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分離操作(separation)
(1)
(2)
(3)
(4)
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単蒸留(Simple distillation)
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ニッカ余市工場
糖化
発酵
熟成
出芽
蒸留
大麦
蒸留の例1 (ウイスキー)
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コスモ石油
蒸留の例2 (原油)
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出光石油
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蒸留の例3 (バイオエタノール)
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P
気液平衡関係(vapor-liquid equilibrium)
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0.0 0.2 0.4 0.6 0.8 1.0330
340
350
360
370
380
液組成(x) 蒸気組成(y) 平衡温度[K]
0 0 373.2
0.3 0.665 351.2
0.5 0.779 346.3
1.0 1.0 337.8
水-メタノール系 気液平衡関係
温度ー組成線図
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0.0 0.2 0.4 0.6 0.8 1.00.0
0.2
0.4
0.6
0.8
1.0
x-y線図
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0.0 0.2 0.4 0.6 0.8 1.00.0
0.2
0.4
0.6
0.8
1.0
0.0 0.2 0.4 0.6 0.8 1.00.0
0.2
0.4
0.6
0.8
1.0
共沸混合物
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気液平衡の計算
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ラウール(Raoult)の法則
ダルトン(Dalton)の法則
気相中の成分1の分圧p1は、純成分の液体の蒸気圧P1と液相中の成分1のモル分率x1との積で与えられる。
気相中の成分1の分圧p1は、気相中の成分1のモル分率y1と全圧Pとの積で与えられる。
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理想溶液が成り立つ組み合わせ
非理想溶液の場合
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単蒸留(Simple distillation)
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フラッシュ蒸留(Flash distillation)
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水蒸気蒸留
減圧蒸留
抽出蒸留
共沸蒸留
その他の蒸留法
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連続蒸留 原理
0.0 0.2 0.4 0.6 0.8 1.00.0
0.2
0.4
0.6
0.8
1.0
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0.0 0.2 0.4 0.6 0.8 1.00.0
0.2
0.4
0.6
0.8
1.0
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理論段数の計算
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Benzene-toluene
X
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Y
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
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理論段数と還流比
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最小理論段数の求め方
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最小還流比の求め方
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理論段数と還流比の関係
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蒸留塔の高さ
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充填塔(Packed Tower)