™-LW (patent pending). The key features of PolyAquol™-LW reside in its ability to form O/W emulsion in a cold-process environment while achieving very low levels of viscosity. It can be incorpo-rated in the water phase or in the oil phase, independently. Those characteristics make PolyAquol™-LW perfectly suited for “one-pot” emulsions and also low-energy process avoiding the use of heat or homogenization. Moreover, its Cosmos status and palm-free origin make it an ideal candidate for green formulations. Thanks to its molecular de-sign, PolyAquol™-LW outperforms other emulsifiers with an apparent similar chemical composition.
Technical information INCI (proposed): Polyglyceryl-4 Laurate, Polyglyceryl-6 Laurate
Cold process O/W emulsions
One-pot emulsions
Low energy systems
Recommended use level: 2-5%
Works in a pH range from 3 to 9
Whitish thick liquid
PolyAquol™-LW is compatible with:
– Lipid phase with different chemistry and polarity
– Synthetic and naturally derived thickeners
Applications Skin care
Sprayable lotions
Milks
Wipes
– Baby care
– Cleansing
– Makeup removal
Fabric masks
Sun care
Green emulsions
Background
Formulation
Innovacos corp.111 Howard Blvd, Suite 160 Mt. Arlington New Jersey 07856
www.innovacos.com
© 2018 by Innovacos corp. All rights reserved Conception and design Symbiose design-graphique
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