fiber development laboratory

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Matt Weisenberger, PhD Carbon Materials Associate Director University of Kentucky Center for Applied Energy Research 2540 Research Park Drive Lexington, KY 40511 Phone: 859-257-0322 Fax: 859-257-0302 Email: [email protected] Fiber Development Laboratory The UKY CAER Fiber Development Laboratory contains the largest soluon spinning line found in an academic seng in North America. The Carbon Materials research group has decades of experience in process development for experimental polymers and fibers. The fiber devel- opment laboratory bridges lab-scale to pilot-scale manufacturing development. Fiber Development Laboratory Research Areas include: Mulfunconal fibers, smart texles, and composites Electrically conducve/thermal texles Polymeric precursor fibers Use of bio-derived polymers Thermally conducve composites and interfaces Incorporaon of acvated carbons for lightweight/wearable chemical/biological protecon Details of the UKY CAER Soluon Spinline: Soluon spinning (PAN as precursor for carbon fiber, PES, biopolymers, etc.) 8 hour day start up, operaon and stop—no shiſt work required Mulfilament (500-count), connuous tow wet-jet and/or air-gap soluon spinning Dope formulaon from polymer powder, including rheological characterizaon Spinline includes: dope filtraon, jet formaon, coagulaon, washing, stretching, hot-stretching, spin-finish applicaon, drying and winding Other Capabilies: A hollow fiber/mulcomponent fiber spinline for developing membrane separaon and mulcompo- nent fibers Melt spinning of thermoplasc polymers, coal-tar and petroleum pitch (isotropic and mesophase) www.caer.uky.edu (Top Leſt) Over 700 m of 0.5k tow connuous PAN fiber. (Top Right) SEM cross secon of PAN fiber. (Boom Leſt) Air-gap soluon spinning. (Boom Right) Wet-jet soluon spinning PES hollow fiber UKY CAER mulfilament, connuous tow soluon spinning line Mesophase pitch fiber

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Matt Weisenberger, PhD

Carbon Materials Associate Director

University of Kentucky Center for Applied Energy Research

2540 Research Park Drive

Lexington, KY 40511

Phone: 859-257-0322

Fax: 859-257-0302

Email: [email protected]

Fiber Development Laboratory

The UKY CAER Fiber Development Laboratory contains the largest solution spinning line found in an academic setting in North America. The Carbon Materials research group has decades of experience in process development for experimental polymers and fibers. The fiber devel-opment laboratory bridges lab-scale to pilot-scale manufacturing development.

Fiber Development Laboratory Research Areas include:

Multifunctional fibers, smart textiles, and composites

Electrically conductive/thermal textiles

Polymeric precursor fibers

Use of bio-derived polymers

Thermally conductive composites and interfaces

Incorporation of activated carbons for lightweight/wearable chemical/biological protection Details of the UKY CAER Solution Spinline:

Solution spinning (PAN as precursor for carbon fiber, PES, biopolymers, etc.)

8 hour day start up, operation and stop—no shift work required

Multifilament (500-count), continuous tow wet-jet and/or air-gap solution spinning

Dope formulation from polymer powder, including rheological characterization

Spinline includes: dope filtration, jet formation, coagulation, washing, stretching, hot-stretching, spin-finish application, drying and winding

Other Capabilities:

A hollow fiber/multicomponent fiber spinline for developing membrane separation and multicompo-nent fibers

Melt spinning of thermoplastic polymers, coal-tar and petroleum pitch (isotropic and mesophase)

www.caer.uky.edu

(Top Left) Over 700 m of 0.5k tow continuous PAN

fiber. (Top Right) SEM cross section of PAN fiber.

(Bottom Left) Air-gap solution spinning. (Bottom Right)

Wet-jet solution spinning

PES hollow fiber

UKY CAER multifilament, continuous tow solution spinning line

Mesophase pitch fiber