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Attachment C14(h) Proponent Phase I and Phase II Environmental Site Assessment (8/8)

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Page 1: Cover - Attach C14h

Attachment C14(h)

Proponent Phase I and Phase II Environmental Site Assessment (8/8)

Page 2: Cover - Attach C14h

12

of 1

2:

Pa

ge

Wo

rk O

rde

r::

Clie

nt

ES

20

03

48

1

60

62

35

99

_1

.1-B

urro

ws IE

:P

roje

ct

AE

CO

M A

ustra

lia P

ty Ltd

Su

rrog

ate

Co

ntro

l Lim

its

Reco

very

Lim

its (%)

Su

b-M

atrix

: SO

IL

Co

mp

ou

nd

CA

S N

um

be

rL

ow

Hig

h

EP

066S

: PC

B S

urro

gate

Decach

loro

bip

hen

yl

20

51

-24

-33

91

49

EP

068S

: Org

an

och

lorin

e P

estic

ide S

urro

gate

Dib

rom

o-D

DE

21

65

5-7

3-2

49

14

7

EP

068T

: Org

an

op

ho

sp

ho

rus P

estic

ide S

urro

gate

DE

F7

8-4

8-8

35

14

3

EP

075(S

IM)S

: Ph

en

olic

Co

mp

ou

nd

Su

rrog

ate

s

Ph

en

ol-d

61

31

27

-88

-36

31

23

2-C

hlo

rop

hen

ol-D

49

39

51

-73

-66

61

22

2.4

.6-T

ribro

mo

ph

en

ol

11

8-7

9-6

40

13

8

EP

075(S

IM)T

: PA

H S

urro

gate

s

2-F

luo

rob

iph

en

yl

32

1-6

0-8

70

12

2

An

thra

cen

e-d

10

17

19

-06

-86

61

28

4-T

erp

hen

yl-d

14

17

18

-51

-06

51

29

EP

080S

: TP

H(V

)/BT

EX

Su

rrog

ate

s

1.2

-Dic

hlo

roeth

an

e-D

41

70

60

-07

-07

31

33

To

luen

e-D

82

03

7-2

6-5

74

13

2

4-B

rom

oflu

oro

ben

zen

e4

60

-00

-47

21

30

Reco

very

Lim

its (%)

Su

b-M

atrix

: WA

TE

R

Co

mp

ou

nd

CA

S N

um

be

rL

ow

Hig

h

EP

080S

: TP

H(V

)/BT

EX

Su

rrog

ate

s

1.2

-Dic

hlo

roeth

an

e-D

41

70

60

-07

-07

11

37

To

luen

e-D

82

03

7-2

6-5

79

13

1

4-B

rom

oflu

oro

ben

zen

e4

60

-00

-47

01

28

Page 3: Cover - Attach C14h

Fals

e 4 4

.00

Tru

e

Envir

onm

ental

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:ES

2003481

Pa

ge

:1

of 1

2

::

La

bo

rato

ryC

lien

tE

nviro

nm

enta

l Divisio

n S

ydney

AE

CO

M A

ustra

lia P

ty L

td

:C

onta

ctM

R A

LE

X L

AT

HA

M:

Conta

ctB

renda H

ong

:A

dd

ress

LE

VE

L 2

1, 4

20 G

EO

RG

E S

TR

EE

T

SY

DN

EY

NS

W, A

US

TR

ALIA

2000

Ad

dre

ss:

277-2

89 W

oodpark R

oad S

mith

field

NS

W A

ustra

lia 2

164

::

Te

lep

ho

ne

+61 0

2 8

934 0

000

+61 2

8784 8

555

:T

ele

ph

on

e

:P

roje

ct

60623599_1.1

-Burro

ws IE

Da

te S

am

ple

s Re

ceive

d: 3

1-Ja

n-2

020

:O

rde

r nu

mb

er

60623599_1.1

Da

te A

na

lysis C

om

me

nce

d:0

5-F

eb-2

020

:C

-O-C

nu

mb

er

----Issu

e D

ate

:10-F

eb-2

020

Sa

mp

ler

:K

urtis W

ath

en, R

EB

EK

AH

PA

NO

ZZ

O

Site

:----

Qu

ote

nu

mb

er

:E

N/0

04/1

6

No

. of s

am

ple

s rece

ive

d23

:

No

. of s

am

ple

s an

aly

se

d10

:

This re

port su

perse

des a

ny p

revio

us re

port(s) w

ith th

is refe

rence

. Resu

lts apply to

the sa

mple

(s) as su

bm

itted. T

his d

ocu

ment sh

all n

ot b

e re

pro

duce

d, e

xcept in

full.

This Q

uality C

ontro

l Report co

nta

ins th

e fo

llow

ing in

form

atio

n:

l

La

bo

rato

ry D

up

licate

(DU

P) R

ep

ort; R

ela

tive P

erce

nta

ge

Diffe

ren

ce (R

PD

) an

d A

cce

pta

nce

Lim

its

l

Me

tho

d B

lan

k (MB

) an

d L

ab

ora

tory C

on

trol S

pike

(LC

S) R

ep

ort; R

eco

very a

nd

Acce

pta

nce

Lim

its

l

Ma

trix S

pik

e (M

S) R

ep

ort; R

eco

very a

nd

Acce

pta

nce

Lim

its

Sig

nato

ries

This d

ocu

ment h

as b

een e

lectro

nica

lly signed b

y the a

uth

orize

d sig

nato

ries b

elo

w. E

lectro

nic sig

nin

g is ca

rried o

ut in

com

plia

nce

with

pro

cedure

s specifie

d in

21 C

FR

Part 1

1.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

sitio

n

Ala

na

Sm

ylie

Asb

esto

s Ide

ntifie

rN

ew

castle

- Asb

esto

s, Ma

yfield

We

st, NS

W

Ce

line

Co

nce

ica

oS

en

ior S

pe

ctrosco

pist

Syd

ne

y Ino

rga

nics

, Sm

ithfie

ld, N

SW

Ed

wa

nd

y Fa

dja

rO

rga

nic

Co

ord

ina

tor

Syd

ne

y Ino

rga

nics

, Sm

ithfie

ld, N

SW

Ed

wa

nd

y Fa

dja

rO

rga

nic

Co

ord

ina

tor

Syd

ne

y Org

an

ics, Sm

ithfie

ld, N

SW

R I G

H T

S O

L U

T I O

N S

| R I G

H T

P A

R T

N E

R

Page 4: Cover - Attach C14h

2 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Gen

era

l C

om

men

ts

Th

e

an

aly

tica

l p

roce

du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

ve

lop

ed

fr

om

e

sta

blis

he

d

inte

rna

tion

ally

re

cog

niz

ed

p

roce

du

res

such

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/

dig

est

ate

dilu

tio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis

. W

he

re t

he

LO

R o

f a

re

po

rte

d r

esu

lt d

iffe

rs f

rom

sta

nd

ard

LO

R,

this

ma

y b

e d

ue

to

hig

h m

ois

ture

co

nte

nt,

insu

ffic

ien

t sa

mp

le (

red

uce

d w

eig

ht

em

plo

yed

) o

r m

atr

ix in

terf

ere

nce

.

An

on

ymo

us

= R

efe

rs t

o s

am

ple

s w

hic

h a

re n

ot

spe

cific

ally

pa

rt o

f th

is w

ork

ord

er

bu

t fo

rme

d p

art

of

the

QC

pro

cess

lot

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

da

tab

ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l A

bstr

acts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

RP

D =

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce

#

= I

nd

ica

tes

faile

d Q

C

Ke

y :

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

D

up

lica

te

refe

rs

to

a

ran

do

mly

se

lect

ed

in

tra

lab

ora

tory

sp

lit.

La

bo

rato

ry

du

plic

ate

s

pro

vid

e

info

rma

tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

erc

en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:

0%

- 5

0%

; R

esu

lt >

20

tim

es

LO

R:

0%

- 2

0%

.

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

C L

ot:

2847945)

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

30

74

-00

1

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g4

40

.00

No

Lim

it

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

2<

20

.00

No

Lim

it

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

98

0.0

0N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g<

5<

50

.00

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

5<

50

.00

No

Lim

it

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itB

H1

02

_0

.3-0

.4

ES

20

03

48

1-0

10

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g5

50

.00

No

Lim

it

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g3

43

6.4

No

Lim

it

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g2

32

46

.27

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g7

16

67

.68

0%

- 5

0%

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

49

55

11

.50

% -

50

%

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

) (

QC

Lo

t: 2

847951)

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

19

.72

0.0

1.6

10

% -

20

%A

no

nym

ou

s E

S2

00

30

74

-00

3

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

7.3

7.1

3.1

6N

o L

imit

An

on

ymo

us

ES

20

03

51

8-0

01

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

) (

QC

Lo

t: 2

849180)

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

3.4

3.2

6.9

20

% -

20

%A

no

nym

ou

s E

S2

00

33

37

-01

2

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

4.2

4.0

3.9

60

% -

20

%A

no

nym

ou

s E

S2

00

35

18

-01

1

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

C L

ot:

2847946)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

<0

.10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

30

74

-00

1

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g0

.1<

0.1

0.0

0N

o L

imit

BH

10

2_

0.3

-0.4

E

S2

00

34

81

-01

0

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

841944)

Page 5: Cover - Attach C14h

3 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

841944)

- c

on

tin

ued

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.1<

0.1

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

35

9-0

01

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.1<

0.1

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

36

0-0

01

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

841947)

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

35

9-0

01

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-E

nd

osu

lfa

n3

32

13

-65

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

ald

eh

yde

74

21

-93

-40

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

36

0-0

01

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-E

nd

osu

lfa

n3

32

13

-65

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

Page 6: Cover - Attach C14h

4 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

841947)

- c

on

tin

ued

EP

06

8:

En

drin

ald

eh

yde

74

21

-93

-40

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

36

0-0

01

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

841947)

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

59

-00

1

EP

06

8:

De

me

ton

-S-m

eth

yl

91

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl

55

98

-13

-00

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Pirim

ph

os-e

thyl

23

50

5-4

1-1

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

60

-00

1

EP

06

8:

De

me

ton

-S-m

eth

yl

91

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl

55

98

-13

-00

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Pirim

ph

os-e

thyl

23

50

5-4

1-1

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

Page 7: Cover - Attach C14h

5 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

841947)

- c

on

tin

ued

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

60

-00

1

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

C L

ot:

2840428)

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

45

5-0

42

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

45

5-0

59

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

Page 8: Cover - Attach C14h

6 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

C L

ot:

2840428)

- c

on

tin

ued

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

55

-05

9

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2840427)

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

55

-04

2

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

55

-05

9

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2841489)

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

42

5-0

03

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

48

0-0

13

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2840427)

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

45

5-0

42

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

--5

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

45

5-0

59

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

--5

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2841489)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

25

-00

3

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

80

-01

3

EP

080:

BT

EX

N (Q

C L

ot:

2841489)

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

25

-00

3

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

it

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

80

-01

3

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

Page 9: Cover - Attach C14h

7 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

080:

BT

EX

N (Q

C L

ot:

2841489)

- c

on

tin

ued

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

34

80

-01

3

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2845751)

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

11

-00

1

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

11

-00

7

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2845751)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

31

1-0

01

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

31

1-0

07

EP

080:

BT

EX

N (Q

C L

ot:

2845751)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

11

-00

1

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

33

11

-00

7

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

Page 10: Cover - Attach C14h

8 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

pik

e

(LC

S)

refe

rs

to

a

cert

ifie

d

refe

ren

ce

ma

teria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

2847945)

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

10

52

1.7

mg

/kg

12

68

6.0

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

19

5.2

4.6

4 m

g/k

g1

13

83

.0

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g<

28

4.1

43

.9 m

g/k

g1

28

76

.0

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g<

59

0.2

32

mg

/kg

12

08

6.0

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

59

0.2

40

mg

/kg

11

48

0.0

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

29

5.7

55

mg

/kg

12

38

7.0

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

90

.56

0.8

mg

/kg

12

28

0.0

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

CL

ot:

2847946)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

84

.32

.57

mg

/kg

10

57

0.0

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

841944)

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.18

3.0

1 m

g/k

g1

26

62

.0

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

841947)

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

91

.70

.5 m

g/k

g1

13

69

.0

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

93

.50

.5 m

g/k

g1

17

65

.0

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

59

1.1

0.5

mg

/kg

11

96

7.0

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

97

.50

.5 m

g/k

g1

16

68

.0

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

59

2.5

0.5

mg

/kg

11

76

5.0

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

59

6.0

0.5

mg

/kg

11

56

7.0

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

51

03

0.5

mg

/kg

11

56

9.0

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

51

02

0.5

mg

/kg

11

86

2.0

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

51

08

0.5

mg

/kg

11

76

3.0

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

10

40

.5 m

g/k

g1

16

66

.0

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

51

00

0.5

mg

/kg

11

66

4.0

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

<0

.05

97

.80

.5 m

g/k

g1

16

66

.0

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

10

20

.5 m

g/k

g1

15

67

.0

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

96

.40

.5 m

g/k

g1

23

67

.0

EP

06

8:

be

ta-E

nd

osu

lfan

33

21

3-6

5-9

0.0

5m

g/k

g<

0.0

51

06

0.5

mg

/kg

11

56

9.0

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

10

20

.5 m

g/k

g1

21

69

.0

EP

06

8:

En

drin

ald

eh

yde

74

21

-93

-40

.05

mg

/kg

<0

.05

10

20

.5 m

g/k

g1

20

56

.0

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

51

08

0.5

mg

/kg

12

46

2.0

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

10

40

.5 m

g/k

g1

20

66

.0

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

10

40

.5 m

g/k

g1

22

64

.0

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

97

.60

.5 m

g/k

g1

30

54

.0

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

841947)

Page 11: Cover - Attach C14h

9 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

841947)

- c

on

tin

ued

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

58

4.1

0.5

mg

/kg

11

95

9.0

EP

06

8:

De

me

ton

-S-m

eth

yl9

19

-86

-80

.05

mg

/kg

<0

.05

99

.20

.5 m

g/k

g1

28

62

.0

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.21

02

0.5

mg

/kg

12

65

4.0

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

57

4.8

0.5

mg

/kg

11

96

7.0

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

58

3.7

0.5

mg

/kg

12

07

0.0

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl5

59

8-1

3-0

0.0

5m

g/k

g<

0.0

58

4.5

0.5

mg

/kg

12

07

2.0

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.28

7.0

0.5

mg

/kg

12

06

8.0

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

58

2.7

0.5

mg

/kg

12

26

8.0

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

10

30

.5 m

g/k

g1

17

69

.0

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

51

01

0.5

mg

/kg

11

87

6.0

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

92

.90

.5 m

g/k

g1

22

64

.0

EP

06

8:

Pirim

ph

os-

eth

yl2

35

05

-41

-10

.05

mg

/kg

<0

.05

99

.40

.5 m

g/k

g1

16

70

.0

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

59

4.0

0.5

mg

/kg

12

16

9.0

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

51

04

0.5

mg

/kg

11

86

6.0

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

78

.20

.5 m

g/k

g1

24

68

.0

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

51

01

0.5

mg

/kg

11

26

2.0

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

59

6.7

0.5

mg

/kg

12

06

8.0

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

51

01

0.5

mg

/kg

12

76

5.0

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

56

2.6

0.5

mg

/kg

12

34

1.0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

2840428)

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.59

7.7

6 m

g/k

g1

25

77

.0

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

94

.76

mg

/kg

12

47

2.0

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

99

.76

mg

/kg

12

77

3.0

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

96

.86

mg

/kg

12

67

2.0

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

99

.46

mg

/kg

12

77

5.0

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

99

.86

mg

/kg

12

77

7.0

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

96

.76

mg

/kg

12

77

3.0

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

96

.86

mg

/kg

12

87

4.0

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

91

.06

mg

/kg

12

36

9.0

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.59

3.7

6 m

g/k

g1

27

75

.0

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.59

0.3

6 m

g/k

g1

16

68

.0

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.59

3.3

6 m

g/k

g1

26

74

.0

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

10

06

mg

/kg

12

67

0.0

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.58

3.1

6 m

g/k

g1

21

61

.0

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

84

.96

mg

/kg

11

86

2.0

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

82

.06

mg

/kg

12

16

3.0

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2840427)

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

09

5.5

30

0 m

g/k

g1

29

75

.0

Page 12: Cover - Attach C14h

10

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2840427)

- c

on

tin

ued

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

09

7.5

45

0 m

g/k

g1

31

77

.0

EP

07

1:

C2

9 -

C3

6 F

ract

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tal P

etr

ole

um

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rocarb

on

s (Q

CL

ot:

2841489)

EP

08

0:

C6

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9 F

ract

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mg

/kg

<1

08

4.1

26

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/kg

12

86

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080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2840427)

EP

07

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10

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16

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ctio

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98

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75

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57

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34

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92

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25

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CL

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EP

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84

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EX

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CL

ot:

2841489)

EP

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Be

nze

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71

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85

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66

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67

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ylb

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zen

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00

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90

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76

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me

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68

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EP

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ph

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LC

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Sp

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%)

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ltC

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cen

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Hig

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mp

ou

nd

CA

S N

um

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LO

RU

nit

EP

080/0

71:

To

tal P

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um

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s (Q

CL

ot:

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EP

08

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C6

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9 F

ract

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83

.82

60

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75

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CL

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77

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EX

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CL

ot:

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EP

08

0:

Be

nze

ne

71

-43

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36

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zen

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70

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me

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tatic

Re

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pe

r la

bo

rato

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e w

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in t

he

eve

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of

sa

mp

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atr

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terf

ere

nce

.

Page 13: Cover - Attach C14h

11

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

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M A

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Ltd

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b-M

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ix:

SO

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atr

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pik

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MS

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ikeR

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very

(%)

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very

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its (

%)

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Hig

hL

ow

MS

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ncen

trati

on

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ple

ID

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mp

ou

nd

CA

S N

um

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EG

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D093)T

: T

ota

l M

eta

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P-A

ES

(Q

CL

ot:

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An

on

ymo

us

ES

20

03

07

4-0

01

74

40

-38

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G0

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T:

Ars

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ic1

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50

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/kg

13

07

0.0

74

40

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dm

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40

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07

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39

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ad

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13

07

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74

40

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40

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by F

IMS

(Q

CL

ot:

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An

on

ymo

us

ES

20

03

07

4-0

01

74

39

-97

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G0

35

T:

Me

rcu

ry8

7.0

5 m

g/k

g1

30

70

.0

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

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QC

Lo

t: 2

841944)

An

on

ymo

us

ES

20

03

35

9-0

01

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EP

06

6:

To

tal P

oly

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en

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85

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13

07

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EP

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rgan

och

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ne P

esti

cid

es (

OC

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QC

Lo

t: 2

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on

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20

03

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9-0

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13

07

0.0

76

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11

40

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g/k

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70

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30

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EP

06

8:

Ald

rin

11

40

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g/k

g1

30

70

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60

-57

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P0

68

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ield

rin

84

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.5 m

g/k

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30

70

.0

72

-20

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P0

68

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nd

rin

99

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13

07

0.0

50

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68

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DD

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06

2 m

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70

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EP

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rgan

op

ho

sp

ho

rus P

esti

cid

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OP

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QC

Lo

t: 2

841947)

An

on

ymo

us

ES

20

03

35

9-0

01

33

3-4

1-5

EP

06

8:

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zin

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98

.60

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g/k

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70

.0

55

98

-13

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68

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hlo

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07

0.0

23

50

5-4

1-1

EP

06

8:

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ph

os-

eth

yl9

2.3

0.5

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13

07

0.0

48

24

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P0

68

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rom

op

ho

s-e

thyl

79

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30

70

.0

34

64

3-4

6-4

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06

8:

Pro

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74

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30

70

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EP

075(S

IM)B

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oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

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s (Q

CL

ot:

2840428)

An

on

ymo

us

ES

20

03

45

5-0

42

83

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75

(SIM

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hth

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10

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13

07

0.0

12

9-0

0-0

EP

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5(S

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10

mg

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13

07

0.0

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2840427)

An

on

ymo

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ES

20

03

45

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42

----

EP

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1:

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C1

4 F

ract

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98

.35

23

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13

77

3.0

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EP

07

1:

C1

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C2

8 F

ract

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11

32

31

9 m

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31

53

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EP

07

1:

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9 -

C3

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ract

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12

51

71

4 m

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52

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EP

080/0

71:

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tal P

etr

ole

um

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s (Q

CL

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2841489)

An

on

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ES

20

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EP

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9 F

ract

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89

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13

07

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EP

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tal R

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NE

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racti

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CL

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An

on

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ES

20

03

45

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15

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Page 14: Cover - Attach C14h

12

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

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ow

s IE

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Su

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ix:

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ILM

atr

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pik

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MS

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ep

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ikeR

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very

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very

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%)

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Co

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Lab

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CL

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2841489)

An

on

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ES

20

03

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5-0

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EP

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10

Fra

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37

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70

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EP

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BT

EX

N (Q

CL

ot:

2841489)

An

on

ymo

us

ES

20

03

42

5-0

03

71

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80

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en

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86

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95

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TE

RM

atr

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pik

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ep

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ikeR

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very

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very

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its (

%)

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um

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EP

080/0

71:

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tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2845751)

An

on

ymo

us

ES

20

03

31

1-0

01

----

EP

08

0:

C6

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9 F

ract

ion

11

83

25

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30

70

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EP

080/0

71:

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tal R

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NE

PM

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racti

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s (Q

CL

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2845751)

An

on

ymo

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ES

20

03

31

1-0

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10

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13

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EP

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EX

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CL

ot:

2845751)

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on

ymo

us

ES

20

03

31

1-0

01

71

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80

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en

zen

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0.6

25

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30

70

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10

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08

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90

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13

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10

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EP

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10

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10

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08

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me

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ara

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70

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95

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07

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Page 15: Cover - Attach C14h

Tru

e

Envir

onm

ental

QA

/QC

Co

mp

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e A

ss

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sm

en

t to

as

sis

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Qu

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Wo

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:E

S2003481

Pa

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of 8

::

La

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Envi

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AE

CO

M A

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ple

s R

ece

ive

d:31-J

an-2

020

Site

:--

--Is

sue

Da

te:10-F

eb-2

020

Kurt

is W

ath

en, R

EB

EK

AH

PA

NO

ZZ

O:

Sa

mp

ler

No

. o

f sa

mp

les r

ece

ive

d:23

:O

rde

r n

um

be

r60623599_1.1

No

. o

f sa

mp

les a

na

lyse

d:10

Th

is r

ep

ort

is a

uto

mati

cally g

en

era

ted

by t

he A

LS

LIM

S t

hro

ug

h in

terp

reta

tio

n o

f th

e A

LS

Qu

ality

Co

ntr

ol R

ep

ort

an

d s

evera

l Q

uality

Assu

ran

ce p

ara

mete

rs m

easu

red

by A

LS

. T

his

au

tom

ate

d

rep

ort

ing

hig

hlig

hts

an

y n

on

-co

nfo

rman

ces, fa

cilit

ate

s f

aste

r an

d m

ore

accu

rate

data

valid

ati

on

an

d is d

esig

ned

to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

Co

ntr

ol (

QC

) R

ep

ort

.

l

NO

Meth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

NO

Du

plicate

ou

tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

NO

Matr

ix S

pik

e o

utl

iers

occu

r.

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, N

O su

rro

gate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

l

NO

An

aly

sis

Ho

ldin

g T

ime O

utl

iers

exis

t.

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

uality

Co

ntr

ol S

am

ple

s

l

NO

Qu

ality

Co

ntr

ol S

am

ple

Fre

qu

en

cy O

utl

iers

exis

t.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 16: Cover - Attach C14h

2 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

tim

e

is

7 d

ays;

o

the

rs

14

da

ys.

A

re

co

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes

of

inte

rest/

con

cern

.

Ho

ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

Ass

ess

me

nt

com

pa

res

the

le

ach

d

ate

w

ith

th

e

sho

rte

st

an

aly

te

ho

ldin

g

time

fo

r th

e

eq

uiv

ale

nt

so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

A r

eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

If s

am

ple

s a

re id

en

tifie

d b

elo

w a

s h

avi

ng

be

en

an

aly

sed

or

ext

ract

ed

ou

tsid

e o

f re

com

me

nd

ed

ho

ldin

g t

ime

s,

this

sh

ou

ld b

e t

ake

n in

to c

on

sid

era

tion

wh

en

inte

rpre

ting

re

sults

.

Th

is

rep

ort

su

mm

arize

s e

xtra

ctio

n

/ p

rep

ara

tion

a

nd

a

na

lysi

s tim

es

an

d

com

pa

res

ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

nci

ng

U

SE

PA

S

W

84

6,

AP

HA

, A

S

an

d

NE

PM

) b

ase

d

on

th

e

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

rese

nt

first

da

te o

f e

xtra

ctio

n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A lis

ting

of

bre

ach

es

(if

an

y)

is p

rovi

de

d h

ere

in.

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

A055)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

5_

1.7

-1.8

,B

H1

02

_0

.3-0

.4,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

14

-Fe

b-2

02

0--

--07

-Feb

-202

0--

--31-J

an

-2020

----

ü

So

il G

lass J

ar

- U

np

reserv

ed

(E

A055)

BH

10

1_

0.1

6-0

.26

14

-Fe

b-2

02

0--

--09

-Feb

-202

0--

--31-J

an

-2020

----

üE

A200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

Sn

ap

Lo

ck B

ag

(E

A200)

BH

10

5_

0.4

-0.5

,B

H1

02

_0

.5-0

.6,

BH

10

1_

1.3

-1.4

29

-Ju

l-2

02

0--

--05

-Feb

-202

0--

--31-J

an

-2020

----

ü

EA

200N

: A

sb

esto

s Q

uan

tifi

cati

on

(n

on

-NA

TA

)

Sn

ap

Lo

ck B

ag

(E

A200N

)

BH

10

5_

0.4

-0.5

,B

H1

02

_0

.5-0

.6,

BH

10

1_

1.3

-1.4

29

-Ju

l-2

02

0--

--05

-Feb

-202

0--

--31-J

an

-2020

----

ü

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

So

il G

lass J

ar

- U

np

reserv

ed

(E

G005T

)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

5_

1.7

-1.8

,B

H1

02

_0

.3-0

.4,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

29

-Ju

l-2

02

02

9-J

ul-2

02

007

-Feb

-202

007-F

eb

-20

20

31-J

an

-2020

üü

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

So

il G

lass J

ar

- U

np

reserv

ed

(E

G035T

)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

5_

1.7

-1.8

,B

H1

02

_0

.3-0

.4,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

28

-Fe

b-2

02

02

8-F

eb

-20

20

08

-Feb

-202

007-F

eb

-20

20

31-J

an

-2020

üü

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

P066)

BH

10

1_

0.1

6-0

.26

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

Page 17: Cover - Attach C14h

3 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

P068)

BH

10

1_

0.1

6-0

.26

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

P068)

BH

10

1_

0.1

6-0

.26

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P075(S

IM))

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

5_

1.7

-1.8

,B

H1

02

_0

.3-0

.4,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

14

-Fe

b-2

02

01

4-F

eb

-20

20

07

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

16

-Ma

r-2

02

01

4-F

eb

-20

20

06

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

14

-Fe

b-2

02

01

4-F

eb

-20

20

07

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

EP

080:

BT

EX

N

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

5_

0.4

-0.5

,B

H1

05

_0

.85

-0.9

5,

BH

10

2_

0.5

-0.6

,B

H1

01

_0

.7-0

.8,

BH

10

1_

2.2

-2.3

14

-Fe

b-2

02

01

4-F

eb

-20

20

07

-Feb

-202

005-F

eb

-20

20

31-J

an

-2020

üü

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

QC

30

31

4-F

eb

-20

20

14

-Fe

b-2

02

007

-Feb

-202

007-F

eb

-20

20

31-J

an

-2020

üü

Page 18: Cover - Attach C14h

4 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

QC

30

31

4-F

eb

-20

20

14

-Fe

b-2

02

007

-Feb

-202

007-F

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Page 19: Cover - Attach C14h

5 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

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Pty

Ltd

60

62

35

99

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urr

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s IE

:P

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Qu

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ntr

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req

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om

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Th

e f

ollo

win

g r

ep

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su

mm

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s th

e f

req

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ncy

of

lab

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QC

sa

mp

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an

aly

sed

with

in t

he

an

aly

tica

l lo

t(s)

in

wh

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th

e s

ub

mitt

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sa

mp

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) w

as(

we

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ctu

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Su

mm

ary

of

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trix

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lua

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%)

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up

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P)

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PM

20

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& A

LS

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20

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8

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IMS

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LS

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20

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l Me

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S)

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PM

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PM

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LS

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stic

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P0

68

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20

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LS

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lych

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6

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20

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20

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TR

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Se

miv

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71

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LS

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NE

PM

20

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LS

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6 5

.00

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Pe

stic

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P0

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0 5

.00

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35

T

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PM

20

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& A

LS

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nd

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5.0

0 5

.00

12

To

tal M

eta

ls b

y IC

P-A

ES

EG

00

5T

NE

PM

20

13

B3

& A

LS

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nd

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5.8

8 5

.00

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TR

H -

Se

miv

ola

tile

Fra

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nE

P0

71

NE

PM

20

13

B3

& A

LS

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Sta

nd

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5.2

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.00

11

TR

H V

ola

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s/B

TE

XE

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Ma

trix

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ike

s (M

S)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

5.2

6 5

.00

11

PA

H/P

he

no

ls (

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

5.2

6 5

.00

11

Pe

stic

ide

s b

y G

CM

SE

P0

68

NE

PM

20

13

B3

& A

LS

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nd

ard

6.2

5 5

.00

11

Po

lych

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6

NE

PM

20

13

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LS

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nd

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20

13

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LS

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TR

H -

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PM

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13

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H V

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nt

Eva

lua

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na

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eth

od

sM

eth

od

Page 20: Cover - Attach C14h

6 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tio

n: û

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy

no

t w

ithin

sp

eci

fica

tion

; ü

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy w

ithin

sp

ecifi

ca

tion

.

Qu

alit

y C

on

tro

l Sp

ecifi

ca

tion

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y C

ontr

ol S

am

ple

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e

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dQ

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ula

rA

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al

Ra

te (

%)

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ontr

ol S

am

ple

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nt

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lua

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nA

na

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al M

eth

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eth

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up

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(DU

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NE

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20

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LS

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0 1

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LS

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H V

ola

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P0

80

Page 21: Cover - Attach C14h

7 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

03

48

1

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

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Bri

ef

Meth

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Su

mm

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Th

e a

na

lytic

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du

res

use

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y th

e E

nvi

ron

me

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ave

be

en

de

velo

pe

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rom

est

ab

lish

ed

in

tern

atio

na

lly r

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gn

ize

d p

roce

du

res s

uch

as

tho

se p

ub

lish

ed

by

the

US

EP

A,

AP

HA

, A

S a

nd

NE

PM

. In

ho

use

de

velo

pe

d p

roce

du

res

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em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Th

e f

ollo

win

g r

ep

ort

pro

vid

es

brie

f d

esc

rip

tio

ns

of

the

an

aly

tica

l pro

ced

ure

s e

mp

loye

d f

or

resu

lts r

ep

ort

ed

in t

he

Ce

rtifi

cate

of

An

aly

sis.

So

urc

es

fro

m w

hic

h A

LS

me

tho

ds

ha

ve b

ee

n d

eve

lop

ed

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in t

he

Me

tho

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esc

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An

aly

tica

l Me

tho

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Me

tho

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esc

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sM

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ixM

eth

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In h

ouse

: A

gra

vim

etr

ic p

roce

dure

base

d o

n w

eig

ht lo

ss o

ver

a 1

2 h

our

dry

ing p

eriod a

t 105-1

10 d

egre

es

C.

This

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Schedule

B(3

) S

ect

ion 6

.1 a

nd T

able

1 (

14 d

ay

hold

ing tim

e).

Mois

ture

Conte

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EA

05

5S

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AS

4964 -

2004 M

eth

od for

the q

ualit

ativ

e id

entif

icatio

n o

f asb

est

os

in b

ulk

sam

ple

s

Analy

sis

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Pola

rise

d L

ight M

icro

scopy

incl

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g d

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tain

ing

Asb

est

os

Identif

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n in

Soils

EA

20

0S

OIL

Asb

est

os

Cla

ssifi

catio

n a

nd Q

uantit

atio

n p

er

NE

PM

2013 w

ith C

onfir

matio

n o

f Id

entif

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n b

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S 4

964 -

2004

Gra

vim

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ic d

ete

rmin

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n o

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sbest

os

Conta

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ate

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Fib

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Asb

est

os,

Asb

est

os

Fin

es

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ple

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alc

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atio

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NE

PM

pro

toco

ls. A

sbest

os

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es

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ibro

us

FA

+A

F)

is r

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s th

e e

quiv

ale

nt w

eig

ht in

the s

am

ple

rece

ived a

fter

acc

ountin

g for

sub-s

am

plin

g (

where

applic

able

for

the <

7m

m a

nd/o

r <

2m

m fra

ctio

ns)

.

Asb

est

os

Cla

ssifi

catio

n a

nd

Quantit

atio

n p

er

NE

PM

2013

* E

A2

00

NS

OIL

In h

ouse

: R

efe

rence

d to A

PH

A 3

120; U

SE

PA

SW

846 -

6010. M

eta

ls a

re d

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rmin

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win

g a

n a

ppro

priate

aci

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igest

ion o

f th

e s

oil.

T

he IC

PA

ES

tech

niq

ue io

nis

es

sam

ple

s in

a p

lasm

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ittin

g a

chara

cterist

ic

spect

rum

base

d o

n m

eta

ls p

rese

nt. In

tensi

ties

at se

lect

ed w

ave

length

s are

com

pare

d a

gain

st those

of m

atr

ix

matc

hed s

tandard

s. T

his

meth

od is

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plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

Tota

l Meta

ls b

y IC

P-A

ES

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00

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SO

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In h

ouse

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S 3

550, A

PH

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g -

B (

Flo

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genera

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AA

S)

FIM

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S is

an a

uto

mate

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mele

ss a

tom

ic a

bso

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erc

ury

in s

olid

s are

dete

rmin

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win

g a

n

appro

priate

aci

d d

igest

ion. Io

nic

merc

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nlin

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tom

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heate

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ll. Q

uantif

icatio

n is

by

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paring a

bso

rbance

again

st a

calib

ratio

n c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

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l Merc

ury

by

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35

TS

OIL

In h

ouse

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efe

rence

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SE

PA

SW

846 -

8270D

E

xtra

cts

are

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sed b

y C

apill

ary

GC

/MS

and q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

) (M

eth

od 5

04)

Poly

chlo

rinate

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iphenyl

s (P

CB

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P0

66

SO

IL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8270D

Ext

ract

s are

analy

sed b

y C

apill

ary

GC

/MS

and q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

tech

niq

ue is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

) (M

eth

od 5

04,5

05)

Pest

icid

es

by

GC

MS

EP

06

8S

OIL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8015A

S

am

ple

ext

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s are

analy

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apill

ary

GC

/FID

and

quantif

ied a

gain

st a

lkane s

tandard

s ove

r th

e r

ange C

10 -

C40. C

om

plia

nt w

ith N

EP

M a

mended 2

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TR

H -

Sem

ivola

tile F

ract

ion

EP

07

1S

OIL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8270D

. E

xtra

cts

are

analy

sed b

y C

apill

ary

GC

/MS

in S

ele

ctiv

e Ion

Mode (

SIM

) and q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

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) (M

eth

od 5

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nd 5

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henols

(S

IM)

EP

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IM)

SO

IL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8260B

. E

xtra

cts

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y P

urg

e a

nd T

rap, C

apill

ary

GC

/MS

.

Quantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5 p

oin

t ca

libra

tion c

urv

e. C

om

plia

nt w

ith N

EP

M

am

ended 2

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TR

H V

ola

tiles/

BT

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0S

OIL

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ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8260B

W

ate

r sa

mple

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rior

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by

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/MS

and q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

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C r

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of N

EP

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2013)

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B(3

)

TR

H V

ola

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BT

EX

EP

08

0W

AT

ER

Page 22: Cover - Attach C14h

8 o

f 8

:P

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Wo

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Clie

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20

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1

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Pre

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sM

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In h

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. H

ot B

lock

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mple

is h

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itric

and

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ero

xide is

added a

nd s

am

ple

s heate

d a

nd c

oole

d a

gain

befo

re b

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ere

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and b

ulk

ed to v

olu

me for

analy

sis.

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igest

is a

ppro

priate

for

dete

rmin

atio

n o

f se

lect

ed m

eta

ls in

slu

dge,

sedim

ents

, and s

oils

. T

his

meth

od is

com

plia

nt w

ith N

EP

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lid is

shake

n w

ith s

urr

ogate

and 1

0m

L m

eth

anol p

rior

to a

naly

sis

by

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e a

nd T

rap -

G

C/M

S.

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anolic

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ract

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rap

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ouse

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anic

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tion (

tum

ble

r). 10g o

f sa

mple

, N

a2S

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nd s

urr

ogate

are

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ith 3

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ceto

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ver

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ble

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olv

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rate

d a

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once

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by

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the

desi

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olid

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A 5

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OR

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6-W

WA

TE

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Page 23: Cover - Attach C14h

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES2003481

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Brenda Hong

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60623599_1.1-Burrows IE Page 1 of 3

:Order number 60623599_1.1 :Quote number EB2017AECOMAU0014 (EN/004/16)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : ----

Sampler : Kurtis Wathen, REBEKAH PANOZZO

DatesDate Samples Received : Issue Date : 04-Feb-202031-Jan-2020 18:00

Scheduled Reporting Date: 10-Feb-2020:Client Requested Due

Date

10-Feb-2020

Delivery DetailsMode of Delivery : :Carrier Not AvailableSecurity Seal

No. of coolers/boxes : :2 Temperature 1.2'C - Ice present

: : 23 / 10Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Sample No: 19- BH101_1.5-1.6 received as BH101_1.3-1.4.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (3 weeks), Solid (2 months ± 1 week) from receipt of samples.

l Please be aware that APHA/NEPM recommends water and soil samples be chilled to less than or equal to 6°C for chemical

analysis, and less than or equal to 10°C but unfrozen for Microbiological analysis. Where samples are received above this

temperature, it should be taken into consideration when interpreting results. Refer to ALS EnviroMail 85 for ALS

recommendations of the best practice for chilling samples after sampling and for maintaining a cool temperature during transit.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 24: Cover - Attach C14h

:Client AECOM Australia Pty Ltd

Work Order : ES2003481 Amendment 02 of 3:Page

04-Feb-2020:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

MethodSample Container Received Preferred Sample Container for AnalysisClient sample ID

Asbestos Classification and Quantitation per NEPM 2013 : EA200N

BH105_0.4-0.5 - Snap Lock Bag - Snap Lock Bag: Separate bag received

BH102_0.5-0.6 - Snap Lock Bag - Snap Lock Bag: Separate bag received

BH101_1.5-1.6 Received as

BH101_1.3-1.4

- Snap Lock Bag - Snap Lock Bag: Separate bag received

Any sample identifications that cannot be displayed entirely in the analysis summary table will be listed below.

ES2003481-019 : [ 31-Jan-2020 ] : BH101_1.5-1.6 - Received as BH101_1.3-1.4

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

(On H

old

) S

OIL

No a

naly

sis

requeste

d

SO

IL -

EA

055-1

03

Mois

ture

Conte

nt

SO

IL -

EA

200N

Asbesto

s in

Soils

- (

<1kg s

am

ple

s O

NLY

)

SO

IL -

EP

075 S

IM P

AH

only

SIM

- P

AH

only

SO

IL -

S-0

2

8 M

eta

ls (

incl.

Dig

est

ion)

SO

IL -

S-1

3

OC

/OP

/PC

B

SO

IL -

S-2

6

8 m

eta

ls/T

RH

/BT

EX

N/P

AH

ES2003481-001 31-Jan-2020 00:00 BH105_0.15-0.2 ü

ES2003481-002 31-Jan-2020 00:00 BH105_0.4-0.5 ü ü ü

ES2003481-003 31-Jan-2020 00:00 BH105_0.65-0.75 ü

ES2003481-004 31-Jan-2020 00:00 BH105_0.85-0.95 ü ü

ES2003481-005 31-Jan-2020 00:00 BH105_1.7-1.8 ü ü ü

ES2003481-006 31-Jan-2020 00:00 BH105_3.5-3.6 ü

ES2003481-007 31-Jan-2020 00:00 BH105_4.4-4.9 ü

ES2003481-008 31-Jan-2020 00:00 QC108 ü

ES2003481-009 31-Jan-2020 00:00 BH102_0.135-0.2 ü

ES2003481-010 31-Jan-2020 00:00 BH102_0.3-0.4 ü ü ü

ES2003481-011 31-Jan-2020 00:00 BH102_0.5-0.6 ü ü ü

ES2003481-012 31-Jan-2020 00:00 BH102_0.9-1.0 ü

ES2003481-013 31-Jan-2020 00:00 BH102_1.3-1.4 ü

ES2003481-014 31-Jan-2020 00:00 BH102_3.4-3.5 ü

ES2003481-015 31-Jan-2020 00:00 BH101_0.16-0.26 ü ü

ES2003481-016 31-Jan-2020 00:00 BH101_0.3-0.4 ü

ES2003481-017 31-Jan-2020 00:00 BH101_0.7-0.8 ü ü

ES2003481-018 31-Jan-2020 00:00 QC109 ü

ES2003481-019 31-Jan-2020 00:00 BH101_1.5-1.6 Recei... ü

ES2003481-020 31-Jan-2020 00:00 BH101_2.2-2.3 ü ü

ES2003481-021 31-Jan-2020 00:00 BH101_3.4-3.3 ü

ES2003481-023 31-Jan-2020 00:00 BH102_4.4-4.5 ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 25: Cover - Attach C14h

:Client AECOM Australia Pty Ltd

Work Order : ES2003481 Amendment 03 of 3:Page

04-Feb-2020:Issue Date

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

ES2003481-022 31-Jan-2020 00:00 QC303 ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

- Chain of Custody (CoC) (COC) Email AP_CustomerService.ANZ@aecom.

com

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 AECOM (EQUIS_V5_AECOM) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

Page 26: Cover - Attach C14h
Page 27: Cover - Attach C14h
Page 28: Cover - Attach C14h
Page 29: Cover - Attach C14h
Page 30: Cover - Attach C14h
Page 31: Cover - Attach C14h

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l

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l

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Page 32: Cover - Attach C14h

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uiv

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nt

Qu

otie

nt

(TE

Q)

pe

r th

e N

EP

M (

20

13

) is

th

e s

um

to

tal o

f th

e c

on

cen

tra

tion

of

the

eig

ht

carc

ino

ge

nic

PA

Hs

mu

ltip

lied

by

the

ir T

oxic

ity E

qu

iva

len

ce F

act

or

(TE

F)

rela

tive

to

Be

nzo

(a)p

yre

ne

. T

EF

va

lue

s a

re p

rovi

de

d in

bra

cke

ts a

s fo

llow

s: B

en

z(a

)an

thra

cen

e (

0.1

), C

hry

se

ne

(0

.01

), B

en

zo(b

+j) &

Be

nzo

(k)f

luo

ran

the

ne

(0

.1),

Be

nzo

(a)p

yre

ne

(1

.0),

In

de

no

(1.2

.3.c

d)p

yre

ne

(0

.1),

Dib

en

z(a

.h)a

nth

race

ne

(1

.0),

Be

nzo

(g.h

.i)p

ery

len

e (

0.0

1).

Le

ss t

ha

n L

OR

re

sults

fo

r 'T

EQ

Ze

ro' a

re t

rea

ted

as

ze

ro.

l

Page 33: Cover - Attach C14h

3 o

f 7

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

BH

111_0.6

5-0

.75

BH

109_0.9

-1.0

BH

107_1.5

-1.7

BH

108_1.3

-1.4

QC

100

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

30

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2004

680

-005

ES

20046

80-0

04

ES

2004

680

-003

ES

2004680-0

02

ES

2004680-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EN

33:

TC

LP

Leach

8.7

7.7

8.2

8.3

9.1

pH

Un

it0

.1--

--In

itia

l p

H

1.5

4.1

4.1

1.8

5.2

pH

Un

it0

.1--

--A

fter

HC

l p

H

11

11

2-

1--

--E

xtr

acti

on

Flu

id N

um

ber

5.2

5.7

5.8

5.8

4.7

pH

Un

it0

.1--

--F

inal p

H

Page 34: Cover - Attach C14h

4 o

f 7

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

114_1.3

-1.4

BH

117_2.2

-2.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

03

-Fe

b-2

02

0 0

0:0

03

0-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2004680-0

07

ES

2004680-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EN

33:

TC

LP

Leach

8.8

8.1

----

----

----

pH

Un

it0

.1--

--In

itia

l p

H

1.5

2.1

----

----

----

pH

Un

it0

.1--

--A

fter

HC

l p

H

11

----

----

----

-1

----

Extr

acti

on

Flu

id N

um

ber

5.7

5.6

----

----

----

pH

Un

it0

.1--

--F

inal p

H

Page 35: Cover - Attach C14h

5 o

f 7

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

BH

111_0.6

5-0

.75

BH

109_0.9

-1.0

BH

107_1.5

-1.7

BH

108_1.3

-1.4

QC

100

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

TC

LP

LE

AC

HA

TE

(M

atr

ix:

WA

TE

R)

30

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2004

680

-005

ES

20046

80-0

04

ES

2004

680

-003

ES

2004680-0

02

ES

2004680-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

----

Cad

miu

m1.7

3--

----

----

--m

g/L

0.0

57

44

0-4

3-9

----

Ch

rom

ium

<0

.1<

0.1

<0

.1--

--m

g/L

0.1

74

40

-47

-3

0.2

Lead

33.7

8.7

2.3

32.9

mg

/L0

.17

43

9-9

2-1

----

Nic

kel

2.0

<0

.10

.6--

--m

g/L

0.1

74

40

-02

-0

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

----

Hexavale

nt

Ch

rom

ium

<0

.01

0.0

2<

0.0

1--

--m

g/L

0.0

11

85

40

-29

-9

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

<0

.5B

en

zo(a

)pyre

ne

----

----

----

----

µg

/L0

.55

0-3

2-8

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

22.0

Ph

en

ol-

d6

----

----

----

----

%1

.01

31

27

-88

-3

50.0

2-C

hlo

rop

hen

ol-

D4

----

----

----

----

%1

.09

39

51

-73

-6

46.5

2.4

.6-T

rib

rom

op

hen

ol

----

----

----

----

%1

.01

18

-79

-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

61.6

2-F

luo

rob

iph

en

yl

----

----

----

----

%1

.03

21

-60

-8

78.2

An

thra

cen

e-d

10

----

----

----

----

%1

.01

71

9-0

6-8

84.3

4-T

erp

hen

yl-

d14

----

----

----

----

%1

.01

71

8-5

1-0

Page 36: Cover - Attach C14h

6 o

f 7

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

114_1.3

-1.4

BH

117_2.2

-2.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

TC

LP

LE

AC

HA

TE

(M

atr

ix:

WA

TE

R)

----

----

----

03

-Fe

b-2

02

0 0

0:0

03

0-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2004680-0

07

ES

2004680-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

----

Hexavale

nt

Ch

rom

ium

<0

.01

----

----

----

mg

/L0

.01

18

54

0-2

9-9

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

<0

.5B

en

zo(a

)pyre

ne

----

----

----

----

µg

/L0

.55

0-3

2-8

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

26.7

Ph

en

ol-

d6

----

----

----

----

%1

.01

31

27

-88

-3

55.7

2-C

hlo

rop

hen

ol-

D4

----

----

----

----

%1

.09

39

51

-73

-6

64.7

2.4

.6-T

rib

rom

op

hen

ol

----

----

----

----

%1

.01

18

-79

-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

80.9

2-F

luo

rob

iph

en

yl

----

----

----

----

%1

.03

21

-60

-8

86.0

An

thra

cen

e-d

10

----

----

----

----

%1

.01

71

9-0

6-8

86.6

4-T

erp

hen

yl-

d14

----

----

----

----

%1

.01

71

8-5

1-0

Page 37: Cover - Attach C14h

7 o

f 7

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

Su

rro

gate

Co

ntr

ol L

imit

s

Reco

very

Lim

its (

%)

Su

b-M

atr

ix:

TC

LP

LE

AC

HA

TE

Co

mp

ou

nd

CA

S N

um

be

rL

ow

Hig

h

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

Ph

en

ol-

d6

13

12

7-8

8-3

10

44

2-C

hlo

rop

hen

ol-

D4

93

95

1-7

3-6

14

94

2.4

.6-T

rib

rom

op

hen

ol

11

8-7

9-6

17

12

5

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

2-F

luo

rob

iph

en

yl

32

1-6

0-8

20

10

4

An

thra

cen

e-d

10

17

19

-06

-82

71

13

4-T

erp

hen

yl-

d14

17

18

-51

-03

21

12

Page 38: Cover - Attach C14h

Fals

e 3 3

.00

Tru

e

Envir

onm

ental

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:E

S2004680

Pa

ge

:1

of 4

::

La

bo

rato

ryC

lien

tE

nvi

ronm

enta

l Div

isio

n S

ydney

AE

CO

M A

ustr

alia P

ty L

td

:C

onta

ctM

R A

LE

X L

AT

HA

M:

Conta

ctB

renda H

ong

:A

dd

ress

LE

VE

L 2

1, 420 G

EO

RG

E S

TR

EE

T

SY

DN

EY

NS

W, A

US

TR

ALIA

2000

Ad

dre

ss:

277-2

89 W

oodpark

Road S

mith

field

NS

W A

ust

ralia

2164

::

Te

lep

ho

ne

+61 0

2 8

934 0

000

+61 2

8784 8

555

:T

ele

ph

on

e

:P

roje

ct60623599_1.1

-Burr

ow

s IE

Da

te S

am

ple

s R

ece

ive

d:29-J

an-2

020

:O

rde

r n

um

be

r60623599_1.1

Da

te A

na

lysis

Co

mm

en

ce

d:13-F

eb-2

020

:C

-O-C

nu

mb

er

----

Issu

e D

ate

:18-F

eb-2

020

Sa

mp

ler

:--

--

Site

:--

--

Qu

ote

nu

mb

er

:E

N/0

04/1

6

No

. o

f sa

mp

les

rece

ive

d7

:

No

. o

f sa

mp

les

an

aly

sed

7:

This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. T

his

docu

ment sh

all

not be r

epro

duce

d, exc

ept in

full.

This

Qualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

La

bo

rato

ry D

up

lica

te (

DU

P)

Re

po

rt;

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce (

RP

D)

an

d A

cce

pta

nce

Lim

its

l

Me

tho

d B

lan

k (M

B)

an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

l

Ma

trix

Sp

ike

(M

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

Sig

nato

ries

This

docu

ment has

been e

lect

ronic

ally

sig

ned b

y th

e a

uth

orize

d s

ignato

ries

belo

w. E

lect

ronic

sig

nin

g is

carr

ied o

ut in

com

plia

nce

with

pro

cedure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

sitio

n

An

kit

Josh

iIn

org

an

ic C

he

mis

tS

yd

ne

y In

org

an

ics,

Sm

ithfie

ld,

NS

W

Ed

wa

nd

y F

ad

jar

Org

an

ic C

oo

rdin

ato

rS

yd

ne

y O

rga

nic

s, S

mith

field

, N

SW

Iva

n T

ayl

or

An

aly

stS

yd

ne

y In

org

an

ics,

Sm

ithfie

ld,

NS

W

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 39: Cover - Attach C14h

2 o

f 4

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Gen

era

l C

om

men

ts

Th

e

an

aly

tica

l p

roce

du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

ve

lop

ed

fr

om

e

sta

blis

he

d

inte

rna

tion

ally

re

cog

niz

ed

p

roce

du

res

such

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/

dig

est

ate

dilu

tio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis

. W

he

re t

he

LO

R o

f a

re

po

rte

d r

esu

lt d

iffe

rs f

rom

sta

nd

ard

LO

R,

this

ma

y b

e d

ue

to

hig

h m

ois

ture

co

nte

nt,

insu

ffic

ien

t sa

mp

le (

red

uce

d w

eig

ht

em

plo

yed

) o

r m

atr

ix in

terf

ere

nce

.

An

on

ymo

us

= R

efe

rs t

o s

am

ple

s w

hic

h a

re n

ot

spe

cific

ally

pa

rt o

f th

is w

ork

ord

er

bu

t fo

rme

d p

art

of

the

QC

pro

cess

lot

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

da

tab

ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l A

bstr

acts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

RP

D =

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce

#

= I

nd

ica

tes

faile

d Q

C

Ke

y :

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

D

up

lica

te

refe

rs

to

a

ran

do

mly

se

lect

ed

in

tra

lab

ora

tory

sp

lit.

La

bo

rato

ry

du

plic

ate

s

pro

vid

e

info

rma

tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

erc

en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:

0%

- 5

0%

; R

esu

lt >

20

tim

es

LO

R:

0%

- 2

0%

.

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

(Q

C L

ot:

2862670)

EG

00

5C

: C

ad

miu

m7

44

0-4

3-9

0.0

5m

g/L

<0

.05

<0

.05

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

94

6-0

01

EG

00

5C

: C

hro

miu

m7

44

0-4

7-3

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: L

ea

d7

43

9-9

2-1

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: N

icke

l7

44

0-0

2-0

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: C

ad

miu

m7

44

0-4

3-9

0.0

5m

g/L

0.0

50

.05

0.0

0N

o L

imit

BH

10

9_

0.9

-1.0

E

S2

00

46

80

-00

4

EG

00

5C

: C

hro

miu

m7

44

0-4

7-3

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: L

ea

d7

43

9-9

2-1

0.1

mg

/L2

.32

.30

.00

0%

- 2

0%

EG

00

5C

: N

icke

l7

44

0-0

2-0

0.1

mg

/L0

.60

.60

.00

No

Lim

it

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

C L

ot:

2862888)

EG

05

0G

-C:

He

xava

len

t C

hro

miu

m1

85

40

-29

-90

.01

mg

/L<

0.0

1<

0.0

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

45

94

-00

1

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

C L

ot:

2864907)

EG

05

0G

-C:

He

xava

len

t C

hro

miu

m1

85

40

-29

-90

.01

mg

/L<

0.0

1<

0.0

10

.00

No

Lim

itB

H1

08

_1

.3-1

.4

ES

20

04

68

0-0

02

Page 40: Cover - Attach C14h

3 o

f 4

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

pik

e

(LC

S)

refe

rs

to

a

cert

ifie

d

refe

ren

ce

ma

teria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EN

33:

TC

LP

Leach

(Q

CL

ot:

2857446)

EN

33

a:

Initi

al p

H--

--0

.1p

H U

nit

1.0

----

----

----

----

EN

33

a:

Aft

er

HC

l pH

----

0.1

pH

Un

it1

.0--

----

----

----

--

EN

33

a:

Fin

al p

H--

--0

.1p

H U

nit

1.0

----

----

----

----

EN

33:

TC

LP

Leach

(Q

CL

ot:

2861763)

EN

33

a:

Initi

al p

H--

--0

.1p

H U

nit

1.0

----

----

----

----

EN

33

a:

Aft

er

HC

l pH

----

0.1

pH

Un

it1

.0--

----

----

----

--

EN

33

a:

Fin

al p

H--

--0

.1p

H U

nit

1.0

----

----

----

----

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

(Q

CL

ot:

2862670)

EG

00

5C

: C

ad

miu

m7

44

0-4

3-9

0.0

5m

g/L

<0

.05

95

.90

.1 m

g/L

11

88

0.0

EG

00

5C

: C

hro

miu

m7

44

0-4

7-3

0.1

mg

/L<

0.1

95

.60

.1 m

g/L

11

48

8.0

EG

00

5C

: L

ea

d7

43

9-9

2-1

0.1

mg

/L<

0.1

11

30

.1 m

g/L

11

88

0.0

EG

00

5C

: N

icke

l7

44

0-0

2-0

0.1

mg

/L<

0.1

94

.20

.1 m

g/L

11

58

3.0

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

CL

ot:

2862888)

EG

05

0G

-C:

He

xava

len

t C

hro

miu

m1

85

40

-29

-90

.01

mg

/L<

0.0

11

02

0.0

5 m

g/L

11

78

3.0

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

CL

ot:

2864907)

EG

05

0G

-C:

He

xava

len

t C

hro

miu

m1

85

40

-29

-90

.01

mg

/L<

0.0

11

02

0.0

5 m

g/L

11

78

3.0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

2862115)

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5µ

g/L

<0

.57

5.8

5 µ

g/L

11

76

3.3

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

2862604)

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5µ

g/L

<0

.58

4.8

5 µ

g/L

11

76

3.3

Matr

ix S

pik

e (

MS

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

atr

ix

Sp

ike

(M

S)

refe

rs

to

an

in

tra

lab

ora

tory

sp

lit

sam

ple

sp

ike

d

with

a

re

pre

sen

tative

se

t o

f ta

rge

t a

na

lyte

s.

Th

e

pu

rpo

se

o

f th

is

QC

p

ara

me

ter

is

to

mo

nito

r p

ote

ntia

l m

atr

ix

eff

ects

o

n

an

aly

te r

eco

verie

s. S

tatic

Re

cove

ry L

imits

as

pe

r la

bo

rato

ry D

ata

Qu

alit

y O

bje

ctiv

es

(DQ

Os).

Id

ea

l re

cove

ry r

an

ge

s sta

ted

ma

y b

e w

aiv

ed

in t

he

eve

nt

of

sa

mp

le m

atr

ix in

terf

ere

nce

.

Su

b-M

atr

ix:

WA

TE

RM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

Reco

very

Lim

its (

%)

Sp

ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

(Q

CL

ot:

2862670)

An

on

ymo

us

ES

20

04

48

8-0

01

74

40

-43

-9E

G0

05

C:

Ca

dm

ium

79

.00

.25

mg

/L1

30

70

.0

Page 41: Cover - Attach C14h

4 o

f 4

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

Reco

very

Lim

its (

%)

Sp

ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

(Q

CL

ot:

2862670)

- c

on

tin

ued

An

on

ymo

us

ES

20

04

48

8-0

01

74

40

-47

-3E

G0

05

C:

Ch

rom

ium

81

.41

mg

/L1

30

70

.0

74

39

-92

-1E

G0

05

C:

Le

ad

93

.71

mg

/L1

30

70

.0

74

40

-02

-0E

G0

05

C:

Nic

kel

77

.51

mg

/L1

30

70

.0

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

CL

ot:

2862888)

An

on

ymo

us

ES

20

04

59

4-0

01

18

54

0-2

9-9

EG

05

0G

-C:

He

xava

len

t C

hro

miu

m7

8.0

0.0

5 m

g/L

13

07

0.0

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

(Q

CL

ot:

2864907)

BH

10

8_

1.3

-1.4

E

S2

00

46

80

-00

21

85

40

-29

-9E

G0

50

G-C

: H

exa

vale

nt

Ch

rom

ium

71

.80

.05

mg

/L1

30

70

.0

Page 42: Cover - Attach C14h

Tru

e

Envir

onm

ental

QA

/QC

Co

mp

lia

nc

e A

ss

es

sm

en

t to

as

sis

t w

ith

Qu

ali

ty R

ev

iew

Wo

rk O

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:E

S2004680

Pa

ge

:1

of 5

::

La

bo

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lient

Envi

ronm

enta

l Div

isio

n S

ydney

AE

CO

M A

ustr

alia P

ty L

td

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onta

ctM

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ph

on

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555

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roje

ct60623599_1.1

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ow

s IE

Da

te S

am

ple

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ece

ive

d:29-J

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020

Site

:--

--Is

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te:18-F

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----

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ple

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r60623599_1.1

No

. o

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mp

les a

na

lyse

d:7

Th

is r

ep

ort

is a

uto

mati

cally g

en

era

ted

by t

he A

LS

LIM

S t

hro

ug

h in

terp

reta

tio

n o

f th

e A

LS

Qu

ality

Co

ntr

ol R

ep

ort

an

d s

evera

l Q

uality

Assu

ran

ce p

ara

mete

rs m

easu

red

by A

LS

. T

his

au

tom

ate

d

rep

ort

ing

hig

hlig

hts

an

y n

on

-co

nfo

rman

ces, fa

cilit

ate

s f

aste

r an

d m

ore

accu

rate

data

valid

ati

on

an

d is d

esig

ned

to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

Co

ntr

ol (

QC

) R

ep

ort

.

l

NO

Meth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

NO

Du

plicate

ou

tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

NO

Matr

ix S

pik

e o

utl

iers

occu

r.

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, N

O su

rro

gate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

l

An

aly

sis

Ho

ldin

g T

ime O

utl

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ple

ase s

ee f

ollo

win

g p

ag

es f

or

full d

eta

ils.

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

uality

Co

ntr

ol S

am

ple

s

l

Qu

ality

Co

ntr

ol S

am

ple

Fre

qu

en

cy O

utl

iers

exis

t -

ple

ase s

ee f

ollo

win

g p

ag

es f

or

full d

eta

ils.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 43: Cover - Attach C14h

2 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime

Co

mp

lia

nc

e

Ma

trix

: S

OIL

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

n

Da

te a

na

lyse

dD

ate

extr

acte

dC

on

tain

er

/ C

lient S

am

ple

ID

(s)

Days

overd

ue

Days

overd

ue

Du

e f

or

extr

actio

nD

ue

fo

r a

na

lysis

Meth

od

EN

33:

TC

LP

Leach

No

n-V

ola

tile

Leach

: 14 d

ay H

T(e

.g. S

V o

rgan

ics)

----

11

-Fe

b-2

02

0Q

C1

00

----

15

-Fe

b-2

02

04

----

Ou

tlie

rs :

Fre

qu

en

cy

of

Qu

ali

ty C

on

tro

l S

am

ple

s

Ma

trix

: W

AT

ER

Qualit

y C

ontr

ol S

pecific

ation

Qualit

y C

ontr

ol S

am

ple

Typ

e

Meth

od

Expecte

dQ

CR

egula

rA

ctu

al

Ra

te (

%)

Qualit

y C

ontr

ol S

am

ple

Typ

eC

ou

nt

La

bo

rato

ry D

up

lica

tes

(DU

P)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

0.0

0 1

0.0

00

12

Ma

trix

Sp

ike

s (M

S)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

0.0

0 5

.00

01

2

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

tim

e

is

7 d

ays;

o

the

rs

14

da

ys.

A

re

co

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes

of

inte

rest/

con

cern

.

Ho

ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

Ass

ess

me

nt

com

pa

res

the

le

ach

d

ate

w

ith

th

e

sho

rte

st

an

aly

te

ho

ldin

g

time

fo

r th

e

eq

uiv

ale

nt

so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

A r

eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

If s

am

ple

s a

re id

en

tifie

d b

elo

w a

s h

avi

ng

be

en

an

aly

sed

or

ext

ract

ed

ou

tsid

e o

f re

com

me

nd

ed

ho

ldin

g t

ime

s,

this

sh

ou

ld b

e t

ake

n in

to c

on

sid

era

tion

wh

en

inte

rpre

ting

re

sults

.

Th

is

rep

ort

su

mm

arize

s e

xtra

ctio

n

/ p

rep

ara

tion

a

nd

a

na

lysi

s tim

es

an

d

com

pa

res

ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

nci

ng

U

SE

PA

S

W

84

6,

AP

HA

, A

S

an

d

NE

PM

) b

ase

d

on

th

e

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

rese

nt

first

da

te o

f e

xtra

ctio

n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A lis

ting

of

bre

ach

es

(if

an

y)

is p

rovi

de

d h

ere

in.

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EN

33:

TC

LP

Leach

No

n-V

ola

tile

Leach

: 14 d

ay H

T(e

.g. S

V o

rgan

ics)

(EN

33a)

QC

10

0--

--1

1-F

eb

-20

20

----

15-F

eb

-20

20

28-J

an

-2020

û--

--

No

n-V

ola

tile

Leach

: 14 d

ay H

T(e

.g. S

V o

rgan

ics)

(EN

33a)

BH

11

7_

2.2

-2.3

----

13

-Fe

b-2

02

0--

--13-F

eb

-20

20

30-J

an

-2020

ü--

--

No

n-V

ola

tile

Leach

: 180 d

ay H

T (

e.g

. P

FA

S, m

eta

ls e

x.H

g)

(EN

33a)

BH

11

1_

0.6

5-0

.75

----

28

-Ju

l-2

02

0--

--15-F

eb

-20

20

30-J

an

-2020

ü--

--

No

n-V

ola

tile

Leach

: 28 d

ay H

T(e

.g. H

g, C

rVI)

(E

N33a)

BH

11

4_

1.3

-1.4

----

02

-Ma

r-2

02

0--

--15-F

eb

-20

20

03-F

eb

-2020

ü--

--

No

n-V

ola

tile

Leach

: 28 d

ay H

T(e

.g. H

g, C

rVI)

(E

N33a)

BH

10

8_

1.3

-1.4

,B

H1

07

_1

.5-1

.7,

BH

10

9_

0.9

-1.0

----

25

-Fe

b-2

02

0--

--15-F

eb

-20

20

28-J

an

-2020

ü--

--

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

Page 44: Cover - Attach C14h

3 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

Cle

ar

Pla

sti

c B

ott

le -

Nit

ric A

cid

; U

nfi

ltere

d (

EG

005C

)

QC

10

0,

BH

10

8_

1.3

-1.4

,

BH

10

7_

1.5

-1.7

,B

H1

09

_0

.9-1

.0,

BH

11

1_

0.6

5-0

.75

13

-Au

g-2

02

01

3-A

ug

-20

20

17

-Feb

-202

017-F

eb

-20

20

15-F

eb

-2020

üü

EG

050G

: H

exavale

nt

Ch

rom

ium

by D

iscre

te A

naly

ser

Cle

ar

Pla

sti

c B

ott

le -

NaO

H (

EG

050G

-C)

BH

10

8_

1.3

-1.4

,B

H1

07

_1

.5-1

.7,

BH

10

9_

0.9

-1.0

,B

H1

14

_1

.3-1

.4

14

-Ma

r-2

02

0--

--17

-Feb

-202

0--

--15-F

eb

-2020

----

ü

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P075(S

IM))

BH

11

7_

2.2

-2.3

26

-Ma

r-2

02

02

0-F

eb

-20

20

17

-Feb

-202

015-F

eb

-20

20

13-F

eb

-2020

üü

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P075(S

IM))

QC

10

02

8-M

ar-

20

20

22

-Fe

b-2

02

017

-Feb

-202

017-F

eb

-20

20

15-F

eb

-2020

üü

Page 45: Cover - Attach C14h

4 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Qu

ality

Co

ntr

ol P

ara

mete

r F

req

uen

cy C

om

plian

ce

Th

e f

ollo

win

g r

ep

ort

su

mm

arise

s th

e f

req

ue

ncy

of

lab

ora

tory

QC

sa

mp

les

an

aly

sed

with

in t

he

an

aly

tica

l lo

t(s)

in

wh

ich

th

e s

ub

mitt

ed

sa

mp

le(s

) w

as(

we

re)

pro

cess

ed

. A

ctu

al r

ate

sh

ou

ld b

e g

rea

ter

tha

n o

r e

qu

al t

o

the

exp

ect

ed

ra

te.

A li

stin

g o

f b

rea

che

s is

pro

vid

ed

in t

he

Su

mm

ary

of

Ou

tlie

rs.

Ma

trix

: S

OIL

Eva

lua

tio

n: û

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy

no

t w

ithin

sp

eci

fica

tion

; ü

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy w

ithin

sp

ecifi

ca

tion

.

Qu

alit

y C

on

tro

l Sp

ecifi

ca

tion

Qualit

y C

ontr

ol S

am

ple

Typ

e

Exp

ecte

dQ

CR

eg

ula

rA

ctu

al

Ra

te (

%)

Qualit

y C

ontr

ol S

am

ple

Typ

eC

ou

nt

Eva

lua

tio

nA

na

lytic

al M

eth

od

sM

eth

od

Me

tho

d B

lan

ks (

MB

)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

9.5

2 9

.09

22

TC

LP

fo

r N

on

& S

em

ivo

latil

e A

na

lyte

sE

N3

3a

Ma

trix

: W

AT

ER

Eva

lua

tio

n: û

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy

no

t w

ithin

sp

eci

fica

tion

; ü

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy w

ithin

sp

ecifi

ca

tion

.

Qu

alit

y C

on

tro

l Sp

ecifi

ca

tion

Qualit

y C

ontr

ol S

am

ple

Typ

e

Exp

ecte

dQ

CR

eg

ula

rA

ctu

al

Ra

te (

%)

Qualit

y C

ontr

ol S

am

ple

Typ

eC

ou

nt

Eva

lua

tio

nA

na

lytic

al M

eth

od

sM

eth

od

La

bo

rato

ry D

up

lica

tes

(DU

P)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

33.3

3 1

0.0

02

He

xava

len

t C

hro

miu

m b

y D

iscr

ete

An

aly

ser

- L

ea

cha

ble

EG

05

0G

-C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

10.5

3 1

0.0

02

19

üL

ea

cha

ble

Me

tals

by

ICP

AE

SE

G0

05

C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

0.0

0 1

0.0

00

12

ûP

AH

/Ph

en

ols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)

La

bo

rato

ry C

on

tro

l Sa

mp

les

(LC

S)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

33.3

3 5

.00

26

üH

exa

vale

nt

Ch

rom

ium

by

Dis

cre

te A

na

lyse

r -

Le

ach

ab

leE

G0

50

G-C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

5.2

6 5

.00

11

Le

ach

ab

le M

eta

ls b

y IC

PA

ES

EG

00

5C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

16.6

7 5

.00

21

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

EP

07

5(S

IM)

Me

tho

d B

lan

ks (

MB

)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

33.3

3 5

.00

26

üH

exa

vale

nt

Ch

rom

ium

by

Dis

cre

te A

na

lyse

r -

Le

ach

ab

leE

G0

50

G-C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

5.2

6 5

.00

11

Le

ach

ab

le M

eta

ls b

y IC

PA

ES

EG

00

5C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

16.6

7 5

.00

21

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

EP

07

5(S

IM)

Ma

trix

Sp

ike

s (M

S)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

33.3

3 5

.00

26

üH

exa

vale

nt

Ch

rom

ium

by

Dis

cre

te A

na

lyse

r -

Le

ach

ab

leE

G0

50

G-C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

5.2

6 5

.00

11

Le

ach

ab

le M

eta

ls b

y IC

PA

ES

EG

00

5C

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

0.0

0 5

.00

01

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

EP

07

5(S

IM)

Page 46: Cover - Attach C14h

5 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

0

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Bri

ef

Meth

od

Su

mm

ari

es

Th

e a

na

lytic

al p

roce

du

res

use

d b

y th

e E

nvi

ron

me

nta

l Div

isio

n h

ave

be

en

de

velo

pe

d f

rom

est

ab

lish

ed

in

tern

atio

na

lly r

eco

gn

ize

d p

roce

du

res s

uch

as

tho

se p

ub

lish

ed

by

the

US

EP

A,

AP

HA

, A

S a

nd

NE

PM

. In

ho

use

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Th

e f

ollo

win

g r

ep

ort

pro

vid

es

brie

f d

esc

rip

tio

ns

of

the

an

aly

tica

l pro

ced

ure

s e

mp

loye

d f

or

resu

lts r

ep

ort

ed

in t

he

Ce

rtifi

cate

of

An

aly

sis.

So

urc

es

fro

m w

hic

h A

LS

me

tho

ds

ha

ve b

ee

n d

eve

lop

ed

are

pro

vid

ed

with

in t

he

Me

tho

d D

esc

rip

tion

s.

An

aly

tica

l Me

tho

ds

Me

tho

d D

esc

rip

tion

sM

atr

ixM

eth

od

In h

ouse

: re

fere

nce

d to A

PH

A 3

120; U

SE

PA

SW

846 -

6010: T

he IC

PA

ES

tech

niq

ue io

nis

es

leach

ate

sam

ple

ato

ms

em

ittin

g a

chara

cterist

ic s

pect

rum

. T

his

spect

rum

is then c

om

pare

d a

gain

st m

atr

ix m

atc

hed s

tandard

s fo

r

quantif

icatio

n. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

Leach

able

Meta

ls b

y IC

PA

ES

EG

00

5C

SO

IL

In h

ouse

: R

efe

rence

d to A

PH

A 3

500 C

r-A

& B

. H

exa

vale

nt ch

rom

ium

is d

ete

rmin

ed d

irect

ly o

n le

ach

ate

sam

ple

s

by

Desc

rete

Analy

ser

as

rece

ived b

y pH

adju

stm

ent and c

olo

ur

deve

lopm

ent usi

ng d

ephenyl

carb

azi

de. E

ach

run

of sa

mple

s is

measu

red a

gain

st a

fiv

e-p

oin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

Hexa

vale

nt C

hro

miu

m b

y D

iscr

ete

Analy

ser

- Leach

able

EG

05

0G

-CS

OIL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

8270D

S

am

ple

ext

ract

s are

analy

sed b

y C

apill

ary

GC

/MS

in S

IM M

ode

and q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt

with

NE

PM

(2013)

Sch

edule

B(3

)

PA

H/P

henols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)S

OIL

Pre

pa

ratio

n M

eth

od

sM

eth

od

De

scrip

tion

sM

atr

ixM

eth

od

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846-3

005. M

eth

od 3

005 is

a N

itric

/Hyd

roch

loric

aci

d d

igest

ion p

roce

dure

use

d to p

repare

surf

ace

and g

round w

ate

r sa

mple

s fo

r analy

sis

by

ICP

AE

S o

r IC

PM

S. T

his

meth

od is

com

plia

nt

with

NE

PM

(2013)

Sch

edule

B(3

)

Dig

est

ion for

Tota

l Reco

vera

ble

Meta

ls

in T

CLP

Leach

ate

EN

25

CS

OIL

In h

ouse

QW

I-E

N/3

3 r

efe

rence

d to U

SE

PA

SW

846-1

311: T

he T

CLP

pro

cedure

is d

esi

gned to d

ete

rmin

e the

mobili

ty o

f both

org

anic

and in

org

anic

analy

tes

pre

sent in

wast

es.

The s

tandard

TC

LP

leach

is for

non-v

ola

tile

and S

em

ivola

tile test

para

mete

rs.

TC

LP

for

Non &

Sem

ivola

tile A

naly

tes

EN

33

aS

OIL

In h

ouse

: R

efe

rence

d to U

SE

PA

SW

846 -

3510B

100 m

L to 1

L o

f sa

mple

is tra

nsf

err

ed to a

separa

tory

funnel

and s

erially

ext

ract

ed thre

e tim

es

usi

ng D

CM

for

each

ext

ract

. T

he r

esu

ltant ext

ract

s are

com

bin

ed, dehyd

rate

d

and c

once

ntr

ate

d for

analy

sis.

This

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

) . A

LS

defa

ult

exc

ludes

sedim

ent w

hic

h m

ay

be r

esi

dent in

the c

onta

iner.

Separa

tory

Funnel E

xtra

ctio

n o

f Liq

uid

sO

RG

14

SO

IL

Page 47: Cover - Attach C14h

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES2004680

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Brenda Hong

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60623599_1.1-Burrows IE Page 1 of 2

:Order number 60623599_1.1 :Quote number EB2017AECOMAU0014 (EN/004/16)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : ----

Sampler :

DatesDate Samples Received : Issue Date : 12-Feb-202029-Jan-2020 15:45

Scheduled Reporting Date: 18-Feb-2020:Client Requested Due

Date

18-Feb-2020

Delivery DetailsMode of Delivery : :Samples On Hand Not AvailableSecurity Seal

No. of coolers/boxes : :---- Temperature 4.1

: : 7 / 7Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Rebatch of ES2002807, ES2002766, ES2003147 and ES2003366.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (3 weeks), Solid (2 months ± 1 week) from receipt of samples.

l Please be aware that APHA/NEPM recommends water and soil samples be chilled to less than or equal to 6°C for chemical

analysis, and less than or equal to 10°C but unfrozen for Microbiological analysis. Where samples are received above this

temperature, it should be taken into consideration when interpreting results. Refer to ALS EnviroMail 85 for ALS

recommendations of the best practice for chilling samples after sampling and for maintaining a cool temperature during transit.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 48: Cover - Attach C14h

:Client AECOM Australia Pty Ltd

Work Order : ES2004680 Amendment 02 of 2:Page

12-Feb-2020:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

SO

IL -

EG

005C

Leachable

Meta

ls b

y IC

PA

ES

SO

IL -

EG

050G

-C

Hexavale

nt C

hro

miu

m in T

CLP

Leach

ate

SO

IL -

EN

33a

TC

LP

Leach

ate

SO

IL -

EP

075 S

IM P

AH

only

SIM

- P

AH

only

ES2004680-001 28-Jan-2020 00:00 QC100 ü ü ü

ES2004680-002 28-Jan-2020 00:00 BH108_1.3-1.4 ü ü ü

ES2004680-003 28-Jan-2020 00:00 BH107_1.5-1.7 ü ü ü

ES2004680-004 28-Jan-2020 00:00 BH109_0.9-1.0 ü ü ü

ES2004680-005 30-Jan-2020 00:00 BH111_0.65-0.75 ü ü

ES2004680-006 30-Jan-2020 00:00 BH117_2.2-2.3 ü ü

ES2004680-007 03-Feb-2020 00:00 BH114_1.3-1.4 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

- Chain of Custody (CoC) (COC) Email AP_CustomerService.ANZ@aecom.

com

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 AECOM (EQUIS_V5_AECOM) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

Page 49: Cover - Attach C14h
Page 50: Cover - Attach C14h
Page 51: Cover - Attach C14h

0 0

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mp

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sed

This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. T

his

docu

ment sh

all

not be r

epro

duce

d, exc

ept in

full.

This

Cert

ifica

te o

f A

naly

sis

conta

ins

the follo

win

g in

form

atio

n:

l

Genera

l Com

ments

l

Analy

tical R

esu

lts

l

Surr

ogate

Contr

ol L

imits

Ad

dit

ion

al

info

rmati

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p

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t to

th

is

rep

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w

ill

be

fou

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in

th

e

follo

win

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sep

ara

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att

ach

men

ts:

Qu

ality

C

on

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ep

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A/Q

C

Co

mp

lian

ce

Assessm

en

t to

assis

t w

ith

Qu

ality

Revie

w a

nd

Sam

ple

Receip

t N

oti

ficati

on

.

Sig

nato

ries

This

docu

ment has

been e

lect

ronic

ally

sig

ned b

y th

e a

uth

orize

d s

ignato

ries

belo

w. E

lect

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sig

nin

g is

carr

ied o

ut in

com

plia

nce w

ith p

roce

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s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

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ory

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andy

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s, S

mith

field

, N

SW

Ivan T

ayl

or

Analy

stS

ydney

Inorg

anic

s, S

mith

field

, N

SW

R I

G H

T

S O

L U

T I

O N

S

|

R I

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T

P A

R T

N E

R

Page 52: Cover - Attach C14h

2 o

f 5

:P

ag

e

Wo

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Clie

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ES

20

04

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2

60

62

35

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AE

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M A

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Pty

Ltd

Gen

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men

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Th

e

an

aly

tica

l p

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du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

velo

pe

d

fro

m

est

ab

lish

ed

in

tern

atio

na

lly

reco

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ize

d

pro

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ure

s su

ch

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

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in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/d

ige

sta

te d

ilutio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis.

Wh

ere

th

e L

OR

of

a r

ep

ort

ed

re

sult

diff

ers

fro

m s

tan

da

rd L

OR

, th

is m

ay

be

du

e t

o h

igh

mo

istu

re c

on

ten

t, in

suff

icie

nt

sam

ple

(re

du

ced

we

igh

t e

mp

loye

d)

or

ma

trix

inte

rfe

ren

ce.

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en

sa

mp

ling

tim

e in

form

atio

n is

no

t p

rovi

de

d b

y th

e c

lien

t, s

am

plin

g d

ate

s a

re s

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wn

with

ou

t a

tim

e c

om

po

ne

nt.

In

th

ese

insta

nce

s, t

he

tim

e c

om

po

ne

nt

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s b

ee

n a

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y th

e la

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rato

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or

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a r

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lt is

re

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ire

d t

o m

ee

t co

mp

lian

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mits

th

e a

sso

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un

cert

ain

ty m

ust

be

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ere

d.

Re

fer

to t

he

AL

S C

on

tact

for

de

tails

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CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

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ase

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ract

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Ch

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ivis

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of

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Am

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n C

he

mic

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oci

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R =

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it o

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^ =

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aly

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or

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ove

th

e le

vel o

f re

po

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g

ø =

AL

S is

no

t N

AT

A a

ccre

dite

d f

or

the

se t

est

s.

~ =

In

dic

ate

s a

n e

stim

ate

d v

alu

e.

Ke

y : B

en

zo(a

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en

e T

oxi

city

Eq

uiv

ale

nt

Qu

otie

nt

(TE

Q)

pe

r th

e N

EP

M (

20

13

) is

th

e s

um

to

tal o

f th

e c

on

cen

tra

tion

of

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eig

ht

carc

ino

ge

nic

PA

Hs

mu

ltip

lied

by

the

ir T

oxic

ity E

qu

iva

len

ce F

act

or

(TE

F)

rela

tive

to

Be

nzo

(a)p

yre

ne

. T

EF

va

lue

s a

re p

rovi

de

d in

bra

cke

ts a

s fo

llow

s: B

en

z(a

)an

thra

cen

e (

0.1

), C

hry

se

ne

(0

.01

), B

en

zo(b

+j) &

Be

nzo

(k)f

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ne

(0

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nzo

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.0),

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no

(1.2

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d)p

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(0

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nth

race

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(1

.0),

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0.0

1).

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ss t

ha

n L

OR

re

sults

fo

r 'T

EQ

Ze

ro' a

re t

rea

ted

as

ze

ro.

l

Page 53: Cover - Attach C14h

3 o

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31

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

ES

20046

82-0

04

ES

2004

682

-003

ES

2004682-0

02

ES

2004682-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

----

EN

33:

TC

LP

Leach

8.6

8.5

8.8

8.6

----

pH

Un

it0

.1--

--In

itia

l p

H

1.6

1.6

1.6

1.6

----

pH

Un

it0

.1--

--A

fter

HC

l p

H

11

11

----

-1

----

Extr

acti

on

Flu

id N

um

ber

5.3

5.3

5.2

5.2

----

pH

Un

it0

.1--

--F

inal p

H

Page 54: Cover - Attach C14h

4 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

2

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

BH

102_0.5

-0.6

BH

105_1.7

-1.8

BH

105_0.8

5-0

.95

BH

115_2.5

-2.6

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

TC

LP

LE

AC

HA

TE

(M

atr

ix:

WA

TE

R)

----

31

-Ja

n-2

02

0 0

0:0

03

1-J

an

-20

20

00

:00

31

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

ES

20046

82-0

04

ES

2004

682

-003

ES

2004682-0

02

ES

2004682-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

----

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

<0

.1A

rsen

ic--

----

----

----

--m

g/L

0.1

74

40

-38

-2

54.1

Lead

8.6

20.6

0.9

----

mg

/L0

.17

43

9-9

2-1

0.2

Nic

kel

----

0.2

----

----

mg

/L0

.17

44

0-0

2-0

EG

035C

: L

each

ab

le M

erc

ury

by F

IMS

----

Merc

ury

----

----

<0

.00

10

----

mg

/L0

.00

10

74

39

-97

-6

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

----

Ben

zo(a

)pyre

ne

<0

.5--

--<

0.5

----

µg

/L0

.55

0-3

2-8

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

----

Ph

en

ol-

d6

23.8

----

25

.5--

--%

1.0

13

12

7-8

8-3

----

2-C

hlo

rop

hen

ol-

D4

53.7

----

54

.9--

--%

1.0

93

95

1-7

3-6

----

2.4

.6-T

rib

rom

op

hen

ol

50.7

----

61

.5--

--%

1.0

11

8-7

9-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

----

2-F

luo

rob

iph

en

yl

66.4

----

72

.9--

--%

1.0

32

1-6

0-8

----

An

thra

cen

e-d

10

81.1

----

92

.4--

--%

1.0

17

19

-06

-8

----

4-T

erp

hen

yl-

d14

91.3

----

85

.2--

--%

1.0

17

18

-51

-0

Page 55: Cover - Attach C14h

5 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

2

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

Su

rro

gate

Co

ntr

ol L

imit

s

Reco

very

Lim

its (

%)

Su

b-M

atr

ix:

TC

LP

LE

AC

HA

TE

Co

mp

ou

nd

CA

S N

um

be

rL

ow

Hig

h

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

Ph

en

ol-

d6

13

12

7-8

8-3

10

44

2-C

hlo

rop

hen

ol-

D4

93

95

1-7

3-6

14

94

2.4

.6-T

rib

rom

op

hen

ol

11

8-7

9-6

17

12

5

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

2-F

luo

rob

iph

en

yl

32

1-6

0-8

20

10

4

An

thra

cen

e-d

10

17

19

-06

-82

71

13

4-T

erp

hen

yl-

d14

17

18

-51

-03

21

12

Page 56: Cover - Attach C14h

Fals

e 2 2

.00

Tru

e

Envir

onm

ental

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:E

S2004682

Pa

ge

:1

of 3

::

La

bo

rato

ryC

lien

tE

nvi

ronm

enta

l Div

isio

n S

ydney

AE

CO

M A

ustr

alia P

ty L

td

:C

onta

ctM

R A

LE

X L

AT

HA

M:

Conta

ctB

renda H

ong

:A

dd

ress

LE

VE

L 2

1, 420 G

EO

RG

E S

TR

EE

T

SY

DN

EY

NS

W, A

US

TR

ALIA

2000

Ad

dre

ss:

277-2

89 W

oodpark

Road S

mith

field

NS

W A

ust

ralia

2164

::

Te

lep

ho

ne

+61 0

2 8

934 0

000

+61 2

8784 8

555

:T

ele

ph

on

e

:P

roje

ct60623599_1.1

-Burr

ow

s IE

Da

te S

am

ple

s R

ece

ive

d:03-F

eb-2

020

:O

rde

r n

um

be

r60623599_1.1

Da

te A

na

lysis

Co

mm

en

ce

d:15-F

eb-2

020

:C

-O-C

nu

mb

er

----

Issu

e D

ate

:18-F

eb-2

020

Sa

mp

ler

:--

--

Site

:--

--

Qu

ote

nu

mb

er

:E

N/0

04/1

6

No

. o

f sa

mp

les

rece

ive

d4

:

No

. o

f sa

mp

les

an

aly

sed

4:

This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. T

his

docu

ment sh

all

not be r

epro

duce

d, exc

ept in

full.

This

Qualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

La

bo

rato

ry D

up

lica

te (

DU

P)

Re

po

rt;

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce (

RP

D)

an

d A

cce

pta

nce

Lim

its

l

Me

tho

d B

lan

k (M

B)

an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

l

Ma

trix

Sp

ike

(M

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

Sig

nato

ries

This

docu

ment has

been e

lect

ronic

ally

sig

ned b

y th

e a

uth

orize

d s

ignato

ries

belo

w. E

lect

ronic

sig

nin

g is

carr

ied o

ut in

com

plia

nce

with

pro

cedure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

sitio

n

Ed

wa

nd

y F

ad

jar

Org

an

ic C

oo

rdin

ato

rS

yd

ne

y O

rga

nic

s, S

mith

field

, N

SW

Iva

n T

ayl

or

An

aly

stS

yd

ne

y In

org

an

ics,

Sm

ithfie

ld,

NS

W

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 57: Cover - Attach C14h

2 o

f 3

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

2

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Gen

era

l C

om

men

ts

Th

e

an

aly

tica

l p

roce

du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

ve

lop

ed

fr

om

e

sta

blis

he

d

inte

rna

tion

ally

re

cog

niz

ed

p

roce

du

res

such

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/

dig

est

ate

dilu

tio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis

. W

he

re t

he

LO

R o

f a

re

po

rte

d r

esu

lt d

iffe

rs f

rom

sta

nd

ard

LO

R,

this

ma

y b

e d

ue

to

hig

h m

ois

ture

co

nte

nt,

insu

ffic

ien

t sa

mp

le (

red

uce

d w

eig

ht

em

plo

yed

) o

r m

atr

ix in

terf

ere

nce

.

An

on

ymo

us

= R

efe

rs t

o s

am

ple

s w

hic

h a

re n

ot

spe

cific

ally

pa

rt o

f th

is w

ork

ord

er

bu

t fo

rme

d p

art

of

the

QC

pro

cess

lot

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

da

tab

ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l A

bstr

acts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

RP

D =

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce

#

= I

nd

ica

tes

faile

d Q

C

Ke

y :

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

D

up

lica

te

refe

rs

to

a

ran

do

mly

se

lect

ed

in

tra

lab

ora

tory

sp

lit.

La

bo

rato

ry

du

plic

ate

s

pro

vid

e

info

rma

tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

erc

en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:

0%

- 5

0%

; R

esu

lt >

20

tim

es

LO

R:

0%

- 2

0%

.

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EG

005(E

D093)C

: L

each

ab

le M

eta

ls b

y IC

PA

ES

(Q

C L

ot:

2862670)

EG

00

5C

: A

rse

nic

74

40

-38

-20

.1m

g/L

<0

.1<

0.1

0.0

0N

o L

imit

An

on

ymo

us

ES

20

03

94

6-0

01

EG

00

5C

: L

ea

d7

43

9-9

2-1

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: N

icke

l7

44

0-0

2-0

0.1

mg

/L<

0.1

<0

.10

.00

No

Lim

it

EG

00

5C

: A

rse

nic

74

40

-38

-20

.1m

g/L

<0

.1<

0.1

0.0

0N

o L

imit

An

on

ymo

us

ES

20

04

68

0-0

04

EG

00

5C

: L

ea

d7

43

9-9

2-1

0.1

mg

/L2

.32

.30

.00

0%

- 2

0%

EG

00

5C

: N

icke

l7

44

0-0

2-0

0.1

mg

/L0

.60

.60

.00

No

Lim

it

EG

035C

: L

each

ab

le M

erc

ury

by F

IMS

(Q

C L

ot:

2864781)

EG

03

5C

: M

erc

ury

74

39

-97

-60

.00

01

mg

/L<

0.0

01

0<

0.0

01

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

45

94

-00

1

Page 58: Cover - Attach C14h

3 o

f 3

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

2

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1-B

urr

ow

s IE

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

pik

e

(LC

S)

refe

rs

to

a

cert

ifie

d

refe

ren

ce

ma

teria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EN

33:

TC

LP

Leach

(Q

CL

ot:

2861763)

EN

33

a:

Initi

al p

H--

--0

.1p

H U

nit

1.0

----

----

----

----

EN

33

a:

Aft

er

HC

l pH

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it1

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----

----

--

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33

a:

Fin

al p

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b-M

atr

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TE

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MB

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ort

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ora

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LC

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%)

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ea

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yd

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ple

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pre

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se

o

f th

is

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ara

me

ter

is

to

mo

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r p

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l m

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ects

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n

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aly

te r

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s. S

tatic

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cove

ry L

imits

as

pe

r la

bo

rato

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ata

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alit

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ea

l re

cove

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ge

s sta

ted

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y b

e w

aiv

ed

in t

he

eve

nt

of

sa

mp

le m

atr

ix in

terf

ere

nce

.

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b-M

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TE

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atr

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MS

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its (

%)

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ow

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ncen

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on

Lab

ora

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ple

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Clien

t sam

ple

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od:

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mp

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eta

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y IC

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ES

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ot:

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on

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ot:

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Page 59: Cover - Attach C14h

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Envir

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Th

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uto

mati

cally g

en

era

ted

by t

he A

LS

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S t

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h in

terp

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Qu

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rs m

easu

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LS

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his

au

tom

ate

d

rep

ort

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hlig

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y n

on

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on

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d is d

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t in

tern

al exp

ert

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r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

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ntr

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QC

) R

ep

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l

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od

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nk v

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utl

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r.

l

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tlie

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l

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ora

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l

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r all r

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ccu

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aly

sis

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l

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aly

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ldin

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ple

ase s

ee f

ollo

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qu

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Page 60: Cover - Attach C14h

2 o

f 5

:P

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Wo

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Clie

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20

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68

2

AE

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Pty

Ltd

60

62

35

99

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Ou

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An

aly

sis

Ho

ldin

g T

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Co

mp

lia

nc

e

Ma

trix

: S

OIL

An

aly

sis

Extr

actio

n /

Pre

pa

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n

Da

te a

na

lyse

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ate

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/ C

lient S

am

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(s)

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overd

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Days

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Du

e f

or

extr

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nD

ue

fo

r a

na

lysis

Meth

od

EN

33:

TC

LP

Leach

No

n-V

ola

tile

Leach

: 14 d

ay H

T(e

.g. S

V o

rgan

ics)

----

14

-Fe

b-2

02

0B

H1

05

_0

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5,

BH

10

2_

0.5

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15

-Fe

b-2

02

01

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Ou

tlie

rs :

Fre

qu

en

cy

of

Qu

ali

ty C

on

tro

l S

am

ple

s

Ma

trix

: W

AT

ER

Qualit

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ontr

ol S

pecific

ation

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ple

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e

Meth

od

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CR

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al

Ra

te (

%)

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ontr

ol S

am

ple

Typ

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nt

La

bo

rato

ry D

up

lica

tes

(DU

P)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

0.0

0 1

0.0

00

9

Ma

trix

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ike

s (M

S)

NE

PM

20

13

B3

& A

LS

QC

Sta

nd

ard

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

0.0

0 5

.00

09

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aly

sis

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ldin

g T

ime C

om

plian

ce

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

tim

e

is

7 d

ays;

o

the

rs

14

da

ys.

A

re

co

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes

of

inte

rest/

con

cern

.

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ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

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ess

me

nt

com

pa

res

the

le

ach

d

ate

w

ith

th

e

sho

rte

st

an

aly

te

ho

ldin

g

time

fo

r th

e

eq

uiv

ale

nt

so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

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eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

If s

am

ple

s a

re id

en

tifie

d b

elo

w a

s h

avi

ng

be

en

an

aly

sed

or

ext

ract

ed

ou

tsid

e o

f re

com

me

nd

ed

ho

ldin

g t

ime

s,

this

sh

ou

ld b

e t

ake

n in

to c

on

sid

era

tion

wh

en

inte

rpre

ting

re

sults

.

Th

is

rep

ort

su

mm

arize

s e

xtra

ctio

n

/ p

rep

ara

tion

a

nd

a

na

lysi

s tim

es

an

d

com

pa

res

ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

nci

ng

U

SE

PA

S

W

84

6,

AP

HA

, A

S

an

d

NE

PM

) b

ase

d

on

th

e

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

rese

nt

first

da

te o

f e

xtra

ctio

n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A lis

ting

of

bre

ach

es

(if

an

y)

is p

rovi

de

d h

ere

in.

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EN

33:

TC

LP

Leach

No

n-V

ola

tile

Leach

: 14 d

ay H

T(e

.g. S

V o

rgan

ics)

(EN

33a)

BH

10

5_

0.8

5-0

.95

,B

H1

02

_0

.5-0

.6--

--1

4-F

eb

-20

20

----

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eb

-20

20

31-J

an

-2020

û--

--

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n-V

ola

tile

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ay H

T (

e.g

. P

FA

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eta

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x.H

g)

(EN

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5_

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20

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ay H

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eta

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g)

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0--

--15-F

eb

-20

20

31-J

an

-2020

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--

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

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actio

nD

ate

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tain

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/ C

lien

t S

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(s)

EG

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eta

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y IC

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ES

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ar

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ott

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nfi

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EG

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BH

11

5_

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_0

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13

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01

3-A

ug

-20

20

17

-Feb

-202

017-F

eb

-20

20

15-F

eb

-2020

üü

Page 61: Cover - Attach C14h

3 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

04

68

2

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

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urr

ow

s IE

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roje

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trix

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AT

ER

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= H

old

ing

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e b

rea

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; ü

= W

ithin

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ldin

g t

ime

.

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aly

sis

Extr

actio

n /

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pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

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an

aly

sed

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lua

tio

nD

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fo

r e

xtr

actio

nD

ate

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tain

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t S

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ury

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20

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Page 62: Cover - Attach C14h

4 o

f 5

:P

ag

e

Wo

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Page 63: Cover - Attach C14h

5 o

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atr

ix m

atc

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s fo

r

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n. T

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Page 64: Cover - Attach C14h

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES2004682

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Brenda Hong

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60623599_1.1-Burrows IE Page 1 of 2

:Order number 60623599_1.1 :Quote number EB2017AECOMAU0014 (EN/004/16)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : ----

Sampler :

DatesDate Samples Received : Issue Date : 12-Feb-202003-Feb-2020 15:40

Scheduled Reporting Date: 18-Feb-2020:Client Requested Due

Date

18-Feb-2020

Delivery DetailsMode of Delivery : :Samples On Hand Not AvailableSecurity Seal

No. of coolers/boxes : :---- Temperature 4.1

: : 4 / 4Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l This is a rebatch of ES2003481 and ES2003147.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (3 weeks), Solid (2 months ± 1 week) from receipt of samples.

l Please be aware that APHA/NEPM recommends water and soil samples be chilled to less than or equal to 6°C for chemical

analysis, and less than or equal to 10°C but unfrozen for Microbiological analysis. Where samples are received above this

temperature, it should be taken into consideration when interpreting results. Refer to ALS EnviroMail 85 for ALS

recommendations of the best practice for chilling samples after sampling and for maintaining a cool temperature during transit.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 65: Cover - Attach C14h

:Client AECOM Australia Pty Ltd

Work Order : ES2004682 Amendment 02 of 2:Page

12-Feb-2020:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

SO

IL -

EG

005C

Leachable

Meta

ls b

y IC

PA

ES

SO

IL -

EG

035C

Leachable

Merc

ury

SO

IL -

EN

33a

TC

LP

Leach

ate

SO

IL -

EP

075 S

IM P

AH

only

SIM

- P

AH

only

ES2004682-001 29-Jan-2020 00:00 BH115_2.5-2.6 ü ü

ES2004682-002 31-Jan-2020 00:00 BH105_0.85-0.95 ü ü ü

ES2004682-003 31-Jan-2020 00:00 BH105_1.7-1.8 ü ü

ES2004682-004 31-Jan-2020 00:00 BH102_0.5-0.6 ü ü ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

- Chain of Custody (CoC) (COC) Email AP_CustomerService.ANZ@aecom.

com

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 AECOM (EQUIS_V5_AECOM) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

Page 66: Cover - Attach C14h
Page 67: Cover - Attach C14h
Page 68: Cover - Attach C14h

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carr

ied o

ut in

com

plia

nce w

ith p

roce

dure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

sitio

n

Edw

andy

Fadja

rO

rganic

Coord

inato

rS

ydney

Org

anic

s, S

mith

field

, N

SW

Ivan T

ayl

or

Analy

stS

ydney

Inorg

anic

s, S

mith

field

, N

SW

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 69: Cover - Attach C14h

2 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

Gen

era

l C

om

men

ts

Th

e

an

aly

tica

l p

roce

du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

velo

pe

d

fro

m

est

ab

lish

ed

in

tern

atio

na

lly

reco

gn

ize

d

pro

ced

ure

s su

ch

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/d

ige

sta

te d

ilutio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis.

Wh

ere

th

e L

OR

of

a r

ep

ort

ed

re

sult

diff

ers

fro

m s

tan

da

rd L

OR

, th

is m

ay

be

du

e t

o h

igh

mo

istu

re c

on

ten

t, in

suff

icie

nt

sam

ple

(re

du

ced

we

igh

t e

mp

loye

d)

or

ma

trix

inte

rfe

ren

ce.

Wh

en

sa

mp

ling

tim

e in

form

atio

n is

no

t p

rovi

de

d b

y th

e c

lien

t, s

am

plin

g d

ate

s a

re s

ho

wn

with

ou

t a

tim

e c

om

po

ne

nt.

In

th

ese

insta

nce

s, t

he

tim

e c

om

po

ne

nt

ha

s b

ee

n a

ssu

me

d b

y th

e la

bo

rato

ry f

or

pro

cess

ing

pu

rpo

ses.

Wh

ere

a r

esu

lt is

re

qu

ire

d t

o m

ee

t co

mp

lian

ce li

mits

th

e a

sso

cia

ted

un

cert

ain

ty m

ust

be

co

nsid

ere

d.

Re

fer

to t

he

AL

S C

on

tact

for

de

tails

.

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

da

tab

ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l Ab

stra

cts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

^ =

Th

is r

esu

lt is

co

mp

ute

d f

rom

ind

ivid

ua

l an

aly

te d

ete

ctio

ns

at

or

ab

ove

th

e le

vel o

f re

po

rtin

g

ø =

AL

S is

no

t N

AT

A a

ccre

dite

d f

or

the

se t

est

s.

~ =

In

dic

ate

s a

n e

stim

ate

d v

alu

e.

Ke

y :

Page 70: Cover - Attach C14h

3 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

21_200212

MW

11S

_200212

MW

17_200212

MW

16_200212

MW

105_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-005

ES

20051

13-0

04

ES

2005

113

-003

ES

2005113-0

02

ES

2005113-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

0.0

03

Ars

en

ic<

0.0

01

<0

.00

10.0

18

<0

.00

1m

g/L

0.0

01

74

40

-38

-2

0.0

007

Cad

miu

m0.0

026

0.0

006

<0

.00

01

<0

.00

01

mg

/L0

.00

01

74

40

-43

-9

<0

.00

1C

hro

miu

m0.0

02

<0

.00

1<

0.0

01

0.0

10

mg

/L0

.00

17

44

0-4

7-3

<0

.00

1C

op

per

0.2

31

0.0

32

<0

.00

1<

0.0

01

mg

/L0

.00

17

44

0-5

0-8

0.0

29

Nic

kel

0.0

45

0.0

39

0.0

23

0.0

02

mg

/L0

.00

17

44

0-0

2-0

0.0

03

Lead

0.0

08

0.0

01

0.0

04

<0

.00

1m

g/L

0.0

01

74

39

-92

-1

1.7

6Z

inc

2.5

61

.28

0.4

55

0.0

59

mg

/L0

.00

57

44

0-6

6-6

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

<0

.00

01

Merc

ury

<0

.00

01

<0

.00

01

<0

.00

01

<0

.00

01

mg

/L0

.00

01

74

39

-97

-6

EP

074D

: F

um

igan

ts

<5

2.2

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

55

94

-20

-7

<5

1.2

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

57

8-8

7-5

<5

cis

-1.3

-Dic

hlo

rop

rop

yle

ne

<5

<5

<5

<5

µg

/L5

10

06

1-0

1-5

<5

tran

s-1

.3-D

ich

loro

pro

pyle

ne

<5

<5

<5

<5

µg

/L5

10

06

1-0

2-6

<5

1.2

-Dib

rom

oeth

an

e (

ED

B)

<5

<5

<5

<5

µg

/L5

10

6-9

3-4

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<1

Vin

yl ch

lori

de

<1

<1

<1

<1

µg

/L1

75

-01

-4

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<5

0D

ich

loro

dif

luo

rom

eth

an

e<

50

<5

0<

50

<5

g/L

50

75

-71

-8

<5

0C

hlo

rom

eth

an

e<

50

<5

0<

50

<5

g/L

50

74

-87

-3

<5

0V

inyl ch

lori

de

<5

0<

50

<5

0<

50

µg

/L5

07

5-0

1-4

<5

0B

rom

om

eth

an

e<

50

<5

0<

50

<5

g/L

50

74

-83

-9

<5

0C

hlo

roeth

an

e<

50

<5

0<

50

<5

g/L

50

75

-00

-3

<5

0T

rich

loro

flu

oro

meth

an

e<

50

<5

0<

50

<5

g/L

50

75

-69

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<5

1.1

-Dic

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roeth

en

e<

5<

5<

5<

g/L

57

5-3

5-4

<5

Iod

om

eth

an

e<

5<

5<

5<

g/L

57

4-8

8-4

<5

tran

s-1

.2-D

ich

loro

eth

en

e<

5<

5<

5<

g/L

51

56

-60

-5

<5

1.1

-Dic

hlo

roeth

an

e<

5<

5<

5<

g/L

57

5-3

4-3

<5

cis

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-Dic

hlo

roeth

en

e<

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5<

g/L

51

56

-59

-2

<5

1.1

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rich

loro

eth

an

e<

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g/L

57

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rop

rop

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ne

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µg

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56

3-5

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on

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ach

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de

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<5

<5

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µg

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56

-23

-5

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roeth

an

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51

07

-06

-2

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Tri

ch

loro

eth

en

e<

5<

5<

5<

g/L

57

9-0

1-6

Page 71: Cover - Attach C14h

4 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

21_200212

MW

11S

_200212

MW

17_200212

MW

16_200212

MW

105_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-005

ES

20051

13-0

04

ES

2005

113

-003

ES

2005113-0

02

ES

2005113-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

- C

on

tin

ued

<5

Dib

rom

om

eth

an

e<

5<

5<

5<

g/L

57

4-9

5-3

<5

1.1

.2-T

rich

loro

eth

an

e<

5<

5<

5<

g/L

57

9-0

0-5

<5

1.3

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

51

42

-28

-9

<5

Tetr

ach

loro

eth

en

e<

5<

5<

5<

g/L

51

27

-18

-4

<5

1.1

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ach

loro

eth

an

e<

5<

5<

5<

g/L

56

30

-20

-6

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tran

s-1

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ich

loro

-2-b

ute

ne

<5

<5

<5

<5

µg

/L5

11

0-5

7-6

<5

cis

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-Dic

hlo

ro-2

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ten

e<

5<

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5<

g/L

51

47

6-1

1-5

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ach

loro

eth

an

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57

9-3

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59

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an

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57

6-0

1-7

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rom

o-3

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pro

pa

ne

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µg

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96

-12

-8

<5

Hexach

loro

bu

tad

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g/L

58

7-6

8-3

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds

<5

Ch

loro

ben

zen

e<

5<

5<

5<

g/L

51

08

-90

-7

<5

Bro

mo

ben

zen

e<

5<

5<

5<

g/L

51

08

-86

-1

<5

2-C

hlo

roto

luen

e<

5<

5<

5<

g/L

59

5-4

9-8

<5

4-C

hlo

roto

luen

e<

5<

5<

5<

g/L

51

06

-43

-4

<5

1.3

-Dic

hlo

rob

en

zen

e<

5<

5<

5<

g/L

55

41

-73

-1

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1.4

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hlo

rob

en

zen

e<

5<

5<

5<

g/L

51

06

-46

-7

<5

1.2

-Dic

hlo

rob

en

zen

e<

5<

5<

5<

g/L

59

5-5

0-1

<5

1.2

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rich

loro

ben

zen

e<

5<

5<

5<

g/L

51

20

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-1

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1.2

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rich

loro

ben

zen

e<

5<

5<

5<

g/L

58

7-6

1-6

EP

074G

: T

rih

alo

meth

an

es

<5

Ch

loro

form

<5

<5

<5

<5

µg

/L5

67

-66

-3

<5

Bro

mo

dic

hlo

rom

eth

an

e<

5<

5<

5<

g/L

57

5-2

7-4

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rom

och

loro

meth

an

e<

5<

5<

5<

g/L

51

24

-48

-1

<5

Bro

mo

form

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<5

<5

<5

µg

/L5

75

-25

-2

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<2

0<

20

<2

0<

20

<2

g/L

20

----

C6 -

C9 F

racti

on

<5

0<

50

<5

0<

50

<5

g/L

50

----

C10 -

C14 F

racti

on

<1

00

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

C15 -

C28 F

racti

on

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0<

50

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0<

50

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g/L

50

----

C29 -

C36 F

racti

on

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0<

50

<5

0<

50

µg

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0--

--C

10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

Page 72: Cover - Attach C14h

5 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

21_200212

MW

11S

_200212

MW

17_200212

MW

16_200212

MW

105_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

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eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-005

ES

20051

13-0

04

ES

2005

113

-003

ES

2005113-0

02

ES

2005113-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s -

Co

nti

nu

ed

<2

0C

6 -

C10 F

racti

on

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0

<2

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0-B

TE

X

<1

00

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

>C

10 -

C16 F

racti

on

<1

00

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

>C

16 -

C34 F

racti

on

<1

00

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

>C

34 -

C40 F

racti

on

<1

00

^ <

10

0<

10

0<

10

0<

10

g/L

10

0--

-->

C10 -

C40 F

racti

on

(su

m)

<1

00

^ <

10

0<

10

0<

10

0<

10

g/L

10

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<1

Ben

zen

e<

1<

1<

1<

g/L

17

1-4

3-2

<2

To

luen

e<

2<

2<

2<

g/L

21

08

-88

-3

<2

Eth

ylb

en

zen

e<

2<

2<

2<

g/L

21

00

-41

-4

<2

meta

- &

para

-Xyle

ne

<2

<2

<2

<2

µg

/L2

10

8-3

8-3

10

6-4

2-3

<2

ort

ho

-Xyle

ne

<2

<2

<2

<2

µg

/L2

95

-47

-6

<2

^ <

2<

2<

2<

g/L

2--

--T

ota

l X

yle

nes

<1

^ <

1<

1<

1<

g/L

1--

--S

um

of

BT

EX

<5

Nap

hth

ale

ne

<5

<5

<5

<5

µg

/L5

91

-20

-3

EP

074S

(SIM

) :

VO

C S

urr

og

ate

s

104

1.2

-Dic

hlo

roeth

an

e-D

499.8

105

11

4111

%5

01

70

60

-07

-0

EP

074S

: V

OC

Su

rro

gate

s

97.1

1.2

-Dic

hlo

roeth

an

e-D

493.9

87.9

96

.18

8.8

%5

17

06

0-0

7-0

113

To

luen

e-D

8104

102

11

59

9.1

%5

20

37

-26

-5

102

4-B

rom

ofl

uo

rob

en

zen

e94.8

93.9

10

09

0.4

%5

46

0-0

0-4

EP

080S

: T

PH

(V)/

BT

EX

Su

rro

gate

s

114

1.2

-Dic

hlo

roeth

an

e-D

4111

104

11

3104

%2

17

06

0-0

7-0

114

To

luen

e-D

8104

104

11

5100

%2

20

37

-26

-5

110

4-B

rom

ofl

uo

rob

en

zen

e105

105

11

0102

%2

46

0-0

0-4

Page 73: Cover - Attach C14h

6 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

QC

305_200212

QC

304_200212

MW

102_200212

MW

01_200212

MW

19_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-010

ES

20051

13-0

09

ES

2005

113

-008

ES

2005113-0

07

ES

2005113-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

0.1

39

Ars

en

ic0.0

02

0.0

02

----

----

mg

/L0

.00

17

44

0-3

8-2

0.0

042

Cad

miu

m<

0.0

00

1<

0.0

00

1--

----

--m

g/L

0.0

00

17

44

0-4

3-9

0.0

04

Ch

rom

ium

<0

.00

1<

0.0

01

----

----

mg

/L0

.00

17

44

0-4

7-3

0.2

47

Co

pp

er

<0

.00

1<

0.0

01

----

----

mg

/L0

.00

17

44

0-5

0-8

0.2

94

Nic

kel

0.0

02

0.0

02

----

----

mg

/L0

.00

17

44

0-0

2-0

0.0

05

Lead

<0

.00

1<

0.0

01

----

----

mg

/L0

.00

17

43

9-9

2-1

3.3

6Z

inc

0.0

87

0.0

06

----

----

mg

/L0

.00

57

44

0-6

6-6

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

<0

.00

01

Merc

ury

<0

.00

01

<0

.00

01

----

----

mg

/L0

.00

01

74

39

-97

-6

EP

074D

: F

um

igan

ts

<5

2.2

-Dic

hlo

rop

rop

an

e<

5<

5--

----

--µ

g/L

55

94

-20

-7

<5

1.2

-Dic

hlo

rop

rop

an

e<

5<

5--

----

--µ

g/L

57

8-8

7-5

<5

cis

-1.3

-Dic

hlo

rop

rop

yle

ne

<5

<5

----

----

µg

/L5

10

06

1-0

1-5

<5

tran

s-1

.3-D

ich

loro

pro

pyle

ne

<5

<5

----

----

µg

/L5

10

06

1-0

2-6

<5

1.2

-Dib

rom

oeth

an

e (

ED

B)

<5

<5

----

----

µg

/L5

10

6-9

3-4

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<1

Vin

yl ch

lori

de

<1

<1

----

----

µg

/L1

75

-01

-4

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<5

0D

ich

loro

dif

luo

rom

eth

an

e<

50

<5

0--

----

--µ

g/L

50

75

-71

-8

<5

0C

hlo

rom

eth

an

e<

50

<5

0--

----

--µ

g/L

50

74

-87

-3

<5

0V

inyl ch

lori

de

<5

0<

50

----

----

µg

/L5

07

5-0

1-4

<5

0B

rom

om

eth

an

e<

50

<5

0--

----

--µ

g/L

50

74

-83

-9

<5

0C

hlo

roeth

an

e<

50

<5

0--

----

--µ

g/L

50

75

-00

-3

<5

0T

rich

loro

flu

oro

meth

an

e<

50

<5

0--

----

--µ

g/L

50

75

-69

-4

<5

1.1

-Dic

hlo

roeth

en

e<

5<

5--

----

--µ

g/L

57

5-3

5-4

<5

Iod

om

eth

an

e<

5<

5--

----

--µ

g/L

57

4-8

8-4

<5

tran

s-1

.2-D

ich

loro

eth

en

e<

5<

5--

----

--µ

g/L

51

56

-60

-5

<5

1.1

-Dic

hlo

roeth

an

e<

5<

5--

----

--µ

g/L

57

5-3

4-3

<5

cis

-1.2

-Dic

hlo

roeth

en

e<

5<

5--

----

--µ

g/L

51

56

-59

-2

<5

1.1

.1-T

rich

loro

eth

an

e<

5<

5--

----

--µ

g/L

57

1-5

5-6

<5

1.1

-Dic

hlo

rop

rop

yle

ne

<5

<5

----

----

µg

/L5

56

3-5

8-6

<5

Carb

on

Tetr

ach

lori

de

<5

<5

----

----

µg

/L5

56

-23

-5

<5

1.2

-Dic

hlo

roeth

an

e<

5<

5--

----

--µ

g/L

51

07

-06

-2

<5

Tri

ch

loro

eth

en

e<

5<

5--

----

--µ

g/L

57

9-0

1-6

Page 74: Cover - Attach C14h

7 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

QC

305_200212

QC

304_200212

MW

102_200212

MW

01_200212

MW

19_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-010

ES

20051

13-0

09

ES

2005

113

-008

ES

2005113-0

07

ES

2005113-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

- C

on

tin

ued

<5

Dib

rom

om

eth

an

e<

5<

5--

----

--µ

g/L

57

4-9

5-3

<5

1.1

.2-T

rich

loro

eth

an

e<

5<

5--

----

--µ

g/L

57

9-0

0-5

<5

1.3

-Dic

hlo

rop

rop

an

e<

5<

5--

----

--µ

g/L

51

42

-28

-9

<5

Tetr

ach

loro

eth

en

e<

5<

5--

----

--µ

g/L

51

27

-18

-4

<5

1.1

.1.2

-Tetr

ach

loro

eth

an

e<

5<

5--

----

--µ

g/L

56

30

-20

-6

<5

tran

s-1

.4-D

ich

loro

-2-b

ute

ne

<5

<5

----

----

µg

/L5

11

0-5

7-6

<5

cis

-1.4

-Dic

hlo

ro-2

-bu

ten

e<

5<

5--

----

--µ

g/L

51

47

6-1

1-5

<5

1.1

.2.2

-Tetr

ach

loro

eth

an

e<

5<

5--

----

--µ

g/L

57

9-3

4-5

<5

1.2

.3-T

rich

loro

pro

pan

e<

5<

5--

----

--µ

g/L

59

6-1

8-4

<5

Pen

tach

loro

eth

an

e<

5<

5--

----

--µ

g/L

57

6-0

1-7

<5

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

<5

<5

----

----

µg

/L5

96

-12

-8

<5

Hexach

loro

bu

tad

ien

e<

5<

5--

----

--µ

g/L

58

7-6

8-3

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds

<5

Ch

loro

ben

zen

e<

5<

5--

----

--µ

g/L

51

08

-90

-7

<5

Bro

mo

ben

zen

e<

5<

5--

----

--µ

g/L

51

08

-86

-1

<5

2-C

hlo

roto

luen

e<

5<

5--

----

--µ

g/L

59

5-4

9-8

<5

4-C

hlo

roto

luen

e<

5<

5--

----

--µ

g/L

51

06

-43

-4

<5

1.3

-Dic

hlo

rob

en

zen

e<

5<

5--

----

--µ

g/L

55

41

-73

-1

<5

1.4

-Dic

hlo

rob

en

zen

e<

5<

5--

----

--µ

g/L

51

06

-46

-7

<5

1.2

-Dic

hlo

rob

en

zen

e<

5<

5--

----

--µ

g/L

59

5-5

0-1

<5

1.2

.4-T

rich

loro

ben

zen

e<

5<

5--

----

--µ

g/L

51

20

-82

-1

<5

1.2

.3-T

rich

loro

ben

zen

e<

5<

5--

----

--µ

g/L

58

7-6

1-6

EP

074G

: T

rih

alo

meth

an

es

<5

Ch

loro

form

<5

<5

----

----

µg

/L5

67

-66

-3

<5

Bro

mo

dic

hlo

rom

eth

an

e<

5<

5--

----

--µ

g/L

57

5-2

7-4

<5

Dib

rom

och

loro

meth

an

e<

5<

5--

----

--µ

g/L

51

24

-48

-1

<5

Bro

mo

form

<5

<5

----

----

µg

/L5

75

-25

-2

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<2

0<

20

<2

0<

20

<2

g/L

20

----

C6 -

C9 F

racti

on

<5

0<

50

<5

0--

----

--µ

g/L

50

----

C10 -

C14 F

racti

on

<1

00

<1

00

<1

00

----

----

µg

/L1

00

----

C15 -

C28 F

racti

on

<5

0<

50

<5

0--

----

--µ

g/L

50

----

C29 -

C36 F

racti

on

<5

0^

<5

0<

50

----

----

µg

/L5

0--

--C

10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

Page 75: Cover - Attach C14h

8 o

f 9

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

QC

305_200212

QC

304_200212

MW

102_200212

MW

01_200212

MW

19_200212

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

01

2-F

eb

-20

20

00

:00

12

-Fe

b-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2005

113

-010

ES

20051

13-0

09

ES

2005

113

-008

ES

2005113-0

07

ES

2005113-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s -

Co

nti

nu

ed

<2

0C

6 -

C10 F

racti

on

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0

<2

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0-B

TE

X

<1

00

<1

00

<1

00

----

----

µg

/L1

00

----

>C

10 -

C16 F

racti

on

<1

00

<1

00

<1

00

----

----

µg

/L1

00

----

>C

16 -

C34 F

racti

on

<1

00

<1

00

<1

00

----

----

µg

/L1

00

----

>C

34 -

C40 F

racti

on

<1

00

^ <

10

0<

10

0--

----

--µ

g/L

10

0--

-->

C10 -

C40 F

racti

on

(su

m)

<1

00

^ <

10

0<

10

0--

----

--µ

g/L

10

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<1

Ben

zen

e<

1<

1<

1<

g/L

17

1-4

3-2

<2

To

luen

e<

2<

2<

2<

g/L

21

08

-88

-3

<2

Eth

ylb

en

zen

e<

2<

2<

2<

g/L

21

00

-41

-4

<2

meta

- &

para

-Xyle

ne

<2

<2

<2

<2

µg

/L2

10

8-3

8-3

10

6-4

2-3

<2

ort

ho

-Xyle

ne

<2

<2

<2

<2

µg

/L2

95

-47

-6

<2

^ <

2<

2<

2<

g/L

2--

--T

ota

l X

yle

nes

<1

^ <

1<

1<

1<

g/L

1--

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Page 76: Cover - Attach C14h

9 o

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Page 77: Cover - Attach C14h

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Tru

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QU

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10

:

This

report

supers

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any

pre

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report

(s)

with

this

refe

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. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. T

his

docu

ment sh

all

not be r

epro

duce

d, exc

ept in

full.

This

Qualit

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ontr

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eport

conta

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the follo

win

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form

atio

n:

l

La

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lica

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DU

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Re

lativ

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RP

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nd

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ep

tan

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imits

Sig

nato

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This

docu

ment has

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lect

ronic

ally

sig

ned b

y th

e a

uth

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21 C

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Page 78: Cover - Attach C14h

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en

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re r

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a r

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less

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an

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n t

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mp

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em

plo

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r m

atr

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terf

ere

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am

ple

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r =

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term

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a

ran

do

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lect

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tra

lab

ora

tory

sp

lit.

La

bo

rato

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pro

vid

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ga

rdin

g

me

tho

d

pre

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on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

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en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

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an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

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of

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pa

riso

n

to

the

le

vel

of

rep

ort

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: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

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n 1

0 a

nd

20

tim

es

LO

R:

0%

- 5

0%

; R

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tim

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LO

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0%

- 2

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.

Su

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Du

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Co

mp

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um

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nit

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very

Lim

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%)

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lved

Meta

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02

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dm

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74

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40

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it

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02

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pp

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74

40

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imit

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02

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Zin

c7

44

0-6

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0.0

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No

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02

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Ca

dm

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74

40

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02

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Ch

rom

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74

40

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imit

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02

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pp

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74

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10

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10

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it

EG

02

0A

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Le

ad

74

39

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1m

g/L

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1<

0.0

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imit

EG

02

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Nic

kel

74

40

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imit

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02

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02

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00

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05

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02

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02

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rom

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0.0

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02

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Co

pp

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74

40

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20

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Page 79: Cover - Attach C14h

3 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

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06

-93

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

2.2

-Dic

hlo

rop

rop

an

e5

94

-20

-75

µg

/L<

5<

50

.00

No

Lim

itM

W0

1_

20

02

12

E

S2

00

51

13

-00

7

EP

07

4:

1.2

-Dic

hlo

rop

rop

an

e7

8-8

7-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

cis-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

1-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

2-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

-Dib

rom

oe

tha

ne

(E

DB

)1

06

-93

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

2861277)

EP

07

4E

(SIM

): V

inyl

ch

lorid

e7

5-0

1-4

g/L

<1

<1

0.0

0N

o L

imit

MW

10

5_

20

02

12

E

S2

00

51

13

-00

1

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

2861276)

EP

07

4:

1.1

-Dic

hlo

roe

the

ne

75

-35

-45

µg

/L<

5<

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

48

75

-00

1

EP

07

4:

Iod

om

eth

an

e7

4-8

8-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.2

-Dic

hlo

roe

the

ne

15

6-6

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

-Dic

hlo

roe

tha

ne

75

-34

-35

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

cis-

1.2

-Dic

hlo

roe

the

ne

15

6-5

9-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.1-T

rich

loro

eth

an

e7

1-5

5-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

-Dic

hlo

rop

rop

yle

ne

56

3-5

8-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Ca

rbo

n T

etr

ach

lorid

e5

6-2

3-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

-Dic

hlo

roe

tha

ne

10

7-0

6-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Trich

loro

eth

en

e7

9-0

1-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dib

rom

om

eth

an

e7

4-9

5-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2-T

rich

loro

eth

an

e7

9-0

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rop

rop

an

e1

42

-28

-95

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Te

tra

chlo

roe

the

ne

12

7-1

8-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.1.2

-Te

tra

ch

loro

eth

an

e6

30

-20

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

tra

ns-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

10

-57

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

cis-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

47

6-1

1-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2.2

-Te

tra

ch

loro

eth

an

e7

9-3

4-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.3-T

rich

loro

pro

pa

ne

96

-18

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Pe

nta

chlo

roe

tha

ne

76

-01

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

96

-12

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

He

xach

loro

bu

tad

ien

e8

7-6

8-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dic

hlo

rod

iflu

oro

me

tha

ne

75

-71

-85

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Ch

loro

me

tha

ne

74

-87

-35

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Vin

yl c

hlo

rid

e7

5-0

1-4

50

µg

/L<

50

<5

00

.00

No

Lim

it

Page 80: Cover - Attach C14h

4 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

2861276)

- c

on

tin

ued

EP

07

4:

Bro

mo

me

tha

ne

74

-83

-95

g/L

<5

0<

50

0.0

0N

o L

imit

An

on

ymo

us

ES

20

04

87

5-0

01

EP

07

4:

Ch

loro

eth

an

e7

5-0

0-3

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

4:

Trich

loro

fluo

rom

eth

an

e7

5-6

9-4

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

4:

1.1

-Dic

hlo

roe

the

ne

75

-35

-45

µg

/L<

5<

50

.00

No

Lim

itM

W0

1_

20

02

12

E

S2

00

51

13

-00

7

EP

07

4:

Iod

om

eth

an

e7

4-8

8-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.2

-Dic

hlo

roe

the

ne

15

6-6

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

-Dic

hlo

roe

tha

ne

75

-34

-35

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

cis-

1.2

-Dic

hlo

roe

the

ne

15

6-5

9-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.1-T

rich

loro

eth

an

e7

1-5

5-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

-Dic

hlo

rop

rop

yle

ne

56

3-5

8-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Ca

rbo

n T

etr

ach

lorid

e5

6-2

3-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

-Dic

hlo

roe

tha

ne

10

7-0

6-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Trich

loro

eth

en

e7

9-0

1-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dib

rom

om

eth

an

e7

4-9

5-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2-T

rich

loro

eth

an

e7

9-0

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rop

rop

an

e1

42

-28

-95

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Te

tra

chlo

roe

the

ne

12

7-1

8-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.1.2

-Te

tra

ch

loro

eth

an

e6

30

-20

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

tra

ns-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

10

-57

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

cis-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

47

6-1

1-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2.2

-Te

tra

ch

loro

eth

an

e7

9-3

4-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.3-T

rich

loro

pro

pa

ne

96

-18

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Pe

nta

chlo

roe

tha

ne

76

-01

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

96

-12

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

He

xach

loro

bu

tad

ien

e8

7-6

8-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dic

hlo

rod

iflu

oro

me

tha

ne

75

-71

-85

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Ch

loro

me

tha

ne

74

-87

-35

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Vin

yl c

hlo

rid

e7

5-0

1-4

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

4:

Bro

mo

me

tha

ne

74

-83

-95

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Ch

loro

eth

an

e7

5-0

0-3

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

4:

Trich

loro

fluo

rom

eth

an

e7

5-6

9-4

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds (Q

C L

ot:

2861276)

EP

07

4:

Ch

loro

be

nze

ne

10

8-9

0-7

g/L

<5

<5

0.0

0N

o L

imit

An

on

ymo

us

ES

20

04

87

5-0

01

EP

07

4:

Bro

mo

be

nze

ne

10

8-8

6-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

2-C

hlo

roto

lue

ne

95

-49

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

4-C

hlo

roto

lue

ne

10

6-4

3-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rob

en

zen

e5

41

-73

-15

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.4

-Dic

hlo

rob

en

zen

e1

06

-46

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dic

hlo

rob

en

zen

e9

5-5

0-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.4-T

rich

loro

be

nze

ne

12

0-8

2-1

g/L

<5

<5

0.0

0N

o L

imit

Page 81: Cover - Attach C14h

5 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds (Q

C L

ot:

2861276)

- c

on

tin

ued

EP

07

4:

1.2

.3-T

rich

loro

be

nze

ne

87

-61

-65

µg

/L<

5<

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

48

75

-00

1

EP

07

4:

Ch

loro

be

nze

ne

10

8-9

0-7

g/L

<5

<5

0.0

0N

o L

imit

MW

01

_2

00

21

2

ES

20

05

11

3-0

07

EP

07

4:

Bro

mo

be

nze

ne

10

8-8

6-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

2-C

hlo

roto

lue

ne

95

-49

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

4-C

hlo

roto

lue

ne

10

6-4

3-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rob

en

zen

e5

41

-73

-15

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.4

-Dic

hlo

rob

en

zen

e1

06

-46

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dic

hlo

rob

en

zen

e9

5-5

0-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.4-T

rich

loro

be

nze

ne

12

0-8

2-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.3-T

rich

loro

be

nze

ne

87

-61

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

074G

: T

rih

alo

meth

an

es (Q

C L

ot:

2861276)

EP

07

4:

Ch

loro

form

67

-66

-35

µg

/L<

5<

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

48

75

-00

1

EP

07

4:

Bro

mo

dic

hlo

rom

eth

an

e7

5-2

7-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dib

rom

och

loro

me

tha

ne

12

4-4

8-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Bro

mo

form

75

-25

-25

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Ch

loro

form

67

-66

-35

µg

/L<

5<

50

.00

No

Lim

itM

W0

1_

20

02

12

E

S2

00

51

13

-00

7

EP

07

4:

Bro

mo

dic

hlo

rom

eth

an

e7

5-2

7-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dib

rom

och

loro

me

tha

ne

12

4-4

8-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Bro

mo

form

75

-25

-25

µg

/L<

5<

50

.00

No

Lim

it

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2860528)

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

g/L

<1

00

<1

00

0.0

0N

o L

imit

MW

21

_2

00

21

2

ES

20

05

11

3-0

05

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2861275)

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

48

75

-00

1

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itM

W0

1_

20

02

12

E

S2

00

51

13

-00

7

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2860528)

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

--1

00

µg

/L<

10

0<

10

00

.00

No

Lim

itM

W2

1_

20

02

12

E

S2

00

51

13

-00

5

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

µg

/L<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

µg

/L<

10

0<

10

00

.00

No

Lim

it

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2861275)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

An

on

ymo

us

ES

20

04

87

5-0

01

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

MW

01

_2

00

21

2

ES

20

05

11

3-0

07

EP

080:

BT

EX

N (Q

C L

ot:

2861275)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

48

75

-00

1

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

Page 82: Cover - Attach C14h

6 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

080:

BT

EX

N (Q

C L

ot:

2861275)

- c

on

tin

ued

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

An

on

ymo

us

ES

20

04

87

5-0

01

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itM

W0

1_

20

02

12

E

S2

00

51

13

-00

7

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

Page 83: Cover - Attach C14h

7 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

pik

e

(LC

S)

refe

rs

to

a

cert

ifie

d

refe

ren

ce

ma

teria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S (Q

CL

ot:

2864122)

EG

02

0A

-F:

Ars

en

ic7

44

0-3

8-2

0.0

01

mg

/L<

0.0

01

10

00

.1 m

g/L

11

48

5.0

EG

02

0A

-F:

Ca

dm

ium

74

40

-43

-90

.00

01

mg

/L<

0.0

00

19

4.4

0.1

mg

/L1

10

84

.0

EG

02

0A

-F:

Ch

rom

ium

74

40

-47

-30

.00

1m

g/L

<0

.00

19

5.1

0.1

mg

/L1

11

85

.0

EG

02

0A

-F:

Co

pp

er

74

40

-50

-80

.00

1m

g/L

<0

.00

19

3.7

0.1

mg

/L1

11

81

.0

EG

02

0A

-F:

Le

ad

74

39

-92

-10

.00

1m

g/L

<0

.00

19

3.8

0.1

mg

/L1

11

83

.0

EG

02

0A

-F:

Nic

kel

74

40

-02

-00

.00

1m

g/L

<0

.00

19

4.3

0.1

mg

/L1

12

82

.0

EG

02

0A

-F:

Zin

c7

44

0-6

6-6

0.0

05

mg

/L<

0.0

05

89

.50

.1 m

g/L

11

78

1.0

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S (Q

CL

ot:

2864126)

EG

02

0A

-F:

Ars

en

ic7

44

0-3

8-2

0.0

01

mg

/L<

0.0

01

10

00

.1 m

g/L

11

48

5.0

EG

02

0A

-F:

Ca

dm

ium

74

40

-43

-90

.00

01

mg

/L<

0.0

00

19

5.9

0.1

mg

/L1

10

84

.0

EG

02

0A

-F:

Ch

rom

ium

74

40

-47

-30

.00

1m

g/L

<0

.00

19

5.6

0.1

mg

/L1

11

85

.0

EG

02

0A

-F:

Co

pp

er

74

40

-50

-80

.00

1m

g/L

<0

.00

19

3.3

0.1

mg

/L1

11

81

.0

EG

02

0A

-F:

Le

ad

74

39

-92

-10

.00

1m

g/L

<0

.00

19

3.1

0.1

mg

/L1

11

83

.0

EG

02

0A

-F:

Nic

kel

74

40

-02

-00

.00

1m

g/L

<0

.00

19

6.2

0.1

mg

/L1

12

82

.0

EG

02

0A

-F:

Zin

c7

44

0-6

6-6

0.0

05

mg

/L<

0.0

05

10

70

.1 m

g/L

11

78

1.0

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

(Q

CL

ot:

2864123)

EG

03

5F

: M

erc

ury

74

39

-97

-60

.00

01

mg

/L<

0.0

00

11

03

0.0

1 m

g/L

10

58

3.0

EP

074D

: F

um

igan

ts (Q

CL

ot:

2861276)

EP

07

4:

2.2

-Dic

hlo

rop

rop

an

e5

94

-20

-75

µg

/L<

51

01

10

µg

/L1

22

68

.0

EP

07

4:

1.2

-Dic

hlo

rop

rop

an

e7

8-8

7-5

g/L

<5

98

.91

0 µ

g/L

11

87

6.0

EP

07

4:

cis-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

1-5

g/L

<5

97

.31

0 µ

g/L

12

06

2.0

EP

07

4:

tra

ns-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

2-6

g/L

<5

94

.31

0 µ

g/L

11

46

0.0

EP

07

4:

1.2

-Dib

rom

oe

tha

ne

(E

DB

)1

06

-93

-45

µg

/L<

51

03

10

µg

/L1

17

69

.0

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

2861277)

EP

07

4E

(SIM

): V

inyl

ch

lorid

e7

5-0

1-4

g/L

<1

10

31

0 µ

g/L

12

67

0.0

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

2861276)

EP

07

4:

Dic

hlo

rod

iflu

oro

me

tha

ne

75

-71

-85

g/L

<5

07

1.0

10

0 µ

g/L

13

86

0.6

EP

07

4:

Ch

loro

me

tha

ne

74

-87

-35

g/L

<5

08

1.9

10

0 µ

g/L

13

06

7.4

EP

07

4:

Vin

yl c

hlo

rid

e7

5-0

1-4

50

µg

/L<

50

89

.41

00

µg

/L1

29

69

.4

EP

07

4:

Bro

mo

me

tha

ne

74

-83

-95

g/L

<5

09

3.3

10

0 µ

g/L

14

05

6.0

EP

07

4:

Ch

loro

eth

an

e7

5-0

0-3

50

µg

/L<

50

93

.01

00

µg

/L1

39

61

.0

EP

07

4:

Trich

loro

fluo

rom

eth

an

e7

5-6

9-4

50

µg

/L<

50

91

.31

00

µg

/L1

31

69

.0

EP

07

4:

1.1

-Dic

hlo

roe

the

ne

75

-35

-45

µg

/L<

59

4.0

10

µg

/L1

24

70

.0

EP

07

4:

Iod

om

eth

an

e7

4-8

8-4

g/L

<5

70

.71

0 µ

g/L

12

87

0.2

Page 84: Cover - Attach C14h

8 o

f 10

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

2861276)

- c

on

tin

ued

EP

07

4:

tra

ns-

1.2

-Dic

hlo

roe

the

ne

15

6-6

0-5

g/L

<5

93

.01

0 µ

g/L

11

87

4.0

EP

07

4:

1.1

-Dic

hlo

roe

tha

ne

75

-34

-35

µg

/L<

59

3.8

10

µg

/L1

20

74

.0

EP

07

4:

cis-

1.2

-Dic

hlo

roe

the

ne

15

6-5

9-2

g/L

<5

96

.11

0 µ

g/L

11

97

7.0

EP

07

4:

1.1

.1-T

rich

loro

eth

an

e7

1-5

5-6

g/L

<5

96

.51

0 µ

g/L

11

96

7.0

EP

07

4:

1.1

-Dic

hlo

rop

rop

yle

ne

56

3-5

8-6

g/L

<5

96

.31

0 µ

g/L

11

97

3.0

EP

07

4:

Ca

rbo

n T

etr

ach

lorid

e5

6-2

3-5

g/L

<5

95

.41

0 µ

g/L

12

06

2.0

EP

07

4:

1.2

-Dic

hlo

roe

tha

ne

10

7-0

6-2

g/L

<5

95

.71

0 µ

g/L

12

37

3.0

EP

07

4:

Trich

loro

eth

en

e7

9-0

1-6

g/L

<5

99

.11

0 µ

g/L

11

87

6.0

EP

07

4:

Dib

rom

om

eth

an

e7

4-9

5-3

g/L

<5

97

.81

0 µ

g/L

11

97

3.0

EP

07

4:

1.1

.2-T

rich

loro

eth

an

e7

9-0

0-5

g/L

<5

94

.21

0 µ

g/L

12

67

2.0

EP

07

4:

1.3

-Dic

hlo

rop

rop

an

e1

42

-28

-95

µg

/L<

59

6.5

10

µg

/L1

29

71

.0

EP

07

4:

Te

tra

chlo

roe

the

ne

12

7-1

8-4

g/L

<5

90

.41

0 µ

g/L

12

47

2.0

EP

07

4:

1.1

.1.2

-Te

tra

chlo

roe

tha

ne

63

0-2

0-6

g/L

<5

97

.71

0 µ

g/L

11

46

6.0

EP

07

4:

tra

ns-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

10

-57

-65

µg

/L<

58

5.8

10

µg

/L1

20

60

.0

EP

07

4:

cis-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

47

6-1

1-5

g/L

<5

99

.71

0 µ

g/L

12

87

0.6

EP

07

4:

1.1

.2.2

-Te

tra

chlo

roe

tha

ne

79

-34

-55

µg

/L<

59

7.3

10

µg

/L1

24

70

.0

EP

07

4:

1.2

.3-T

rich

loro

pro

pa

ne

96

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2861276)

EP

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EP

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Page 85: Cover - Attach C14h

9 o

f 10

:P

ag

e

Wo

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Clie

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20

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Be

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Page 86: Cover - Attach C14h

10

of 10

:P

ag

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Wo

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rde

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Clie

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20

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Page 87: Cover - Attach C14h

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Envir

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rep

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ing

hig

hlig

hts

an

y n

on

-co

nfo

rman

ces, fa

cilit

ate

s f

aste

r an

d m

ore

accu

rate

data

valid

ati

on

an

d is d

esig

ned

to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

Co

ntr

ol (

QC

) R

ep

ort

.

l

NO

Meth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

NO

Du

plicate

ou

tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

NO

Matr

ix S

pik

e o

utl

iers

occu

r.

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, N

O su

rro

gate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

l

NO

An

aly

sis

Ho

ldin

g T

ime O

utl

iers

exis

t.

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

uality

Co

ntr

ol S

am

ple

s

l

NO

Qu

ality

Co

ntr

ol S

am

ple

Fre

qu

en

cy O

utl

iers

exis

t.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 88: Cover - Attach C14h

2 o

f 6

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

tim

e

is

7 d

ays;

o

the

rs

14

da

ys.

A

re

co

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes

of

inte

rest/

con

cern

.

Ho

ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

Ass

ess

me

nt

com

pa

res

the

le

ach

d

ate

w

ith

th

e

sho

rte

st

an

aly

te

ho

ldin

g

time

fo

r th

e

eq

uiv

ale

nt

so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

A r

eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

If s

am

ple

s a

re id

en

tifie

d b

elo

w a

s h

avi

ng

be

en

an

aly

sed

or

ext

ract

ed

ou

tsid

e o

f re

com

me

nd

ed

ho

ldin

g t

ime

s,

this

sh

ou

ld b

e t

ake

n in

to c

on

sid

era

tion

wh

en

inte

rpre

ting

re

sults

.

Th

is

rep

ort

su

mm

arize

s e

xtra

ctio

n

/ p

rep

ara

tion

a

nd

a

na

lysi

s tim

es

an

d

com

pa

res

ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

nci

ng

U

SE

PA

S

W

84

6,

AP

HA

, A

S

an

d

NE

PM

) b

ase

d

on

th

e

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

rese

nt

first

da

te o

f e

xtra

ctio

n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A lis

ting

of

bre

ach

es

(if

an

y)

is p

rovi

de

d h

ere

in.

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

G020A

-F)

MW

10

2_

20

02

12

10

-Au

g-2

02

0--

--17

-Feb

-202

0--

--12-F

eb

-2020

----

üC

lear

Pla

sti

c B

ott

le -

Nit

ric A

cid

; F

ilte

red

(E

G020A

-F)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2

10

-Au

g-2

02

0--

--17

-Feb

-202

0--

--12-F

eb

-2020

----

ü

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

G035F

)

MW

10

2_

20

02

12

26

-Fe

b-2

02

0--

--18

-Feb

-202

0--

--12-F

eb

-2020

----

üC

lear

Pla

sti

c B

ott

le -

Nit

ric A

cid

; F

ilte

red

(E

G035F

)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2

11

-Ma

r-2

02

0--

--18

-Feb

-202

0--

--12-F

eb

-2020

----

ü

EP

074D

: F

um

igan

ts

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

26

-Fe

b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074E

(SIM

))

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

26

-Fe

b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

Page 89: Cover - Attach C14h

3 o

f 6

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

26

-Fe

b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

26

-Fe

b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

EP

074G

: T

rih

alo

meth

an

es

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

26

-Fe

b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P071)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

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00

21

2,

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01

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21

2,

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10

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02

12

28

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r-2

02

01

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eb

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20

19

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

MW

10

2_

20

02

12

,

QC

30

4_

20

02

12

,Q

C3

05

_2

00

21

2

26

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b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P071)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

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01

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21

2,

MW

10

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20

02

12

28

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r-2

02

01

9-F

eb

-20

20

19

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

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11

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20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

_2

00

21

2,

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10

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20

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,

QC

30

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20

02

12

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05

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21

2

26

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02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

Page 90: Cover - Attach C14h

4 o

f 6

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

080:

BT

EX

N

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

MW

10

5_

20

02

12

,M

W1

6_

20

02

12

,

MW

17

_2

00

21

2,

MW

11

S_

20

02

12

,

MW

21

_2

00

21

2,

MW

19

_2

00

21

2,

MW

01

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00

21

2,

MW

10

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20

02

12

,

QC

30

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20

02

12

,Q

C3

05

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00

21

2

26

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b-2

02

02

6-F

eb

-20

20

17

-Feb

-202

017-F

eb

-20

20

12-F

eb

-2020

üü

Page 91: Cover - Attach C14h

5 o

f 6

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

05

11

3

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.0 B

urr

ow

s IE

:P

roje

ct

Qu

ality

Co

ntr

ol P

ara

mete

r F

req

uen

cy C

om

plian

ce

Th

e f

ollo

win

g r

ep

ort

su

mm

arise

s th

e f

req

ue

ncy

of

lab

ora

tory

QC

sa

mp

les

an

aly

sed

with

in t

he

an

aly

tica

l lo

t(s)

in

wh

ich

th

e s

ub

mitt

ed

sa

mp

le(s

) w

as(

we

re)

pro

cess

ed

. A

ctu

al r

ate

sh

ou

ld b

e g

rea

ter

tha

n o

r e

qu

al t

o

the

exp

ect

ed

ra

te.

A li

stin

g o

f b

rea

che

s is

pro

vid

ed

in t

he

Su

mm

ary

of

Ou

tlie

rs.

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trix

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Page 92: Cover - Attach C14h

6 o

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WA

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Page 93: Cover - Attach C14h

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES2005113

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Brenda Hong

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60623599_1.0 Burrows IE Page 1 of 2

:Order number 60623599_1.0 :Quote number EB2017AECOMAU0014 (EN/004/16)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : ----

Sampler : Kurtis Wathen

DatesDate Samples Received : Issue Date : 18-Feb-202013-Feb-2020 15:30

Scheduled Reporting Date: 20-Feb-2020:Client Requested Due

Date

20-Feb-2020

Delivery DetailsMode of Delivery : :Undefined Not AvailableSecurity Seal

No. of coolers/boxes : :1 Temperature 0.2 - Ice present

: : 10 / 10Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l This is an updated SRN which indicates the addition of 8 metals analysis for sample MW102_200212.

l Dissolved metals analysis for sample MW102_200212 has not been added as both red metals

bottles received were marked as 'unfiltered'. as requested, subsample from orange amber for

filtered metals.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (3 weeks), Solid (2 months ± 1 week) from receipt of samples.

l Please be aware that APHA/NEPM recommends water and soil samples be chilled to less than or equal to 6°C for chemical

analysis, and less than or equal to 10°C but unfrozen for Microbiological analysis. Where samples are received above this

temperature, it should be taken into consideration when interpreting results. Refer to ALS EnviroMail 85 for ALS

recommendations of the best practice for chilling samples after sampling and for maintaining a cool temperature during transit.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 94: Cover - Attach C14h

:Client AECOM Australia Pty Ltd

Work Order : ES2005113 Amendment 02 of 2:Page

18-Feb-2020:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

MethodSample Container Received Preferred Sample Container for AnalysisClient sample ID

Dissolved Mercury by FIMS : EG035F

MW102_200212 - Amber Glass Bottle -

Unpreserved

- Clear Plastic Bottle - Nitric Acid; Filtered

Dissolved Metals by ICP-MS - Suite A : EG020A-F

MW102_200212 - Amber Glass Bottle -

Unpreserved

- Clear Plastic Bottle - Nitric Acid; Filtered

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

WA

TE

R -

EP

074 V

inyl

Chlo

ride S

IM

VO

C S

IM V

inyl

Chlo

ride O

nly

WA

TE

R -

EP

074D

EF

G

VO

C -

Fum

igants

, H

al A

liphatics, H

al A

rom

atics

,

WA

TE

R -

W-0

5

TR

H/B

TE

XN

/8 M

eta

ls

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

ES2005113-001 12-Feb-2020 00:00 MW105_200212 ü ü ü

ES2005113-002 12-Feb-2020 00:00 MW16_200212 ü ü ü

ES2005113-003 12-Feb-2020 00:00 MW17_200212 ü ü ü

ES2005113-004 12-Feb-2020 00:00 MW11S_200212 ü ü ü

ES2005113-005 12-Feb-2020 00:00 MW21_200212 ü ü ü

ES2005113-006 12-Feb-2020 00:00 MW19_200212 ü ü ü

ES2005113-007 12-Feb-2020 00:00 MW01_200212 ü ü ü

ES2005113-008 12-Feb-2020 00:00 MW102_200212 ü ü ü

ES2005113-009 12-Feb-2020 00:00 QC304_200212 ü

ES2005113-010 12-Feb-2020 00:00 QC305_200212 ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

- Chain of Custody (CoC) (COC) Email AP_CustomerService.ANZ@aecom.

com

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- Chromatogram (CHROM) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 AECOM (EQUIS_V5_AECOM) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

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Latham, Alex

From: Grace White <[email protected]>Sent: Monday, 17 February 2020 3:17 PMTo: Wathen, KurtisCc: Latham, Alex; Helen SimpsonSubject: RE: [EXTERNAL] - RE: ALS Workorder ES2005113, Client AECOMAU, Project

60623599_1.0 Burrows IE

Hi Kurtis,

No problem, thanks for sending this! I believe this has now been updated.

Kind regards,

Grace WhiteClient Services Officer, EnvironmentalSydney

T +61 2 8784 8555 D +61 2 8784 8531F +61 2 8784 [email protected] Woodpark RoadSmithfield, NSW, 2164

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From: Wathen, Kurtis [mailto:[email protected]]Sent: Monday, 17 February 2020 2:49 PMTo: Grace White <[email protected]>Cc: Latham, Alex <[email protected]>; Helen Simpson <[email protected]>Subject: [EXTERNAL] - RE: ALS Workorder ES2005113, Client AECOMAU, Project 60623599_1.0 Burrows IE

CAUTION: This email originated from outside of ALS. Do not click links or open attachments unless you recognize the sender

and are sure content is relevant to you.

Hi Grace,

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As discussed over the phone, could we please use the unpreserved sample provided for MW102 and lab filter it fordissolved metals.

Thanks for your help,

Kurtis WathenEnvironmental EngineerD +61 2 8934 0840 M +61 447 224 [email protected]

AECOMLevel 21, 420 George Street, Sydney, NSW 2000PO Box Q410, QVB PO, Sydney, NSW, 1230T +61 2 8934 0000 F +61 2 8934 0001www.aecom.com

Please consider the environment before printing this email..-. -.. -

From: Latham, Alex <[email protected]>Sent: Monday, 17 February 2020 2:34 PMTo: Wathen, Kurtis <[email protected]>Subject: FW: ALS Workorder ES2005113, Client AECOMAU, Project 60623599_1.0 Burrows IE

Mate,Could you please advise.Dissolved metals were one of the main Contams of concern..cheers

Alex LathamAssociate DirectorD +61 2 8934 0451 M +61 400 973 [email protected]

AECOMLevel 21, 420 George Street, Sydney, NSW 2000PO Box Q410, QVB PO, Sydney, NSW, 1230T +61 2 8934 0000 F +61 2 8934 0001www.aecom.com

Please consider the environment before printing this email..-. -.. -

From: Helen Simpson <[email protected]>Sent: Monday, 17 February 2020 2:24 PMTo: Latham, Alex <[email protected]>Subject: ALS Workorder ES2005113, Client AECOMAU, Project 60623599_1.0 Burrows IE

Hi Alex,

For the attached COC, we have received 2 red bottles labelled MW102_200212. Unfortunately, both are marked asunfiltered. Since both filtered and total analysis is required, we think that one of the bottles has been miss-tickedand therefore have not added any metals analysis to this sample.

Please let me know if you need me to do anything.

Kind Regards,

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3

Helen SimpsonSample Admin, EnvironmentalSydney

T +61 2 8784 8555F +61 2 8784 8500

[email protected] Woodpark RoadSmithfield NSW 2164 AUSTRALIA

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