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EXPANDED SITE INSPECTION REPORTFOR
H.O.D. LANDFILLANTIOCH, ILLINOIS
U.S. EPA ID: ILD980605836SS ID: IL2F
TDD: F05-8702-124PAN: FIL0141XB
VOLUME 3 OF 4
Field Investigation Team Zone II
EPA39
HAZARDOUSSITEEVALUATIONDIVISION
CONTRACT NO.68-01-7347
EXPANDED SITE INSPECTION REPORTFOR
H.O.D. LANDFILLANTIOCH, ILLINOIS
U.S. EPA ID: ILD980605836SS ID: IL2F
TDD: F05-8702-124PAN: FIL01A1XB
VOLUME 3 OF 4
SEPTEMBER 22, 1989
ecology and environment, inc,111 WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL 312-663-9415
International Specialists in the Environment
recycled paper
TABLE OF CONTENTSVOLUME 3
Appendix • Page
G LABORATORY ANALYTICAL DATA OF FIT-COLLECTED SUBSURFACESOIL SAMPLES.............................................. G-l
11
Contract Laboratory ProgramTarget Analyte Ujt
Inorganic Quantitation Limits
COKFOUND
Aluminum. Ant loony
ArsenicBarltmBerylliumCadalumCalciumChromiumCobaltCopperIronLeadKagnesiumKanganeseKercuryKickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
PROCEDURE
ICPFurnacefurnace1C?ICPICPICPICPICPICPIcpFurnaceICPICPCold VaporICPICPFurnaceICPICPFurnaceICPICP
SOILVATER
200 ug/L601020055
50001050251005
5000150.240
5000510
5000105020
SEOIHEKTSLUDGE
*0 ag/Kg2.424011
10002105201
100030.0088
100012
10002104
Cyanide Color 10
Contract Laboratory ProgramTarget Compound List
Pesticide and PCS Quantitation Limits
COMPOUND
alpha-BBCbeta-BBCdelta-BBCgamioa-BflC (Lindane)BeptachfcoCAldriaBeptachlor epoxldeEndosulfan IOieldrln4.4MXTCEndrioEndosulfan H4,4'-000Endostufan sol fate4t4'-ODTHethoxychlor (Maria te)End r in ketooealpha-Chlordinefault— chlordaneToxapheneAROOJO&-1016AROCLOR-1221AROCLOR-1232AROCLOR-1242AROCLO&-1248AROOO&-1254AROCLOR-1260
CAS ff
319-84-6319-85-7319-86-858-89-976-44-e
309-00-21024-57-3959-98-860-57-172-55-972-20-8
33213-65-972-54-8
1031-07-850-29-372-O-5
53494^70-55103-71-95103-74-28001-35-2
12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
WATER
0.05 tig/L0.050.050.050.050.050.050.050.100.100.100.100.100.100.100.50.100.50.51.00.50.50.50.50.51.01.0
SOILSEOIKEKT
SLUDGE
8 «g/X«8888888
1616161616161680168080
1608080808080
160160
Contract Laboratory ProgramTarget Compound List
Seaivolatlles QuantiUtIon L
COMPOUND
Pluorene4-Nltroaqillne4 , 6-Olnl tro-2*«e thylphenolH-nitrosodlphenylaalne4-Bronophenyl~phenyletberBexachlorobenzeneFen tachlorophenolPhenan threatAnthraceneDi-o-butylphthalateFluoranthenePyreneButylbenzylpbthalate3f3'-0ichlorobentldlneBe&zo(a)*nthraceneChryceneb 1 a (2-E tbylhexyl) ph thala t eDi-n-octylphthalateBenzo(b) floortn thcaeBenzo(k)noorantheneBenxo(a)pyreneXndeao(lv2t3-«d)pyreneDlbenz(afh)antAraceneBenzo(g(ht l)perylene
CAS 1
86-73-7100-01-6534-52-186-30-6
101-55-3118-74-187-86-385-01-8
120-12-784-74-2
206-44-0129-00-085-68-791-94-156-55-3
218-01-9117-81-7117-84-0205-99-2207-08-950-32-8
193-39-553-70-3
191-24-2
VATER
10 ug/L5050101010501010101010102010101010101010101010
SOILSLUDGE
SEDIMENT
330 ug/Kg16001600330330330
1600330330330330330330660330330330330330330330330330 -330
Contract Laboratory ProgramTarget Compound List
Se»lvol«tll«s Quantitatloa Limits
COMPOUND
Phenolbis(2-Chloro«thyl) ether2 -Oilo ro phenol1 f 3-Oichlorobenzene1 f 4-OlchlorobenzeneBenzyl Alcohol1 , 2-Oichlorobenzen«2-Hethylphenolbls(2-Chlocolsopropyl) ether4-HethylphenolN-Nitroso-dl-a-dipropylaalneBexachloroe thaneNitrobenzeneIsophorone i2-Nitrophenol2,4-OiBethylphenolBenzole Acidbls(2-Chloroethoxy) Methane2 , 4-Oichloropbenol1,2,4-TrlcalorobenzeiieNaphthalene4-ChloroanillaeBexachloroba tad iene4-Chloro-3-*ethylphenol2-He thylnaph thalen«Bexachlorocyclopentadlene2 , 4 , 6-Trlchloropbenol2 « 4 1 5-Trlcbloro phenol7— TMi>rfwiiphT*'*l Tvt2-MitroanllineOinethylphthalateAcenaphthylene2 , 6-Olnl t rotoloene3-NitroanilineAcenaphthene2 , 4-Olni trophenol4-NltrophenolDlbenzoCuran2,4-DlnltrotolueneDlethylphthalate4-Chlorophenyl-phenyl ether
CAS 1
108-95-2111-44-49S-57-8541-73-1106-46-7100r51-695-50-195-48-7108-60-1106-44-5621-64-767-72-1 .98-95-378-59-188-75-5105-67-965-85-0
Ul-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-4M-Sft-7^w— •88-74-4131-11-3208-96-8606-20-299-09-283-32-951-28-5100-02-7132-64-9121-14-284-66-2
7005-72-3
VATER
10 ug/L10101010101010101010101010101050101010101010101010105010501010105010505010101010
SOILSEDIMENTSLUDGE
330 ug/T330330330330330330330330330330330330330330330160033033033033033030033033033033016003301600330330330160033016001600330330330330
Contract Laboratory ProgramTarget Coapound ListQuantltatlon Ll«its
COMPOUND
Chloroae thaneBcooooe thaneVinyl chlorideChloroe thaneKethyltn* chlorideAcetoneCarbon disulfide1 1 1-dichlocoetheneltl-dlchloroe thane1,2-dichloroethene (total)Chloroform1,2-dichloroe thane2-butanone (HEX)1,1, 1-trichloroethaneCarbon tetrachlorldeVinyl acetateBrooodichlorooe thane1,2-dlchloropropanecls-lf3-dlchloropropeneTrichloroetheoeDibroftocblor o*e thane1 1 l«2-trlchloroe thaneBenzeneTrans-1 ,3,-dichloroBtopeneBrooofon4-Kethyl-2-pentanoae2-BexftnoneTe t rachloroe theneTolene1 , 1 , 2 , 2-tetrachloroe thaneChlorobenzeneEthyl benzeneStyreneXylenes (total)
CAS I
7A-87-374-83-975-01-A75-00-375-09-267-64-175-15-075-35-A75-34-3
S40-S9-067-66-3
107-06-278-93-371-55-656-23-5
108-05-475-27-478-87-5
10061-01-579-01-6
124-48-179-00-571-43-2
10061-02-675-25-2 -
108-10-1591-78-6127-18-4108-88-379-34-5
108-90-7100-41-4100-42-51330-20-7
VATER
10 ug/L1010105
10555555
1055
10555555555
10105555555
SOILSEDIMENT
SLUDGE
10 ug/K«10101055555555
1055
10555555555
1010 -5555555
ecology and environment, incr111 WEST JACKSON BLVD.. CHICAGO. ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
FTDate Received for ReviewTO: ^VnFrom: Zena Gold-KaufmSubject: HOO
PAN:
Date Review Completed
Case
Sample Description______Organics (VOA, ABN, Pest/PCB
Kb Low SoiLow WaterDrinking WaterOther
Inorganics (Metals, Cyanide)
Low SoilLow WaterDrinking WaterOther
•Project Data Status Completed!
Incomplete, awaiting:
FIT Data Review Findings:Samples
Voft 51/UJm fLSb? o>>'
Cci nrnOA jlttirQjrd p /LO lfe .
Compounds were detected in sample(s); see enclosed Chemical• Evaluation Form.
Book No. Page No. sk
/if
: T/t/17
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V
LJM It. i f f y u f .—•
/•^
SUBJECT: Review of Region V CLP Data..Received for Review on
FROM: Curtis Ross, Director (5SCRL)Central Regional Laboratory
TO: Data User: pi T
We have reviewed the data for the following case(s).
SITE NAME:__ttoT) Z^AfSFfC*-__________SMO case No.No. of D.U. /Activity
ERA Data Set No .spy* tr/SF*to<.9 Samples: /& Numbers
CRL No.
SMO Traffic No. g7 Mrs. Required
CLP Laboratory: ^/V/I//^ODVAJ*£' for Review:
Following are our findings:
^-^^ P&sr/c,/z>e/'p<L8'5 ,#7- /*7&>sur> ^eTi/^'c FOR v&ur/ces . .i, OTM€# AMfityscs uje*.g fir
( ) Data are acceptable for use.(**) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory(z<) Data are unacceptable. *& e<_*67 p&r
cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas
EPA FORM 1320-6 (Rev. 5/87)
//
DATA QUALIFIERS
CfCase TV
Below is a summary of the out of control audits and the possible effecton the data for this case:
X
<?/r ,$•> fc- rve
/5
V
Reviewed by:
Phone:
Date:
//
DATA QUALIFIERS
Contractor:Case 735-v
. . - . - . . . - .Below Is Vsummary of the out of control audits and the possible effecton the data for this case: rf\
AT
AT
TO
Reviewed by:
Phone:
Date:
I
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
VOLATILE HSL COMPOUNDS7357 - - - CONTRACTOR £
W/#y7&Av?»7- 5-?**--*
DATE/TIME:
ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Oisulfide1,1-Dichloroethane1,1-Dichloroethene>ans-l,2-Dichloroethene
^vhloroform2-Butanone1,2-Dichloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1,2-DichloropropaneTrans-l.3-D1chloropropeneTrichloroetheneDi bromoch 1 oromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Di chl oropropene2-Chl oroethyl vi nyletherBromofonn'-Methyl -2-Pentanone
-]2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem-Xvleneo/p-Xylene
AFFECTEDSAMPLES:
nit. Cal.C-3-S7
F
•
IRSD *
€Tor-€J-;aJttjr4-«j4-7et-*etf3ffCSJ-tf^Jl)
Cont. Cal.*->J7/'*:VX
RF %0
591 3
3/2
3.J.Or/.A
37. A
*
J
J
JJ
3"
«JI*T" erwie<- ui- cuts*
Cont. Cal .\-^.f? /607
RF to3/3
*
J
fcCa^TyHJ
Cont. Cal.•y-rr /tt:*3
RF ID
*
*
€cas-?/*fS5
Cont, Cal. '*\
RF *D *
vo
These flags should be applied to the analytes on the sample data sheets.
1/87
//
UNITED STATES
CASE* 7W/ '
/#&—£**** €*>T ***$•-/DATE/TIME:
ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Pisulfide1,1-Dicnloroethane1,1-DichloroetheneTrans-l,2-DichloroetheneChloroform2-Butanone1,2-Di chl oroethane1 , 1 ,1-Tri chl oroethaneCarbon TetrachlorideVinyl AcetateBromodi ch 1 oromethane1 , 2-Di chl oropropaneTrans-l,3-DichloropropeneTrichloroetheneDibromochl oromethane1 ,1 ,2-Tri chl oroethaneBenzeneci s-1 ,3-Di chl oropropene2-ChloroethylvinyletherBromoform4-Methyl-Z-Pentanone2-KexanoneTetrachloroethene1,1,2 ,2-Tet rachl oroethaneTolueneChlorobenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene
AFFECTEDSAMPLES:
EWIRONMENTAL PROTECTION AGENCY REGION V. CALIBRATION OUTLIERS -VOLATILE HSL COMPOUNDS _ '£
" * CONTRACTOR &twtoSb>*J£ \e
nit. Cal.&-S~-€7
F
•
XRSD3f
*
O"
&JU.9- fLJLC*
..
Cont. Cal.£•//•>? /C-lfRF %D
— •
*,0"
*r^S(io
--T^— — -—— ' -
Cont. Cal.-'/ *7//?.'/e
RF XD
s*>
*
J
J-
zt-s&i-etA^-s
Cont. Cal.•/A-f7A:a*
RF ID
vy
3<*
'
*
J3*
, -
et?4^-frX364
Cont. Cal.
RF •-o
-
*
• • . . -.; j t
\^^
1
V3
tP
These flags should be applied to the analytes on the sample data sheets.
CASE*
UNITED STATES EHVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
VOLATILE HSL COMPOUNDSCONTRACTOR
-DATE/TIM£:ChloromethaneJromometnaneVinyl ChlorideChloroethaneMetnylene ChlorideAcetoneCarbon Oisulfide1,1-Dichloroethane1,1-DichloroetheneTrans-1 ,2-DichloroetheneChloroform2-Butanone1,2-Dicnloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1,2-DichloropropaneTrans-1 ,3-Di chl oropropeneTrichloroetheneDi bromochl oromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Di chl oropropene2-Chl oroethyl vi nyl etherBromoform4-Methyl-Z-Pentanone2-HexanoneTetrachloroethene1,1,2 ,2-Tet rachl oroethaneTolueneChlorobenzeneEthyl benzeneStyrenem-Xyleneo/p-Xylene
AFFECTEDSAMPLES:
nit. Cal.£-AT- ? 7
F
-
•
tRSO
7^6>9
•- -
*
•To
&J3CS)«6»t7-««
i=<J47/ aO
;ont. Cal .•vd'-/7//'-''*IF %D
?<6
JJ*31
48
37
*
J"J
J0"
0*
J*
^ca<i7<=£-*& 7#SffC?67>H5&
Cont. Cal.lCont. Cal .
RF ID * RF-
ID
-
*
-
Cont. Cal.
RF %D *
k\
* These flags should be applied to.the analytes on the sample data sheets,
1/87
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION .OUTLIERS
SEMIVOLATILE HSL COMPOUNDS. .. j. :.: JPage 1)
"• •-• : ' • - - ' - - ; - CONTRACTOR
• / **y4b*>ifMT s~??<~DATE/TIME:
Phenolbis(-Z-Chloroetnyl JEther2-ChloPOphenoll,3-0ichlopobenzene1 ,4-Di chl orobenzeneBenzyl Alcohol1,2-01 chl orobenzeneZ-Methylphenolbis(2-chlopoisoorooyl JEther4-Methyl phenolN-NitPOSO-Di-n-? ropy 1 ami neHexachlopoethaneNitrobenzeneIsoohoponeZ-Nitrophenol2, 4-01 methyl phenolBenzole Addbis(2-Chlopoethoxy)Methane2 ,4-DI cnl opophenol1 ,2 ,4-Tpi chl orooenzeneNaphthalene4-Chloroan111neHexachlopobutadiene4-ChloPO-3-Methyl phenol2-Methyl naphthaleneHexachl opocyclooentadi ene2,4 ,6-Tpi chl opoohenol2,4,5-TplchloPophenol2-Chloponaohthalene2-NitPoanil1neDimethyl PhthalateAcenaohthylene3-NitPoanilineAcenaphthene2,4-DinitPOPhenol4-NitrophenolOlbenzofuran
AFFECTEDSAMPLES:
Enit. Cal.^-/?-Jf7RF XRSD *
•
^.y&>?.£>
?Tf
j
JO*
«=j-/as~€JWW>»S<£JV< r>»*&T/-7C.
:ont. Cal. Cont. Cal.
RF *D
••-.
*
--
"- - -
RF -0 *
;ont. Cal.lCont. Cal.
RF
.
•
%D * RF %0
-
*
* These flags should be applied to the analytes on the.samole data sheets,
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDSPage 2CONTRACTOR
•xv/#STKtv»etoT $"?f&.
DATE/TIME:
2,4-D1nitrotoluene2,6-OinitrotolueneDiethylpmnalate4-Chloroohenyl-phenyletnerFluorene4-N1troaniline4,6-D1nitro-2-MethylphenolN-Ni trosodi pheny 1 ami ne4-3romoohenyl-phenyletnepHexachl orobenzenePentachl orophenolPhenanthreneAnthraceneDi -n-Buty } phtnal ateFluoranthenePyreneButyl benzyl phthal ateBenzo( a) Anthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyt PhthalateBenzo( b )F1 uorantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneOibenz(a,h)AnthraceneBenzo(g,h,1 ) Perylene
[nit, Cal.£•/» - 9 7RF 1RSU
SQg
*
CT
Cont, Cal.
RF %U
-
*
Cont. Cal.lCont. Cal.
RF I ID * RF
•
ID *
Cont. CiV.*£«
RF M * • t
SEE PAGE 1 FOR AFFECTED SAMPLES.
These flags should be applied to the analytes on the sample data sheets.
1/87
CASE?
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDS(Page 1)
CONTRACTOR \/W57*c4/>7fA/r $-rr&DATE/TIME:
Phenolbis(-2-Chloroethyl )Ether2-Chloroohenol1 ,3-Oi chl orobenzene1,4-01 en 1 orobenzeneBenzvl Alcohol1 ,2-5 i chl orobenzene2-Mernylohenolbisi2-chloroisoorooyl JEther4-Metnyl phenolN-Nitroso-Di-n-? ropy 1 ami neHexachloroethaneNitrobenzeneIsoohorone2-Nitrophenol2, 4-Qi methyl phenolBenzoic Acidbi s ( 2-Ch 1 oroethoxy )Methane2,4-Oichlorophenol1,2,4-TrichlorooenzeneNaonthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-Methyl phenol2-Methyl naphthaleneHexachl opocyclooentadi ene2,4t6-Trichloroohenol2,4,5-Trichlorophenol2-ChloronaPhthalene2-Nitroanil1neDimethyl PhthalateAcenaohthylene3-NitroanilineAcenaohthene2,4-D1nitroohenol4-iNitroohenolDibenzofuran
AFFECTEDSAMPLES:
Init, Cal.C'tj-g-r
RF XRSD *
I1
•
<&&3L.S-
Cont. Cal. Cont. Cal. Cont. Cal. Cont. Calic^
RF %D
O"3"
er/37^rag
€-<-?j<-ffd*47
-
* RF %0 *
1
i
iRF ID » RF %D *
•
1 1
i
* These flags should be applied to the analytes gn,the.sample data sheets
1/87
CASEI 73^7
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDSPage 2 __
CONTRACTOR
'ATE/TIME:
2,4-Dinitrotoluene2,6-DinitrotolueneDietnylohthalate4-Chloroohenvl-phenvletnerFluorene4-Nitroaniline4, 6-Qinitro-2-Methy] phenolN-Ni t rosodi pheny 1 ami ne4-3 romoohenyl-phenyl etherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButyl benzyl pnthal ateBenzol a JAnthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl PhthalateBenzo(b)FluorantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneOibenzt a, n) AnthraceneBenzo(g,h,1) Perylene
Init6-/3
RF
. Ca-97%RSD
&$,3
. I
*
3"
Cont
RK
. Ca
%0
•
* 11
Cont
kh
. Ca
*D1
11
1
.1
*11
Cont
kh
. Ca
%D
.1
*
Cont
kH
. Ca
ID
-^*
SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytes on the sample data sheets.
1/87
//f //ENVIRODYNEENGINEERS
June 25, 19871990-07351
Ms. Carol ShaefferSample Management Office300 North Lee Street, Suite 200Alexandria, Virginia 22314
Dear Ms. Shaeffer:
Enclosed are'the results of analysis of sixteen samples from Case 7351 forvolatiles, semivolatiles, and pesticides/PCB's performed under Contract68-01-7087. This report covers eight soil samples, EJ 125 through EJ 128and EL 256 through EL 259, received by Envirodyne on May 27, 1987, andeight soil samples, EL 260 through EL 267, received on June 4, 1987. Onematrix spike and matrix spike duplicate for low level is included withthese samples.
All samples were screened and extracted by the low level method for BNA'sand pesticides/PCB1s. One volatile sample, EL 267, was outside the lowlevel range in several compounds, so was analyzed by the medium level soilmethod. The limits of detection for the HSL's given on the data sheets formedium level VGA's in this package represent a dilution of 125 from the lowlevel method, because 0.04 grams of soil was purged as compared to thenormal 5 grams aliquot. A matrix spike and matrix spike duplicate were alsoprepared from sample EL 267 for volatile analysis.
If you have any questions about this report, please contact me.
Sincerely,
Margaret C. WinterProject Manager
MCW/sgcEnclosures
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY ^REGION V *X
^DATE ?-V-f 7 <&
SUBJECT: >P<ec./<3^^c. £e5^uAjSt? To CCS /=^/> ^/o^-^ -7^5-, ^0
X7 .. , . . — .. *X ~ « _FROM:
TO:
7 /s «ejec.7f-o ffcc^sc /r
2>/o
EPA FORM 132&4 (REV. 3-7C)
~
Caa« No.Low ——
Contract Laboratory HLOJWk)6 Contract No. Vft-CM-Medium
VOLATILE SEMI-VOLATILE
U.tflC•0.
Ui-uf l
i.i oi(tHtlif -04 •CNllNC-OI
111- (HI
• 14
nt-un II*- Mil lll'iltl lt*-llt|
• lltltfi**
4174
It, UMnq 113
EL2 (oU HL, (oM
It_S-X.
Hi 4,-? 33-
II SO 6(0yos -U 50 57•si 55-
Ubno 36,
102. 53lo I 94 53 q i
±* VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS
**AftulCnov LIMITS ONLY
VolstilesiSsml-Ptstlcidtl!
O out of kO outsids Of OC limit Ioutside of OC limitsoutildt of QC limit!
M- 4o
7/65
FORM II
Caaa He1 ow „
!•»•'(£•0.
fafc* IH- 1 *\l •*!e L- (*\A I
£t- at! MS£t, 31,1 <W>
,
* VALUES1 *ADVISOR1
Coffvnwi
. M'iSl r.
M«r1bvn I/
on tract Lat
r
inrAlnry fc rWUlRODWAJ^ ST <*nnlr»*l Mn L.X-OI-7f lX7
Ut-ltfl
I DOJl SI ft'ft
> ^'l
•*•lf*-IIU
iGftM>^^
Ml
I.I •>C«tO*0-
>mq^^5
• CHlfNt-lt
111- lift
k)fr
^
-
l-riwcMO*
AlAz^
^t—4^
.
•<*iu-un
A^fl^^ I
1xU
ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS Voliti
f LIMITS ONLY Sami~Ptstic
•^
CMI-VOLATlL
IK-llM
Affl-
.. /-,.^^
Iftll 0 . OUt «f , I 3-- |
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outsidt of QC limit! 7/85outsidt Of QC limit!wtild* of QC limit!
.
FORM II
cL(
4-OIL _.VTL...
•M No, 13 .1 ———————— C
>w lovoL, ^ - *
FRACTION
VOASMO
SAMPLE NO.
B/NSMO
SAMPLE NO.
ACIDSMO
SAMPLE NO.
PESTSMO
SAMPLE NO.
COMPOUND
1.1-0ldtok>rtthtntTrichlorotlhcntChlorobtnitntTolutntBfnnnt1 ,2.4'Trichlorobtntin«Actn«phihtnt2.4 DiniiroiolutntPVrtntN Niiroiodl-n-Propvltmtnt1 ,4-DichlorobtniintPcnucMoro phtnolPhtnol2-CMorophtnol4-Chloro-3-MetHylphtnol4-NitrophtnollindintHtpuchlorAldrinOiiWrlnEndrin4.4'-DDT
SI ..."
rontraol
lotflum
CONC. SPIKEADDED lug/Kg}
toL /S
*tt\fTG
i r
i i/>^c>o
vl/(n.510Sla 3"
1
I
0$-
P^
1 1*0.
' '.....TH... SP. ...; U .1
ar ^K)V/ IR.OOV^^'
Ltvi 1
SAMPLERESULT
AAD
i
5
,
O
^ /
O
CONC.MS
SK5*/^. 55£. )-^•/.3SO. 5H5M650? Gl^ri^QHl O
1417^3^V^t>A<fa_An loCTTiOOc"^
ftMolOSoo
M(0I* (a
*^^-
3-OU/07<Zo
REC
PV1>P59?$*<?-5(j(o3-15*^loO404*f53(/ 16nUMTDloi
1 Cl"7<0GK«r
C F T ",O<
Contract No.
CONC.M5D
(/?._5S/.-556-. 59."5Si\^t*
•j,T)
f,q<jft>1i oRlVoOTl^/sSSVfiTtffLol 36bmtoi)1^-^60IUl'60
64W7SS
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^1 «Q
U»Ov*xfl O
144
m*fc3-
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130|^5f\5I*lU^K
RPD
/ 9/^f
JOlOo\IU1*3T3^10a*743*3S3T•'T
80*n
0, X•73*•XQ*
IV
or I»MIT«*RPD22242121212319473638274735SO3350503143384550
RtCOVCRY50.17262-13760-13359-13966-14238-10731-13728-8935-14241.12628-10417-109269025-10226-10311.11446.12735.13034.13231-13442-13923-134
'ASTERISKED VALUES ARE OUTSIDE oc LIMITS.RPD: vOAi_Q_om of
B/N — Q TT out ofACID—L. out ofPCCT ^* V* V * ^H.
Cofflflwrts; - _ou,
outiWt QC llmlitoutildt QC llmliioutiidt OC II ml 11oulild* OC llmlii
RECOVERY: VOAiJL^out of /° *B/N — Q_out ofACID -C_ outPEST _2Loul of J r;
outtW* OC limit*outiidt QC llmiiiounldt OC llmliioutiidt QC llmiti
FORM III7/85
JOI. JA1....C S CB.~ATL... S1...E l..'LK. CO RY
Contract No.
LOW LtVtl Uadlum L«««l
FRACTION
VOASMO
SAMPLE NO.
tL^U"?
B/NSMO
SAMPLE NO.
JOA
ACIDSMO
SAMPLE NO.JO*
PESTSMO
SAMPLE NO.
•k>A
COMPOUND
1,1-OlcholortthfnfTrichlorofthtntOlorob«nifntTolutntBfnitnt1 ,2.4-TrichlorobentfntActniphthfne7,4 DinitroiolufntPvrtntN-Nitrowdl-n-PropyUmin*1 ,4-Oichlorobtntf mPcntichlorophtnolPhtnol2-ChloropHtnol4.Chloro-3-Mfihylphtnol4-NitrophtnolLindtniHtpttchlofAldnoOitkJrinEndrin4.4'-OOT /
CONC. SPIKEADDED fug/Kgl
C?^ foo
^
_,/
//
/
SAMPLERESULT
L>OfOD
a^oWhut>
* •.
^S"
s
CONC.MS
4010M-tt^b
J5*- 30|l ^6bOTK>
_,s^
/
•
%REC
bt*ao1§i4^a
>^X"
CONC.MSD
SlSlNMlpSOIP Odt>41^0umo
. ^"1^
%REC
5i**U~J^3lo IS
W 9
S
^
RPO
ri\0SC
~fr-
or i IMITS •RPO
7?242121212319473638274735503350SO31433845SO
RECOVERY50-17262-13760-13359-13966-142 ,38-10731-13728-8935-14241.12628-10417-109269025-10726-10311-11446-12735-13034.13231 13442-13973-134
^ASTERISKED VALUES ARE OUTSIDE OC LIMITS.
RPO: VOAi—Q_out of 5 i• ' ; ; B/N«V ACIDlv PESTCofflflwntt!..
out of.out ofout of
outildt QC llmltioutildt OC llmtiioutiidt OC llmliiouiild« OC llmili
RECOVERY: VOAiJL-outofJO.;B/N ———— out of——.;ACID —— out of——.;PEST,__.out of __;
owtiMt OC llmltioutikta QC llmliiouttldt OC llmliioultldt OC llmlti
FORM IM7/85
SOIL MATRIX SPI. ,/MATRIX SPIKE DUPLICA._ RECOVERY•' 1 2 f t f
I ^S ^^ I J — b\ • J AXV 7 * —- ^ A ACat* No. _c=i-LL_________. Contractor g/iki/TQgy/rt;_____. Contract No.
low L«v*l. Medium
FRACTION
VOASMO
SAMPLE NO.
B/NSMO
SAMPLE NO.
ACIDSMO
SAMPLE NO.BL JO?
PESTSMO
SAMPLE NO.
COMPOUND
1,1-Oicnolorethene
TrichloroethcneChlorobenieneTolueneBcn*cn«1 ,2,4-Tr tchlorobenitneAcenaphihent2.4 Dmiiro toluenePyreneN-Nitrotodi-n-Propylamint1 ,4-0ichlorob*nftnePentachlorophtnolPhenol2-Chlorophtnol4.Chloro-3-Mfthvlph«nol4-NiirophtnolLindantHeptachlorAldrinDitldrinEndrin4.4'.DDT
CONC. SPIKEADDED lug/Kg)
too .OOOiI11
V^?/y).ADO
\o?/y)0j
V
.5000
N/
SAMPLERESULT
0
\ /o
*\<" I)/-
\ '
CONC.MS
tf£300//VOOO3 5. OO/J6»COO/01000t\./l\f\J \t/
*^ *^ *^^^Vl
Jtu*y^OLiX5fX>oj?/ 9^007*>L/(Y)O~^C'u' tJ
\fa7(tiJf.%%1
ut2 0
110 A/-><>/*
REC
/03/t^5/O?-^/i/i/ ^yjk5t i t yMl XJ/V 5fi «j*- / y\fr *% J^ Sf
Vs<2(AX-tlfap?J/-)f
^7S ^«
CONC.MSD
Sf/ yiOo}/<focc4*7popllfdob*?V7X?5?^j06/A/.VW)/QtloCQD^/XO^D7pfX>/3ir^£)< (p6O/ rH^n9>^3f?S& /i7a t't/y)
REC
q d/3d6;/ v -jfM/ttil-*?3OG'X/IrT
/0J
fys
JOOf55 ifyos/079i
RPD
ifLf
/O
t£^/>-30//)J l5/ I
t/f> y55 ^?V2>•5 L/
v^V
X v
I1U_ _0p MMITS*HPD
22242121212319473638274735503350503143384550
RECOVERY59-17202-13760-13359-139W-14238-10731-13728-8935-14241-12628-10417-10928-9025-10726-10311-11446-12735-13034.13231-13442.13923-134
*ASTCRISKEO VALUES ARE OUTSIDE OC LIMITS.
RPO; VOAi_——out ofa/N . 0— out ofArm 0 -... OfPEST -oi—. out of
outiidt OC Mmlliouitidt QC Ifmiisoutiide OC llmiiioutiidt OC llmlll
RECOVERY: ^out ofB/N J out ofAC 10. 7 out of/iL;PESTM_out of
outikH QC Mmltioutlkt* QC llmitioutiide QC llmitioutiide QC llmiti
FORM III7 /85
METHOD BLANK SUMMA,.f4
K> V > Con,,.,., Ng
0.1*
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FORM IV 3-1 7/85
ۥȥ No. 1351 Cortrte,
OAK OfAMACTI4 MAtMW SBfe M»t.« COUrOUHB IH»l.,TlC OK UHMtKMNI CMC. UmTI cut*.
10
K
tAMkJtvnu*.
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Comment*:
JjQ»0 -7 ID mfi.,~0^
FORMtV Poj ^cr|3 7/C
$' W' SjvCase No. n»qinn ~5L Contraclor Contract No.,(f % "P '
to 04ICOT r li ACTION en COMPOUND (HSL.fIC ON UNKNOWN) CONC.
-JLUu^Umu^
1O063
BWA smo
5003"
QilC.
Comments:
FORM IV 7/85
Organics Analysii Data Shttt(Pig, i) :—————— ——— ————-———.
t Samplt Nnmbtr: EJ 123
Laboratory Namt: ENVIRODYNELab Samplt ID No: 17002399Samplt Matrti: SOILData Rtloait Aathoriitd By: .
!Cast No: }5QC Rtport No:Contract No: .Datt Samplt Rtctivtd:
Voli11 It Compoondf
Conctntrat ion: LOWDatt Eitracttd/Prtparad:Datt Analysed: (-3-17Cone/Oil Factor: 1Ptrctnt Moiitort (not dtcanttd): 11.24
CiS Nt: •Of CaS It: •1*1
74-17-174-IJ-fTs-ii-475-ll-JH-lf-2(7-44-173-13-173-35-473-14-3134-41-347-U-3117-14-17M3-371-33-4«-23-slll-IS-473-27-4
CklirtBttiaat 1IriBtBttkaatfiijl CkltridtCkltrittkaitHttkrltit Ckl t r idtieittitCarkai Dif iKidi i1,1-DlckUrtitkmI,l-Diekl*rittk»ttriM-l.Z-OUklttottatftiCkltrtftral.Z-Dltiltrtttkut2-litutul.M-TritklireitkiMCarkti Tttriekltrtltfiifl icitattIrtttdlekltrtittkait i
I 9: v2 02 VS*
VI1V0011
2 t11
12 f1 I
71-17-31II41-II-479-IM124-41-171-11-371-43-2lllil-IM111-73-173-J3-2141-11-1J91-7I-4117-11-479-34-Slll-ll-tlll-fl-7111-41-4111-42-3
1.2-DitkIiritritiattraaf-l,3-DickIititrtt»tTrleklirittkiBtBikmi£kltrnttk»t1,1,2-TriaitrtttkaBtItlltBI
cif-1.3-OUklirttrtt»*2-aitrtitkrlTiiflttktrIrmftn (4-RltkfI-2-IIBtlBtBt1-1*1 11 II*TttutklirtttkiBtI.l,2.2-TttraaitrtttkaBtTtlltBICkllttktBftltItkflktBIIBISljriBtTttal XrltBM
0V0VfVV
12 1V
22
0V
Data Ititttiaf Biallfitrf
YUUI:If tkt milt ii a raltt friattr tkti tr tfial tt tki dtttetitiliiit, rt|trt tkt tain.I:Itdieattt eti|tn< vai aialrstl fir kit att 4tttctt4. Itttrt tkt•iiim Itttetiti liiit ftr tkt tamflt vitk tkt 0 (tf.im kaitd•• itetfiarr ctietit.Uilitlti aetita. (Tkii is ait itetssarll|tkt iutrntat ftttttlti liiit.) Tit ftttattt fkttll rial: V-CtiftiU wi utl;n4 ftr kit itt dtttcttd. T*i inktr li tki•iii ••• attiliaklt Ottctlti I it it fir tki iuilt.J:Iiiicttii ai tftliati4 ft In Till fla| ft Hit titktr vkti»tfutli| a ciietatratiii ftr ttatattttlf idtitifitd etmptndfvktrt a 1:1 rtfltiiit Ii .ajfmt* tr «k» tki un ifietral 4ataii<ieatt< tkt trtstict if a cutm* tkat mti tkt UtitifUatUacriticla kit tkt ruilt It Itfi tkai tki iitcifitt Itttetiti liiitirtattr tk» itrt (if. HJ). If liiit if ditietiti it If t|I aid aetieiitratiti if 3 ifl ii ealetUttd, ttftrt « U.
C:Tkis fla| at|Iitf tt yMtieidt tarautin vktrt tkt idntif ie i -tfti mi etifirmtd ly Kin. Siiflt enptatit M>tUiri«iJ.ll•f/il U tkt (inl Mtcaet iktild kt cnfintd IT CC/HSI:Tkif Utf it utd via aaalfti U ttnt IB klaak ti mil •» alatfli. tt iBdieatti |tiilkli/frikiklt klaak ciituiaatiti udmm tki data Mir tt takt affrttriatt acttti.onn:Otktr flaft aad ftttBittt BIT ti rtfiirtd ti irtftilf itfintkt rtiiltf. If ntd, tktf Mil kt fillr 'tieriktd aid sickdifcriftiti attaektd ti tkt data fvaurr rittrt.
kit
Laboratory Na*e:Case No: 7351
ENVIRQDYNE Sample Number——————————————— -<&- —— i
Organics Analysis Data Sheet(Page 2)
Seaivolatile Compounds
Concent ra t ionDate E x t r a c t *Date Ana lyzedC o n e / O i l FactParctnt Hoist
CASNK
106-45-2Hl-44-495-57-6541-73-1106-46-7WWW95-50-195-W-739638-32-9106-44-5621-64-747-72-19B-95-37WH6B-75-5105-67-965-85-0111-91-112W3-2120-BM91-20-3106-47-887-66-3W-56-791-57-677-47-486-06-295-95-491-5B-7BB-74-4131-11-3•*M «J *OJO TOTJ
9W9-2
: LOWd /P repa red : 6-1-87: -6 ID 0? <o-l3-*"Tor: 1ure (decan ted ) : 18
Phenolbii-(2-aiiraethyl)vthcr2-ttlcrcphenoll,3-Dichl(ratMZB»l,4HhchlerabeizeneBenzyl Alatel1,2-OichlDrabenzent2-ftethylphenalbis-(2-Oilcroi«iprofiyl)ethcr4-fethylptaalH-nitrou-Oi-a^ropylatiMHecachliraethmKtntaamIsgpharm2-ttitrophBwl2,4-toMthylphBBlBsnzoic Acidbis- (Dilaraethay) Nethane2,4-Didilirophenol1 ,2, 4-Trichlarofa«i2B»Niphtlulew4-QilaroaniUnaHn art Icr abut jdieot4-Oil(ro-3-«thylphmol2-HKhylMphthilewHeiachlonrycl opmtadim2^4,fr-TndiIarc?h8nal2,4,5-Trichlonphml2-Chlaronaphtlulnt2-NitroaniliniDiiethyl pbthalatiAcviapthylm3-ttitrMnilini
.2
uokg
810 U810 U810 UB10UBtOUB10U810 U810 U810 U810 U810 U810 U810 U810 U610 U810 U3900 U810 U810 U810 U810 U810 U810 U610 U810 U810 U610 U3900 U810 U39000810 U810 U3900 U
GPC C leanup i YESSep. Funne l E x t r a c t i o n : YES 'Cont in . Liq.-Liq. Ext. : YES (
CASNo:
8>32-951-2H10H2-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-OW534-5M86-30-6101-55-3118-74-187-96-5B5-OH120-12-764-74-2206-44-0129-00-085-68-791-94-156-B-3117-B1-7216-01-9117-64-0205-99-2207-OS-930-32-6193-39-553-70-3191-24-2
Acnapfathene2,4-Oiratn9tmi4-*trop6molDitazohran2,4HKiutrotDluB»2,6HhnitnitQliM>Ktthyl phttulitf4-QUtnphtnyl-phBtvl etherFllKTCOlA-fctnaraline4,4-frioitro-HrthYtphmolM-ui U lauUphenylaiim (1)4-flronptanyl-flb0yl etherItaachlarobenzeMrntadtloraptmlf^m 11I imnmnlt mmARthracneDi-fi-butyl phthalatfFluor «tbe»ryrewButyl-tauyl-pMItilatt3f 3' -Dichlontezidin*BBuo(a)aathraawbis-(2-Ethylhsiyl)phthaliteQryseneDi-irxtyl phthiltttBnzo(b)fluara0thmBnotUflunnthntBmodJpyrenfIndenot 1 , 2,3-cd)pyreneKbetnoii,h)aBtlracw»Bvuol^ulperylm
j^*\GLQ) ( c i r c l e one)^o) ( c i r c l e one)
<**
610 U3900 U3900 U810 U810 U810 U810 U610 U810 U3900 U3900 U810 U810 U610 U3900 U610 U810 U610 U810 U810 U610 U1600 U610 U
fy*610 U810 U810 U810 U810 U610 U810 U610 U
(D-Cannot be separated froa diphenylaaine
FORM 1
Laboratory
NoSample Number
Concentration
Organics Analysis Data Sh*«t(Page 3)
Pesticide/PC Bs
Medium (Circle One) GPC Cleanup^Tes DNo
75
Date Extracted'Prepaced _____Q
Date Analyzed: _____6~tt>'l~l
Cone/Od Factor:
Percent Moisture (decanted)
CASNumber
Separatory Funnel Extraction QYes
Continuous Liquid * Liquid Extraction OYes
ugv*Cg^(Circle OneT
319-84-6319-85-7319-86.858-89-976-44-8309-00-21024-57.3959-99-960-57-172-55-972-20-833213-65-972-S4-81031-07-850-29-372-43-553494-70-557-74-98001*35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha -BHCBeta-BHCDelta -BHCGam ma -BHC (LmdanelHepiacftlorAldrmHeptacWor £poxid«Endosutfan 1DfeWrin4. 4--DOEEndrmEndosutfan II4. 4--DODEMosutfan SuHate4. 4--OOTMetttoxychlofEndrin KcioneChlordancToxaphcntAroclor-1016AfocIor-1221Aroclot-1232Aroclor-1242Atocl<X-1248Aroclof-1254
Aroclor-1260
/6U|t> UIk U.)b aIt uit «_ft [4U U32-W-32. (L72. (A?ZLt?ZU_52 UZl W.(do U31 U.Ifeo U52<?16Ifeo 1^li U,)b9 U
Ifrff U.1t«7 U
32J> W.5Z.n u.
V- * Volume oC extract injected (u(|
V ' Volume of water extracted (ml)
W£ * Weight of sample extracted (g|
V * Volume of total extract (ul)
orW. 3o . 600
Form 1 7/85
•oratory Name , _£-Ml) \\L
• No _____
GASNumber
Organics Analyses Data Sheet(Page 4)
Tanlativftly Identified Compounds
'-.
3..
0-.
Compound
- Pucanong A', KHd rD
i<i roo a r be o
r b© r>
cm
TUiJi/xa^f
Fraction
"7'ftrL_L
10.(I. 1
IS- 5IS . 1
IV S. I
3-l-U. -7
3-S.-I
(ug/f
i10-0 S
morn
For<m 1. Pan B ? es
O r g a n i c * A n a l y s i s D a t a Shut( P a g i 1) !--
5a*pl« Namber: EJ
Laboratory Nami: ENVIHODYNELib SaapU ID No: 87002400SiapU M i t r i i : SOILData Rilttsa Anthociitd 87: .
Caff NoQC Rtport No:Contract Mo: (fQ-6l-Dttt Savpli Rictiftd
V o l a t i I t Compound!
C o n c t n t r a t i o n : LOWD a t a E i t r a c t i d / P r t p a r t d :D a t t A n a l y n d : 4-3-17C o n c / D i l F a c t o r : 1Ptrcint M o i f t o r t (not d t can tad ) 15.43
CIS Ki: CU *•:
74-17-174-ll-f7S-I1-475-11-1TS-lf-247-44-171-tS-l75-15-475-14-1154-41-347-44-3117-14-1M-fl-171-55-434-11-3in-15-475-27-4
Cklirmtkail 1
IriatattkABi 1Tiiyl CklltKi tCklirittkait IRitkrlui CklirUticttiitCirfcti Oii i t lUi1.1-DUkHrtltktil
1,1-DiekIiriitkanttaaf*l,2-DiekI»iutkiitCkliriftra1,2-Bleklirtitkuil-iitu»tl.l.l-TriefclirittkaiiCarbia Titfuhltfiitf l iyt leitatiIrnitflcklicnitkui
2 B2 D2 02 B121110B011
2 V11
12 11 I
11
7I-I7-S11141-12-47»-ll-4124-41-171-11-5Jl-41-211141-11-5111-75-175-2S-2lll-ll-lSH-71-4127-11-479-14-5lll-ll-llll-fl-71IM1-41II-42-S
1,1-OiekUripnpiii 4tiaas-l,l-Ditklit«praptM 4Ttlckltmtktu 4lilriaieklittaitkaii i1.1.2-TriekIiriitkaai 4Bill IB! tclf-l,l-DiekIiripriiiii i2-UIiriitkyltiBylitkir 1Briaifm 44-HitkyI-2-tHtaam2-ItiaataiTitraeklitittkiii1.1,2.2-TitraekliriitkaBiTiliiitQlitiktastiiItkylktiiittItfttaiTital Zyliais
BVBBBBB
2B
22
Data lt|«itlif Qialif i ttf
C:TUDE:If Ui iftilt if a vain frutir tkii »r tiiil t« tkt <*t*eti»liait. iipfrt tk* riln8:
ctBftntf vas aialyii< ftr kit ait Jttiettc'. lipitt tkiJi tKtif i l imit (tr tki umpti vitk tki B (if, 110) laittf
» uctfiarr ctictat. / l i l i t it i actin. (Tiis it Ml i iciff iri lytkt luttntat Ittietlta I l t i t . ) Til (ittuti iioU ctal: V-C»B|i»< wi ualyit4 ftt kit itt 4tt*ct«4. Tki infeir it tkiBitira attt i iafclt littetiii lUlt dr tki tuilt.J:talieatti u tftiutt< Tain. Tkii (Uf li aft< titkir «fc»tftliatiii a ciitaitratiii Ur ttitttirtly ia»t i f i i< CHf»*dtvkiti a 1:1 nittisi li atsntl 11 «k» tkt un f^tctral litaii4ieatatf tki iriiiiet •( a CMtintf tkit uitf tkt UtitUttatltier i t i r ia kit tki milt It Itfi tkai tki iMCifiit Itttetin liait litfriatir tkai itri ( i f , 1IJ). If Halt »f tfitietiia It II t|I u< ituciittatiii if 1 i|I it etleiUtU, rtpirt at JJ.
nil f laf atf l f i f ti f i f t i e i t t Miuittrt vkni tki i l t a t i f i e i -titi nt c»flrai4 ky K/Itt. Siiili e»i*mt itsticUis)*!!ai/il ii tkt fiaal tittaet ikiiU ki eufirai* ky CC/K5I:Hit fla| it till vku tiaiyti ti fml la klaik at nil ai alaafli. It lafieatts |iiiiklt/trikakli klaik ctitiiiiitiii ai<vtrn tki <ata ttir ti Ukt aiyriyriati ictin.OTtU:Otktt (Uff aa4 (tttaitit aiy ki riiiirid ti rr*M^T <*<>•*tkt rti i l tt . If ui4. tkty ant ki f i l l y 4iierikitf aid lickfistriitin atUcki4 ti tki lata tnaary
Laboratory Na>e:Case No: 7351
E N V I R O D Y N E Saaple Nuaber: EJ 12a
Organic* A n a l y s i s Data Sheet(Page 2)
5e*ivolat i le Compounds
Concentrat ion: LOWDateDateC o n c / D i lPercent
xtr ac ted /Prepared: 6-1-87nalyzed: 6-13-87il Factor: 1t Moisture (decanted) : 15.4
CASta
108-95-2 Ptwnol111-44-4 bii-{2-QU<TQBtbyl)ether95-57-fi 2-Ol(rophBiQl541-73-1 l,3-QichlcniwuB)i106-46-7 J,44icfal(rQbnzB*100-51-6 Bmzyl Uotel95-50-1 l,2-Didilx(taizB«95-46-7 2-*thylphral39638-32-9 bii-(2-Q>l(roisopropyl)ether106-44-5 4^ethylphnol621-64-7 H-aitrnHh-ft-propylakne67-72-1 taadtlorathn98^5-3 tttnteum78-59-1 IfflphtrmBB-75-5 2-Nitropnnol105-67-9 2,4-fce*hylphe»l45-65-0 Bwuoietad111-91-1 bii-(Chlxaethmy)nvtham120-0-2 2,4-ttchlxcplwnoli2Hfc™i li2i4~Triciu7D8CW91-20-3 taptithalm106-47-6 4-Qax«niUneB7-6B-3 IfaactilorofefUdiBw59-50-7 4K3u(TQ-3-erthylpnflttl91-57-6 2-fMhyln^hthalew77-47-4 faachla-KyclcvBitadiBitao~vo~2 244)6-Tnoil(n ilMDl95-95-4 2t4,5-Trichlxq)nwol91-58-7 2-OavcnaphtlultneBB-74-4 2-ttitnaniUnB131-11-3 KeKhyl phthalite208-96-€ Aonapthylm99-09-2 3-tfitroanilitt
Sep. Funnel Extract ion : YESQ.
*M
780 U780 U780 U780 U780 U780 U780 U78011780 U780 It790 U780 U780 U780 U780 U780 U3800 U780 U780 U780 U780 U780 U780 U780U780 U790 U780 It3800 U780 U3800 U780 U780 U3900 U
Contin.
Gttfe
B3-32-951-28-5100-02-7132-64-912M4-2606-20-28H6-2
Liq.-Liq. Ext. : YES(
AuMpbtbm2,4-Dira tn hnl4-ttitropb«)lDibenzoftran2,*-tKiitn)tolutt»2,6-DinitratolumDifthyl phtlulitt
7005-72-3 4*{hlaraphe<iyl' )tienyl etherB6-73-7100-01-6534-52-116-30-6Wl-55-3tffl-74-1C-Kr5e-oi-e120-12-781-74-2206-44-0129-00-0B-tt-791-94-156-55-3117-81-7218-01-9117-84-4205-99-22D7-OB-95D-32-8193-39-5SHO-3191-24-2
fluarnt4-fctnurahne416-Oiutro-2-fHhrlphtnolM-nitnaiiiphmylanne (1)4-firoK9tarl-pb«rl etheritaadu nrobenznrBudil oropnBuPtienaitthreniiRttracneDi-n-fautyl phthalateFlurmtliatryrtmBtttyl-bwiyi-pfctJuliti3f3 ' -Dichlmbcaidi neBeno(a)anthracmbis-(2-EthylhByl )phthal«tiQTYIMDi-n-octyl phthalateBeno(h)fliaravtiteMBn»(kmurvth«8mDi4}pyrneInd«i(l,2,3-aI)EnTw»DibeBO U,h) arthr acevBenzo( u)pryle«
i_Nm^ ( c i r c l e one)NQy ci rcl e one)
»- — s
upkg
780 U3800 U3800 U780 U780 U790 U780 U780 U780 U3800 U3800 U780 U780 U780 U3900 U780 U780 U11007VU790 U790 U1600 U780 UWi Sf US -tFTV ^* *^ C^Trf
780 U790 U790 U790 U780 U780 U780 U780 U
(1 ) -Canno t be separated f ro* d i p h e n y l a e , i n e
FORM 1
Laboratory Name
case NO _':._Sample Number
Concentration f°™J Medium\^^-Date Extracted 'Prepared ____b_:
Date Analyzed ______o "" fo"~
Cone/Oil Factor: ___________L_
Organlcs Analysis Data Sheet(Page 3) t
Pesticide/PC Bs
(Circle One) GPC Cleanup^Yes DNo
_____ Separatorv Funnel Extraction DYes
————— Continuous Liquid - Liquid Extraction DYes
of\
Percent Moisture (decanted)
CAS ug/lorug^KgNumber (CircU Onet319-84-6319 85-7319-86-858-89-976-44-8309-00-21024-57-3959-96-860-57-172-55-972-20-833213-65-972-54-81031-O7-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha -BHCBeia-BHCOelli-BHCGammj-BHC (Undane)HeptachlorAldrm
HeotacMor EpoxideEndosutfan 1Oieldnn4. 4--OOEEndrinEndosuKan U4. 4--OOOEndosutfan Sutfate4. 4--ODTMettwxvchlorEndrin KetoneChkxdaneToxapneneAroclor-1016AfockK-1221Arocloi-1232Aroc lor- 1242Aiocior-1248Aroclor-1254Aroclor-1260
/ f cUIt U;t \JLIfo i.L\'0 LiIt «Ifc UIt U32- U.3itLTi (A7iU.7zcc52 U-31 1(_Ifco U7^ U.tfe» U52? U.
»f?9 f.d
Uj U')b? iXitr ix\k& U
3^ tc52.1 fx
V- » Volume of extract injected |u()
Vs * Volume of water extracted (ml)
Ws * Wetght of sample extracted (g)
Vt « Volume of tola! extract (uO
orW. 30* lo, ooo
Form 1 7/85
Organic* Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CAS
(««g/t D
n-o
ift.lU-2,
m CjOu f
IS.i 5563
. 6 5^03
4-1.
3*65tJiikftI I . -_ !„ .
*JL* -
? 85
Otginici Xnilytis Dttt Shift(Pigt 1)
1 Simpl t Nambt r tJ 127I——— ——— _- —— —— „ —— _.
L i b o t t t o r y Nimt: ENVIRODYNELib Staplt ID No: 87002401SimpU M i t t i i : SOILD4t» Rilttit A o t h o r i n d By:
C4.. No: ^QC Rtport No: /.1 UContrtct NoD i t t S*mplt R t c t i t t d :
VoUt i l* Compoandf
Conctntrttion: LOWD4t* EitrtcttdfPrtptrid:D4tt Anilytid: 4-3-87Cont/DiI Fictor : 3Ptrcint Koiiturt (not dtctnttd) 15.98
om
OC/5
-O
CO.
CIS Hi: CU Mr
74-17-174-13-175-11-473-11-175-11-147-44-175-15-173-13-473-14-3134-41-347-44-3117-14-1tl-H-l71-53-*54-11-31H-IS-473-17-4
ChlttimtthiitIttmtmttkmTiiyl Ckltti4tUlitittktatE« tljl.it Chltrilt•Cttlll
Cuioi Di i i lUftl . l-DUhlittithtii1,1-Ditkllt i itkutti 4M-1, l-DiekltrtttktitCklittfinI.l-Dithlmtti4*t1-titutiti.l.MilemUitftlmutCttbti Tttutkltti4tTiiyl IttUUItf»t4ltkliinttkiii
41 D41 I41 8il 1fr*l
11 131 131 IIIII11ilII3141II
1) 1
71-17-3llltl-ll-4
71-43*1llltl-ll-3UI-75-173-X3-:lll-ll'l
U7-1I-47t-»-5lll-ll-llll-fl-7111-41-4
TrickltrtttktiiBibimeklttiMtktitI,l,l-Tttek[itittk4iiItutu
Itntdr*
Tili4tklir»»tkntl,l,l.l-Ttti4ckUttitkiitttlitfti
ItkflbtmiimiityituTtt4i tyltiii
31 131 Q31 V3i aII III U31ilII414131II31IIIIIIII
B«U lifirtiif (hil if itn
4itieU»iHUT:U tkt milt ii t vtlit fiittti tkit ti t*nl ttlimit, ttfirt tkt »»ln1
ctmfttmd «•• 4m4lyn4 (tt bit mtt 4ittcti4. li»trt tki4itieti» limit (n tht iimfli with tki 0 drllQ) bi*i4
tm itcifitty et iet i t .Miltt i tm ttliti. (Tk.ii ii tit mtcni4tllytkt iuttatit 4tticti» l i m i t . ) TV« (ttttitt ikt«I4 tti4: B-Cimf«n< vu U4lyit4 (it kit tit ittttt«4. Tki inkit it thtmikima ittunHt 4it»ctl» l imit (it tki iim»ltJ:Imiie4tti 4m tttimati4 ttlit Thli (Uf ii tft4 titbit wbiitittAititf 4 t»etiti4titi tti ttmtittfily 14iiti(it4 ctmyindi•ktti 4 1:1 tt*M"i ii timtl tt wktt tkt min iitetnl i*Uitiitttti tkt itiittci il t cimttnl tk»t a»ti tki Uittidcitltieritiru kit tht ttult ti lilt th4m tht i|ict(lt4 4tttctiim limitlittttr th4t itit (t|, 1IJ). II limit tf 4tttctin ii II <l' *>d itvictitrititi •( 1 ill li c4lc«Utt4, tttttt 4« 3J.
fU| iMliii ti |itticl4i ^iiuitin vktti tkttit* HI etitlrmi* by CCfHS Siiili eii»omt ri«tlei4t<)«ilM'li t« tki (iul ntnet ikitU bt etifirmtl by CCfKSI:Tkii (U| i> "*4 •••» ttiiyti it (ti«4 i» bluk u vtil n 4IU|U. It ii4iutti |tiiibli/|tibiblt bluk e««tuii4tin 4m4«4tu tki 44ti tut ti ttki i f l t tff l ttt t fc t i i t .OTHH:otkti (U|i u< (iitntM MT i« mi'ti* tt in^ t r iT ttiiittki tnilti. II tit4, thif milt bi ( i l ly 4ucitbt4 it4 tick4tictifti«i 4tt4ckt4 ti tht 4tti tomuif t t f i i t .
bit
Laoaratory Naae:Case No: 7351
ENVIRODYNE Sa*ple Nuntier: EJ 12//
Organic* Analysis Data SheetiPage 2)
Setivolatile Conpounas
Concentration: LOWDateDateConc/Di1Percent
x t rac tenalyzef l
a /P repa red : 6-1-87: 6-13-87
Sep. Funnel E x t r a c t i o n : YES \Contin. Liq.-Liq. Ex t . : YES (
J^y ( c i r c le o n e )NQJ ic i rc le one*
il Factor: 1 ^-^t Moisture ( d e c a n t e d ) i 16
CAStta:
108-45-2111-44-495-57-8541-73-1106-46-7100-51*695-50-195-46-73%3fr-S2-9106-44-5621-64-747-72-198-95-378-59-1BB-75-5105-67-965-65-0111-91-1120-63-2120-82-191-20-3106-47-8B7-6B-359-50-791-57-677-47-4BB-06-295-95-491-5B-788-74-4131-11-3208-46-899-09-2
Phenoltu G - (2-QU orathy 1 ) rtrv2-Oilcrop6«ol1,3-Oichlcnteirent1,4-ftchlrobenzentBvayl Alotall,2HhctilcrobmzBW2-HKhylpteulbii-(2-Chloroiscpropyl)ether4-*thylfr*iolIrHl bTOCQ*vl " t~OrQOVl 4B W
F^Bt dOU VQ^CThdftt
tttrcboiatInnhcrtn2-tttnyheiol2,4-OiMthylphmoltaucric Acidbis-IIM£nKthaiy)nBth«2,4-ttdilQrophenol1 ,2, 4-TrichlxobeJueneMjhthilmt4-Qil crovuliniHBadilorobutadicne4-Oiltro-3-wthylphmol2-VthyluphthalencHexachl crocyd cventadi en*2,4,6-ThcfalDrQphcnol2,4,5-Trichlcnptanol2-ChlGrDMphtfealerw2-MitroanilintKvthyl ptithalattAorupthyleit3-tbtnunilint
^
790U790 U7%U790U790U790 U790 U790U790U790U790 U790U790 U7WU790U790 U3BOOU790 U7901179011790 U790U790 U790U790 U7%U790U3800 U790 U3800U790U790U3BOOU
CKfe:
83-32-951-28-5100-$2-7132-M-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-9120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-91-721MI-9117-64-0205-99-2207-06-450-32-8193-39-553-70-3191-24-2
tanaphth«2,Hhnitntfwral4-tttrcpbnolDibvzotirn2,4-Dinitrotolum2tHKnitrotalmDirthyl phtbalatc4-Oilanvteiyl-phenyl ethrFluorne4-tttnunihne4,6-Oi ni tro-2-Hetfayt ptwwlIHutnBotiiphenylMitt (1)4~firoiDpoBiyl' nBtyl etfavta«±Icnt«uwtatadiloroptwnolPtwunthmAntlrKnrOi-n-fautyl phthalati \FliarMtbBWPyrweButyl-totzYl-pbth&lite3,3 ' -OieW crrteu idiwBeuDialanthracBttbi f - 12-Ethyl tey 1 i phthal auQrrsemDi-rrxtyl phthalatiBmiDtblflixrxthinfBmzoOclfluranUcniBBUotal rm!ndena(l,2,3-ol)pyrmDilwizo (*, hi nttar acswBmzofgtulperylm
*,*>7901)38001)3800 U790U790U7?OU790U790U790U3800 U3800 U79011790U790U3BOOU790U
_790U ._ _ _ ^ J \
79o u79411790U1WO U7VOU510 *T VJ'f.Tt790U790U790U790U7WU790U790U790U
(l)-Cannot be separated irom diphenylaaine
FORM 1
Laboratory Name gto \Mft-OPH >^C
Organics Analysis Data Sheet(Page 4)
Tentatively Idontifiod Compounds
Smm&le Number
E3- 1-3-"?
CASCompound NMTM Conc«n(r>t*on
(ug/1
) V ' ™ 1 JLfi.Amir*
ID. 110 ^
13.
14.
15.
16.
17.
IB.
19-
20._
21..
22. _
24..
25..26..27..28..
29..30..
lu^Ar-iv a.rbgv^
VOX)
form 1. P»*1 8 7 85
Organic! Ana Iyiis Data Sheet(Paga 1) I--
Laboratory Name: ENVIHODYNELab Sample ID No: 17002402Sample Hat rii: SOILData Ralaaia Authorised By: .
Ca.. Ho:QC R t p o r t No:C o n t r a c t N o :Data Sample Received
Velat ila Compound!
Concentration: LOWData Citracttd/Piaptrid:D a t a A n a l y s t d : 4-3-17Cenc/Dil factor: 5Parcant Moiitan (not decanted); 14.74
CIS Ma: CIS Ka: aarg
74-17-374-II-f7S-H-475-11-1TS-lf-I47-44-175-15-173-15-475-H-JISt-il-S47-44-1117-li-l71-fl-l71-55-4S4-2I-Illl-IS-475-17-4
Cklarnatkaae 12 9IretaMtkaae It Vfiiyl Ci lar i4a 12 1Cklinataua tl 1Hatkj laaa Ckliti l i 54 1Icataaa &J 1Cirkaa Dtn l f i i tt , l-Dlekltrattkiia1,1-OttkIatMlkaait r>ai- l ,2-DieklateatkaaaUlarafara1,2-Dicklaraatkaaat-htaiau1,1,1-TrieklinathaaaCarlaa Tattiaiarllaftijl leatati 1Z 1lr«aa'taiarnatk«aa * >
71-17-5 l ,:-OickUttBMBaaa 4 U11141-12-4 ttm-l.l-DiekUtiaiatiaa 4 V7f-IU4 Tricalamtktai 4 V124-41-1 liiiiuekUiaMtkaii 4 ffn-lf-S l. l .I-Trieklariatkiaa 4 V71-41-2 laaiata 4 0lllil-ll-S e i i - l , l -Diekl«t«acaftaa 4 9tll-75-l 1-aiartatkTl'iarlitkar 12 I73-25-2 Iraudra 4 0111-11- 4-HatkTl-2-itiUaaaa 12 V3H-7I- 2-liiaam 12 I127-11- TatricklaraatkataT1-J4-S |.l.2.2-Tatnaiaraatka»111-11- Talaaialll-tl- QIar*k»iaia111-41- Elkfliaaiaia1M-42-5 Stfraia
TaUI IT I tin
Data liatrtiaf Qaalidan
III til:If tka raailt if a ralta a,ieater tkaa ar taail ta tka e'etattiealint, raaart tka talae.I:Ia4ieate« eeiaewad MI aulyiaf far kat aat 4atacle4. leant tka•iaiia* aatacttai Iliit (ar tka laaala vitk tka V (af.HQ) iifat*ta aaeasiary caicaat . /J l lat i i i tctiaa. (Tkli (a iat tacanarilytka iaitrtmaat itttctiti H a l t . ) Tka faataati ikaaU raa4: V-Camaaaatf vai aulfta4 (ar kat aat 4it«etia. Tka tamkar !• tka•iaira attaiaakla atttetiti ttiit (ar tka iam|Ia.J:Ii4icita« aa aft imata4 talaa. Tlii (Ia| ii an I" aitier "»*atittutlif a ctteaatrattai (ar ttitatltalf 14aati(ia4 caiaendflvfcara a 1:1 ra«aaaia ti aima4 ar vkaa tka un iitctnl 4ataIi41uta4 tka arenaee at a cnptn< tkat atiti tka t4t i t i f icat ie icriteria kit tka Taialt it laaa tkaa tka faec i f ia4 lataetlaa Itiitl iaatar tkai lara ( i f , 1 IJ ) . If Halt if it tic tin ii II ifl aa4 acaiceatratiai t( I aal ii c«lcitata4, rtptrt " *J
C:fU| aaBliaa ta ya f t i c i l i Baruntiri vkaia tka i t f aa t i t i e i -
tita via caafinaa' if CC/IB. S ia f l a caiaaaaat i * i t i e i l * i ) « l laf/tl ii tka fi ial aitiut <kaal i ba cnlirati IT CC/RSI:Tkii f lat ii "<< vk" aitlfta ti fatal la kliar ai wal l ti ai up It It iilieitti aaf i ikla/ iraaakla blaak eaatuiaitl ia ia4Mru tka iata aiar ta Ula affrafrlata aet iaa .OTUI:Otkar f laft aia* faataatai iaf »a ra^airai ta i t»Mt'T 'afliatka rtniti K ntl, tkaf Hit ka ( a l l y <aicriba4 aatf tack4aicriatiaa itUtkt* ta tka data IOMI; r iaert .
kat
Laboritory Na«e:Case No; 7351 ENVIRODYNE
Samp le Nugfaer j EJ
Organic! Analysi, Data Sheet2)
128
Concentration: LOWDate Extracted/Prepared: 6-1-87Date Analyzed: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)
Se«ivolati1e Compounds
14.6
CASttx
111-44-495-57-fl541-73-1106-46-7100-51-695-50-195H8-739638-32-9106-44-5621-64-767-72-198-95-378-5H»-75-5105-67-965-B5-0111-91-1120-63-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3
Bvevl Alcohol1,2-OidilarobauiMZ thylphml61 s- (2-flil croi sopf opyl ) rthr
*hii troso-ft -fr-pr opyl an MHBachliroeUuni
Inphonn
tosoicbii-<QUatcthuy)fethm
1 ,2, 4-TrichlorcteaentIbphthalm4-Chl<nianilin*teacblorriutadim*
2- thylnaphthalent
2,4,6-Trichlcroptewl2,4,5-Trichl(raphBwI2-Chl(rmapt)thalcM
fcmapthylnW-W-2 Wtromliot
770 U770U7TOU770 U770 U770U770 U770 U770 U770 U770 U770U770 U770U770 U770 U3BOOU770U770U770U770 U770U770U770 U770 U770U770U3BOOU770 U3800 U770 U770U3900 U
6PC Cleanup : yesSep. Funnel ExtractionContin. Liq.-Liq. Ext.
83-32-951-2M100-02-7132-64-912-14-2606-20-284-66-27005-72-386-7^7
534-52-1B6-3N101-55-3118-74-187-86-5B5-01-8120-12-784-74-2206-44-0129-00-085-69-791-W-l56-55-3117-B1-7
117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
2,4-Ouutr^hmol
2,4-ffiritrotoliant
Fluornt
4,6-«Bitro-2-(W)ylphwol(1)
ette-
W-tHxrtyl phthalat*
( c i r c l e0~)<c i rcU
one ^one)
K-n-octyl phtiulati
770 U3800 (J3BOOU770 U770U770U770U770U770 U3800 U3800 U770U770U770U3BOOU770U
770 U770U77001500 U770U560 »770 U770 U770U770U770 U770 U770 U770 U
We.
___ —— _--i» = = as»*»»M*«««*z = «»»»«»**»»«s:ss*»»a
(U-Cannot be lepabated fro* diphenylaaine
.. - _r-- . FORH 1
Laboratory Name
Case No
Organics Analysts Data Sheet(Page 3)
S«mpt« Numb«r
-nz-.
Concentration
Date Extracted'Prepared
Date Analyzed ______
Medium
-1-17
Pesticide/PC Bs '
(Circle One] GPC Oeanup^Yes ONo
___ Separator^ Funnel Extraction QYes
——— Continuous Liquid - Liquid Extraction DYes
Cone/Oil Factor
Percent Moisture (decanted)
CAS ug/loruguKgNumber (Circto One)
319-84-6319 85-7319-86-858-89-976-44-83O9-00-21024-57-3959-98-860-57-172-55-972-20-633213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCSeta-BHCDefta-BHCGamma-BHC (UndanelMeptachlorAldnnHepiacnior CpoxideEndosuKan 1Dietdnn4. 4--OOEEndrinEndosutfan U4. 4--000Endosutfan Surfate4. 4--DDTMetnoxychkxEndrin KttoneChlordancToxaphen«Aroclor-1016Ar odor-1221Aroctor-1232Aroclor-1242
Arockx-1248Aroclof-1254Aroclor-1260
/6UIf U
/fc U.it au u.Ib KIt UIb U32- U-31 \L7i (AJ2-U.72. LC3l U3i U.Ibo U3i u.Ifco U32916
tfco (XUa UJt5 U
l&(? U-»fe? U310 K.
5Z.o fX.
Vj * Volume of extract infected (ul)
V » Vofume of water extracted (ml)
Wt * Weight of sample extracted (g)
V( * Volume of total extract (ul)
3o<\ _ v IO.AOO
7/85
No
Organic^ Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASCompound N
(ug/l
10..11..
13..
17..
18..
21.
22.
24
26..27..
29..
30..
V » / n V
M\JULA (d roGCLr be n
bo n
- 1
10.uu13
ISM
35.
3 6 - 1
l lGTJ^A
Ifc-oo 3
5503
60 3
-o
Form 7 65
Organics Analysis Data Shut(Pigi 1)
5a»plt Nomb«r: El
,-v
"£&Laboratory N*«i: ENVIROOYNELab 3a»pJi ID No: 17002*03Simpli Hatrii: SOILData Rtlcaic Anthoriitd By:
C... N,: ' } TJ6>QC R*port No:Contract No: _Dati Sampli Rtctitod
V o l a t i l t Coaponndt
Conctntrat ion: LOWDatt Eitracttd/Prtpartd:Datt Analyttd: 4-3-87Conc/Dil Factor: 1Ptrctnt Moiftort (not dicantid): 14.74
CIS Nt: •1*1 CIS Rt: 1919
74-17-174-13-t73-11-473-H-I73-l»-l47-44-173-13-173-13-475-14-1134-41-3(7-44-1117-14-171-fl-l71-33-434-11-3111-13-473-17-4
CkliiiMtkat* 1]IrUHltktll 1f i ty l Ckl i r td i 1Cklenitkati 1RitkylHi Cil i r idiIcitii* ^Carkit D i n l f i d tl.l-Blckliriitkiti1,1-Diaiiriitkatitraii-l.l-DickliriitkitiCklirifinI.l-Dickliriitkati1-lltUltl1,1,1-TrickIirntkuiCarkit TitraekliridtTiifl Icitati 1Imidiekliriutkiti 4
9t 91
( 917#>
t >I1
1 11
7I-I7-J1M41-I1-47M1-4H4-4I-17MI-J71-O-111141-11-31II-7J-I75-15-1lll-ll-l3fl-7l-4117.11-4Tf-14-3lll-ll-lIII-fl-7111-41-41II-4M
1,1-DichUrttretiittrati-t,l"0ickIir«pr»M"TricklirntkitiBikrmcklir nit k*uI.I.S-TiieklirttUmlimiteii-1.3-DiekliriiriM | f
l-CkUriitkfltii?Iitk«rIrmfirm4-Kitkfi-i-Mttiioti1 -IliumTitrickliriitkni1.1,1,1-TitraUUnitkatiTiliitiCklinkitiiiiitkfikiiiiiiStymiTital If 1 iiti
0UVI00V
1 10
tl Vtl
BV
DiU Diallfiiri
C:
. B-tki
THIrt:If tki milt i« i "In fti ittf tk«i tr MI«! U tkil iv i t , t t f« r t tki rail*.B:Ittieittf ciu^tH vai tialrt*' («r kit ««t ddietiT liytrt tkilimn ditietiit l i i i t fir tki luplt vitk tki V ( i f . I l l f ) kauri•• sieiisarr client . / i i l i t i i i attiii. (Tkit ii tittki listrtmiit 4iticti» l i i i t . ) Tki t»tnti ikiild rtiiCeiM"' «* ualyiil fir kit tit 4it iet itf . Tl* tnkir iilima itt i i i tklt ittictin i i i i t fir tli ia*»Ii.J:Iiriieitif at ittiMtii* rtlii. Tkii (U| if tsid iltkir•itiiatltf a CHCiitratlii fie t i i ta t i f i l r i< i i t i f l i 4trkiri * 1:1 riifiiii ii limit ir wkn tki uis tyittril 4at«ItriicatH tki fri»Mci if a ciifinri tktt Miti tki Kitt i f lcat l i ter i t i r ia kit tki null Ii I»n tkit tki tfttiliti l itietlit Hut kittr iat ir tkat lit* ( i f , 1 I J ) . If l imi t if l i t ict itt ii II ifl aid aeiieiitntiii if 1 ifl if calctlati4. nftrt at IJ
i i i t ie i t f i yaruitits tfkiri tki i d i t t i f t e i -If CC/I1S. Siifli eimfotiit ft* t icHn)«llutraet f hoi 1 4 ki eitfiiaid IT
Tki* f l a t *Mli«tilt vai citfirmidM/iI Ii tki f i t a lI:nil f l i f ii tiH wkit i it lfti if (»n< t> bl t tk is *•!! tf afufli. It liditatii ^ i f i ik l i /pr ikakl i kUtk ciitaiintitt aidvarti tki data mr ti taki a|fti|riiti ac t i i t .OTttl:Otktr (li|f attf f i i tutM lay Ii ii|iiriri ti y r o f i r l f i i f lutk« r i i t l t i . If ifid. tkif uit ki f i l l f Oiciikid aid iitk
t attackiri ti tki data
Laboratory Na«e:Case No: 7351
ENVIRQDYNE Sample Nunber
Organic* Analysis Data Sheet(Page 2)
SentvolatiIs Compounds
Con c an tr at i on : LOWDate Extracted/Prepared: 6-1-87Date A n a l y z e d : 6-13-B7C o n c / D i l Fac to r : 1Percen t M o i s t u r e ( d e c a n t e d ) : 14 .
CAS NK
108 5-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3W106-44-5621-64-767-72-198 95 378-59-i8B-7W105-67-965-65-0111-91-1120*5-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-45-491-58-783-7M131-11-3*** HI •ffJO TO Q
99-09-2
Phenolbi5-(2-QU(raethyl)rthr2-Odaraqhenol1 ,3-DioMflnteunl,4-fcchIxQbB«B»Bwuvl WcoSol1,2-ftchl.irotanzB*2-fethylphaulbif- (2-Otl oroi foprafryl ) rttw4-fethylphrolH-ni tr oso-ft -tt-prniyl m wteachlomthantKtrobBttmIiophorm2HtttropheioI2,4-Di«thylphBioiBenzoic Acidbii-ttMaroethoxy)Nethane2,4HKdilirqitm)L1 ,2, 4-TrichlflntenzBnIbptithalm4-OJtroinihntttaadUcrdbutkim4-Qaoro-3-^trylph0X)l2-fethylnaphthalmHnachl tncydopentadi me2,4,6-TridilcrophBiol2, 4,5-Tri dd orophexil2-Dil oronaphthilwf2-HitroaniliniBivtbyl phthalatiAcnapttiylne3-tttrtwuliw
B
uqtq
770 U770 U770 U770U770 U770 U770 U770 U770 U770 U770 U770U770 U770U770U770U3800 U770U770U770 U770 U770U770 J770U770 U770U770U3800 J770U3BOOU77011770U3800 U
6PC Cleanup : YESSep. Funnel Extraction : YES CC o n t i n . L i q . - L i q . E x t . : YE5 (
CAS to:
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27006-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-OH120-12-7B4-74-2206-44-0129-00-085-68-7tl-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
kenapfethm2,4-Oinitrflptwnol4-tftn3pheaolDibenzottran2,4-OiutrotoluiM2r6-0initrotoliantDitthYl phtlulatc4-QiIorflDhBiyl-phenyi ethe*RUOTB*4-tbtroaiilin*4,6H)initro-2^VthYlphB)olH-nitrnodiphEnylaiini (1)4-Bro^«nyl-phmyt etherteadilonteiZHifrBitacfaloroyhcMiFtvunUv ••AntbricM ,Di-trbutyl phtiuiit* /FlmrvthmPyrentButyl -b«yl-j*thtlite3,3 '-Oi chltrobenzi dimBouodJirthracentbif-(2-EthylteKYl)phUulatcOryffMDi-n-octyl phthalatcB*UD(b)fluoranthcntBBaotklfluranthiniBfrao(i)pyrB»Indni(ll2T3-oi)pyrnR bwzo ta.h) wthraontBenzolghilprYlvii
^1 (circle one)v N Q / ( c i r c l e one >
oqlq
770 U3800 U3800 (J770U770 U770U770 U770 U7701)3800 U3BOOU770 U770U770 U3800 U770U
r-Jauu— 22LLJ77&~T
770 U770U1500 U770U490 » MJ- fJ-^_770 U770 U770 U770U770 U770 U770 U770 U
11)-Cannot be separated fro* diphenyla-nine
.FORM 1
Laboratorv Name
Case No ___'Sample Numb«r
Concentration £o*t/ Medium
Date Extracted'Prepared ____P_
Dat« Analyzed _______LllkliZ
Cone/Oil Factor ________L^
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs ^>
(Circle One) GPC Cleanup^Yes QNo
- * '_______ Separatory Funnel Extraction QYes
———————__ Conltnuous Liquid - Liquid Extraction OYes
Percent Moisture (decanted)
CAS ug/Iofug^KoNumber {Circle One|
319-84-6319-85-7319-86-868-89-976-44-8309-00-21024-57-39S9-98-860 57-172-55-972-2O-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469 21-912672-29-611097-69-111096-82-5
Alpha -BHCBeu-BHCD«lu-SHCGamma-BHC (Undane)
HepuchlorAWnn
HcptxcMor Epox»d«EndosuHan 1Oietdnn4. 4'-OOEEndnnEndosuHan U4. 4'-DODEndosuHan Sutfate4. 4--OOTMeirxKvchlorEndnn KetoneChk>rdan«Toxjp^eneAroclor-1016AroclOf-1221AroclOf-1232Aroclof-1242Arocior-1248Arodcx-1254
Aroclor-1260
lt> U
(b U
/t UH, ILIt U)b KIt UIfc U.37- tA32. OC71 tA7iU.?2 U_3^ u1 U.
(bo U3* U.)feo Lt320 Itit-o 1^Ua U)ba Urtc- It\bc U3~o M.5Z.o (A
orW.
V( « Volume of e«tra« wheeled (ul)
V * Volume of waief extraaed (ml]
W$ s Weight of sample ertracted (g)
v( * Volume of total emraa (ul)
3o^ _ „ IO.AOO
Form 1 7/85
EL-Organic* Analysis Data Sheet
(Page 4)
Tentatively Identified Compounds
GAS
7
10..11-
is..16..
17..
18..
50
23
23—
24—ZS._
2G._
27..28._
29._
Compound
u-f jf\ rpp /L r hx5T^Li AAV_ n fru/v .
Fraction
JL_L
IQ • 0
is. \
. L,
\
S6.0
956\-StTb 3
M**o-\
VO
%
? es
O r g a n i c * A n a l y i i i D a t a S h t t t(Pagt 1) I
Laboratory Mam*: ENVIRODYNELab Samplt ID No: 17002*04Samplt Katriz: SOILData Rtltife A u t h o r i i t d BT <V\CXU
S a m p l i N a m b t t„„ —— .-.
EL
Can No: * "QC R e p o r t No:C o n t r a c t No: _______Dat i SaapIt Rtct iv td:
Voiat i1* Compound•
Concentration: LOWDttt Eitracttd/Priparid:Datt A n a l f l t d : 4-3-87Cone/Di1 Factor. 1Ptrctnt Moiftnrt <not dicantid) 14. i
US Mi: Ci! Me •Ik?
74-17-374.-I3-?73-11-475-M-I73-11-2•7-44-173-13-173-33-473-34-3134-41-347-44-3117-14-271-11-171-33-434-J3-!111-13-4T3-J7-4
CklirtMtkanIrtMHtkanTlif l CkltridiCiItiDttkaitRttkfltit Ckltti itiCltlll |
CarkH Dii i l l idt1,1-Diekltttttktit1.1-DiekUtittkaattraii-1.2-DUkltmtkiiiCkltrtftn1,2-Dtaitrtttkui2 -H taitia1,1.1-TrttiUrittkkitCarkti TttiackltrldtTiayl lettattIrntdiekltrmtkut
122217i
i121 1
BVVV
0 i
-I
71-17-3llltl-12-iTt-ll-4124-41-17J-II-S71-43-2UI41-I1-3lll-TJ-l73-23-2lll-ll-l3»l-7l-<1Z7-U-47f-14-3lll-ll-llll-fl-7HI-41-4111-42-3
1,2-Ditkliritrttaattra*i-li3-DickItrBir«|titTricklartitktiiliktntckltrtittkaii1.1,2-TrickltrtttkaitIttitittif-l,3-DltkIiritr«ttii1-CiliriitkjliliYlitktrIcMidnf.-Hitkrl-2-rtitaitit2-Itiaitll
Tttraekltrtitktit1.1.1.2-TitratkIirtitkaitTtllHtCklttlhlltllfl
lUTlkusiiittrrtuTftil IfltKII
IV
12 11 D12 912 I
1fI1VI1
Dttt
fKBI;tl tht ruilt ti i Tilti irittn tin tr 1411! ti tkil imit , rt|trt tkl »*i««
OitlHltrs
Tkii Maf aiiliis tt f t i t i c idt laraatttri witit tkititi vai etafiritd IT CC/fB. Sliflt etBftatitit/il ii tkt dial t itrtet iktild 11 etidntd kf CC/NS
Iilicttti c«f«n< •*• tulyttri (•! kit ut <itict*4. lifirt tktBtiimo ItttetUi liiit dc tkt inpli vitk tki V (M.IIO) ktfidti itttiittf t i ietit . /IUitit i ictttt . (Tkts U i»l itctiitrilftkt lutrntit (ttittiii l i m i t - ) Tkt ftit ittt iktil« ml: V-Cnftnd vtt «»IytH fit kit itt I t t tetH. Tkt inker li tkt•inia tttiinbli littcti» l i» i t (ti tkt tuplt.J:Iitfieittt u tittutid ftlit. Tkii fli| ti nti titktt vktitittmitiii • ctieiittititt ftt t t i t t t i t t l f irititi l it l etifonlivktit a 1:1 rtflfotflt ii aiint^ K wk» tki tan i f iet tal dataI i f le i t i4 tkt ittftiet K a cn|«n' tkat uiti tkt td t i t l f icttitictittrit kit tkt i t i t l t li l i ft tkai tkt i^tiliti < i l tc t i* i lliit kitIttattr tkas itrt (t|, 1IJ) . II I i » i t •( t f t t tet l t i Is II tfl ud acnciittattii t( ! i|l ii ealetlttti, tiptt ai )J.
Tki i flaf It nt< wkii aialfti It ftiid Ii klaik at vill ai a•aa|lt. It lidicatti |tii iklt/ |rtkaklt klaik eiituiittiii uivacii tkt data ifit U takt «||titrtatt actit i .
Otktt f l t f f aid (ittiftti uy W ttftirti tt i t t f ir ly lifiittkt rmlti. If md, tktf ntt kt f i l l f di ici ikid aid sickiitcriititi attaektd tt tkt data tatary nptrt.
Laboratory Naue:Case No: 7351
ENVIRODYNE S a m p l e N u m b e r : EL 2
Organic* Analysis Data Sheet(Page 2)
'
Concentration: LOWDate Extracted/Prepared: 6-1-B7Date Analyzed: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)
Seiivolatile Compounds
6PC Cleanup : YES
14.6
CASJto: uqkq
108-95-2111-44H95-57-fl541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-5621-64-767-72-19H5-378-59-1BB-75-5105-67-465-85-0111-91-1120-B3-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47SBB-06-295-95-491-58-788-74-4131-11-3208-96-*99-09-2
Phenolbii-12-ailxoBthyUtthjr2-Qilorcphenal1,3-Dichlardwruerw1,4-DidilxofaenzeneBeruyl Wcrfcl1,2-OichlxDbenzene2-fethylphaulbis- (2-Cblxoisopropyl ) ether4-fethylphenalIhii tr oso-Di -tt-pr op y 1 ati nfHexachlxoethaniNitntenzewiBQphxmeT-tttrophenol2,4Hhwthyl phenolBnzoic Acidbis-{EMxorthmv)nithane2,4-Oichl tropoennl1,2,4-TridUxobenzH*Ibphthalene4-QUxoanilinetoachlxcbutadiene4-Qaxo-3-fethylphenol2-HethyIuphthalBiiteachl xttydcpentadiew2^4,6-Tridilxaphenol2,4,5-TridilxQphenol2-Otlxonaphthalene2-totro*iihf»Diwthyl phthalateAcBiapthylene3-tttroaoilint
770 U770 U770 U770 U770 U770U770 U770 U770 U770 U770 U770 U770 U770U770 U770U3700 U770U770 U770 U7701)770 U770 U770U770 U770 U770 U3700 U770 U3700 U770 U770 U3700 U
), F u n n e l E x t r a c t i o n : YES \i t i n . L i q . - L i q . E x t . : YES (
CASfet
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-5MB6-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44H)129-00-085-68-791-94-156-55-3117-81-7BB-01-9117-84-0205^9-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaphthene2,4-Oinitrophanl4-tttrophenolDibenzofiran2,4-ttnitnjtolutne2,6-DirutrotolueneDiethyl pbthaliti4-Qilxopnenyl-pnenyl etharFluor ent4-tttroaniline4 , 6-Oi ni tro-2-ttethyl phenolH-nitrosodipnflnylatdne (1)4^roaaphertyl-phenyl etherHexadvlantotteMPentadilxophmlPhenanthreneAnthraceneDi-n-fautyl phthalatenucrnthcnePyreneButyl -benzyl -phthal ate3,3'-DichlxobHi2iilineBenzo (i) anthracenebis-l2-€lhylhoyl)phthaUt«OirysentOitroctyl phthalateBnzo(b)fluoranttwne&nzo(k)fluorantheneBnzo(a)pyreMlndero(l,2,3-cd)pyrtneDi beozo (a f h ) antiracmeBeraoighilperylant
H&iV ( c i r c l e o n e )^JlJO) ( c i r c l e o n e )
770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700 U770 U770U770 U3700 U770 U770 tk.
^9wi)770 U770U770 U1500 U770 USWWWj-p^770 U770 U770 U770U770 U770 U770 U770 U
(l)-Cannot be separated fro« diphenyl*«ine
FORM 1
Laboratory Name
Case No ' ' "7Numb«f
Concentration fey/ Medium
Date Extracted'Prepared ____2J
Date Analyzed ._______^
Conc/Dil Factor \
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs
(Circle One) GPC Cleanup^Yes DNo
______ Separatory Funnel Extraction OYes
_____ Continuous Liquid - Liquid Extraction QYes ^p
Percent Moisture (decanted)
CAS ug/loru^KoNumb«r (Circta Onef
319-84-6319-85-7
319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-2111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeia-BHCDelta -BHCGamma-BHC (Liodane)HeptachlorAldrin
Heptachlor EpoxideEndosulfan 1Dieldrin4. 4--DDEEndnnEndosuttan It4. 4'-000Endosulfan Sufaie4. 4*-ODTMeihoxyctiforEndrin KetoneChlordaneToxapheneAroclor-1016Aroclof-1221Aroctor-1232Aroclor-1242Arociof-1248AroclOf-1254
Aroclof-1260
/fc UIt U
1h U.It Uli UIb l(It (4Ifc U
32- IA
3iU-71 UJiU.?ZtL52 U?!. IXfto U31. U.) fco U5zoU.'to LlU.3 U
t feo \iI'j? IX\fccr U"JZO L<.
5Z.o U
orW.
V( * Volume of extract injected (ul)
V = Volume of water extracted (ml]
W = Weight of camp(« extracted (Q)
(ul)
0, 600
V. - Volume of total extract (ul)
'Form 1 7/85
Organic* Analysis Data Sheet(Page 4)
Tenlativoly Identified Compounds
CASCompound
~7.0
t613 3
I Q - 6 940It. 1
J3,
rflQO. rb^. J^J.10.
i*.is.16.
17.
18.
20.
21.22.
23.
25.2€.27.28.
^
Uj
ttn I. ? as
Organ i ci Ant I yi i i Data Shctt(Pigt 1)
Samp It Number: EL
Laboratory Naat: ENVIRQDYNELib Samplt ID No: 87002405Simplt Matrii: SOILData Rtltut Authorised By:
50Cast No: :*'QC Rtport No:Contract No: _f/.?_-_Qj;Datt Saaplt Rtciivid
Volat iIt Compoundi
Conctntrit Ion: LOWDttt Eitrtettd/Prtptttd:Dttt Antlyxtd: A-3-87Cone/Oil Factor: 1Ptrcant Moiitnrt (not dtctnttd) 1 8 . 7 1
CIS Mo CIS Ml
74-17-374-13-?73-11-473-11-373-lf-247-44-173-13-173-33-473-34-J134-41-3•7-44-3117-14-27I-71-3Tl-33-434-21-3111-13-473-27-4
Cklt iomttkta t 1IrtmomttkiatTiByl Ckl tc id t 1CklenitkiBiHttkyltat Ck l t t i d tIctttatCttboi D i f i l f i l t1,1-DlcalortttktatI , l-Dtekltrt t tk»ttr iBB-l r2-Dicki t tot tktatC k l t c e f t r m1,2-Oickltrtttkut2-littatatl.l.l-TtieklttottkutCitkti Tt t r t tkl t i idtVlayl icittliIrntdiekltrtmatktaB
2 U1 U2 D1 0^0'10909QV8
2 0V0
U VI 0
TI-17-5IHH-ll-i7»-ll-i124-41-1Tf-M-S71-43-2lllU-ll-511I-7S-I73-23-2lll-ll-t5T1-7I-*127-11-47»-I4-3lll-ll-Jlll-fl-7ltl-41-4111-42-3
1,2-OickItttptiptitttiaf-l,3-DieBlo[apropintTilekltrittktaiBibromtckiaroattktatl,l,!-TriciIeri.U*BiItattat (cif-l,l-DiekI«roprBptat i2-Ckltt*ttkylTiaylitktrItmftrm i4-IIttkTl-2-ptattafiBt2-BtitaeatTttrtekltttttktat1,1.2,2-TttitekliitttktatTil nitCkltrtktaitatttkflitaitatStyrtatTtttI Ifliati
U0U00DU2 DD2 U2 V000000D
Diti I tptr t iaf Qulif i tcs
ULUE:If tkt titolt is i ftltt fritttr tk» ir tt.«il tt tkt dtttctitalimit, rtptit tkt ?»ln.B:ladiettts oaf end vaf tatlyiid (it lit itt dtttettd. Itptrt tkta in an dtttetita lint (or tkt ftmplt witk tkt U (19,110) ktstdta atctiftry ctaetat./dilitita ttti». (Tlii ii act accifinilftat iaitrntat 4tttcti» liait.J Tkt ftttattt ikoiU rud: 0-
vis utlyti< f*r tit att 4ttteti4. Tkt anbir it tktittsiaiklt <ttteti«a limit ftr tkt iu|Ii.
J:la^icitti ta tftimattl rUit. Tkif flif if aittf titktr vktatftimitiaf t etaetatntita tit ttaUtiftlf idtati(it< c*m»otadf•atrt » 1:1 ttiM"* t« »samt< tr vfcta tkt un ittctrtl fittiat*iettt< tkt irtsiiei If « etmtatal tktt mtttt tkt ttftatifltitieae r i t t r i i lit tkt ttiiit it litr ta*a tkt ificifit* ttttctita limitftiitir tkia itrt (t|, 1IJ). K limit t( Itttctita ii II ifl tad tcvactatiitita t( 1 i|l If eileiUUrf. rttttt » JJ.
C:Tki« fltf itplitf t« ftiticidt iitutttri vktri tkttioa vii etafirmtd If CC/KS. Stiflt cemtoBtit iistitidtil-llaffil ia tkt (iul utrict iktild it etafintd by CC/K5I:Tait fUq it tit! wata utlrtt if lond ia il»k n vtl l *f iftmilt. It iadieittt t t i i i k l t / i f t k tk l t tlial c iatuiatt i ta tadmrif tkt d*ti »tr tt tttt itpriiri itt i c t i o i .OTRU:Otkti (Ii(f tad (tttattti may •• itt.iiitd t« ttotnir difiattkt ttfilti. If ictd, tktf mift It f i l l f dtieiibid tid fickdtfcriptioa itttektd tt tkt dttt saury tipart.
lit
Laboratory Naae:Case No: 7351
ENVIRQDYNE Sample Nuaber: EL 258
Orqanics Analysis Data Sheet(Page 2)
Concentration: LOWDateDateConc/DilPercent
Seaivolatile Compounds
GPC Cleanup : YESx t r a c t e d / P r e p a r e d : 6-1-87n a l v z e d : 6-13-87i l F a c t o r : 1t M o i s t u r e ( d e c a n t e d ) : 18.
CftSto:
108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-W-73963S-32-9106-44-5421-44-747-72-198-95-378-59-1BB-75-5105-47-965-85-0111-91-1120-83-2120-82-191-20-3106-47-8B7-4B-359-50-791-57-677-47-4B8-06-295-95-491-5B-78B-74-4131-11-3200 % Q99-09-2
Phenolbi*-(2-0)laraethyl)etiw2-Oilorophenoll,3-0ichlareben2ene1,4-OitMorabenzeneBenzyl Alcttal1,2-Oicblarobenzene2-fethylphenalbis-(2-ChlQroi50propyl)ether4-nethylpnenalIhri trow-to -n-propylainetaachlaroethaneNitrobenzeneliophorane2-Mttropheral2,4-fli*thylphenalBvtzoic Acidbis-IOilirwthoy) tethane2,4-Oidilorophenol1,2,4-TrichlGrobenzenebpfattulene4-OilxoanilineHetachlorobutadiene4-QU aro-3-trthylphewl2-ltthyl naphthaleneteachl crocyd opentjdi ene2^ 4 ,6-Tri ch 1 or ophenol2,4,5-Trichlarapnenal2-Qilaronapt)thalen(2-ttitroaniUneDiwthyl phthalatiAcenapUrylene3-)*itrwnilint
7
uqkg
810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 I)810 U810 U810 U3900 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U3900 U810 U390QU810 U810 U3900U
Sep. F u n n e l E x t r a c t i o n : YES <C o n t i n . L i q . - L i q . E x t . : Y E S
CASfc:
B3-32-451-2B-5100-02-7132-44-9121-14-2606-20-284-44-27005-72-386-73-7100-01-4534-52-186-30-4101-55-3118-74-187-B6-585-01-8120-12-784-74-2206-44-0129-00-0B5-48-791-94-156-55-3117-81-721B-OH117-84H)205-99-2207-0&-950-32-8193-39-553-70-3191-24-2
Acenaphthene2,4-DiiutrDpnGnol4HbtrcpheralDifaenztrfiran2,4-OinitrotolueDe2,6-OinitrotoluneHietbyl phthalatf4-QUtn?ihenyl-pinnyI etherFluorine4-Hitroanilinc4 , 6-Di ni tro-2-*Wryl phtoolH-nitrTBodiphenylanni (1)4-fircaophenyl'pt)cnyl ithertaachlorobercemtatachlorophenolPhcnanthremAnthracentOi-nHwtyl phthalatfFluorantteMPyraieButvl-toUYl-phthalate3,3 ' -Oichl tnteui rfi ntfienzotiJ anthracenebii- (2-EthylhexyI ) phthal ateQryseneDi-n-octyl phthalatcBenzotbmuoranthentBcnzo(k)fluranthentBenzolaJpyrentIndeno ( 1 , 2 , 3-cd) jrvreneBibenzo(a,h)antbracene8enzo(ghi)perylene
^£& (ciQjOjjici
oqtq
810 U3900U3900U810 U810 U810 U810 U810 U610 U3900U3900U810 U810 U810 U3900 U810 UJ1QJJ
^JTOO^ifmr
810 U810 U1600 U810U320 CBIO U810 UB 1 0 U810 U810 U810 UB10U810 U
(circle one)circle one)
(l)-Cannot be separated iron diphenyla»in« : ._
FORK 1
Latxxaiory Name
Case No ___ .Sample Number
Concentration
Date Extracted'Prepared
Date Analysed .
Cone/Oil Facior
Medium
i'J-
t» - /4 "
Organics Analysis Data Sheet(Page 3) *
Pesticide/PCBs(Circle One) GPC Cleanup,QYes DNo
L_________ Separator^ Funnel Extraction DYes
__________ Continuous Liquid - Liquid Extraction DYes
-2.
-\\0
Percent Moisture (decanted) / *^ /
CAS ug/loru^K^Numt>«r (CircU Or**)
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHC
Beta-BHCDeita-BHCGamm»-BHC (Linda netHepiachlorAldrm
Heptachlor EpoxideEndosutfan IOieldrin
4. 4--ODEEndnnEndosuHan II
4. 4--ODOEndosulfan SuHate4. 4'-ODT
McthorvchlorEndrin Keton*ChlordaneToxaph«f>eAroclor-1O16Afoclof-122lArOClor-1232
Aroclor-1242
Aroclo'-1248Aroclor-1254
Aroclor-T260
/& U
|t> U
\k Ltib aIt UIb ViIt IXIb U.3z- u-31 U,7L tA12. U.?ZtL52 U-31 U.fbo U31* U.Ifcfl U-_?isa_ifeo 11Uo U)b3 \1lfr<? (^\£«? U32-0 K3in LC
V( = Volume of e*lr»ct injected (ul|
V$ = Volume ot waief ettracied (ml)
W$ = Weight of sample extracted (g)
V( s Volume ol total extract (ul)
of W.
Form 1 7/85
fc -JHO
• too Orgaoics Analysis Data Sheet(Page 4)
[ b L
T«n(a(ivoly Id«ntifi«d Compounds
CAS
(wg/l
il/Y\\f
ib.oii.
So -3IS. I
5..
Oo- Icm
3-M.3
tl
O r g a n i c s A n a l y s i s D a t a Shtt t( P a g t 1) :--•
L a b o r a t o r y N a m t : C N V I R O D Y N EL a b S a m p l * I D N o : 1 7 0 0 2 4 0 *Saap la M a t r i i : S O I LD a t a R i l i a c t A u t h o r i s e d B y :
Cast No: 1^QC Rtport NoContract No:Datt 3a»plt Rictivid:
Saaplt N u n b t r : EL
"is"/""""""""
fig-QI-"?D9"7
V o l a t i I t Compounds
C o n c t n t r a t i o n : LOVD a t t E i t r a c t t d / P r t p a r i d :D a t t A n a l y i t d : 6-3-87Conc/Dll Fac to r : 1P t r c t n t M o i s t u r e ( n o t d t c a n t t d )
CU Mt: CIS It:
74-17-374-13-t73-11-473-11-}73-11-247-44-t73-13-173-33-473-34-3134-41-347-44-3117-14-271-73-171-35-434-21-31H-I3-473-27-4
Ckltr tmttkait 1Iromemttkait 1Tiiyi CiltrUt 1Cklort t tkai tftt tkyltit CkUtit tietttit 1Carkti Di t i i fKt1,1-DlekItrtttktitl . t-Ditkltrtttkaitt rau-l ,2-DickIt t t t tkt i iC k l t r t f t r m1.2-DitkItrtttkaitMttmti1,1.1-TrtckItrtitkaitCarkti Tttrackltri i tTiiyi icttattIrtmtti tkltrtmttkaai
2 92 92 92 9
•?£JO9D99V9
2 999
11 9I 9
71-17-3 1 ,2-Dicklertprtptai1M41-I2-4 l t »« - l , I -D i c i I i r o i rop i i iTf-ll-4 Tritkltrtttktit1X4-41-1 Bllrtmtchltrtmttktit71-11-3 1.1,2-Trlckltrtttkait71-41-2 Itiitit11141-11-5 eis-l,3-8iaitrttreptittll-73-l 2^kltrtttkylrii;lttkir73-23-2 liMtftrmlll-ll-l 4-Xttkyl-X-ptitaititSfl-71-4 2-Itiaitit1X7-11-4 Tttrackltrtttkait7T-14-3 1,1.1.2-TttraekItrtttkaattll-ll-1 TtlitMlll-fl-7 Ckltrtfctittit111-41-4 Itkylktmstmt111-42-3 StyriM
TtUI Xyltus
4 Q4 U4 94 V4 94 94 912 I4 912 911 9
Data Itptrtiii Qtalifitrt
.'ILDt:If tkt rmlt ti a ralit f r t i t i r tkii ar it.it 1 tt tkt itttctltil im i t , rattrt tfct Tain.J:Iilicattf CHioni vai aiaiytt< ftr kit lit ItUctid. Itttrt tkt• niin ttttctiti limit dr tkt samslt witk tit 9 (if,110) kastlit itttssary etietit./i'ilitii* actlti. (Tkis ti itt itcisiaiilftki intrant itttctlti limit.) Tki ftttaitt skull rta<: 9-Ctmptiatf wai atalyiiri lor kit itt <«tictt< Tkt inktr If tktmiiimn tttiinklt Itttctiti l i m i t ftr tkt iimftt.4:Ii4ieatts ti tftimattl ralit. Tkii ftif ti ntd titkir vktititimatlif i ctietitratioi ftr tt i t a t i r t l y Htitifitd ctm|ends«ktrt a 1:1 rtxttist tt animtd tf vkti tkt miif tttetril fataIaiicatt4 tkt prtitict if a tntoiad tkat mtttt tkt UtttificatUicrittria bit tkt null If list tkai tki ifteifitt littctlti l i m i t kitirtattr tk«a itrt (t|. 1IJ). If limit tf <ittcU» li II i|I aid atoictitrititi tf 3 i|l is calcilattd, rtfvrt ai JJ.
Tkii flag ifftiif tt ititlcilt taramtttrs vkirt tkt i d t i t i f i c i -tl» «ai etafirmtri ky CC/KS. Siiflt cnptitit lift icidn)«llt|/il li tkt (ital titnct ikttU kt etifirmt* ky CC/HSI:Tkii (Uf is istd wfcti amalytt is ftntf la klui as vt!I as ifUflt . U litfieitti |« is iktt / trt i ikl t klttk e tatamiat t t t i ail•arts tkt lata istr tt takt ai irtprlatt act loa .
Otktr flags aitf ftttittts may I* rtfiirtl tt trtM^T 'tfiattkt rtsilts. If ntl, tkty mtit kt filly ttierikttf »4 nekitieriitioi attaektl U tki Uti stmmacr ti i o t t .
Labor ator v Nane:Case No: 7351
E N V I R Q D Y N E SaiolB Nueber: EL 2S&
Qrqanics Analysis Data Sheet(Page 2)
S e a i v o l a t i l e Co*pound§
Concentration: LOWDate Extracted/Prepared: 6-1-87Date Analyzed: 6-13-87Conc/Di1 Factor; 1Percent Moisture (decanted) 19.2
OSfc: uqkg
108-W-2111-44-495-57-fl541-73-1106-46-7100-51-695-50-195-48-739638-32-106-44-5621-64-767-72-193-95-378-59-1BB-75-5105-67-965-S5-0111-91-1120-B3-2120-82-191-20-3106-47-8B7-t8-359-50-791-57-677-47-488-06-295-95-491-58-780-74-4131-11-3200 96^99-09-2
Phenolbis-(2-Qiltrnethyl)ether2-Qilorophenol1,3-Dichlorobenzenel,4-DichIaraben2eneBenzyl Alcohol!,HKchlcrobenzme2-fethylphenalbi s- (2-Qi 1 or oi sopropyl ) ether4-tethylphenolH-ni tr oso-Di -rrpr opyl ui neIteachl methaneNitrobenzeneIsapharon2-tttrophenol2,4-th KthylphmalBmzoic Acidbis-(Dilimethmy)tetha«2«4-DichlcrQph«K)l1 ,2,4-Trichlorcbenzenetaphthalene4-Qilaroanilir«teachlorobutwiiene4-QUaro-3-«thyl phenol2-*thyl naphthaleneHex achl trocydopaitadi ene2,4,6-Trichlxcphenol2,4,5-Trichlcrophenol2-Oilxowph thai ene2-MitroanilineDiKthyl ptithiliteAtenapthylent3-Mitroaniline
820 U820 U820 U820 U820 U820 U82008200820 U820 U820 U820 U820 U820 U8201)820 U40000820 U820 U820082008200820 U820 U820 U820 U820 U4000 U820 U4000 U820 U820 U4000 U
Sep. F u n n e l E x t r a c t i o n : YES (
C o n t i n . L i q . - L i q . E x t . : YES C
CA5MK
83-32-951-28-5100-02-7132-64121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-5BWH120-12-784-74-2206-44-0129-00-085-6B-791-94-156-55-3117-81-7218-01-9117-94-0205-99-2207-06-950-32-8193-39-553-70-3191-24-2
Acenaahtbent2,4-QinitrQphenal4Hbtrap6enalDi benzol iran2,4-OipitrotoIueM2,6-OirutrotfllueniDietbyl phthaliti4-ChlornphenYl-phenyl etherFluor en*4-fbtroaniline4,6-ftni tro-2-fWiyl phenolLI - 1 i' i i • it *«™fUu uMJLUyJ HIT llfW ll/
4-aroK9h0tyt-phtByl itlwrteachlu (ixsuenePntadilaro^eoolntenanuimntnracEntfii-n-^utyl phthalateFluor aothen*PyrweButyl -fcenzvl-phthalit*3,3'Hhchlarabenziihne6enzD(i)vithracHWbis-(2-ethylheiyl)phthalateChrvuneDi-n-octyl phthalateBetuo(b)flutrwthewBmzDlkHlua-arrtJw*BwiodJpyTBwlndeno(l,2,3-cd)pyreneOi bemo U, h) anthr at eneBenzo(ghi)perylmt
Si^tci^NGjici
820 U4000 U4000 U820 U820 U820 U8200B20U82004000 U4000 U820 U820 U820040000820 UR2CJl^
L41Qj^820 U820U820 U1600 U8200370 ST82008200820 U820 U8201)820 U820 U8200
(circle one)i c i r c l e one)
(U-Cannot be separated fro* diphenylaaine
FORM 1
Orgaoics Analysis Data Sheet(Page 4}
Tentatively Identified Compounds
.3*
-f It
VOrt
-0-nn-n-nam-o
90,3-
7 8S
Organic* Analysis Data Sheet(Page 1)
Saaple Nu»ber: EL
Laboratory Naae: ENVIRODYNELab Saaple ID No: 87002776Sa*ple Matrix; SOILData Release Authorized By:
Case No: 7351QC Report No: ./30___.Contract No: ..IfiXr.Qj.Date SaBple Received:
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted) 10.2
<fe
CAS to: CASto: uqkq
74-S7-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278 3-371-55-656-23-5108-05-475-27-4
ChlorotethawBromethancVinyl ChlorideQtloroethsnefrthylene ChloridefcfitmeCarbon BisulfideItHHchhraethcneM-Dithloroethanetrans-1 ,2-tochloroeUwneQtlaroftn1,2-QichloraRthane2-ftitanone1,1,1-ThdUtroethnCarbon TetracbloridiVinyl AcetateBr otodi chl arowthanc
111111 U \11 U l11 U958
• ^'£43W6 U6 U6 U6 U6 U& U11 U6 U6 U11 U6 U
78-67-510061-02-67M1-6124-48-179-40-5
^ 71-43-210061-01-5110-75-875-25-2ioa-io-1591-7B-61Z7-1B-479-34-5lOft-ffl-3106 0-7100-41-4100-42-5
1,2-OichliriroKtrans-1 ,3-OichloniprQ(w»TridUoroetheneDi bronchloraethane1,1,2-TrichloroethaneBenzenecis-1 ,3-OichloroprDpem2H>1 or cethyl vi nyl etherBroKrfori4-ftrthyl-2-penUnone2-tinUKniTetrachl onxthvc1 , 1 , 2, 2-Tetr acil or oethaneTolueneOUorobenzeneEthylbenzeneStyrcntTotal lylenes
6 U6 U6 U6 U6 U6 U6 U11 U6 U11 UU U6116 U6 Ud U6 U6 U
f UM I • mul t (• * *•!»• ^vvtv
trltvl* hwt Ov r»»Mlt !• ! lrt *B««C*IM UiKt •••»
Laboratory Naae:Case No: 7351
ENVIRQDYNE Number: EL 260
Organic* Analysis Data Sheet(Page 2)
Sen! volatile Compounds
C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : 6-10-87D a t e A n a l y z e d : 6-13-87Conc /Di l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 10
CASMo:
108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-5421-64-747-72-198 75-378-59-1BB-7W105-67-945-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-477-47-48B-06-295-95-491-58-78B-74-413H1-3
, 208-96-fl99-09-2
Phenolbii-l2-QilxaEthyneth*r2-Oilo- thcnoli,3-0ichlxobenzan«l,4-ffichlxabejiz»tBenzyl Alcohol1,2-frchlxctanzent2-fcthylphenalbis-(2-QilQroisoprapyl)ether4^tethylphenolH-ni troso-Oi-n-pr cpyl aii HteachlxostharaNitrobenzeneItoptaront2"mtrQphtnol2,4-&i«*hylphenolBenzoic Acidbis-tfMcnxthtsylfethane2,4HHchloraphenol1 ,2 , 4-Tri chl xobenzen*Naphthalene4-QiloroanilintHexichlxcteitadient4-Odxo-3-«thylphHcl2-tethylNphthaleneHB achl xocycl nwtadi ene2,4,irTnthlcrDphenoi2,4 ,5-Tri chlxophwol2-QilcroniptithiImf2-MitnuniliniDiMttwL phUulateAcB^thyler*3-Mtroaniliw
.2
^
730 U730 U730U730 U730 LI730 U
- 7 3 0 U730Q730U73011730 U730 U730 U730 U730 U730 U3600 U
. 730U730U730U730U730U730U730 U730U730 U730U3600 U730 U3600 U730 U730U3600 U
BPC C l e a n u p : YESSep. F u n n e l E x t r a c t i o n : YES \C o n t i n . L i q . - L i q . E x t . : YE5 '
CASNo:
83-32-951-28-5100-02-7132HM-9121-14-2406-20-284-66-27005-72-386-73-7100-01-4534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-OChO85-68-791-94-156-55-3117-81-7218-01-9117-84-0205- 2207-08^50-32-8193-3M53-70-3Wl-24-2
AcBnaphthenc2,4-Oinitnvtad4-tetrcphenolDibeuofiran2^4-OiiiitrotDiicnt2,6-Oinib-DtaliM«Di ethyl ptithalate4-Chl(rmhoiyl-phBTyl etherRutrent4-*tnHnili«4, 6-Oinitro-2-hethy 1 phenolKidtrasadiphenylatini (1)4HkroKph«Tyl-phiRYl ttiwrto achl Tries a*hntachlxophenolPheunthrenetathrxmDi-trbutyl phthalateRuxarthenePyrowButylHtenzyl-phthalati3 ,3 ' -Oi chl tntenz i di mBruoii) anthracenettii- (2-Cthvlteyl ) phthalateChryumDi-trtttyl phthalateBnuo(b)flnr»theM8Bao(k}flurantheniBn20(a)pyraielrdcr«(l,2,3-cri)pYremDibaao(4.h)«thracntBBUt>(ghi)perYleni
r^)(ci<^J(Cl
w730U3600U3600 U730 U730U73011730U730U730U3600 U3600 U730U730U730U3600 U730Urau^<c^s>
^T30U730U7301)1500 U730 U_
/ 1300 8^OlT
730U730U730U730U
KOU730U730U
ci rcl e one)
(t)-C*nnot be separated froa diphenylaaine
FORM 1
Concentration
Date Extracted'Prepared
Date Analyzed
Conc'Dil Factor
Percent Moisiure (decanted)
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs
(Circle One) GPC Cleanup^QYes DNo
Separatory Funnel Extraction OYes
Continuous Liquid - Liquid Extraction
Alpha-SHC
Beta-BHCDclta-BHC_______Gamma-BHC (LindanelHepiacMtxAldnnNeptachtorEndosulfan IDieldrin4. 4--DDEEndnnEndosuWan II4. 4'-OOD
Sutfate4. 4'-Dpf~MelhoKycMofEndnn
Chlordane
Aroclof-IOTSAjoctoT-1221Afoclor-1232AroclQf-124?
DYes
or W.
V -* Volume of extract m|ected (oil
V - Volume of water extracted (m()
W = Weigh! of sample ertracied (gl
V * Volume of total extract Ml
3o lo:
Form 17/85
Afo: 73 5"/ Organic* Analysis Oata Sheet(Page 4)
Tentatively Identified
Concentration
~B*)A ' /•ft
3-M6
<S< t MbOtT
1±M5C.3
3 -3 . 1
drocoL
A* A r^co jf bo
s.
? 85
Organic; Analysis Data Sheet(Page 1)
Saaple Nuaber: EL 261
Laboratory Naae: ENVIRQDVNELab Sample ID No: 87002777Si.pl* Hatrix: SOILData Release Authorized By:
Case No: 7351DC Report No: _£3_Q_Contract No: __ip_3__QiDate Saaple Received:
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted)
Ximn03<:mo
GOrn
CO
COCO—J
14.2
CASto: uqkg OB to:
74-67-374-83-975-01-475-00-375-09-247-64-175-15-075-35-475-34-3156-60-547-66-3107-06-278-93-371-55-454-23-5108-05-475-27-4
OiloroiethaReBroBMetnaneVinyl Oil or id*QtloroeUunefethylww Oil TideAcetoneCarbon Disulfide1,1-DichIoroetter*1,1-Dichlxoethanetrans-l,2H)ichlxaeth«Olxofxi1,2-Didiloroethan*2-ftrtanone1,1,1-TrichloroethaneCarbon TetradilxideVinyl tartateBrondi cftlxo«thane
12 U12 U12 U12017*43"14* <*3-
4U **61)4 U4 U4U6U12 U4 U4 U12 U4 U
7B-&7-510041-02-479-01-4124-48-179-00-571-43-2
c 10061-01-5110-75-875-25-2108-10-1591-78-4127-18-479-34-5108-98-3108-40-7100-41-4100-42-5
1 .2-0i dil or opr opinetrans-1 ,3-DichIxapropmTridilxoethewDi bnnadtl xaetharcl,ltMridilxorthaneBenzenecii-1 , 3-Oichl xopropew2-Qil oroethy 1 vi ny 1 etnerBrocrfon4-tMhyl-2-pottanoneHteanowTetrachloraetheiel,l,2,2-Tetrachlarccth«wTaltBieOilorobeuBwEthvlbauawStyrawToUl Ivlenes
6U4116 U4 U6 U4 U6U12 U4 U12012 U4U4114 U6 U6 U4 U6 U
U <*«,
«M ll««t.> TH*
•*/«! In tM* «l*Mi
t ct «B»X>1 0
M fully
but th» rMMlt !• !••• thwi Uw tatvctlvi llMt bwt
L a b o r a t o r y Naae:Case No: 7351
ENVIRQDYNE 5a«ple Number: EL 261 f\o
Organic* Analysis Data Sheet(Page 2)
Concentration: LOWDate Extracted/Prepared: 6-10-67Date Analyied: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)
Seaivolatile COMpounds
GPC Cleanup : YES
14.2
CftS to:
106 5-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9104-44-5621-64-767-72-19*45-378-59-189-75-5105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-46B-06-295-95-491-5B-788-74-4131-11-3'Vfi-Oi—H£M 70 U
99-09-2
Pbenolbi s- 12-Qtl tnethyl 1 eUw2-Oiltropbenoll,3-OidiIord)euBtt1,4-Oidila-DbwieneBenzyl WortilI12-&ichlcriteaene2-fethylptenolbi s-(2-Chl oroisopropyl ) ether4-ftthylphmolH-ni trcwHh-inr opyl MI ottoachlEroethaMNitrobenzmiInpnortiM2-tttrophBtol2,4-ttHthylphmlBenzoic Acidbi s- (Qu(rarthmy ) Methane2,4-Oidiloropheool1 ,2,4-TrichlcrDbsttentIbphUula*4-Chltroaralinetoachlorciwtsdimt4-Oilcrcr3-«thylpnenal2-fethYlnaptithalattteadU trocycl opoitadi aw^4,6-Trichlorophaul2 , 4 ,5-Trichlxcpnenol2-Chlar(naphthalent2HtitnunilintDiKthvl phthalateAcEnapthvlB*3-Hitroanilirv
- 770 U770 U770 U770 U770 U770 U
. 7 7 0 U770 U770 U770 U770 U770U770 U770U770 U770U3700 U770 U770 U770 U770 U770U770 U770 U770 U77011770 U3700 U770 U3700 U770 U770 113700 U
-o
) . F u n n e l E x t r a c t i o n : Y E S 'i t i n . L i q . - L i q . E x t . : YES <
83-32-951-2B-5100-02-7132-64-9m-14-2606-20-2B4-64-27005-72-386-73-7100-01-4534-52-184-30-4101-55-3119-74-187-84-505-01-6120-12-784-74-2204-44-0129-00-0B5-6B-791-94-156-55-3117-91-721B-OH117-94-0205-99-2207-OM50-32-fi193-39-553-70-3191-24-2
AceupbthB*
4-tttraphenolDibaaofxan2,4-Oiaitrotoliane2,6-Dinitrotolunfcrthyl phthalate4-Qutrpphenyl-phBiYl etherFltureM4-tttrwniline4t6-0i oi tro-2-fWiylphwolIhutnHDdiphsrylimnt (1)4-firacphenyl-pbenyl ithrwtauuxobenznPntadilcrQphenalnwanthrenttathracmeDi-rrbutyl phthalateRuoranttontPyrnButyHwzyl-pbthilate3,3'-DichI(rttetziiiiniBRnzD(i)antlratentbit- (2-Ethyltevl ) phthal ateOryfentOi-ff-octyl phthalateBenzolblfluorantheneBmzotkHlutrxrthnB«nzo(i)pynneIndm ( 1 , 2,3-d) pyrmDibetzota^hlaDthracneBBtza(Ai)prYlene
Uigjici^OJ(ci
770 U3700 U3700 U770 U770 U770U770 U770 U770 U3700 U3700 U770U770 U770U3700 U770 U770 U
^"-fflni770U770 U1500 U770 U300*"770 U770 U77011770 U770U770U770 U770U
(circle one)e one)
(l)-Cannat be separated froi diphenylaaine
FORM 1
Laboratory Name
Cas€ No -7TS7Sample Numb«r
Concentration f-°y^ Medium
Date Extracted'Prepared fe -10-
Date Analyzed ______^>" ^ b"T7
Conc/Dil Factor ______!_______
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs
(Circle One) GPC Cleanup^Yes DNo
_____ Separately Funnel Extraction DYes
_____ Continuous Liquid - Liquid Extractron DYes
On
Percent Woisture (decanted}
CASNumber
ug/lor(CircU One)
319-84-6319-85-7319-86-858- 89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha -BHCBeia-BHCDelta -BHCGamma-flHC {LirvJanelHeptachlorAfdnn
Heptachlof EpoxtdeEndosulfan 1Dieldrin
4, 4'-DDEEndrmEndosutfan N4. 4'-DDDEr*dosulfan Sutfate4, 4'-ODTMethorycMorEodrrn KeioneChlordaneToupheneAroclor-lO16A/oclor-1221Afoclor-1232Aroclor-1242AroclcK-1248Aroclor-1254Aroclor-1260
It UIt U
Ih U.It, UL
ft U.it UIt UIt U3z-u~3i 1C7i IA7i U.?z u.^2 U?2 U./ f e o UJ? U.Ifco U-Jz^a*^o ll\lv Uibo a1'sc U-\bc U?ZV U.52.0 fx
CDCO
V( a Volume of ectraci m|ected (ul)
V - Volume of water extracted (ml]
W - Weight of sample extracted (gj
V. * Volume of total extract (ul)
orW.
Form 1 7/85
K yr^-w.**- -r rv*
Organics Analysis Data Sheet(Page 4)
CAS
T_.
I..
U *
ti
Tantativoly Idantifiod Compounds
v^b cm
in
_iS_L
11-1
- /- °l
lioo(wg/l oc
iiSCTD 3320 3
500-3
morn
o<sn".
cc
P»«l 0 7 85
Grganics Analysis Data Sheet(Page 1)
Simple Nunber: EL 262
Laboratory Na*e: ENVIRODYNELab Saiiple ID No: 87002776Sample Matrix: SOILData Release Authorized By:
Case No: 7351QC Report No: /3.Q.Contract No: _I__lp_iDate Sample Received:
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted)i 14.5
X)mom-<mocr>m-o
CJO00
CASto: uqkg CAStot
74-87-374-63-975-01-475-00-375-09-247-64-175-15-075-35-475-34-3lSr*0-547-66-3107HJ6-2Tfl- 371-55-656-23-5108-05-475-27-4
Chlor MethaneBraoKthancVinyl ChlorideChl oroethaneHethylene ChlorideAcetoneCarbon Bisulfide1,1-Oichloroethenel,HKchlaroethanetrans-1 ,2-DichloroetheneChlxofori1,2-Di chl (methane2-Butanone1,1,1-TridtloraethaneCarbon TrtradilorideVinyl AcetateBr Modi chl oroiethane
12 U12 U12 U12 U46 B
• 190 B61)6 U6 U6 U6 U6 U12 U6U61)12 U6U
78-87-510061-02-67W1-4124-48-179-00-571-O-210061-01-5110-75-fl75-25-2108-1H571-7B-*127-18-479-34-5108-flB-3106-90-7100-41-4100-42-5
1,2-Dichlaraprapanftrars-1 ,3-Oichlaraprop**TrichlorottheneDifaroachl araethane1,1,2-TrichtoroethaneBnzncii-l,3-0ichlaropro(«w2-Oil oroethyl vi nyl etherBroiofari4-Hetiryl-2-pentanane2- xanamTrtrachloraithmla^^TetracUxDFthmToluemDilarabenzeneEthylbBQBwStyrewTaUl Ivlen«
b U6 U6 UA U6 U6 U6 U12 U6 U12 U12 U6 U6 U6U4 U6 U6U6 U
••*• ttavartlnt
U IB^.
t«»i ltMt.> tit*
«a«wttw HMt «w **• MB*!*.
*•
OWi— • «!•«• •*« «•*•!»*
. 14 tMMM, th
t* prvtvly tf^ltw
»• fully
Labor at or y Name:Case No: 7351
ENVIRQDVNE Saiole Number: EL 2b2
Organics Analysis Data Sheet(Page 2)
;OO
1
Concentration: LOWDate Extracted/Prepared: 6-10-87Date Analyzed: 6-13-B7Conc/Dil Factor: 1Percent Moisture (decanted)
Sen volatile Compounds
6PC Cleanup : YES
M.
CftSto: uotg
106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-562-64-767-72-196- 5-378-59-188-TH105-67-965-85-0111-91-1120-63-2120-8H91-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-78B-74-4131-11-3*v*a fti nfJQ TO 0
99-09-2
Phenolbi5-(2-(Jairoethynett«r2-Oilornphenoll,3-OichJ(rttouenB1 , 4-Oi dil orobenzentBmzyl Alcohol1,2-Uichlorcterupw2HtothyIpheralbi s- (2-Chlaroi sflprapyl ) ether4-ftothylphanl(Hiitroso-ft-n-propyluinfteadUaraethaMNitrabenzeneInphorone2-Utrophenol2,4-DiMthylphenalBnzoic Acidbi s- (OU roethaty) Methane2,4-Oidilorophenol1 , 2 , 4-Tri chl ontenz meMitfithalene4-OtlxoanilineHBtachlorobutadiene4-QtI oro-3-«thy 1 phmol2-HetiiylrufhthaleneHex achl (rood op&itadiene2*4t6~TrichIxojrftfnol2,4,5-Tridilorqinenol2-Chloronaptithalenf2HtitnunilineDiwthyl ph thai ateAcmapthylene3-Mitroafliline
770 U770U770 U770 U770U770 U
.770U770U770 U770 U770 U770U770 U770U770 U770 U3700 U770 U770 U770 U770 U770U770 U770 U770 U770U770 U3700 U770 U3700 U770 U770 U3700 U
i. Funnel Ex t rac t i on : YES iitin. Liq.-Liq. Ex t . : YES (
CM KB
83-32-951-28-5100-02-7132-64 J?121-14-2606-20-2B4-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7210-OH117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acmaphthene2,4-Dinitrq)henal4-tttroptauIDibenzofxai2,4-ttnitrotoluaw2,6-DifutrataluBwKetiiyl phthalate4-QUxopnenyl-phenyl etfwFluor CM4Htitn«fuhne4,6-ft ni tnr2-fcthyl phenolIHutnscdiphotylaum (1)4-firMQpbBiyl-jihenyl ethertfaadilonteizenePntjdtlarcphaolnMNntlvEntAnttracen*Di-n-butyl phthalat* (RuoraatbcncPyrentButyl-bmiyl-phthalatt3,3'-DidUcntoizidi(«BenzofaJaotbricentbis-12-EthylteyI)phthalatiChryieuDi-n-xtvl phthalateBBizo(b)fluorintheneteuotkHluxanttaiBBzo(a)pyreuIndm(l,2.3-ol)pvrBWDibnzD£a,h)anthracB»Bauo(Qhi)pryle«
3JfiJ(circle one)NO )( c i r c l e one t
ugkg
770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700 U770 U770U770U3700 U77011
' l O o o N^-flfr-tt^
770 U770 U1500 U770 Uao-w u^ p^^770 U770 U770 U770U770 U770 U770 U770 U
<1)-Cannot be separated froa diphenyla«ine
FORM 1
Laboratory Name
Cas« NoSample Number
Concentration f*°y/ Medium
Date Extracted "Prepared P*"i'
Date Analyzed ____I—f o ~W
Conc/Dil Factor ____1_______
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs(Circle One) GPC CleanupJQfes QNo
j_7_______ Separatory Funnel Extraction QYes
_________ Continuous Liquid - Liquid Extraction OYes
Percent Moisture (decanted)
CAS ug/lorug^KgNumb«r (Circle One)
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494.70-557-74.98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Alpha-BHCBeta-BHCDelia -BHCGamma-BHC (LindanelHepiachlor
Aldrm
Heptachlor EpoxideEndosutfan tDtekJnn4. 4^DOEEndnn
EndosuHan It
4. 4'-DOD
EndosuHan SuHate4. 4*-ODT
MethorycnlofEndrin Ketone
ChlordaoeToxaphen«Aroclor-1016AroclOf-1221
Aroclor-1232
Aroclor-1242
Arocior-1248
Aroclor-1254
AfOClor-1260
/6 Ut& U
/fc U
fb aU U,fb K_
It UIfc U31- U-31 a7i (A?2. U.?2- U_32 U-3"! (X.Ibo U31 U.Ito U?2*? It
*fco alie? U.)ba ylIbC1 (X\t*j U32-1? K.
52_o LC
V( * Volume of extract injected (ul)
V$ = Volume of watef extracied (ml)
W = Weight of sample extracted (0)
V * Volume of total extract (ul)
or W. 30
morn-cmaCOm-o
CO
, 600
Form 1 7/85
NO
Organics Analysis Data Sheet(Page 4}
T«n(aiiv«ly Identified Compounds
70
0..
3.:
drsga.rbon
jdyt>on.rhoo* h «» _ * j -_mda
n.o
r*. I.&>>?-
. -7^3-6
Camc+ntrt t too
7 85
Qrganics Analysis Data Sheet(Page 1) ! —
Sample Number: EL 263 rT\|
Laboratory Nane: ENVIRQDYNELab Sa-ple ID No: 8700277?Saaplt Matrix: SOILData Release Authorized By:
Case No: 7351OC Report No:Contract No: ___U. _-_01;_"lp_ .Date Saaple Received: J^^.^-^.
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted) 15.0
CAS to: WSta
74-87-374-fiH75-01-475-00-375-09-247-64-175-15-075-35-475-34-3156-60-547-66-3107-06-278-43-371-S-656-Z3-5108-05-475-27-4
CM or MethaneBrtmethaneVinyl ChlorideChloroethanenpthylen* ttlxideAcetmeCarbon Disulfide1,1-DichlxQethene1,1-Oi chloroethanetrans-l,2-DidilxaetheneOil or W or i1,2-OichlxDethane2-flutancw1,1,1-TrichlorocthaneCarbon TetracMorideVinyl AcetateBr nod i chl oroiethane
111t
6i&6i61iiI6
2 U2 U2 U2 U18 9 t/3*77 f U3-
6U ?"UUuuu
2 UUU
2 UU
78-87-510061-02-A79-01-6124-48-179-00-571-4>2
**" 10061-01-5110-75-875-25-210&-10-1591-7B-6127-18-479-34-5106-88-3108-90-7100-41-4100-42-5
l,2-Did)laraprop*wtram-1 ,3-Oichl(raprQpeneTndilxoetheneDi bronchi onaethane1,1,2-TrichlxoethaMBenzeneci s-1 , 3-fii chlxopr opent2-Chl xoethyl vinyl etherBrovrfxi (HWiyl-2-penUxre2-HexanawTetracKIaraethene i1,1,2,2-Tetradaxatthwe (Toluene iChlorobnzene <Ethylbenzene tStyrm tToUl lylns i
UUUUUUU
2 UU
.2 U2 U
U» U> U
UUUU
w HMt f«r U f««,
fully
ill !• !••• UMN t
. 1OJ). t* Ilirtt
•**!•• HMt
1O 1*1 an«
Labor at ory Name:Case No: 7351
ENVIRODYNE Sa«nle Nunber: EL 263
Organics Analysis Data SheetiPaoe 2) or-
Concentration: LOWDate Extracted/Prepared: 6-10-B7Date Analyzed: 6-14-87Conc/Dil Factor: 1Percent Moisture (decanted) 15
CAS
Seat volatile Compounds
GPC Cleanup : YES,cc.
uqkq
106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3M106-44-5621-64-767-72-19B-95-378-59-18B-7H105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-5U-791-57-677-47-488-06-295-95-491-5B-788-74^131-11-3£K TU tJ99-09-2
Phenolfais-(2-Qilxaethyl)ethB-2-0)1 trapheool1,3-Oichltnbenzene1,4-OidilaroberuentBenzyl Alcoholl,2-&idil(TDb«nien*2-fethylphcnolbis-(2-ChlormscprQpyl}ether4-HethylphenoiK-ni troso-Oi -fr-prnpyl ati neHetachltraethamNitrobenzeneIsophcront2-ntropMnol2 * 4Hh tethy 1 phenolBenzene Acidbi 5- (Oil troethray ) frthane2,4-DidUcropnenol1,2,4-TricnlorobenzEneNaphthalene4-QUtroanihr«teach iTobutadiene4-QUxo-3-tethylphenol2-Hrthylnaphthalencteachl orocycl opentadi ene2,4,6-Trichlxaphenol2,4,5-Tridilorophend2-Chl xarupnthal ene2-WtroanilineDiecthvi phthalateAtvupthylene3-Hib-Qiniline
790 U780U790 U780 U780 U780 U
- 780 U790 U780 U790 U790 U790 U790 U790 U790 U790 U3900 U780 U790 U790 U7BOU780 U790 U780 U790 U790 U7801)3800 U790 U3800 U780 U790 U3BOOU
j. Funnel Ex t rac t i on : YES (itin. Liq.-Liq. Ex t . : YES 7
CASfc:
B3-32-951-28-5100-02-7132-6W121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-311B-74-187-86-5B5-OH120-12-784-74-2206-44-0129HXH)B5-6B-791- -156-5-3117-81-7218-01-9117-64-0205-99-2207-48^50-32-6193-39-553-70-3191-24-2
Acenaphthene2,4-Dinitra?nenal4-tttrophenoiDibenzofiran2,4-Oinitrotoluen*2,HhnitrotolueneDi ethyl phthalatf4-Qilxqpnenyl-phenyl etherFluorenf4-)titroanUint4,6-Dinitro-2-fctJ>yl phenolN-nitroaxtipheiylMir* (1)4-BroBflpbenyI-ptanyl etherteadilorobenzenePtotacfalxopnenolRienanthreneAnthraceneDi-ft-butyl phthalaUFluoranthenePyrentfiutyl-twcyl-ptititalite3,3 ' -Di chl tntonidineBenzo (a) anthracenebi i- (2-EthyI hayl ) phthal ateChryseMDi-n-xtyl phthalateDBUOtu/filfirjPuW
DBHZD ' KJ T lU iVIUW
Benzol a) pyreneIndeno(l,2,3-crf)pyraKfiibenzo (a,h) anthraceneBBnzotghilpa-ylme
NO")ICI
itflkq
7BOU3800 U3BOOU780 U7BOU790 U790 U790 U780 U3800 U3800 U790 U780 U790 U3900 U790 U
r S/ 650J 'U7anrj790 U790 U1600 U790 U240 W780U790 U790 U790 U780 U780U790 U780 U
one)one i
( l ) -Cannot be separated irom diphenylai ine
FORM 1
Laboratory Name
Case NoSample Number
-2
Concentration
Date Extracted'Prepared
Date Analyzed ______
Conc/Dil Factor ____
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBsMedium (Circle One) GPC Cleanup^Yes DNo
D " JO""T7_________ Separator Funnel Extraction DYes
' "' o ° >___________ Continuous Liquid - Liquid Extraction DYes
o
oc/>m
Percent Moisture (decanted)
CAS wg/( or U<K KgNumber (CtrcU Olrvef
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-O7-850-29-372-43-553494-70-557-74-98001-35-212674-11-2111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeta-BHCOelia-BHCGamma-BHC (UndarwJHepiachiorAldnn
Heptachior EpoxideEndosulfan 1
Dieldrin
4. 4--DDEEndrmEndosuHan II
4.4<-DOOEndosulfan Sutfate4. 4--DDT
MethoKyChlor
Endrin KetoneChterdaneTo*apn«neAroclor-1016
Aroclof-1221
A/oclot-1232
Aroclor-1242
Aroclor-1248Aroclor-1254
Aroclor-1260
/6U
Ifr U
\i- U.Ifo U-It U.fb K.It UIt U32- U-31. (L72. (A7iU,
3-ZU.32 U.
• 3z U.Ifco U7^ U.Ifea UJzo U,
' fco \LUj U.Ibs U':•? U»ix7 U
32.0 u.52.0 u
orW.
V( = Volume of extract injected (ul|
V = Volume of water extracted (ml)
W - Weight of sample extracted (g)
V. * Volume of total extract (ul)
_ v -ZO, 400
COCO
Form 1 7/85
00
•J
33
^b
^
[Ao
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Organic* Analysis Data Sheet(Page 1)
Staple Number: EL 264
Laboratory Naae: ENVIRQDVNELab Saiple ID No: 87002780Saaple Matrix: SOILData Release Authorized By: Jfl_CU)_
Case No: 7351QC Report No:Contract No:Date Sa»ple Received:
CftSMK
Volatile Compounds
Concentration; LOWDate Extracted/Prepared:Date Analyzed: 6-12-87Conc/Dil Factor: 1Percent Moisture (not decanted)
CflS
15.3
74-87-374-5S-975-01-475HJO-375-09-267-64-175-15-075-35-475-34-3154-60-567-66-3107-06-27B-93-371-55-656-23-5108-05-475-27-4
DU or MethanefrmethancVinyl Oil TideQUoncthanefethyleM QilxidtfcitiMCarbon Bisulfidel.Hhchlaraethene1,1-Oidiloroethanetrans-1 ,2-DichlcroEthawQUarofaril,2Hhchlarcethane2-fiutanone1,1,1-TrichIirDethjneCarbon TetradilohdtVinyl fceUttBrModidil or Methane
12 U12 U12 U12 U17 B57*4
' 6U61)6 U6116 U6 U12 U6 U6 U12 U611
78-57-510061-02-679-01-6124-48-179-00-5
0- 71-43-2KT*- 10061-01-5
110-75-875-25-2108-10-1591-78-6127-18-*79-34-510HB-3108-90-710MH100-42-5
l,2H)idilirqn|H»trani-1 ,3-DirfdtnpropeneTridtloroethneDi bronchi oroKthane1,1,2-Tridil methaneBnzncis- 1 ,3-fc ddtrqropwe2-ChloTjethylvinyletMrBrovfori4-ftrthyl-2-penUa»2-HBaKMTvtrachlu uethcv1,1,2, 2-Tetrxfal iroRhantToiuemCblorobenzBieEtfaylbeue»StyreneTotal Xyloe
6 UUUUUUU
12U61112U12 U6116 U6 U6 U6 U6 U611
orn<moCOm
CO
COoo
tvi Holt f«r tlwt
t». t* MBri,
Ui* r>.ult
L a b o r a t o r y Naee:Case Noi 7351
ENVIRODYNE
3A
Saeo 1 e Number : EL 2
Organic* Analysis Data Sheet(Page 2)
VX3
Seaivolat i le Coepounds
Concentrat ion: LOWDate Ex t rac ted /P repa red : 6-10-87Date A n a l y z e d : 6-14-87C o n c / D i 1 Factor : 1Percent Moisture (decan ted) 15.8
CAS to uqkg
108-45-2111-44-495-57-fl541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5421-64-747-72-198 95" 37B-59-189-75-5105 7-945-fl5-0111-91-1120-83-2120-BH91-20-3106-47-flB7-68-359-50-791-57-677-47-4ae-06-295-95-491-58-7BB-7M131-11-3tffi m n43JQ TffTl
99-09-2
Phetolbifi* i2*lJxIorTEuiYl J ffuvr2*ut 1 or opncooi1,3-DichlirtbenzBnt1,4-th til (Tobmz meBnzyl Alcdfill,2-0ichlxab*ramt2-fVthylptodb i s- (2-£hl xw sopr cpyl ) rther4-ttethylphenolH-ni tr oio-Oi-ft-propyl ui rwHecachlcrathantMtrobcozntIfophorm2-tttraphaol2,4-ftMthylptaralBvzoic Aciibii- WW (TtKthaty) fcthant^4-Dichlaroiitwnol1,2,4-TrichltrtteumiIbphthalm4-Oilfroanilini(fexachlorooutadiBtt4-Ovloro-3-«ethyl phaiol2-fMhvluphthaleMteadilcrcydcxHitadiene2, 4,6-Tr i cbl wcohewl2,4,5-Tndaarchenal2-Qil xonaphthalene2-*traaniliniDivtbyl phthalatttawpthylon3-Mitroanilint
790 U780 U790 U780 U790 U790 U
. 790 U790 U780 U780 U790 U780 U790 U780 U790 U780 U3BOOU790 U790 U780 U780 U780U7BOU780 U780 U790 U780 U3800 U790 U3800 U780 U7BOU3800 U
i. Funnel E x t r a c t i o n i YES Citin. Liq.-Liq. E x t . : YES
CASte
83-32-951-29-5100-02-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-01-6534-52-184-30-6101-55-3118-74-1E7-66-S85-01-6120- 12-784-74-2206-44-0129-00-0B5-68-791-94-156-55-3
218-01-9117-84-0205-99-2207-08-950-32-6193-39-553-70-3191-24-2
fcnapiittwnt2,4-Qinitraphcnol4-ttitrophnolDibmofuran2,4-Dinitrotnlueni2t6-0initn)toljentDirtfayl pbthalatf4-CilxcphHiyl-phBTyl eti*rFluormt4-ttitnianiIint4, 4-fc nitnr2HWiy 1 pboolN-iutnaodiptKTtylaiinf (1)« *----- i —— i ,L, . 1 -11--BroapMnyi -poea y i KMrnB^acVu GrtD0&Enir^Btt ACnl QTCDItenOl
PtananthrnfcrthracHJtDi-n-butyl phthalatfFluor an tbmPyrmBKtyl-bnzyl-ptttbalate3,3 ' -ffi chl or [tec idineBHUO (a) anthracene
OrysawDi-fr-ortyl phthalatcBeuo(tt)fluDranthcntBnofkHlurvithnBnzo(a)pyre)iInderoU,2,3-td)pYrH»K beoz D (a> ) anthr acawhrao(ctii)OTlent
. N _ 0 2 < c i r c l e one)&\j ^ c i r c l e one j
uqtg
790 U3300 U3800 U790 U790 U780 U780 U790 U790 U3800 U3BOOU790 U790 U790 U3800 U790 U780 U2400790 U780 U780 U1600 U780 U
780U790 U7»U790 U790 U780 U790 U790 U
(1)-Cannot be separated Iron diphenylaaine
: --- FORM 1
Namt
Case No -73*7
Organics Analysis Data Sheet(Page 3)
Sample Numt>«r
Concentration <tow? Medium
Date Extracted'Prepared *r~ T
Date Analyzed ._______ll^
Conc/Dil Factor ________
Pesticide/PCBs
(Circle One) GPC Cleanup^Yes DNof~i2_i________ Separatory Funnel Extraction QYes
__________ Continuous Liquid - Liquid Extraction DYes
\Percent Moisture (decanted)
CAS ug/1 or ugQ'KgNumber (Orel* Oo«]
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Atpha-BHCBeia-BHCDeita-BHCGamma-BHC (Lmdanel
HeptachtorAldnn
Heptachkw EpoxtdeEndosulfan 1Die'dnn4. 4--ODEEndrmEndosutfan 114. 4'-ODDErvdosulfan SuHate4. 4'-DDTMethOKychltxEndrm KeioneChlordaneToxapheneA/oclor-1016Aroclor-1221Aroclor-1232
Aroclor-1242
Arociof-1248AroCtor-1254
AroctOr-1260
ft UIfc Uft aifc ait u.>b ULIt UIb U
32- V~31 a7i tA7i U.^z u.52 U-?Z (X.ibo aJ7 U.IfeB U-
?zo U,^9 f,Ct f i j U.1fe3 U
It? IXIfetf u310 u.
52.0 U
orW.
V( = Volume of enraci injected (ul)
V = Volume of water enracied (ml)
W = Weight of tample enraaed (g)
V * Volume of total extract (ul)
_ v 1 &, 6 0
Form 1 7/85
OrganJcs Analysis Data Sheet(Page 4)
Tentatively Idontifiod Compounds
CAS
^Lfi. .3B.
iL3.
Moo 3
,S..
18.,
>«
23. _
? as
Organic* Analysis Data Sheet(Page 1)
Simple Nuaber: EL 263\
Laboratory Na«e: ENVIRODYNELab Sample ID No: 67002781Sa.plt Matrix: SOILData Release Authorized By: ]V\£Uj_
Case No: 7351QC Report No:Contract No: __b^rCU_-JDCL*i_"^____,_..^1^2.Date Saaple Received: _U_-_4rXrL
Volatile Coapoundt
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-12-B7Conc/Dil Factor: 1Percent Moisture (not decanted): 14.B
CM tew CKfe
74-B7-374-C-975-01-475-00-375-09-267-M-l75-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-37I-B-656-23-5tOB-05-475-27-4
aioroiethaMBrathawVinyl ChlorideEMoropthjneNethYlcnt ChlcrideACBtETCCartaon Wsulfidt1,1-DidUxoethene1,1-Oichlcroethanttran5-l,2-0ichlcmethenettitrcrfxi1,2-Oichliraethani'2-fiut.ncTCl,l,Mrichlcneth.mCarbon TetradiloridtVinyl AdtatiBroealichl oroeethaw
12 U12 U12 U12 U2 9 &190
UElUUUU
[2Uk U> u12U> U
78-87-510061-02-679-01-6124-W-l79-00-571-43-210061-01-5110-75-675-25-2108-10-1571-78-6127-18-479-34-5108-9-3108-W-7100-41-4100-42-5
1,2-Didilcropropanttrans-1 ,3-DidilarapropsitTrichlaroetbencDi braeadU onwthane1,1,2-TricUoraethaneBenzBiedi-l,3-&ichltrDprapBW2H3d(raethyl vinyl etherBraeofort4-fcthyl-2-pent*«ne2-4tsanaMTetrachltroethene1,1,2,2-Tetr .riil methaneTolueneQtlorobeniBWEUiYlbmzmStyrswTotal lylnn
6 U6 U6 U6 U6 U6 U6 U12 U6 U12 U12 U6U6 U1«
61)6U6116 U
•> TM* «!•« •**!!•• t»
••/•I
1M* «!•« 1*
». It K
riiBaltB. 1< «••*. tMnr «Mt
•rlMtM MtacM^ t» tJM M*i
(••). 1**]. If Halt
L a b o r a t o r y Na«e:Case No: 7351
Organic* Analysis Data Sheet(Page 2)
Nuiber: E&265^——— _ „ _ , - , _ _ _ _ _
Seaivo la t i le Compounds
Concentration: IONDate Extracted/Prepared: 6-10-87Date Analyzed: 6-14-87Conc/Di1 Factor: 1Percent Moisture (decanted): 14.8
CAS No: uqkq
100-95-2 Phenol111-44-4 bit-(2-QilaT»thyl)ether95-57-8 2-aiorophenol541-73-1 1,3-OidiloTiefuw106-46-7 1.4Hhchlorob«uen«100-51-4 Bvcyl Alcoxl95-50-1 l,MHdJloro6Bnzew95-48-7 2-tethylphenol39438-32-9 bis-(2-Oil£roi5a?ropyl)rth«r106-44-5 4-tethylphenol421-64-7 lhiitro5oH)i-iri)rapyIiiiM47-7M faachlororthane98-95-3 Mitrcbenzem78-59-1 Ifflphoront88-75-5 2-tob-cpMrwl105-47-9 2,4-DiMthylphBul45-85-0 Benzdc Acitl111-91-1 bi«-«Mtrt»ttey)hrth«12CKffi-2 2,4-Oidilarcphenol120-82-1 1,2,4-Trichlorobmzefle91-20-3 Miphthilne10M7-8 4-OU(roanilint87-68-3 tetdilarofettadirnt59-50-7 4-Qatrcr3- hylphenol91-57-4 2-fethylMpfiUuient77-47-4 HBachlcrocydopentadienc88-06-2 2,4,6-Trichlflrophenol95-95-4 2,4,5-Tridil(rn>nenDl91-58-7 2-ChloraaphthalewBB-74-4 2-tttroanilint131-11-3 Kiethyl pbthalatc208-96-8 Aonapthylem99-09-2 3-tetroaoilin»
770 U770 U770 U770U770U770 U
. 770 U770 U770 U770 U770 U770 U770 U770 U770U770 U3BOOU770U770 U770 U770 U770 U770U770 U770 U770 U770 U3BOOU770 U3800 U770 U770U3800 U
6PC Cleanup : YESSep. Funnel Ext ract ion : YESContin.
Ofi to:
83-32-951-28-5100-02-7132-44-9121-14-2406-20-284-64-27005-72-386-73-7100-01-4534-52-186-30-4101-55-3HB-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-48-791-94-154-55-3117-81-7216-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Liq.-Liq. Ext. : VES
Acmapttthnt2,4-thrutnphenQl4HfttroptolDitwzohran2,4-ftnitnjtoluent2,6-ferutrotaluBWferthyl ptttaUtt4-Oil(roptayl-ptwnYl fttarFluareM4-ltitniaiulini4,6-0iwtTD-2-ni*hylphiriolK-nitrondiphBnylaiiv U)4- roBpfcarl-ptartyi ethrteach! trotes emPtttadtlorqteiolPhaunthrnAntbracnDi-rHwtvl ptthalatcFluor aithmPyrmBotrt-beKyi-pdthalat*3, 3 '-ft chl oniBniiiintBno(i)aatfracBWbii-<2-Ettiyltevl)phthalat*OrysHwDi-n-actyl phttttlat*BenzolblfluaraithenehnzQfttflurvttnewBBno(alpyrn»IndenoU,2,3-cri)pyrer*K iMnzo (a,h) anthr actntBcnzolaMJpa-ylvN
G3D<cir(^Qicir
«rfl
770 UTBVI IIJWJ U
3800 U770 U770 U770U770 U770U770 U3BOOU380CU770U770 U770U3800 U770U
^iooj^
770 U770 U1500 U770 U320-£</J-770 U770 U770 U770U770 U770U770 U770 U
one*
= = SSS = S=SZSK=S»3BEX = S 3 X X X = «>
(l)-Cannot be separated fro« dipnenylaaine
FORM i :.rrf"
Latxnaiory Name
Case No ' -*
Organics Analysis Data Sheet(Page 3)
Sample Number
Concentration £°w.) Medium
Date Extracted'Prepared b "ll
b i , vw».,...._.,*— ________"'o 8
Cone/Oil Factor: ______I_____
\Pesticide /PCBs
(Circle One) GPC Cleanup^Yes DNo
1LZ________ Separatory Funnel Extraction DYes
_________ Continuous Uquid - Liquid Extraction DYes
Percent Moisture (decanted)
CAS ug/loruovKgNumber (Circta One)
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Alpha -BHCBeta -BHCDelia -BHCGamma-BHC (LindanelHeptachiorAidnnHeptachlor EpoxideEndosutfan 1Otetdnn4. 4'-ODEEndnnEndosuffan II4.4'-DDDEndosutfan Sutfate4. 4'-DDTMethoxyctilorErtdrin KetooeChlordaneToxapneneAroclor-1016
Aroclof-t221
Aroclor-1232
Aroctor-1242
AroclOf-1248Arocfor-1254
ArocIor-1260
/fa Uh U!h U.ife ait U.'b (XIt, (4u u3z- u-32.0.7i UJiU.?2. U.32 LL71 U.tbo U7z u.|{-D \J_3zv\L1fc0 |,L
Uo UIfe? U'iC1 IX\te UT2-0 l^-52.n (^
orW,
V( s Volume of extract injected (u)|
V s Volume of water extracted (ml)
W = Wetjjht of sample extracted (g)
V( * Volume of total extract (ul)
3o<\ v lo.aoo
form 1 7/85
No* Organics; Analysis Data Sheet(Page 4)
Tentatively Identified Compounds '%CAS
Cooc •*!< f • t
3B2.
3..
S..
7..6..
10..
14..
15..
16..
17..
18..
19..
21..
3i$- "S303J3
27..
28..
3O..
form 1 Pan 8 ? 8S
Organic* Analysis Data(Page 1)
Sheet
1 S aaple Nuaber: EL
Laboratory Naie: ENVIRQDYNELab Saaple ID No: 67002782Saaple Matrix: SOILData Release Authorized By:
/3Case No: 735LQC Report No:Contract No:Date Saiple Received: __U_-_.y_-_V7
Volatile Compounds
Concentration: LDUDate Extracted/Prepared:Date Analyzed: 6-12-87Conc/Di1 Factor: 5Percent Moisture (not decanted) 15.4
A
CASNo; uqkg
74-B7-374-85-175-01-475-00-375-09-267-64-175-15-*75-35-475-34-315WO-567-66-3107-06-27W3-371-95-656-23-5IOBHJ5-4T5-27-*
QltrarthanfbmwthaniVinyl QilorideQiloroethwfMfaylm GhlxideAcetateCarbon ftiuHidc1,1-Oidil trothe*l,Hhthloroethanetrans-1 ,2-Oichl(roethBiettlffoftril.HndUxMthw2-ftitancml,l,Hrichloroeth»Carbm TrtradtLiridtVinyl ftotatflBrnodi chl or owtiunc
39 U59U59 U591)
1708. TOB
30 U30 U30 U30 U30 U30 U59 U30 USOU59 U30 U
7W7-5100il-02-i79-01-*124-W-l79-00-571-43-210041-01-5110-75-875-25-2106-10-1591-78-61Z7-1M79-34-5ioe-w-3108- 71«HH10M2-5
1,2-DichIcn^rDpanetrans-1 ,3-Di chl cropropeneTridilaroetheMDibraBchlarnethnl,l,HridilB-MthaneBmiffccif-1 T3-Oidil orqrDpene2-OJ oroethyl nnyl etherBronfcrt4-Mhyl-2-pmtaroic2-te«r»Tftradtlorathml,lA2-Tttr«tl(rMttwToljsieQvlorobenincEthvlbnznStyrwiToUl lylmes
301)30 U30 U30 U30 U30U30 U59U30 U59U59 U30 U30 J30 U301)30 U30 U30U
rwultk. t* MM, th»v •—« M fully
Laboratory Nane:Case No: 7351
ENVIRDDYNE Satple Nuaher: EL 2oc
Organic* Analysis Data Sheetipage 2)
Seaivolatile Compounds
Concentration: LOWDateDateConc/Di1Percent
x t r a c t e d / P r e p a r e d : 6-10-87n a l y z e d : 6-U-B7il Factor: 1t H o i s t u r e ( d e c a n t e d ) : 15. A
06 to:
108-95-2 Phenol111-44-4 bii-lHSilorwUwl) ether95-57-fl 2-Qil(rDpheoQl541-73-1 l,3-0idd(rtteuene106-46-7 1,4-fcdilircfcnzenf100-51-6 Benzyl Motel95-50-1 l,2-&id>larobenze«95-AB-7 2-ttthylphwol39638-32-9 bis-(2-ChIoroiscorDfiyl>ether106-44-5 4-tethylpt*cl621-64-7 IKitroaHh-ftTr^latiM
98-95-3 totrabwzene78 5r 1 . liophoroncBB-75-5 2-fttropherwl105-67-9 2,4-ttwthylptaal65-85-0 Benzoic Acid111-91-1 bii-tDiltrathiMyUkthm120-fl3-2 2,4Hhthlarcctenal120-82-1 1 ,2,4-Trid\l(rabenzB«91-20-3 tephtbilene106-47H3 4-{Morowilinf87-68-3 teachlircbutadiene59-50-7 4-tWcrtr3-«thyl phenol91-57-6 2-ftethYlMphthalene77-47-4 tearfUcnrydnsntaihent88-06-2 2,4,6-Trichlorcptwnol95 75-4 2,4,5-TridUtro()hi«il91 -5B-7 2-aicrcr*hUnlMBfi-74-4 2-fctro*iilir»131-11-3 Diwthyl phthalate208 96 '8 AceMpthyleni99-09-2 HbtruniliM
uqkq
7801)7BOU780 U7801)790 U780 U780 U790 U780U780U790 U^ 11Tot) U780 U780 U780 U780113BOOU7801)790 U790 U7901)780 U780 U780U780 U780 U780U3800 U780 U38001)780 U780 U3800 U
Sep. F u n nC o n t i n . L
OS to:
83-32-51-28-5100-0 7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6
. 534-52-1
101-55-3118-7HE7-66-585-01-8120-12-764-74-2206-44H)129H30-0B5-6B-791-94-156-55-3117-W-721B-OH117-W-O205-99-2207-08-950-32-8193-39-553-70-3191-24-2
el E x t r a c t i o n : YES(^i q . - L i q . E x t . : YES (
Acauptithcne2,4-Oinitn^nenol4-fctrcDMnoiDibcnzofuran2,4-ftnitrotoluent2,6-OinitrDtalumDiethvl phtkaltte4-Qaorophenyl-phwyl etherRuoreM4-ttltnHnilinc4,6-fcnitnr2-ftthTlphenol
4* flro*Dpwjyi"pnwyl tuwHexhltnbenzemPent ich 1 on^MnolPticnxithrEniftothraceMto-n-butyl phthalat*Fluor mtheoePyrentBtttyl-tazvl -ptithal ate3,3'-OictJarabenzidineBenzoUlcthrKRiebis- Mhyl heiy 1 ) phthal iteDryswtDi-n-ortyl phthalatiBenzolbHluorvttteMBenzotkJfluranthencBenz o ( ii pyrernItvfro ( 1 1 2) j"Qi ) pyrweHi bfnzo U^) anthr xer»Bnzolghiiperylent
NAjlciSOci
qk,
780 U3800 U3800 U78011780 U790 U780U780 U790 U3800 U3800 U780 U790 U790 U3800 U79011ffiftu
£7470 J790 U790 U790U1600 U790 U650 Bf780 U790 U7BOU790 U780 U780U7BOU7BOU
(l)-Cannot be separated tram diphenylaaine
FORM 1
T\
ft03.one Ione )
Latx>raiory Name
Case No "
Organics Analysis Data Sheet(Page 3)
Sarnpla Numt>«r
^V-
<£>Concentration f°^ Medium
Date Exacted'Prepared k "
Date Analyzed _____K> ~i t^
Conc/Dil Factor: _______/
Pesticide/PCBsi
(Circle On«) GPC Cleanup^Yes DNo
'-SI______ Separator^ Funnel Extraction QYes
—————————— Continuous Liquid - Liquid Extraction DYes
Percent Moisture (decanted) is.CA5 ug/l of ugl/ KgNumber (CirefcOn*)
319-84-6319-85-7319-86-858-89-976-44-8309-OO-21024-57-3959-98-860-57-172-55-972-2O-833213-65-972-54-8
1031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-21HQ4.28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeta-BHCDelu-BHCGamma-BHC (L<r\danetHepiacniorAldrin
Hepiachlor EpoxideEndosu'fan 1Dteldrm
4. 4--DDEEodrinEndosuMan If4.4'-DDOEndosuKan SuWate4. 4'-OOTMethoiychlorEndrin Ketone
ChlordaneToKjphen*Aroclor-1016
Aroctor-1221
Aroclor-1232Aroclor-1242
Aroc(0'-1248AroclOf-1254
Aroclor-1260
Ib UIt UIb U.?fo au utb KIt \4U UZz- w-32. LL7i (A7i U.^Z U.52 U31 U.f f c o UJ2 U.K:2 U
3l» \LU?5 l,t
lij U)t? a'i? IX\b<3 U
1^ U.
^2.o K
V( = Volume of ertraci injected (ul|
V * Volume of water extracted (ml)
Ws = Weight of sample ertracted (g)
V » VoJume of total extract (ul)
or W.
Form 1 7/85
E LOrganic! Analysis Data Sheet
(Page 4)
Tantativaly td«ntifi«d Compounds
CASN Number
(ug/(
I "PnspOLncuc, OQxi
12..13..
15..
17..
18..
19..
24..
27..
28..
30.,
1.01.06
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Laboratory Name:Case No: 7351
ENVIRODYNE Sane I e Nuaber : EL 2 6 7
J'-a•O
Organic* Analysis Data SheetiPage 2)
See ivo l a t i l e C o m p o u n d s
Concentration: LOWDate Extracted/Preparea: 6-10-87Date Analyzed: 6-14-87Conc/Dil Factor: 1Percent Moisture (decanted) 15.4
CASto: uctq
108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3W106-44-5621-64-767-72-198-95-378-59-18B-75-5105-67-965-85-0111-91-1120-83-2120-flM91-20-3106-47-887-68-359-50-791-57-677-47-4BB-06-295-95-491-58-788-74-4131-11-3208-96-899-09-2
Phenolbis-(2-Qacroethyl}etherHMcrocfwnoll,3-0ichlcni)enzeneU4-Oichl7d>enzB»Benzyl Mortal1,2-DichlGrobenzene2-flEthylphenolbis- (2-Qiloroi scprcpyl ) ether4-MhylphenolH-ni troso-Oi -trpr npy 1 m neHeKacMtroethaMNitrctouentla^hcrtm2-thtri h«ool2,4-OieethylpheralBenzene Acidbi s- (Oil tmethm y ) Hethane2,4-Dichlarophenol1,2,4-TrichlardwueneHaphttulene4-QUtroaniUnetteactil or abut aril ene4-Q\l aro-S-B-thyl phenol2-Hethylnaphthalenetoachl trocyd opentadi ene2,4,6-Trichlorophenol2,4,5-Trichltrophenol2-Qtl nronapnthal ene2-ttitroanilineDiwthyl pttthalateAcenapthylET*3-Mitroaniline
7BOU790 U790 U790 U780 U780 U
- 780 U790 U780 U790 U790 U790 U790 U790 U780 U790 U3800 U790 U790 U790 U780 U790 U7BOU730 U790 U780 U780 U3900 y780 U3BOOU780 U780113800 U
) . F u n n e li t i n . L i e
CA£ to:
83-32-951-2B-5100-02-7132-6M121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-48-791-94-156-55-3117-81-7218-01-9117-94-0205-99-2207H36-950-32-8193-39-553-70-3191-24-2
Ex t r ac t ion : YES <I . - L i q . E x t . : YES C
keniphthew2,4-tonitrophenol4-MitrcphenolDibsuriiran2,4-DUitrotoluene2,6-OirutrotoluBieDiethyl phthilate4-Chlxapnenyl-phenyl etherFlunrmt4-*traaniIine4,6-Oinitro-2-fcthylphwolH-mtnBotiphenylaiint (114* u'UKpMnyl-pnenyl etherItaxachl orcfaenz eniPentadilcrflptanolPhenanthrentfetiracawDi-n-fautyl phthalateFlvranthenePyrmButyl-benzYl-phtNalate3,3 ' -Di chl cntett i di neBenzo (a) anthracewbiK-(2-ethYlhoyl)phthalat»OryseneDi-n-octyl phthalaUBenzo<b)flutraothfncBeruolUflutr anthemBentotaJpyrewIntBtt(l,2,3-cd)pyrH»Dibenzod.h) anthraceneBenzo (ghi)perylene
^NOJ^c i r
7BOU3BOOU3800 U790 U790 U780 U790 U790 U790 U3800 LJ3SOOU790 U780U7BOU3800 D780U7BQJJ
[_7M i f/it IT*
-780UTfiOU1600 U780 Ueoor i7BOU790 U780U790 U790 U790 U790 U7BOU
(l)-Cannot be separated fro* diphenylaame
FORM 1
e one)s one)
Laboratory Name
Case No _ ——Numb«r
26-7-
Concentration f ^ Medium
Date Exiracted 'Prepared
Date Analyred ______ b-f
Conc/Dil Factor _____ !
Organics Analysis Data Sheet(Page 3) "o
Pesticide/PCBs -
(Circle One) GPC Cleanup^Yes DNo
2________ Separator^ Funnel Extraction QYes
__________ Continuous Liquid - Liquid Extraction DYes
Percent Moisture (decanted)
CAS ug/lorug^K^Numb«r (CJrcV* Of>«)
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860 S7-172-55-972-20-833213-65-972-S4-8
1031-07-850 29-372-43-553494.70-557-74-98001-35-212674.11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Afpha-BHCBeia-BHCOUa-BHCGammj-BHC (UndJnelHejjiachlorAJdrm
Hemactiior EpoxKteEndosutfan 1DiekJnn
4. 4--DDEEndrmEndosulfan tl4. 4'-DDDEndosuMan Surtate4. 4'-ODTMethox>chlorEndnn Keion«ChiordaneToKjQt^neA/odtx-1O16Aroctof-1221
A/ociof-1232Aroclor-1242Aroc1(X-1248Aroctof-1254
Aroclor-1260
Ik U\b U
1h U.It, iJLit U.Ib U(It Uifc U.3Z-IA^2.L672. CA.71 U.^z u.52 U71 U./bo UJ^ U.Ifeo U-7^o U
»t?o \L\io U.lie? U
its' a^fco U3in K52. L<.
\
orW.
V- = Volume of extract in|*cted (ul|
V = Vofurne of water eitracted (ml)
W « Weight of umpte e«tr»aed (gt
V. * Volume of total extract (ul)
Form 1 7/85
K/O-. Organios Analysis Oata Sheet(Page 4)
Tentatively Identified Cocnpouods
CAS
Ui n - on.
3.
3 - 2 Sac 3
ArpCart^n8. i-s-o
TV-opQAmV ac^J ;2-ii._
? es
ecology and environment, inc.111 WEST JACKSON BLVD., CHICAGO. ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
Date Received for Review _TO: -fcim Paehc ic^From: Zena Gold-KaufmanSubject: HOD
PAN: XUOI4
Sample Description ______Organics (VOA, ABN, Pest/PCB)
LowLow WaterDrinking Water
Other
Date Review Completed
Case t ?3bll
Inorganics (Metals, Cyanide)
Low SoilLow WaterDrinking WaterOther
Project Data Status
Incomplete, awaiting:
Completed!
FIT Data Review Findings:
CAC&Smol
fcf,0
errcr
____\s Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.
Book No- ^ Page No.
t.1
V0A"
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),
~~$6Q Ludf'f, . ' 'COMPOUND J
cMororicthanebromomclhsnev i n y l chloridechloroethanemethylene chlor ideacetonecarbon dlaulflde1,1-dlchloroethene1, 1-dichloroethan*trans-1,2,-dlchloroethenechloroform1,2-dlchloroethana2 -but a none1,1,1-trJchloroe thanecarbon te t rachlor ldevinyl acetatebrotnodlchloromethene1,1,2,2-tetrechloroethene1,2-dlchloropropanetrane-1, 3-dichloropropcnetrichloroethenedibromochlorome thane1,1, 2-tr lchloroethanebenzenecle-1,3-dlchloropropena2-chloroethylvlnylelherbromororn2-^exanone4-melhyl-2-pentenonetetrechloroethenetoluenecMorobenreneethylbenzeneatyrenetotal xyleneiH-nllrosodlBiethylemlnephenolanilineble(2-chloroethyl)ether2-chlorophenol1 ,3-<Jlchlorobenzene1 ,4-dichlorobenzervebenzyl alcohol1,2-dlcMorobenzene2-««thylphenolbla(2-chlorol8opropyl)ether4 -me thy 1 phenolN-nitroBO-di-n-propylsmlnenexacMoroethanenitrobenzeneJeophrona2-nitrophenol2,4-dlftethylphenolbenzole acidbla(2-chloroethoxy)me thane2,4-dlchlorophenol1,2,4-trlchlorobenzeneoapthalene4-chloroanllInehexachlorobutedlene<-chloro-3-methyIphenol2-methylnaplhBlenehe*act)lorocyclopentadlcne2,4,6-tr lchlorophcnol2,4, 5-trlchlorophenol•> -ti , .„„„„... k . - . i , _ w
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HGO. m$\COPOUNO
dlMlhyl phthalsts•cenapt hyleno
3-oitroenilln8•cenaphthene
7,4-dinltrophenol4-Mt rophenoldib^n; of*iranJ,<-dlnltroLoluen« '3,$-dlnitrotoluenedlcthylphthsUto4-chlorophenyl-phenyletherr 1 no r ann4-ol t rosni line*,£-dinitro-2-methylphenol
N-n 1 1 r osod I pheny 1 BJD I ne4-broaxiphenyl-phenylether
herach]oroben?epa
pentechlorophenolphenanthreneanthracenedi-n-txjtylphthelBtefluor«nthenebenildlnepyten«
butylbeniylphthelata3, 3'-dJchlorobenzldineben7o(a)8nttir8cenebi»(2-ethylhflxyl)phth8tatf l
chryeenadi-n-octylphthalatubenlo(Wl<}fluor8nthenebervio(«)pyreneindano(1,2,3-cd)pyrenedlbenxo(*,h) anthracenebenio(q,h, i)peryler>«• lpht~6HCbeta-6HCdelta^HCgaena~€HC(llndan0)
hept«chlor•IdrlnheptacMor epoxldaerxJosulftn Idleldrln*,*'-OOCerxJrinerxJosul fan II4,4'-«JO•ndrin aldehydaerxJoaulfan sulTate4,«'-OOT•»«thoxychlorendrln k«tonoctitordtruitoxapherteAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Artx:lor-1254Aroclor-1260
/•
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ij
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i^cn
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ch 1 or Q"1clhen ebromon-.cthanevinyl chloride
Drr.
chloroethanemelhylene chlorideacetonecarbon dlsul fide1,1-dlcMorocthene1,1-dlchloroelhanat rang-1 t2,-dtchloroethenechlorofor1,2-<JlcMo roe thane2 -bu IB none1,1jJ-t rich1o roe t hanecarbon te t rachlor ldevinyl acetatebroroodichloromethane1, 1 ,2 ,2- te t rechloroe thene
Jjj-dlchloropTopanetrana-1, 3-dlchloropropcnet r lchloroethenedlbromochlorome thane1 ,1 ( 2- t r l ch lo roe thanebenzenecie-1 , 3-dlch]oropropen«2^chloroethylvinylether^broflioform2-hexenone^-ffiethyl-2-pentenonatetrachloroethen*toluenechlorobenzeneethylbenzena•tyrenetotal xylenesN-nitrosodl me thy laminaphenol^•nlllnabia(2-chloroethyl)ether2-cMorophenol1, J-dichlorobenzene1,4-dichlorobenzenebenzyl alcohol1, 2-dicMorobenzene
j HMtttiy 1 phe no 1biBj2-ch]oroi9opropyljether4-»ethylphenolN-nitro8o-di-n-propyla«inehexacMoroethanenitrobenzeneJeophrone2-ni t ropnenpl2,^-dInethylphenolbenzole acidble(2-chloroethoxy)methane2,4-dicMorophenol1,2,4-trlchlorobcnzen*napthalene4-chloro*nllin«heicachlorobutadlene4-chloro-3-<nelhyl phenol2HnethylnapthalenehexBctt lorocyclopentadlcr te2, ^,6-tricMorophenol^2, fl, 5-t r ich3o£c>pji^nol_
Ir
£/
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ff5T
Po0
COMPOUNDdimethyl p h t h a l e t eacennpthyleneJ-ni t roeni l lneecenephthene?,4-dlnitrophenol4-nllrophenoldibiruof-inn?,4-dinltrotoluen« '?,4-dinitrotoluen«diethyJphthalsU4-chlorophcnyl-phenyletherf l u o r a n *fl-nitroBnUina4,6-dInltro-2-fnethy]phcnolN-nit roeodlpheny lamina4-bromopNenyl -p^ienylctherhex8chlorobtn?epepent ecMorophenolphenanthreneanthracenadi-n-butylphthalaterjuoranthenebenzldlnepyrenebuty lbenzy jph tha la te>,3'-dlchloroben7ldinebenzo(a)anthr8ceneb l« (2 -e th> lh ' )xynph thBla t f lchryeenadi-n-octylphthalatf lbenzo(b4k ) fluor anthenabenzo(t)pyrenelrxJ*rx>(1,2,3-cd)pyrenadlbenzo(i,h) anthracenabenzo(q,h,l)perylen«tlpna-BHCbct«-6HCdelta-BHCgamna -8HC ( 1 1 ndane )heptichlor•Idrlnheptachlor epoxideervdoeuir«n Idlaldrln«.4'-ooeendrlnerxJosulTtn II«,4'-000endrln aldehydeendoaulfan sulfate4.4'-OOT•lethoxychlorendrln ketonachlordanwtoxaphenaAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-12^4Aroclor-1260
/
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- ————
_ X T E :
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V
•J3JECT: Rev iew of Region V CLP DatRece ived for Rev iew on
PROM: Curtis Ross. Director (55CRL) <f££^i j?- d/~^ /tCentral Regional Laboratory / '
TO: Data User:r-Pj^T
We have reviewed the data for the fol lowing case (s ) .
SITE NAME: //O O £-C\f\\^£\H SMO case No.T ~~T No. of D.U. /Activity
EPA Data Set No. F^l J-±> Samples: // Numbers 79oS"/Cl.7M/o O
CRL No
SMO Tra f f i c No.Mrs. Requi red
CLP Laboratory: £rt V* Q^yne ______________ for Review:— ~~ ~* ~~ ™* —i-- - - - . . . - — •
Fol lowing are our f indings:
( ) Data are acceptable for use. /~) .- ft InI(/-'( \f Data are acceptable for use with qual i f icat ions noted above. f<f (7 . / / // \( \ D a t a are preliminary - pending ver i f icat ion by Contractor Laboratory. '( ) Data are unacceptable.
cc: Duane Geuder, Quality Assurance Of f i ce r , EPA Suppo.rt Serv icesJames Petty, Chief Qual i ty Assu rance Research , EMSL, Las Vegas
EPA FORM 1320-6 (Rev. 5 /87 }
70
DATA QUALIFIERS
Contractor
Below 1s a summary of the out of control audits and the possible effecto n t h e data f o r this case: " . . . . V
C
bJ I J~h«— V> TKe 7 ?
we Theo//t
f- e
S*
C/5
Reviewed by:
Phone:
Date:
3DATA QUALIFIERS f-
Contrctor:Case
1s a summary of the out of control audits ;*nd the possible effect _.on the data for this case: " .... - ._ .. ,,v.
(C^^^"
n
f?- ^ L />r/f 7-^
Piet- b o /ut I kc-
1 IP MC- I iv-/r M6-
• Z. /_.{tG-/t&
/'/-f
Reviewed by:
Phone:
Date:
DATA QUALIFIERS
Contrctor:Case 73
Below Is a summary of the out of control audits and the possible effecton the data for this case:
5ffyvfy@ n
s: M s / in $ b ffL cA/t/./t/r J
e,/
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j \
14
Reviewed by:
Phone:
Date:
DATA QUALIFIERS
nrm- ...a '*•
Contractor:Cise 71 r/
fBelow 1s a summary of the out of control audits and the possible effecton the data for this case: . .
CDCO
1(1 1 nflPSTlct'de
At i.^i
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Reviewed by:
Phone:
Date:
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
VOLATILE HSL COMPOUNDS- - CONTRACTOR
7'vr
'AQ
/fco7«c*-f £W .s-f W- /DATE/TIME:
ChloromethaneBromomethaneVinvl ChlorideChloroethaneMethylene Chloride
Imt. Cal . Cont. Cal. lCont. Cal. Cont. Cal.£-/i"-f7 \£r*r- <•?/•¥»RF I5RSD * RF
Acetone )Carbon Oisu l f ide1 ,1-01 en 1 oroetnane1,1-Di chloroetheneTrans-1 ,2-Oi chloroetheneChloroform
•70£,?
j-J
50
^0?/33
^,-3utanone I1,2-Dichloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1 ,2-Oi chl oroorooaneTrans-l,3-DichloroorooeneTri chloroetheneDi bromochloromethane1,1,2-Tri ChloroethaneBenzenecis-1 ,3-Oichloroorooene2-Chl oroethyl vi ny let herBromoform4-Methy 1 -2-Pentanone
'?-Hexanone.'etrachloroethene1,1,2,2-TetracnloroethaneTolueneChlorobenzeneEthvlbenzeneStvrenem-Xvleneo/o-Xv lene
AFFECTEDSAMPLES:
1
*
j*J
RF 50 *'
\J
_ _ _RF |5D
. 1
*
1
f 1
/V?*? ^6 * 3c= -*f f ST ff>» f S*
Cont. Cal/. . -•*-•*_-•.'• J;:.-
RF 50 i*
1
__ ^^ n i _, _..^__^ _
I1t
1 11 I1
*v1 '
•
* These flags 'should be applied to the analytes on the sample data sheets.
1/87
/i-U N I T E D STATES E N V I R O N M E N T A L P R O T E C T I O N AGENCY R E 3 I O N V
C A L I B R A T I O N O U T L I E R SVOLATILE HSL COMPOUNDS
CASE.it 73.5V '_____ - - CONTRACTOR
/A&TtwetiT £~r*5--A.DATE/TIME:
ChloromethaneBromomethaneVinyl ChlorideChloroethaneMetnvlene ChlorideAcetoneCaroon Disul f ide1,1-Oicnioroethane1,1-QicnloroetheneTrans-l,2-QichloroetheneChloroform2-3utanone1,2-Dichloroethane1,1 , 1 -Tri chl or oe thaneCarDon TetrachlorideVinyl AcetateBromodicnloromethane1,2-OichlorooroDaneTrans-l,3-DichloroDrooeneTrichloroetheneDibromochloromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Oi chl oroprooene2-Chloroethyl vinyl etherBromoform4-Methvl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorooenzeneEthvlbenzeneStyrenem-Xylene0/o-Xvlene
AFFECTEDSAMPLES:
Inlt. Ca .t5-/jf-^TRF *RSO <r
1
Y</./ ,T
1
•
/^«*.'
Cont. Cal .i-73-*?/;rao(RF iO *
3^-9 J
Cont^ Cal .1-2V-P7/VJIRF XD 1*
*.
Cent. -Cal.;•.- '
R= liD
1V3.7 JIsr.v J
/wn*/
,
1t
^
1
1
*
Cont.' Cal . ;-' ,— '-.:--!••-*. •
RF %0 1* *
1
/"*-•?A/s*2. Ie"t^i^-*s"t-a7o «^sr¥
«.36i- ti2?O fntfr.'-tf *ffj-qft->r/-e-i*jry6/V/J-6- F/Mf^S
_ . . . .
ff>»W<i-ff ,•«$•)?1
—— T
1
.
a£
* These f lags should be applied to the analytes on the sample data sheets.
1/87
CASE?
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
VOLATILE HSL COMPOUNDS73ft _ -• ' CONTRACTOR
Init. Cal. iCont. Cal.lCont. CaU iCorrt.. Cal. iCont. CalD A T E / 1 *..*,:
IRF ]«SOChlororretnaneBromcmetnaneVinv i CnlorideChlo^oe'haneMetnvte-.e CnlonaeAcetoneCarc:n Dlsul f ide
-: C"; oroetnane- 1 cnoroeinene
Trars-1,2-01chloroethene
RF
'hlc-oform
1,2-Cic .11 o roethane1,1,--i rlchloroethaneCarcsn (etracniondeVinv i AcetateBromodlcnloromethanel^-jlcnlorooropaneTrar.s-l,3"DichioropropeneTricnloroetheneOibrcrrcchlorome thane1.1t2-~rich1oroethaneBenzene
\
cis-l,5-DlchiorooroDene2-Chloroethylvinyli etherBromoform4-Me-hvl-2-Pentanone?-HexanoneTetracnloroethene
,1,2,2-TetrachlgroethaneTolueneChlc-o-enzeneEthv;benzeneStvrenem-Xvie^aO/D-<V": ene
AFFECTEDSAMPLES:
RF RF |%0 I- RF |%Oc^r
* These flags should be applied to the analytes on the sample data sheets.
1/87
CASE* 73 f/
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDS(Page 1)
CONTRACTOR
•t#3rA.u/tftr*jT s-+?<*DATE/TIME:
Phenolbisi-Z-Chloroethyl )Ether2-Chloroohenol1 ,3-Oi chl orobenzene1 ,4-Oi en 1 orobenieneBenzvl Alconol1,2-Di cnlorobenzene2-Metnvl phenolbisi2-cnloroisoorooyl )Ether4-Me^nvlphenolN-N -itroso-Oi-n-? ropy! ami neHexacnloroethaneNitrooenzeneIsoonorone2-Nitroohenol2 ,4-Oi methyl phenolBenzole Acidbi s ( 2-Chl opoethoxy )Methane2,4-Oichlopoohenol1,2,4-irichlorooenzeneNaontnalene4-CMoroanil1neHexacn ioroDutadiene4-Chloro-3-Methvl phenol2-Metnvl naphthaleneHexacn lorocyclooentadiene
_j 2,4,6-TpichloPOohenol2,4,5-Trichloroohtfnoi2-CnlcronaDhthalene2-N-,troanilineDimetP.vl PhthalateAcenasnthylene3-NitPoanil1neAcenacntheneZ,4.Qin1tPOOhenol4-NitroohenolDicanzofupan
_. _ - -AFFECTED-—-SAMPLES:
[nit. Cal.y-/-f7
RF
Wi
1RSD *
•
?f-r?33. f
%
>T^*
€•636?<£La70
Zrtss-f -<r/v?A"a.
Cont. Cal.
RF M *
Cont.-Cal.lCont. Cal.lCont. Cal.*
RF M * RF
i•
ID *
-
RF %D |*
t
Cofr-t-
V7
tcCO•v
* These flags should be applied to the analytes on.the.sample data sheets,
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEHIVOLATILE HSL COMPOUNDSPage 2
735*; CONTRACTOR Om/yVST*t,/*ftTA-T £ff t
DATE/TIME:
2,4-Oinitrotoluene2,6-OinitrotolueneDletnylontnalate4-Cnlorooneny l-oneny letnerFluopene4-Nitroaniline4,6-QinitPO-Z-MetnvlpnenolN-NitPOSodipnenylamine4-3 pomoonenyl-oneny letnepHexachloroDenzenePentachlopoohenolPhenanthreneAntnraceneDi -n-Buty 1 ohthal ateFluorantfienePypeneButyl benzyl phthal ateBenzo(a)Antnpacenebis(2-Ethylhexvl)PhthalateChryseneDi-n-Qctvl PhttialateBenzo(b)FluopantheneBenzo(k)FluorantheneBenzo(alPyreneInaeno(l,2,3-cd)PypeneDi benz(a,h)AnthPaceneBenzo(g,h,1 ) Pepvlene
[nit. Cal.f-t'^7
RF
&;£
"1RSD
•36*1
»
/?
Cont. Cal.-tCont. Cvl.lCont. CaV.
RF ZU
...
* RF
-
ID
-
* RF
•
%U
-
*
- -
Conr» earnO
RF
- - •
-.u -*s.-f•(
ff
n
1
SEE PAGE 1 FOR AFFECTED SAMPLES.
These flags should be applied to the analytes on the sample data sheets.
1/87
UNITED STATES E N V I R O N M E N T A L PROTECTION AGENCY R E G I O N VC A L I B R A T I O N OUTLIERS
SEMIVOLATILE HSL COMPOUNDS
CASE? IS^t(Page 1)
CONTRACTOR € */l//£C2>VX;€
/*/srm,*9**JT s-?»^ Unit. Cal. ICont. CaUCoat, Cal.lCont, Cal . tCont.- Cal .DATE/ TIME: '7-J-77
IRF %RSO w
Phenol 1
\RF %0 1* RF %3 I" RF 110 1* |RF 10 "
bis(-2-Chloroetnyl )Ethep 1 12-ChloPOonenol 11 ,3-Oicnlorooenzene I
1 1 11
1 11 1
1,4-Oicnlorooenzene • — i —— |— I IBenzvi Alconoi 11,2-Oicnlorooenzene 12-Me*nvlonenoi 1bis t2-ch ioro isooroov l JEtner 14-MetnylDhenol 1 1N-N i t POS o-01 -n-? POO v laminaHexacnlopoetnaneNitPooenzeneIsoonorone2-Nitroohenol2,4-OimethylohenolBenzole Acidbi s ( 2-Chl oroethoxv )Methane2,4-Dichloroohenol1 ,2 ,4-Tri cnl orooenzeneNaonthalene 14-Chloroaniline 1HexacnloroDutadiene 14-ChlopQ-3-Methvlohenol 12-Methylnaonthalene 1Hexacnlorocvclooentadiene 12,4,6-Trichlopoohenol2.4,5-Tpichlopoohenol
3/.3
2-C'nloronaonthalene 1 1-2-iNitroanilineDimethvl PhthalateAcenaontnylene • 1 -3-N1 troani line l irlAcenaohtnene 1
3*
1
-
\1
1%
2.4-Oinitroonenot 1 1
1
1 - 11 11 1
1
11 I1 1
11
11 I I I I I1 1 1
I I 11 - 1i i ii I
1 1- 1 11 1 1 1
4—Nltpoonenoi \ys.8 t.T 1 1Dicenzofuran ly^.a l o - 1 1 1 1 1 1
AFFECTED" * SAMPLES:
i l l
€*flT9 MS \ 1 1 1• ^f v 1 1 i 1
1 1 \ ' '\ ' ~ -
1 1 1 1
1 1 1 1
1 1 1 1
t i l l
1 1 1 1
1 1 1 1
1 - 1 1 I .
mnn<-•=maCOrn•o
01
* These flags should be applied to the analytes p n < t h e . s a m p l e data sheets
1/87
c
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY RESIGN VCALIBRATION OUTLIERS - - ' ' , . . _
SEMIVOUTILE HSL COMPOUNDSPage 2
ASEI "73 <T/ CONTRACTOR £*JWAOWH&
/ASlT&vSirMT flit.
DATE/TIME:
2,4—2initrotoluene2.5-Cinitrotoluene
[mt. Ca• * - -
. ICont. Ca * Cont. Ca7-a-y*F 1WSO
D*e*^vlon-naiate•i-Cr * orocrenvl-onenvietrierF'tucreneA-';- -roam "i ine .*&•i,5— Di ni tro-2-Metnv lonenolN— v: troscaionenvlamined-Sramoonenvl-onenvletner
« 'H
1
. - - .. _ _. Cont. Ca . ICont. Ca
•* IRF 110 1* IRF
1 1 II 11 t
JO
1
*
- • r(!
.RF 'iD "
1 - 1-
C 1
hexccnlorooenzene ' 1PentachloroohenolPher.antnreneAntnraceneDi -n-Butvl ontha! ateFluoranthenePyraneBu*vl benzvl phthal ateBer.zot a lAntnraceneois'v2-Ethvlhexvl ) Phthal ateC'nrvseneQi-n-Oczvi f*htha ateBenzo{b)FluopantheneBenzo(k)F1uopantheneBer-,zo(a)PyreneIr.ceno(l,2,3-cd)PyreneDi Denzta,h)Anthracene
1
1
1
Be".zo(a,h,i ) Pervlene 1 1
'.i'1i
t I111111111 .11I
1
\
11
onnTlSrmaenm-ow
o
SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytss on the SIT.;".a data sheets.
1/87
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVQLATILE HSL COMPOUNDS(Page 1)
CASE.? 736~} . CONTRACTOR eAJt//*oT>y*e
/jj$rKv*i&*fT S'lff-z, llnit. CalO A - i / i IME: 1-7-2- f 7
IRFPhenolbTSt-2-Chloroetnyl )Echer2--nioroohenol1 , 3—3 1 chl orooenzene1 ,--3: cnlorooenzeneBe-Z ' / t Alconol1 ,2-0 i en 1 orooenzane2-'-1e~nvlDnenolbis i 2-chloroisooroovl }Ether4-Me~rivlDhenolN-Nitroso-Di-n-?PODvlamineHexacn loroethaneN-.zrcoenzeneIsoor.orone2-Nitroohenol2. 4-0 i methyl phenolBenzcic Acidbist2-Chloroethoxy JMethane2,4-Dichloroonenol1,2,4-Trichlorooenzene
. ICont1
XRSD «
. Cal .ICont:. -Cal . ICont.- Cal .ICont. Cal.1
RF *Q
1 11
11 1
NsDnzhalene 14-Ch'ioroani line 1 lj .7Hexacn 1 orooutadi ene4-Ch'iopo-3-Methvlonenol
3"1
2-Me'hvlnaohthalene 1Hexacn1! orocyclooentaoi ene2,4,6-Tpichloroohenol2,4,5-Tpichloroohenol2-Cn loronaontnalene2-Ni troani lineC:me-nvl PhtnalataAceraontnvlene3-?4izPoani line lv^.7 J
11
RF
1
11111
-
Acaranhthene t2.*i— Dinitroonenol lva-3 T--N". trooneno 1 I3/.V U
13 - |RF %0
1I1111
1
111
11 I1 1
C'-enzofuran I
AFFECTEDSAMPLES: "
1
1
•
* IRF
1
1
»0 w
--
1I
1 1 !i 1 1
tf^Z&f \ 1 1t^gtt \ 1 1
_p i t t
— I | - 1 - -
1 11 1 11 1 11 1 11 1 11 1 1t I I
RECEIVED SEP 1 5 1387
* These f lags should be app l ied to the analytes on . the.sample data sheets,
1/87
/sr
CASE.?
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLVTILE HSL COMPOUNDS• ' Page 273 yv • CONTRACTOR
•ropn
/MfTfi^Mf^rDATE/TIME:
*- ?~
2,4-Qlnitrotoluene2,6-Olnltrotoluene01 etnvlomna ate«i-Cn loroonenvl-onenv leanerFiucrenei-Nitroanlline
Lnit. Cal.r-t-~t7RF iRSU *
Cont. Cal. Cant. Ca . Cont. Cal.lCont. Cal.1
RF %0
1 -1
1 1\.0it
4,6-01nitro-2-MethvlohenolN-Ni trosodi onenvl ami ne4-3rcmoonenv 1-onenvletnerHexacnlorooenzenePentachloroohenolPhenantnreneAnthraceneDi-n-Butylohthalate .FluoranthenePyreneButvl benzyl phthal ateBenzot a) Anthraceneb1s(2-Ethvlhexvl IPhthalateChrvseneDi-n-Octvl Phtha ate
- Benzo(b)FluorantheneBenzo(k)FluorantheneBenzo(a)PyreneInceno(l,2.3-cd)PyreneDi &enz( a, h) Anthracene 1Benzo(Q,h,1 ) Perv ene 1
C. 1
i
* Rh
1
"U « RF |%0
1
1
* RF ID
-4 —— 1.
1
*
1 1
c
SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytas on the sample data sheets.
1/S7
ENVIRODYNEENGINEERS
July 10, 1987
Ms . Carol Shaef f erSample Management Office .209 Madison Street, Suite 200Alexandria, Virginia 22314
Dear Ms. Shaeffer;
Enclosed are partial results of analysis of Case 7351 for Volatiles, BN'As ,ar.d Pesticide/PCBs performed by Envirodyne under Contract No. 68-01-7067.Eleven soil samples, EL268 through EL270, and EM851 through EM858, werereceived on June 12, 1987. The samples were screened for semi volatilelevels by GC; EL268 and EM853 were run as medium level samples based onscreening results. All low level semivolatile extracts were cleaned upon GPC. -
A matrix spike and matrix spike duplicate, the second for this case, wererun for both levels of semivolatiles . Volatile QC to cover the second setof twenty samples on the case will be submitted with the samples receiveden June 19, 1987.
Three volatile samples, EM856, EM857, and EM858, showed solvents (methylenechloride and acetone) above the calibration range. These samples werererun with smaller aliquots on July 7. The dilutions also showed themethylene chloride above the calibration range, and concentrations of thecompound were much higher than those on the 5 gram aliquot. The sampleshad a very muddy consistency, and we feel that the surface area of soilexposed during purging is a factor in determining purge efficiency ofr.ethylene chloride. Another explanation for these results could be thatthe solvents were a contamination from the sample bottles; if this werethe case, different locations of the sample in the bottle could yielddifferent solvent concentrations. We are submitting both the "undilutedand diluted sample results, but have no results below the calibrationrange. Toluene-do was higher than the control limits for two of thethree undiluted samples, but in control on one of the diluted samples.
If you have any questions about this report, please contact me.
Sincerely,
m
COm-o
_oo
Margaret C. WinterProject Manager
XCW/jagEnclosure
METHOD BLANK SUMMARY
No. Region Contractor Contract No.
or VltMlI CONC.Ltvfl C*S COMPOUND (HSL.flC ON UNMNOVMI CONC. CHOL
n-n-S7ii nms
in-ii-7 IMA l3.Ji..4fu^ KM J *) 330u^n t ncru/x,
UM IcV Htru,
\JOA ! e r\e
U-3M-17 u;13 f 0
Comments:
FORM IV 17/85
METHCT BLANK SUMMARY
Ca9« No. .Region Contractor g/V.yM*o ^ Contract No.
rue >o 0*tt Or UttHll COMC INS MO c*s COMPOUND (MSL.tIC O" UH*MOVNt CONC. UHlfl
JT5
UML W\ flfi^. line. CM rru. els^M 10
id10*1 --v -
L 1110
L,-*
-5
Commenls;
FORM IV
CMC No.Low
SOIL SURROG. E PERCENT RECOVERY SI 'MARYv.._^^
__ Coolracl Laboralory £KJ V I E-Q CW/U 6________ Conlracl No.Medium
- - V O L A T I L t --- --- - - - - . - - . - - - - - - . - - . - - - - SCMI-VOLAUU
ta.viM-0*
in-tin Ut-ltll
-01
III- Itll HI'1141 111- till
**
III-till
_ _ _ . - - >fc t OX* fv\ecias..loo
H C
J_L
0 •SOS *
U>0il A 0.3 *
OU1n £Lon I53-*
5T
asMO
In sotQ 3-
3 /
i _._i«J 3-7
lol
* VALUES ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS**ADVISORY LIMITS ONLY
Volatiles:Semi-Vola tilts:Pisticidas:
out oTout ofout of
I outiidi of OC limitst outiidt of OC limit iI outiidt of QC limit! ;•''.
7/85
FORM IIHT^V3
C*se No,Low ——
. JRC-..T I...JCK _.IY _ Mht....Y**
Contract Lob^tocy GM.Ui R.CJ>/M6- _______ __ Contract No. Of" "?OYMedium _yi
i*t*rtc•o.
&L~ A.(t> Btw "jS!x\IVHV 1tLOlAfrt)kuSl^rrv-jC
Ill-Mil
'\
> •'*, (It-ilM
\
^X^>^ ^
1
1
t 1 OiCHiO*0
«•• tto
^'/•'
-\
^^
•CMKMf -»»
III- 1141
"2 3*3 I-i
u ^>n 11
t-'iuOMft-
lit- Mil
O *i
^STU*&9^2>
*
Dl*
^5*<J4
. 1V,q^*S5
_.
t
* VALUES ARE OUTSIDE OP CONTRACT REQUIRED QC LIMITS voiaii^ADVISORY LIMITS ONLY S"m'"~
Psatic
•
111- Mil
SI"? 1IpU^i o1 1
l*«! O OUt Of Q t
r\ *%. f~)X/nlafilA*^ , ,. mil of nJ x j
idest —— i — out of —— b , t
Ill-llll
101^Sn t7*1Ss
iii-nii
Mo*13(a*!SoSo
-
11
,
•PESTICIDE--
^log\ \ a-1^5"^ci'5'*
outsidi of OC limits 7/B5outaidt of OC limitsoutiids of OC limits
Comm«nU:
FORM II
IOC.V
SOIL MATRIX SPIKT MATRIX SPIKE DUPLICATE ^COVERY
CM« No. Contractor Contrtot Mo.
Low L«v«l KUdlum
FRACTION
VOASMO
SAMPLE NO.
8/NSMO
SAMPLE NO.
ku^'BACIDSMO
SAMPLE NO.ku atA
PESTSMO
SAMPLE NO.
EL 9^<g
COMPOUND
1.1-OictX)lortlh«ncTfichlorotthf n«Ch>OfOb*nicntToluentBfnitn** ,?.4-Tiichtorob*nitntAccniphlhtnc7.4 Dmi|roiolutf>tPyuritN-Nitrowdi-n-Propylcmint1 ,4-Dichlorob«nicn«Penuchlo'ophtnotPhtnol
2-Chlorophcnol4-Chloro-3-Mt|hylphtnol4-NilrophtnolLtndtntH«puchtofAldrmDitidrinEndrm
4.4'-DDT
CONC. SPIKEADDED (uq/K9|
100,
>
poo
/^OO. CjOCt
\ s
Oot^o
^ sr
Fi OOO
SAMPLERESULT
Oi
\
. _•_•
, >
\~
/
*c,Ktn-=t
CONC.MS
^^s^oII^Ooo*1s3o&la^CColU'looc•^Ul/OO^1-2 OCO3D 'Son,Ons DOC;>riO6o|»>Moco
MOCb
MO"H/MifaiIMM-J-110'1 _-v ^\l.
%REC
1ft
Jjft-^?A| i»>01^1V I I*\o^uv\o>T1
ioi*3lM»^Ml*IM$>fSM*i-\ i
CONC.MSD
•memil^OOq^OTT)1HHTL
^V'lot^fsr^friti^^riro1*34 m/HTrl
2or?cin1*\^ ArtftosoKKM^OMZ-bOTA5^4-1
%REC
fij>111qt|K1 ( 4°»15^5^ri-1;v»loaIO4<run103»OT>
15S*lo;s»01ft i
RPO
1O4to1^133010ItS(iW5*6-5*M33'|3(,•a^
or i IMITS *RPD
72242121212319473638274735503350503143384550
RECOVERY59-17202-13760-13359 1396614238 10731.13778-6935-1424102628-10417-109289025-10276-1031 1-11446-12735-13034.1323M3442-13923-134 ,
'ASTERISKED VALUES ARE OUTSIDE oc LIMITS.RPO: outiidi OC limit i
OUltidi QC limiuoutiidt QC limiuouliidt OC limiu
RECOVERY: VOAi__out ol.__;B/N £• - out o» .12s;ACIO-U——OUt 0» \Q: J
PEST _U,out of 12;;
outiUf OC HmlnoutiW* OC Hnwliourtld* OC Hmfliouliidt OC Mmilt
FORM III7/65
C«M NO. 135SOIL MATRIX S P i ; /MATRIX SPIKE OUPLICAT RECOVERY
Contractor &KJ1/IE MDVMfc Contract No.
Low L«v«l Mtdlum Lovtl
FRACTION
VOASMO
SAMPLE NO.
B/NSMO
SAMPLE NO.
ACIDSMO
SAMPLE NO.G.M <&£>**
PESTSMO
SAMPLE NO.
COMPOUND
1.1-Oictxitorfthtnt
TrichlorOfflhcncCNoro ben lent
Totu«ntBrnren*l,?.4-Ttichlofob*nr«nfAc*n«phthenc7.4 Dmiirololuff*PyreneN-Nilrotodi-fl-Propvlimin*1 ,4-DichlorobcnttntPeniichlorophtnolPhtnol2-Chlorophenol4.CMoro-3-M«1hvlphinol4-NilrophtnolLindmt
HflpuchlofAid* mDittdrinCndrm4.4--ODT
CONC. SPIKEADDED <uq/K9|
LuT O
_/\*\ 3OO
v
M
/)
^0<«G
150ISO|-i/»
SAMPLERESULT
^
\
i
^
V
<CR-Pt-
CONC.MS
•^TIOF\n.^oIflH "iC>H'TS I r»SH IDCM-iuriST^OlaptroI WtlU DOT)
^V't)l frO•» i3.T
61HO°\^•-III
REC
5"Un*i!\o\ttnsi5°1414
M1)^0(01<rt3IS") A135*
v IT
"1*1
TiUB11 M
CONC.MSD
Ulo^O/S' lO
5tw*o53s'OLmo3^Crti'^290JitcrOi id ti
1 0 T OO
^ I^ObL?*1M976
ISOJQ.Ou <y
REC
HIM^T
_5JDfL
i)X
n^^^>DMA/^X*lb-5^115"*Ka111linSoI.e.
RPD
^ IS3*ni*•i.
5 rg
/3c50*M^c^^f,<jt
ri i*^SL
OC IIMITS*RPD
722421212123194736382747355033505031433B4550
RECOVERY50-1726213760-13359-13966-14233 to;31-137288935 14741-17678-10417-109769025-10276-10311-11446-17735-13034-13231-13442-13973-134
*ASTERISKEO VALUES ARE OUTSIDE OC LIMITS.
RPO:
Convn
VOAI ___ out of ___ :B/N —— 1 — out ol ..'fl, ;ACID g- out of — -;PEST —^ — out of — Lz — ;
outiidt OC limliiouiiidt QC liminouliidi OC limit!ouliid« OC llmiii
RECOVERY: VOAi __ out of __ IB/N —— L,. out ofJ-i;
PEST _I_ out ol JA;
owttUt OC Mmltiovlild* OC llmliounldt OC Hmlliouiiidt QC llmiti
.....
1
FORM Ml7/85
S d3S
Organic* Analysis Data Sheet(Page 1)
Sample Number: EL 26B
Laboratory Mane: ENVIRODYNELab Sample ID No: 87003034Saaple Matrix: SOILData Release Authorized By:
Case Not 7351DC Report No:Contract No:Date Sample Received:
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-23-87Conc/Dil Factor: 5Percent Moisture (not decanted)
mom
aCO
enu503
12.8
US to: ugkg WSto:
74-87-374-83-975-01-475-00-375-09-267-44-175-15-075-35-475-34-3156-60-567-66-3107HJ6-278-93-371-55-456-23-510&-05-475-27-4
* .1- BT.
• v*lu*.
* lloMt far '
EM«t./«11Wtll
M*CtlB« 11-
Oil or MethaneBroKMethaneVinyl ChlTid*Oilxoettunetethylew QilxideAcEtcneCarbon Disulfidc1,1-ftchkraettael,l-IHchlxoeth«netrans-1 ,2-ftchlxoethmeDilarofxi1 ,2-Oichlxoethane2-ftitancne1,1,1-TridtloraBthaneCarbon TetrachlorideVinyl AcetateBroBoii chl or Methane
B~. l
MV tM. -• ——— »1 t. t». *^-t,
. *- *«. «k «-W-. «- t
•n artlBn. 11MB ta n*t nv^>*avl
It.) 1TW «BM*W«B *—— U« TBBtfl U-
57 U57 U57 U57U
1100 B290
29U29U291129U29U29 U57U29 U29 U571)29U
Ci
•n till*
>«/<a
•M TklB
IV ——— 1
^•••l
78-97-510061-02-679-01-6124-48-179-40-571-43-210061-01-5110-75-fl75-25-2108-10-1S1-7&-6'127-1W79-34-5108-9-3108-90-7100-4H100-42-5
i
flBB BPpllMB «• •••<
__ r— «.™- »y .e/
*lB« t* *m+4 ahBP an
V, It IntflCBtM PBVM
> tMB «*t« UBV t* *•
l,2-&idUoraprDiMnftrans- L, 3-Oi chl ornpr opecTridilxoethenDi bro-ochlaraBfthane1,1,2-TrichIcroethan*Bnzeneci i-l , 3-Oi chl oropropew2-DU xnethyl vi ny 1 ethe-tartari4-hBthyI-2-pHitanDnt2-fteiwn*Tetrachloroetha*l,i,2,MitradilorDtthiwTduBWDdxobcnzeiMEthvlbenzBvStyrmeTotal Iyler.5
1C1«. BM-«^» ————— • «*. 1
•». Mn.1. .... .1 MM1.1
•lyta IB *•*>« !• klM r BB i
l.l w^MI. .!« —— n—— -
** apa»-B»rl«tB Bctl«n.
29U29U29U29U29U29U29U57U29U57U57U29U
_29UrQ? J29 U29U29U29U
..M1M..-
LB*»>-10
•Ml BB B
taiUwi an*
B« wmllM. T>llB »!•• I
multB. 1* uaart. UMPIT wvC •• *ullv •Mcrttow* MX
Laboratory Name:Case No: 7351
ENV1RQDYNE Sample Nunder: EL 269
Organics Analysis Data Sheet(Page 2)
Seaivalatile Compounds .CO
Concentration: MEDIUMDate Extracted/Prepared: 6-26-67Date Analyzed: 7-2-87Conc/Dil Factor: 1Percent Moisture (decanted): 12.8
CASto: uqtq
106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-B87-68-359-5&-?91-57-677-47-486-06-295-95-491-58-786-74-4131-11-3206-96-899-v9-2
Phenolbis-(2-OUm*thyliether2-Qil or c^teral1,3-Oichltnbeniene1,4-DidilorctenzeneBmryl Alcohol1,2-Oichlcrobeizene2-HBthylpnsnlfcis-IHhloroisoprDpyl lether4-ftBthylphaxilH-nitroKHh-n-propyliiiiwHaachlaroethaneHitrobenzoteIsophorane2-tttrophmot2,4-OiMthylphenolBenzol c Acidbi s- tDiltroeUtt y ) Hethane2,4-frichiorophenol1 ,2,4-TridilorcbenzEneNapftthalene4-QilxtuniHneteachlorobutaiieoe4-akro-3-«thy 1 pnerral2-MhvlnaprithaleneHoachlorocyLlcpBitadierie2,4,6- Trichl or ophenol2,4,5-Tridilarcphenol2-Qil7aiaphthalene2-*troarilineDiwthyl ptithiliteftcen*pthvlff>e3-fetroaniline
23000 U23000 U230COU23000U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U110000 U23000 U23000 U
. 23000 U23000 U23000 U23000 LJ23000U23000U23000 U23000 U110000 U23000 U110000 U23000 U23000 U110000 U
Sep. FunneContin, Li
CASfc:
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6554-52-186-30-6 '101-55-3118-74-187-86-585-01-812H2-784-74-2206-44-0129-00-085- 8-791-94-156-55-3117-81-7218-01-9117-64-0205-99-2207-08^50-52-8193-39-553-70-3191-24-2
1 Extract ion : YES 'q.-Liq. E x t . : YES ,
AteMOhttww2,4-ihrutrn*wol4-*tn$benolDibenzofiiran2,4-DUitrotfllaBit2,6-DinitrotQlifl*fttthyl pfcUuiitt4-Qilarnjhenyl-pnenyl etherHucrenf4-HitroamIine4,6-fonitrD-2-Metrtylp6enolM-mtrwodiphsiylaiint (1)4* Brotaphflnyi -phwyl cthirteachlarEbenzer*FwtactilorophenolFtcnanthnreAnthraceneDi-rHwtyl phthalateFl or anther*ryranButyl-benzyl -phthaUUw»j wiuuU LucnziQincBBiioiiJ itfiLnriccntbis-(2-Ethvlr«vl)phtKalatBDryMfieDi-rroctyl pnthalateBBttoibHlucrttttieneBBUOtk)flucrantheneBBuouipyrentiKtrod^^-dlpyrvieDibemou.hiarttwacerwBenzotgruiperylene
<NO) (cir(J^)(cir
ugkg
23000U110000 U110000 U23000 U23000 U23000 U23000U23000 U23000U110000 U110000 U23000 U230W U23000 U110000023000 U23000U23000 U23000U23000UZ3000LJ45000Uaooou_
(2400 J^2050123000U23000UZ3000U23000 U23000U23000 U2300UU
(l)-Cannot be separated from diphenylamne
FORM 1
Laboratcxr Name
Case No
Organics Analysis Data Sho«t(Page 3)
Numb«r
Concentration Low
Date Extracted 'Prepared1
Date Analyzed —————
Posticide/PCBs
(Circte Ooe) GPC Cleanup CD Yes QNo
Separatory Funnel Extraction QYes '"• *'
Continuous Liquid - Liquid Extraction QYes
X)mo
oConc/Dil Factor
Percent Moisture (decanted)
CAS ug/1 oK^gyKg.Number (CircU On*)
319. 84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553169-21-912672-29-6H097-69-111096-82-5
Alpha- BHC
B«ta-BHC
Oetta-BHCGammj-BHC (L«rxJanelHeptactilorAWnn
Heptacnio*- EpoxwleEndosulf an 1Ontldfin
4. 4--OOEEndrinEnbosuHan II4.4'-DODEndosuKan Sulfate4.4'^ODT
M*thorvchIO«'
Endrm KeioneCWordan*
Touphene
Arod(X-1016
Aroclof-1221Afoc1o»-1232Afoctof-12-:2Aroc(o»-1248A/OClOf-1254
Afoc(0f-1260
IZO, 0 01/PO, <5 K.120, O IL}lG U:rt-c • u[7-c tL_JA^.O U730,0 U
-Z-Vo -USffO.O U..We U
*JWQ.O aXVO.Q U*</o.o U*y-n U.
~I3LOQ,0 U2<JQ<0 11
IZOO,0 U
MQO.O a/2oo.£ IJLMOO.O U
1300,0 UW«=o,o Ujsoo.o Ufftfoo.O Uytjc&.Q Ui
V( = Volume o< ertraci inj«cied (u()
V = Vo<um« of water enracted (ml)
W « Wetght of Mimple e«tr»cted (g)
V * Volume of iota) extract (utj
orW.
Form 1 7/85
urqanics Data SheetiPaqv 1)
Si-pie Nue-ber: EL269
Laboratory Naae: ENVIRQOYNELab Staple ID No: 87003035Saiplt Matrix: SOILData Release Authorized By: _Q?£lU__
Catff No: 7351QC Report No: ~/S /Contract No; _(cA__QjDate SaaplB Received:
Volatili Coipoundi
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-87Conc/Dil Factor: 5Percent Moisture (not decanted) 13,0
CAStte CK to
74-«7-374- 3-975-OH75-00-37W9-267-64-17V15-075-35-475-34-3!&-6iH67-66-3107-06-27^3-371-55-656-23-5108-05-475-27-4
EMoroKthantBroKMethaneVinyl ChlxideOtlortEttuninpthylne ChlcridtAutmCarbon Dlsulfide1,1-IhcKlraetherw1,1-Oirtla-oKhawtr«-l ,2-Oichl croethemOil or of xil,2-Dichl(rtiftha{v2-Butancne1,1,1-TrichlororthaneCjrlKii TrtrachlorideVinyl AcEUtfBrondichlorotetluni
57U57U57115711730300
29U2 9 U291129U29U2 9 U57U29U29U57U2 9 U
7B-B7-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-B75-25-210B-10-'l591-79-61Z7-1B-479-34-5ioiHfi-3106-90-7100-41-4100-42-5
i^cftlT^tjan.tr ans-f, 3-Di chl on^rtpwtTrichlxoetheM&i broeochl (methane1,1,2-TridilcraethawBenzeneaj-l,3-ftdilcrcprcvM2-OU ornethyl vi nyl etherBroeafxi4-fethyl-2-pent2xn2-HnmaneTetracMraetha*1,1,2,2-TetradilcroethaneTolueneDUtrobenzmEUrrltureewStyreneToUl him
2?U2 9 U29U29U» U2 9 U2 9 U57U2 9 U57U57U2 9 U29 U
»52 9 U2 9 U2911
•«/M! IN
t^H«l«lCI
tlB1«B»»10
lw IkMt far
l -ill ill
U (•«,
*v kwt not 4M*t*M. Ifia m^kv !• tM
1T M^tn*
Laboratory Name:Case No: 7351
ENVIRQDYNE Saagle Number: EL269
Qrganics A n a l y s i s Data Sheet(Pag* 2)
o
Concentration: LOWDateDateCone/Di1Percent
Seiivolatile Compound*
GPC Cleanup i YES: x t r a c t e d / P r e p a r e d : 6-19-07malyzed : 7-1-87i 1 Factor : 1t hoisture (decanted): 13
CASto:
108-95-2111-44-495-57-8541-73-1106-44-7100-51-695-50-195-48-739638-32-9106-44-5421-64-767-72-1on fie TW-TJ-J78-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-5B-788-74-4131-11-3208-96-899-09-2
Phenolbis-(2-QUcmethyl}«ther2-Qilorophtnoll,3-Dichl(rubenzene1,4-DichlorobenzeniBenzyl Uriell,2-0ichlorobai:ene2-fethylphmalbis-l2-OilaraisojirQpyl)ftt«r4-fethylphenol(Hii tnwHH -n-pr apy 1 ui ntHesachl methaneIK L — *- —— ——ntrooenzene
2-tktroplwwl2,4-fc«thylphenalBenzine Acidbis-iQilxaethnylnWvane2,4-Oictiltropbenol1,2,4-TrichltrobenzewNaphthalene4-Q\ltrojniHneHeiachlorDbutuliene4-Oil iro-3-tethyl phenol2-fHhyluphthileneHex achl arxvd Gpait idi ere2,4,6-TrichIorophenol2,4,5-Tnchlartphenol2-Qilirauphthalenc2-NitroanihneDivthyl phthaUteAcenapthylene3-ttitr owi lint
ugkg
740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U74011740 U740 U3700 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U3700 I)740 U3700 Q740 U740 U3700 U
Sep. Funnel E x t r a c t i o n : YE5 'Contin, Liq.-Liq. E x t . : YES
CAS to:
83-32-951-28-5100-02-7132-44121-14-2404-20-284-64-27005-72-3Bfr-73-7IKHH-6534-52-1-86-30-6101-55-3118-74-187-84-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-fl ~193-39-553-70-3191-24-2
Aanaphthene2,4-Oinitn?nenol4HtitroQh8wlDibenzofu-an2,4-fcnitrotoluoc2,4HhnitrotolueneKethyl pttthalati4-QUQn^hBiyl-phenvl etherFluor ene4-tttroanihnc4,4-Oinitro-2-h>thylph«olM-nitnsodipnenylauni (1)4- DroiDphenvl-phenYl etherHaadYlontenzenePent icn 1 x opnenolRtenantn ••fcithracK*Di-n-butvl fnttulateFlutrwtheofPyrmeButyl-bwzyl-phthilate3,3'-&ichlini«zidif«Benioiil anthracenebii-(2-Ethylhnyl)phthaiat«ChrysewIh-n-octyl pnthilateBenzotbtnurantheneBenzodclfluranthene
'Bemo(i)pyreneIndBnd^ -oiipyrBCIKbenio(a,h)aflthracencBenzolghilperylene
bjrt (c i rc l e one)(tify ( c i r c le onei
*to
760 U3700 U3700 U740 U740 U740 U760 U760 U760 U3706 U3700 U74011760 U740 U3700 U760 U740 U710 J740 U740 U760 U1500 U7 4 0 U ,
r-<srr"/THTTj760 U760 U760 U760 U - —— -740 U740 U740 U
(D-Cannot be separated 4roe diphenylaaine
FQRtt 1
Cat* No
Concentration: tow Medium
Date Extracted'Prepared:
Date Analyted
Conc/Oti Factor
Organic* Analysis Data Sfxwst(Page 3)
Pestictde/PCBs(GrcfeOne) GPCCleanup CSYes QNo
Separatory Punnef Extraction OYes
7""/~*£*7 r<wiiif
r* {fi*r*mi«1] ) S x =>
CASNumb*r
319-84-6
3)9-85-7319-86-8
58-89-976-44-6309-00-21024-57-3959-98-*60-57-172-55-972-20-833213-S5-972-S4-81031-07-fl50-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53469-21-912672-29-611O97-69-1
11O96-82-5
Alpfu-BHC
8eta-BHCO«Ua-8HCGamnu-BHC {(.tndane)
HeptachiorAldnn
««ptacnkx Epo»«ieEndoiurtan 1Dtetdrin
4. 4*-ODE
Endrin
EndosuMan U
4. 4--ODD
EndosuHan Svtf ate4. 4'-ODT ^
Mett>OK>chlor
Endrin (CeioneChlordaneTo«Jptxn«
Arocfor-1016
A/octor-1221Aroclor-1232Aroclof-1242A/ odor. 1248AfOC tor -1254
Afoctof-1260
luous Liquid - LJ
s — \ug/lorf»9/Ko,
(CirefirOnel
/4. 0 UL1^.0 tlIL.O «.
-- /A^o WJ-fc,o a?to a.
/4-O «
/4-<3 t<.^^^ W.j 3,O U.
rz*o a' ^3^3 «
Jp,O t(ja-o t<
" £2-0 U' ILO.£> U.
33.0 U
f(r£>.O U.
33G.& H
]t>O.C> Ullo.a Kf£6~Q U/u>.& u/&6.O U.j^d.^ a32&.O U.
-o
orW.
= Volume o( extraa (u()
V = Volume of water extracted (ml)
t = We*ghl at (gl
V. * Volume o4 total extract (ull
3..0-JL
7/85
flrqanics Analysis Data Sheet(Page 1) !--
Saaole Nuiber: EL
Laboratory Na,»e:Lab Saaple ID No:Si-pie flatrixi
ENVIRQDYNE87003036SOIL
Data Release Authorized B y : _ ( y _
Case No: 7351QC Report No:Contract No:Date Saaple Received: __^L"i>.i*
Volatile Compounds
Concentration; LOWDate Extracted/Prepared:Date Analyzed: i-24-87Conc/Dil Factor: 5Percent Moisture (not decanted 14.0
-o
OS to: CASfc: ugkg
74-97-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-27-4
• .ali« ar-
Oil (methaneBrmethaneVinyl ChlorideQtloroethaneHethylene QtlorideAcetateCarbon Dial fide1,1-Didtloraetbene1,1-DichlDroethanetrara-U2-Dichl QroetheneQUcrotori1,2-OichIcrorth.fle2-Butanone1,1,1-Trichlcraeth.r*Carbon TetradilxideVinyl AcetateBrotodi ch 1 or Methane
•at* «
•at.- tH— ar •«M| t. tta *
SBU5BUSBUSBU940.170 6
29U29U29U29U29U29USBU29U27USBU29 U
•
Ci
MKttan Tdla Maa apal
71H7-510061-02-679-OK124-48-179-00-571-43-210061-01-5110-75-875-25-2108-10-1591-78-6-IZ7-1M79-34-5lOB-eB-3108-90-710CH1-4100-42-5
11 a. t« .Mtt
l,2-DidilarDpra(wn»trans-1 ,3-DichlmjpnB«TrithloriethentDibmachlanaeth.Y»l,l,2-Trichloroeth»eBeweneci s-1 , 3-&i chl tropropene2-Chl xoethy! vi nyl etherBrnotor*4-tethyl-2-pentanone2-HeivnncTftrachloroethme1,1,2,2-Tetr.dilxotth.MTolueneDilarobenzmEthvlbenznStyreneToUl lylenes
.1*. ^ara»t*-« rtwa U- 1—— rt
29U29U29U29U29 U2?U29U5BU29U5BLJSB U29U79 LitTT29U29U29U29U
me.-
*«/ttl In
anAly*** 1m- but
^ UMt *«r Uw ••••IB ^t* W*W U (•v.
T "MUrMur •cxlan. «TtH« !• «•»
^•cttan UXt.> TIM *••*•••• •Maul* r»a*t V-
nvrt f«r (kwt "•* MMa tM. Tfw «!»••• !• Uv
THta «laaj !• i ari aitfiar
41 •• !•
1*. It l««l
tit* «•*•
tn«tcatart Ww pi ••anea *f * BVBPHV^ Uwt •••*• Uw loanctf t«««lan
art tar I a kwt UM r««»it IB !•«• tlun t>» •aaclfl«« aMartlan Halt
t»an «ar* (•«. IB4) . 14 lta*t •< Mt*«lan »• 10 layl MM
Laboratory Naie:Case No: 7351
ENVIRQDYNE Saaole Number: EL
Organic* Analysis Data Sheet(Page 2)
Concentration: LQNDateDateConc/DilPercent
Senivolatile Compounds
GPC Cleanup : YE5x t r a c t e d /P repa red : 6-19-B7n a l y z e d : 7-1-87il Factor : 1t Moisture (decanted): 14
CAS to:
106- 2111-44-495-57-6541-73-1106-46-7100-51-695-SM95-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-186-75-5105-67-965-85-0111-91-1120-63-2120-32-191-20-3106-47-887-68-359-50-791-57-677-47-4BB-Ob-295-95-491-58-788-74-4131-11-3208 •% fl99-09-2
uqkg
Phenolbis-{2-Chlxaethynether2-Chloraphenat1,3-Dichlxabenzml,4-Did)lxobenzen*tenzyl AlatolIf2-0ichlarab«nzcne2-tethyl phenolbis-(2-Qilaroiwpropyl)pther4-ttthylphenalH-ni trosiH>i -n-prqiy 1 au ncHnachlxcethanenitrobenzenelupnxone2-*trophenol2,4-DiwthylphrolBvuoic Acidbi s- (Oil xoethcB ytttethane2,4-Oichlorcphenol1,2,4-Trichlarabenzenttaphthilene4-QilanuniIineHRachlorabutuJiene4-Qilxcr3-«thvl phenol2-teUiyl naphthaleneHexachlxacyclcpentadiene2,4,6-Trichlorophenol2,4,5-Trictilcrnphenol2-Chlxanaphthalene2-Nitroanihne&i«ethyl phthalateAcHuothylene3-th troaru line
770770770770770770770770770770770770770770770770
UUUUUUUUUUUUUUUU
3700 U770770770770770770770770770770
UUUUUUUUUU
3700 U770 U3700 U770770
UU
Sep. Funnel E x t r a c t i o n : YESC^Mc iContin. Liq.-Liq. Ex t . : YEa QNQJ(c i
CAS to:
83-32-951-28-5100-02-7132-64^121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-L-86-30-6101-55-3118-74-187-86-585-01-fi120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-91-7218-OH117-84-0205-99-2207-W-950-32-8193-39-553-70-3191-24-2
Acenaphthene2,4-ttnitrcpnenQl4-tttraptanolDibenzottran2,4-Oinitrotoluene2,6-Oinitrotoluenefo ethyl phthalaie4-Oiloraphenyl-phenyl etherRucren*4-tatroafulint4,6-Wnitro-HlrthylptawlK-nitraodipnenylaune (1)4-Brcnophenyl-?henyl rtherffaachloTQbenzenePentidilrophmolPhBunthrenetetbraceneDi-rrbutyl phthalateFluor anthenePyreneButyl -beicyl-phthaUte3,3'-DichlxcBfn2idineBen:o(i)»thrKem [bi»-(2-Ethyl^a¥l)phthalateChryseneDi-n-octyl phthaliteBeuotblfluirartfwoeBenza(k)flicrantheneBwzoUJpyrmf •Indenotl,2.3-ol)pyrweDiberuo(t,h)inthruen«Benzo(qtu)perylene
ugkg
770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700U770 U770 U770U3700 U770 U770 U
UflOuJD J "
WJUJ1500 U.~ —— -^juH550 «•
_770_y.[tfl'j^sT)[69 J_PQ(J"62Jl1 65 J_l
770 U3700 U
( c i r c l e one)e one;
(l)-Cannot be separated from d i p h e n y l A m i n e
FORM 1
No
Organic* Anarysis Data Sheet3)
Concentration: (j-&**) Medium
Date Extracted 'Prepared: ____x2
Date Analyzed: ______/"'
P«st*c*de/PCBs
(Circle One|
X)moGPC Cleanup BYes ONo
Separatory Funnel Extraction O res ~' ^S•—*
Continuous Uqukt * Liquid Extraction Oresco
Cone/Oil Factor:
Percent Moisture (decanted)
CASNu«nt>«r
orW.
V = Volume o/ ertract infected (u<)
V - Volume o( wate« extracted (ml)
W = Weigh! of cample extracted (Q|
V( * Volume of total ««*raa <ul|
3C'«
CO
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-t72-S5-91
72-20-833213-65-972-54-81031-07-8SO-29-372-43-5534 94-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1
11096-82-5
Alptu-8HC
Be»-BHCDelia-BHCG*fT»ma-BHC (LmdanelHep(act>lorAWr-o
HeptactUor Epox*deEndosutfan (D4efdrin4. 4--OOECnoVtnEnoosutfan 04. 4'-OOOEndosutfan Sutfat«4.4'-ODT v
Metttocychlor
Endfin Keton*ChlordaneTouptteneAroctof-1016Aroctof-1221Ar octof- 1232ArodOf-1242
A/oc*<x-1248A/octor-1254
Arocto*-1260
!(*.& W/t.o nit.o a
., l*>*o utt'O a.lk,o U.
it»o utL.O K-S^'tt.33.0 tt
~3t>& UL* .-3QO «
'SJ.O K33*O t<
p 7£, o «, IL<>.£> U_
ji.O Utl*&O U330.0 U.1t>6.0 Utto.O UKr&.Q U
ILQ.O U/&6.O «.320.Q U3*O.O U.
7/85
Qrganics Analysis Data Sheet(Page 1) ! —
Saaple Nuaber: EH
Laboratory Naie:Lab Saaple ID No:Saiple Matrix:
ENVIRQDYNE87003037SOIL
Data Release Authorized By:
Case No: 7351QC Report No:Contract No:Date Saaple Received: ._U-'_J_' _-_
O
Volati1e Compounds
Concentration: LOUDate Extracted/Prepared:Date Analyzed: 6-24-B7Conc/Dil Factor: 1Percent Moisture (not decanted 12.9
c/im-o
CASte: iqkg uqkq
74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-315WO-567-66-3107-06-27S-93-371-55-f.56-23-510fr05-475-27-4
Oiler Diet hamfirowtluniVinyl QilcrideDilxoethancNtthylnw QiloridtAcEtoneCarbon Disulfide1,1-Diddaroetheie1,1-Dichlarorttunetrans-l,2-0ichlxoethawChlorafori1,2-Oidilaraethdne2-fiutanoncI,l,l-Trichlirt3eth«Carton TitradiliridiVinyl AceUteBrtModichltroiethaM
11 U11 U11 U11 U
f73&OJ
6 U6 U6 U6 U6 U6 U11 U6 U6 U11 U6 U
7B-87-510061-02-679-01-6124-48-179-00-5
^ 71-43-210061-01-5110-75-875-25-2106-10-15W-7H,127-1W79-34-510MB-3106-90-7100-41-410CH2-5
_ _
l,Hidil(rarcfinetr»s-I,3-Oichl(n$rcpeneTridilorpithwto bronchi oro«thani1,1,2-Tnchliroethan*BBUBCds-l,3-0idilarnropew2-Oilaroethyl vinyl etherBroMrfori4-fethyl-2-pntanam24fR«naneTetradUcraetheie1,1,2,2-TetrjeMflraethintTalumQilcrabenzawEthylbenznStyrm*Total lylra
6 U6 U6 U6 U6 U6U6 U11 U6 U11 U11 U6116 U6 U6 U6 U6 U6 U
Ci
Tftt
lly
minimi- »ttAl(u*l« ••••cttvt Halt *«r tiw t* m*~rlr «Wi'
Thla *!•« 1* IM«« Mtmr
t*» •-mat I* !••• UMH UM BpacKlM *M*ctlvi llBtt tort
Labo ra to ry Naae:Case No: 7351
ENVIRODYNE Staple Nu«ber: En 851
Qrganics Analysis Data Sheet(Page 2)
70nn
mo
S**ivolatiIB Compounds
Concentration: LOWDate Extracted/Prepared: 6-19-87Date Analyzed: 7-1-87Cone/Di 1 Factor: 1Percent Moisture (decanted)
CftSto:
12.9
uqkg
lOfr-95-2111-44-495-57-8541-73-1106-46-7100-5H95-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-39-186-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-48B-06-295-95-491-5B-7BB-74-4131-11-3208-96-a99-09-2
Phenolbis- 12-Qil cn-ethy 1 ) eUw2-Qilcraphenoll,3-Dichl(roberuenett4-Didilxoben2eneBsuyl Alatall -Oichlontenzene2-tethylphenolbi5-(2-Qilcroi5Cpro()yl)ether4-Heti.ylphmalIHH troso-Di -n-propyl aaincte^hlmiethwtbtrobeniBttIs hxcne2-Wtrophenol2,4-OiKthylpnmlBenzine Acidbis-taitroethcByltethtf*2,4-Di-nitrDp.wnol1,2, 4-Tr i dU cnteu meH thilene4-0.1 Toani lineHexadtlorcbutadiene4-Qil aro-3-iethYl phenol2-ftothylnaphtlulenehaxMTxyclqcntadiene2,4,Hrichlorophenol2,4,Hhdiltnphenol2-Oil croup fit hilew2~(titroa(ulineDivthyl (rtittulateAcaupthylene3-totroanihne
760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760U760 U760 U760 U760 U760 U760 U760 U3700 U
- 760 U3700 U760 U760 U3700 U
i. Funnel E x t r a c t i o n : YES (itin. Liq.-Liq. Ext. : YES <
CASfc:
83-32-951-.B-5100-02-7132-64-9121-14-2606-20-2B4H6-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-46-585-01-8120-12-784-74-2206-44-0129-00-0BtB-791-94-156-55-3117-81-7218-01-9117-64-0205-99-2207-OM50-32-8193-39-55J-70-3191-24-2
Acenapbtbene2,4-Oi[\itn$h6nol4-NitrqtenolDibenottran2,4-OiiitrotDluen*2,6-OinitratoliMneDl ethyl phtbalate4-O.lQnvhaiyI-pnB.yl etha-Fluorene4-tetnaniline4,fr-Oi.itro-2-*thylph«nolH-rutnsodiphBiylaBine (1)4-8roiQphenyl-pnBiyI ethertaachlcr*wuff»rwtaoUoroqhwolrheiUllUff H*
AnthraoneW-n-twtyl phttolrti (FluorMthentPyreneButyl-benzyl-phthalate^S'-DidUT-benzidineBenioiAJ anthracenebi«-(2-€thyltwyl)phthalaUQvyvneDi-n-xtyl phthalateBvzolbHluorwttieReBenzotb luoranthflwSBiioiaJjryrme _ _ _ _ _Ind_.no(l,2l3-alJpyrer.e_Kbe«2o.a,h)..flttYacene8enzQ.ghi)pe-ylent
J§ (ciJ5> (ci
760 U3700 U3700 U760 U760 U760 U760 U760 U7601}3700 U3700 U760 U760 U760 U3700 U760 U
^ZKU"O
^-^aou760 U760 U1500 U760 U3706*760 U760 U760 U760 U760 U760 U760 U760 U
-o
(circle one-)-1
PTC
ID-Cannot he separated fro« diphenylaaine
FORM 1
U«txxaiofy
No
Concentration: ( Low) Medium
Date Extracted 'Prepared:Date Analyzed: ______
Organics Analysis Data Shoot(Page 3)
Postic»de/PC8s(Circle One) GPC Cleanup
___ SeparatofY Funnel Extraction QYes
___ Continuous Liquid - Liquid Extraction QYcs
Cone/Oil Factor:
Perceni Mo*store (decanted), 12-?CAS ug/l O'W'K^Numbar m CCircffTTrwl
319-84-6319-85-7
319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-55-972-54-81031-07-850-29-372-43-553494-70-557-74-98O01-35-212674-11-211104.28-211141-16-553*69-21-912672-29-611097-69-111096-82-5
Aipha-BHCB«tJ-BHCDelta -8HCGamm*-BHC (Li<xJanel
HcptachlorAldr.n
Heo»crWor £pox«JeEndosulfan IOieldrin4. 4--OOE£n&inEndosuHan tt
4. 4--OOOEndosutfao Surfate4. 4'-ODT
Mettx>KVCMor
Gndfin KcioneChtcxTJar**ToupheneArockK-1O16A/oct<x-l22lA/octof-1232ArocI<X-1242
A/ockK-1248Aroc(<X-l2S4
Aroc*o*-l26O
if+.o a./t . 0 tttC.O (L
- .16.0 W/4,» Uf fcxO U.
/t>.o u/£>.£>• K
,l2.J> U.33.0 «.^z-c? a.
' .^&-o *iVP.O «^3^3 «
" ^i-<? «f- /<-<>.£> U.
J .O «/(^X^J W
JU .«O U)l>0.& Ult£>.0 U£6.6 UIWjQ U/6AO U.3.3<>,0 ^3 . 5 6C
orW.
V^ = Vofum« of extract infecred (ul|
V = Vo4um« o< watef extracted (ml)
W = Weight of t*onp<« extracted (gl
V( * Vofume o< total ear»a (uf|
7/8S
Organics Analysis Data Sheet(Page 1)
Saiple Number: EM 852
Laboratory Nane: ENVIRODYNELab Saaple ID No: 87003038Saaple Matrix: SOILData Release Authorized By: _{Y\
Case No: 7351OC Report NoiContract No: __la 3.-Date Sample Received
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-87Conc/Dil Factor: 1Percent Moisture (not decanted 12.8
CftSlta CflSMo: uqkg
74-67-374-63-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-S-656-23-5108-05-475-27-4
Oil or MethaneBraoeethaneVinyl ChloribtChloraethantHrthylene ChloridefcEtontCarbon DisuHide1,1-Didiloroethenel,HKchlcroethinetrans-1 ,2-ihchlorDethweCbloroforil,2-Didu(roethanB2-Gutamm1,1,1-TridUxoethaneCartxii TetrachlxidcVinyl AcetattBro«odidil or Methane
11 U11 U11 U11 U56 B45 940
6 U6 U6 U6 U6 U6 U11 U6116 U11 U6 U
78-67-510061-02-67W1-6124-48-179-00-5
r 71-43-210061-01-5110-75-fl75-25-2106-10-1591-78-61Z7-1B-4'79-34-51C6-9B-310*40-7100-41-4100-42-5
1,2-Mcraprcw*trans-1 ,3-ttchlcraprapmeTrichlaroetherwvibrtMQchl trapthanel,l,Mncfiloro«hir*Bnzcnedi-l,3-DidilorD9rafiBir2-Qiloroethylnnyletherft-oiDtori4-ftethyl-2-p«tjnonE2-teanmTetrachluoettenel,l,2,HrtradilxwthiMTolueneQilorobenzentEthylbeuowStyrmeTotal lylenes
6 U6 U6 U6 U6 U6U6 U11 U6 U11 U11 U6 U6 U6U6 U6 U6 U6 U
If Ut*
llatt. •tn«lB
n«/ul in ttw ftn«] H tract
ltvrl* kvt UM rnult !• !••• Utwi th» ••vclft** **t«tl«n ttMt
!•*. IOJ1. If lt«4t •« rivfcaMlan !• 1O u»l
Laboratory Name:Case N=: 7351
ENVIRQDYNE Simple Number: EM 852
Organics Analysis Data Sheet(Page 2)
Concentrat ion: LOWDateDateConc/DilPercen t
Seaivolati le Compounds
BPC Cleanup : YESx t rac ted / Prepared: 6- 19-87naly ied: 7-1-B7il Factor: 1t M o i s t u r e ( d e c a n t e d ) : 12.
CftS to:
106-95-2111-44-495-57-fl541-73-1106-44-7100-5K95-50-195SB-739638-32-910M4-5621-64-767-72-198 75-378-59-1BB-75-5105-67-965-85-0111-91-1120-93-2120-fl2-l91-20-3106-47-8B7-6B-359-50-791-57-677-47-488-06-295-95-491-58-78B-74-4131-11-3208 96 699-09-2
Phenolbii-{2-Oilxoethyl) ether2-Qiltrcohenol1,3-OichlcrabenzH*1,4-DichlorQbenzB*Bmzyl Ma*nl1,2-OichloroBenzene2-fethylphenolbis-(2-£hlxoisaprapyUether4-tethylphenolM-nitrosD-ft-n-propylaiiwHex*hlxTKth«nitrobenzeneIscphcnne2-tttmohenol2,4-foMthylphenolBemoic Acidbi s- (Olcroethcay) teth«2,4-OichlxDphenol1,2,4-TrichlorcteueneNaphthalene4-QilxoanilineHnachlxobutadiene4-CW xo-3-«thy 1 phenol2-Hethylniphthaiewteachl crocycl opentadi me2,4,6-TnchlcrDphenDl2,4,5-Trichlxcphenol2-Qilorauphthiiene2-*btraanilineDiwthyl phtKiJiteAcmapthylene3-Hitrwfiiline
! = = = = = = = = = :
,6
uqkg
760 U760 U760 U760 tl760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U3700 U760 U760 U3700 U
Sep. Funnel E x t r a c t i o n : Y E S <Cont in . Liq.- l iq. E x t . : YES
CKto
83-3251-28-5100-02-7132-M ?121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6 ,101-55-3118-74-1B7-&-5GE-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-721H»H117-84205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaptithene2,4HhnitropMral4-tttrcpherolDibcnzotran2,4-ttnitrotoliete2l6HhnitrotniuBKDiethyl pbthalate4-OilcTQp6enyl-phenyl etherFluor ene4-*btnuniUne4,6-Oinitro-2HWhyl[>henolN-nitrtHoiipnenYlaiine (1)4-BroMpNenyl-phenyl ttherteach IxotwupwPentachl xtjjhenclPhBunthnneAnthraceneOi-ft-butyl phthalatiFlutranthene"PyrsieButyl -benzyl -phthil ate3 ,3 ' -to chl onaenz i dinefenio(i}»thrttenebi5-(2-Elhylhoyl)phth4ljti!ChryuneDi-n-octyl pnthalittBenzotblflucrartheneBenzotkJUurantheneBenioiupyrtnelndBXi(l,2,3-ai)pyrneIKbenzDU^h) anthraceneBaizQtghiipe^lenc
^NQj)<ci
uqkq
760 U3700 U3700 U7601)760 U7UU760 U760 U760 U3700113700 U760 U760 U760 u37001)760 Uliflu
dS^760 U760 U760 U1500 U760 U410 «760 U760 U760 U7601)760 U760 U760 U760 U
one)
( l ) - C a n n o t be separated iron d iphenylas ine
FORM 1
C»s< No
Concentration: tow Medium
Date Extracted 'Prepared:
Date Analyzed: ______
Organtes Analysis Data Sheet(Page 3)
Peiticid«/PCBs
(Crete One) GPC Cleanup Ores QNo
___ Separatory Funnel extraction
___ Continuous Liquid - Liquid Extraction QYes
nG-"2.
Cone /Oil Factor: 1Percent Moisture (decanted) II-
GAS ug/forfcjg/K^.Number „ (CJrcMTUne)
319-84-6319-85-7319-86-858-89-976-44^309-00-21024-57-3959-98-860- 57- 172-55-972-20-833213-65-972-54-81031-07-S50-29-372-43-553494-70-557-74-98O01-3S-212674-11-211104-26-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Alph*-8HCBeia-BHCO«fu-BHCGamma-BHC (Lindarvel
HeptachiofAkJnn
Hep»c*kx Epox*deEndosutfan IOteWrin4. 4--OOEEndrinEndosutfan fl4. 4'-OOO
Endosotfan SuHate4. 4--DDT ^
Mettioxvchlor
Endrin KetooeChtortfaneTos*pf»eoeAroc(or-1016
A/ocVx-1221Aroctof-1232A/oclof-1242
A/oc*or-1248
AroCior-1254
Aroc*o»-1260
/6. o a/ f r .O fi
K.O a.- yt^o «
/Ax(7 af^Olt
/4.0 «
/i. ) a.ry^t»~u.x>.o U.32x0- a
' .j33^> t^>p.o U.XXO «
r ^2,c? «- /<-£>.£> U.
JAO «
/CA^> yJUd. > U)t>O.O UI6.0.O UK6.6 UILC.O UIL6.0 U.320.0 a3*0.0 &
orW.
V. = Volume at extract infected (u(|
V = Volume o( wJter extracted (mt)
W - We*gt« ot c«mp4e extracted (g(
V * Volume at total extract <vt|
30
7/85
Qrganics Analysis Data Sheet(Page 1)
Staple Number: En 953
Laboratory Na«e: ENVIRQDYNELab Saaple ID No: B7003039Saaple Matrix: SOILData Release Authorized By:
Case No: 7351QC Report No:Contract No:Date Sample Received
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-87Conc/Dil Factor: 1Percent Moisture (not decanted)
ofr^fTcon
13.7
CASHo: unkg CAS to: uofcg
74-S7-374-83-975-OH75-00-375-09-267-AH75-15-075-35H75-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-27-4
ChlorotethaneBroeoiethaneVinyl ChlorideOilonvthtfcHethylen* ChlorideAcetoneCarbon Bisulfide1,1-Qichloroethene1,1-Dichlxcethanetrans-t ,2-DichloroetheneChlxofori1,2-OichlorotthaneHut-none1,1,1-TrictilcrorthaneCarbon TetrachlcnbeVinyl fcttatiBroKXJichlxDKthane
•
12 U12 U12 U12 U
_ *T
6 U6 U6 U6 U6 U6U12 U6 U6 U12 U6 U
7M7-510061-02-679-OK124-4&-179-00-5
** 71-43-210061-01-5110-75-875-25-2108-10-1591-7W127-1B-4'79-34-51QB-B-3108-90-710MHKXM2-5
1, Hhdil or opr opinetrans-1 ,3-OichlxGprapeneTrichlxoetheneDibronctil oravUune1,1,2-TrichloroethaneBenzenecis-1 ,3-ftchloropropene2-Chl orcethyl vi nyl etherBroiotxi4-Hrthyl-2-pwtanane2-teirtneTetrachloraetnavl,l,2,Hetr*ddorDeth*ntTaltaneDilarabeiKtneOhylbaueneStyrewToUl lylenes
6 U6 U6 U6 U6 Utu6 U12 U6 U12 U12 U6116 U6 U6 U6U6 U6 U
•V/ul in th* MM! ••wact
CM* LMts-wit *j*«BettM( ll*4t.) TH* Imatna*.
Mf»l*>a *tt«lM^l* **«*c«i*>i tt«*t f*r Ut*
it
lB*tCB*«* •> *BtlMt*« VKlu^ TK1* <!•« t*
•rtt*r-i* but t*- r• ault i* 1*** tkwi tit* *v*ct41** *vt*e«lwt n*it kwt
•r-^rtv t»t«t !•>-• (•*. 1OJ). K UMt •* **t*ctl*n i* 1O u*J *n* •
i*n«*mrati pi. •« i •*,! i* ckic*a«tB*. i *'t •• U.
«. tt In«t
tit* *at« taar t*
Laboratory Na•e:Case No: 7351
ENVIRQDYNE ! Saaple Nuaber: EM 853
Organic* Analysis Data Sheet(Page 2)
Seal volatile Compounds
Ornmarn
C o n c e n t r a t i o n : M E D I U MD a t e E x t r a c t e d / P r e p a r e d : 6-26-87Date A n a l y z e d : 7-2-87C o n c / D i l Fac tor : 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 13.7
OS to:
106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85H)Ul-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295 75-491-58-7BB-74-4131-11-3208-96-899-09-2
Phenolbis-(2-Qil(rtBthyl>tther2-Chlorophenol1,3-OidiltrdMizHie1,4-ftchlirQbenztneBenzyl Motel1,2-Oichlorobenzenf2-fethylphenoll>is-(2-Qilaraisopro()yl)ether4-fethylpneralIhii tr oso-Di -n-propy lua MteaoMtraethaneNitrobenzeneI9?harone2-fctrophenol2,4-Die*thylphenalBenzole AcidbiHOUoroethatylhethane2,4-DichlTophenol1,2,4-TnchlirobenzeneNaphthalene4-(WoraaniliiwHniachl orcbutuf i cne4-Q>ltro-3-e«thyiphHwl2-Hethyl naphthaleneto achl trocycl cpentadi me2,4,6-Trichlxophenol2,4,5-Trichlo-n)Nenol2-ChloriiJaphthilin*2-MitnunilineDivthvl phthilateAcaupthyle^e3-MitrDaniliiw
SPC C l e a n u p : NO -^Sep. F u n n e l E x t r a c t i o n : Y E S C j S t c i rC o n t i n . L i q . - L i q . E x t . : YES (W\ i c i r
-
23000 U2300. U23000 U23000 U23000 U23000 U23000 J23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U110000 U23000 LJ23000U23000 U23000 U23000 U23000 U23000 U23000 U23000 UZ3000LJ110000 U23000 U110000 U23000 U23000 U110000 U
CASfe:
B3-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-3B6-73-7100-01-6534-52-1 ~86-30-t101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-69-791*94-156-55-3117-81-721S-01-9117-84-0205-99-2207-06-950-32-8 -193-39-553-70-3191-24-2
Actnaptithene2,4-OinitrqitaQl4-ntrop&enolDibenztrfifao2,4-OinitrDtoluene2,6-OinitrotolueneDivUiyl pfcthilite4-Chl(rq>nflnyl-pnenyl etherFluortM4-fctnunihne4,6-{hnitrD-2-fkthyIphenolIhiitrosodiphenylatine (1)4 Droiophenyl-phenyl rtherHkachlxcbenzenePwtathlorophtnolrnenanthmAnthraceneIh-rrbutyl phthilat*RucraRtheMPyreneftttyl-faeftzyl-phthalite3 ,3 ' -Oi chl ontetz idineBenzofalanthricencbii-(2-Ethyl hexyl) phthal ateQtryseneDi-n-ortyl phthal at*Berno (b H 1 uor utheneBcnzoOclflnranthflntBBuo(a)pyreMInderad ,2,3-dt)pyreneHi benzo(a,h) anthraceneBenzat^iilperylene
•akg
23000 U110000 U110000 U23000 U23000U23000 U23COOU23000U23000U110000 Unoooou23000 LJ23000 U23000 U110000 U23000 LJ23000 U23000 U23000 U23000U23000U46000U23000U23000U23000U23000023000 U23000U23000 U23000 LJ23000U23000 U
circle one)
(U-Cannot be separated froi diphenyl aaine
FORM 1
Laboratory Name £rtt/>rv»
Case No
Concentration Low
Date Extracted 'Prepared-
Date Analyred —————— 7--7-T7
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs
(Circle One) GPC Oeanup QYes
_ Separatory Funnel Eirtraction QYes
_ Continuous Uqutd - Liquid Extraction QYes
QN
Cone /Oil Factor-
Percent Moisiure (decanted)
CASNumber
319-84-6319-85-7319-86-8
58-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-9U672-29-611O97-69-111O96-82-5
Alpha- BHC
Beia-BHCOelta-BHCGamma-BHC (Lrodane)HeptactilorAkJrm
Hepiachlor EpoxtdeEtvtoiuHan 10»e*drin4. 4--OOEErxlrmEodosuHan 114. 4'-DOOEndosulfan Sulfate
4.4--DDT
M*thoryctitof
Endrtn tCetone
ChlordaneToKjpheneArocJo<--1016
Aroclof-1221
Aroclof-1232Afoclor-1242
AfOC(eH-V248
Aroclof-1254
Arocloc-126O
iz&, o ajzo. o aIZQ,O \LIK> Wno • uv<? iL_}*O.Q UiI2A.O. U
W0 U.mo.o a.*ye a
*Jiqo.Q Uwo.o uaqo.Q (1-24n U
'13.00,0 U3<JO,0 U
IZoo.O QMGOtO (1
/P<X>,^ tJLIAOO.O U\300tO UI3GO.O U\200.0 Uaqoo.O U.j?V^>-O R
orW.
V. * Volume of extract (ut)
V = Volume of water extracted (ml)
W = Weight oA sample extracted (gl
V * Volume of total extract (ut)
Form 1 7/85
Organics Analysis Data Sheet(Page 1)
Sample Nu«ber: EM 354
Laboratory Na»e:Lab Saiple ID No:Saaple Matrix:
ENVIRQDYNE87003040SOIL
Data Release Authorized By:
Case No: 7351QC Report No: JContract No:Date S*«ple Received: .Jfl-
Volatile Compounds
Concentration: LQWDate Extracted/Prepared:Date Analyzed: 6-24-B7Conc/Dil Factor: 1Percent Hoisture (not decanted) 13.6
CASMo:
74-87-374-S3-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-Z7-4
Oil or methaneBronAhaneVinyl Oil videDUtroethanehVthylene Oil TideAcetoneCarbon Disulfidel,HKchl(Toethenel,HHchlxoethafletrarn-1 ,2-OichlxoetheneQilorofori1,2-Dichl methane2-But2none1,1,1-TrichlxoethantCarbon TrtrachlxideVinyl AcetateBr OKXJ i di 1 or owthanc
- -
"9*9
12 U12 U12U12 U31BHT60 B ur
6 U P T C
6 Uf c U6 U6 U6 U12 U6 U61112 Ui U
CASNo:
78-B7-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-fl75-25-2108-10-1591-78-6'127-19-479-34-5109-8B-3108 0-7100-41-4100-42-5
1,2-Dichloropropanetr aw - 1 , 3-Oi chl oropr openeThchlofoetnewDi brtBDchl xtarthane1,1,2-TndilxDrthanefimzowcii-l,3-DidiloropropBie2-Qil xorthyl vi nyl etherBroBfxi4-ftethy 1 ~2~pHitanone
TetradUxoethene1,1^2-TetradilxDethaneTO!UB«ChlxotwnzBwEthylbenzemStyreneTotal lylenes
uqiq
6 U6 U6 U6 U6 U6 U6 U12 U6 U12 U iotl6 U6 U4 U6 U6 U6 U6 U
yivtf «w tart no*
Tkl« *!•« •**!(•• t*
Uwi ••• cw*«lr«« kv K/W. Mn«l
BtMr
Laboratory Na«e:Case No: 7351
ENVIRQDYNE Saaple Nunber; EN 854 •£Organic* Analysis Data Sheet-
(Page 2)
Se»ivolatile Compounds
Concentration: LOWDate Extracted/Prepared: 6-19-B7Date Analyzed: 7-2-87Conc/Di 1 Factor: 1Dercent Moisture (decanted) 13. a
CASto:
106 5-2111-44-495-57-fi541-73-1106-46-7100-51-695-50-195-48-73963B-32-*106-44-5621-64-747-72-198 5-378-59-iBB-75-5105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-fl87-68-359-50-791-57-677-47-4BB-06-295-95-491-5B-7BB-74-4131-11-3208 96 699-09-2
Phenolhii-(2-ChlrQethyl}etha-2-aioroph«nol1,3-DichltrcbenzHw1,4-OichlarQbenzeneBmzyl Alcatel1,2-Oidilarctenzene2-hethylpnmilbis-(2-Qilxoisoprcpyl)pther4-ftpthYlpnendK-ni tr oso-fli -n-propyl ui neHecachlcrarthaneUtrriwniHWIsophcniv2Hktr (phenol2,4-DivthylphaulBenzoic Acidbi i- ( Qi 1 (Ttethm y ) Hethane2,4Hhchlxcpfiefiol1 , 2, 4-Tri chl mtem entNaphtha! etw4-ChlaroanilineHBachlorobututiene4-CM tnrS-nthvl phewl2-ftet h y 1 naphth il en BHD ach 1 orocycl opsi t ad i ene2,4,6-TrichIorophenol2,4,5-Tnchlxophenol2-ChloronaphtbaleRe2-fatrwnihneDivthyl phthalateAcenapthylene3-Witrtwiilin*
766 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 UPOOU
" 760 UPOOU760 U760 UPOOU
. F u n n e l E x t r a c t i o n : YES CjiO) < c i r c 1 e o n e )t i n . L i q . - L i q . E x t . : Y E S ( R u ) ( c i r c l e o n e )
CAS No: uqkg
83-32-951-29-5100-02-7132-64-9UH4-2606-20-2B4-66-27005-72-386-73-7100-01-6534-52-1 -86-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-*117-84-0205-49-2207-08-450-32-8193-39-553-70-3191-24-2
Acenaphthene 760 U2,4-Oirutrqjrienol POO U4-tbtrophinol POO UDibenzoriran 760 U2,4-OinitrBtolune 760 U2,6-{hnitrotfllua» 1*& t'iKethyl phthalate f» J4-OUoTcpnoiyl-jwnYl etna- 760 URurene 760 U4-tttroaniliM 3700 U4,6-Oiaitrcr2-tkthylphBiol 3700 UIHutroMtiptarylaiing U) 760 U4-flroMptwnyl-piwyl ether 760 U
Pwtachlorcphwol POO U
Anthracene 760 UKirbutyl phthalatB OSr*Fluoranthew 64 Jfy«ne 69 JftrtyHwnzvl-phtlnlitf T5"'j313'-DichlcrabeniidiK 1500 UBer:oii)intfiracm* 760 Ubis-(2-€lhylhnvlifihtnaliti 390 >&" MX pj eDrysew 760 UDi-n-actyl ohthilaU 760 UBenzoibHluorantJww 57 J IBmzo(kmucrantra« 760 UBenzodlpyrene 760 Ulntara(l,2,3-alJpyrem 760 UK6enzo(a,h)anthrKm 760 U
( 1)-Cannot be separated fran diphenvlanine
FORM 1
No
Organic* Analysis Data Shoot(Page 3)
Pesticido/PCBs
Concentration: ^^X Medium
fete Extracted 'Prepared:
Date Analyzed:
(Circle One) GPC Cleanup Bv'es DNo
Separatory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction QYes
Cone/Oil Factor:
Percent Moisture (decanted)
CAS wg/lofLNumb«r . (OfCfi
319-84-6319-85-7319-86-858-89-976-44 -63O9-OO-21024-57-3959-93-860-57-172-55-972-20-833213-65-972-54-81031-07-8SO-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-21H41-16-S53469-21-912672-29-6U097-69-111096-82-5
Alpha -BHCBew-BHCrXia-BHCGammj-BHC (Lindane)HepwchlorAldnnHepcacWor Epox*deEndosutfan 1O*e<drin4. 4--OOEEndrinEndosutfan fl4. 4'-OOOEndosuWan Suftate4. 4--ODT ^MethoKychtorEndrin (Celcx>eChkxdarveToupn«r*
Aroctef-1016A/oclof-1221Aroctw-1232Afoclof-1242
A,oc*x-1248Arockx-1254Aroc(or-126O
rg/Ko,-Cn^J
H~.0 UL/t.r>IL.O
/A«,
.- Ib'O U\b.v aib-o u.
lt>*O Uil.O. u(.
_ ?l*0 U.33.0 «.3i-0 a
* *33-0 «33.0 14J3WD tc.
r ~Zl,o U' / LO.£> u.
ji.o UILAO U
JU4.& U1&>O.O uI(.£>.O U
fc&.Q U/tA.Q UK.6.O U.32 0,6
3*O.Ouu.
orW.
V = Volume of eKtraci (ul)
V = Volume of waie* CKiracied (ml)
W * We«ght of camp4« exacted (g)
V. * VoftMTve o< tot*l CKiract MlI
I Offtt I 7/85
drganics Analysis Data Sheet(Page 1)
Saaple Nufiber: Eh 855
Laboratory Nane: ENVIRQDYNELab Saaple ID No: 870030415a«ple Matrix: SOILData Release Authorized By: _
Cast No: 7351QC Report Moi _/i[_Contract No: __jfii-Date Sample Received
Volatile Compounds
Concentration: LQHDate Extracted/Prepared:Date Analyzed: 6-25-87Conc/Dil Factor; 1Percent Moisture (not decanted)
-nnm<ma~V)m-Q
en
12.7
CASta: CASto:
74-67-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-371-55-656-23-5108-05-475-27-4
ChloroiethaneBrcmethaneVinyl ChlorideChloroethaneto bylaw ChlorideAcetoneCarbon Bisulfide1,1-Oichl oroethene1,1-Dichloroethinetrans-1 , 2-Di chl oroetheneQilcrofori1,2-Dichloroethane2-Manane1,1,1-TricMaroethaneCarbon TetradilorideVinyl Acetatefir otodithl or Methane
-
11 U11 U111)11 U21 B*J82 B *•*",:
6 U6 U6 U6 U6 U611n u6 U6 U11 U6 t )
7B-87-510061-02-679-01-6124-48-179-00-5
r<. 7H3-210061-01-5110-75-875-25-2108-10-1591-7&-6,127-18-479-34-5108-8B-3108-9&-7100-41-4100-42-5
1,2-Oichi or opr opinetrans- 1 , 3-Oi chlxopropeneTrichloFoetheneDi broBchl oroKthane1,1,2-TrichloroethaneBenzeneci%-l,3-Dvchlarapropene2-Chl oraethyl vi ny letherBronfcri4-»tethyl-2-pentanoneHteacrv*Tetrachlaroethene1,1,2, 2-TftracMaroethafteTolueneDilorobenzemEthyl benzeneStyreneTotal Xylenes
6 U6 U4 U6 U6 U6 U6 U11 U61111 U11 U6116 U6 U6 U6 U6 U6 U
t* »J*» rwvwlt tl •WttftB
tlCl«BB>*ia
••Mr* • HI
tnttli
vltwl* kwt t*m
y**i*r uwn trt
c^«cwitr«tlBi •*
(•«, 1OJ1. 1< l lMt
nil !• calculate*
•« ••>.»' li»> !• 1O u«l
Laboratory Naae:Case No: 7351
ENVIRODYNE Saaple Number
Organic* Analysis Data Sheet(Page 2)
Concentration: LOWDate Extracted/Prepared: 6-19-97Date Analyzed: 7-2-87Conc/Dil Factor: 1Percent Moisture (decanted)
Seaivolatiie Compounds
6PC Cleanup : YES
12.7
CASto; uqkg
ioe-95-2lU-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-106-44-5621-64-747-72-198-95-37B-59-18B-75-5105-67-965-85-0HI-91-1120-33-2120-B2-191-20-3106-47-B87-68-359-50-791-57-677-47-488-06-295-95-491-5B-7 .flB-74-4131-11-3•VIQ 01 a4W Tfl O
99-09-2
Phenolbis-a-QUtroethyUeUwr2-Qtlorophenoll,3-ttchl(rcbenzenel,4-ttthlcro&enzmeBenzyl Alcdwl1,2-DicMorobenzene2-tethylptanalbi s- (2-Cht or oi sopr opy 1 ) et her4-ftthylphenolIKii trtwHh irpr opy 1 au MHBadilcroethaneNitrabmzentIsophormMbtroptenol2,4-OiKthylphe«lBwitnc Acidbis-CQvlorarUuiy)frthm2,4-Didilcropbawll,2,4-Trichlxti«n2mekwnthiler*4-tJll(TTHfUlir«
facichlorobutadiene4-QU tr u-3-«tlivl phmol2-tethYlnapnthilmeHex adtl xxytl opeitadi ene2,4,6-Trichloropheool2,4,5-TrichlaraphenoI2-Oilaranaphtltalene2-KitriunilineDiKthyl phthiliteAcEMpthylste3-HitroaniUne
760 U76011760 U760 U760 U760 U760 U76011760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U
__760 U3700 U760 U760 U3700 U
i . Funne l E x t r a c t i o n : YESi t i n . L i q . - L i q . E x t . : YES '
CftSta
E3-32-951-2B-5100-02-7132-64-9121-14-2606-20-294-66-27005-72-3B6-73-7100-01-6534-52-186-30-6'101-55-3118-74-1B7-96-585-01-fl120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-721B-OH117-84-0205-99-2207-06-950-32-9193-39-553-70-3191-24-2
Acenaphther*2,4-Oirutnshenol4-HitrophenoiDiberaofcran2,4-Oinitrotflluene2,6-frnitratalueneDi ethyl phthilate4-aUa-Qpfwyl-phfnyl etherFlucreoe4HhtrDiniline4 , 6-to D i trtr2-tethyl phenolH-nitroaitiphenylatitw (1)4-firotflphenyl-phenyl etherHExadilorcbcnzBiePntadilxaphcnolFteunUrentAnthraceneth-n-butyl phthalateFlucraathencPyreneButyl-beniyl-phthilate3 , 3 ' -Oi oM omwu i di neBenzo(a) anthracenebis- (2-Elhvi heryl ) phthal ateOiryseneDi-froctyl phthalateBeruoib)fluoranthencBenzo(k)nuratither«Benzoi upyreneIndeno ( 1 ,2,3-cd) pvreneOibenzouJU anthracBwBeruoiainw^lw
t o J t c i r c l e o n e )t s N p J t c i r c l e one )
760 U3700 U5700 U760 U760 U760 U760 U766 U760 U3700 U3700 U760 U760 U760 U3700 U760 U7&U
c^notTN^TRHJ
760 U760 U1500 U760 U650.W *T e^760 U760 U760 U760 U760 U760 U76£> U760 U
( l ) -Canno t be separa ted f r on d ipheny laa ine
FORM 1
Njirne
Case No
Organics Analysis Data Sh««t(Page 3)
Coocentrjtion; tow Medium
Date Extracted Prepared:
Date Analyzed:
Cone /Oil Factor:
(Grcle One)
Peslicide/PCBs
GPC Cleanup QYes ONo
Separatory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction QYes
-»•.;?
Percent Moisture (decanted]
CAS «g/lofbg/KjiNumber . <CircHTJne|
319-84-6319-85-7
319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-650-29-372-43-553494-70-557-74-96001-35-212674-11-211104-28-2nut. 16-553469-21-9
12672-29-611097-69-111096-82-S
Alpha -8HCBeta-BHC
D*lia-BHCGammj-BHC (Lioda ne}
HcptachiofAkJrtn
HepucMof Epo*KJeEndosulfan 1Oteldrin
4, 4' JOEEndrinEndosuHan U
4. 4'-DODEndosulfan Sutfatc4. 4 '-DOT
MethosvcWofEndrin Ketoo*CMordaneTotaphene
Aroclor-1016
A/ockK-1221A/oclo(-1232Aroclof-1242
Aroc«x-1248
AroC(<X- 1 254
Arocl<x-126O
Kr.0 Ui
/L.o nK..O U
" .'t.p Utis<? alb,C U.
/t>.o uIL.O.U^~&-Q U-.-w.o U.r?i-<? a
1 03-^ t^tfP.O £/J3^3 «
r VW «h /ta^> u
J3.& U
tL.6.0 U
J30.0 U]t>O.O UIt'0,0 U
KA.Q Wiu>.o u/^AO U320.6 U3ZO.O It
V^ = Volume of cMrjct injected <ul|
V = Volume of waier enrj<ied <rrt<|
W = Weiflhi o< cample extracted (fll
V x Volume o< total extract (ul)
<XW.
7/85
DECEIVED SEP 1 5 1287,
uc1LJ
.12
L-*J01
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aUl — «
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i a.c --*•X
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Organic? Analysis Data SheetiPage 1) !--
Laboratory Naae: ENVIRODVNELab Sanple ID No: B7003042Sample Matrix: SOIL .Data Release Authorized By: JlV^Ul-
! S a c a l e Nusiber: Eh 8SoDL;
Case No: 7351QC Report No:Contract No: _.U.-_OJ.-.lClDate Sample Received: fc - \J2. - "&— -— - ___
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 7-7-87Conc/Dil Factor: 3Percent Moisture (not decanted;
CASHo: uqkq CftSNo:
74-57-374-63^?75-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-Z7W3-371-55-656-23-5108-05-475-17-4
CMxoaethaneBroKaethaneVinyl ChlxideChlxoethaneMethyl ene ChlorideAcetoneCarbcn lisulhdet.Hichloroethene1,1-Dichixoethanetrans-l,2-DidilxDetheneChlxofxi1,2-Dichltroethane2-Butanone1,1,1-TrichlxocthaneCarbon TetrachlxideVinyl AcetateBroiodichlxDwthane
3 4 U34U34U34U
1600 B300B
17 U17 U17 U17 LJ17 U17 U34 U17 U17 U3 4 U17 U
7B-87-510061-02-679-01-6124-48-1
' 79-00-57H3-210061-01-5110-75-875-25-2105-10-1591-78-6127-18-479-34-5ioe-ffl-3106-90-7100-41-4100-42-5
1,2-Dichloraoropanetrans-l,3HhcnlxopropeneTrichlxoettwneDibro-Dchlxaae thanel,l,Mrichloroeth»neBenzenea j- 1 , 3-Oi chl xccropene2-ChloraethYivinvlstnerBrotcrfori4-flethyl-2-pentanone2-Hei:anoneTetrachlxorjiene1,1,2,2-Tetr.cnlxQethaneTolueneChlxobenieneEthvl benzeneStyreneTotal Xvlenes
17 U17 U17 U17 It17 U17 U17 U34017 U3 4 U3 4 U17 U17 U4 6 J
17 U17 U17 U17 U
Data Aa~«rtlnf
trw V*|UB.
B*tlMttn« • c
^••r* • 111 ri
ln«lc*tBB UHI
crltBi-l* hvt *
. Tbi« «!•« !•
itt !• !••• than tk« BB
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lM •vt*ctt*n llatt >ut
lox )• 1O u«l •«• •
klanh cant Mil n*t I mr>
L a b o r a t o r y N a m e :Case No: 7351
ENVIRQDVNE Sample Number: EM
Organics Analysis Data Sheet(Page 2)
S e n i v a l a t i l e Compounds
x t r a c t e d / P r e p a r e d : 6-19-67na l y red : 7-2-67il F a c t o r : 1
Sep. Funnel E x t r a c t i o n : YESCont in. L iq.-Liq. E x t . : ¥ E 5
Olg,( (ciC^O) *ci
t M o i s t u r e ( d e c a n t e d ) : 12
CAS No:
106-95-2111-44-495-57-6541-73-1106-46-7100-51-695-50-195-48-739636-32-9106-44-5621-64-747-72-198-95-378-59-188-75-5105-67-965-65-0111-9I-1120-B3-2I20-E-!91-20-3106-47-667-66-359-50-791-57-677-47-438-06-295-95-491-58-7 -88-74-4131-11-3206-96-699-V9-2
Phenolbis-(2-Oilxoethvl)ether2-Chloraphenol1,3-Dichlarabenzene1,4-tochlorobenzeneBenzyl Al canal1,2-Oichlorobenrene2-Methyl phenolbis- t2-ChloroisopropyU ether4-flethylpnenolU-ni tr Dso-Di -n-propyl ail neteadiloroethaneNitrobenzeneIsaphorone2-fetrophenol2, 4-Oiiethyl phenolBen; OK Acidbis-(QUoraethaxyiNetMne2,4-Oichloropnenol1,2,4-TnchlorooenzeneNaphthalene*-Gil oraam lineHBichlorobutauiene4-Oii arQ-3-*ethyl phenol2-tethvlnaphtnileneHer adil arocyc 1 apentad; sne2,4,trTrichlorQphenc:2.4,j-TnchlxDphenol
-2-Diloronapnthalene2-fctroinihne&iKtnvl phthalateAcenapthvime3-Nitroinihne
uqkq
750 U750U750U756U750U750 U750U750U750U750 U750U750U750U750U750U750U3600 U750U750U750U750U750U750 U750 U750 U750 U750 U3600 U750U3600U750U750 U3600U
CAS fe:
83-32-51-2B-5100-02-7132-64-9121-14-2606-20-284-*6-27005-72-386-73-7100-01 -b534-52-1,86-30-6101-55-3118-74-187-86-585-01-6120-12-784-74-220e-44-0.129-00-085-66-791-94-156-55-3117-81-7216-01-9117-84-0205-99-2207-06-950-32-6193-39-553-7<>3191-24-2
Acenaphthene2,4-Oirutrophenol4-tbtroghenolDibenzoturan2,4-Oinitrotoluene2,HHnitrotolueneDi ethyl phthilite4-Oilorophwvl-phenyl etherFlLDTHie
4-Nitroaniline4, 6-Oi ni tro*2-ftthy 1 phenolK-nitrosodipnenvlatine (1)4-froiDphenyl-phenyl rtherHexachlTobenzenerWtachlorophenolPhenanthreneAnthraceneDi-rHwtyl phttelateFluor ant henePvreneButyl -ben:yl-phthal ate3, 3 ' -Oi chi or obenz i m neBenzou) anthracenebis-(2-Ethvif«rvliphtnali:eChryseneDi-n-octyl phtnalateBefi:o(b)fluorantheneBenzolkHlutrandiene&cn;o(UpyrenelnoencU,2,3-cfl)DvreneDibenzota.h) anthraceneBer,;cigni)pff\'iene
uqkq
750U3600 03600U750 U750U750U750U750U750U3600U3600U750 U750U75&U3600U750U750 U .
< lfaC^/Sull750U750 U1500 U750U250 «f750U75u U750U750 U750 U75C' U750 U750 U
(1^-Cannct be separated from a i p h e n v l a m i n e
FORM 1
M
Case No *
AC-- -
Organics Analysis Data Shoot(Page 3)
S*mpf« tyurn b*f
<£Concentration: ( low.) Medium
Date Extracted'Prepared;
Date Analysed: ______
Pasticide/PCBsS* • ' " ^"~S
(Circle One) GPC Cleanup OJres ONo ,,.,*'
____ Separatory Funnel Extraction QYes
___ Continuous Uqu*d - Liquid Extraction QYes
Cooc/Dif Factor:
Percent Moisture (decanted)
CAS uq/lofJL/g/Kg,Numb*f . (GrcfiTJoe)
319-04.6319-85-7319-86-858-89-976-44 -a309-00-21024-57-3959-98-860-57-172-55-91
72-20-833213-55-972-54-81031-07-850-29-372-43-553494.70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6
11097-69-111O96-82-S
Alpha -8HC
Beu-BHC
Oefta-BHCGamma-BHC (Li«xJan«|HeptJChlOr
AkJrtn
McpiacWor £po«»dcEndosulfan 1
Oieldrin
4. 4*-ODEEndrinEndosutfan (14. 4*-ODOEftdosuifan SuHaie4. 4 '-DOTM«thOKVCtilorErtdnn <eiooeO(ordan«Toupheo*Arocfor-1016
A/oclOf-1221A/oclor-1232ArocIor-1242
AfOchx-1248Aroc(0f-1254
AroC«X-126Q
/4.0 W/ f c .O MIt.O iL
-•• ll*c Uh.c (J./Lt U.
tt>,0 Url.O ^Q-d u-.sa.o M.fisC a
' *3a.o «^ _A?.O ^.32,0 W
3:. «^tO,£> U
-?.?.o «/fcAO W
JU .<5 U
/&£>.£> W/^^.^ i/&A.6 U/U>.& U
/ .<? Uj.a0.0 ^/3^^.^> W
orW.
V. £ Volume of einraa (o(J
V = Volume of waier CKlraoed (mlj
o<
V. * Volume of total extract (ul|
(gl
Form 1 7/85
Qrganics Analysis Data SheetiPage. 1 >
Sample Nuaber: EM B57
Laboratory Naae: ENVIRQDYNELab Simple ID No: 87003043Saaple Matrix: SOILData Release Authorized By:
Case No: 7351QC Report No:Contract No: __kS-rDate Staple Received
Volatile Coapounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-67Conc/Dil Factor: 1Percent Moisture (not decanted): 12.7
CA5 uqkg CflSNo:
74-67-374-33-475-OH75-00-375-0 -267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-371-55-Q56-23-5106-05-475-27-4
Chl or MethaneBroKMethaneVinyl ChlorideOil a- oe thaneHethylene ChlorideAcetoneCarbon Disulfidc1,1-Cichlaroethenel,l-0i:hloroetnanetrans-l,2-fcchloroetheneChlorotxil,2-&ichloroethane2-Butanone1,1,1-Trichltraethan*Carbon TetrachlorideVinyl AcetateBrotod i ch I or oiethane
11 U11 U11 U11 U350 B200 B
6 U6 U6 U6 U6 U6Un u6 Ut u11 U6 U
7B-67-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-975-25-2106-10-1591-78-6-127-18-479-34-5106-88-3106-90-710CM1-4100-42-5
l,Hhd)l(ri*n,»etrans-1 ,3-Di chi DropropeneTridilorDetlw*DibroBochl oroiethane1.1,2-TridilarorthaneBenzenecis-l,3-i)ichlorapropene2-Oil or aethy 1 vi nv 1 etherBnwrfori4-hWiyl-2-pent*wne2-Hei anoneTetrachloraettiBifi1,1,2,2-TetrathlToethineTolueneChlorobenzeneEthylberaeneStyreneTotal Xvlenes
6 U6 U6 U6U6 Uc L Jo U11 Uo 'J11 uIt U& Uf*-
LJJ.6 U
6 Uo U6 U
I* ttt* r««ttJt l« a vaku* arMtvr than
llatt. r>B«rt Uw valta*.
U laf.
lwt UMt . )
Halt for tit*
«. It
tit* *
tMIMr *!•••
UM r»mlt».
I ank a* ••! 1 a* a
lwi t» IO u«l
Organics Analysis Data Sheet(Page U :-
Number: EM 857DL
Laboratory Na«e: ENVIRQDVNELab Sanple ID No: 87003043Saaple Matrix: SOILData Release Authorized By: JVJ
Case No: 73S1DC Report No:Contract No:Date Saaple Received: _jL?_-_
JL3J
Volatile Conpounds
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 7-7-87Conc/Dil Factor: 5Percent Moisture (not decanted) 12.7
cs
CASHo: UOkQ CASNo: ugkg
74-87-374-S3-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4
ChloroKthaneBrojKwethaneVinyl ChlxideQilxoethaneMettiyleoe ChlorideftcetoneCarbon Bisulfide1,1-Oichloroetlwnel,H)khloroethinetrafts-l,2-DidilcroetheneOil or of or i1,2-Oichloroethane2-Butanone1,1,1-TrichlaraethaneCarbon TptnchlorideVinyl AcetateBroaodichl or Methane
57U57 U57U57 U
1600 B340 B
29U29U29U29U29U29U57U29U29U57 U29U
- -
7B-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-TH75-5-2106-10-1591-78-4.127-18-479-34-5108-ffi-3108-90-7100-41-410CM2-5
1,2-Oichloroorooanttran5-l ,3-DidiloropropeneTnchloroetheneDi bronchi Dnvthane1,1,2-TnctiloroethaiieBenienecis-li3Hhchlxopropene2-Di 1 or otthy 1 vi ny 1 etherBrcwfori4-rtethyl-2-oentanone2-HKafloneTetrachloroethene1,1,2,2-TttriCtiloroettianeTolueneChlTD6en:en«Ethyl benieneStvreneTotal Xylenes
29U29U29U29U29U29U29U57 LJ29U57 U57U29U29LJ7 f t
29U29U2 9 U29U
VMJJKl
I* tlk« »••-• tlw l««"tltltl
tictaw>-tci
»<!<•••« hv K/r«
In klMik •• veil M •
«« ••* •*
Laboratory N a m e :Case No: 7351
ENVIRODYNE Sample N u m b e r : EM 657 Up
O r g a n i c s A n a l y s i s Data Sheet(Page 2)
C o n c e n t r a t e on: LOWDateDateC o n e / D i 1Percent
S e m i v o l a t i l a Compounds
GPC Cleanup : YESx t r a c t e d / P r e p a r e d : a-19-67n a l v z e d : 7-2-87il Fac to r : 1t Moisture ^decan ted ) : 12
CASNo:
lCfr -2111-44-495-57-8541-73-1106-46-7100-51-495-50-195-48-73963B-32-910d-44-5621-o4-767-72-198-95-378-59-186-75-5105-67-965-85-0111-91-1120-B3-2120-82-191-20-3106-47-887-66-3S-50-791-57-077-47-4BB-Oo-295-95-491-58-788-74-4131-11-3208-?o-699-09-1
Phenolbia-(2-Chlxoethvliether2-ailorophenol1,3-Dichlarawnzen*l,4-Dichlxoben:eneBvzvl Mcoholl,2-0ichlxoben;ene2-«ethylphBwlbis-(2-ChloroisopropyU ether4-Hethyl phenolH-ni troso-Oi -n-pr opyl an netetachlxoethaneNitrobenzeneIsopnarone2-Nitrophenol2, 4-DiKthyl PhenolBen: 01 c Acidbis-itJlxoethtttvlMethane2,4-DicMorophenoll,2,4-Trichlxoben:eneNaphthalene4-OilxoanihneHeiictilcrobutadiene4-Chlxa-3-*ethti crenel2-fletnylniotith4ierEHex achl xocycl opentadi ene2,4,6-TnchixD()hefiol2,4,5-Trichlxophenol2-OilorDn4ohthilene "2-+*itrtianiIineDiKthvl ph-.r.iUtEAcenapthylene3-Nitroamhne
. 7
+9
760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U766 U760 U3700 U
- 760 U3700 U760 U760 U3700 b
Sep. Funnel E x t r a c t i o n : VE5Contin. Liq.-Liq. Ext. : >EB
CAB to:
83-32-951-28-5100-02-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-01 -ft534-52-1,86-30-6101-55-3118-74-187-86-585-01-8120-12-7B4-74-2206-44-0129-OOHJ85-bB-791-94-156-55-31 17-81-721B-01-9117-84-0205-99-2207-06-5
- -50-32-8193-39-553-70-"191-24-2
Ateruphthene2,4-Oinitropnenol4-fttroehenolDibenzoturan2,4-Oinitrotoluene2,6-OinitrotDlueneDi ethyl phthalate4-Oiltrnphenyl-phenyl etherFluor ene4-Nitroanihr*4,6-Ihnitrcr2-flEthylphenolM-nitrosodiphenylaiane (1)4-firoiOQhenyl-phenvl etherHexactilorobenzenePentidilcrophenolPtcntfithreneflnthraceneDi-fHxitvl phthalate (Fluor an thenePyrsneButvl -benzyl -phthilate3,3'-thchlaroDeruiiline.BenzDU) anthracenebis-(2-€thvlhwYl 'phthalateChryseneDi-ft-octvl phthalateBenzot b)Uuoran:heneBemoik; fluoranthene
- - &en:oi*)pyren*-Indeooil,2,3-cdjpvreneEribeniDii.hj anthraceneBenzcighi'ijervlene
MO (c i rNO (cir
^0
76011POOU3700 U760 U760 U760 U760 U766 U760 U3700 U3700 U760 U760 U760 U3700 U760 U
^\^ 2300 J• THHT
760 U760 U1500 U760 U370 J 57oO U760 U7&OL760 li760 U7tt; U760 U760 U
(It-Cannot be separated f r o m d i p h e n v l a m i n e
FORM 1
Ljoof jtorv
No
4 AC-* -
Concentration. ( LowJ Medium
Date Ejaracied'Prepared: ____^6~f
Oate Analyzed ______i /_•"/" T7
Organtcs Analysis Data Shoat<Page 3)
Pesticide/PCBs
(Circle OneJ GPC Cleanup GJYes ONo
___ Separatory Funnel Extraction
___ Continuous Liquid - Liquid Extraction OYes -oCone/Oil Faaor:
Percent Moisture (decanted) 12,7
CAS og/l o<f*g/K^Numt>«r . (CirtrfclJn*]
319-84-6319-85-7319-86-858-89-976^4-6309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70557-74-9
8001-35-212674-U-2111CW-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
A(oha-BHC
8eu-8HC
Delia- 8 HCGarnmj-BHC (LtndjrteJ
H«trtachlorAkJr.n
Heptacnicx Epox*deEndosuffan 1
0»eMrin
4. 4--OOE
EndrinEnbosuHan fl
4. 4--DDOEndosw^fan SuHaie
4. 4 '-DOTM«rhoK>chloc
Endftn Keion*ChtortUne
ToKapher>eX^rockx-1016A/oclo^-1221A/ock>f-1232Aroclcx-1242
A/odcK-1248Aroc(cx-125'»Aroc(tx-126O
^.£> 6t/t.rt /i/t.o tc
-- ALc a.It*: a
\h,» «./t.o «._/i,^)-K.Ji,» U-33.0 U
. -c* a* ^s^-o n
33.0 143S-0 t<
5t-.-c K' IL0.0 U
J3.0 U
It, 6.0 UXJO.& U
}&>0. 0 UIL&.O U&6.G Uiu>.o u/&6.O U330.6 a3*0. 0 IL
V^ = Volume of eruaa mj«ne<J (ulj
V = Volume of water eKiracird (ml)
W - Weight of t*m0<e enracied (gt
V( * Volume of t«*( ectract (ul|
7/85
Grganics Analysis Data SheetiPage 1)
Saftple Number: EM 356
Laboratory Na«e: ENVIRQDYNELab Sample ID No: B7003044Saaple Matrix: SOILData Release Authorized By: _
Case No: 7351QC Report No:Contract No: .I]aSr_PJ-.nZ>_i.l.Date Sample Received: __Le.~-.
-TV-nrn
Volatile Conpounds
Concentratlon: LOWDate Extracted/Prepared:Date Analyzed: 6-24-37Conc/Dil Factor: 1Percent Moisture (not decanted 1 1 , c
COm-o
CAB ft: ugrg CftSto:
74-67-374-83^?75-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-Z7-4
CM or MethaneBroKMetnaneVinyl ChlxideChlxoethaniItethylene ChlorideftcetoneCarbon Bisulfide1,1-OidilxoBthenel,Hhchlxoettijnetrans-l,2-DichlxoethcneChlxofxi1,2-tochlxoethane2-Butanone1,1,1-TrichlxoethaneCarbon TetrathlorideVinyl AcetateBr Modi chlor Methane
11 U11 U11 U11 U300 B190 B
6 U6 U6 U6 U6 U6 U11 U6 U6 U11 U6 U
- -
78-67-510061-02-679-01-6124-48-179-00-571-4J-210061-01-5110-75-G75-25-2108-10-1591-78-6-127-18-479-34-5ioe-ffl-3ioe-w-7100-41-4100-42-5
1,2-Oichloropropanetrans-1 ,3-&ichlxopropeneTrichlocoethen*Dibronchlxoa«thane1,1^2-TrichlxoethaneBenzenecis-t ,3-Dichlxopropene2-QUon»UiylYinvletherBTCWOITI4-hBthyl-2-oaitanone24triACfi(Tetrachlxorthenei,l,2,2-TrtrachloroethaniTolueneChlxobenzeneEthvloenzeneStyreneTotal Xylenes
6 U6 U6 U6 U6 U6 U6U11 U6 U11 U11 U6 UULLLi
6 U6116 U
If tn* r*mult im • VK!UB ^rm»tmr tttvi v mmitml t* t»w »«t»cliwi TDIB «!•« a**!!** (• t** p>r>aMBr* Mar* tx*
tn tN* final •« tract •M«iU
«n*ir»»* fv kut n«t Mtactv*. ^Mi
MfiOka ••^•cttvn Uut far !*• aaa«l« -ttti ttt* U tva.lOU)
•n naw:a<iar^ nncvnt. /«» lutlan art. 1 an.
Ui« ln«tru«ant ••tactlon Matt.) Th» *
OeaapOkn* na* an*lvia^ far but
•tniaHB attMna*t* MKKttv* Halt far til*
Jl
Tut* «l«a I
aaawla. It
awn* tit* a
an^lyt* 1* ««M In klwik M n*l I
Mriar «!««• an* fa*tra«*« a«v •• r»«uirMI (• arawly «
th» raaulta. If i.iaaa . tNav auat a* fully •••cftfca* an*
eomttratlan
ttarl* »vt tha> ravult la )•«• tHan tn*
a*tar Cn«n lava !«a, IOJ). If HMt •«
tnv l«antlflc*tl«n
a* *a«actlan Halt kwt
lof I* 1O t^l and •
Grganics Analysis Data Sheet(Page 1) !--
Sanple Number: EM BSBDL
Laboratory Mane: ENVIRQDYNELab Saiple ID No: 87003044Saaple Matrix: SOILData Release Authorized By: _IYlC.Ui
Case No: 7351QC Report Nor _i3.JContract Not __(^?_rDate Saaple Received: __ia-.
Volatile Compounds
Concentration: LOWDate Extracted/Prepared:Date Analysed; 7-7-87Conc/Dil Factor: 5Percent Moisture (not decanted):
i
11.6
CASNo: ugfcg CASNo:
74-07-374-83-975-OH75-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-276-93-371-55-656-23-5108-05-*75-27-4
ChloroKthaneBroraettaneVinyl DilorideOil xoe thaneHethvlwe ChlorideAcetoneCarbon Bisulfide1,1-Oichlorocthene1,1-Dichloroethanetrans-1 ,2-DichlaroetheneChlorofori1,2-Oichlaroethjne2-ButanoneM.HridilxaethaMCarbcn Tetr .chlorideVinyl fcetite&-D4wn:Mcr at* thine
571157 U57U57U
1100 B150 &
28 U23 U26 U2 8 U28 U2 S U57U2 8 U28U57U2 8 U
78-67-510061-02-479-01-6124-48-179-00-571-43-210061-01-5110-75-875-25-2108-10-1591-78-0127-18-4 -79-34-5108-88-3108-90-7100-41-4100-42-5
1,2-Oicnloropropwetrans-l,3-DidiIir[j)rcp€neTridiloroethewDibroiDchloroaethane1,1,2-TridilGTorthaneBenzenecis-l,3-OichlorDprop«ie2-Chl xoethyl « nyl etherErurixi4-flethyl -2-pentanonB2-HKjnoneTetrachlxoethene1,1,2,2-TetradUoroethaneToluswChlorobenzeneEthyltHTceneStyrweTotal Wires
28 U28 U28 LJ29 U28U28 L)26 U5 7 U2 6 U5 7 U57U23 U2 8 U8 W
2 8 U28U28 U28 U
If tM
HMt,
••/ul in th» final •• tract
fla« I* iiMtf •!»•« «««ly<« IB «•»»»• In »lw>k •• ••! 1 4*
>•. It trMICBt** •*••.!>l»/^-••••la blank cwtMiMtlan
aa> «n B*tlMit«« -ralu*. Thl» flM '» u**^ Hthar iri««ft
t.tan »»r- tantatlrvly I«w>tl4laa1 caawaun**
•fur* • 111 •'•••ana^ 1m Hi n i« V ultan tit* aaaa apaMtral ««t.a
IntflCBt** IX* pi iia.K.» *f • i IBM mi I Wv*« •••*• tfw l*ontlflc«tl«n
crltarla but t*» raw.)* t* !«•>• than ttw BavclflM avtactlvn llMt but
tr*a.tar tNar. iar-« laaj, lOJi. If Hut *f «rt.actlBn la 1O ka|l am a
cwteantratlBH a* 3 ual I* caleulvtM, rvwart » W.
OUt«r flat* MM «••*(•*«•• *w •• f*aulr*« t* *r«a«rly
th* r«*Kt)t*. I* waaM, tfvy au»t »• fully •••tribal an
•*«:rl»tl«B attachari tv tlv* «at* MaMMry raawt.
Labor atory Name:Case No: 735 1
ENVIRQDYNE Sanp 1 e Number EM 956 rrt
Organics Analysis Data Sheet(Page 2)
S e f i i v o l a t i l e Com pounds
C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : b-19-87D a t e A n a l y z e d : 7-2-6"C o n c / D i l Fac tor : 1P e r c e n t M o i s t u r e ( d e c a n t e d ; : 11
CASNo:
108-95-211 1-44-495-57-8541-73-1106-46-7100-51-095-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-07-9o5-65H>111-91-1120-83-2120-32-191-20-3100-47-887-66-359-50-791-57 -B77-47-486-Oc-295-95-4
— —91-56-7 -88-74-4131-11-320S-96-B99-09-2
Phenolbis-(2-Qiloroethyl)ether2-Dilorophenoll,3-0ichlxafaen:ene1.4-Dictiloroben;eneBenzyl Alcohol1,2-Dictilorabenzent2-tethyl phenolbis-(2-ailoroisoprDpyl)ether4-ttethvlphenolH-ni trreo-Di -n-pr apylui tieHeachloraethane(btrobenreneIsophorone2-Hitrophenol2,4-OitethyiphenclBen: OK Acidbis-Oiltrwthosyihethane2,4-Dichlorcphenoll,2,4-Tridiloraben;eneKapnthalene4-GUoroanilinEHeiacMorooutadiene4-Chl oro-3-iet.hvl phenol2-ttethvl naphthaleneHexacMorocycloDentadiene2,4,6-Trichlorophenol2,4,5-Tnchlcropnenol
-2-Qiloronaphthalene -2-KitroafiihneDiKthyl phtnalateftcenjpthylene3-Nitroanihne
.6
^
750U750U750U750U750U750U750U750U750U750U750U750LJ750U750U750U750U3600U750U750 U750U750U
. 750U750U75-) U750U750 U750U3600U
_ 750U3600U750U750U3600U
6PC C l e a n u p : YE5Sep. F u n n e l E x t r a c t i o n : Y E 5 {C o n t i n . L i q . - L i q . E x t . : Y E S
CASfc:
83-32 ?51-2B-5100-02-7132-64-9121-14-2606-20-264-66-27005-72-386-73-7100-01-6534-52-1fc-30-o'101-55-3118-74-187-66-585-01-3120-12-784-74-2206-44-0129-OCH;85-6B-791-94-i56-55-3117-81-7216-01-9117-fl4-.j205-99-2207-«'*-T50-32-8193-39-553-70-3191-24-2
Acenaphthene2,4-&initrophenol4-totrophenolDibenzoturan2,4-OinitrDtoluene2,6-OinitrotolueneDiethyl phttalate4-Oiloropnenyl-pnenyl etherRuorene4-*btroanihne4,6-fonitro-2-ftetnylphenolH-nitrosodiphenvlaune (1)4-&roiophenvi-phenyl etherfatachlarabenzenePentachlorophenolPteianthreneAnthraceneDi-n-butyl ohtnaliteFluor jnthenePyreneflutyl-fcnzvl-phthilitf "3,3 -OiduxoberuidineBenzoia) anthracenebii-{2-ElhvlhovlionthilateQiryseneIri-n-ortyi phtnalatetei:o(bJfiuorantheneBeniotkjiluorsrtneneBenzotatpvreneInoern U , 2 , 3-cdi pyreneDibenzDia.hlanthraceneBenzoiortiiDerYiene
\f
N£ ( c i r c l e o n e ;\»^ (C i re 1 e one i
unkq
750U3600U3600U75011750 U750U750 I)750U750 U360u U3600 U750U750U750U3600U750 U750 UIfo750 u750 U750U1500 U750 U4% W U3" pj^750 u750 LJ750 U75u U750 U750U750U750 U
(li-Cannot be s e p a r a t e d rrom d i p n e n y l a m i n e
FORM 1
Name S*mp4« tyurntxai
rM Try
Concentration; ( LowJ Mediumi
Date Extracted'Prepared:
Date Analyzed: _____
Conc/Oil Factor: _____
Organic* Analysis Data Sheet(Page 3)
Pesticide/PCBs(Circle One| GPC Cleanup fSres ONo
___ Separatory Funnel Extraction
___ Continuous Liquid - Liquid Extraction QYes
Percent Moisture (decanted)
CAS «g/l<Kt»g/K^Number . (CircKTjnel
319-84-6319-85-7319-86-858-69-976-44-6309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-650-29-372-43-553494-70-S57-74-96001-35-212674.11-211104-26-211141.16-553469-21-912672-29-611097-69-1l 1096-82-5
Alpha -8HCB«ta-BHCDelia-BHCGamma-BHC (LindanelHe0**chl<x
AkJrm
Heptachfor £pOK*deEocJosulfan |
Otefdrtn
4.4'-OOEEnoVinEndosuMan (I4. 4'-DOOEndosuifan SwHaie4. 4'-ODT *
M«ttxiKvchI<xEndrin (CeioncChkxtlarx
Tocaphen«Aroc(<x-1016
A/oc(of-1221Arocloc-1232Aroclor-1242
A/odcx-1246
Aroc«x-1254
AfocKx-1260
!<*.0 U.1(>.O ILIC..O U
- H,& a16<o a.1^0 W-tL*O Uit,.O K_Q-fi'-U.33.0 U3z,o a
' »J3^ U>P.O l<
Jp^ t<"%-^C3 M/to.;? Ujyj.^? «11,0.0 UJ30.& U
;6<3.<5 UIt-0.0 U&6.0 Ul&c.o uM6.O Ujji>.o a310.O VL
r>m. -• o
oom-o
V( = Volume of enracr injected (u<|
V - Volume of water extracted (m(|
W - Weight o* «mp*e extracted (gj
V * Volume ot total extract (ul)
Focm 1 7/85
Contractor: (TtJ Vl fit)~
TENTATIVELY I D E N T I F I E D COMPOUNDS tgMATCH ASSESSMENT
enNOTi: Reviewer should note directly on Organic Analysis Data Sheet (QACS) —
those matches that 1n his op in ion (based on contract cri teria) are counreasonable .
CP.ITE31A
(1) Relative intensities of major Ions (>10-) reference spectrumshould be present 1n the sample spectrum.
(2) Relative intensities of major ions In sample spectrum shouldagree to within +_ 201 of reference spectrum ^intensities.
(3) Molecular ions present in reference spectrum should be present1n sample spectrum.
(4) Ions present in sample spectrum, but not in reference spectrumshould be reviewed for possible background contamination orpresence of coeluting interferences.
(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelut-ing interferences.
(5) If, in the reviewer's opinion, no valid identification canbe made the compound should be labelled as "unknown" and theinitials and date of the reviewer placed on the OAOS.
Analysis Data Sheet(Page 4)
Tantativoly Idontifiod Cofnpounds•A)&O
CAS
2.
3.
S.
7.
e>.t.
2...
17.
J8.
iO
-o
? 8S
No
Organtes Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASCompound
"feu/v~T(/0 3
6.
7.
9.
10.
11.
12.13.
14.
15.
16.
17.
18.
20.
~ V
510.3
U U O3^0-3
GarbOO (-7-63603
•Lud-roQXLrb&n3-1
£±LA5_Z :nox
1*
MM
27.
28.
30.
? 8S
No: ^ \
£ K) VJ 1 Analysis Data Sheet(Page 4)
Tentatively ldonttf*«d Compounds
I EL
- %CAS
Compoond F» action Concentration(wg/l
,2-io-c 5
i:: 35C5403
no9. I'M
MUCLTII.
13.. lud rocar hxc
17.
18. tore dGL r b c o
0 l l 35.2 Moo1/64
I. P»n 6 7 8S
No-
Organic* Analyns Data Sheet(Page 4)
Tentatively Identified Compounds
CASCompound N*m«
(wg/l
-FuAOLnetrvg t d'llL^dm-•*^ I ft A *
. 2.. 3
I7
10.
11.
13.1*.
17.
r8-Its.20.
(21.
23.24.25.
26.
27.
26.
29.
IS. 3 USO 3
IS- 2.id vr) o a. r t>6-u^u
UW d rri (i/i rhvrv .
rbc xi 3-1- -7
a*1-7 (TOT
IMCTD
XxIA j
f o«n I.P»n B 7 85
No:
£N 01 £6t>V IsJG- Organic* Analysis Data Sheet(Page 4)
Tentatively td«ntifi«d CompoundsXJmommac/>m•o
f <xm 1. P*n 6 ? 8S
VrtM
GASNumb**'
*
13.
1*.
15.
16.
19-
, I
27..
29..
30..
P-OD V^J£Pr9anics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
•Compound Fraction
A/M.
RTocScwiConcentration
(vg/lor wg/kg|
X)•Tlom
aCf>
CO"
1. Pan 6 7 85
•*e No:
Organics Analysis Data Sheet(Page 4)
T«nCativ«ly ld«ntifi«d Compounds s«=*«
1.2.
3.
BtoA -7.S.0
not)3^03
IS-S
7..
. e.,
! 9--
111..il2..
13..
15..
16..
8..
in.b
0>(03\lCro
5903-CA
1'
fbrm H 3303
^^ JIM
27.,
26..
3O..
fcxm \ 85
Organics Analysis Oata Sheet(Page 4)
Tenlativoly Identified Compounds
-umo
oCO
en
30
FO*«» 1. Pan 6 7 8S
:-sc NO:
Organlcs Analysis Data Sheet(Page 4)
Tentatively Idontifiod Compounds
Cocnpouod
t 3t-i> 3
H.S M 5C 3'5.2. t ^MC
.r btrw
1O.,
II..12..
S-I.-1CCLrbfv.
. 1
16.
17.
20.
21.
7.4.
zs.26.
Z7.
28.
1^03rt
rhr*
^udt Sc-2 SHCJ
form I. Pan B 8S
DECEIVED SEP > 5
o£w«w«o ^
~£>c3
ctt0)
\r,cT|r5 o« Z\ *\i
• '
W^
i.1*•**eo•3>s«c«K
,.ISJ « s
IIu* 5 "0 ?
T o*
Sc*
«N
wm
b«f
C
.!Sii
fZ
CA
SN
umbe
r
•£Ci
C
<:<^CA
Cic
•
*^
• t1 r•» ir tjri f» tD 0r. <3 »- f
-
-J 1
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t *
,<f.
t VJf) M
*
j r* 0a r 1 *• r4 r
ii
t «J V ut r a CI Q
ari
No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds on}
1CASNomb*< Cofnpoond Nam*
, - ^MVCI 2.———————
i::
,26..» 27..
IB..
I!3
If . vWEatemnoic lacu
n
L ocxd ,^3'-Ud^bis-^
Mtrt
HOC 3
n.i MMC1- 2.
I. Pan 6 ? 85
Organic* Analysts Data Sheet(Page 4)
CAS
*
9.1O.
1.,12...
13..
IS..
"6..
18..
:O..
/3.24.
26.
T7.
:e.
Ito.
Tentatively Identified Compounds
rr.r-n
rbev*cv-
6
Fraction NwmtMf
ILi
(1.0
so.So -335.2
Ct(«m*t*d
iIE.? 6
^700 T
-noCI
7 8S
ecology and environment, inc.111 WEST JACKSON BLVD., CHICAGO. ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
Date Received for Review
From: Zena Gold-KaulxanSubject: MOD
PAHtltO/*//
Date Review Completed
Case # IISample Description _____
Organics (VOA, ABN, Pest/PCB)
Low SoilO*Low WaterDrinking WaterOther
Inorganics (Metals, Cyanide)
Low SoilLow WaterDrinking WaterOther
•Project Data Status Completed!
Incomplete, awaiting:
FIT Data Review Findings:
- bei^ur C£DL
Book No-
Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.
Page No.
K ecology and environment, inc.CHICAGO, ILLINOIS
CHEMICAL EVALUATION FORM
DATE:
CASE
TOX/PERS
735") UNITS' REVIEWER:
COMPOUND CRDL 3-SxCRDLE/M
10Chfusenfe 530
5 •CTss
Oi-n-cc&j' 330
DATE:
SUBJECT
FROM:
TO:
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V
/<
Review of Region V CLP DataReceived for Review on
Curtis Ross, Director (5SCRL)Central Regional Laboratory
Data User: P ^ T/
<<\
Vo
tP
We have reviewed the data for the following case (s ) .
SITE NAME: /-Pn£.£"%H
EPA Data Set No.
CRL No.
No. ofSamples: Q
SMO case No.TLU. /ActivityNumbers
SMO Traff ic No.
CLP Laboratory: '' ^ok^/^oeHrs. Requiredfor Review: 6
Following are our findingsfT^
Data are acceptable for use.( ) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory{ ) Data are unacceptable.
... — -cc: Du'ane Geuder, "Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas
EPA FORM 1320-6 (Rev. 5/87)
CASE I
\UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION V
CALIBRATION OUTLIERSVOLATILE HSL COMPOUNDS
' ' - - CONTRACTOR
DATE/TIME:
Chl oromethaneBromomethaneVinyl ChlorideChloroethaneMethyl ene ChlorideAcetoneCarbon Dlsulfide1,1-Dichloroethane1,1-DichloroetheneTrans-1, 2-Oi chl oroethenerhloroform,-Butanone1,2-Di Chloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi chl oromethane1,2-DichloropropaneTrans-1 ,3-DichloropropeneTrichloroetheneDi bromoch 1 oromethane1,1,2-Tri ChloroethaneBenzenecis-l,3-0ichloropropene2-Chloroethyl vinyl etherBromoform4-Methy 1 -2-Pentanone2-Hexanoneetrachloroethene
1,1,2,2-Tetrachloroethane'tolueneChlorobenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene
AFFECTEDSAMPLES:
nit. Cal.-/^"-Jf7F
•
1RSD
70(o%
*
JJ"
&L lAtotLe*
*ont • Cal .£ Sf'£7 /?:V5*
*F *0
yo313?
*
J3-J-
££M&<a&
<£M%d
Cont. Cal .-J6-ST /7:7«
RF to
¥/¥o
*
crJ
e^f^i-f^ttLf
Cont. Cal.-jt-/7 //t:rr
RF ID
5^
/oi"/
^?^
^7?
*
CT
JJ
T
J
€>f8"66
Cont. OLlj.(<\
RF *D *^o ^— V 5\ *
— - c<
"^ac°.
These flags should beTppHed to the analytes orTthe sample data'sheets.""1----;
1/87
CASE? 7 3 57
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDS(Page 1)
CONTRACTOR
••.DATE/TIME:
Phenolbisl-Z-ChloPoetnyl )Ether2-ChloPOohenol1 ,3-Oi chl orobenzene1 ,4-01 en 1 orobenzeneBenzyl Alcohol1,2-01 chl orobenzene2-Metnylphenolbis(2-chloro1sooropyl }Ether4-MethylphenolN-Nitroso-Di-n-?POpylamineHexachloroethaneNitrobenzeneIsoohorone2-Nitroohenol2,4-OimethylphenolBenzole Acidbi s( 2-Chl opoethoxy )Methane2,4-OlcttloPOphenol1 ,2 ,4-Tri chl orooenzeneNaphthalene4-Chloroanil1neHexach 1 opobutadi ene4-Cn 1 OPO-3-Methyl phenol2-Methyl naphthaleneHexacnlopocyclooentadiene2 ,4,6-Tri chl opoohenol2,4,5-Tpichloroohenol2-Chloronaohthalene2-Nitroan1l1neDimethyl PhthalateAcenaonthylene3-Nitroanil1neAcenaohthene2,4-OinitPOphenol4-NitrophenolDibenzofupan
. AFFECTEDSAMPLES:
_ . . . . _ - - . ._ . . . . . . _
[nit. Cal.f'3-Sr*F %RSO »
,0V?
M-V
•
S&.0
3?.J
J
^
J
tfv*rf^-e%vJ65*
II MI r. Cal . I'X'JiT. Cal .
*F %D *7- 6-8 7 \RF
I
*D * tt
I II I I
%o *
I
7-/tf-S"7RF |%D *
I I
I
II I I
II
3*,7
VrP-7
V0.3
J"
f
J~
*?/wrS-9
I
.
*
• .
.«7
3(9.6
33.3
T
%
J
&H9<a4>
9
^
* These flags should be applied to the analytes on.the-.sample data sheets.— -
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDSPage 2 _
CONTRACTOR
DATE/TIME:
2,4-Qinitrotoluene2,6-OinitrotolueneOietnylpnthalate4-ChloPOonenvl-phenvleinerFluorene4-Nitroaniline4, 6-DinitPO-Z-Methyl phenolN-Nitrosodiphenylamine4-Bromoohenyl-ohenyl etherHexachlorobenzenePentachl orophenolPhenanthpeneAnthracene01 -n-Butyl phthal ateFluoranthenePypeneButyl benzyl phthal ateBenzo( a) Anthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl. Phthal ateBenzo(b)FluopantheneBenzo(k)FluopantheneBenzo(a)PypeneIndeno(l,2.3-cd)Pyrene01 benz( a ,h ) AnthraceneBenzo(q,h,1) Perylene
Init. Cal.7-a-?7RF
.Oil
-RSD *
^
iTwiT. Cal *
RF 10
I
ii
*
' .llwrt-.. Ca*y.j7-6- S- 7 1
RF M 1*1
RF 1%0 1*
•
.en ft
*• cRF
- •--
.«a^1
to » "
•
/^
SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytes on the sample data sheets.
1/87
ENVIRODYNEENGINEERS
12161 Lackland Road.St Louis, Missouri 63146(314)434-6060
July 17, 1987
Ms. Carol SchaefferSample Management Office290 Madison Street, Suite 200Alexandria, Virginia 22314 - • ' ' ' '
Dear Ms. Schaeffer:
Enclosed are partial results of analysis of Case 7351 for Vola tiles, BNA'sand Pesticide/PCB's performed by Ehvirodyne under contract no. 68-01-7087.Soil samples, EMS59 through EM866 were received on June 19, 1987.
The samples were screened for Semi-Volatile levels by GC and they were allshown to be low level samples. All samples were cleaned up on GPC forPesticide analyses.
A matrix spike and matrix spike duplicate, the second for this case, were runfor volatile organic analysis only. Semi-Volatiles and Pesticide/PCB QualityControl Samples were submitted with previous samples on July 10, 1987*
In general, all quality control criteria were met, except sample EM866 had tobe re-extracted and analyzed for SNA due to low recovery of one surrogate.
In second column confirmation of pesticides, we observed higher than allowedpercent difference for the compounds of interest. However, the samples hadbeen analyzed in between the calibration check standards. The analyses wereterminated for corrective action for samples following the last calibrationstandard.
If you have any questions, please call Dr. Margaret Winter at 314/434-6960.
Sincerely,
Shaaban Ben-PooratLaboratory Operations Manager
SBP/smb:198Enclosures
f? fi? *L-JUL 201937
U S CPA, CEN lfcAL MtGlONAL j>B.536 S. CLARK STREET
CHICAGO. ILLINOIS 60OA
CAM Ho.Low.——
SOIL SI DOGATE PERCENT RECOV tY SUMMARY——— Contrtot Laboratory E-rrVt. f~6 **f*&-*_________ Contract No.
MediumVOLATILE SEMI-VOLATILE •PESTICIDE-
• HO**rr•a.
tOLUCNC-H iri 1.1 AiCHLMft*CTM4MC-»«
If «- 11 II
MiTflO- 1-fLUMO-•I'MIMTL
rtft'NtMIL• 14
(14- M»)
t'fVUOMOPMtNCK.
lt»*tllt III- III)
•numNLMCNt
110- 1*0)
**
lUL2tfL &£
tOL HB_ &&
W/Of 'it K>A *
mia5_ j£&- m±_
1: * VALUES ARE OUTSIDE OF CONTRACT REQUIRED- QC LIMITS: **ADVISORY LIMITS ONLY
VoUtllasiS«ml-VolitlU8t
CJ ft"* ofJ— out of
O
t outild* of QC llffllttI outildt of OC llmltiI outild* of QC
C
7/66
SOIL MATRIX 'IKE/MATRIX SPIKE DUPLir TE RECOVERY
Low L«v«l
Contractor
Medium L«v»l
FRACTION
VOASMO
SAMPLE NO.
8/N iSMO
SAMPLE NO.
ACIDSMO
SAMPLE NO.JO/I
PESTSMO
SAMPLE NO.
DA
COMPOUND
1.1-Dichok>rtlhtn«Trichlorotlhen«1&rt W*Tolutrf*
CA/*t>fc*ft««41,7,4-Tfichlorobtnicn*Aciniphihtni2,4 DmiuotQlutn*PvrtntN-Niiroiodl-n-Propytimint1 ,4-DichlorobtnnniPenuchlorophtnolPhtnol2-Chlorophcnol4-Chloro-3-Mtlhvlph«nol4.Ni|rophtnolLind*niHtptachlorAldnnOitWfinEndrin4.4'-DDT
CONC.ADDED
SPIKElug/Kg)
tf3f3$sH*$
*Jfl1
fljft
=1=
SAMPLERESULT
A)DA->T>A)P1.0Pt>
>l
*\J/
CONC.MS
•6(0S/rt(ofi^ft
T*M 1 A
X /AJ/^*\1/
XREC
97*fjtltfY1T?3)('
\
A
/MI
CONC.MSD
6,3.445V56goJuA
/JL>/i
\
RECf&f7U>
j
V.
/I
\
ft
•••^
>•
RPO
/3L34-
C2aJ>l
aL)f\
\X
1 1 UA.//I
OC LIMITS*RPD
2224 /j
C2lr217123194738382747356033506031433845SO
RECOVERY
59-17262-13760-13369-139M-14238-10731-13728-8935-14241-12878-10417-10978-9075.10778-10311 11448-17735-13034-13231-1344213923-134
^ASTERISKED VALUES ARE OUTSIDE OC LIMITS.
RPD: VOAi—L_out «• £ ;B/N——£_<>« ol A ;ACID Q.. om of Jp ;PEST ——2L out ol
OC llmltiouiiide OC llmiuouliidt OC llmitlouttidt OC llmiu
RECOVERY: outtkt* OC MmlnoutiM* QC llmitloutlidf QC llmiuOuttidt OC Mmili
FORM III7/85
Orginics Analyiii Data Shctt(Pagi 1)
Saaplt Nuaber: EMB59
Laboratory Naae: ENVIRODYNELab Siaple ID No: 87003138Saaple Mitrii: SOILData Release Authorised By:
Gift No: 7351QC Riport No:Contract No: .Datt Samplt Rcctiftd
VoIitiU Co»ponndf
Concent rat ion: LOWDate E x t r a c t e d / P r e p a r e d :D a t e A n a l y x e d : 4-25-87Conc/Dil F a c t o r : 1Percent Moiitore (not decanted): 13.73
CIS Ho: iqtf CIS Mi igkg
74-17-174-13-?73-11-473-fl«-373-l»-247-44-173-13-173-35-473-14-313(-ll-347-44-3117-14-17M3-171-33-434-11-3UI-B3-475-17-4
CklatOBitkait [ItBBBBitkaaiTiByl CklBt id i 1CklBiBitkaaiHitkylm CklnidikCltBBI
Cirboi D i f iK id il . t -OicklBioi tkiniLl-Dicklir t i tkaiittaii-U2-Dickl«r«itkiiiCklindn1,2-DieklitiitkaBt2-litaiiB«t.l.l-TrickIt[»itkniCaibfi Titruklirii iVti|l ke i ta t iItOBBdiehiitflEitkaii
i7~li o J
2 12 021 1If 11V9tVi
2 V11
11 01 1
71-17-3lltil-12-t7f-l t-41H-U-17T-II-S71-43-2lMU-ll-3ltl-73-l73-13-1ltl-10-13fUTI-4127-11-477-34-31II-II-3lll-fl-7111-41-4111-42-3
1,2-DtckI iTBpt tpant r iBf- l ,3-OlekUiBft r f i i t i*TricklotoitkniDlbr»*ekItr»Bitkiii1,1,1-TticklBiiitkaBilinitie i f - l , 3 - D i c k I i r B B t B p t n <1 - C k l O t B l t k f I f i B T l l t k B I
Ir»ifin4-IUtkrI-2-p«ttiiiti2-RltttBBITitrickliriitkiBi1,1,1.2-TitKcklariitkaiiTo I • tilCklmkiBiiitItkflbtlllBtStfr tnTttll tfllltl
0QD9U0D
12 BQ
11 0L2 1
VV00ff0n
Oatt ItpirtiBo, Qialifiiri
if • vilu jriatir tin ir iivil ti tki ditictiiBthi
C:WLK:If thi ttivltlilit, tlBBlt
I:Ii4ictl»i tiBfflnl MI tulfi** I«t lit »t 4ttteti4 Itftit Ui•iiiau dittcti*! liiit ftt tht itmfli «ttk tki 0 Ufl . l lQ)» itctititT CBtetit. / l i lttiBi aetifli. (T&ii U ntIht iutmBSt 4tt*ttiBt l i l i t . ) Tki f*»ti*ti ikoiU rial: I-Ciiptid vu tit lf itd fti »«t ait 4itBCti4. Tkt ink it ii tkiBiaiin at tainkl* It t tct lat lUit fit tk* lupU-J:iBdicitii *i titiMtai* tain, nil fltf if lit* iltkti wkiiHtiiatUf i ctittitrttiBt, (tt tiitiliiili iiiitifiil ctEfoodi - „•hut a 1:1 rtiaoiiB if iftn*d ir «t» tka man iiictril iatt --":•--ii41catH tkt ptistiei •( i ciatoiad tkat Miti tfci iititllicatloierittiia kit tki tifilt ii lin tkai tki ii«cidH dttictin lii.it kitftttiir tkn uta (if, tlJ). If lilit if dittctioi ii II i|I aid t
nil flat iiplin (• iBfticidi Mi"<titi vkttB tkitiii was etilirmtf IT CC/KS. Siiqli cnpBint itittcidtsl'll•l/il ii tki final iitttct (koiU •• tBifiiktd kf CC/HSI" - • - -nil f la f if tfil vk» atatyti Ii fond ti kl»k u «<ll ai alill!i It iiduitii piiiibU/irikibli klank cBitutiatitn andmm tki data nit tt taki afpupt i i t i tct ioi .OTHE1:Otk*t fliii aid foattotn may 11 riqurid ti |iB|irlT difintki rifilti. It isid, tiif Hit ki (tllr disciibid aid tickdncrittiii attickid t« tki dtt* nutty
Laboratory Nt»«Cist No: 7351
ENVIRODYNE S i m p i t N u » b « r
Organic* Analysis Data Sbttt(P«gfl 2)
Scaitolttilt Compounds
C o n c e n t r a t i o n ; LOVDiUt E t t r a c t e d / P r e p a r e d : 4 - 2 4 - 8 7
t A n a l y s e d ; 7 -2 -87c / D i l F a c t o r ; 1cent M o i s t u r e ( d e c a n t e d ) ; 1 3 . 7 3
CIS K>:
lll-fS-2 FkiBol111-44-4 k l s - ( 2 - C B l t C M t k f l ) t t k t i13-37-1 2-CkUroBktBaI341-73-1 1,3-DickUrilti itBt114-44-7 l ,4-DickUr*bmeit111-31-4 Itttyl lletktlf3-3l-l 1,2-OickUttbtutiifS-41-7 2-IUtkTltkiBtl3f43l -32-f b i i - ( 2 -Ck lorB i f e i i o»r I ) i tk« i114-44-3 4-Kttk7l|ktB«I421-44-7 l-iitrti»-Di-t-Brtpfla»iBt47-71-1 ImckUttttkaufl- f3-3 litrikmiBt7l-3f-l Istektrtit11-73-3 2-Ntt iopkiBil10S-47-* 2,4-DiaitkylihiBtl43-13-1 Iwttie Icii111-fl-l ii«-(CkIei«tktiT>H«tkaBt121-13-2 2,1-DUkUratkiBtl121-12-1 l ,2 .4-Tritklu«i<BimM-10-3 RiBktkalm114-47-1 4-CkIitoiiilin17-41-3 luaekUrtkit adieu37-10-7 4-Ckl«n-J-mttkjlik*aelf l -37-4 l -Hatkf lBafktkal»i77-47-4 liiickItriCTcltp»ta«i*Bi11-14-2 2 , 4 , 4 -T i t tkUrDBkiBt lT3-f3-4 2,4,3-TiickliitpkiBtlf 1-51-7 2-CkliriBipktktliBi11-74-4 l-litr»tBilifte131-11-1 Oi i t tkyl iktkilitilll-fi-l IctBiptkrliuff.|f-2 3-Nitr iaBi l i ie
( l>-C»nnot bt
S e p .Cont
Mk,
310 0311 V111 Q110 V111 0no o310 0311 V311 0311 U311 Q311 V111 V311 I311 V310 1tfll 0310 «311 B301 1311 Q111 V311 0310 Q311 0310 V111 DItll D311 1Ifll 0311 0111 1If l l U
t tparat td
Funne l E x t nin . L i q . -L i q
CIS No:
13-31-f31-21-3111-02-7132-44-f121-11-2414-21-214-44-27013-71-314-73-7111-01-4334-32-114-31-4111-33-1111-74-117-14-313-11-1120-11-714-74-22H-44-Illf-OI-l13-41-7fl-M-134-33-1117-11-7211-ll-t111-14-1H3-tf-2217-ll-f
_ 31-32-1lfl-3f-333-71-3ltl-24-2
f rom di phtny 1
i c t i on : YES C J W U i r c I e. Eit . : YES (tity ( c i r c l e
ICtBlpktktBI
1 , 4 -DUi t i tpk i i o I4-Xit lD |k lBQl
DiktBiof i r iB2 , 4 - D i a i t r > U l i t f t «2 , 4 - O i B i t t i t B l i t B iDi i tky l iktUUti4-CkUropki iTl-pki iy l t tk trFliotut4 -N i t re«B i l i i f f4 ,4 -Di i i t ro-2-Ki tkr lphiBolM-iitraii4i |k*Bf limin <1)4-ltek«ikiirl-ik«iTl ttktrItiickUititini*Ftitackltrtiknolfktiaitkrti*iitkraeiBiOl-t-bitTl pktkiUt ifli irtBtkiicFfllBI
I l t T l - k C B t f l - I B t k l l l t l
3,3' -DickIttebiBtidiBtIcBttdl iBtkrattBtUl - ( 2 -CtkT lk t iT l ) | k tk iUt iCktTintgt-1-tttfl iktkalatiI t B I B t k H l l O K B t k l B t
ltBi«(k)tlten»tkiBiItBItdltTtBB*
Iiiii»(t,l,l-t4)|fii«Dikt t i i<a ,k )a i tk [ i c tB iliBi«(|ki)ttryltit
amint
one )one )
i^kq
310 QI f l l 0mo o311 U310 D311 D311 Q310 QJ l f l 0Itl l UI f l l V311 U311 D310 6mo Q311 U310 0410 1311 D310 3311 D771 U310 Q710 131 BX
QjJL^310 U310 0310 Q310 Q311 D311 D
FORM 1
Laboratory
Case No __
Organic* Analy*1"5 Data Shoot(Page 3)
Pesticide/PCBsConcentration: ( Low) Medium
i _Date Extracted'Prepared:
Date Analyred: ____L£L
Cone/Oil Factor: ____
(Grcle GPC Cleanup B^es ONo
Separatory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction OVes
Percent Moisture (decanted)
CAS ufl/lo^fc*9/Ko,Numb*r . (GrcleT7n«l
319-64-6319-85-7319-86-858-89-976-44 -fl
309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-M-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6UO97-69-1M 096-82 -5
Alpha-BHC
Seia-BHCOUa-BHCGammj-BHC (Lindine)
HeptJch'Of
AWnn
HeptacMor EpoxtdeEodosulfan 10*e(drin4. 4' JOE£ndftnEndosutfan d4. 4--OOOEndosuffan Sutfate•4. 4--DDT ^MemovycMorEndf in KeiooeChlordaneTo«Jpn«f>«
Arodof-1016A/octor-1221A/ockx-1232Aroclof-1242A/odo<-1248Afoc(or-1254
Arocfo<-1260
«.. a/ t .<0 flIL.O U
- /6.0 «
/6.0 «./A-0 «./t.o uH.O K _33.0.VL.-53.0 U
JS,<? a*33^J «jrp.o uJ30 «J3JJ U
1 (*&.£> U.
Jl.0 UH~AO U
Jwo. ) Uite.o ulL£>.Q U£6.O Uiu>.o ul(,t>,0 UJ20.0 U
320.O IL
V- * Volume of e*iraci infected (u<|
V * Volume of water extracted (ml)
Wfi * Weight of cample extracted (gj
V( * Vofume of total ectrao fuQ
orW.
7/85
Organic! Ana l y s i s Data Shttt(Page 1)
St>pIt Nu«b*r
Laboratory Naat: CNVIRODYNCLab Samplt ID No: 17003140Simplt M i t r i i : SOILData Rtltast Aathoriitd By:
Case No: 7351QC Riport No: _Contract No: _____Date Saaplt Received
Vo 1 at iIt Compoandf
Conctntrat ion: LOWDate E i t r a c t e d / P r e p a r e d :Datt Analysed: 4-25-87Conc/Dil Factor: 1Percent Moisture (not decanted) M.I
CIS No: •fkf CIS Ko
74-17-374-13-179-11-473-M-37S-II-1•7-44-175-15-175-35-475-34-S151-il-Si?-ii-l117-li-l7I-I3-!71-35-iSi-11-3lll-IS-473-17-4
Ckltrei t tkait 1lioieittkait 1TtiTl Ckltridt 1CklottttkaitKit If I tit Ckl t r id tictttitCarkoi D i n l f i d t1,1-Dickloittthtit1,1-Dicklerit tkaitttais-l,l-0ickltrectkntC k l t r t f e r i1,2-Oickltitttiait1-littieii1,1.1-TriekltrottkaitCailti Tt t taekl t t ldtTiifl ictt i t iIt iitdiekl tint t kut
2 D1 02 D2 DVI 194 1
V00s11
2 6V1
1 V1
71-17-3llltl-12-i7f-lt-t124-u-iTI-H.S71-43-1lllil-ll-311I-7S-I73-13-1lll-ll-ISJ1-7M117-11-47T-34-Stll-ll-Jlll-M-7111-41-1111-42-5
1,1-DiekUitprtputt t i i s - l ,3-Di tkI0reptDi in tTricklervttkiKl i fcl lBOCklBtt l t tkal l
l , l , l -Ti ichlet«i tki i iItiititc i i - l , 3 -Dick Io ia f topcnil-CkltrottkyUiiyittfcKIrate fo ra4-Httkfi-i-ptiUioitI -It I ail II
Tttrackltrtt tktit1,1,2,2-TttratkIirutkiitTtlititCklttiktiiiititkf ikciitiiStyrtiiTttil Iflnti
0DVBDQ0
11 D0
1 IJ[2 V
I1
2 IJVVD0
DtU Itptrttif Qitl ifUri
If tkt molt If i f i l i t f inti i tkti ti MCI! t« titl i i i t , r tyo i t tkt f t l i t .
Utftcitt i eiKptntf v» atilfiH dr lit lit tftttetii*. I t f t t i tkt•iiiia ttttetlti l i i it fit tkt fuplt v i tk Ui Q ( i f . l I D ) Iift4•i itetfsitf et i t t i t . / l i l i t l i i ictltt. (Tkii if itt nciiutilytkt intiaiit tkttctiti l i m i t . ) Ht (ictioti ikeild ttit: V-
•«> «iil|iH (ir bit lit Ittictit . Tki laku is tktitt intkU tftttctUi l int fit tki itmplt.
J:Itf lcit if u t*timitt< ?«Iit. Tkit f ltf i f l f l< *itktt vktiii lima til) * eiittitnttii (tr tnUtlfilf iditil i i i
a 1:1 r»M*<* tf «•«•*' •' •*«« tki Uitkt friinei tf a e»find tk*t uit> tkt i l t i t i f i c t t io i
e r i t t r i a kit tkt rit i tt ii 1m tkai tkt *t*titi*i ( t ttct it i l i i i tir t i t tr tkn itrt (t|, 1IJ) . If lint if ritttcti i i ii U til aid a
C:Tkii tlif i p p l i i f ti ytitiei't Miuittrs vhiic tki i<tati(ict-titi vif ciifiiatd kf CC/HS, Slitlt cetpoint piittcidn)»II•f/il ti tkt liial ntriet ikailri bt e»»(ir»i< hr "^
Tkii flii is in* viti aialftt Is ftii< ii kUik is wtil as a•ABpIt. It iiiititti ttssiklt/srtkiklt H*it coituintiia tndmm tkt lati is*t tt till apsttpriatt «ctiti.OTHE1:Olktr (Ufi »< f t i t i t t ts UT I* ti^iittd ti i r sp tr ly <t(iittkt rmlti If titi, tit; «i>t kt f i l l r d t i e r ikcd aid sickftseuptit i itttckttf tt tkt data imatf
lit
L a b o r a t o r y NaaeCase No: 7351
ENVIRODYNE Nuabtr
Otganici Ana Iyf i § Data Sheet(Page 2)
Seaivolatile Compounds
e E i t r a c t e d / P r e p a r e d : 4 - 2 4 - 8 7e A n a l y z e d : 7 - 2 - 8 7c / D i l F a c t o r : 1cent M o i s t u r e ( d e c a n t e d ) : 1 4 . 7 8
CIS Mi:
111-93-1 fkinel111-44-4 k i i - ( l - C k l o t » i t k f I ) t t k i r93-37-1 1 -Ckloropkt io I341-71-1 l ,3 -0 iekl*t*kt i t t»lli-44-7 1,4-DicklflroktBitBi111-31-4 Inifl i lcoktl93-31-t 1,1-Dickltieknttit93-41-7 2 -Ki tk f lpkt io l39431-32-f k i i - {2 -CkI«ro i f*pro i r l ) i tk t r114-44-5 4-HitkjIpktiol411-44-7 M-itttoft-Di- i -propylui i t47-71-1 ImcklitMtkait98-f3-l Mitrtkiai t ie71-39-1 I i tpkoiDBi11-73-3 2-Nittipkttot113-47-f 2 ,4 -DtMtk i t fkne l45-15-1 leetoic JLciit l l - f l - 1 k i i - <CkIo t f l i t k f l i y )H i tkaM121-13-2 2 , 4 -D i ckIoropk iw l111-12-1 l , l , 4 -Tr i ck l i r»k<Bi i i e91-20-3 Napktkalin114-47-1 4-Ckloruii l iBi17-41-3 BiiackUr*kitadi»t39-31-7 4-CkIir i - l -MtkrIpkeBol91-37-4 2-Hitkyl iapktkaI iBi77-47-4 I i iackI«r*tTcl tpeBta<iue11-14-2 1,1,4-TrickUrepkift i l93-93-4 1.4.3-TiiekIit ipki i«l91-31-7 2-CkIir»apktkaUBtH-74-4 2 -Ki t r0a i f l iB t131-11-1 D in tky l fktkal i t iIl l -f4-l le iBaptkyli i i99-19-1 3 -Ni t r0aBtI ia t
SepCent
tfltq
Ifl V3fO QIfl 9191 9391 9191 9191 9Ifl 9Ifl 9Ifl 9Ifl 9391 9191 9Ifl V191 9191 9If l l 9191 9191 9Ifl 9Ifl 9191 9191 9191 9Ifl 0Ifl 9Ifl 91911 DIfl 9Ifll 0Ifl 9Ifl 91911 0
F u n n e l E i tin . L i q . -Li
CIS No:
11-12-951-11-5111-12-7132-44-9111-14-24K-2I-214-44-17115-71-314-73-7111-11-4334-32-114-11-4111-53-1111-74-117-14-3IS-l l- l111-11-714-74-2214-44-1119-11-113-41-791-94-134-33-1117-11-7111-11-9117-14-13 IS - f f - 2117-11-9SI-11-1191-19-351-71-1191-14-2
r a c t i o n : YES [N&<; < c i r c l eq. Eit . : YES Q K p f c i r c l e
Ituapktkuil , 4 - D i B i t t o e k i B « I4-Kitr»tk»«lOiktaitf iraa2.4-Dtiitittaliiae1 ,4 -DiHi tr i toUi i tSl i tky l pktkalaU4-CkUrepkiif I -pkcny l i tk i tFlierm4-Mit toaBiI i i i4,4-OiBitr0- l -Ritk rI ik»0II-aiti«i0i'itkiiy!amiit (1)4-lr0Bopk»yI-0kityl etket••iackl»r0ktaitatPeatackUrtpkitelfkiititkriiiUtkraciB*Dl-a-kityl pktki lat iriiitiitiiitFyriBil i t r l -k0Bt r l -pktkiUtel , r -DickI0t ik iBi i r i i t iIiiiadtiitkricmki i - (2 - t tkr [knr l ) ek tk<Ut<CkryctitDi-i- ietT l p h l k i l t t il i i f id l f l i t iaBtkiBil»it(k)f [tirutkutltni(«)iyriit *Ii<0ae(l l l l]-c4)|yr0i0DikiBi«(a .k)aBtkia»Biic i t tCfki lptr i l in
one )one )
igk;
3ft 9mi v1911 93ft 91ft 9Ifl 9191 93fl 8391 VI f l l 0I f l l 9391 9Ifl 93ft 9I f l l 9Ifl 0391 91411 1Ifl 03fl 03ft 9771 93ft 0451 13fl 03H 03ft 03fl 9391 0191 9191 93ft 9
(l)-Cannot bt itpirtttd (torn diphtnyIi,min«
FORM 1 ~ ,
Laboratory Narpe
Gate No "~
Organtes Analysis Data Shoot(Page 3)
Posticid«/PCB$
Concentration ( LowJ Medium (Circle One)/ ._ 9</ -
Date Extracted'Prepared ____o *\~1
Date Analyzed: ____ (~~ * ' • _
Cone/Oil Factor: _________f
GPC Cleanup SYe* ONo
Separatory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction OYes
mom<cmo
Percent Moisture (decanted)
CAS
319-84-63I9-8S-7319-86-858-89-976-44 -6
309-00-21024-57-3953-98-860-57-172-55-972-20-633213-6S-972-S4-81031-07-650-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111O96-82-5
Alph»-8HC
Beia-BHC
Defta-BHCGamma-BHC(UxJ*oelHeotachforAkJrm
NepiacWor EpoxideEndosulfan 10*eldrin4. 4--QOEEndrin
Endosurfan 04. 4'-OOOEndosuffan Svtfate4. 4-.ODT ^
M«tfK>«Y«hl<X
£ndrin KetooeChtordaneToup<t«rt«
Arocfor-1O16Aroctof-1221ArocIor-1232
AroclOf-1242
A/oclor-1248
ArocKH-1254
Aroc«x-l260
H*.o uIL.O tiIt.O tt
.- !(,.& U/£•£> UM.O «./4.O y/*»<0 *t
JTJt-O «..-0,0 a^3-<3 tt
1 *3?0 Uj-p,o UJ3-O K
r ^3^3 «/<.£>.£> U
JJ. «/tA^ U
JUo,£> U)tfO,o uite>.o uKA& u./£&& UI16.O U330.^ i/326.O Ut
oo
extract iojeacd (ut|
V = Volume of water enracted (ml)
W *• Weifftit of cample extracted (gl
V( * Vofume o< tocaf
orW.
7/8S
Orginics Anilfsif Diti Shit t(Pigt 1)
SiapIt Number: E
Libontory NIBC ENVIRODYNELib Sinplt ID No: 87973141StmpI* Hitrii: SOILDiti Rclcif• Aathoiind By:
Cis t No : 7351QC R t p o r t No: __C o n t r a c t No: __!____D » t t Siapl t R t c i i v e d :
V o l a t i 11 C o m p o u n d !
C o n c i n t r a t i o n : L O WD i t t E i t r i c t t d / P r t p i r c d :D i t c A n a l y n d : i -U-67C o n c / D i 1 F a c t o r : 1P t r c i n t K o i s t u r t ( n o t d t c a n t t d ) 1 5 . 2 ?
CIS Ho: ift?
74-17-374-13-973-I1-473-10-373-17-147-44-173-13-175-33-473-34-313(-il-347-44-3117-li-l71-73-371-33-431-13-3111-83-473-17-4
Ckl t iOMtkt i i 1Iratoiitktitf i i f i Ck l t r id i 1Chloret tk in iHitkTlm C k l t r i d tUeteiiCirkoi D i i i l f i d i1,1-Dicklarai tht ic1 ,1 -Dickl ir i t tktEitr»i- l . l -DiekltrottkiitCkUrtfirm1.2-Ditklirutkiit1- lit 11 lit1.1,1-TrickltriitkinCirkft Tituekliridif i i f i Icit ittIr »o< i ck 1 ir »t t ktit
2 02 0i a1 V21 1U 10u009V
2 fVV
12 0( 0
CIS Ki:••••••mi
71-17-3
igkq
79-11-4124-41-177-11-371-43-2
111-73-173-13-2111-11-371-71-127-11-7Y-34-3111-11-in-»i-1IC-41-111-42-
1,1-Dieklutf i tpi t tt ra i f - l ,3 -DickTuefcUi.ttktii
1,1.1-TrickleteitktiiItitin
Iroieform
1-IisiioitTitrickUrittktitl , l . l ,2-Tit t«ckl»i t t tk»iTilttn
Tittl
4 U4 V4 04 0i U4 04 V11 U4 D12 011 I
0I
V0t0
DiU leportitf
C:ttlUI:If tki rtin It is t filit iriittr tkia «r Mitt ti tkt l ittetitiI t i i t . nptrt tkt flUt.B:Iidtettei cMfttid vit »tlfit< (tr kit itt dtttet id. l iftrt tki•inin Jt t i c t i t i lint (it tki (U|U v i tk tki V (19,110) kiitd•• itciftitj t i itnt. / l l l it i i i ittiii . (Tkif is itt ucMiiri lftkt iutrntit dittetlti l i m i t . ) Ti. (tttieti ikeiU mi 0-Ciueii< vis »4lfs«< fir kit lit dt t ic t id . Tkt mktr if tki•iiiin t t t i i iakl i dt t tct ioi liiit fir tki iiafli.J:Ulictttf » t it imittd f«Ui. Tkis fU( if •<•< t i tk ir vkii•ftiutiif « ciictvtntiii fir t i i t i t iT iI f i ln t l f i t l cit^endivkiri t 1:1 rifptii! is tssntd ir vkii tki uts siietril dittt idieit id tki iritiici if a e»iond tkt t Btiti tki td i i t t f i e i t i o ie i i t ir i* kit tki rtf i l t is Iifi tUi tki f p t c i f i i d di t tct i t i liiit kitf i c i t tr tkn nci ( i f , 1 I J ) . If l int if d i t i c t i e t is II igi »d i
Tkis (Uf tpptits ti f t s t i e id t ftruttirf wktrt tbt i d t i t i f i E i -till vtt cttfimd If CUK5, Si ig l i ctipeint i t i t i c idts ) - ! !M/il U tki f inl utricl ikt i ld ki eitftmd k? CC/KSI:nil f l« | if isttf wkit mlftt Is ftnd ti klt ik is Mil is i•u|li It i idicitis p i f s i k l i / p r i i t k l t kUit eiituiittiii indvain tki d«ti iitr ti till i tpretri it i ict i t t .OTHE1:Otktr f l i q f nd f i it i it i i uj kt riff.iirtd ti prop t r l r dif i i itkt rts i i ts . If istd. tkty list it ( i l l y d i t cr ik id nd lickdner ip t io i i t t icktd ti tki diti SVBBIIT r i p e r t .
L a b o r a t o r y NameCase No: 7 351
ENVIRODYNE Sa»ple Nanber
Organics Ant Iff is Data Sheet(Page 2)
Sealvolatile CoBpoands
e Ei t r a c t e d / P t t p a r e d : 4 - 2 4 - 8 ? S e p . Funne l E i t r a c t i o n : YES Q^a c i r c 1 e o n e )e A n a l y i e d : 7 - 2 - 8 7 C o n t i n . L i q . - L i q . E i t . : YES Q^) t c i r c 1 e o n e )c / D i l F a c t o r : 1cen t M o i s t u r e ( d e c a n t e d ) : 1 5 . 2 9
CIS Ni:
111-93-1111-44-495-37-1541-73-1104-44-1lll-Sl-(93-30-193-41-739131-31-910(-44-3(ll-(4-7(7-72-191-93-371-39-111-75-31IJ-47-9(3-15-1111-91-1121-13-1lll-ll-l91-28-3lli-47-l17-11-339-51-791-37-477-47-411-04-295-93-491-51-714-74-4131-11-120l-9(-l99-19-2
PhtBOl
bt i - ( 2 -a i e rB i tkr l ) i tk i r2 -Ck lBrBBkea t l1 ,3-DUfcUrtttBiiBt1,4-OicMfrBktBieBtItiifl lleokel1 , 1 -D i eh l e rabBBiBB il - N i t k y [ p h > B B lb i s - ( 2 - C k I e t e t f 0 p r 6 i f l ) t t k i [4-Ktthf lpktBtlK-BitrBie-Di-B-prop- luiBBI i i ickUrtttkiBilitrobeiiiieI l B p k B C B B C1-XitropkiBol2 ,4-Di i i tkYlpk«BlItBteic Ac idbi i - (Ckl troBtke iY>Retkaae2,4-Oicb.{*ropk*Bol1,1,4-Tt ithUribmiiiMapktba l tBe4-CkUrBaBiI iBeiBiaeklBrobetadi iBi4 -CklBrt -3 -Mtk T lpkBBi l2-K*tkf lBipktkaItBtItfacklBrecfcUBflBtai ' ieBe2 ,4 .4 -TrUkl*rf lBktBel2 , i ,3-Trickl«tBpbiBi lI-CklcroiMitkiUit2-Rl troaBi l iBeDiBt thy l pitkalat iIc tBapthr l iBB3-Ni troa i i l iBe
•4kg
391 D391 V391 0391 V391 V398 9390 0190 U190 D198 1190 5191 1190 V198 1398 tf198 11910 V198 1398 D398 V398 0391 V190 U198 B390 0191 8390 V1988 D398 U1908 D190 V391 01900 V
CIS KB:
13-31-931-11-3188-82-7131-14-9121-14-2401-20-214-11-27803-72-311-71-7180-01-4334*32-114-38-4101-55-3110-74-117-04-313-81-1120-12-704-74-1184-44-8129-08-813-18-791-94-154-33-3117-11-7211-11-9117-14-0285-99-2287-01-958-12-1193-39-553-71-1191-24-1
IctBapktkBB*2 , 4 - D l B i t i « p k i B o l4-Kitrtpfc iB»lDibtt iof i t i i2 , 4 - O i B i t r c t i l B i a e2 , 4 -D lB l t r t tB l t iBeD i i t h f l p b t k t l a t B4 -CklBrBpkcBf l -pk tBf 1 B t k i rrinriBe4-Ri t iBaBiUBi4 .4-DiBitr»-2- fUtkTlpkeB*II-BitrBieiipktBjluiBt (1)4-lrtMpkiBfI-pkiBf 1 etkstIiitcbliribtiKBiPiBtiekl i tefkiBiIPkiBaBtkriBiiBtkrtCIBt
ni-B-kityl p k t k t l a t eTI ior tBth iBtPfitifll a t T l - b i B i T l - p k t k a l a t B3 ,3 ' -D i :kUrob in i idn«l i i iadl iBtktictt ib i s - a - C t k T l k i i r l l p k t k i l i t iCkrfitBiDl-B-tctf l p k t k a l a t el e B i B ( k ) ( I i i r < i t k B B >l iBt«(t)f InrutktBtleBiB(a)efi*BtlB<tBt( l , l ,3 -Cf Ippttt
01ktB iB(a ,k )aBtkracBBtl iBiB(gkUp»r;IeBe
•in391 D1911 U1910 U3TI UIfl 0390 13fl 03U U391 01911 01910 V191 0390 V3(1 V1908 03*1 0191 ?211 BJ3ft 0311 U311 U711 9311 tf311 I311 D111 03TI 0311 D310 0311 D310 U318 9
<l)-Cannot be separated from diphenylamina
FORM 1
Laboratory
No
Organtes Analysis Data Sheet(Page 3]
Cooccntration: tow Medium
Date Extracted 'Prepared:
Date Analyzed: ?7" ^
Cooc/Dil Factor: _____1
Pasticide/PCBs(Grcle One) GPC Cleanup GTYes ONo
(/ ^7f!"*/>_____ Separatory Funnel Extraction \
Continuous Liquid - Liquid Extraction OYes *^
Percent Moisture (decanted)
CAS ug/l<xf»g/K£Numb«r . (CircleTJKe)319-84-6319-85-7319-86-856 89-976-44-8309-00-21024-57-3959-98-86O-S7-172-55.9*72-20-833213-65-972-54-81031-O7-850-29-372-43-553434-70-557-74-98001-35-212674-11-21UO4-28-211141-16-553469-21 -91 2672-29-6U097-69-1110S6-82-S
Alpha -BHCBetJ-BHCD*Ua-BHCGamma-BHC (Ltodar*)HeotacfiUxAldrtnNeptacntor EpoxideEndosulfan 1Dtetdrin4. 4' )OEEndrinEndosuKan 04. 4--OOOEndosutfan Sutfaie4. 4'-ODT ^MethORVCtUor
Endrin KeioneChlordan«ToxapheneAroc«<x-10l6Arocio*-1221A/octef-1232Arodof-1242A/ocl<x-1248Aroci<x-1254Afoct<x-l26O
Ho.O UtL.<y ILtC.O tL
.- /fc.O «i(,.o ait,.o u./t,.o utl>,C> U.
xf.o U-.• .o U3i.e> u.
1 i3tPO «JJ-o UJ3-0 Hja^3 «
/CA£> U.J3-& «/tAO «
JLJO. > U
Hrt.G UlLo.0 UKAA UIM£> U116.0 U.320.6 U33&.O U.
V- * Volume of exlrad «nf«cied (uf|
V * Volume at water extracted (m)|
W^ « Weight of camp(e extracted <g|
V. * Volume o4 total extract (ufj
orW.
7/es
Envirodyne Engineers^
O«y»mcx Analysis O*t» Sheet'(\
Tentatively W«ntif»«<J Compounds
CAS•C<m»e*«nlM«m«
4&kJu
TT
IT10,
cris.16.17.
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7LVOA
Organics Analysif Data Sheet<Pagt 1)
Samp It Number EM842 j>
Lab o r a t o r y Name: ENVIRODYNELab Sample ID No: 87003142Samp 1e Ka t r ii: SOILData Reltast Authoriitd By:
Cast No: 7351QC R e p o r t No:C o n t r a c t No: . • 70Date Sample Received
V o l a t i l e Compound!
Concent rat ion: LOVDate Eitracttd/Prtpartd:Date Analyied: 4-24-87Conc/Dil Factor: 1Percent Moisture (not decanted): 15.63
CIS No. CIS Mi: igtg
74-17-374-U-t73-11-473-IB-l7S-lf-247-14-173-13-173-33-473-34-313<-il-3i7-i*-3117-li-l7i-n-i71-33-434-21-S111-19-473-27-4
Caloroit thii t 1Itomomitkaairiifi ckiotidi iCkleioitkaiiHitkyUBi Ckl i t id ilettiaiCtriea O i i i l f i d il,l-Bickl»rBitkni1,1-DieklBriitkatit tatf- l ,2-DickUmtkniCklindrm1.2-Ditklitiitkaat2 -lit ami1,1,1-TiickliriitkaieCaibn Tit tacklocidiTiiyl leitatiItHodteklatimitkaii
2 51 02 Q2 011 141 1000VIff
2 91V
12 01 D
7I-I7-S 1 ,1 -Dick l i tap ioptn11141-ll-i t ra i i - l , 3 -DickIeroFton i i7t-ll-t Tiiekloititkin124-41-1 Dib iomocklotomithai t7T-II-5 1 ,1 ,2 -Tt ick loto i tkan71-43-1 IHIIBI1IK1-I1-S c i i - l , 3 - I>UkI i top toptn i
001V0V0
111-73-1 : -CiUro.t iT [ f i iT ! . thtr 12 Q75-IS-l ItiBifirm i V111-11-5tl-TI-127-11-7*-34-3111-11-l l l - f l*111-41-141-41-
4-HitkTl-l-piitai«n 11 02-Iiiaini 12 ITitiacklirntkiii i V1.1 ,2 ,2-TitracklMBitkan < 1Til mi / i jjCklltlbllllll < 0ItkilkniHi * VStytni i VTital I f l i iM i 0
Data Itpittiig Qialifitrt
TlUt:If tki milt ii a «!•• iriatti tkai it intl ti tkil im i t , ttpit tkt ralBi.0:tidicati* citfoiid war ualfsil fir lit lit ditittttf. Iipirt tkimien tf i t ict i i i l imi t ftr tki famil* vitk tki 0 ( i f , 110) landIB iieeiiatf eiiciit./iltitiii actlei. (Tkii is lit ittmaiilftki intrant ditietiu l i m i t . ) Tki ftetnti ikoili i\\i. 0-Ciii«i»4 wai aialysid (it kit lit dititt*4. Tki inkir ii tki•into t t ta i i ak l i ditictii i I t i i t ftr tki laapii.J:Udicatif 11 iitimatii f i ln Tkii (laf Is tiitf l i tkit vkitifttmatiif i ci ictittatioi (»r tiititivilf Uutifii< ciap«nif _ "vkin a 1:1 iiitoin if aisaid it vfeii tki Ban iMttiil latitii'icatii' tki iriinei if > ciifend tkit Miti tki 14itti[itttiait r i l i rU kit tki nsilt it Ini tkai tki i f t e i l i t i <iticti» l im i t•r t i t tr tin ins ( f i . 1 I J ) . IE l im i t •! i iUctioi ti II i|I aid a
C:Tkii fla| afiliu ti inticidi iiruitiri vktn tki idnt i f ica-tin vai eitftrmid kf CC/KS. S i i f l i cempenit r c i t i e i d i i l ' l li|/il ii tki l i t i l uttact iknld hi cnfirmid kf &C/HSI:Tkii fla« ii tsid vkii aialfti If find ia link if mil *• afaajli. It liditatit ufiikli/iiibtvli klail ctatuiiatin tndvatii tki data tut ti tafci i|ttitriati actiei.OTHEI:Otkir fla|f aid (ntiitif w| >i riqund ti M o M f ' T <i ( t»tki f i i i l t t . It ind, tkif nit ki t i l l r d iscr ib id aid tickdi ic i t i t in attackid to tki data inmaif r i i o t t .
kit
laborat or y NtmeCist No 7351
ENVIRODYNE Saiplt Number
Organici Analyiii Data Sheet(Page 2)
S«ni TO I a t i I • Compounds
e E x t r a c t e d / P r e p a r e d : . - 2 4 - 8 7e A n a l y i e d : 7-2-87c / D i l F a c t o r : tcen t M o i s t u r e ( d e c a n t e d ) : 1 3 . 4 3
CIS N>:
101-73-1111-44-475-57-1341-73-1104-44-7100-31-473-30-173-41-737431-32-7114-44-3411-44-747-72-1TO-13-371-Jt-l11-73-3105-47-74S-I3-I111-71-1121-13-1110-01-111-24-3114-47-017-41-337-30-711-37-477-47-401-04-173-73-471-31-700-74-4131-11-3101-74-177-07-2
Fhiflolk i<- ( l -C . l» [» iUf I )» tk*r1-CkloropkiBoIl ,3-. iekI«rabiBiuil ,4 -DichIorobt i ie_ iImyl ll tokel1,2-DichIatcbiBien2 - K i t h y l f l k t i o Ik i i - ( 2 - C U o r f l i f t f t r e i y Hi the r4-Hitkylpkt iBlK-iitr»sa-Dl-B-ptBpylaiiiileiickliiottkui•ItribeisiBiIsiakacBBcl-Klttopkmll ,<-Di«t-y!pktioIliBsoic Acidb i s - (Ckluo i tkBiy>Ht tkau2 ,4 -Dlcb . lB iBpki io l1 ,1,4-TrUkUrt.iiitnMipbUlltn4-CkUrttiiIii*Hincklotebat idi iBi4-C_lor»-3-«tkylpk«ol2-Kitkylupkt. i l ineIt i iekloracTcUpttUditf t t2 ,4 ,4 -Tr iekIe iopk iBs l1, ' ,3-TricBliropkcBoll-CkletB.ipktkiliBff2- l i t rBaai l iBiD i M t h y l pktki l t teIciBiptkylm3-KittBti i l i ie
S*p F u n n e l E i t r a c t i o n : YES (N£/< c i r c 1 e o n e )C o n t i n . L i q . - L i q . E i t . : Y E S QNJX ( c i r c l e o n e )
•9H
371 0310 V310 037C Q370 0310 0310 9310 0370 U371 V371 V310 V370 0370 I370 9370 91700 9310 1310 9310 9370 9374 9371 9370 9310 9310 9371 01700 0170 91701 9370 9370 91104 9
CIS No:
13-31-131-21-3100-02-7131-44-7121-14-2404-10-114-44-27005-72-314-73-7100-01-4314-32-114-30-4101-35-3111-74-117-14-315-01-0110-12-7H-74-1104-44-4111-40-0IS-44-7fl-74-154-33-3117-11-7111-01-1117-44-0243-77-1207-04-730-32-4173-31-533-70-3171-24-1
ICtBlpktklBI
1 ,4 -DiBi t r epk i io l4-Xi t r tpht i t lDi i t i i t f i r tB1 , 4 - O i i i t r o t t l B f B i2 ,4 -Di i i t r e tB l i t t iD i i t k y l pk tk i l t t t4 - C k I o r « p k c i f 1-pkcByI i th t rriieciii4-Mitr**BiIii i<,4 -OtBi t r e -2 -Hi tky lpk»o lM-iitrtfli4ipkurlaiitc (1)4-lroB*phetyl-phiiyl i tktr
. IciacklfltBbflBiiBtFittickUitpkciaiPkentitkriie-itkraeiBBDi-B-bi ty l p k t k a l a t iriioititktBify t iB*I t ty l -k i i iy l -pktk tUte3 ,3 ' -Dick l t tBb«Bi i l iB it i i t t<«)ti tkncti tb i f - ( 2 - C l k T [ B « i y U p k t k t i i ( *CkryteieOi-i-«ctyl p h t k t U t il - i t i tbXliirai tkiBiIl*It(t)f I l t fUtkt l t
liBiedlpytiiilBdiM(l , l ,3-cOpfrntoibitt*u,k)ii tk[iciBti t n« (gk i )p i iy t iBC
< q k g
310 911B4 0HOD U311 U310 9370 9374 9370 9374 D1701 91744 V374 Q374 9314 9
__U40 9/ soTI
1TTTT134 BJ370 9314 D310 9710 9310 9410 1374 D370 9314 9370 9314 9314 9370 9314 9
{1)-Cannot bt fiparattd Iro» diphcnylamin*
FORM 1
Case Mo
Organic; Anafyiis Data Shoot(Page 3)
Pesticide/PCBs
Concentration: (Low^ Medium (Circle One) GPC (— L - 74 "?-yOil* Fjrtracf*d/Pr*riar*rt U • * { -&/_ ^-^r
O*tf Anrntyrrd l^^-\/. r/wifi
f!ftnc/Dil Far-Tor- /
pfrr^ni Moicrurp (ri<*fjini*rf) _ /->.»
CASNumtw
319-84-6319 85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-9*72-20-S33213-65-972-54-fl1031-07-8[SO- 29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21 -912672-29-611097-69-111096-82-S
Aloha -BMC
8eia-8HC0«iia-6HCGamma -8HC (L'ndanet
HeptachlorAldfin
Kepiachhx EpoirieEndosutfan 1Oteldrin
4.4--OOEEndrtnEndosoHan fl4. 4--OOOEndosutfan SuH*ie4.4--ODT - *MethOKychlor
Eodrin KetoneChlordaneToiapfeeneArocfor-1016
A/octof-1221Arocioc-1232Afocio^-1242Afocio*-12-»8AroCl<K-1254
A<oc(o*-1260
^eanup CSYes C
a fory Funnel Ex-
luous Liquid - L
ug/lor£ig/Ka,(CircfiTjnc]
((P.O M./t . 0 fl
/^.O tL- /6.0 «
/6.O Uff,.0 «,/t.o «/l.O K
JW-O U..- .o «.JEa.d «.*33^J U3$>0 UJ3^5 tt.
•33-<& tl1 1 d. I/.
JJ. > «
/tA^> U
330.& W
/ .O tt
/ d. > «
^d,-0 «/ 5u5 UM6.O «.J3d, tt3^3. 0 U.
V
V- % Volume of ectraci injected (u(J
V * Volume of water extracted (ml)
W( * Wfrigtn of cample extracted (g)
Vc « Volume «4 total extracs Ml
orW. . C 1 -Xl--'
• Of III 1 7/8S
Envirodyne Engineers
Ai\*tr£t£ Oat* Sheet
«~vUN~mb«
Tentatively Identified Compounds
CAS
CT
z 7-7^-C.
7..
2/t«*
10.n.
S3HM16..
19. 3CLs:
2*.
27.,
in
n
r *
Ocganics Analysis Data Sheet(Page 1) !--
Sample Number: EK863
J4bLabor at ory Name:Lib Sample ID NoSamp 1 • Mat r ii :
ENVIRODYNE87003143SOIL
Datt Release Authorised By
Cast No: 7 3 5 1QC R e p o r t No:C o n t r a c t No: {&j?"*D a t t S a m p l e R e c e i v e d
~ 70
Volat iIt Compounds
Concent rit i on: LOWDatt E x t r a c t e d / P r e p a r e d :Datt Analysed: 4-26-87Conc/Di1 Fact or: 1Ptrctnt Moi s t u r e (not decanted) 1 7 . 3 4
CIS Me:
74-17-374-13-t75-11-475-10-375-H-247-44-175-13-175-35-473-34-3ISi-il-S(7-ii-I1I7-U-271-tJ-J71-5S-431-23-5111-03-473-27-4
Ckliromitkaii 1IteieittkiniViiTl Cklnidi 1CklereetkaaeKetkTliti CkierideIceteteCatkoi Difilfide1,1-DickioreitkiBcl.l-Dickletietkaietrais-l,2'DickIiiiitkiiiCklirefera1,2-Oieklereetkaie2-letaiite1.1.1-TcieklereetkaiiCatket TitrackleiideTiifl Acetatelt»edlckleie»etkaia
2 V2 02 V1 V31 144 15QBVI12 0V1
12 VI V
CIS He:
71-17-5l l l f l - l l -<71-11-4124-41-171-ll-S71-43-2lllil-ll-5111-75-173-23-1lll-ll-lSfl-71-4117-11-47J-I4-S1II-II-3lll-M-7111-41-4111-42-5
•fl
l ,2-DickI«r t i i ip i i ittaii-l.i-OickleiiiioH"TriekleriitkiuDikriioekliieutkaii1,1.1-TrickIereetkaiileitiiieii-1 , J -DtckUroi topt t t2 -CkIen i tk r ln iy I i tk i tli*mefera4-Hitkyl-2-piitami2-biaieiiTitraeklireitkiie1,1,1.1-TitracklereetkaiiTel • HICklirikett*iittkyikeisiieStfteieTetal Ifltin
H
VVVVu0a
i iV
12 1\ 11IDI9Ua
Dili lipittiif Q i a l i f l e t f
VaLUI:If tki itMlt ii a tain friatu tkii it «<nl ti tki <ttieti»liiit, fipott tfci tain.I:f i i ic i t t f eaii on 4 was aialf"' («r lit lit 4eticti4. Itpttt tkt•inin «it*etl» l int (ii tit lampli witk tki I df . l lU) lisidei iteifsatr c»c»t./41Ittiit actlti . (Tlii if let iictfianlftkt i«ttn«it i t t ie l iM lint ) Tkt dotiiti ikoi i i rud 0-C»Mpiii< was aialTi*4 (tr kit nt i i t ic l td. Tie tnkti ti tkaBitiin a t ta i iak l i r f i t ie t io i lint fir tki taapli.
Iiiicitu ii nHutid filn nit f l a g is •••* i l tk i t whettitiiatiti a eeteiitratiet Iir tettiUulf i € i t t i ( U 4vkiie a 1:1 iistotse is aisaed et wket tki iaii iiicttal lataitUeita* tke irintci ef a ciiteiid tk i t leitf tki i l e i t i f i ea t l o tc t i t i r ia kit tki unit Is Im tkai tke > M c i f i i 4 let ict i i t l intI t iat ir tkai mi ( i f , 1 IJ ) . If l in t ef 4it iet i» ii II til aid t
C:Tkit flaf apilin te p e s t i c i d e inuttdi wken tki idntifiei-tlei was cotfirud k| CC/RS. Sitale cimpaiett i*ftfcides)»!!tf/il it tke fital uttact ikield ke citfirted kf CC/KSI: -Tkis flaf ii tied wkit atalfti Ii fend it klitk at will it amill It itdicates piiitkli/icikikli klail ciitaiiittiii udwarn tki data eiic ti taki a p p t i p r i i t e ictiai.OTHH:Otket flaff aid (eettitit ma; ke teqtited te proiitly difititke tesiitfl. If end, tkiy »it ke I i i l f deictiktd aid tickdeieiiptiet attacked ti tke data traitT upott.
kit
Labor& t ory Nine:Cast No: 7351
ENVIRODYNE Simple Number: EM84
Organic* Analysis Data Shttt(Ptgt 2)
Seftivolitil* Compound!
t E i t r a c t e d / P r e p a r e d : 4 -24 -87t A n a l y x e d : 7 - 2 - 6 ?: / D i I F a c t o r : 1c e n t M o i s t u r e ( d e c a n t e d ) : 1 7 . 3 4
CIS N»:
101-95-Z111-44-493-37-1541-71-1114-44-7110-Sl-i95-50-19S-4I-73f43l-3Z-9114-14-3•21-44-747-72-191-95-371-39-111-75-5115-47-945-13-1111-M-liii-n-i120-12-191-Z8-3104-47-117-41-339-51-791-37-477-47-4ll-Oi-Z93-93-4Jl-31-711-71-1131-11-3ZII-94-199-19-2
fhlBOlki i - (2-CUomtk?n«t fc t t2-Ckloropketol1,3-DickIarobeiti ie1,1-Qieklflrokentenileityl Ucokai1.2-DiekIerobeBitBe2 - K i t k y l f k e i o Ib i i - ( Z - C k I o r « i i c p r o p f I ) e t k i r4-Hitkj l iki i i IM-iitr«o-Di-i-irotyIi«iieItittaliMttkiBiRitr«b«BiiBtIitikoioii2-KitropieMl1,1-OimttkylphiBolItncic lci<k i i - (Ck lo io« tk» i j ) l f» tk4«Z,1-DickUropkeieII , l ,4 -Tr ick l i r»b«i i«a»Kipktfc i l tn1-Cklore»iliieKeiaekler ibst idi i ie1-CkIore-l- i t tkyIpkii t lZ-Rt tky l i ipb tk i l en iEtiachlir iCTcIapCBUfl ' i tBiZ,1 ,4-Tr ieklor«fhtBiI2,4.3-TriekIiropkiBOl2-CkloroiapklhaliBi -2-Mi t re iBi l iBtDimethyl y k t k a l a t eIciBiptkyliBi3-Mittitiiltii
Sep .C e n t
•III
401 9111 9110 9101 9400 9100 Q111 9401 9401 9411 9111 9401 9111 9400 9401 9401 91901 9411 9401 9400 9400 9410 1411 9400 9400 9401 9411 91910 9400 01900 9401 9401 91901 9
F u n n e l E i t r a c t i o n : YES (JiG^ c i r c Iin. L i q . - L i q . E i t . : YES ( N O j ( c i r c ]
US Me:
13-32-951-ZI-3111-12-713Z-44-9111-14-1414-10-114-44-27015-72-314-73-7111-11-4534-32-1U-30-4101-53-1HI-74-1I7-I4-S15-11-1111-11-711-74-2104-44-01Z9-II-013-41-791-94-154-55-3117-11-7211-11-9117-14-0ZI5-f9-ZZI7-OI-93I-JI-I193-39-333-71-1191-14-2
-
IcciapktkiBiZ . I -Qi i i tMfk t io l4-Nitropbti«IOibiiiedraiZ,4-DiiitriteIteii1,4-DiBit r i t i InuD i i t k y l pk tk i l a te4 - C k I e r a p k t t f l - p k n y l i tk t rFlttllBt
4-litreaBiIiii1,4-OiBitre-Z-RetkyIpkiBtIR-iitr»iidi|hiif luiBe (1>l-lromepkeiyl-fkii;! etket•iiackliMbmit*FtiticklirtiknelPkiiiitkniiUtkraeeBeBi-i-bityl p k t k a l a t iFlitnitktiiPyriBiI t t r l - b i B t f l - f k t k a U t f fl ,3 ' -DltkU(«biat idi ieleise(4}aitfcracitel i i - (Z-E tky lke iy t ) ik tk iUt iCkryieBiOi-i-ictyl i k t k a l a t elllll(lt(ll(Tll thillIiBtefktf IiirutkutleBit(a)fyriieIi4»«(t,l.l-cd>pT"ieBikiiiid.klaitkiictiiItiii{|ki)ptrytiii
e one )I e one >
t f l t j
111 9I f l l 9I f l l 9111 Q401 9111 9111 9111 Q111 91911 DIfll D111 9110 9111 9I f lO 9
OH)401 9141 BJIII 9lie 9401 DIII 0111 9til 1ni y >
1 11 A J111 9111 0111 9410 9401 0111 0
<I)-Cannot b« tepartted fiom diphtnylamin*
FORM I
No
Organic* Analysts Data Shoot(Page 3)
Pcsticide/PCBs
Concentration. ( LowJ Medium
Date Extracted'Prepared ____£_T
Date Analyzed: ____/""•("" V/.
Cone/Oil Factor: I_______
(Grde OneJ GPC Cleanup C3^es ONo
Separatory Funnel Extraction OYes
Continuous Liquid - Liquid Extraction
-nr>(SI
Percent Moisture (decanted)
CAS
319-84-6319-85-7
319-86-858-89-976-44-8309-00-21024-57-3959-98-660-57-172-55-972-20-833213-65-972-54-fi1031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53469-21 -912672-29-611097-69-111096-82-5
Alpha -BMCBeia-BHC
Oeita-BMCGamma-BHC (LtndjnelHeptachtorAJdnnHeptacnlor £po«id«Endosutfan 1Oieldrin4. 4--OOEEndrinEndosuHjn 0
4. 4'-DDOEndosutfan Sutfate4. 4'-DOT *MetfwxvctUorEndrin KetoneChlordaneTotapneneA/octor-1016
A/octor-1221Aroctor-1232A/odor-1242
A/ockx-1248
A/ockK-1254Arod<x-I260
ft,.0 U./L.O MIL.O H
., /t,,o atC-O Uit,.o u./(nO U.tL.Q t*.
J3-0 U-.-o.o ajjj.d U.
' *33^> M.XP,o 14.32-0 «
" ja^> «!(.£>.£> U
JS.O «iu>,o Ujad. ult&,& ull£>.£> U
&£.& U/£O.& UIL6.O UJ2d. U3ZO.O tjL
V( * Volume of extract infected (uf|
V * Volume o* water eAracied (ml)
W( * Weight o* campfe extracted (gl
V( * Volume of lot*! extract (ut)
7/85
Orginici Analysis Data Shift(Page 1)
Laboratory Name: ENVIRODYNELab Si up It ID No: B7003H4Simple M a t r i i : SOILData Reltast Aathociitd By:
Case No: 7351QC Repor t No:Contract No: _____Datt Sample Rece ifed
Volatile Compounds
Concent rat i on: LOWDate E i t r a c t e d / P r t p a r e d :Date Analyzed: 4-24-87Cenc/DU Factor: 1Percent M o i s t u r e (not decanted) 22 ?3
-no
Simplf Numbtr: EM864:rn:OJ COm-o
oo
CIS No: •fkf CIS Mo tgkq
74-17-374-13-f73-11-475-00-373-lf-I»7-«4-l73-13-073-33-473-34-315t-iO-5i7~ii-l117-01-27M3-371-33-*34*13-3111-13-473-M-4
Ckliromitk»e 1Irotomttktni 1Tiiyl Ckl i r id i 1Cklonitkaai 1Rithyl i ie C k l i r i d iicitoaeCarboa D t s i l f i d el, l-Dickloriitli»i1,1-Dicklirietktiitr»f-l,2-DickliroitkiiiC k l i r i f i r m1,1-Dieklirietkiii2-lit»«ie1.1,1-TrickliroetkaiiCarbon Tetuckloi ideTiiyl acetateI r imodickUi imi tk in
3 U3 D3 V] V41 104 I000aV•
3 D09
13 V1 0
7I-I7-SUOil-02-i7»-01-4114-40-17f-00-S71-43-:lflOil-01-Siie-73-i73-I3-Illl-tl-t3M-73-4117-11-471-34-3tll-ll-1110-10-7111-41-4111-42-5
1,1-DickIiieprepiietnn-l ,3-Bickloroprop«niTr i tk lo r i i tk tBiBibtomockloroutkiBe1,1,1-TrickIorntkiatIIBIIIIc i f f - l , 3 - D i e k l o r i p r o p » el -Ck lo t i i t ky l i i i f l i t k i rI romofon4-Hitkyl-l-putaaeii1-IeiaieiiTitraeklirutkiii1,1,2.2-Titrackliroitkii tTiluniCkleriktiimEtkf IktticnStfrneTlllI I f l lB t f
V00uV00
13 UU
11 93 1
nVD90V0
Dati Itportitq Qitlifitii
flLtrt:If tki resilt ii a ralie frutir tk» «r MDI! ti tki ditictittliiit, report tki Title.9:Iidicatis ttmpaiid vtf aBalyted (ir bit lit <ettcUd. leport tke•itiin dttictiii limit fir tke sample witk tki I (i|,UU) lased•i iicisstry eeiceit./diliti»i utioi. (Tkii it let ieci«f«iilrthe iutrncit ditictiia l i m i t . ) Hi feitnti ikiild rud: V-CoKfiHd vti itilftid fir kit lit dttictid. Tki aabir ii tke•ililts ittttiibl* delicti!! limit fir tki iimple.J:Indicate! » iitimi.tid valie. Tkit flaf ii lied iltker vkiieitimatiif i ceBctitratioi fir tutatirily i d i i t i f i i d cotiondivmiri i 1:1 retpoiie if aimed n "kti tke mait spictrtl ditalidleited tki presiBce if a etmpond tkat mutt tki idiitifieatioieritirti kit tki reult Ii lesi tk» tki ipieifiid ditictioi limit
C:Tki i (I»j ippliis ti |i>ticidi paruitirt wkcn tki i d e n t i f i e rtin vii ciifirmid by CC/KS. Siifli componit p i f t i c t d i i ) « l l•t/il ii tke fiaal eitrtet ikitld be ciitirmid by CC/KSI : . - . . - . . -.:_.Thii (Uf If tied vk» aiilyte it find ti bluk 11 well as aitipli. It tidteites ifistkli/irobtble blaik ciituiiitiiB ind•atBi tki ditt iser ti tike ipproitiite ictiiB.OTHU:Otker (lags ltd feotiotii miy be ri^iirid ti p i e p e r l y didiitki r e f i l l * . If icid, tkiy net bi f i l l y dner tb td iid tickdeicr ipt io i i t t ickid ti tke data inmiry r ip i t t .
bit
-n
L*bon t ory N«atCast N o : 7 3 5 1
ENVIRODYNE SiBplt Number: EM664
Organic* Ana Iyiif Dat a Shttt(Figt 2)
Stmi»o1 at iIt Compounds
e E i t n c t e d / P r e p a t e d : 6 - 2 4 - 8 7• A n a l y z e d : 7 - 2 - 87c / D i l F a c t o r : 1ctnt M o i s t u r e ( d e c a n t e d ) : 2 2
US Me:
101-93-1111-44-495-37-1341-73-1114-44-7111-31-493-31-193-41-739131-31-9114-44-3411-44-747-71-1H-93-171-Sf-t11-73-3119-47-945-15-1111-91-1111-13-1UI-II-1tl-20-3114-47-117-41-359-5B-791-37-477-47-411-14-293-93-191-31-711-74-4131-11-31BI-94-I99-*t-l
Fhuili i f -a-aionttkyhttkirl-Ckloropkei«l1 ,3-Dickl ir i f t i i t i i il ,4-DickIit»biit»Blinyl l lcaki ll ,Z-DickloE«biniu1-Ritkf Ipk iBo lk i f l - (Z -CkIe i o i i i p ropy I ) i t k i r4-HitkrlpkiialN-iitr«ii-Di-i-propTluinleiicklinetktiflIttl lklBSIM
IfitketuiZ-Kitttpk»«Il,4-OiHtky[yk*»lliBisie UHk iB - (CkIoro i tk i iT>Hc tk i»1 ,4 -D ickIaropk iBo l1,1,4-Ttickli i ibBitBitItpkthtllBI
4-Cklor i iBi l i t el incklartiBtidiiBi4-Cklirt-l-MtkTlpkinl1-ItitkTli ipktkiIi i iIii ickltricyclgpiitidiiii1.4 ,4-Trtekl irvpkei i l2 .4 ,3 -Tr ickI iMpkiBi l2-CkUr»ipktkiI»e2-l lttmilUiBiictkjl BktkiUtiactBiptkyli i i3 -Ki t ro iB i l iB t
S e p .Cont
. ? 3
«•>.431 V431 1431 B431 V43B B43B V43B V43ft B431 B431 043B B41B B111 V111 113B 0431 B1111 V431 B131 9431 B411 043B B431 B431 B43B 0431 V431 Bmi o
: _ 431 V -1111 V431 V431 B1111 B
F u n n e l E i t r a c t i o n : Y E S f m / t c i r c Ii n . L i q . - L i q . E i t . : YES7^ ) ( c i r c I
US Mo:
13-31-f31-1B-31IB-B1-713Z-44-9111-14-14B4-1I-114-44-17IIS-71-1B4-73-71IB-I1-4334-31-1B4-3I-4111-33-3111-74-117-14-3I3-B1-I111-11-7B4-74-11B4-44 -B129-IB-fl15-41-791-94-134-33-1117-11-7111-11-9117-14-11B5-T9-Z1I7-BI-I31-11-1193-39-333-71-1191-Z4-Z
IctBipktkcii1 ,4-Di i i tnpkiBoll-XitripkiioIBibtuofirii1 ,4 -D i i i t r i t o I i iB i1 ,4-Dl i i t i i toI i iuB i i t k y l pk tk i l i t i4-CkI»rcphiByI -pktsyI i t h e rFluriiB4-Kit i«t i l I i i t4 .*-Dit i t i t - I -Httkylpki i« ll - i i t iosidlfkBirluiBB t t )4-liBB»pkti.yl-pk»yl itknIiiieklitBbiiiiiiFtitickloteibiBolFkiiiatkriiBiitkrietuBi-i-bityl pk th i l i t iFllOraatktlt
FT milityl-tiBiTl-pktkilitt3 , 3 ' -D i tk l i i i b tB i i d iB iItiiidliitkuciiil i s - ( l -E tk j l k« i ynpk th iUdCkrfi iBtDi-i-tcly! pk tk i l i t il iB i i (k ) f l i i r i i tk ia il iB i i (k) l l t i r lit kmliin(i)pfriitI idi t«( l , l 13-ci '} iTriBiBikmid.kl i i tkrict i il i i i i (ok i )p irr l i i i
e one )e one )
iqi;
431 U1111 Ut i l l 0431 B431 B430 1411 Bue Q431 1mi Bmi B431 B411 f411 Bn i i B/nn
^3lT111 8J431 B411 B431 8Id B431 Bt!i 3J431 B431 B411 B411 B411 a431 B431 B411 B
(l)-Cannot be ttparattd from diphtnylamint
.-:" -T ":"-" -"-'FORH 1
Laboratory
Cate No
Ac..
Organtes Analysis Data Sheet(Page 3)
Concentration: (Low^) Medium (Crete One)
Date Extracted''Prepared: ____*L
Date Analyzed: '^~ -f \Z
Factor:
Pesticide/PCS s
GPC Oeanup QYes ONo
Separato/Y Funnel Extraction OYes
Continuous Liquid - Liquid Extraction OYes
(-0
Percent Moisture (decanted)
CAS uo./lorkg/Kg.Numb** . (CircfiTUne)
319-84-6319-8S-7
319-86-858-89-976-44-8309-00-21024-57-3959-98460-S7-t72-SS-91
72-20-S33213-65-972-54-81031-07-$50-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53*69-21-912672-29-611097-69-111096-82-5
Alpha -BMC
Be»-BHCD«lta-8HCGamma-BHC (LtrxJjoelHcpt»ch»orAWftn
Keoiactikx EpoxideEndotulfan IOtddrin4. 4--ODEEndfirt
EndosuKan fl4. 4'-ODOEndocuffan SuHaie4. 4--OOT *Metttoxyctilor
Endrm KeioneChkKdarwToxjf>t>er>eArocfcx-1016A/ockx-1221Aroc«of-1232AfodOf-1242
Arcx^<X-1248
Aroc*oc-12S4
Ar odor -1260
Kr.O 0.
rL.f> ti1L.O IL
.- /6.0 U
&.o atf,.0 U./t-o «__/t.o KJ*.0 «.^5.0 U.
^a-o a' *aao «.
^P-o ttJ3^3 t<
f ja^) u/to.^> itJ-7-0 «
KrAO U
330.& U; >. u1^0.0 U&A.O UItAJ> UI16.O U.330.Q a320.O U.
V- * Volume of extract injected (ul|
V * Volume of water extracted (ml)
W « We«otn of cample extracted (gl
V( * Volume of total extract full
orW.
Form 1 7/8S
L a b o r a t o r y N a a t : E N V I R O D Y N EL a b S a m p l t I D N o : 8 7 0 0 3 1 4 3Saap 11 Mat r ii: SOILD a t a R t l c a i e A a t h o r i s t d B y :
Organic* Analfsis Data Shctt<Pagc 1) :--
N u B b t r : E M 0 6 5t -
Cai* No: 7351QC Report No:Cont ract No: _Datt Saaplt Rictivid:
Vo1 at iIt Compound!
Conctntration: LOWDatt E i t r a c t i d / P r t p a r t d :Datt Analyzed: 4-16-87Conc/Di1 Factor: 1Ptrctnt Moisturt (not decanttd) 1 1 8 6
CIS No: CiS No:
74-17-374-13-173-11-4T3-BI-373-lf-Z47-H-l73-tS-l75-33-473-34-313i-il-3i7-i*-J1I7-K-271-93-371-33-431-13-3101-43-473-27-4
Cklor iMotkaiolr»»otkaioTiiy! CkloridoCklireitkanHitkflii i C k l o r i d oAc it inCukei D i n l f l d i1 ,1-OickIoro i tkcBO1,1-QickIorootkaBOtraif-1.2-Dick1i[oitkiioCktor i forel .Z-Oieklir i i tkato2-litanit1,1,1-TrickIiriitkanCarkoi Ti t raeki i r id iTti f l icotatoIr iBidiekloroMtkaio
3 03 Q3 03 0U 1If 1Q0DIVI
3 0V9
13 QI 0
7I-I7-Slllil-12-i79-ll-i124-41-17f-ll-371-43-2iiiti-u-5iie-73-i75-25-2lll-ll-lSM-71-4127-11-471-34-3lll-ll-llll-M-7111-41-4111-42-3
1 ,2-Dick loroprop in <t r a i f - l , 3 - D i c k I o r i p t o p i n iTrickloriothoio IDikimcki or e« thin1,1 ,1-Tr ickIoiootk iBo 1lOBIOBO 4eii-1, J -Di t l l c r e i r ep in t (2-CkI f i ro i t i fU iBTl i t h i rIroBifon 14-NitkfI-l-piitaiin2-Htia»nTitrackloriotkoio1,1 ,2 ,2-Totracklor iotkaioTolioioCkloroonioiot t k f l k O I I O l OStyronTotal Xjl t i i i
V0VB900
3 09
3 13 09001
1 IJ00
Data I tport i i f Q i a l l f i i r i
ViLfft:If tkt r tin It it a Tilai inatir tkai ir cival t« tki dittctiiiItiit, riport tkt rain.V:Iiditatts cimpiud wn nalfiid Itr kit itt diticttd loport tki• iiiin dotoetioB Iii.it for tki ia»plt nitk tkt Q (of.HD) katid01 ueissarj eiicnt./dilitiii aetiii. (Tkii it itt iieiifarilftht iBitrniBt dotictiii liiit.l Tko ftoticto ikoill toad: 0-
vas iialyitd fat kit »t iitictid. no tabor It tkoitttiiiilc doUctioi limit for tki lutlo.
11 i ittutod talio. Tkli fU| if ind oi tki t vkii• coicntratioi fit Ui tat l fo l f Id t i t i f i i t eoifondf
wkno a 1:1 iiiioBio ii iiiaod or wfcti tko uis ipoctral dataitdlc<tt< tko ironic* of t coipoiid tkat Hiitt tko Id i i t i f ieat lo ic r i t i r i a kit tki milt ii Itn tkai tko t p i c i f i i d dotict i i i liiit
C:Tkif fltf ippUof to p i i t i e i d i paraiottri vkitc tko t d i n t i f i c i -tin "ii eiifirud if CC/HS. Siifli eoipeioit t t f t i c i d c i ) « l l•f/tl it tki fiial oitraet «k»ld ki cnfirnd kf CC/KSI: . _Tkif flag if ifid vfcot aialfto it find ii kltnt at mil n a•a>pli. It iidicatii lofiikli/priiibli klaik eiituiaatliB ndvarif tko data nor to taki a p p r i p r i a t i actin.OTHU:Otkir tla«f aid teitietii mty It tiqiittd to fitftilj difintki roiiltf. If n*4, tkif Kift ki f i l l y d o t e r i b o d aid ncfcdncriptlii attackid ti tki data inmair ripott.
lit
Labor at ory NamtCast No: 7351
ENVIRODYNE Saaplt Namb«r: EMB65
Organic* Analysis Data Shut(Fagt 2)
i1* Co»poandi
t E i t r a c t e d / P r t p i r e d : 6 - 2 4 - 8 7t A n a l y s e d : 7 -2 -87: / D i l F a c t o r : 1cent M o i s t u r e ( d e c a n t e d ) : 2 1 . 8 6
CIS No:
iii-ts-:111-44-4T3-37-I341-71-1114-44-Tuo-51-475-31-173-41-73f(3l -32-t104-44-3ill-44'747-71-1M-73-371-Sf-l11-75-5113-47-f43-13-1l l t - f l -1121-13-2UI-12-1fl -20-3114-47-117-41-33I-SO-771-57-477-47-411-14-2?3-f3-4tl-31-711-74-4Ul-11-32II-U-IM-l?-2
Fktiell i i - ( 2 -CkI« [« i t ky t ) i t k i r2-CkIiropkiiall , 3 -0 iek l«r»bt i i f l i tl ,4 -DickI0tot iBi t»l i i t ft l lcobol1,2-DitkUrobtfiiiat1 -Ht tky lpkt iv lk i i - ( l -CkIoro i i »pr0py l ) i tk i r4-Kitkf lpki iQlM-iitraii-Di-i-proiyluUeIttiekUtMtkiatXitrtbiiitu(i«pkar««i2-Kitnpkiiil1,4-DiBitkylpkti i lBencic icilk i f l -<CkI t to i tk« iy )Ht tkn il ,4 -DiekIor«ph»oI1,2,4-Ti iekliiibtutitMapklkaUie4-CkIoteaai l i i eEtiichUrabittdiini4-Ckleri-3'UtkyIpkiaol2-H*tky[iapktkil«atItnckltitcycUptitaliiBi1,4.4-TricklaropkeitI2,4 ,3-Ti ickUrBphnol2-CkUt«itpktktIiit2-Kittmili i iDiMtky l pktka la teIcnaptkyUit3 -Ni t t»a i i l i i i
S e p . F u n n e l E i t r a c t i o n : YES AjnJ( c i r c I e o n e )C o n t i n . L i q . - L i q . E i t . : YES p^P < c i r c 1 e on* )
•111
421 Q410 1411 V411 I421 0421 V410 V410 U411 V411 I420 9411 I411 U420 1410 V410 11000 0410 1421 Q421 1421 0420 Q421 U420 0421 V42fl V120 02000 D410 02100 Q421 9421 92111 D
CIS No:
13-31-f31-11-3101-11-7131-44-f111-14-1484-11-214-44-17013-71-314-71-7110-01-1334-32-1I4-3M101-33-3111-74-117-14-313-OUI110-11-704-74-1104-44-1llf-00-913-41-7M-14-134-35-1117-11-7l l l - l l - f117-14-02I3-M-11I7-M-?30-11-1H3-1I-333-71.3171-14-1
actaipktkiu1 ,4 -D i i i t t tpk t t o l4-Nitropkti i lDibet iof i i t i1 ,4-Di i i tr i t i I i ia il , i -0 i i i tr»t i l i« i«Dlitkyl iktkilati4-Ckloropki iy 1-pkaayl otkctFluriai4-Nltroaii l i i i4, i -Di i i tr i -2-f letkylpki i«IH-i itroi*tf ipkiaylaBiae (1)4-Braiepkttf I-pknyl i tkicItitckl»tob«iit»PiitacklortpkiialfkiaaitkriitUtkraeiieDi -a -b i ty l p k t k i l t t iriittiitkiBtPfrml i tT l -b ia ty l - ik tka l i t eJ ,r-DiekUr6l inni i i iItiioUUitknctilb i s -d -E tky lk i i rDpktk tUt tCkryitaiOi-a-oetyl pktktlitiIt i i t lblUiaraatktaiB»i«(k) f l i« t» tk i icB»i*{a}pytt»lit'iiid.l.J-ci'lpTrtaeDibei i«(a ,k) i t tkiaciailt i i»(fi i}pit |Itat
MM
410 9llll U2111 Q411 Q421 9411 9411 0411 9411 9llll 92111 9411 9411 9411 9llll 9411 U411 9Ul BJ411 0411 9111 U111 9411 Q411 BJ411 Q/jHD* <iiV411 9410 9411 0421 9111 9
(1)-Cannot b* ftparattd from diphtnyiamint
FORK 1
Laboratory Ac.-
Organics Analysis Data Sheot(Page 3)
Concentration: fiLow/ Medium
Date Extracted'Prepared: ____*LL
Date Analyzed: ____'j.
(Crete OneJPosticide/PCBs
GPC Cleanup Q'v'e* QNo
Separatory Funnel Extraction
Continuous Liquid - Liquid Extraction QYes
X)mom<:mo
COm
Cone/Oil Factor:
Percent Moisture (decanted)
CAS
319-84-6319 85-7319-86-858-89-9
76-44-8309-00-21024.57-3959-98-860-57-172-55-972-2O-S33213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6
11097-69-111096-82-5
Alpha-BHC0*ta-8HCD*lia-BHCGammj-BHC(L«odar»ei
HeptacWorAldrtn
Hepiachtor Epo»deEndosulfan 1DteWfin
4.4--O06EndrinEndoswHan fl4, 4--OOOEndosuffan Sutfaie4, 4--ODT ^Mettx>crchlorErtdrin KetooeCritordaneTocapOeneA/octor-1016A/ockH-1221Aroctot-1232Aroclor-1242A/octo^-1248Aroc tor- 1254
Aroctor-1260
iL.o a/ t .O /AIt.O tL
.- t(,.e> ai<>.o atf,.O U.tl,.O Uti.O Af.
J3.0 U..-53.0 U.
Ss.o U.' *33-O U
JP'O W520 «.
" J3.0 «/tO.£> U.
31. & U
IL6.0 UJtJd. > U]^o.o u/£.£>.& U£6.6 U/U>4> U/60.O U.330.6 ^3^.O fct
V- * Volume of extract infected (ul|
V * Volume of water extracted (ml)
Ws « Weight of cample extracted (g|
V( « Volume of total extract (ul)
orW.
7/85
:0Organic* Analysis Data Shtkt
/o . -. i^ >._(P*gt 1Nuabcr: EK8&6
L»bor»tory Niai ENVIRODYNELab Saapli ID No: 17003146Simplt Matrii SOILData Rtltast Authorized By:
Cast No: 7351QC Rtport No: __Contract No: <£ &•Datt Samp It Rtctivtd
Vo I at i11 Compounds
Concent rat ion: LOWDatt E i t r t c t t d / P r i p a r i d :Datt Analysed: 6-26-87Conc/DiI Factor: 1Pi rcent Mo is tur t (not dtcanttd)
&// ff? 7
13.48
US No CIS le:
74-17-374-13-173-11-4.73-IB-J75-lf-l17-44-173-13-B73-13-473-14-3134-il-*47-44-3117-14-271-fl-S71-33-434-13-3tll-«3-473-17-4
CkleieiitkiitItoiiittkaitTiiyi Cki i t td tCklototthiniHitkylni Ckl t i id tIcitlBI
Catben D i i i l f i d tl . l -Dieklot t t tkt i t1,1-DiekIiititkintrats-l,l-Di£kItriitk»tCklit«(«rmt,2-0icklir»tkait2-litaiui1,1,1-TriekltctttkiitCitbn TttiaekUildtTiiyl iciUttliindickl HIM I kail
11 BU 013 B11 B111 14f 1
7 B7 87 B7 B7 B7 B13 V7 87 B11 B7 B
7I-I7-S11*41-11-47t-ll-4114-41-177-11-371-43-111141-11-3111-75-175-23-1lll-ll-lW-71-4127-11-471-14-3lll-ll-liu-ri-7111-41-4111-43-3
1,1-DickUrtpropantrati- i . l -DicbloropropiniTttcklonitkmHifcriaiekloriittkaii1,1.1-TriikIouiUanilimitc i i - l . l -DUkloro frap iB i1 - C k I i t o i t k y I f i B y I i t k i iIroiaioral-Hltkyl-l-piitlBOii2-BliaintTitraekltrtttkiit1.1 ,2 .2-TtUatkIir i i tktnTtlititCkliribiBttiiItkTlkiiitiiStyrmT«UI If lilts •
7 B7 B7 07 87 B7 B7 B13 U7 B11 V11 I7 B7 B
1 IJT 07 B7 B7 B
Oitt liputiif Q i a l i t i i r i
T1WI:If tkt riinH ii a ftU» |tiatit tku it iqnl t* tki Itttctiialitit, tijott tki Ttlii.
«ti tiilriid fti kit ut iitietttf. Itpitt tktItttctiu l imi t ftr tkt ftk|lfl vitk tkt 0 <t« ,UO) kistd
•• itctfitry c»ct i t . /4t l i t i« i tetivi. (Tkis li itt itcitittiETtki iutttatit l i ttct ita l i m i t . ) Tkt (tfttiitt ikuld rtid: U-Cii|ind vn utlfi id fit kit ut dittct id. Tkt mbit ii tkt•iiim tttaiiaklt dtttctioi lliit (ir tkt fuplt.J:tidieaUf u •itimttU filn. Tin (U| ii uid k i tkt t wfeti•it ii4 tli| * ciiciitntiii for tut i t i f i l f Unt i f i id eei|endivktri i 1:1 riipoui ii tuned tt vku tkt usi ipictttl dtUfidicittd tki yristict if i t»poHd tkit »itti tkt tdtitlfleitiiBer i t t r i i kit tki rtult it Im tku tkt t p i c i f i t d dttittiii l im i t
Tkis fli| ippl i t i tt fisticidi fituittri vbtti tki i d i s t i f i e i -tlet vti etiHtiid by CC/HS. Siigti eo»p«itat p«tiei4«s>«llil/il ii tkt fiial utriet iiuld kt ctifiiaid by CC/K5I: --- _Tkif Iltf ii utd vkti »4tytt ii ftiid ii bl iak if mil if :•upU. It i idicitt i y i i f ik t i /yn l ib l i blank coituiutiii andwit u tki data ifti tt Ukt ipprsprUt i i c t io i ,OTHEI:Otktr fltqi ltd (titiitti Uf ki itqiind ti ftoptily dtfiittki tiiiltt It uid, tkty mt bi I i l l i ditcribid aid lickdiicii|ti» attackid tt tki dita ifmiaiy riport.
lit
L a b o r a t o r y N a m e : E N V 1 R O D Y N ECas t N o : 7351
Or g a n i cs
.
I S a m p l e N u m b e r : E M B 4 6
A n a l y s i f( P t g e 2
Semi v o l a t i l e
C o n c e n t r a t i o n : L O WD a t e E x t r a c t e d / P r e p a r e d : 7 -4 -87D a t e A n a l y z e d : 7 -9 -87C o n c / D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( d t c a n t t d ) : 2 3 . 4 8
CIS MB :
lll-fS-2 FkeBol111-44-4 b i i - ( 2 - C k l « T B i t k y l ) « t k i [73-57-1 I -CkUropkinol341-73-1 1,3-DitkIiniiiiBie114-44-7 1,4-OUkIorBteBitiitll-St-4 Iiityl UcBkBl•3-31-1 1.2-DiehlerBkeaiiBi•5-41-7 2 - K B t k f l p k B B B l3f43l-32-f k i i - (2 -CkIemiop t f l iy I ) i tke r114-44-5 4-lUtbyliktBBl421-44-7 M-aitroio-01-B-irBiylaftiie47-72-1 IntchUciitkiiBfl-13-3 litiokiitiBi71-St-l IiBpkBtBte11-73-3 1-Hitrtiktitl113-47-V 2 ,4-Di ie tkyI ik tBBl43-13-1 iBiSBie lei 4111-11-1 k i i - ( C k l B r B B t k B i T > K t t k a i e121-11-2 2 , 4 - D i c k l B f B p k t B B l121-12-1 1,2,4-TricklBrBkBiiBiBM-21-3 Kapktki lBae114-47-1 4-CalBrB»iI i ie17-41-3 •iiacBlorikitiiiiit31-51-7 -CklBte-3-ietkyIpkBiBlf 1-3 7-4 -HelbylupktkiltBe77-47-4 a iack l f r tcyc lBi tBta i ' iBa i11-04-2 ,4,4-Triekl tr«pkeaBlH-tS-4 ,4.3-TiickIitBikciolfl-SI-7 -Ckloraiipitkilt i t11-71-4 -litriaiiliie131-11-3 Bimetal ihtkiUte2II-T4-I IcHiptkyliiif f - l t -2 3-Nitroai i l iu
GPCS e p .C o n t
• gko
431 0431 1431 0431 0431 0431 0431 0431 0431 0431 9431 0431 9431 9431 9431 9431 92111 9 »431 9431 0431 9431 0431 9431 0431 9431 9431 9431 02111 0431 02111 0431 0431 02111 0
D a t a Shee t
*
C o m p o u n d f
C l e a n u p : NO s* —— VF u n n e l E x t r a c t i o n : YES f HZj( c i r c 1 e
V. jf~r£i n . L i q . - L i q
CIS MB:
13-32-f31-21-5111-12-7132-44-f121-14-2414-21-214-44-27«3-72-314-73-7ltl-ll-4334-32-114-31-4111-33-3111-74-117-14-3IS-ll-l121-12-714-74-2214-44-1m-n-i13-41-7M-f4-l34-33-3117-11-7211-ll-f117-14-12l3-?t-2117-ll-f31-32-1113-37-333-71-3l«l-24-2
Eit . : YES ( N D ^ M c i r c I t
Iciiapktkne2,4-Dii i t rBpki i f l l4-Nitr»iiBiilBibiatBfirti2,4-Diii tr i t i I icie2 ,4-DlBi t r i te I ie i iD i i t k y l iktUUte4 - C k l B f B p k i B y l - i k B i y ! e tkcrfliereBB4-MitrBtBil l i t4,4-Oiaitri-2-llitk;lpk»el1-BitreiBdiikBByIuiti (1)4-9rH*pkeiyI-pkiBf I etkBtliitcklitibttiiiiPuticklBrepbiialFkiiiitkctitaitkracBiBBi-i-fcBtyl p k t k t l t t iriitrntbtiiFyriBel i t r l -btBiyl-Bktki l i t i3,3 '-DiekIirBb»iidii ilean(i)tBtkr«ciBeb i i - ( 2 - E t k T l k t i y I } B b t f c t U t BCkiyieBiDl-i-BCtyl Bk tk iUt itut a (b) f l ie r tit butI t l f t t t l f I lBfUtkBBIItiioUliyriat .ti<»tU,l,3-c<)Bfrntt lb«IIt(t ,b)«BtkttCllf
9 e B i B < f k i ) p B i y l B H
30T1
ft?<
COm
LO
tooo" J
one )one )
•qtq
431 92111 02111 0411 0411 0411 0431 0411 0411 02111 02111 0411 0411 0431 02111 0431 0411 0341 BJ411 0411 0411 0Id 0411 0If l BJ431 0131 0411 0410 0411 0411 0411 0411 0
( l ) - C a n n o t b t f « p « r » t t d f r o m d i p h t n y l * » i n «
FORM I
Laboratory
NOOrganics Analysis Data Sheat
(Page 3)
Concentration: ( Low) Medium*—~-^Date Extracted 'Prepared
Date Analyzed; ____^2.
Pesticide/PCBs
(Circle One) GPC Cleanup GlYes QNo
Separator? Funnel Eirtradion QYes
Continuous Liquid - Liquid Extraction
Conc/Dil Factor: I
Percent Moisture (decanted)
CAS og/l<Kfjg/KgNutnb«f . (GrcioTJo*)
319 84-6319-85-7319-86-858-89-976-44 -fl309-00-21024-57-3959-98-860-57-172-55-972-20-833213^5-972-54-81031-07-850-29-372-43-S53494-70-557-74.98001-35-212674-11-211104-28-211141-16-S53469-21-912672-29-611097-69-111096-82-5
Alph»-8HCBeta-BHCDelia- BHCG*mma-BHC (LindanelHeotacWorAJdr.n
Hepuenior EpoxKJeEndosu'fan 1Otetdrin
4. 4--OOEEnd/in
EndosuHan D4. 4--DOO
Endosuffan Sutfate4. 4'-DDT ^
Mettwicychlo*£ndrm KeioneChlordaneTOKJO*^*"*Aroctor-1016
A/oc(of-1221A/ocloe-1232Aroclcx-1242
A/odCK-1248AroClCK-1254
Arocttx-1260
/<..£> 6t/ t - o /I/t.O «_
- /6.0 W
/c.o alt,.0 U./4-0 «/i.O H
33-0 U..-w.o «.J3,o a<3JO «^P.o KJ3^3 t<
^J^» M/*.£>.£> U.
J .O «/t,AO U
330. £> U/£<9.<9 U/t.0.0 U.
&Q.O U]U>.£> UIL6.O Ujao.6 £/3ZO.O U.
a
V * Volume of extract *nfecied (ul|
V * Volume of wJier extracted (ml|
W * Weight of umpfe enracted (g|
V * Volume of total enract (ufl
7/85
ecology and environment, inc.Ill WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
Date Received for ReviewTO:From: Zena Gold-KaufmanSubject:
PAN:
Date Review Completed
Case I -?35/
Sample Description______Organics (VOA, ABN, Pest/PCB) Inorganics (Metals, Cyanide)
Low Soil *Low WaterDrinking WaterOther
Low SoilLow WaterDrinking WaterOther
froject Data Status
Incomplete, awaiting:
Completed
FIT Data Review Findings:
CI?DLdetected in
enclosed sheet-
Book No.
Compounds were detected in sampTe(s); see enclosed Chemical• Evaluation Form.(p__ Page No.
736"/
^
£/
/rV
p£6T
P6-5
COMPOUNDdimethyl phthaleteacenepthylena3-nltroanllinaacenaphthena2,4-dinltrophenol4-nitrophcnolaibiniof'ittn2,4-dlnitrotoluene '2,6-dlnltrotoluenedlethylphthalata4-chlorophenyl-phenyletherf lnorarm4-nltroanllina4,6-dJnitro-2-fltethy]phcnolN-nltrosodlphenylsmlne4-bromophenyl -phenyletherhexschlorobenzenapentachlorophenolphenanthrene•nthracenedl-n-butylphthalatefluoranthennbenzldin*pyrenebutylbenzylphthelata}, V-dlcMorobenridineben2o(a)anthraceneblt(2-«th)lhnxyl)pNthalat4chryaenedi-t-octylphthalat*ben2o(bik)rjuoranthen« 'benzo(a)pyrcn«Indano(1t2,3-cd)pyrenadlbenzo(aih)anthracenebanzo(q,h,l)pery]ane.lpha-6HCbett-8HCd«lta-6HCqafma-8HC(llndsne)heptachloraldrlnheptachlor epoxldeendosulfan Idlaldrin4.4'-M)eendrlnendosulfan II4, 4 '-000andrln aldehydeendoaulfan sulfate4,4'-OOTatethoxychlorendrln Ice tonecMordanotoxaphen*Aroclor-lOUAroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260
r
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HQO <Mio£L,s •COMPOUND t _ J
chlorowethanebrocwx&e thanevinyl chloridechloroelhanewelhylene chlorideecetonacarbon dlsulflde1, 1-<fichloroethene1,1-dJchloroeth«netranf-1i2,-dichloroelhenechloroform1,2-dlchloroethane2-butanona1,1,1-trlchloroe thanecarbon tetrachlorldevJnyl acetateb r o»od 1 ch 1 o r omet h ane1, 1,2,2-letrachloroethane1,2-dlchloropropanetran«-1»3-dlchloropropenetrlchloroethenedJbronochlorome thane1,1,2-lrJchloroethBnebenzenecle-1,3-dichloropropene2-chloroethylvlnyletherbrowoform2~hexanone4-tiethyl-2-pentBnonetetrachloroethenetoluen*chlorobenzen*•thylbenzenaatyran*total xyleneaN-nitroaodlaiethylsnlnephenol•nil In*bia(2-cMoroethyl)ether2-chlorophenol1,3-dlchlorobeniene1 ,4-dlcMorobenzenebenzyl alcohol1 , 2-dlcMorobenzena2 -«ethyl phenolbJi(2-cMorolsopropyl)ether4 -Methyl phenolH-nltroao-dl-n-propylamlnahexachloroethanenitrobenzeneJeophron*2-nitrophenol2, 4 -dlaethyl phenolbenzole acidbla(2-ch]oroethoxy}methane2.4-dichlorophenol1,2,4-trlcMorobenzenenapthalena4-chloro*nllin«hexachlorobutadlena4-chloro-3-«ethylphenol2-«ethylnapthalene 'hexacMorocyclopentadlene2.4, 6-tr Ichlorophenol2,4.5-trlchlorophenol2-chloronaphthalen* i?_n)t rr.«ni 1 1 ne
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fUNITED STATES ENVIRONMENTAL PROTECTION AGENCY / 4
REGION V
-, - Q\~L\~ Ql
DVTE : 4SUBJECT: Review of Region V CLP Data
Received for Review on___
F30M: Curtis Ross , Director (5SCRICentral Regional Laboratory
c i -rTO: Data User: F I T
We have reviewed the data for the fol lowing c a s e ( s ) .
SITE NAME : H Q D LANDF ILL ________SMO case No.____________~ ~~~—————No. of r D . U . / A c t i v i t y _ ,
EPA Data Set No. ^ 4l3b Samples: D Numbers 79Q5/C~JZJOQ
C R L No.________&1FP\\S1S ^ , - :
SMO'Traffic N6Vr—"~"r
.:_ :--Hrs. Required;— «'• V -for Review:- ^^
Following "are "our findings:'
Data are acceptable for use.{ v) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory( ) Data are unacceptable.
cc: Duane Geuder, Quality Assurance Off icer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas
EPA FORM 1320-6 (Rev. 5/87)
DATA QUALIFIERS
Contractor; f —1 •"» *»•Case 7 A A
Below Is a summary of the out of control audits and the possible effecton the data for this case:
oo
/C v. / g / 0 \i U'l ..", A
,{-•'* 'l-t,-^'."
., a
Reviewed by:
Phone: __
Date: slain
UNITED STATES
CASE*
ENVIRONMENTAL PROTECTIONCALIBRATION OUTLIERS
VOLATILE HSL COMPOUNDS
R E G I O N V
CONTRACTOR
,QATE/Ti.w.E:
-Chloroir.eina.neBrorr.ometnaneVinvl ChlorideChloroethaney.etnvlene ChlorideAcetoneCarbon Disulf ide1,1-Oic.nloroethane1,1-DichlorostheneTraris-l,2-DichlorcetheneChloroform2-Sutancne1,2-Qichloroethane -= —1,1,'1-TrlcMoroethane .... •Carbon Tetrachlor.ide :Vinyl Acstate . - ^ r f T_ -BromocSichloromethane ~s- •-.-1,2-DichloroorooaneTrans-l,3-DichloroorooeneTrichloroetheneDibrcnochloromethane1,1,2-TrichloroethaneBenzeneci s-1 ,3-Di chl oroorooene2-Chloroethyl vinyl etherBrotnofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-Tetrachl oroethanaTolueneChlorobenzeneEthylber.zeneStyrenem-Xyleneo/p-Xylene
AFFECTEDSAMPLES:-
H
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RF
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&&,^r
if
fr
:i Carl(ffl'^RSO
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* These flags should be applied to the analytes on the sample data sheets.
CASE? 7357
STATiS ENVP.OWENTAL PP.OTEITIDN AGENCY REGION VC.-LIBP.ATIO'i CUTLIE'3
'MI'.'iM A T T I ~ PC; r^vr"i:';f;<;*, **. i 4 9 \* t», I 1 U ta 1* ., h_ \ # W i - . v ^ » I W * J
(Pace 1} ,,_______ COH73ACTOR . ' > ,; tlye?d L|
nit, Cal. ICont. C;:.ICc-.z. Cal Cont. Cal.tCon:.DA11/
IRF 10 * .0 -Pr.enolbisi-2-Chicrce:hvl;E-ner2-Cnlcrocheno1 .S-Oicnlcrcoenze-.s.-i cruorocerue".*
Eer.rvl Alccr.c.*! i c rcenze- .=
t is {2-cn1oro1 scare:-/ i )£:r.er
K-Nitrcsc—Ji-n-PrtrKexcchicroe'haneNizrccenzsneIscchorone2-Nlrrocneno'2»4-D.imeth"vToh6nol
2,4-Oicr.loroonenoi I -
4'Chlcrccr.i lineHexachlorobutadier.e4-Chloro-3-Me*nvi:.re.r:ol2-MsthylHexacniorocvciooenteciiene2,4,6-TrichloroohenoT2,4,5-Trichloroohe-.ol2-ChloronaDhthaler.e2-NitroanilineDimethyl PhthalateAcenaDhthvlene3 - N i t r o a n i l i n eAcenaohthene2,4-Dinitrocnencl4-NitroDhenolDibenzofuran t I I
AFFECTED•SAMPLES:
I
* These flags should be applied to the analytes on the sample data sheets.
1 /Q7
CASES
UNITE-0 STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLAT1LE HSL COMPOUNDS- / ' Page 2 x' - {
I CONTRACTOR T v p yt pi'AvnoIS
DATE/TIME:
2,4-DinitPotoluene2,6— DinitPotolueneDierriylpntnalateA-Criloroohenvl-phenyl etherFlucrene - „. _4-Nitroani line4, 5-Qirhtro-Z-Methyl phenolN-Nitrosodiohenvlanine4-SrontCDhenvl-onenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthracene
- Di -n-Buty 1 phthal ate - — — — -Fluoranthene _ ... ^^-^~~~,-
-Pyrene-,- --— — r,~^;- ~- ~:-r-r-Butyl benzvl phthal ate-^ -;-.-? •.-Benzo( a JAnthracene -.?. -T- "=.._:---bis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl PhthalateBenzo(b)FluopantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneDi benz ( a , h ) ArthraceneBenzo(g,h,i) Perylene
Initt Cal.7/.r/* '/RF
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SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytes on the sample data sheets.
1/87
STATES ENVI5CWE:i7AL F307E:7;0:; AGE"CV RE-SICK V
SEMIVCLA7ILE HSL C'jX?:u:;DS(Pacs 1)
Cr.Si? i f .' \
. . •OAi i / i i t f t : . |
Phenolbis'.-2-Cnlcros:nyl jEiner2-Cnlcr3cneiol1.3-DicnlcrcDer.2e-;£1.4-D*cnlcro^enze".=
-E-£-".zvl Alc^noll.Z-Dic.nicrc^enze^s2-Me^nvl3r.enol&isl2-chloroi score:-/ 1 Jcir.er<i-V.cC?.v"iDher.olN-:iitrcsc-Ci-n-?r;;vlam .-=HsxacnloroetnaneMi trccenzeneIscsrtcrcne -— --- -.
•-Z-Nirroshanol'Tr.^--— •-- .- ••. 2.Z.4-01 methv-1 ohenol. "iV' r^ ;;- Ee^zcric~Acia_ ..-•^rf^^^^-r"-'1
bist2-Ch-loroethoxv JMeihana-2,4-D1cr'.loroonenoi- -1 ,2,4-TricnlorcbenzeneKarr.chclene4-Chlcrcc.r.ilineKexccnloro&utadler.e4-Cnloro-3-Mg-jivlGre.no]2-Methvlnashzhale^sHaxacnlorocvclooentadiene2,4,6-Trichloroohenol2,4,5-Trichlorophenol2-Chloronaohthalene2-NitroanilineDiinethvl PhthalateAcenanhthylene3-Nitroani lineAcena^hthene2,4-Dinitrocher.ol4-Ni troonenolDlbenzofuran
- AFFECTED•SAMPLES:
V
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,
£ ftG. \Yr/r€f
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* These flags should be applied to the analytes on the sample data sheets,
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDSPace 2 X
CONTRACTOR ^t U
DATE/TIME: .
2,4-Dinitrotoluene2,6-OinitrotolueneDietnylpntnalate4-Cr.lcroonenyl-phenyl etherFluorene4-NizPoani line4, 6-Dinitro-2-Me:hvl phenolN-N1 irosodi phenvl ami ne4-3 rofTiGcnerwl-pnenvl etherHexachlorcoenzenePentachlorophenolPhenanthreneAnthracene
-Di-n-Butylohthalate.Jluoranthene— r ; -...- —— —
Pyreneir^— ~=~~^= -—•'-— :. -~.~• Butyl benzvl phthal ateBenzotaJAnchracene -•'* -. -•bis(2-Ethylhexvl)PhthalateChrvseneOi-n-Octyl PnthalateBenzo(b)FluprantheneBenzoCtcJFluorantheneBenzo(a)PyreneIndeno(l,2,3-cd)PyreneDibenz(a«h)AfrthraceneBenzo(g,h,i ) Perylene
I nit7/ytRF '
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SEE PAGE 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the anal^tes on the sample data sheets.
1/87
i!
ENVIRODYNEENGINEERS
JUly 24, 1987
Ms . Carol Schacf ferSample Management Office209 Madison Avenue, Suite 200Alexandria, Virginia 22314
Dear Ms. Schaeffer:
Enclosed are the results of analysis of five samples from Case 7351 forvolatiles, semivolatiles, and pesticide PCBs performed under Contract68-01-7087. TCiis report covers five soil samples, EM867 through EM871 ,received by. Ehvirodyne on June 27, 1987. One matrix spike and 'matrix spikeduplicate for low -level. is included: with these samples, -and will- apply to the
the. -case- that was received ~on "
J£s^^seTlteuti^^Acid fraction ^there :are~:tw:
.samples
If you have'any questions about this report, please contact me.
Sincerely, /—\
Shaaban Ben-FooratLaboratory Director
CAJ/smb
Enclosures JUL 27 1987
US .S3C £. CLA^K STREET
CHICAGO. ILU-JG1S 5060*
Case No.
REAGENT BLANK SUMMARY ..AUG 1 8 1987
Contractor contract
FB.C 10 CMC orAMALT9I* FRACTION fBfc Mtr.iO CAI NUUICR COMPOUND (HSL.TlC OH UNMHOVN) CONC. UMtTt CHDL
-
MS- 0-1
X- /x
-c
xnmonti:
FORM IV4/84
RECEWEO * SOIL SURROGATE PERCENT RECOVERY SUMMARY
lft"*.« ^ Unrffc»w
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— —— — —— —— - — - —— • i . . - . , . , , . . .• .-,1 - ] • • - • ._______________ ___ ___________ __ ____ '" .' '" : _______________ __ —— . ———— . —— — -
SOIL MATRIX SPIKE/MATRIX 3MKt; • . ! • . ! . . '
* ™. * v. * .nContractor
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PESTSMO
SAMPLE NO.
COMPOUND
1.1'DichotortttwrwTrichlorotlhcn«ChlO'OtKnung
I TolutntBtnitnt1 .7,4-Trichlorob*nitn«Acfln*phlhcnt2.4 0<ni|rololu*n«Pyrtn«N-Nitrotodl-n-PropvUmint1 ,4-Oichlorobtntcn*PmiichlorophcnotPhtnot2-Chlorophcnol4.ChlorO-3-Mtthy|phtnol4-N<irophtnolLindint
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ERISKED VALUES ARE OUTSIDE OC LIMITS.
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OCIIMITS*HPD
22242121212319473838274735503350503143384550
RECOVERYW.17262-13760-13359-139M-14738-10731-13728-8935-14241.17028-10417-10928-9025-10226-10311.11448-12735-13034-13231-13442-13923-134
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Organic* A n a l y s i s Data Sheet(Page 1)
S a m p l e Number • EM867
L a b o r a t o r y Nine: ENVIRODYNELab Sample ID No: 670032*1Staple M a t r i x : SOILDat» R e l e a s e A u t h o r i s e d By:
Case No: 7351QC Report No:C o n t r a c t No .Date Sample Rtceiftd
V o l a t i l e Compound!
Concent rat ion: LOVDate Eitiacted/Prepired:Date Analyzed: 07-01-B?Cone/DiI F a c t o r : 1Percent Moisture (not decanted) 15 .4.
CIS No:
74-17-374-13-1
C h l o t O B e t h i t ilioiontbiniVii f l C h l o r i d e
. ChUrotlbinr ,73-lf-l
"47-44-r
75-34-3134-4B-S47-44-31I7-B.-2
71-55-434-23-3111-13-473-17-4
icttoue
1,1-DiekUretthia*t r iB i - I , 2 -Dick lo ra i tk iB iC f c l e r o f o ul , l -Dtchlor«i thaa il - l l t lBOBI1,1,1-TrithloroitkaBeCarkei T i t i a c k U t i d eTiiyl UitateiMBodi th lor iBt tha i t
12 U12 U12 0
: 11 U_ 124 I
5U002 V0V
U V4 a
CAS No:
71-17-5t B O f l - l l - 477-11-4124-41-1-7?-ll-371-43-2 -HI4i'-lt-3111-73-175-25-1
5»l-7l-4127-11-471-34-3tll-ll-3tlt-M-7tl«-41-4lflt-41-S
igtg
1 . 1 - D i c k U r o p r o p i n il i i s s - I , 3 - D U h U r o p r B p t n iTt ick lere t t i t i tD i l r i i i c b l o r B M t h a n t --
cis-Jl.j-Ditklptcproptie
1-ItsinoBtTitriCBlorettBini1,1,1.1-TituekloieithiniTltBBBC
CtBf lb lBSIBB
StyriBtTtttl I
Diti Q u l i f i t M
TILUE:II tkt r isul t is i Tilat g r t i t i t tkiB eit i i it . ti»«tt tki
to tk i i » t « c t t o B
SidniUdnitis cimpevBd vis iBi l jud for knt BOt d i t i e t t d I tpv i t tbi
nifioi lBt tc t i«> l i i i t (or tkt s»pli *ltk tki D ( t g . t f l O ) »n*4•B itTuitri tuc tB t .Mi l i t i oB itt iot . <nif is Bot BBces s i i i l ytbi ikjhttBiit OUetieB l i i i t . ) Tki fiotsolt ikoBld tt id 0-
a i t l f i td (ot bit tot d o t i c t i d . Tki inbcr it tfciiKblt dotoEtioB lint (or tko saiplt
Iiiicttcs^ est i t i t id uU« Tail (Uq is «s«d t i t k c t VBBBest i f t t t i>t^ .ef lBtiBtr i t ioB (or t f l n t t t i i t l f i d i i t i l u d cotpotodivhire i l:^g«»poii( is iss»td «: vktB Ike B*JI s p t c t i a l 4 t t4i B d i t k t t d tta prosiBd o( » CBipeoBd tkit »tts thi id in t if ic i t lonc i i t i t i i bit t t i run It is lesc tkia tkt i p t e i f i i d e t t t c t ioa Hutfti t t ir tku ier» (if , 10J). K liiit »( Cittttiot it 10 iql tad icoici i t t i t i iB of 3 iql is c i l e i U t o d , r i pe r t as 3J.
This (Ug i p p l i i f l i p i s t i c i d * i t tmt t t i warn tki i d t a t i f i c itioB vis confuted ky CC'KS. Singlt eopoaint put i c idn) -U
ii tkB ( i ta l u t r i c t i k e a l d I t eoBt incd by CC/KS
Tkis (lag is «id wkti mltti ii foind it kliak n ««11 if iiiipli It iidicatti pemfcli/irebibli blioi centinmt IPB todwarns Iki data isir to l»l* appropriate actios.OTHE8:Qtker (U|s aid (aotittti aay it nqaitid to p i o t t r l f d t t i B itki r i i B l t i . H B i i d , tk*i Hit bi l i l l y duc i i e td isd cichd i f c r i p t i B B a t t ack id t t tko da ta SBBBIIT r i p o t t .
•ot
Liberate:?.NineCist No: 7351
ENVIRODYNE S i m p l e Number EM867
Otginics Ant 1ys i f Di t a Sheet(Page 2)
Stmivolatilt Compoundi
Concentration: LOWDate E x t t a c t e d / P r t p t r t d : 07-02-87Dat t Analyzed : 07-1 1-B7Cone /Di I F a c t o r : 1P e r c e n t Moisture (decanted): 15.4
GPC Cltanup : NOSep Funnel Ext r a c t i o nC o n t i n . L i q - L i q E x t .
i r c l e o n e )0 ] ( c i rc le o n e )
CIS Mi. CIS No iql?
— - - _ _— -
rC-r--"-- -
" - - • _
^SJ
SO
CO
<cQUJ
UJo
101-15-2111-44-495-57-1541-73-1114-44-7 »-.-.lOf l -S I -4 v.~95-51-195-41-739131-32-9101-44-5421-44-717-71-191-95-3II-JM11-75-5105-47-943-15-0111-91-1111-13-1110-02-191-21-3101-47-017-41-359-51-791-S7-477-47-411-04-295-95-4fl-51-701-74-4131-11-3iii-n-i99-19-2
F b t B f l lb i i - ( 2 - C h U i B i t b j l ) i t k « i1-Chlo ioph tno l1,3-Di tb lBiobia i iBi , ^^^1 ,4 -Dich I f l i f l b«nua i~ ~:l iBiy i^ l Icf lkf l l — —--_• ------i ;2-DickUrol«niiBe ;;7l - n t t b y l p h « B B l ~- -.b i i - ( l - C a i o r o i « o p t B p y l ) t t B i r4-tltthf I p h e a s lM - i i t r o i B - D i - B - p r o p j l u u a iKtmkUrf l t t a i aeK i t T B b l B l l B I
InphOIOBt
2-KittBpbiBOl2 , 4 - D i i « t k y l p k i B 6 litoioic A c i dbi i - (Ci l« [ ai t keif )Hi tk«ai2 . 4 - O i c h l f t r o p h i B 6 l1 . 2 , 4 - T t i c h l B t B b l B t B B CN l p b t b l l t B B
4-CkUtsiBiliBtH e i i c b l o t B b t i t i d i i B C4-CkUrB- l - t t t kT lphcsB l2-Ht tk f i B l p h t b l l C B B
K c n c b l o r a c T c I o p e B t i d i f B i2 , 4 , f - T r i c b [ B i B p h c B o l2 , 4 , 5 - T l l C B l B t B p b l B B l
2-CklBIBBlpbtklI lB*
1 - K i t l B l B i l i B I
D i m i t h i l p h t b i l i t tletBipthf ItBt3 - K i t r o t n i l i n t
( l ) - C a n n o t
390 V390 Q390 0
_---.»• "-_ 39J 0. 390 V .; "391 «
390 939« 0390 V390 D390 0390 V390 1391 t390 11900 0390 0390 V390 9390 V390 9390 V390 0390 0390 V390 If1901 D390 01901 0391 0390 «1910 0
be i t p a r a t c d I
13-32-951-10-5100-02-7131-14:9lli-14-240t :20-3:
"-- l«7fcT-l70J5-71-3 ~
""01-73-7 _f100-ll-iS34-32-1Oi-31-i111-55-3111-74-117-1*-!15-01-0120-12-704-74-2201-M-O119-10-0IS-il-791-94-1Si-SS-3117-11-7lt l-l l-9117-14-0205-99-1207-01-950-32-0193-19-353-70-3191-24-1
r OBI d i p h e n y 1
ic i i iphthtni1 , 4 - D i f l i t r B p b i D o l4 - I i t t o p b t B B lDiii t iefnt i2,4-DiBitt«UivtBi2 , 4 - D i a i t r « U l B t f l «D i i t k f l i k t k i U t i4 > C k l l I 6 p k f B f i - B k t B } l i tk i r
Flionai4 - K i t r o t B i l i a i ~ ~ '4 , 1 - D i B i t r B - l - K i t k T l p b c B o lM-BitroiediphdiUai i i U)4-lroiophiBf I - tk iayl i th t iItltCllttttlBIIBt
FtBtickl0t«pb(BelFktBtBtkClf l t
latktietBtDi-a -bo ty t B b t h i U t iFli trnt l iktFyraatl l t f l -k tBIf l - p b ( k l l t t «U'-DicaUiBbiBtidiBil l B I B d l l B t k r t C t B Ii i s - ( 2 - C t k y l a c i | l ) p b t k i ] t t iC k r f f i a iD i - B - B c t y l p b t B i l i t il t t l e ( k ) f l B O K B t k t B «
l lBIoUHl t l l lB tkCBI
l iBiedlifiiBil a d i a e ( l , 2 , 3 - c d ) p T [ | i tO i k i B i f l ( t , k ) a a t k t i c t B illBIt(|ki)|tIf ItBt
a m i n t
310 U110B Q1100 031B U390 0390 K "
"~- 390 C390 V390 B190f UHOB 03tl U310 0390 V1900 939B 03JJLU
/""*TTo~)^ —— l»TO
310 0390 0710 0310 D170 BJ110 Q310 t)31D 0310 U390 U390 019B Q390 C
or FORM 1
Case No
Organic* Analysis Data Sheet(Page 3)
Concentration; ( LowJ Medium.*-*
Date Extracted 'Prepared
Date Analyzed
Cone/Oil Factor:
Pesticide/PCBs
(Grcle One) GPC Oeanup QYes ONo
Separatofy Funnel Extractkxi
"7- fo - vy rfwiii
;rf {drenntfd) /^ - T
.._.:- -_ - .'.. -.-
'FT- --—— '--— —
.-.-••_;-_-•- - - . - •
CASNumber
3)9-64-6319-85-7
319-86-858-89-976-44-8
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BOOl-35-22674-11-21104-28-21141-16-S
53469-21-92672-29-61097-69-1
1096-82-5
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Libsnt czy. NiaeCase No 735 1
ENVIRODYNE Sattp 1 « Numbe r• EMB 6B
Or gin i c s A n a l y s i s Data Sheet(Page 2)
Concentration: LOWDate E x t r a c t e d / P r e p a r e d : 07-02-87Datt A n a l y i e d : 07-14-87Conc/DiI F a c t o r : IPercent M o i s t u r e (decanted)
S e m i v o l t t i l c Compounds
CPC Cle a n u p :U<0Sep. FtCont in.
14
CIS He
10l-f5-2'll 1-44-495-57-1541-73-110(-4i-7 .llfl-Sr-4'5-51-1 _:»S-4I-T' '.3fi3l-32-f111-44-5121-14-717-72-1fl-tS-37l-5f-lII-73-5115-17-fis-is-iIII-* 1-1110-13-2i:i-i:-l91-2B-3lli-47-117-11-351-50-7Tl-57-i77-47-4ll-Oi-2tS-15-4fl-51-711-74-4131-11-32GI-t<-lff-flf-2
P h e n o lb t s - ( 2 - C b U i o c t h T l ) e t b t r2 - C h I o r o p b e n o I1 , 3 - D i c b U t o b t n i e B k
I l ixy l1 , 2 - D i c b l o t o b i n t c i L e "_ . ,2 - K * t b j I p b e n o l , • - "~" Lb i f - ( 2 - C b I o t o i s o p r o p r n c t b e r
M - B i t r o s o - D i - B - p r o p y l n i n iH c i i c h U r o c t b t n tX i t r o b c o i i D iI f i p b o t O B t2 - K i t r o p b e n o l1 , 4 - O i i e t b y l p b i B o l
b i s - ( C i U r o « t b 6 i T ) K t t b « B i1 , 4 - D i c b l o r e p l i C B o l1 , 2 , 4 - T t i c h U r b b i B t c x tN a p h t b U c o i4 - C h I o t o a B i l i B iH e i i c h U r c b o t i d i t B *4-Ch lor o-3-i« thy 1 p h e n o l2 - n c t h y l B t p h t b i I e n t
2 , 4 , 1 - T n c b l o t o p b e n o I2 , 4 , 5 - T i i c b U i o p h i B o I1 - C U a r o a i p h t b i l t B e2 - K i t i e i B i I i B tD i i c t b y l p b t b i l i t eI c i n i p t b y l i a c3 - K i d o i n i l i n «
310 0310 U310 D310 D.310 U^310 U310 0310 U3ID U310 U310 Q310 0310 0310 0310 U310 01100 Q310 V310 D310 V310 U310 U310 D310 D310 Q310 0310 QIfOO U310 ITIfOO U310 U310 U1100 Q
i n e l E x tL i q -L i
CIS Ho.
13-31-t51-21-5100-12-7132-14-f,121-14-2101-20-214-11-27005-72-3li-73-7100-fll-l534-52-1li-30-1101-53-3111-74-117-11-5I5-B1-I120-12-714-74-2201-44-0121-00-015-11-711-14-131-5S-3117-11-7111-01-1117-14-0205-M-2107-OI-f50-32-1113-31-553-70-3111-14-2
r a c t i o n : YES (Kp^( c i rq. Ext . : YES (^(cir
I t t n i p h t h i B *2 . 4 - D i a i t r o p h e n o I4 -Ni t t opb tno i .D i b i B J c f a r a a ,,_-_..2 , 4 - D i a i t r o t a I n e a e _ _2 ,1 -Oia i t ro to i s iBCD i t t b y l phtbi l i t r
,4-Ci Ioropat iy l -pkiBj 1 e t b c rr iBorcie ~n"< :--•••••• '-----:•4 - K i t r o i B i I i a t4, 1-DiBi t r o-2 -H* thy I p h e n o lH - B i t r o t f l d i p b i D y l i i i a e ( 1 )4 - B r o i o p b t B y I - p b e a y l i t b i rR e i a c k l o i i b t B i i a iP i n t i c h U r o p h t D o IP f l t B i B t k t i n tIntknetBiD i - k - b B t y l B b t b i U t cTIiBinti tniP y r i B tI n t y l - l e B i y l - p h t i i U t t3 , 3 ' - D i C B l o i o b c n i t d i B eI t B i B f i U i t h r i t e B fb i f - ( l - t t h y l b e i y l ) p h t h i l i t iCb . iy i f f i (D t - i - o c t y l i h l b i l i t cI t B i o ( b ) f l a o r « B t b i f l el e i i e d i n n o t i n t k i n iI c B i o d t p y i e f i it B d t B o ( l , 2 , 3 - e d } p y i i B iD i b c B i o ( i , B ) a B t h r i c t n eI t B i o f g b i l i e r f E c B t
c 1 e one )nit one )
n g t g
310 Ui i o e u1100 U
- 310 U.- sia o -J
310 0 :..310 D
310 0^3 1 0 01UC U1100 U310 U310 U310 U1100 U310 U
^^Jlfl D
C 1100^^310 U310 U310 D770 U310 U110 BJ310 U310 U310 U310 U310 Q310 Q310 U310 U
1 = i • = :
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FORM 1
Case NoS *rnpt« W jj rn b-« f
Concentration ( Low) Medium
Date Extracted'Prepared
Dale Analyzed
Conc/Dtl Factor
Organics Analysis Data Shoet(Page 3)
Pesticide/PCBs
(Circle One) GPC Cleanup
Separafory Funnel Enracaion OYes
•1- \O • V7 rVinfi*
1i-r o •
r (rf*cani<"d} ' * • f
- . - ~~ ' -'-- - • - • • - - -,
CASNumber
319-84-6
319-85-7
319-86-858-89-976-44-8309-00-21024-57-3959-98-860-S7-1-- _72-55-9 — -72-20-6 -"33213-65-972-54-81031-07-850-29-372-43-S53494-70-557-74-9
8001-35-212674-11-211104.28-211141-16-S53469-21-912672-29-6
11O97-69-1
» 1096-82-5
Alpn»-8HCBeia-BHC0*lia-BHCGamma-BHC(Lirw3jr*|
HeptachlofAkJrtn
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Laboratory Ntme: ENVIRODYNELab Sample ID No: 67003293S a m p l e K a t r ii : SOILData R e l e a s e A u t h o r i i e d By
Case No: 7351QC R e p o r t No:Cent rict No: _Da t e Samp Ie Rece i red
Vol 11 i It Compounds
Concentration: LOWDate E i t r a c t e d / P r e p a r e d :Date A n a l y t e d : 07-01-B7 ___Cone /DiI F a c t o r : 1Percent M o i s t u r e (not d e c a n t e d ) 13
CIS No
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•- . -'-r-COcn20*"<a"*C
. -^
7*-l7-374-83-»75-01-475-88-375-81-2 :47-44-173-13-075-35-475-34-3151-40-54 7 - 4 4 - 3117-04-27l-»3-371-33-454-23-5101-13-473-27-4
LUOUloc
C k l e r a i e t b a n eI roaa ie tbane?iayl Cbloridc—^: - ...C h l o r o e t k a n e - _ _^ — -H c U y l e B c - C k U r i d e ' — .-icetoae -------- • _ ^ _ L _ _ _C a r b o n D i s n K i d e --- - -1 , 1 - D i c h l o r o i t b e n e —1 t l - D i c b l o r o t t b a i L et r a a s - 1 , 1 - D i c h l a r o e t h i n eC h l o r o f o r m1 , 1 - D i c h I o r o i t h i n e2-latatose1 ,1 ,1 -Tr i ch lo roe tk ineC a r b o B T e t r i c b l o r i d cV i a y l A c e t a t eI r a B e d i c b l o r o m e t b a i c
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If the resnit is a talne greater thin ot equal to the detectionlint, r e p o r t the Taint.U:Indieites compound was analysed for bat lot detected, teport thiliiiin tfitection liiit (or tbe fatplc wtlb tbc U (15,1011) bendon Bccessarf etactnt./diliticB ictioi. (This is aot ncfffiril|Ut iBstrntat detectian liiit.) Tbc footaetc ikooH riad: V-Coiponnd vas »«lrtid for bat let d t t c c t i d . Tkt aombir ii tbi• iaiira attiiaabU dctiction limit far tbc tuple.J:ladicitu aa estititcd film, Tbic (lag i« iftd litber whenistimitinq a tontnttition far tcatitiTiiy idintificd coipoondiwh*n i 1:1 rtfpoott is asined or when tbe mi i p i c t r i l ditiindicated tke piescnci o( a coBpaand tbit teetf tkc ideatificitiontritirii but tke resalt is less Uin tbc ipecified detcctiaa tinterntir tkaa lire (eg, 1BJ). If liiit of detectioa is 10 ag! a«4 icoacenttitiei of 3 oql is ca l c n t i t c d , report at 3J.
Tiii flio applies to pesticide pirnettrs wheri thi i d e n t i f i c i -tioa vts coafirattd by CC/K5 Siagli toipontot p e s t i c i d e s ) = 1 0ag/al ti tbe final eitrict sbeold be confiracd bf CC/KSI:This (lag is ased vtea aaatyte is foaiid in blinl is well as isample. It iadicitcs possiblt/prebable blank coatiiinition *nd*»irnj tbe data flser to tike a p p r o p r i a t e i c t i o n .OTHER:Otber flags aad foetnatcs Biy be reqaired to profitly definetke r e s a l t s . If ased. tbey init be f i l l ] t e i c r i b e d nd sicbd e i c t i p t i o n a t t a c k e d to tke d « t a snuir; r e p o r t .
bat
L i b o r i t o i y ' N i n eCase No: 7351
ENVIRODYNE Simplc N u m b e r
Organic* Analysis Data Sheet< P a g e 2)
Concentration: LOUD»te E i t r a c t e d / F r epared : 07-02-87Date Ana lyte'dT 07-14-87Conc/Di1 F a c t o r : IPercent Moisture (decanted)
SeaiTo1 at iIe Compounds
GFC Cleanup
13 9
CIS Ka:
S e p . F u n n e l E x T c t i o nCon t in L i q - - L i q . Eit .
CAS No;
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101-15-21H-44-413-57-1 _ _3U-73-1 - •'-.1I4-U-7 —100-31-4 --?3-5o-r ~_J5-4I-73H3I-31-1101-44-3i21-44-747-72-111-15-371-31-111-73-5113-47-1iS-13-0111-11-11ZC-I3-2121-11-1H-20-3lli-47-l17-41-337-30-711-57-477-47-411-04-2JS-15-411-51-7OI-74-4131-11-1211-14-111-Ot-l
Sib™;11111111111 ,3 -Dicb te rob tBi iB i __~~~ __l,4-Ditfi!erob«nitai -" "-ZliTv-,I tB t j I i lcohel ~" ~~- :"~--~. -l ,2 -Dicb . Ie iobent iB» — ~ *_ii2-Hetf l j lpf l iBfl I " • " - ~;_.bis- t 2 - C h l o r o i sop r o p y IJ i tb . t r4-Rttb.f Iph iBolK - B i t r o s o - D i - B - p r o p j l a a i a *Ht i i caUio t th imNitrobeaitfitIsoph*[«Bi2 -Ki t i opBcno l2 , ( -Dia* t i j lph inoIIcBte ic acid• ii-(Cb.Uro«tb.«tf >Htt»iBt2 , 4 - D t c B l o i a p b c B o l1 , 1 , 4 - T r i e b . l f t T o b e B t t B Ct U p b t B l I t & l4 - C U e r o i B i l i a tHtiitBlocobflUdiiBt4 - C U o r o - 3 - i t t B T L p h t B o l2 - H t t h f l B l p b t b l l l B t
HeitchlerocTctoptBtidiiBt2 , 4 , 4 - T i i c B l o t o p b e o e i2 , 4 , 3 - T r i c b I e t o p h c B o l2 - C b l Q t a B i p b t b a I t B C2-Ki U o i B i l i B iOiattbTl phtBi la teI t t n i p t h j I i B t1 - N i t i f t i B i l i B i
310 U310 tl310 Qno u •
"/ ^318 0...JT.SII D -_ _3IO B"_ 310 0
300 Q300 D310 B110 U310 ano B300 fno ot t l f l D310 V310 0310 B310 B300 B110 Bno ono Bno ano B1110 U311 B1700 Uno Bno BHOD B
13-32-1
100-02-7
- 121-14-1
14-44-270*5-72-304-73-7lDO- f l t - 4314-31-10 4 - 3 0 - 4lfll-53-1111-74-117-14-503-01-0120-12-714-74-1201-44-0121-00-005-11-7
S4-I5-!117-11-7111-01-1117-14-0205-17 -2207-00-150-32-1
33-70-1111-14-2
c i r c l e o n e )N O ) < c i r e I e o n e )
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D i t t h y ! fb th i l i t iethn
4-HitieaBiliBt4 , 1 - D i B i t i o - l - n i t B T l p b . i n o lM - B i t r o f o d i p h i t f l * a i i e ( I )4-lre«ephtBTl-pkiBfI tthtrHciachla tobtBi ta if cBtac i l e topBiBo lFktBlf t t l t tBt
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(l)-Cinnot be fepirated from diphenyI mine
FORM 1
Case No
Orgonics Analysis Data Sheet(Page 3]
Concentration: C LowJ Medium
Date Exiracted'Prepared:
Date Analyzed: ______
Pesticide/PCBs
(DVcte On«J GPC Cleanup QYes'ONo
Separalory Funnel Extraction
Continuous Liquid - Liquid Extraction OYes
Cone/Oil Factor:
Percent Moisture (decanted)
oocr>
CASNumber319-84-6
319-85-7319-86-856-89-976-44-8309-00-21024-57-3959-98-860-57-172-S5-972-20-633213-65-972-54-8
1031-07-850-29-372-43-553494-70-557-74-9
8O01-35-212674-11-2M1O4-26-211141-16-5
53469-21-912672-29-6
MO97-69-1
11O96-82-S
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oIi a .
f Ho M a u 10
w ; o .' ' . >M• »4 ' W **H
n'i n «j
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— O M —— I—— W L
I I I l i t
I I 1 I I
S r »5 ^I "I - - : .5 £
•- .— 1 o —
iiffii 819^ — ft « 2 " B3 S S -2 B g-^ ft
• «v . o
L a b o r a t o r y . NineCast No: 7351
ENVIRODYNE Staple Number: EM870
Orginics Analysis Dati Sheet(Page 2)
Stmlvolitili Compounds
CFC Cleanup NOD a t e E i t r a c t e d / P r e p a r e d : 0 7 - 0 2 - 8 7 S ep .D a t e A n a l y s e d : 0 7 - 1 4 - 8 7 Cen tConc /D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 1 5 3
CIS No:
101-73-2111-44-493-57-8 ,
—— — 341-73-1.
fhtaolk i i -O-CBloro t ta j I ) « th i r2-CkIorapataoI .l ,3 -Ditklor*btai ta i -
"~--~ ~ 184-44-7 --l-,~4-Dicflttr«ktnieni - . . - - : r~-X-. — -^88-31-4 . %--. Ji 75-38-l_ . ._ - ; -7. ~ " "73-48-7 ---1 39433-32-7
184-44-5421-44-747-72-178-75-373-37-188-73-3103-47-713-85-0111-91-1UO-03-2128-03-1
rg 71-28-3g> 101-47-030 07-40-3_ 39-38-7,:> 71-37-4
> 77-47-4rn •»-•*•*l7j 93-95-4> 71-38-7UJ 00-74-4O 131-11-3gi 208-94-0
77-09-2
UBIJI i iccioi . „ ...„.._; -:.1,2-DiehlotobiBiiae ; . ._ .2-Httkf rpkiaol, :;-.'.'. "-'•kis-d-CUflroifoptopyPitaet4-IUthf lpbiBolK-a i t rBSQ-Di -B -prop j i i a iB tRi i tca loTBithtBtNittobcottaiInphoroBi2-HitrvpkiaolI,4-DiiitayIpflta«Ileaioic Icidkif-(CkUi«ttboiy)Kttkui2 .4-Dichl«ropatao ll ,2 ,4-7richUr«btBtffatKipathil iBi4 - C k I o r » a a i l i a i•• i icBl«r*bBtidi iBi-Chlor«-3-«tbj I p k i a o l-HithfUipfithilinii i i cb l o r e c f t l op i a t td i iB i,4.4-TtickUropbeBol, 4>5 -Tr i ch l « t opbcao t-CkUrt&apbUaliat- K i t r e i B i l i B *
OlMtbfl BBtk i l l t tICIBlpUyltBI3-Ki troa i i l i a t
•Ikl
390 0390 B390 0».* "
. ...370 0^ ;^*370 8-• r"^ J« B
370 1 . - -390 8 . --"390 V390 0390 Q390 Q370 8370 8370 81700 0390 Q390 Q390 V390 8398 8390 8390 Q390 Q390 8390 81900 8390 U1700 8370 8370 81700 8
Funne l E i t ri n L i q - L i q
CAS No:
03-32-951-10-3100-02-7132-44-7
- ', l2i-(4-2•'lY-S.M
" 8 4 - 4 4 - 2^ - 7005-71-3
•"-' 84-73-7 _"180-01-4534-32-104-30-4101-55-3110-74-137-04-513-01-8118-12-704-74-2204-44-0129-00-005-41-791-74-134-55-3117-01-7211-01-9117-04-0183-99-2207-00-950-32-0193-39-553-78-3191-14-2
a c t i o n : YES (N^X c i r c l e one >Eit . : YES (^Jo)<c i rc l e o n e )
I
IcutpbtatBt1 , 4 - Q i B i t i a p k e a o l4-Hitropb.tBolDiktaicf t i ia~274-DiYit"r«t~6lBiay " ' —2,4- jDi f i i t iaUJBiacBiitkyl |ktkiliti "" •" •• —4-Cklerepb«Bjl-pi iBji ethir * _FlBortae4-Nit ie»iI iai4, 4 -Dia i lr •-!-«• tkj l phenolM - a i t r o f o 4 i p B i B T l u i B i ( 1 )4-8ifl iopkiB|l-phiBjl ttherHiiackliribtaicBfFeatickleropbtaol?k»tatkriifietkneiMDi-i-ifltyl ibtkaLite (f l ie i tatkcBiFjteailBtT>ktaiTl- |btki lattS . J ' - D i c h l f l t o b i D i i d i i il iBiofaUatkt ietaik i i - d - C t k y l k t i j D p h t b i l i t fCkryuniDi -B-oc t j l ik th iUt iliaia(b}(lBor«Btbtflt8 i B t « ( i l ( I i o t i a t B C B i8ffaieU)pfttBBIa4tao{ l , l , 3 -e<}pfr iBCOikiaiB(a,k)tatkrtccBiI tB tB tak i l p i t f l t a t
9^
390 8tw u1900 8394 0390 8iib'T398 8390 *« ;398 8not 81 9 0 0 8391 8390 8390 81900 8390 8
JUSD010M
*T7O390 B39G 5710 8390 8710 8390 839G 839G 8390 8398 8390 8390 8398 8
(l)-Cinnot be separated from dipheny1arnint
FORM 1
Case NOOrganic* Analysis Data Sheet
(Page 3)
Concentration. -Ow Medium
'7 "-
Pesticide /PC Bs(Circle One) GPC Cleanup QiYes'ONo
flail- Annlyr^- , , "7- JO - V7 <-ftni;
rnnr/nif Parlor- I
Pf rr*nt Mnicfiir»(H»rxn^ri) 73. J
""-' _ - - . ^ ~ ^, -^ ^ _ — ^
_ .—•--:, — - -ryr- rr-rirrL'-- ~— : *._ ~- ~ --»-• t"T '- '• J?fr— ."-sf= -i-'
.-•.ST.-TTT=: " :--, •:- .-).--- = - ---
--'::-.-^—— -------- -• ••"—— - " '
•
r*-CO
. - oo.
CASNumber
319-84-6319-85-7
319-86-856-89-976-44-8309-00-21024-57-39S9-98-8 -60-57-1— -72-55-9 -72-20-833213-65-972-54-8031-07-8
50-29-372-43-S53494-70-S57-74-98001-35-22674-11-21104-28-2114I-16-S
53469-21-92672-29-61O97.69-11O96-82-S
A(phj-BHCBeu-BHCO«UJ-8HCG<mma-8HC{Lind>nelHeouchlocAWr.n
HeptacMof Epox*de
Oteldrfn- -*-— • v - -. - -• -4.4*ODE-Erttfrin '• —EndosuKan II4. 4*-OOOEndoso fan SuKate4.4--DDTMethocvchlorEndrin ICetoneOi'ordJne
ToKjpneneA/oclor-1Ol6A/octof-1221A/ocior.1232Aroclor-1 242
A,OC10'-1248
A^oCtOf'1 2$4
A.ocKx-1260
luous Liquid.- Liquid Extraction QVes
~~ (CJrctotJneJ
!(*.& U.H.O /A11. 0 VL.
. ]b.(? M
/A'P »A/*.p U
^°-*<'
-2i.^ ^V,O UJ^-i? U
- sJ3^> UJ-P*0 It
33-0 Kr Ti.c) U
/60.*> U.JJ-O «/£,£.£ U
JUd. > U; .<9 Ullt>.o U&£,A U
I&O.O UMAO UJ 3 <?• 5 £(2*>&a O UL,
. __ V. s Volume of exif *CI *n|ecled (ol)
^ V = Volume of water extracted (ml|
"™ W * Weight of cample extracted (gj
LUfy, V * Vofume at total eciraa (ut(
-! —————————— -..i.™. ——— --'.-I- ——-—— --
t---^=^a"^^^--^---r:;:--^-- ---" -"fe^T"
r - _ . - ; . - . __ , —— .^ - , . . -
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ofW.
7/85
Organic* A n a l y s i s Data Shtit(Page 1) !--
Sample Number: EM871
La b o r a t o r y Nime: ENVIRODYNELab Sample ID No: 87003295Simple W a t r i i : SOILDatt Rtltait Authorixed By:
C a s e N o : 7 3 5 1Q C R e p o r t N o :C o n t r a c t N o : _ _ * £ ? 'D a t t S a m p l e R e c e i v e d
V o l a t i l e C o m p o u n d s
C o n c t n t r a t i o n : L O VD a t t E i t ne t t d / P r e p a r t d :D a t t A n a l y z t d : 07-01-87C o n c / D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( n o t d e c a n t e d ) 23
CIS tat;« « 3 «74-d5?-3
"74rl3-?17511-4
Cklorometkaae 13 B13 .B
CIS No:•CCSCSXI
71-17-3 1 ,2-Diek lorepropaactrau-l,3-DieUTtitkloreetktae
:DiSremetfc_UrflmeSS]Siil-'«^"^^ ;Jek]ereelkrBV
73-14-3
(7-U-3117-14-27I-V3-371-35-4
111-13-473-17-4
-._,.—. 5 s^-__,—-. :«a»»wwre.T»rt«>
I , l - D i c k l « r c i t k a a et r aBi* l , l -DickI f l r»e tkeaeC n l c r o f o i B1,2'DiekIetBttkaail-litai«Be1,1,1-TrichUroithiBiCtrbflB
Ice ta te
BU0B
IS 04 B< 6U B( B
73-15-Jlfll-ll-1Sfl-71-4117-11-47»-3<-3111-11*3111-90-7llfl-41-4llt-42-3
IrnitoiB ,. ; • :
4-RitkTl-:-i iBtaBOBt2-Eiiaa0BtTitraekloroetheael,l.].2-Tetrack!ireetkaaeTelBeie
ttkylfceaieatStficaiTetal Xy l iae«
Data liportiBf Qvalifiari
If tkt molt is a raise oreatet tkaa *i eqaal to tke ittectioatiiit, rcftit tke raise.3:ladicates ctipoiad wai aBtlftetf (or kat aet detected lei«rt tkeaiiiBQB iilictioD liait (er the laiple vitk tki B (*{.1IU> kastdIB leceiiarr eoaeeat./dilatieB actioa. CTkis is a«t aecmarilitat iBitrnint ditectioB limit.) T&e faotneti ikoald tiad: 0-Ceipoaad «as aialyied fer kat aet detected. Tke anbir ii tkiliiiita atttisakle detectiea liait for tke taipli.J:Indicates aa istiiated ralai. Tkii Hag ii ated eitker vseaestitatiaf a c«aeiatratioB for tiatatifilv ideatified toapooDdivkiri a 1:1 KSIQBII is assvied or vkca the »is tpeetral dataiadicated tke iteteace *( a tOBpoand tkat Beets tke idffitifititioncriteria lot tke resalt is less tkaa tfci specified d e t e c t i o n ItaitIteater tkaa ser« (eg, tO J > . If limit *f detictioa is ID aot aad aeoiciatratiaa of 3 a«l is calcvlatid, report at 3J.
Tkis (lag applies te pesticide parameters wfteie the identifica-tion wii eonfiind |y CC/IU. Single coipoBtat pesticidcs}>10
la tke fiaal attract skeaid ke confirmed by CC/K5
Tkis flag is iscd VBIB aaalfti is fo»d ia bliak is xell as asample. It iatfieatas pessikle/prokakle bUnt ceataaisit ion aadwaras tke data asec te lake ap p r o p r i a t e actioa.OTHll:Otkir lligi »Bd f*otaetcs aij ke required to prepeily definetke resalts If ised. tkej mast ke t a l l y d e sciibed aid sackdescription attacked te tke data ssuary r e p o t t .
ka t
L a b o r a t o r y - NameCase No: 7351
ENVIRODYNE Sa*pU Number• EM671
Organic* Analysis Data Sheet(Pagt 2)
Semiioltt ile CODpounds
Concent r » t ion ; LOVDate E i t r a c t e d / F r e p a r e d : 07-02-87Date Analyitd: 07-14-87Conc/Di 1 Factor : 1Percent Moisture <d e c * n t e d > 23
CIS Ho vgtg
CFG Cleanup : NOSep funnel Eitra c t i o nC o n t i n . L i q . - L i q . E i t .
US Ho:
c i r c l e one )N o ( c i r c l e o n e )
•gkg
10l-?3-2I11.44_4__
•*:-^$j&2L^•SZ-itiLffi'^
-:.-;r.--M-SI-l-«i^r
- . t^_''"-'*i.f 3-41-7 --^-^~7 39433-32-f
104-44-3421-44-747-72-110-15-371-Jt-l10-73-3103-*7-»
^ iJ-OJ-03 111-M-l30 120-13-2-*^ 120-03-1
r-r» f l -3f l -3"3 104-47-0Q 17-41-3UJ 31-30-7> '1-37-4UJ 77-47-4
UJ "•"-'0? f3-)S-4
91-31-701-74-4131-11-3200-H-3Jf-01-2
Phenolkii-(2-CUor»ttkTl)etker .
^3^icBj.r.b,.»».:=~a
lti.nl ilclk<^-==^-':^-^^4 .2-DicfcIertftjftsMi .^^':^-3-HttflTlBklBttl~'^'r~"~" -±^~?—
k i i - ( 2 - C k l o i < i i o p r o p f l ) e t k e r4- f Ie tkyIpbiaoIN-Btt roso-Oi-B- i ropyla i iBiHnacklereitkaaiXit robe&t i f ieliflBkeioaeJ-Ki t rophtnoI2 ,4-Dt i i tk | lpkcBBliBBioic Acidh i i - (CkUui tke i j )Kt tkaBi2 .4 -DickUropkiBol1 ,2 ,4 -Tr ickIe rob tBt iBf lKapbtha l t a i4-ChIoMiniIiiiHt i tchlotobol id icB*4-Ckl« ro -3 -MtkyIpk iBo l2-Ht thy lBipb tb i l iBCHeiack lo r scyc I tp iB tad icBi2 , 4 , 4 - T r i c k l o c o p k t B o l2 , 4 , 3 - T r i c b l e r o p k i B o l2-CkIor iBapktki leBe2-Ki t re iBi l iB iDi»tkf l p k t k i l a t eAciaaptkfliBi3-Ni t reaBi l ia i
430 0430 V
-J! -^431 P^-y^-^^S'ct-ipss :U 0 -$S-^-^^z7
«^=._4IIJ -.ste^hTfi-JT~- -' 430 0 ' ' -— -*• ~~ •-- •. -• .""«• 0 '"^"rr^T^'
430 0430 0430 0430 0430 0430 0430 02100 0430 V430 0430 V430 0430 0430 0430 0430 U430 0430 02100 U430 02100 0430 B430 92100 0
13-31-131-20-3
»*•*«££
&MA.M-;fi%i-i7 OB 5-72-314-73-7-100-01-4334-S2-104-30-4101-53-3110-74-117-04-303-01-0120-12-714-74-2204-44-012f-00-003-43-7M-H-134-35-3117-01-7210-01-f117-04-0205- f f -2207-00-V30-32-1lf3-3»-333-70-3ltl-24-2
ittaapbtbiBf2t4-Diaitt«pkiBol .
^^llmys^^^g:^^7^DiiilitTtilI^i}-^^Kik;-=*i«lkTl •kikiUte;Iu^i:-.i-:--.itI .. 4-CUiTifitByI-pktifl etkir - :----^TllaoteBe .^-^.iLs^-iV-T ' .'l'..7;^;V '-.-.
4-Mitr»4BiU«4.4-Dif l i t ro-2-HetkyIpkiBoI1-aitreiedipkeByUiiii (1)4-IrciepbiBfI-pfcinjI i thtrIlIiCkIlC»blBIIB«
PeatackltroBkeaelPkeButkriaeAatkractieii-B-bitfl yk tk i la teflioraitbiBiPyrcBil i t f l -keas f l - ik tkaUt t3,3'-DickIirebiBiidiail»ie(>)aBtkraciae» i i - ( 2 - C t k f l k t i y l ) p k t k a l a t iCkiyiiBiDi-B-«tt j l p k t k i U t el » B t « ( b ) ( l B O r i B t k « f l C
l i a i « ( k ) f l B i r a B t k c a il*Bi«(a)pyr»«l B < » o ( l t 2 , 3 - e d ) p T r t B eO i k t B s o ( i , k ) a B t k r a e « a iliiitffkilpiryUae
430 0^ 2 1 0 0 V _ . .
m**j>&^1! JW,-ir_«30.B^-^;
>;r.«JD «-—--:. ' "_ 430 0 .-"::'•'••'-
2100 D2100 0430 U430 0430 02100 0430 U430^
/tiT)^Htt-li
430 0430 U040 0430 0110 8J430 U430 U430 0430 U430 D430 0430 0430 0
( l ) - C a n n o t b e s e p a r a t e d f r o m d i p h e n y l a n i n e
FORM 1
Laboratory
Case No _
Ac..
iOrganic* Anatysis Data Sheet
(Page 3)
S *mpl« ,/yu m txo r
Concentration. C LowJ Medium
Date Extracted 'Prepared:
Date Analyzed: ______
Pesticide/PCBs
(Circle One) GPC Cleanup QYes ONo
Separator* Funnel Exuacjion OYes
Continuous Liquid - Liquid. Extraction OYes
Cone/Oil Facior:
Percent Moisture (decanted)
-^M^»-—---~^;;^^^^?^*-^-^~--
•• r .._- ui. — ;'±;, — -"".-•.-'• r.. ,>."•_ -1_ ' . . " " • - -* '•* —
K8«
«.."Jj
a£a]ou;or
CASNumber
319-64-6
319-85-7319-66-858-69-976-44-8-309-00-2 :1024.57-3-959-98-8 —60-57-1- ---:-72-55-9 .72-20-8 -33213-65-972-54-81031-07-850-29-372-43-553494.70-5S7-74-96001-3S-212674-11-2111O4-28-211141-16-5S3469-21-912672-29-611O97-69-1U096-82-5
Alpha -BHCBeia-BHCDeha-8HCGamma -BHC (LindaneJHeouchlof •- ---^.-r-AWfin , -.—--, ^_
HepiacWof Epoxide ^rtr-—Endosulfan 1 .-.-- -t -^yaiOiefdrin- -.••• " . --•'.*.-.-?=.4.4--OOE —- — ••--Endrin ,
EnoosuHan 114,4'-000Endosuffan Suttat*4.4-.DDTMeinoicvchlorEndrin KeioneChlordaneToKapheneA/octor-1016Ajoclof-1221Aroctof-1232Aroctof-1242A/oc(o**1248Aroci<K.12S4
Aroc«K-1260
**0/lof^q/Kg(GreUUo<
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33.0 U
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V. x Volume of extract injected (ul)
V * Volume of water extracted (mil
W * Weight of ta'mole extracted (g|
V * Volume of total eciraa (ul)
Form 1 7/85
ecology and environment, inc,111 WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
Date Received for ReviewTo:From: Zena Gold-Kaufman?^Subject: HOD
PAN:
Date Review Completed 9 Q| OT~
Case I
Sample Description______Organics (VOA, ABN, Pest/PCB)
Low Soil (JJILow WaterDrinking WaterOther
Inorganics (Metals, Cyanide)
Low SoilLow Watert-Drinking Water-Other
Project Data Status Completed!
Incomplete, awaiting:
FIT Data Review Findings:em
/e tec-ted aHf\|| 6I\fl deeded noid/nfeKfv f€,\€cted^ fcrrReviewer flagged
det d
results-far em 8?,for
Book No.
Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.
Page No. \^
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V
•JSJECT: Review of Region V CLP Data Q ,^ . Q~7Received for Review on O ~ «^ " O /
SOM: Curtis Ross , Director (5SCRL)Central Regional Laboratory
'0: Data User:
We have reviewed the data for the following case(s).
SITE NAME: HOD LANDFILL _______ SMO case No. 73S1- . No. o f T D . U . / A c t i v i t y
EPA Data Set No. or ^t\too Samples: \) Numbers _____________
CRL NO. 8"1FP\\SZ4 - 528____________SMO Traff ic No. EM 8"?2 - Slfe____________________
- — ; M r s . R e q u i r e d ,CLP Laboratory: ENV\RODNM£_____________ for Review: AHQ
Following are our findings:
r/ ( 5^0
( ) Data are acceptable for use.(y.) Data are acceptable for use with qualifications noted above./**( ) Data are preliminary -pending verification by Contractor Laboratory^(Xj Data are unacceptable*. yo AS fl/V/Ji £K ^M *'x?i efa**Ji fi'Ali"Tt<
cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas
EPA FORM 1320-6 (Rev. 5/87)».v
DATA QUALIFIERS
Contractor: 73 J/
Below ts a sumap/ of the out of control audits and the possible e'ffect. on the tfata for this case: .
- C
»7
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7 1
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Phone: 3
At ; fc^ T*.trir* f /I ¥/? 7
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DATA Q U A L I F I E R S
Contractor: £"K»>'I v<? c«e73r/Belo* Is a surmarjr of the out of control audits and the possible e'ffect
. on the data for this case:
O\5. C~(;
C*/ 1 -r
JJ/LT" 4£*'
^ n *-
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"•••f iA.i
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Reytexed
Phone:
DATA QUALIFIERS
Contractor: C'se T35Y
Belo* Is a sumnar/ of the out of control audits and the possible effect ^U .. on the data for this case: *x\x*o
A 1 /^ l/a/lfct J.
ftISAM
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57 5** CUlff 1-1 C-4 U/
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lK (f) o__^ ^T7
by:
Phone:
DATA QUALIFIERS
Contractor; C.se
Belox Is • summary of the out of control audits and the possible effect. on the data for this case:
5. sc%_-»-j*' •tLf-o.T*
»•»
re, £ At• OK .
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RevTe-ed
Phone: O?
DATA QUALIFIERS
Contractor: £****+* <fy* <- Cisec£
"7.
Below ts a jurmap/ of the out of control «udfts and the possible effecton the data for this case:
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*.*•&. 't
S^.*r-ftc*-fl
J. *s+*.
2O Oil T
— -/At.100 /«-SS 4- k.*
30.
LS*
flj-fHO
Reviewed byt
Phone: ra
t c r
CASE?
U N I T E D STATES E N V I R O N M E N T A L PROTECTION AGENCY R E 3 I OC A L I B R A T I O N O U T L I E R S
SEMIVOLATILE HSL COMPOUNDS(Page 1)
____________ CONTRACTOR £W?v-o«gy
Imt . C a l . ICont , C a l . J C o n t . C a U I C o n z . C a 4 . I C o n ; . C a l
IRF IRF |% RF |RF i R rPhenol
JEtner2-Ch io rooneno
Alconc1,2*31 entorosenzsne2-Ve'nvionenotbisU-cnloroisoDPoovi4 - M e t n v i D h e n o iN—Nil ros o-DI *n-rroov1 arm neHexacnloroeinaneNitroDenzeneIsoonorone2-NitPOOhenol2,4-Oimethvionenol y\Benzole Acidbisl2-ChloroethoxvjMetnane2,4-Oichioroonenol1,2,4-Trlen t oropenzeneNaonrnaiene4-Chloroaniline P/ICHexacnloroDutaalene4-Chloro-3-Metnvlonenol2-MetnvlnaontnaleneHexacniorocvclooeniadlene
2,4,5-Trlchloroohenol2-Ch loponaon tna i ene2 - N i t r o a n i l i n eDimethyl Phina lateAcenaontnvlene T \3-Nitroaniline 34 rAceraonthene2,4-DinitrQonenot4-NitPoonenoO i D e n z o f u r a n
AFrZCTEDSAMPLES:
* These flags should be applied to the analytes on the sample data sheets
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDSPage 2 - - -•• -
CONTRACTOR £**'*•-
'
QATE/TIME:Inlt. Cal.
Rr! 2,4-DirntPOtoluerie
2,6-DinitrotolueneDie'nylontp.alate4-cnlcpocneivl-pnenvletierFiuorene
' 4-Nitroam line4,6-Dinitro-2-MethvlohenolN-Nitrosccioherwlamine4-BPcr,c-r.5nvl-onenylethepHexacnlorooenzenePentachlopoohenolPnenantnrene
i AntnraceneDi-n-Sutvlohthalate
•RSD w
Cont. Cal. lCont. Cal.lCont. Cal .1 1
RF ID * IRF
59 T
Fluorantnene tPyreneButvlbenzvlohthalateBenzol a ) Antnracene 1bis(2-Ethvlhexyl)PhthalateChrvsene
1
i01-n-Octvl Phthalate 1 1Benzo(b)FluopantneneBenzo(k)FluopajitheneBanzota JPvreneIndeno(l,2,3-cd)PyreneDlDenz(a,h)Anthpacene-Benzo(a,h,1 ) Pervlene
11
t
10 1- |RF1
I1 111
1 111
11t
t 11
ID *
Cont. Cal . >
RF
1 11
11 t1 1 '
1
t
10 *
•
1
1
1
1
SEE PAGE 1 FOR AFFECTED SAMPLES.
These flags should be applied to the analytes on the sample data sheets,
1/87
ENVIRODYNE St LOUIS Mssoun i3146(314)434-6960
\
1n
nu11alrndddddd
August 7, 19871990-7351
Ms. Carol Schaeffer ^^ •- ..Sample Management Office 52$ - ",**• -i209 Madison Street, Suite 200 ''"'•••iJj "' * -Alexandria, Virginia 22314 '" ''Ui/y-j
Dear Ms, Schaeffer;
Enclosed are partial results of analysis of Case 7351 for volatiles, BNAsand Pesticide/PCBs performed by Envirodyne under Contract Mo. 68-01-7087,Five soil samples, EM872 through EM876, were received by Envirodyne onJuly 7, 1987.
The semivolatile fractions were screened for concentration levels by GC,and extracted by the low level method. Because surrogates were out ofcontrol on the SNA blanks from the original extraction, the SNA fractionswere re-extracted on July 30, 1987.
A matrix spike and matrix spike duplicate were extracted with all fractionswith these samples.
If you have any questions about this report, please contact me.
Sincerely,
Margaret C. WinterProject Manager
MCW/jagEnclosures
PAGE OF
Case: 7?
Contractor:
TENTATIVELY IDENTIFIED COMPOUNDSWATCH ASSESSMENT
NOTE: Reviewer should note directly on Organic Analysis Data Sheet (OADS)those matches that in his opinion (based on contract criteria) areunreasonable.
CRITERIA
(1) Relative Intensities of major Ions (>IQ%) reference spectrumshould be present in the sample spectrum.
(2) Relative intensities of major Ions in sample spectrum should.agree to within +_ 20% of reference spectrum intensities.
(3) Molecular Ions present In reference spectrum should be presentin sample spectrum.
(4) Ions present in sample spectrum, but not in reference spectrum' should be reviewed for possible background contamination or
presence of coeluting interferences.
(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelutinginterferences.
(6) If, in the reviewer's opinion, no valid Identification can bemade the compound should be labelled as "unknown" and the initialsand date of the reviewer placed on the OAOS.
Reviewer's Initials/Date: ~<$sfcAz* ">*>•• w**l y3//?7
CONTRACT LABORATORY PROGRAMDeputy Project Officer Communication Summary
-I .Date DPO Notified of Issue; ?'t'-f7 DPO Notified By: r">Tr •f^'-~' <*
Subject Laboratory: £A/'.W 3 &.VMeT __________ Case/Sas No: 7^
Contact for Resolution:(Laboratory or PO)
Date of Contact: _______________________ Call or Visit (Circle One)
Summary of Issues & Resolutions:Document the issue(s), resolution(s), and action deadlines, if any.
<? 7.35V C^VC/rr-O o,c .Tg/fgf a*
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0-Signature ^ -Date
Region
(1) DPO Copy (2) Project Officer Copy (3) SMO Copy «0 Lab Copy
5/3*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 3REGION V <
DATE: /-J7
SUBJECT: ^^c gesPv***- TV &£* 73-SV
FROM: "
TO:
'3
EPA FORM 13204 (REV. 3-76)
Cait No,Low—
SOIL SURROGATE PERCENT RECOVERY SUMMARY__ Contract Laboratory £lu)ig.QPWtt£______ Conlrtcl No.
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7/86
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Contract No.
ritf Of t t tO f U A f A l l Mil. 10 CM Muvica COMPOUND IHSL.tIC OH UNMNQVHI CONC. umtt
W.n t O.W.6U (b \0ll '0
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SAMPLE NO.
£ YY&f?)**-;/• lo/£?\
COMPOUND
1.1*OlcN)k>r«th«nf
Trichlofotth*™Chlorobcnitn*TolutfltBtnitnt1 ,2.4-TrlchlorotxnicntActntphlhcnt2.4 Dinilrotolutr*PV'in*N-Ni|ro«odl -Propylimine1,4-0ichlorobtni«n«PtnucKloro phenolPhenol2-Chlorophenol4.Chloro-3-M«thylphflnol4-Nilroph«nolLlndmeHepuchlorAldrinOitldrinEndrin4.4'.OOT
ontrtctnr B-UVMdODY
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RECOVERY
50.17262-13760-13359-139M-14738-10731-13728-8935-14241.17028-10417-10920-9025-10220-10311-11440-12735-13034-13231-13442*13923-134
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Laboratory Naae: ENVIRO&YNECase No: 7351
Saaplc Nu*oer: EM-37
Organic* Analysis Data Sneet(Page 3i
Pesticides I PCS s
Concentration: LOWDate Extracted/Prepared: 7-23-87Date Analyzed: 7-28-97Conc/Dil Factor: 1Percent Moisture (decanted): 21
CAS Not
6PC Cleanup : YESSep. Funnel ExtractionContin. Uiq.-Liq. Ext.
uqkg
J
I
31H4-6319-85-7JlH!6-fl**•• f-J- ftJD un7 -44-4309-00-21024-57-39SHHW-S7-172-5H72-20-8JC13-6H72-54-81031-07-fl55-29-372-43-55S474-7M57-74-98001-35-212474-11-211104-3-2534&7-2HS34i9-a-912tf2-29-i11097-49-111096-C-5
AlpbHHCBeta-Ktalta-ftCfiMirflt (LiixtaniiHqtaddorAltHnh rtichlcr EptnidfEndosulta IKeldrin414'-UEEndriiEnkBulfan-U4,4'-R»EnkKuliw Sjliiti4,4'-OOTHrttacydilDrbdrii KrtoneDOcrinTou«ttmfrnJx-1016DrKla-1221fcTtlir-1232fc-xIx-1242AnxUar-124a«rodcr-[254frTClor-m
20 U20 U2flU20 y20U20 U2DU20 U411)41 U41 U41 D41 U41041 U200 U41 U200 U41ft U2DQU200 U200 U2UU2MU410 U410 U
A'1 *•*»*.*srrt*****'*rr .-Afc^'TS
30 9
Vi « Voluae o^ extract injected <ul>Us » Weight of caaplc extracted (g)Vt " Volume oi total extract (uli
Vt " 40,000 ul
FORM 1 ^
Vi « 2.0 ul
Laboratory Naae: ENVIRODfNtCase No: 7351
1 5 a « p l e N u « o e r ; En 573
O r g a n i c * A n a l y s i s Sata sneel2i
106-15-2UM4-495-S7-S5*1-73-1104-4o-7100-51-tt95-50-195-«-739435-S-9104-M-5421-64-747-72-196^5-378-59-1B-75-5105-87-945-fi5-0111-fl-l120-83-2120-82-1tl-20-3lflo-47-fl
Rwnol
2-QilorDptiflml'
l«4-OicMcrc6cn:awBnyl Alcohol
2-fetnylphnlfcis-(2~0ilarmi^re?yl)ethir4-flRhylphmlIHri troscHH-tt-prDpy laai MteadUtroeth**tfi trot BIT meIfi narane
2,4-OiHthytphBiolfinoic Acidbii-(0>!xoettitBy)Hethane2,4HHdU(ropn«nol
5"r-50-791-57-877-47-4BB-Oo-2
HBadUxawtidient 'H1U (TQ-3-wthylphHUl2-ntthyInapttthaJm
71-3-7 2-QlatnaphthalBWB&-74-4 2-tetroafuline131-11-3 Kvtfayi20fl-9e-fl Auruptnyli9M9-2
Seaivolatile Compounds
Date cxtracttd/Fr*par*d: 7-30-S7Datt Analyzed; 6-5-B7C o n c / u i l Factor; 1Percent Moisture (decantidi: 19.7
CASHo:
410 U410 U410 U410 U410 U410 U410 U410 U410(1410 U410 U410 U410 U410 U410 U410 U2000 U410 U410 U410 U4101)410 U410 U41011410 U410 U410 U2000U410 U2000 U410 U410 U2000 U
6PC Cleanup : NuSep. Funnel E x t r a c t i o n : YESContin. Liq.-Liq. Ext . : YES
CAStfc
BS-3M31-2&-5
121-14-2406-20-2B4-6&-27005-72-386-73-7100-01-4534-52-1Bb-30-6101-55-3118-74-1B7-84-585-OH120-U-7W-74-2204-44-0129HJO-0B5-4B-7fl-^4-1Si-55-3117-81-7218-OH117-W-O205-W-2207-06-950-32-8W3-3W55-70-3191-24-2
2,4-irinitrcpnBial4-MtrapiiBialDibfraonran214-DiaitrotaluiM
4-NitnBnilin>4,fr-Oiutro-2-flIHutrosxtipcwnylaiiH (It
FcntacUoropmnalw
pbthalati
Pym
bis-(2-EthylnBylipnth4latiQrysmDi-mctyl phthilitiharo(b}ftooranthmlnB(UHuranthm
Indm 11,2,3-cdJ pyrwwtitauo u,h) anthracint
(U-Cannot fa* separated froa tfipnenylaaine
FORM 1
410 U
20COU410 ij410 U410 U410 U410 U410 y2000 U2000U410 U410 U410 U2000U410 U410 U
410 U410 U410 Uazou410
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Laboratory Na«e: ENV1RQQYNECase No: 7551
Saaple Number
Organic* Analysis Data Sheet(Page 3)
Pesticides I PCB i
Concentration: LOtaDate Extracted/Prepared: 7~/f-Date Analyzed: 7-21-87Cone /&i I Factor: 1Percent Hoisture (decanted):
7-/f -f^
d): 20
CAS No:
31W4-*31WS-7319-flW•» na a3dTT T
74-44-fl309-00-21024-57-3»• »*> *Ul III U
40-57-172-5W72-20-833213-6H72-54-fl1031 -07-850-2^372H3-55M?4-70-357-7W1001-35-212&74-11-2m04-2B-25S4»-2l-f5S4W-21-9Uo72-2KUOW-4WlIWh-a2-5
6PC Cleanup"- Sep. Funnel
Contin. Liq.
Alpha-filCBeta— tKDriti-BCS^a-BC (UndxieJhpUchlirW*iflWaddv ResideEnksuH»IKrldriB4,4'-90EEheriiEndoailfarrll414'-OTbdoulfan Sulfatt4,4 '-HOTIhUatydilorEvHt KrtaneOtlcrdantlaaphiM•nclor-lOUfrttl a-1221(rrdx-lISZArodcr-1242frodx-1246*roclor-l234ftTTltr-UW
I YES -. ——Extract ion : YES VJlflMcircl e onei-Liq. Ext. : YE&^TSd iTii r cle one iV_X
ugkg
201120 U2DU20020 U20020 U20 U40U400401)40(140040040 g2000460200 U400 U2000200U2001}200 U200 U400 U400U
Us * 30 9
Vi • Voluae of extract injected <ul>Hft * Height of laaple extracted (q)Vt « Volume of total extract (ult
Vt " 40,000 ul
FORM l"
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17
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Organic* Analysis OaCa Sheet(Page 4|
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Laboratory Nane:Case No: 7351
ENVlRODYNE Nu«0f: En-674&:urganics Analysis Data Sheet
(F1 a g e Si
Pesticides i PCS s
Concentration: LOWDate Extracted/Prepared:Date Analyzed: 7-21-87Conc/Di 1 Factor; lj | 0 *"Percent Moisture ide^ante
6PC Cleanup : YESSep. Funnel Ex t rac t ion : YE5 fNQVici rcl e one)Cont in. Liq.-Liq. Ex t . : YE5 f "Nu j c i r c l e one
CAS No: ugkgia = e=s
Alptu-3(C
[ ^^_ ,
3I7-35-7
•K -Ml H3D OT T
74-44-fiJOHiO-21024-57-3
W-37-i77-SW72-2H
72-54-6KOl-OT-fl
7H3-55H«-70-5S7-7HfiC«l-3S-21247M1-211104-26-2
DfltHtCEuu-fitC dindane)
EpoxidiEndosultan IDitldrin4,4'-OutEndrinEnoosuliw-ll4,V-OWEndoul{» Sulfati4,4 '-WTIMtayctdorEndriilCfftantOilontantToiapfctntAroclcr-lOla
11W7-6M1109o-82-5
Arxlor-1242frodor-1248Aroctor-125*
160 UIBuU
180
18 U18 U
36 U341)liU3iU180 U36 U160 U3WU160 UIfiOU160 U160 U160 U
^f[*
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Vi * Voluae ot extract injected (ul/Us » Height of caaplt extracted (g)Vt " Voluat of total extract (ul)
*D.|. IMOVt * 40,000 uL
FORM 1
Vi > 2.0 ul
I*i*4r1
J-0i
J!J
I31i a
I 1
3
LaboratoryCase No: 7551
. S"""/* *r .1
ENVIRQDYNE -----Sanp1e Nuaoer:
**J7 * s e*T(*-Organics Analysis Data sheet;»c<- A •/•*•'"?
.faeatvolatile Compound*
(U-Cannot bt separated fro« diphenylieine
FORM 1
•u,-
1 e ^ i * Ih V ^h I" — . - » . —
L-fS u/tv «•»•*- ^J "AA
C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : 7-30-67Date A n a l y z e d : 8-5-87Conc/Di 1 Factor: 1P e r c e n t M o i s t u r e { d e c a n t e d ) : 4
CASfc:
106-45-2111-44-495-57-e541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5421-64-767-72-196-95-378-5H68-75-5105-67-945-85-011H1-1120-33-2120-82-191-20-3106-17-6B7-6B-359-50-791-57-677-47-468-06-295-95-491-58-78B-74-4131-11-320Q 96 fl9W-2
Hanoibis-{2-OJ (methyl Jrther2Oiloroph(nol1,3-OichloratxTOewl,4-fiidiioroben:tnttauyl (UOTdlf2-{Kd)lcrcbn:nff2-ftothylphnlbis- (2-Dil or oi soprc^yl ) rthr4-nethylphcnolM-ni tr oso-Oi it-propyl ui nt(exachlarotthanittttrobnintIsqinoroni2-Mitrophnol2,4-DiiethytphBiolhnimc Andbii-iChlarwthavinrthw2,4-Oichloraphtnal1 , 2, HrioMDnteniBMMftphthalcRf4-Ovlxoanilinitotadilorabutadint4-Chltro-J-Kthylptoal2-fkthylnapiitlttlnffHdKhlxocydipvt^iene2,4,6-Trichlirophtnol2, 4 ,5-TrioM inph«ttlKUorortaphthalm2-MitroaruliniDitftiryJ (MbalatfAcoupthylvt3-tttroaniline
uqkg
34011340 U340 U340 U3401)340 U340 U340 U340 U340 U340 U340 U340 U340 U340 U340 U1700 U340 U340 U340 U340 U340 U340U340 U340 U340 U340 LI1700 U340 U1700 U340 U340 U1700 U
BPC C l e a n u p i NOSep. ' Funne l E x t r a c t i o n : YES^Con t i n . L i q . - L i q . E x t . : Y E a ^
ttSfc:
63-32-951-28-5100-02-7132-64-9121-14-2606-20-264-66-27005-72-384-73-7100-01-6534-52-186-30-6101-55-3I1B-74-167-66-56SH)l-6120-12-764-74-2306-44-0129-00-085-68-791-94-156-55-3117-81-721B-OH117-64-0205-99-22D7KI6-950-32-8193-39-553-70-3191-24-2
-
AceiuphthcnB2,4-Dinitn^ienal4-tttraptitnnlDibttzofirvi2,4-flinitrotolucnt2,6-Dinitrotaluff*Dirthyl pbthalati4-OiIaropfiinyl-phenyl ethrFluartM4-Kitroaniline4,6-Oi ni tro-2-(tethy 1 ph«wlH-nitrosDdiptunylaiine (1)4-frtnophetyl-phenyl rttwrHn**ltro«uMPentacMorophenolPtwnanUf ••fcithracmtDi-tHwtyl phthalitiFluor mtiewPyrveButyl-tarylfhttuUttStS'-OiohlTtbeaidinihnzoialaBttraciMbis-O-EthylhetyUphthalatiOry«ntDi-n-octyl phthalatiBBtzoiblfluoranthmleraol^nuranthnknxDdlpyrenttrim ( 1 ,2,3-d) pyrv*Kbcnzo (L,h) anttracfntInzoighDprYlBv
/
35; (ci: T J u ) ( c i^ — -x
Mgkg
3*0 U. 1700 U
1700 U340 U340 U340 U340 U340 U340 U1700 U1700 U340 U340 U340 U1700 U340 U340 U15&X340 U340 U340 U490U340 U130 Ui340 U340 U340 U34011340U340 U340 U340 U
Ov. f l r* /
( c i r c l e one)(circle onei
»[•
J %Laboratory tUne: ENVIROGYNECase No: 7351
Organics Analysis Data Sneet
Concentrat ion: LOWDate Ex t rac ted /Prepared : "7-Date Analyzed: 7-21-87Conc/Dil Factor: 1 t lO *Percent Moisture (decan ted ) :
Pesticides -v PCb s
GF-C Cleanup : YESSep. Funnel ExtractionCan tin. Liq.-Liq. Ext.
ici rcl e.(circle
one)one i
CAS No: ugkg
50 g
319-W-iJ19-35-7319-66-8m fift B•U VI T
76-44-fi309-00-2W24-S7-3««» m aWf TO B
W-57-I72-5H72-20-833213-AW72-54-810S1-07-85fr-25-372-43-553494-70-557-74-9BOOt-35-212674-11-211104-23-251489-21-9S34A9-21-912&72-29-411097-49-11109i-e2-5
Mpha-ilCBeti-BKEelta-etCCuu-OC Oindaneih itadilorUdrinItaptactilx Epoiiti*EndasuHanlKridrin4,4'-DflEEndhoBtdosultan-II4,r-MOEndoulfw SulUti4,4 '-DOThetha lxEndria KrtcntChlcrtantTaaptimArodtr-lOUlroclQr-1221flrodo-1232Arodv-1242Arodx-l24Bfc-oclx-125*
170 U y.170 U *170 U *170 U *•170 U Xnyfrr17 U17 U33 U331)33 U33 U33 U33U33U170 U33 U170 U330 U170 U170 U170 U170 U170 U330 U330 U
Vi » Voluae or extract injected (ul)Us » Height of sa«ple extracted (g)Vt - Voluie of total extract (ul)
Vt » 40,000 ulA *0°/O*
FORM I
Vi 2.0 ul
•teLabora tory Nane:Case No: 7351
ENVIRQDiNE Sample Nuaoer: EH
Grganics Analysis Data Sheet
j
j
C o n c e n t r a t i o n : LDHDate E x t r a c t e d / P r e p a r e d : 7-30-B7Date A n a l y z e d : 6-5-67C o n c / D i l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 24.8
[AS Ho:
lOft-55-2111-44-495-57-B541-73-1106-44-7100-51-495-50-195-48-7
Phenol
2-Oilcrophenol
teuyl AlcoSol1,2-ttdilcroteBtne
104-44-5621-44-747-72-1
bis~ (2-Chlcr m scpropyl) ether4-fethylpnBiolH-ni tr oso-Oi -n-propy! wineHnachloroethane
Tfi-59-1B&-75-5105-47-945-85-0lli-91-112WS-2120-32-191-20-3104-47-*87-46-359-50-791-57-477-47-4
Inphxm
2,4-DiicthylptaQlBwitric Acidbis-(Oilo*vUffiY>Hethaw
1,2,4-TrichlonteutneMaphthtlmt4-tMtroaniUn*tfacachlorobutadiene
teachl crocyclQxntadm
VS^R-* 2,4,5-Trichlornphmjln-5B-7BB-74-4131-11-3 Diiethyl phthalatff20Q 94 8 KBUputylent99-09-2 3-tttrwniliM
450 U450U450 LJ450 U450 U450 LI4SOU450 U450 U450 U450 U450 U450 U450 U450 U450 U2200 U450 U450 U450 LJ450 U450 Lt450 U450 LJ51 J
450 U2200 U450 U2200 U450 U450 U2200 LJ
e Compounds
'SPC Cleanup t NOSep. Funnel ExtractionContin. Liq.-Liq. Ext.
CKte
B3-3H51-2&-5100-02-7132-44-9121-14-2404-20-2
AcBUphthcne2,4-nnitrQDhenol
Dibnotiran2^4-OinitrotDlufne
phttalztc7005-72-384-73-7100-01-45S4-52-1&HO-4101-55-3na-74-1
Flarwf4-Hitroaniline
IHutrasadiphBiYlaunt Hi
e-oi-a120-12-7B4-74-2204-44-012HO-0
HBChlvoboucnePKtachlorophendFteanthrvte
phthilattFlvantbmFynn
56-S5-3117-81-7
BBQD (a) anthracene
117-W-O265 *9-2
QrYScnefc-n-octylkcolblfluorantJunefcrcoikHlimnttae
50-32-619>39-553-70-3191-24-2
Kbnzola^hlarthracmt
(l)-Cannot bi separattd f roa diphenylaaint
F Q R H 1
(circle(circle
one ione J
uqkg
L a b o r a t o r y Na*e :Case No: 7351
E N V I R Q D Y N E Saflple
Ji Qrganics Analysis Data SheetiPaqe 3>
C o n c e n t r a t i o n : L O WD a t e E x t r a c t e d / P r e p a r e d : 7-Date Analyzed: 7-21-37C o n c / D i l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 27
CAS No:
1
a
H* 30 g
Pesticides k PCS I
GPC Cleanup : YESSep. Funnel ExtractionContin. Liq.-Liq. Ext.
uqfcg
YES one •
319-B4-4.319-85-7
MW6-SBI.BS aJB 07 7
7M4-63W-00-21024-57-3W?'vB Dtf-57-172-55-972-2H3EI3-65-972-54-fl1031-07-fl55-»-372-«-553494-70-557-74-98001-35-212474-11-21U04-29-2SJ4i9-21-953449-21-912672-29-411WHH11096-C-5
Alpha-MBfti*wthltJ-ftC6-w-fiH: (Lindm)HqitadUorAliHaItptidiior Epmide&iteulfan IDieldria4,4'-H£EndriaEncteulf«-II4,4'-OWGndoaiHw Sulfitt4,4'-»T(MtayddirEndria KrtontQdordmTiuphcMfrrxJtr-lOli*roclx-1221frodor-1232*roclor-1242Ardor-124aft-Klor-1254frvclx-12U
22 U22 U22 U22 U22 U22 U22 U221144U44U44 U44 U44U44U -44U .220 U44U220 U440 UZ20U220 U220 U220 U220 U440U440U
Vi * Voluae oi txtract injected (uliMs • Height ai siaple extracted (g)Vt - Voluat of total txtract (uli
Vt » 40,000 ul
FORK I
Vi • 2.0 ul
CAS
3.
«.
7.
IO..
13..
15..
16..
19..
M.
3.
10.
J
£\AOcganlci Analysis Data Shoet
(Page 4)
ld«n(<fie<J Compounds
Compownd N
e vtVJ I 4
Ul
A
U-HdvfrggM
JU rbcn
f
n *
M-3
I t - M
. r12. -5
i±^_in 6
(wg/f or
7/o.J
es
ecology and environment, inc.Ill WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415
International Specialists in the Environment
Date Received for Review
From: Zena Gold-KaufmanSubject: HdO
PAN: ID-0141 X&
Date Review Completed
Case
Sample Description______Organics (VGA, ABN, Pest/PCB)
Low SoilLow WaterDrinking WaterOther
Inorganics (Metals, Cyanide)
Low SoilLow WaterDrinking WaterOther
-project Data Status
Incomplete, awaiting:
Completed!
FIT Data Review Findings:
-556Common lob - Qc£kme(di-n~
Book No.
Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.
Page No. 200
UNITED S T A T E S ENVIRONMENTAL P R O T E C T I O N A 3 E N C YREGION V
:;TE: f/v/fEJECT: Rev iew of Region V CLP Data Q __ ,-, Q-I ^
Rece ived for Rev iew on _____Q "" 1 / " Q '________ jfy
OM: Curt is R o s s , Di rector (5SCRL) /&K*4. & ofa~&4 -&? ^r,Central Regional Laboratory / <£„
TH: Data User: ______F IT____________________ /^%>
1
We have reviewed the data for the following case(s).
SITE NAME: HOD LANDFILL SMO case No. 73S1rr * » « - > No- of A °-u- /Ac t i v i t v
EPA Data Set No. br 4\b3 Samples: 4 Numbers VSQ5/C7ZIQQ
CRL NO.SMO Tra f f ic No. EM &17 " 8&Q
_ ' . Hrs. RequiredCLP laboratory: hNVlRQD^NJE ______________ for Review:
Following are our findings:
/-
( ) Data are acceptable for use.(><0 Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory{ ) Data are unacceptable.
cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas _-
EPA FORM 1320-6 (Rev. 5/87) - ' . . . .
DATA '-JA
C o n t r a c t o r ;
Belt* Is fi suTrr-ar/ of the out of control audits and the possible. on the data for this case:
/,
.2.Vc^At •' 3
•W >•*•• «•«.'* JQ <^V-*C.
4"'* o *>*.
t*>*.*-
>*<f
H
»*oi c ^ 3 •* /A /o£ l S — c 'j dodecy/
R e v i e w e d
Phone:
DATA QUALIFIERS
C o n t r a c t o r ; Case 73 S/
B?1c>* is a sufrr-.jr/ of the out of control audits and the possible ef fect- on the tiata for this case :
•——7u.-H'ie.v-
PK * s r <-« L«- t t
fts : »•<> o uL*4 Iy
77 TO. eg. J_L7n
t £ l
R e v i e w e d by:
Phone: 51
DATA QUALIFIERS•\
Cont rac to r ; Case 735)s
Belorf is a sundry of the out of control audits and the possible e f fec t. on the data for this case: -
** ^f f (0^7,1 f
£faJi>f)r7
_£ 7/23/f?.
Rev iewed by: At .
Phone: 3/ ?-
PAGE 5 OF
Case:
Contractor:
TENTATIVELY IDENTIFIED COMPOUNDSWATCH ASSESSMENT
NOTE: Reviewer should note directly on Organic Analysis Data Sheet (OADS)those matches that in his opinion (based on contract criteria) areunreasonable.
CRITERIA
(1) Relative intensities of major ions (>10%) reference spectrumshould be present in the sample spectrum.
(2) Relative intensities of major ions in sample spectrum shouldagree to within 20% of reference spectrum intensities.
(3) Molecular ions present in reference spectrum should be presentin sample spectrum.
(4) Ions present in sample spectrum, but not in reference spectrumshould be reviewed for possible background contamination orpresence of coeluting interferences.
(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelutinginterferences.
(6) If, in the reviewer's opinion, no valid identification can bemade the compound should be labelled as "unknown" and the initialsand date of the reviewer placed on the OADS.
Reviewer's Initials/Date:
UV.7ED STA'ES E N V I R O N M E N T A L P R O T E C T I O N A G E N C Y R E G I O N VC A L I B R A T I O N OUTL1E-.S
^ c- r VOLATILE HSL COMPOUNDS _0 5 < CONTRACTOR *
3?
l l m * . Ca'i . Ca1 i . C a U l C o n t . C a U I C o n t .
IRF |V.S:l* iRF RF RF
irvl
M5'.-.v i e"e C". i c1"! ce
I ^ I1 i
-
L ,2-D1 cr.'i1,1,1-Tncr.loroetMane
Tet recn ior iceV i n v l Ace ta te
- c r o n e t n a n e1,2-OicnlcrccrcraneTrar,s-l ,3-Di chloroDroreneTn en i oroetnene
cls-1,3--i
*, e * r\ y\ - 2- ? e n t a n o n e2-Kexanone
1,1 .Z^-oiuene
Stvrenen- X v1e n e
AFFECTEDSAMPLES:
II MB* 1 1 A106M
* These f lags should be appl ied to the analytes on the sample data sheets.
1/S7
CASE?
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDS/ (Page 1)' CONTRACTOR £ * v" r*>*&
Imt. Cal. ICont. Cal.ICont. Ca•• r^*~^^* •• ,• •» ••• i ^-^ i •-"—^^^— Cont. C a i . I C o n t . a i
RF f-RSD RF RFPnenoiDi oroetrwi )tne2-Cn i . 3
TO-
Eeizvi Alconoi1,2-Dicn2—Metr.y tone*____________b is \2 - cn lo ro i soDPOOv l )Etr,er
Hexacnloroe'naneNTtro-enzeneIsocnorone2-Nitrooneno2.4»OimetMvlonenolBenzolc A C T Obi st2-C'nloroethoxv jMethane2,4-DicnTorooneno'1,2,4-TricniorooenzeneN a c n i n a l e n e4-ChloroanilineHexacnlorooutaciene4-Chloro-3-MgtnylDneno12-MetnvlnaonrnaleneHexacn'iorocvclooentaaiene T
2,4,5-Trichloroohenol2-Chioronaontnaiene2—NizroanilineDixe-nvl Phtnalate
3-Nizroam lineAce-aonthene
- i mtroonenoi-Nitroonenol
Oioenzofuran
AFFECTEDSAMPLES: £"A\ X go
These flags should be applied to the analytes on the sample data sheets
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY RE-3 ION VCALIBRATION OUTLIERS
SEMIVOLATILE HSL COMPOUNDS2 . -
CONTRACTOR C Mi/I *-o N,^^^*
1 Init. Cal. ICont. Cal .DATE/TIME: I //£
IRF IWSD2,4-Oinitrotoluene I \2,6-DinitrotolueneDietnvlont'ia ate4-Cnlorocneiyl-pneiv leanerFluorene4-Nitroaru line4, 6-Dinitro-2-Metnvl phenolN-Nitroscciohenylamine •
- IRF Ml
3*5 T
4-3rotnoDnsnyl-onenylether jHexacnlorcoenzenePentachloroohenol 1Phenantnrene }AnthraceneDi-n-ButvlohthalateFluoranthene 1Pyrene 1Butyl benzvl phthal ateBenzoia)Antnracenebisl2-£thvlhexyl )PhthalateChrysene 1Oi-n-Octvl Phthalate
t
It t
Benzo(b)Fluoranthene IBenzo(k)FluorafltheneBenzola jPyreneIndeno(l,2,3-cd)PvreneDiDenz(a,h)Anthracene- |Benzo(a,h,1) Pervlene
*
1
Cont. Cal. ICont. Cff l .^ 1
RF
I 1
1
iD lw |RF1
111
1
t 11 1
tI II 1
1
*0 *
1
n3
Cont. Cav£l-o
RF
111
11
11 -
1
1
»0 *I _,
--«*,
1
SEE PAGE 1 FOR AFFECTED SAMPLES.
These flags should be applied to the analytes on the sample data sheets.
1/87
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLATILE KSL COMPOUNDS
/ < CONTRACTOR
mornJ
Unit. Cal . ICcnt. Cal. Cor.t. Cal. Conz. Ca . Con:. Calrt*DAiE/ i iMt : I ?/tl
IRF SRSOPhenolbi s(-Z-Chloroet,nvl JEtner2-ChiOPConenol1 ,3-OicriloPODenze*.e1.4-Dicn opocer.zeneEe".rvi A conc i1 ,2-Dicnlor03enzer.e2-Metnvlonenol
^^is;2-cn orolsooroovl JEtner4-Me^nvlohenolN-Nizroso-Di-n-Proovlar.ineHexacnlopoetnaneNltPODenzeneIsoonorone2-Nitroohenol2.4-OlmethvlonenolBenzole Acid .bi s ( 2-Ch 1 oroethoxv )Me"hane2 ,4-Di cnl opoonenol1,2,4-TricnlorooenzeneNaontnalene4-ChloroanilineHexacnloroDutaaiene4-ChlOPO-3-Metnylonenol2-Metnvlnaontnalene
^Hexacniorocvclooentadiene2,4,6-TpichloPOonenol2,4,5-TplchloPOohenol2-Chloronaontnalene2-NitPoanilineDimetnvl PhtnalateAcenasntnvlene
» t-I
IF ISO
111
11
,0*3! 3^ K/RI11
11
.0| tf/RI1 1
1111
*
3-iNitroanilineAcanaontnene2,^-DimtPooneno'i4-NitPoonenolDlcenzofupan
* AFFECTEDSAMPLES:
En /"T7
_ • I I V- IRF '• J
1i
1
1
iiiI
iti
i3
IRF
1111
11
•
j w
11
r | Mwi | w |1 "~
1|1111
1
g>— j
1
1 11 11 1I I -1 11 1I I1 11 11 1
11
* These flags should be applied to the analytes on the sample data sheets,
CASE*
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS
SEMIVOLAT1LE HSL COMPOUNDSI Pa9e * ^j_______ CONTRACTOR E K 1/1*0 J-
DATE/TIME:
2,4-01r,itrotoluene2»6-Oinitro':olueneDiecnylor^alate4-Cnlcroonsnvl-pne iv letterFlucre-:e4-N1tPOenilinel^-Dinitro-S-Me'nvlonenol
T^N-N-itPoscciDhenvlamine4-3 ro^osneny l-oneny let herHexacn'iorcoenzenePentacnloroohenolPhenar.inreneAntnraceneDi-n-5utylohthalateFluopantnenePypeneButvlbenzvlDhthalateBenzo(a)Antnracenebis(2-Ethvlhexyl JPhthalateChryseneDl-n-Octyl PhthalateBenzol bJFluorantheneBenzo(k)FluopanzheneBenzoiaJPvpene
- Indenot 1 ,2 ,3-cd )PypeneDioenz(a,h)Anthracene-Benzo(o,h,1 ) Pervlene
Init
ftRr
:
I
I
I
I
. Cat(J«SD
I
?r
»- 1
r
i
Cont
RF
II
. Ca
10
11
L
*
i
111
Cont
RF
. (a
10 |i
i
111
1
.11w 1
ii1
1
1
Con*
RF
. Ca
•0
I.I1
* 1
1
Cont
Rf*
-1
. Ca
to
1
i .
*
SEE PAGH 1 FOR AFFECTED SAMPLES.
* These flags should be applied to the analytes on the sample data sheets.
1/87
J3<\OENVIRODYNE
ENGINEERSAugust 14, 19871990-7351
Ms. Carol Schaeffer 3;. ;. j. ,'\A -•Sample Management Office t _..„,,, '.:..-••—••209 Madison Street, Suite 200Alexandria, Virginia 22314
Dear Ms. Schaeffer;
Enclosed are partial results of analysis of Case 7351 for Volatiles, BNAs,and Pesticides/PCBs performed under Contract Number 68-01-7087. Four soilsamples, EM877 through EM880, were received on July 17, 1987. it is ourunderstanding that the case is completed with the submission of these re-sults.
All semivolatiles were extracted and analyzed according to the low) levelsoil protocol. No Pesticide/PCBs were detected on the first GC quanti-tation runs, so second column confirmation was not required.
If you have any questions about this report, please contact me.
Sincerely,
Margaret C. WinterProject Manager
MCW/jagEnclosure
______IVIn Reference to Case No(s)
Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION SYSTEM
Telephone Record Log
Date of Call:
Laboratory Name:Lab Contact:
Region:Regional Contact: ' -|s
Call Initiated By: __ Laboratory ^ Region
In reference to data for the following sample numbeKs):
rT\O
«/
Summary of Questions/Issues Discussed:
i J C
^ .3
Summary of Resolution:
£~ 2T T r-.^i 1 j^. /f *- .-^ A •»../- r^. Q
- y
A t ^.,
f
-f
_ . »."r* /
Signature '
Distribution: (1) Lab Copy, (2) Region Copy, (3) SMO Copy
Date
? ?.
SOIL SURROGX.E PERCENT RECOVERY SUMMARYC«MNct*?*»r _
M»i»*ft*.
mfsn lE.mVttfYiB* 2EfY^b
£[wnerfl^n^
•
•
.
•
* VALUES""ADVISOR
CommMi
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. . ._ -_- . -_ VOLAltLf - - -
1*. *(»<•••&'.."..« 7
ID'4
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~^ff.l.36>juflW
310,%&
TV 10/- -7/4&UA
^55/^^'+tta
,
*"
<?/^?/JU/JQQffft<&t
• t
ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS VolitY LIMITS ONLY Simi"
Pt>tl(
EUI-VOIATIL E -.-.-----_.-._--.
»»t«<K-ll
IH- nil
/ i!5ftjj*ff *{-*
it *l *1
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!•*• „ ,*^ . out of /a iVoUtlUit - — &£. out oIdtsi — C — out o
r . L?^ |r <^ I
t-'iWO**-
111*1111
30v53^/•t-3/Ztt)
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i.*.t i *•••••*•
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37/.?¥36>
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.**
/06///
M\/<?&// -3/£Z£U
ouUidi of QC limits 7/86
outildi or QC limits
«•: ———— - ————— - ——— —— ————————————————————————————————————— j^^ ————
' ——————————————————————————————————————————————————— £jj£» »_
VA)
FORM II
'/'i./1
V;*. No. Rdglon
METHOD BLANK SUMMARY
Contraclor Conlracl
otrc or Vilftll CCMC.LtvfL Mir.io C*S COUfOUNO iNSi.riC M UNIMOVHl CONC. IMlfl CNDL
ov ' u 10
E> Sail 5185-i
Commonta:
FORM IV 7/85
METHOD BLANK SUMMARY
C«)« No. .Region Cootriclor u Contract No.
nc to 0»lt Of VtlHIl !Gb IN jr. 10 CAl NUUtCM COU^CUNO (MSI.. TIC ON UHKHQWH! CMC.
SR1S-1 (HA - 360(.0005
3-503
V.I
Commonl>;
FORM IV 7/85
f 9
CX1TULATED INSTRUMENT DETECTION LIMITS
\
VK, 107-02-t •crolein3V) 107-13-1 •crylorutrUe
V) kcnzencV) carbon
I7V) IOt-90-7 chJoroberacnr0V)IV) 71-39-4 IJJ-frichJoroethfcftt
UJv) 7VK-> M^iehlofBTthant"*VJ 7VO&.3 l,U-TTiehiorpe^h*f*T
3V)(UV) 7VOC-J*\<V) ) ID-TV I 7-cfJftroetf>yl»inyl
47-44-3 chloreform7V35-*
IM-40-5
O3V) 10041-02-4 »vu- l_J»4ichJor opropem10041-01-05
34V) JOG-* I -* nhy IbcnieneChJartoe
7»-47-3 chloremethanc(UV) 7M3-9
7V2V2 kromoformWomodj chlor omcth&nv
75-4V* tluerotrkMoromethvte7V7l-t
Chlor odibromomtthanr127-14-4 ^BUftChiorovthwe
O4V) I04-U-) «»ltmK07V)(UV) chloride
47
TVfV)7 VIVO
104-10-1100^2.)I04-OV4
»* •! xvl*n«t
inn100
252525
252525
2525505025252525252525255050502525
2525252550
100100
2510010025to
"25"
f -C
U»P) JCVOQ-?OOP) 40-37-1C»1P) 57-?*-*»2P) JO-7J-Smp) 7J-SV*t»*P> 72.)*-tttJP) 1IV2V7(WP) I1J.21-7t»7P) 1031-07-1IMP) 72-JO-t<WP) 7*21- »V*(1DOP) 74-44-1UOIP) I024-37-JU02P) Jl*-l*-4(103P) Jl*-tV7(10tP) >lVW-t(105P) «-l^»CIMP) J>*4»-2l-»(I07P) 11017-^Vl(IMP) 11104-71-2(1WP) lll*l-lt-S(HOP) t2i72'7V4(IMP) 11 OH- 12- 5(11 IP) 12474-H.7< I I ) P > &D010V2
tltfrmtficldnnCMord*ne•(»'-DDT«,*'-DDE»,»'-DDD•C-4ndo»u!l»n_^ -*r>do»uli*n•ndcnuHan luMifr•nsrift«n*i fcJOe^wflthf¥t»ctjorhcp\»ctto< tpeuoc•C-&HC^tf-BMC/ -*HC-r-*HC Umtene)K<VI2*2PC6-12HPC B- 127)PCB-1232PCB-12HPC B- 12*0PCB-lOlttouphrnr
1.51 .512
2.2
1.21.22.11.42.11.82.11.51.51.22.02.01.5
302040
40202040
200
n
CALCULATED INSTRUMENT DETECTION LIMITS
\
23.
1JIijiii
21 A)22A)24 A)
"J1A)>A)^7 A);3iA)15'A)
;4CM(41. A)(43A>
(IB)136)UB)(9fi)02B)(UB)UOB)(33B)Q4B)Q7B)C21B)O5B)(34B)(STB)O9B)(*0fi>I+1B)<42B}(43B)
U-04-239-50-795-37-*
120-S3-2105-47-9U-73-3
JOO-02-731-21-5
53^-32-1t7-lfr-5
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