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Attachment C14(f) Proponent Phase I and Phase II Environmental Site Assessment (6/8)

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Page 1: Cover - Attach C14f

Attachment C14(f)

Proponent Phase I and Phase II Environmental Site Assessment (6/8)

Page 2: Cover - Attach C14f

9 o

f 1

1:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

QC

111

BH

02_3.0

-3.1

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

[29

-Au

g-2

01

5]

[29

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529729-0

24

ES

1529729-0

21

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EA

055:

Mo

istu

re C

on

ten

t

41.9

^ 14.6

----

----

----

%1

----

Mo

istu

re C

on

ten

t (d

ried

@ 1

03°C

)

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

----

Asb

esto

s D

ete

cte

d--

----

----

----

--g

/kg

0.1

13

32

-21

-4

----

Asb

esto

s T

yp

e--

----

----

----

----

-1

33

2-2

1-4

----

----

----

----

----

g0

.01

----

Sam

ple

weig

ht

(dry

)

----

----

----

----

----

---

----

AP

PR

OV

ED

ID

EN

TIF

IER

:

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

----

Ars

en

ic60

----

----

----

mg

/kg

57

44

0-3

8-2

----

Cad

miu

m7

----

----

----

mg

/kg

17

44

0-4

3-9

----

Ch

rom

ium

68

----

----

----

mg

/kg

27

44

0-4

7-3

----

Co

pp

er

2240

----

----

----

mg

/kg

57

44

0-5

0-8

----

Lead

2230

----

----

----

mg

/kg

57

43

9-9

2-1

----

Nic

kel

107

----

----

----

mg

/kg

27

44

0-0

2-0

----

Zin

c3460

----

----

----

mg

/kg

57

44

0-6

6-6

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

----

Merc

ury

1.0

----

----

----

mg

/kg

0.1

74

39

-97

-6

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

----

Nap

hth

ale

ne

<0

.5--

----

----

--m

g/k

g0

.59

1-2

0-3

----

Acen

ap

hth

yle

ne

0.8

----

----

----

mg

/kg

0.5

20

8-9

6-8

----

Acen

ap

hth

en

e<

0.5

----

----

----

mg

/kg

0.5

83

-32

-9

----

Flu

ore

ne

<0

.5--

----

----

--m

g/k

g0

.58

6-7

3-7

----

Ph

en

an

thre

ne

7.2

----

----

----

mg

/kg

0.5

85

-01

-8

----

An

thra

cen

e1.8

----

----

----

mg

/kg

0.5

12

0-1

2-7

----

Flu

ora

nth

en

e11.9

----

----

----

mg

/kg

0.5

20

6-4

4-0

----

Pyre

ne

12.1

----

----

----

mg

/kg

0.5

12

9-0

0-0

----

Ben

z(a)a

nth

racen

e5.4

----

----

----

mg

/kg

0.5

56

-55

-3

----

Ch

rysen

e5.2

----

----

----

mg

/kg

0.5

21

8-0

1-9

----

Ben

zo(b

+j)

flu

ora

nth

en

e5.9

----

----

----

mg

/kg

0.5

20

5-9

9-2

20

5-8

2-3

----

Ben

zo(k

)flu

ora

nth

en

e1.9

----

----

----

mg

/kg

0.5

20

7-0

8-9

----

Ben

zo(a

)pyre

ne

5.0

----

----

----

mg

/kg

0.5

50

-32

-8

----

Ind

en

o(1

.2.3

.cd

)pyre

ne

2.3

----

----

----

mg

/kg

0.5

19

3-3

9-5

----

Dib

en

z(a.h

)an

thra

cen

e0.6

----

----

----

mg

/kg

0.5

53

-70

-3

----

Ben

zo(g

.h.i)p

ery

len

e3.2

----

----

----

mg

/kg

0.5

19

1-2

4-2

----

^ 63.3

----

----

----

mg

/kg

0.5

----

Su

m o

f p

oly

cyclic a

rom

ati

c h

yd

rocarb

on

s

Page 3: Cover - Attach C14f

10

of

11

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

QC

111

BH

02_3.0

-3.1

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

[29

-Au

g-2

01

5]

[29

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529729-0

24

ES

1529729-0

21

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s -

Co

nti

nu

ed

----

^ 7.2

----

----

----

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(ze

ro)

----

^ 7.2

----

----

----

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(h

alf

LO

R)

----

^ 7.2

----

----

----

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(L

OR

)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<1

0<

10

----

----

----

mg

/kg

10

----

C6 -

C9 F

racti

on

<5

0<

50

----

----

----

mg

/kg

50

----

C10 -

C14 F

racti

on

220

220

----

----

----

mg

/kg

10

0--

--C

15 -

C28 F

racti

on

240

150

----

----

----

mg

/kg

10

0--

--C

29 -

C36 F

racti

on

460

^ 370

----

----

----

mg

/kg

50

----

C10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

<1

0C

6 -

C10 F

racti

on

<1

0--

----

----

--m

g/k

g1

0C

6_

C1

0

<1

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<1

0--

----

----

--m

g/k

g1

0C

6_

C1

0-B

TE

X

<5

0>

C10 -

C16 F

racti

on

<5

0--

----

----

--m

g/k

g5

0>

C1

0_

C1

6

380

310

----

----

----

mg

/kg

10

0--

-->

C16 -

C34 F

racti

on

160

<1

00

----

----

----

mg

/kg

10

0--

-->

C34 -

C40 F

racti

on

540

^ 310

----

----

----

mg

/kg

50

----

>C

10 -

C40 F

racti

on

(su

m)

<5

0^

<5

0--

----

----

--m

g/k

g5

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<0

.2B

en

zen

e<

0.2

----

----

----

mg

/kg

0.2

71

-43

-2

<0

.5T

olu

en

e<

0.5

----

----

----

mg

/kg

0.5

10

8-8

8-3

<0

.5E

thylb

en

zen

e<

0.5

----

----

----

mg

/kg

0.5

10

0-4

1-4

<0

.5m

eta

- &

para

-Xyle

ne

<0

.5--

----

----

--m

g/k

g0

.51

08

-38

-3 1

06

-42

-3

<0

.5o

rth

o-X

yle

ne

<0

.5--

----

----

--m

g/k

g0

.59

5-4

7-6

<0

.2^

<0

.2--

----

----

--m

g/k

g0

.2--

--S

um

of

BT

EX

<0

.5^

To

tal X

yle

nes

<0

.5--

----

----

--m

g/k

g0

.51

33

0-2

0-7

<1

Nap

hth

ale

ne

<1

----

----

----

mg

/kg

19

1-2

0-3

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

----

Ph

en

ol-

d6

97.5

----

----

----

%0

.51

31

27

-88

-3

----

2-C

hlo

rop

hen

ol-

D4

110

----

----

----

%0

.59

39

51

-73

-6

----

2.4

.6-T

rib

rom

op

hen

ol

97.8

----

----

----

%0

.51

18

-79

-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

----

2-F

luo

rob

iph

en

yl

95.5

----

----

----

%0

.53

21

-60

-8

Page 4: Cover - Attach C14f

11

of

11

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

QC

111

BH

02_3.0

-3.1

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

[29

-Au

g-2

01

5]

[29

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529729-0

24

ES

1529729-0

21

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

075(S

IM)T

: P

AH

Su

rro

gate

s -

Co

nti

nu

ed

----

An

thra

cen

e-d

10

118

----

----

----

%0

.51

71

9-0

6-8

----

4-T

erp

hen

yl-

d14

105

----

----

----

%0

.51

71

8-5

1-0

EP

080S

: T

PH

(V)/

BT

EX

Su

rro

gate

s

97.1

1.2

-Dic

hlo

roeth

an

e-D

4105

----

----

----

%0

.21

70

60

-07

-0

88.4

To

luen

e-D

892.1

----

----

----

%0

.22

03

7-2

6-5

98.1

4-B

rom

ofl

uo

rob

en

zen

e105

----

----

----

%0

.24

60

-00

-4

An

aly

tical R

esu

lts

De

sc

rip

tiv

e R

es

ult

s

Su

b-M

atr

ix:

SO

IL

An

aly

tica

l Re

sults

Me

tho

d:

Co

mp

ou

nd

Clie

nt

sam

ple

ID

-

Clie

nt

sam

plin

g d

ate

/ t

ime

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

EA

20

0:

De

scrip

tion

Pa

le b

row

n c

lay

soil

with

sla

g g

rain

s a

nd

gla

ss d

eb

ris

BH

18

_0

.7-0

.8 -

[2

9-A

ug

-20

15

]

EA

20

0:

De

scrip

tion

Pa

le b

row

n c

lay

soil

with

gre

y ro

cks

BH

20

_0

.5-0

.6 -

[2

9-A

ug

-20

15

]

EA

20

0:

De

scrip

tion

Pa

le b

row

n s

an

dy

soil

with

ple

nty

of

sla

g d

eb

ris

BH

20

_1

.0-1

.1 -

[2

9-A

ug

-20

15

]

EA

20

0:

De

scrip

tion

Pa

le g

rey

cla

y so

il w

ith b

rick

an

d s

lag

de

bris

BH

03

_0

.2-0

.3 -

[2

9-A

ug

-20

15

]

EA

20

0:

De

scrip

tion

Mid

bro

wn

cla

y s

oil

with

sla

g g

rain

s a

nd

se

vera

l fria

ble

asb

est

os

fibre

bu

nd

les

ap

pro

x 5

x 2

x 2

mm

BH

03

_1

.0-1

.2 -

[2

9-A

ug

-20

15

]

EA

20

0:

De

scrip

tion

Pa

le b

row

n s

an

dy

soil

with

gre

y r

ocks

BH

02

_0

.4-0

.5 -

[2

9-A

ug

-20

15

]

Page 5: Cover - Attach C14f

Fals

e 4 4

.00

Tru

e

Envir

onm

ental

QU

AL

ITY

CO

NT

RO

L R

EP

OR

TW

ork

Ord

er

:E

S1529729

Pa

ge

:1

of 8

::

La

bo

rato

ryC

lien

tE

nvi

ronm

enta

l Div

isio

n S

ydney

AE

CO

M A

ustr

alia P

ty L

td

:C

onta

ctM

R A

LE

X L

AT

HA

M:

Conta

ctB

arb

ara

Hanna

:A

dd

ress

LE

VE

L 2

1, 420 G

eorg

e S

treet

SY

DN

EY

NS

W 2

000

Ad

dre

ss:

277-2

89 W

oodpark

Road S

mith

field

NS

W A

ust

ralia

2164

::

E-m

ail

E-m

ail

ale

x.la

tham

@aeco

m.c

om

Barb

ara

.Hanna@

als

glo

bal.c

om

::

Te

lep

ho

ne

+61 0

2 8

934 0

000

+61 2

8784 8

555

:T

ele

ph

on

e

::

Fa

csi

mile

Fa

csim

ile+

61 0

2 8

934 0

001

+61-2

-8784 8

500

QC

Le

ve

l:

NE

PM

2013 S

chedule

B(3

) and A

LS

QC

S3 r

equirem

ent

:P

roje

ct60438840 B

UR

RO

WS

IN

DU

ST

RIA

L

Da

te S

am

ple

s R

ece

ive

d:31-A

ug-2

015

:O

rde

r n

um

be

r60438840

Da

te A

na

lysis

Co

mm

en

ce

d:03-S

ep-2

015

:C

-O-C

nu

mb

er

----

Issu

e D

ate

:08-S

ep-2

015

Sa

mp

ler

:K

AT

E P

IGR

AM

No

. o

f sa

mp

les

rece

ive

d24

:S

ite:

----

No

. o

f sa

mp

les a

na

lyse

d12

:Q

uo

te n

um

be

r:

----

This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted.

This

Qualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

La

bo

rato

ry D

up

lica

te (

DU

P)

Re

po

rt;

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce (

RP

D)

an

d A

cce

pta

nce

Lim

its

l

Me

tho

d B

lan

k (M

B)

an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

l

Ma

trix

Sp

ike

(M

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

Sig

nato

ries

This

docu

ment

has

been

ele

ctro

nic

ally

si

gned

by

the

auth

orize

d

signato

ries

indic

ate

d

belo

w.

Ele

ctro

nic

si

gnin

g

has

been

carr

ied

out

in

com

plia

nce

with

pro

cedure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

siti

on

Ce

line

Co

nce

ica

oS

en

ior

Sp

ectr

osc

op

ist

Syd

ne

y In

org

an

ics

Ch

rist

op

he

r O

wle

rT

ea

m L

ea

de

r -

Asb

est

os

Ne

wca

stle

- A

sbe

sto

s

Pa

bi S

ub

ba

Se

nio

r O

rga

nic

Ch

em

ist

Syd

ne

y In

org

an

ics

Pa

bi S

ub

ba

Se

nio

r O

rga

nic

Ch

em

ist

Syd

ne

y O

rga

nic

s

NA

TA

Acc

red

ited

La

bo

rato

ry 8

25

Acc

red

ited

fo

r

com

plia

nce

with

ISO

/IE

C 1

70

25

.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 6: Cover - Attach C14f

2 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Gen

era

l C

om

men

ts

Th

e

an

aly

tica

l p

roce

du

res

use

d

by

the

E

nvi

ron

me

nta

l D

ivis

ion

h

ave

b

ee

n

de

ve

lop

ed

fr

om

e

sta

blis

he

d

inte

rna

tion

ally

re

cog

niz

ed

p

roce

du

res

such

a

s th

ose

p

ub

lish

ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

NE

PM

. In

h

ou

se

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

atio

n h

as

be

en

pe

rfo

rme

d,

resu

lts a

re r

ep

ort

ed

on

a d

ry w

eig

ht

ba

sis.

Wh

ere

a r

ep

ort

ed

less

th

an

(<

) re

sult

is h

igh

er

tha

n t

he

LO

R,

this

ma

y b

e d

ue

to

prim

ary

sa

mp

le e

xtra

ct/

dig

est

ate

dilu

tio

n a

nd

/or

insu

ffic

ien

t sa

mp

le f

or

an

aly

sis

. W

he

re t

he

LO

R o

f a

re

po

rte

d r

esu

lt d

iffe

rs f

rom

sta

nd

ard

LO

R,

this

ma

y b

e d

ue

to

hig

h m

ois

ture

co

nte

nt,

insu

ffic

ien

t sa

mp

le (

red

uce

d w

eig

ht

em

plo

yed

) o

r m

atr

ix in

terf

ere

nce

.

An

on

ymo

us

= R

efe

rs t

o s

am

ple

s w

hic

h a

re n

ot

spe

cific

ally

pa

rt o

f th

is w

ork

ord

er

bu

t fo

rme

d p

art

of

the

QC

pro

cess

lot

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

da

tab

ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l A

bstr

acts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

RP

D =

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce

#

= I

nd

ica

tes

faile

d Q

C

Ke

y :

Page 7: Cover - Attach C14f

3 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

D

up

lica

te

refe

rs

to

a

ran

do

mly

se

lect

ed

in

tra

lab

ora

tory

sp

lit.

La

bo

rato

ry

du

plic

ate

s

pro

vid

e

info

rma

tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

erc

en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:-

0%

- 5

0%

; R

esu

lt >

20

tim

es L

OR

:0%

- 2

0%

.

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EA

055:

Mo

istu

re C

on

ten

t (

QC

Lo

t: 2

03955)

EA

05

5-1

03

: M

ois

ture

Co

nte

nt

(drie

d @

10

3°C

)--

--1

%1

7.8

21

.71

9.8

0%

- 2

0%

BH

18

_0

.7-0

.8

ES

15

29

72

9-0

02

EA

05

5-1

03

: M

ois

ture

Co

nte

nt

(drie

d @

10

3°C

)--

--1

%1

4.6

17

.31

7.1

0%

- 5

0%

QC

11

1

ES

15

29

72

9-0

24

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

C L

ot:

202940) EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S1

52

97

22

-01

0

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g3

<2

0.0

0N

o L

imit

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

2<

20

.00

No

Lim

it

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g2

51

17

8.5

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g1

21

20

.00

No

Lim

it

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g2

30

.00

No

Lim

itB

H1

8_

0.7

-0.8

E

S1

52

97

29

-00

2

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g2

82

51

4.2

0%

- 5

0%

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g6

87

71

2.8

0%

- 2

0%

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

20

18

8.8

3N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g4

76

40

51

6.0

0%

- 2

0%

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g4

69

46

41

.25

0%

- 2

0%

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

70

47

27

3.2

00

% -

20

%

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

C L

ot:

202942) EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

11

0.0

0N

o L

imit

BH

02

_2

.0-2

.1

ES

15

29

72

9-0

20

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g3

32

81

4.3

0%

- 5

0%

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g2

83

93

1.7

0%

- 5

0%

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

59

49

17

.10

% -

50

%

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g7

83

78

20

.00

0%

- 2

0%

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g1

41

01

66

01

6.5

0%

- 2

0%

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

81

59

56

15

.90

% -

20

%

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S1

52

98

10

-00

3

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g1

01

00

.00

No

Lim

it

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g5

50

.00

No

Lim

it

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g1

21

01

3.8

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g6

70

.00

No

Lim

it

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

94

10

06

.42

0%

- 2

0%

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

C L

ot:

202941)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g0

.1<

0.1

0.0

0N

o L

imit

BH

18

_0

.7-0

.8

ES

15

29

72

9-0

02

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g0

.60

.94

1.4

No

Lim

itB

H0

2_

2.0

-2.1

E

S1

52

97

29

-02

0

Page 8: Cover - Attach C14f

4 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

C L

ot:

201988)

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

itB

H1

8_

0.7

-0.8

E

S1

52

97

29

-00

2

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

1

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

Page 9: Cover - Attach C14f

5 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

201980)

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

15

30

05

1-0

04

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

15

30

05

1-0

01

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

201989)

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itB

H1

8_

0.7

-0.8

E

S1

52

97

29

-00

2

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

1

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

201980)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

4

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

1

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

201989)

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

BH

18

_0

.7-0

.8

ES

15

29

72

9-0

02

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n>

C1

0_

C1

65

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

An

on

ymo

us

ES

15

30

05

1-0

01

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n>

C1

0_

C1

65

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

080:

BT

EX

N (Q

C L

ot:

201980)

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

4

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

it

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S1

53

00

51

-00

1

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

it

Page 10: Cover - Attach C14f

6 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

am

ple

(L

CS

) re

fers

to

a

ce

rtifi

ed

re

fere

nce

m

ate

ria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

202940)

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

10

52

1.7

mg

/kg

13

09

2

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

19

5.6

4.6

4 m

g/k

g1

21

87

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g<

28

7.2

43

.9 m

g/k

g1

36

80

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g<

59

9.8

32

mg

/kg

12

79

3

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

59

7.1

40

mg

/kg

12

48

6

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

29

6.8

55

mg

/kg

13

19

3

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

97

.36

0.8

mg

/kg

13

38

1

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

202942)

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

10

22

1.7

mg

/kg

13

09

2

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

19

7.2

4.6

4 m

g/k

g1

21

87

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g<

28

8.4

43

.9 m

g/k

g1

36

80

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g<

51

01

32

mg

/kg

12

79

3

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

59

7.1

40

mg

/kg

12

48

6

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

29

9.5

55

mg

/kg

13

19

3

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

97

.56

0.8

mg

/kg

13

38

1

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

CL

ot:

202941)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

79

.32

.57

mg

/kg

10

57

0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

201988)

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

98

.36

mg

/kg

12

37

9

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

91

.26

mg

/kg

12

37

7

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

10

16

mg

/kg

12

37

9

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

94

.26

mg

/kg

12

17

3

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

92

.06

mg

/kg

12

27

6

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.59

2.0

6 m

g/k

g1

18

70

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

97

.66

mg

/kg

11

47

2

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.59

8.7

6 m

g/k

g1

23

77

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.59

2.4

6 m

g/k

g1

23

81

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

87

.26

mg

/kg

11

37

2

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

97

.06

mg

/kg

12

37

9

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

93

.86

mg

/kg

12

37

7

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.59

0.2

6 m

g/k

g1

13

71

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.51

02

6 m

g/k

g1

24

80

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

99

.66

mg

/kg

12

37

9

Page 11: Cover - Attach C14f

7 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

201988)

- c

on

tin

ued

EP

07

5(S

IM):

Pyr

en

e1

29

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-00

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g/k

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0.5

97

.36

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/kg

12

57

9

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

201980)

EP

08

0:

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- C

9 F

ract

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mg

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07

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26

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86

8

EP

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tal P

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ole

um

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s (Q

CL

ot:

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EP

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ract

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50

mg

/kg

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01

03

20

0 m

g/k

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31

71

EP

07

1:

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8 F

ract

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0m

g/k

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10

01

08

30

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38

74

EP

07

1:

C2

9 -

C3

6 F

ract

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----

10

0m

g/k

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10

01

07

20

0 m

g/k

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28

64

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

201980)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

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10

77

.03

1 m

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28

68

EP

080/0

71:

To

tal R

eco

vera

ble

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rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

201989)

EP

07

1:

>C

10

- C

16

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ctio

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C1

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C1

65

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10

52

50

mg

/kg

13

07

0

EP

07

1:

>C

16

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34

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ctio

n--

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00

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00

10

73

50

mg

/kg

13

87

4

EP

07

1:

>C

34

- C

40

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ctio

n--

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00

mg

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00

94

.81

50

mg

/kg

13

16

3

EP

080:

BT

EX

N (Q

CL

ot:

201980)

EP

08

0:

Be

nze

ne

71

-43

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g/k

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81

.41

mg

/kg

11

66

2

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

81

.21

mg

/kg

11

85

8

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

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/kg

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5.4

2 m

g/k

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20

60

EP

08

0:

Na

ph

tha

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g/k

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18

8.6

1 m

g/k

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38

62

EP

08

0:

ort

ho

-Xyl

en

e9

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7-6

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mg

/kg

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1 m

g/k

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20

60

EP

08

0:

To

lue

ne

10

8-8

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mg

/kg

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1 m

g/k

g1

28

62

Matr

ix S

pik

e (

MS

) R

ep

ort

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e

qu

alit

y co

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M

atr

ix

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S)

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rs

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in

tra

lab

ora

tory

sp

lit

sam

ple

sp

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d

with

a

re

pre

sen

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f ta

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na

lyte

s.

Th

e

pu

rpo

se

o

f th

is

QC

p

ara

me

ter

is

to

mo

nito

r p

ote

ntia

l m

atr

ix

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ects

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n

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aly

te r

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tatic

Re

cove

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imits

as

pe

r la

bo

rato

ry D

ata

Qu

alit

y O

bje

ctiv

es

(DQ

Os).

Id

ea

l re

cove

ry r

an

ge

s sta

ted

ma

y b

e w

aiv

ed

in t

he

eve

nt

of

sa

mp

le m

atr

ix in

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ere

nce

.

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b-M

atr

ix:

SO

ILM

atr

ix S

pik

e (

MS

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ep

ort

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ikeR

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very

(%)

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very

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its (

%)

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ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

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mp

ou

nd

CA

S N

um

ber

EG

005T

: T

ota

l M

eta

ls b

y IC

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ES

(Q

CL

ot:

202940)

BH

18

_0

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ES

15

29

72

9-0

02

74

40

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G0

05

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en

ic8

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/kg

13

07

0

74

40

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ium

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g/k

g1

30

70

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G0

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ium

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30

70

74

40

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G0

05

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Co

pp

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11

02

50

mg

/kg

13

07

0

74

39

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Le

ad

74

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50

mg

/kg

13

07

0

74

40

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05

T:

Nic

kel

12

65

0 m

g/k

g1

30

70

74

40

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G0

05

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c1

12

25

0 m

g/k

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30

70

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

202942)

Page 12: Cover - Attach C14f

8 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

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ct

Su

b-M

atr

ix:

SO

ILM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

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very

Lim

its (

%)

Sp

ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

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ple

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Clien

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ple

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od:

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29

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9-0

20

74

40

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en

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50

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/kg

13

07

0

74

40

-43

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G0

05

T:

Ca

dm

ium

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.45

0 m

g/k

g1

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70

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40

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G0

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T:

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rom

ium

12

95

0 m

g/k

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30

70

74

40

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G0

05

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pp

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93

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50

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13

07

0

74

39

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ad

11

82

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07

0

74

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kel

11

15

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70

74

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: P

oly

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cle

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Aro

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c H

yd

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s (Q

CL

ot:

201988)

An

on

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75

(SIM

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ap

hth

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7.2

10

mg

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13

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0

12

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en

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02

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mg

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13

07

0

EP

080/0

71:

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tal P

etr

ole

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Hyd

rocarb

on

s (Q

CL

ot:

201980)

An

on

ymo

us

ES

15

30

05

1-0

01

----

EP

08

0:

C6

- C

9 F

ract

ion

89

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2.5

mg

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13

07

0

EP

080/0

71:

To

tal P

etr

ole

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s (Q

CL

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201989)

An

on

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15

30

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1-0

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----

EP

07

1:

C1

0 -

C1

4 F

ract

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99

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23

mg

/kg

13

77

3

----

EP

07

1:

C1

5 -

C2

8 F

ract

ion

10

32

31

9 m

g/k

g1

31

53

----

EP

07

1:

C2

9 -

C3

6 F

ract

ion

12

41

71

4 m

g/k

g1

32

52

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

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s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

201980)

An

on

ymo

us

ES

15

30

05

1-0

01

C6

_C

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EP

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10

Fra

ctio

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EP

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71:

To

tal R

eco

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rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

201989)

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on

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15

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EP

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10

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32

23

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3

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EP

07

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40

Fra

ctio

n1

16

10

58

mg

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13

25

2

EP

080:

BT

EX

N (Q

CL

ot:

201980)

An

on

ymo

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ES

15

30

05

1-0

01

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P0

80

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en

zen

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9.0

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/kg

13

07

0

10

0-4

1-4

EP

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ylb

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zen

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13

07

0

10

8-3

8-3

10

6-4

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EP

08

0:

me

ta-

& p

ara

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en

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13

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0

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10

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lue

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81

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g/k

g1

30

70

Page 13: Cover - Attach C14f

Tru

e

Envir

onm

ental

QA

/QC

Co

mp

lia

nc

e A

ss

es

sm

en

t fo

r D

QO

Re

po

rtin

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ork

Ord

er

:E

S1529729

Pa

ge

:1

of 5

::

La

bo

rato

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lient

Envi

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enta

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ydney

AE

CO

M A

ustr

alia P

ty L

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ct60438840 B

UR

RO

WS

IN

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Sa

mp

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d:31-A

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Site

:--

--Is

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Da

te:08-S

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KA

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RA

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r60438840

No

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Th

is r

ep

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is a

uto

mati

cally g

en

era

ted

by t

he A

LS

LIM

S t

hro

ug

h in

terp

reta

tio

n o

f th

e A

LS

Qu

ality

Co

ntr

ol R

ep

ort

an

d s

evera

l Q

uality

Assu

ran

ce p

ara

mete

rs m

easu

red

by A

LS

. T

his

au

tom

ate

d

rep

ort

ing

hig

hlig

hts

an

y n

on

-co

nfo

rman

ces, fa

cilit

ate

s f

aste

r an

d m

ore

accu

rate

data

valid

ati

on

an

d is d

esig

ned

to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

Co

ntr

ol (

QC

) R

ep

ort

.

l

NO

Meth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

NO

Du

plicate

ou

tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

NO

Matr

ix S

pik

e o

utl

iers

occu

r.

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, N

O su

rro

gate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

l

NO

An

aly

sis

Ho

ldin

g T

ime O

utl

iers

exis

t.

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

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l

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Qu

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Co

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am

ple

Fre

qu

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R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 14: Cover - Attach C14f

2 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

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Th

is

rep

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su

mm

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s e

xtra

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/ p

rep

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a

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a

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lysi

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es

an

d

com

pa

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ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

ncin

g

US

EP

A

SW

8

46

, A

PH

A,

AS

a

nd

N

EP

M)

ba

sed

o

n

the

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

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nt

first

da

te o

f e

xtra

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n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A li

stin

g o

f b

rea

ch

es (

if a

ny)

is

pro

vid

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he

rein

.

Ho

ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

Ass

ess

me

nt

co

mp

are

s

the

le

ach

d

ate

w

ith

the

sh

ort

est

a

na

lyte

h

old

ing

tim

e

for

the

e

qu

iva

len

t so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

A r

eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest

.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

time

is

7

da

ys;

oth

ers

1

4 d

ays

.

A

reco

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes o

f in

tere

st/c

on

ce

rn.

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EA

055:

Mo

istu

re C

on

ten

t

So

il G

lass J

ar

- U

np

reserv

ed

(E

A055-1

03)

BH

18

_0

.7-0

.8,

BH

18

_2

.0-2

.1,

BH

20

_0

.5-0

.6,

BH

20

_1

.0-1

.1,

BH

20

_2

.0-2

.1,

BH

03

_0

.2-0

.3,

BH

03

_1

.0-1

.2,

BH

03

_3

.0-3

.1,

BH

02

_0

.4-0

.5,

BH

02

_2

.0-2

.1,

BH

02

_3

.0-3

.1,

QC

11

1

12

-Se

p-2

01

5--

--04-S

ep

-20

15

----

29-A

ug

-2015

----

ü

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

Sn

ap

Lo

ck B

ag

- S

ep

ara

te b

ag

receiv

ed

(E

A200)

BH

18

_0

.7-0

.8,

BH

20

_0

.5-0

.6,

BH

20

_1

.0-1

.1,

BH

03

_0

.2-0

.3,

BH

03

_1

.0-1

.2,

BH

02

_0

.4-0

.5

25

-Fe

b-2

01

6--

--04-S

ep

-20

15

----

29-A

ug

-2015

----

ü

EG

005T

: T

ota

l M

eta

ls b

y IC

P-A

ES

So

il G

lass J

ar

- U

np

reserv

ed

(E

G005T

)

BH

18

_0

.7-0

.8,

BH

18

_2

.0-2

.1,

BH

20

_0

.5-0

.6,

BH

20

_1

.0-1

.1,

BH

03

_0

.2-0

.3,

BH

03

_1

.0-1

.2,

BH

03

_3

.0-3

.1,

BH

02

_0

.4-0

.5,

BH

02

_2

.0-2

.1,

QC

11

1

25

-Fe

b-2

01

62

5-F

eb

-20

16

04-S

ep

-20

15

04-S

ep

-2015

29-A

ug

-2015

üü

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

So

il G

lass J

ar

- U

np

reserv

ed

(E

G035T

)

BH

18

_0

.7-0

.8,

BH

18

_2

.0-2

.1,

BH

20

_0

.5-0

.6,

BH

20

_1

.0-1

.1,

BH

03

_0

.2-0

.3,

BH

03

_1

.0-1

.2,

BH

03

_3

.0-3

.1,

BH

02

_0

.4-0

.5,

BH

02

_2

.0-2

.1,

QC

11

1

26

-Se

p-2

01

52

6-S

ep

-20

15

07-S

ep

-20

15

04-S

ep

-2015

29-A

ug

-2015

üü

Page 15: Cover - Attach C14f

3 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

18

_0

.7-0

.8,

BH

20

_2

.0-2

.1,

BH

03

_1

.0-1

.2,

BH

03

_3

.0-3

.1,

BH

02

_0

.4-0

.5,

BH

02

_3

.0-3

.1,

QC

11

1

13

-Oct-

20

15

12

-Se

p-2

01

504-S

ep

-20

15

03-S

ep

-2015

29-A

ug

-2015

üü

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P075(S

IM))

BH

18

_0

.7-0

.8,

BH

18

_2

.0-2

.1,

BH

20

_0

.5-0

.6,

BH

20

_1

.0-1

.1,

BH

03

_0

.2-0

.3,

BH

03

_1

.0-1

.2,

BH

02

_0

.4-0

.5,

QC

11

1

13

-Oct-

20

15

12

-Se

p-2

01

504-S

ep

-20

15

03-S

ep

-2015

29-A

ug

-2015

üü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

18

_0

.7-0

.8,

BH

20

_2

.0-2

.1,

BH

03

_1

.0-1

.2,

BH

03

_3

.0-3

.1,

BH

02

_0

.4-0

.5,

BH

02

_3

.0-3

.1,

QC

11

1

12

-Se

p-2

01

51

2-S

ep

-20

15

04-S

ep

-20

15

03-S

ep

-2015

29-A

ug

-2015

üü

Page 16: Cover - Attach C14f

4 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Qu

ality

Co

ntr

ol P

ara

mete

r F

req

uen

cy C

om

plian

ce

Th

e f

ollo

win

g r

ep

ort

su

mm

arise

s th

e f

req

ue

ncy

of

lab

ora

tory

QC

sa

mp

les

an

aly

sed

with

in t

he

an

aly

tica

l lo

t(s)

in

wh

ich

th

e s

ub

mitt

ed

sa

mp

le(s

) w

as(

we

re)

pro

cess

ed

. A

ctu

al r

ate

sh

ou

ld b

e g

rea

ter

tha

n o

r e

qu

al t

o

the

exp

ect

ed

ra

te.

A li

stin

g o

f b

rea

che

s is

pro

vid

ed

in t

he

Su

mm

ary

of

Ou

tlie

rs.

Ma

trix

: S

OIL

Eva

lua

tio

n: û

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy

no

t w

ithin

sp

eci

fica

tion

; ü

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy w

ithin

sp

ecifi

ca

tion

.

Qu

alit

y C

on

tro

l Sp

ecifi

ca

tion

Qualit

y C

ontr

ol S

am

ple

Typ

e

Exp

ecte

dQ

CR

eg

ula

rA

ctu

al

Ra

te (

%)

Qualit

y C

ontr

ol S

am

ple

Typ

eC

ou

nt

Eva

lua

tio

nA

na

lytic

al M

eth

od

sM

eth

od

La

bo

rato

ry D

up

lica

tes

(DU

P)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

10.0

0 1

0.0

02

20

üM

ois

ture

Co

nte

nt

EA

05

5-1

03

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

12.5

0 1

0.0

02

16

üP

AH

/Ph

en

ols

(S

IM)

EP

07

5(S

IM)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

11.1

1 1

0.0

02

18

üT

ota

l Me

rcu

ry b

y F

IMS

EG

03

5T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

10.0

0 1

0.0

02

20

üT

ota

l Me

tals

by

ICP

-AE

SE

G0

05

T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

12.5

0 1

0.0

02

16

üT

RH

- S

em

ivo

latil

e F

ract

ion

EP

07

1

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

11.7

6 1

0.0

02

17

üT

RH

Vo

latile

s/B

TE

XE

P0

80

La

bo

rato

ry C

on

tro

l Sa

mp

les

(LC

S)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

PA

H/P

he

no

ls (

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.5

6 5

.00

11

To

tal M

erc

ury

by

FIM

SE

G0

35

T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.0

0 5

.00

12

To

tal M

eta

ls b

y IC

P-A

ES

EG

00

5T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

TR

H -

Se

miv

ola

tile

Fra

ctio

nE

P0

71

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.8

8 5

.00

11

TR

H V

ola

tile

s/B

TE

XE

P0

80

Me

tho

d B

lan

ks (

MB

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

PA

H/P

he

no

ls (

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.5

6 5

.00

11

To

tal M

erc

ury

by

FIM

SE

G0

35

T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.0

0 5

.00

12

To

tal M

eta

ls b

y IC

P-A

ES

EG

00

5T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

TR

H -

Se

miv

ola

tile

Fra

ctio

nE

P0

71

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.8

8 5

.00

11

TR

H V

ola

tile

s/B

TE

XE

P0

80

Ma

trix

Sp

ike

s (M

S)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

PA

H/P

he

no

ls (

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.5

6 5

.00

11

To

tal M

erc

ury

by

FIM

SE

G0

35

T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.0

0 5

.00

12

To

tal M

eta

ls b

y IC

P-A

ES

EG

00

5T

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

6.2

5 5

.00

11

TR

H -

Se

miv

ola

tile

Fra

ctio

nE

P0

71

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

5.8

8 5

.00

11

TR

H V

ola

tile

s/B

TE

XE

P0

80

Page 17: Cover - Attach C14f

5 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

9

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Bri

ef

Meth

od

Su

mm

ari

es

Th

e a

na

lytic

al p

roce

du

res

use

d b

y th

e E

nvi

ron

me

nta

l Div

isio

n h

ave

be

en

de

velo

pe

d f

rom

est

ab

lish

ed

in

tern

atio

na

lly r

eco

gn

ize

d p

roce

du

res s

uch

as

tho

se p

ub

lish

ed

by

the

US

EP

A,

AP

HA

, A

S a

nd

NE

PM

. In

ho

use

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Th

e f

ollo

win

g r

ep

ort

pro

vid

es

brie

f d

esc

rip

tio

ns

of

the

an

aly

tica

l pro

ced

ure

s e

mp

loye

d f

or

resu

lts r

ep

ort

ed

in t

he

Ce

rtifi

cate

of

An

aly

sis.

So

urc

es

fro

m w

hic

h A

LS

me

tho

ds

ha

ve b

ee

n d

eve

lop

ed

are

pro

vid

ed

with

in t

he

Me

tho

d D

esc

rip

tion

s.

An

aly

tica

l Me

tho

ds

Me

tho

d D

esc

rip

tion

sM

atr

ixM

eth

od

In-h

ouse

. A

gra

vim

etr

ic p

roce

dure

base

d o

n w

eig

ht lo

ss o

ver

a 1

2 h

our

dry

ing p

eriod a

t 103-1

05 d

egre

es

C.

This

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Schedule

B(3

) S

ect

ion 7

.1 a

nd T

able

1 (

14 d

ay

hold

ing tim

e).

Mois

ture

Conte

nt

EA

05

5-1

03

SO

IL

AS

4964 -

2004 M

eth

od for

the q

ualit

ativ

e id

entif

icatio

n o

f asb

est

os

in b

ulk

sam

ple

s

Analy

sis

by

Pola

rise

d L

ight M

icro

scopy

incl

udin

g d

ispers

ion s

tain

ing

Asb

est

os

Identif

icatio

n in

Soils

EA

20

0S

OIL

In h

ouse

: R

efe

rence

d to A

PH

A 3

120; U

SE

PA

SW

846 -

6010. M

eta

ls a

re d

ete

rmin

ed follo

win

g a

n a

ppro

priate

aci

d d

igest

ion o

f th

e s

oil.

T

he IC

PA

ES

tech

niq

ue io

nis

es

sam

ple

s in

a p

lasm

a, em

ittin

g a

chara

cterist

ic

spect

rum

base

d o

n m

eta

ls p

rese

nt. In

tensi

ties

at se

lect

ed w

ave

length

s are

com

pare

d a

gain

st those

of m

atr

ix

matc

hed s

tandard

s. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

Tota

l Meta

ls b

y IC

P-A

ES

EG

00

5T

SO

IL

In h

ouse

: R

efe

rence

d to A

S 3

550, A

PH

A 3112 H

g -

B (

Flo

w-inje

ctio

n (

SnC

l2)(

Cold

Vapour

genera

tion)

AA

S)

FIM

-AA

S is

an a

uto

mate

d fla

mele

ss a

tom

ic a

bso

rptio

n tech

niq

ue. M

erc

ury

in s

olid

s are

dete

rmin

ed follo

win

g a

n

appro

priate

aci

d d

igest

ion. Io

nic

merc

ury

is r

educe

d o

nlin

e to a

tom

ic m

erc

ury

vapour

by

SnC

l2 w

hic

h is

then

purg

ed in

to a

heate

d q

uart

z ce

ll. Q

uantif

icatio

n is

by

com

paring a

bso

rbance

again

st a

calib

ratio

n c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

Tota

l Merc

ury

by

FIM

SE

G0

35

TS

OIL

(US

EP

A S

W 8

46 -

8015A

) S

am

ple

ext

ract

s are

analy

sed b

y C

apill

ary

GC

/FID

and q

uantif

ied a

gain

st a

lkane

standard

s ove

r th

e r

ange C

10 -

C40.

TR

H -

Sem

ivola

tile F

ract

ion

EP

07

1S

OIL

(US

EP

A S

W 8

46 -

8270B

) E

xtra

cts

are

analy

sed b

y C

apill

ary

GC

/MS

in S

ele

ctiv

e Ion M

ode (

SIM

) and

quantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith

NE

PM

(2013)

Sch

edule

B(3

) (M

eth

od 5

02 a

nd 5

07)

PA

H/P

henols

(S

IM)

EP

07

5(S

IM)

SO

IL

(US

EP

A S

W 8

46 -

8260B

) E

xtra

cts

are

analy

sed b

y P

urg

e a

nd T

rap, C

apill

ary

GC

/MS

. Q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5 p

oin

t ca

libra

tion c

urv

e.

TR

H V

ola

tiles/

BT

EX

EP

08

0S

OIL

Pre

pa

ratio

n M

eth

od

sM

eth

od

De

scrip

tion

sM

atr

ixM

eth

od

(US

EP

A S

W 8

46 -

5030A

) 5g o

f so

lid is

shake

n w

ith s

urr

ogate

and 1

0m

L m

eth

anol p

rior

to a

naly

sis

by

Purg

e

and T

rap -

G

C/M

S.

Meth

anolic

Ext

ract

ion o

f S

oils

for

Purg

e

and T

rap

* O

RG

16

SO

IL

In-h

ouse

, M

ech

anic

al a

gita

tion (

tum

ble

r). 10g o

f sa

mple

, N

a2S

O4 a

nd s

urr

ogate

are

ext

ract

ed w

ith 3

0m

L 1

:1

DC

M/A

ceto

ne b

y end o

ver

end tum

ble

. T

he s

olv

ent is

deca

nte

d, dehyd

rate

d a

nd c

once

ntr

ate

d (

by

KD

) to

the

desi

red v

olu

me for

analy

sis.

Tum

ble

r E

xtra

ctio

n o

f S

olid

sO

RG

17

SO

IL

Page 18: Cover - Attach C14f

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1529729

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Barbara Hanna

:: AddressAddress LEVEL 21, 420 George Street

SYDNEY NSW 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60438840 BURROWS INDUSTRIAL Page 1 of 3

:Order number 60438840 :Quote number EB2015AECOMAU0580 (EN/004/15)

:C-O-C number ---- :QC Level NEPM 2013 Schedule B(3) and ALS

QCS3 requirementSite : ----

Sampler : KATE PIGRAM

DatesDate Samples Received : Issue Date : 03-Sep-201531-Aug-2015 3:45 PM

Scheduled Reporting Date: 07-Sep-2015:Client Requested Due

Date

07-Sep-2015

Delivery DetailsMode of Delivery : :Undefined Intact.Security Seal

No. of coolers/boxes : :---- Temperature 18.2' C

: : 24 / 12Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Asbestos analysis will be conducted by ALS Newcastle.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 19: Cover - Attach C14f

:Client AECOM Australia Pty Ltd

Work Order : ES1529729 Amendment 02 of 3:Page

03-Sep-2015:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exist.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

(On H

old

) S

OIL

No a

naly

sis

request

ed

SO

IL -

EA

055-1

03

Mois

ture

Conte

nt

SO

IL -

EA

200

Asbesto

s Id

entif

icatio

n in S

oils

-

SO

IL -

EP

075 S

IM P

AH

only

SIM

- P

AH

only

SO

IL -

S-0

2

8 M

eta

ls (

incl. D

igestion)

SO

IL -

S-0

4

TR

H/B

TE

XN

SO

IL -

S-2

6

8 m

eta

ls/T

RH

/BT

EX

N/P

AH

ES1529729-001 [ 29-Aug-2015 ] BH18_0.25-0.35 ü

ES1529729-002 [ 29-Aug-2015 ] BH18_0.7-0.8 ü ü ü

ES1529729-003 [ 29-Aug-2015 ] BH18_1.0-1.1 ü

ES1529729-004 [ 29-Aug-2015 ] BH18_2.0-2.1 ü ü ü

ES1529729-005 [ 29-Aug-2015 ] BH18_3.0-3.1 ü

ES1529729-006 [ 29-Aug-2015 ] BH18_3.8-3.9 ü

ES1529729-007 [ 29-Aug-2015 ] BH20_0.5-0.6 ü ü ü ü

ES1529729-008 [ 29-Aug-2015 ] BH20_1.0-1.1 ü ü ü ü

ES1529729-009 [ 29-Aug-2015 ] BH20_2.0-2.1 ü ü

ES1529729-010 [ 29-Aug-2015 ] BH20_3.5-3.6 ü

ES1529729-011 [ 29-Aug-2015 ] BH03_0.2-0.3 ü ü ü ü

ES1529729-012 [ 29-Aug-2015 ] BH03_0.5-0.6 ü

ES1529729-013 [ 29-Aug-2015 ] BH03_1.0-1.2 ü ü ü

ES1529729-014 [ 29-Aug-2015 ] BH03_1.4-1.5 ü

ES1529729-015 [ 29-Aug-2015 ] BH03_2.0-2.1 ü

ES1529729-016 [ 29-Aug-2015 ] BH03_3.0-3.1 ü

ES1529729-017 [ 29-Aug-2015 ] BH03_3.8-3.9 ü

ES1529729-018 [ 29-Aug-2015 ] BH02_0.4-0.5 ü ü ü

ES1529729-019 [ 29-Aug-2015 ] BH02_1.0-1.1 ü

ES1529729-020 [ 29-Aug-2015 ] BH02_2.0-2.1 ü ü

ES1529729-021 [ 29-Aug-2015 ] BH02_3.0-3.1 ü ü

ES1529729-022 [ 29-Aug-2015 ] BH02_3.8-3.9 ü

ES1529729-023 [ 29-Aug-2015 ] QC110 ü

ES1529729-024 [ 29-Aug-2015 ] QC111 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 20: Cover - Attach C14f

:Client AECOM Australia Pty Ltd

Work Order : ES1529729 Amendment 03 of 3:Page

03-Sep-2015:Issue Date

SO

IL -

S-0

5

TR

H/B

TE

XN

/8 M

eta

ls

ES1529729-016 [ 29-Aug-2015 ] BH03_3.0-3.1 ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - HLAPro (HLAPro) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

AP_CUSTOMER SERVICE ANZ

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

KATE PIGRAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - HLAPro (HLAPro) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

Page 21: Cover - Attach C14f
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Page 23: Cover - Attach C14f
Page 24: Cover - Attach C14f
Page 25: Cover - Attach C14f

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Genera

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Analy

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Desc

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Sig

nato

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This

docu

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has

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the

auth

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Page 26: Cover - Attach C14f

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led

prio

r to

tra

ce a

na

lysi

s a

s o

utli

ne

d in

IS

O2

39

09

:20

08

(E)

Se

ct 6

.3.2

-2l

Be

nzo

(a)p

yre

ne

To

xici

ty E

qu

iva

len

t Q

uo

tien

t (T

EQ

) is

th

e s

um

to

tal o

f th

e c

on

cen

tra

tion

of

the

eig

ht

carc

ino

ge

nic

PA

Hs

mu

ltip

lied

by t

he

ir T

oxi

city

Eq

uiv

ale

nce

Fa

cto

r (T

EF

) re

lativ

e t

o B

en

zo(a

)pyr

en

e.

TE

F v

alu

es

are

pro

vid

ed

in b

rack

ets

as

follo

ws:

Be

nz(

a)a

nth

race

ne

(0

.1),

Ch

ryse

ne

(0

.01

), B

en

zo(b

+j) &

Be

nzo

(k)f

luo

ran

the

ne

(0

.1),

Be

nzo

(a)p

yre

ne

(1

.0),

In

de

no

(1.2

.3.c

d)p

yre

ne

(0

.1),

Dib

en

z(a

.h)a

nth

race

ne

(1

.0),

Be

nzo

(g.h

.i)p

ery

len

e (

0.0

1).

Le

ss t

ha

n L

OR

re

sults

fo

r 'T

EQ

Ze

ro' a

re t

rea

ted

as

zero

.

l

Page 27: Cover - Attach C14f

3 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

SS

02

SS

01

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

[29

-Au

g-2

01

5]

[29

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529728-0

09

ES

1529728-0

08

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

Yes

Asb

esto

s D

ete

cte

dY

es +

Tra

ce

----

----

----

g/k

g0

.11

33

2-2

1-4

Ch

+ A

mA

sb

esto

s T

yp

eC

h +

Cr

----

----

----

---

13

32

-21

-4

169

381

----

----

----

g0

.01

----

Sam

ple

weig

ht

(dry

)

S.S

PO

ON

ER

S.S

PO

ON

ER

----

----

----

---

----

AP

PR

OV

ED

ID

EN

TIF

IER

:

Page 28: Cover - Attach C14f

4 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

----

SS

04-F

RA

GC

lien

t sa

mp

le I

DS

ub

-Ma

trix

: S

OL

ID

(M

atr

ix:

SO

LID

)

----

----

----

----

[29

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

----

----

ES

1529728-0

11

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

bu

lk s

am

ple

s

Yes

Asb

esto

s D

ete

cte

d--

----

----

----

--g

/kg

0.1

13

32

-21

-4

Ch

+ A

mA

sb

esto

s T

yp

e--

----

----

----

----

-1

33

2-2

1-4

42.3

----

----

----

----

g0

.01

----

Sam

ple

weig

ht

(dry

)

S.S

PO

ON

ER

----

----

----

----

---

----

AP

PR

OV

ED

ID

EN

TIF

IER

:

Page 29: Cover - Attach C14f

5 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

01

MW

17

MW

16

MW

19

MW

21

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

ES

1529

728

-005

ES

15297

28-0

04

ES

1529

728

-003

ES

1529728-0

02

ES

1529728-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

0.0

01

Ars

en

ic0.0

09

0.0

08

0.0

09

0.0

06

mg

/L0

.00

17

44

0-3

8-2

0.0

002

Cad

miu

m0.0

061

<0

.00

01

0.0

002

<0

.00

01

mg

/L0

.00

01

74

40

-43

-9

<0

.00

1C

hro

miu

m<

0.0

01

<0

.00

1<

0.0

01

<0

.00

1m

g/L

0.0

01

74

40

-47

-3

0.0

01

Co

pp

er

0.1

53

0.0

02

0.0

02

<0

.00

1m

g/L

0.0

01

74

40

-50

-8

<0

.00

1L

ead

0.0

09

0.0

04

0.0

04

<0

.00

1m

g/L

0.0

01

74

39

-92

-1

0.0

04

Nic

kel

0.1

28

0.0

07

0.0

26

0.0

03

mg

/L0

.00

17

44

0-0

2-0

0.0

66

Zin

c4.1

80.2

91

0.8

89

0.0

92

mg

/L0

.00

57

44

0-6

6-6

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

<0

.00

01

Merc

ury

<0

.00

01

<0

.00

01

<0

.00

01

<0

.00

01

mg

/L0

.00

01

74

39

-97

-6

EP

074D

: F

um

igan

ts

<5

2.2

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

55

94

-20

-7

<5

1.2

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

57

8-8

7-5

<5

cis

-1.3

-Dic

hlo

rop

rop

yle

ne

<5

<5

<5

<5

µg

/L5

10

06

1-0

1-5

<5

tran

s-1

.3-D

ich

loro

pro

pyle

ne

<5

<5

<5

<5

µg

/L5

10

06

1-0

2-6

<5

1.2

-Dib

rom

oeth

an

e (

ED

B)

<5

<5

<5

<5

µg

/L5

10

6-9

3-4

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<1

Vin

yl ch

lori

de

<1

<1

<1

<1

µg

/L1

75

-01

-4

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

<5

0D

ich

loro

dif

luo

rom

eth

an

e<

50

<5

0<

50

<5

g/L

50

75

-71

-8

<5

0C

hlo

rom

eth

an

e<

50

<5

0<

50

<5

g/L

50

74

-87

-3

<5

0B

rom

om

eth

an

e<

50

<5

0<

50

<5

g/L

50

74

-83

-9

<5

0C

hlo

roeth

an

e<

50

<5

0<

50

<5

g/L

50

75

-00

-3

<5

0T

rich

loro

flu

oro

meth

an

e<

50

<5

0<

50

<5

g/L

50

75

-69

-4

<5

1.1

-Dic

hlo

roeth

en

e<

5<

5<

5<

g/L

57

5-3

5-4

<5

Iod

om

eth

an

e<

5<

5<

5<

g/L

57

4-8

8-4

<5

tran

s-1

.2-D

ich

loro

eth

en

e<

5<

5<

5<

g/L

51

56

-60

-5

<5

1.1

-Dic

hlo

roeth

an

e<

5<

5<

5<

g/L

57

5-3

4-3

<5

cis

-1.2

-Dic

hlo

roeth

en

e<

5<

5<

5<

g/L

51

56

-59

-2

<5

1.1

.1-T

rich

loro

eth

an

e<

5<

5<

5<

g/L

57

1-5

5-6

<5

1.1

-Dic

hlo

rop

rop

yle

ne

<5

<5

<5

<5

µg

/L5

56

3-5

8-6

<5

Carb

on

Tetr

ach

lori

de

<5

<5

<5

<5

µg

/L5

56

-23

-5

<5

1.2

-Dic

hlo

roeth

an

e<

5<

5<

5<

g/L

51

07

-06

-2

<5

Tri

ch

loro

eth

en

e<

5<

5<

5<

g/L

57

9-0

1-6

<5

Dib

rom

om

eth

an

e<

5<

5<

5<

g/L

57

4-9

5-3

Page 30: Cover - Attach C14f

6 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

01

MW

17

MW

16

MW

19

MW

21

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

ES

1529

728

-005

ES

15297

28-0

04

ES

1529

728

-003

ES

1529728-0

02

ES

1529728-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

- C

on

tin

ued

<5

1.1

.2-T

rich

loro

eth

an

e<

5<

5<

5<

g/L

57

9-0

0-5

<5

1.3

-Dic

hlo

rop

rop

an

e<

5<

5<

5<

g/L

51

42

-28

-9

<5

Tetr

ach

loro

eth

en

e<

5<

5<

5<

g/L

51

27

-18

-4

<5

1.1

.1.2

-Tetr

ach

loro

eth

an

e<

5<

5<

5<

g/L

56

30

-20

-6

<5

tran

s-1

.4-D

ich

loro

-2-b

ute

ne

<5

<5

<5

<5

µg

/L5

11

0-5

7-6

<5

cis

-1.4

-Dic

hlo

ro-2

-bu

ten

e<

5<

5<

5<

g/L

51

47

6-1

1-5

<5

1.1

.2.2

-Tetr

ach

loro

eth

an

e<

5<

5<

5<

g/L

57

9-3

4-5

<5

1.2

.3-T

rich

loro

pro

pan

e<

5<

5<

5<

g/L

59

6-1

8-4

<5

Pen

tach

loro

eth

an

e<

5<

5<

5<

g/L

57

6-0

1-7

<5

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

<5

<5

<5

<5

µg

/L5

96

-12

-8

<5

Hexach

loro

bu

tad

ien

e<

5<

5<

5<

g/L

58

7-6

8-3

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds

<5

Ch

loro

ben

zen

e<

5<

5<

5<

g/L

51

08

-90

-7

<5

Bro

mo

ben

zen

e<

5<

5<

5<

g/L

51

08

-86

-1

<5

2-C

hlo

roto

luen

e<

5<

5<

5<

g/L

59

5-4

9-8

<5

4-C

hlo

roto

luen

e<

5<

5<

5<

g/L

51

06

-43

-4

<5

1.3

-Dic

hlo

rob

en

zen

e<

5<

5<

5<

g/L

55

41

-73

-1

<5

1.4

-Dic

hlo

rob

en

zen

e<

5<

5<

5<

g/L

51

06

-46

-7

<5

1.2

-Dic

hlo

rob

en

zen

e<

5<

5<

5<

g/L

59

5-5

0-1

<5

1.2

.4-T

rich

loro

ben

zen

e<

5<

5<

5<

g/L

51

20

-82

-1

<5

1.2

.3-T

rich

loro

ben

zen

e<

5<

5<

5<

g/L

58

7-6

1-6

EP

074G

: T

rih

alo

meth

an

es

<5

Ch

loro

form

<5

<5

<5

<5

µg

/L5

67

-66

-3

<5

Bro

mo

dic

hlo

rom

eth

an

e<

5<

5<

5<

g/L

57

5-2

7-4

<5

Dib

rom

och

loro

meth

an

e<

5<

5<

5<

g/L

51

24

-48

-1

<5

Bro

mo

form

<5

<5

<5

<5

µg

/L5

75

-25

-2

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

1.8

Nap

hth

ale

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

91

-20

-3

1.9

Acen

ap

hth

yle

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

20

8-9

6-8

<1

.0A

cen

ap

hth

en

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

18

3-3

2-9

1.7

Flu

ore

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

86

-73

-7

<1

.0P

hen

an

thre

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

85

-01

-8

<1

.0A

nth

racen

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

11

20

-12

-7

<1

.0F

luo

ran

then

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

12

06

-44

-0

Page 31: Cover - Attach C14f

7 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

01

MW

17

MW

16

MW

19

MW

21

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

ES

1529

728

-005

ES

15297

28-0

04

ES

1529

728

-003

ES

1529728-0

02

ES

1529728-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s -

Co

nti

nu

ed

<1

.0P

yre

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

12

9-0

0-0

<1

.0B

en

z(a)a

nth

racen

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

15

6-5

5-3

<1

.0C

hry

sen

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

12

18

-01

-9

<1

.0B

en

zo(b

+j)

flu

ora

nth

en

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

12

05

-99

-2 2

05

-82

-3

<1

.0B

en

zo(k

)flu

ora

nth

en

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

12

07

-08

-9

<0

.5B

en

zo(a

)pyre

ne

<0

.5<

0.5

<0

.5<

0.5

µg

/L0

.55

0-3

2-8

<1

.0In

den

o(1

.2.3

.cd

)pyre

ne

<1

.0<

1.0

<1

.0<

1.0

µg

/L1

19

3-3

9-5

<1

.0D

iben

z(a.h

)an

thra

cen

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

15

3-7

0-3

<1

.0B

en

zo(g

.h.i)p

ery

len

e<

1.0

<1

.0<

1.0

<1

.0µ

g/L

11

91

-24

-2

5.4

^ <

0.5

<0

.5<

0.5

<0

.5µ

g/L

0.5

----

Su

m o

f p

oly

cyclic a

rom

ati

c h

yd

rocarb

on

s

<0

.5^

<0

.5<

0.5

<0

.5<

0.5

µg

/L0

.5--

--B

en

zo(a

)pyre

ne T

EQ

(ze

ro)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<2

0<

20

<2

0<

20

<2

g/L

20

----

C6 -

C9 F

racti

on

160

<5

0<

50

<5

0<

50

µg

/L5

0--

--C

10 -

C14 F

racti

on

150

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

C15 -

C28 F

racti

on

<5

0<

50

<5

0<

50

<5

g/L

50

----

C29 -

C36 F

racti

on

310

^ <

50

<5

0<

50

<5

g/L

50

----

C10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

<2

0C

6 -

C10 F

racti

on

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0

<2

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<2

0<

20

<2

0<

20

µg

/L2

0C

6_

C1

0-B

TE

X

170

>C

10 -

C16 F

racti

on

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

>C

10

_C

16

120

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

>C

16 -

C34 F

racti

on

<1

00

<1

00

<1

00

<1

00

<1

00

µg

/L1

00

----

>C

34 -

C40 F

racti

on

290

^ <

10

0<

10

0<

10

0<

10

g/L

10

0--

-->

C10 -

C40 F

racti

on

(su

m)

160

^ <

10

0<

10

0<

10

0<

10

g/L

10

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<1

Ben

zen

e<

1<

1<

1<

g/L

17

1-4

3-2

<2

To

luen

e<

2<

2<

2<

g/L

21

08

-88

-3

<2

Eth

ylb

en

zen

e<

2<

2<

2<

g/L

21

00

-41

-4

<2

meta

- &

para

-Xyle

ne

<2

<2

<2

<2

µg

/L2

10

8-3

8-3

10

6-4

2-3

<2

ort

ho

-Xyle

ne

<2

<2

<2

<2

µg

/L2

95

-47

-6

<2

^ T

ota

l X

yle

nes

<2

<2

<2

<2

µg

/L2

13

30

-20

-7

<1

^ <

1<

1<

1<

g/L

1--

--S

um

of

BT

EX

Page 32: Cover - Attach C14f

8 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

MW

01

MW

17

MW

16

MW

19

MW

21

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

ES

1529

728

-005

ES

15297

28-0

04

ES

1529

728

-003

ES

1529728-0

02

ES

1529728-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

080:

BT

EX

N -

Co

nti

nu

ed

8N

ap

hth

ale

ne

<5

<5

<5

<5

µg

/L5

91

-20

-3

EP

074S

(SIM

) :

VO

C S

urr

og

ate

s

85.8

1.2

-Dic

hlo

roeth

an

e-D

4104

88.6

95.3

98.1

%5

01

70

60

-07

-0

EP

074S

: V

OC

Su

rro

gate

s

108

1.2

-Dic

hlo

roeth

an

e-D

4114

101

98.8

107

%5

17

06

0-0

7-0

122

To

luen

e-D

8123

107

10

31

16

%5

20

37

-26

-5

107

4-B

rom

ofl

uo

rob

en

zen

e109

93.9

90.9

100

%5

46

0-0

0-4

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

21.0

Ph

en

ol-

d6

19.2

19.0

17.9

17.9

%1

13

12

7-8

8-3

44.2

2-C

hlo

rop

hen

ol-

D4

44.6

44.2

42.0

44.2

%1

93

95

1-7

3-6

48.0

2.4

.6-T

rib

rom

op

hen

ol

44.0

33.3

41.3

34.8

%1

11

8-7

9-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

66.6

2-F

luo

rob

iph

en

yl

68.4

59.3

59.9

62.4

%1

32

1-6

0-8

54.1

An

thra

cen

e-d

10

84.6

78.9

72.1

79.2

%1

17

19

-06

-8

73.1

4-T

erp

hen

yl-

d14

71.9

69.3

68.9

65.6

%1

17

18

-51

-0

EP

080S

: T

PH

(V)/

BT

EX

Su

rro

gate

s

111

1.2

-Dic

hlo

roeth

an

e-D

4118

104

10

21

11

%2

17

06

0-0

7-0

99.6

To

luen

e-D

8100

87.6

83.9

94.7

%2

20

37

-26

-5

119

4-B

rom

ofl

uo

rob

en

zen

e120

104

10

11

11

%2

46

0-0

0-4

Page 33: Cover - Attach C14f

9 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

TB

QC

201

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

----

----

----

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529728-0

07

ES

1529728-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

----

Ars

en

ic--

----

----

----

--m

g/L

0.0

01

74

40

-38

-2

----

Cad

miu

m--

----

----

----

--m

g/L

0.0

00

17

44

0-4

3-9

----

Ch

rom

ium

----

----

----

----

mg

/L0

.00

17

44

0-4

7-3

----

Co

pp

er

----

----

----

----

mg

/L0

.00

17

44

0-5

0-8

----

Lead

----

----

----

----

mg

/L0

.00

17

43

9-9

2-1

----

Nic

kel

----

----

----

----

mg

/L0

.00

17

44

0-0

2-0

----

Zin

c--

----

----

----

--m

g/L

0.0

05

74

40

-66

-6

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

----

Merc

ury

----

----

----

----

mg

/L0

.00

01

74

39

-97

-6

EP

074D

: F

um

igan

ts

----

2.2

-Dic

hlo

rop

rop

an

e--

----

----

----

--µ

g/L

55

94

-20

-7

----

1.2

-Dic

hlo

rop

rop

an

e--

----

----

----

--µ

g/L

57

8-8

7-5

----

cis

-1.3

-Dic

hlo

rop

rop

yle

ne

----

----

----

----

µg

/L5

10

06

1-0

1-5

----

tran

s-1

.3-D

ich

loro

pro

pyle

ne

----

----

----

----

µg

/L5

10

06

1-0

2-6

----

1.2

-Dib

rom

oeth

an

e (

ED

B)

----

----

----

----

µg

/L5

10

6-9

3-4

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

----

Vin

yl ch

lori

de

----

----

----

----

µg

/L1

75

-01

-4

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

----

Dic

hlo

rod

iflu

oro

meth

an

e--

----

----

----

--µ

g/L

50

75

-71

-8

----

Ch

loro

meth

an

e--

----

----

----

--µ

g/L

50

74

-87

-3

----

Bro

mo

meth

an

e--

----

----

----

--µ

g/L

50

74

-83

-9

----

Ch

loro

eth

an

e--

----

----

----

--µ

g/L

50

75

-00

-3

----

Tri

ch

loro

flu

oro

meth

an

e--

----

----

----

--µ

g/L

50

75

-69

-4

----

1.1

-Dic

hlo

roeth

en

e--

----

----

----

--µ

g/L

57

5-3

5-4

----

Iod

om

eth

an

e--

----

----

----

--µ

g/L

57

4-8

8-4

----

tran

s-1

.2-D

ich

loro

eth

en

e--

----

----

----

--µ

g/L

51

56

-60

-5

----

1.1

-Dic

hlo

roeth

an

e--

----

----

----

--µ

g/L

57

5-3

4-3

----

cis

-1.2

-Dic

hlo

roeth

en

e--

----

----

----

--µ

g/L

51

56

-59

-2

----

1.1

.1-T

rich

loro

eth

an

e--

----

----

----

--µ

g/L

57

1-5

5-6

----

1.1

-Dic

hlo

rop

rop

yle

ne

----

----

----

----

µg

/L5

56

3-5

8-6

----

Carb

on

Tetr

ach

lori

de

----

----

----

----

µg

/L5

56

-23

-5

----

1.2

-Dic

hlo

roeth

an

e--

----

----

----

--µ

g/L

51

07

-06

-2

----

Tri

ch

loro

eth

en

e--

----

----

----

--µ

g/L

57

9-0

1-6

----

Dib

rom

om

eth

an

e--

----

----

----

--µ

g/L

57

4-9

5-3

Page 34: Cover - Attach C14f

10

of

12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

TB

QC

201

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

----

----

----

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529728-0

07

ES

1529728-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

- C

on

tin

ued

----

1.1

.2-T

rich

loro

eth

an

e--

----

----

----

--µ

g/L

57

9-0

0-5

----

1.3

-Dic

hlo

rop

rop

an

e--

----

----

----

--µ

g/L

51

42

-28

-9

----

Tetr

ach

loro

eth

en

e--

----

----

----

--µ

g/L

51

27

-18

-4

----

1.1

.1.2

-Tetr

ach

loro

eth

an

e--

----

----

----

--µ

g/L

56

30

-20

-6

----

tran

s-1

.4-D

ich

loro

-2-b

ute

ne

----

----

----

----

µg

/L5

11

0-5

7-6

----

cis

-1.4

-Dic

hlo

ro-2

-bu

ten

e--

----

----

----

--µ

g/L

51

47

6-1

1-5

----

1.1

.2.2

-Tetr

ach

loro

eth

an

e--

----

----

----

--µ

g/L

57

9-3

4-5

----

1.2

.3-T

rich

loro

pro

pan

e--

----

----

----

--µ

g/L

59

6-1

8-4

----

Pen

tach

loro

eth

an

e--

----

----

----

--µ

g/L

57

6-0

1-7

----

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

----

----

----

----

µg

/L5

96

-12

-8

----

Hexach

loro

bu

tad

ien

e--

----

----

----

--µ

g/L

58

7-6

8-3

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds

----

Ch

loro

ben

zen

e--

----

----

----

--µ

g/L

51

08

-90

-7

----

Bro

mo

ben

zen

e--

----

----

----

--µ

g/L

51

08

-86

-1

----

2-C

hlo

roto

luen

e--

----

----

----

--µ

g/L

59

5-4

9-8

----

4-C

hlo

roto

luen

e--

----

----

----

--µ

g/L

51

06

-43

-4

----

1.3

-Dic

hlo

rob

en

zen

e--

----

----

----

--µ

g/L

55

41

-73

-1

----

1.4

-Dic

hlo

rob

en

zen

e--

----

----

----

--µ

g/L

51

06

-46

-7

----

1.2

-Dic

hlo

rob

en

zen

e--

----

----

----

--µ

g/L

59

5-5

0-1

----

1.2

.4-T

rich

loro

ben

zen

e--

----

----

----

--µ

g/L

51

20

-82

-1

----

1.2

.3-T

rich

loro

ben

zen

e--

----

----

----

--µ

g/L

58

7-6

1-6

EP

074G

: T

rih

alo

meth

an

es

----

Ch

loro

form

----

----

----

----

µg

/L5

67

-66

-3

----

Bro

mo

dic

hlo

rom

eth

an

e--

----

----

----

--µ

g/L

57

5-2

7-4

----

Dib

rom

och

loro

meth

an

e--

----

----

----

--µ

g/L

51

24

-48

-1

----

Bro

mo

form

----

----

----

----

µg

/L5

75

-25

-2

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

----

Nap

hth

ale

ne

----

----

----

----

µg

/L1

91

-20

-3

----

Acen

ap

hth

yle

ne

----

----

----

----

µg

/L1

20

8-9

6-8

----

Acen

ap

hth

en

e--

----

----

----

--µ

g/L

18

3-3

2-9

----

Flu

ore

ne

----

----

----

----

µg

/L1

86

-73

-7

----

Ph

en

an

thre

ne

----

----

----

----

µg

/L1

85

-01

-8

----

An

thra

cen

e--

----

----

----

--µ

g/L

11

20

-12

-7

----

Flu

ora

nth

en

e--

----

----

----

--µ

g/L

12

06

-44

-0

Page 35: Cover - Attach C14f

11

of

12

:P

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Wo

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Clie

nt

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15

29

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8

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40

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RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

TB

QC

201

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

----

----

----

[31

-Au

g-2

01

5]

[31

-Au

g-2

01

5]

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

1529728-0

07

ES

1529728-0

06

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s -

Co

nti

nu

ed

----

Pyre

ne

----

----

----

----

µg

/L1

12

9-0

0-0

----

Ben

z(a)a

nth

racen

e--

----

----

----

--µ

g/L

15

6-5

5-3

----

Ch

rysen

e--

----

----

----

--µ

g/L

12

18

-01

-9

----

Ben

zo(b

+j)

flu

ora

nth

en

e--

----

----

----

--µ

g/L

12

05

-99

-2 2

05

-82

-3

----

Ben

zo(k

)flu

ora

nth

en

e--

----

----

----

--µ

g/L

12

07

-08

-9

----

Ben

zo(a

)pyre

ne

----

----

----

----

µg

/L0

.55

0-3

2-8

----

Ind

en

o(1

.2.3

.cd

)pyre

ne

----

----

----

----

µg

/L1

19

3-3

9-5

----

Dib

en

z(a.h

)an

thra

cen

e--

----

----

----

--µ

g/L

15

3-7

0-3

----

Ben

zo(g

.h.i)p

ery

len

e--

----

----

----

--µ

g/L

11

91

-24

-2

----

^ --

----

----

----

--µ

g/L

0.5

----

Su

m o

f p

oly

cyclic a

rom

ati

c h

yd

rocarb

on

s

----

^ --

----

----

----

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g/L

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(ze

ro)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<2

0<

20

----

----

----

µg

/L2

0--

--C

6 -

C9 F

racti

on

<5

0--

----

----

----

--µ

g/L

50

----

C10 -

C14 F

racti

on

<1

00

----

----

----

----

µg

/L1

00

----

C15 -

C28 F

racti

on

<5

0--

----

----

----

--µ

g/L

50

----

C29 -

C36 F

racti

on

<5

0^

----

----

----

----

µg

/L5

0--

--C

10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

<2

0C

6 -

C10 F

racti

on

<2

0--

----

----

--µ

g/L

20

C6

_C

10

<2

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<2

0--

----

----

--µ

g/L

20

C6

_C

10

-BT

EX

<1

00

>C

10 -

C16 F

racti

on

----

----

----

----

µg

/L1

00

>C

10

_C

16

<1

00

----

----

----

----

µg

/L1

00

----

>C

16 -

C34 F

racti

on

<1

00

----

----

----

----

µg

/L1

00

----

>C

34 -

C40 F

racti

on

<1

00

^ --

----

----

----

--µ

g/L

10

0--

-->

C10 -

C40 F

racti

on

(su

m)

<1

00

^ --

----

----

----

--µ

g/L

10

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<1

Ben

zen

e<

1--

----

----

--µ

g/L

17

1-4

3-2

<2

To

luen

e<

2--

----

----

--µ

g/L

21

08

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Eth

ylb

en

zen

e<

2--

----

----

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g/L

21

00

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<2

meta

- &

para

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ne

<2

----

----

----

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/L2

10

8-3

8-3

10

6-4

2-3

<2

ort

ho

-Xyle

ne

<2

----

----

----

µg

/L2

95

-47

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<2

^ T

ota

l X

yle

nes

<2

----

----

----

µg

/L2

13

30

-20

-7

<1

^ <

1--

----

----

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g/L

1--

--S

um

of

BT

EX

Page 36: Cover - Attach C14f

12

of

12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

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AE

CO

M A

ust

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Pty

Ltd

An

aly

tical R

esu

lts

----

----

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TB

QC

201

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

WA

TE

R

(M

atr

ix:

WA

TE

R)

----

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-Au

g-2

01

5]

[31

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g-2

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5]

Clie

nt

sam

plin

g d

ate

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1529728-0

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um

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EP

080:

BT

EX

N -

Co

nti

nu

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hth

ale

ne

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(SIM

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VO

C S

urr

og

ate

s

----

1.2

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hlo

roeth

an

e-D

4--

----

----

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50

17

06

0-0

7-0

EP

074S

: V

OC

Su

rro

gate

s

----

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hlo

roeth

an

e-D

4--

----

----

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51

70

60

-07

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----

To

luen

e-D

8--

----

----

----

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52

03

7-2

6-5

----

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rom

ofl

uo

rob

en

zen

e--

----

----

----

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54

60

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EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

----

Ph

en

ol-

d6

----

----

----

----

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13

12

7-8

8-3

----

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hlo

rop

hen

ol-

D4

----

----

----

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93

95

1-7

3-6

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rib

rom

op

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ol

----

----

----

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11

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EP

075(S

IM)T

: P

AH

Su

rro

gate

s

----

2-F

luo

rob

iph

en

yl

----

----

----

----

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32

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thra

cen

e-d

10

----

----

----

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17

19

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erp

hen

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17

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PH

(V)/

BT

EX

Su

rro

gate

s

108

1.2

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an

e-D

4110

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----

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06

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94.4

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luen

e-D

886.2

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37

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108

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ofl

uo

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0-0

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An

aly

tical R

esu

lts

De

sc

rip

tiv

e R

es

ult

s

Su

b-M

atr

ix:

SO

IL

An

aly

tica

l Re

sults

Me

tho

d:

Co

mp

ou

nd

Clie

nt

sam

ple

ID

-

Clie

nt

sam

plin

g d

ate

/ t

ime

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

EA

20

0:

De

scrip

tion

Da

rk b

row

n c

lay

soil

with

tw

o p

iece

s o

f fr

iab

le a

sbe

sto

s fib

re b

oa

rd a

pp

rox

4 x

3 x

2 m

m a

s w

ell

as

se

ve

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se b

un

dle

s o

f fr

iab

le a

sbe

sto

s fib

res

ap

pro

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x 1

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01

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EA

20

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scrip

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rk b

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ur

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est

os

cem

en

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pro

x 4

0 x

40

x 5

mm

as w

ell

as

se

vera

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f fr

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sbe

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s ce

me

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etin

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SO

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An

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tica

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tho

d:

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mp

ou

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nt

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ple

ID

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nt

sam

plin

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ate

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f b

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d a

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sto

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etin

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pp

rox 5

0 x

30

x 5

mm

.S

S0

4-F

RA

G -

[2

9-A

ug

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15

]

Page 37: Cover - Attach C14f

Fals

e 3 3

.00

Tru

e

Envir

onm

ental

QU

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OR

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This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

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esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted.

This

Qualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

La

bo

rato

ry D

up

lica

te (

DU

P)

Re

po

rt;

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce (

RP

D)

an

d A

cce

pta

nce

Lim

its

l

Me

tho

d B

lan

k (M

B)

an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

l

Ma

trix

Sp

ike

(M

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

Sig

nato

ries

This

docu

ment

has

been

ele

ctro

nic

ally

si

gned

by

the

auth

orize

d

signato

ries

indic

ate

d

belo

w.

Ele

ctro

nic

si

gnin

g

has

been

carr

ied

out

in

com

plia

nce

with

pro

cedure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

siti

on

Pa

bi S

ub

ba

Se

nio

r O

rga

nic

Ch

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ist

Syd

ne

y O

rga

nic

s

Ra

ymo

nd

Co

mm

od

ore

Inst

rum

en

t C

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s

Sh

au

n S

po

on

er

Asb

est

os

Ide

ntif

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Ne

wca

stle

- A

sbe

sto

s

NA

TA

Acc

red

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La

bo

rato

ry 8

25

Acc

red

ited

fo

r

com

plia

nce

with

ISO

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C 1

70

25

.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 38: Cover - Attach C14f

2 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

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Pty

Ltd

60

43

88

40

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RR

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S I

ND

US

TR

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roje

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Gen

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om

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ts

Th

e

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du

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use

d

by

the

E

nvi

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nta

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ivis

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h

ave

b

ee

n

de

ve

lop

ed

fr

om

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sta

blis

he

d

inte

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ally

re

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p

roce

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res

such

a

s th

ose

p

ub

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ed

b

y th

e

US

EP

A,

AP

HA

, A

S

an

d

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h

ou

se

de

velo

pe

d p

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are

em

plo

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in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

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req

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Wh

ere

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re d

ete

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as

be

en

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lts a

re r

ep

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ry w

eig

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Wh

ere

a r

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less

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an

(<

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n t

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ma

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to

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n a

nd

/or

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re t

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f a

re

po

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iffe

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sta

nd

ard

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R,

this

ma

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e d

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hig

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ois

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insu

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mp

le (

red

uce

d w

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ht

em

plo

yed

) o

r m

atr

ix in

terf

ere

nce

.

An

on

ymo

us

= R

efe

rs t

o s

am

ple

s w

hic

h a

re n

ot

spe

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rt o

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ork

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er

bu

t fo

rme

d p

art

of

the

QC

pro

cess

lot

CA

S N

um

be

r =

CA

S r

eg

istr

y n

um

be

r fr

om

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ase

ma

inta

ine

d b

y C

he

mic

al A

bst

ract

s S

erv

ice

s. T

he

Ch

em

ica

l A

bstr

acts

Se

rvic

e is

a d

ivis

ion

of

the

Am

erica

n C

he

mic

al S

oci

ety

.

LO

R =

Lim

it o

f re

po

rtin

g

RP

D =

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce

#

= I

nd

ica

tes

faile

d Q

C

Ke

y :

Page 39: Cover - Attach C14f

3 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Lab

ora

tory

Du

plicate

(D

UP

) R

ep

ort

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

D

up

lica

te

refe

rs

to

a

ran

do

mly

se

lect

ed

in

tra

lab

ora

tory

sp

lit.

La

bo

rato

ry

du

plic

ate

s

pro

vid

e

info

rma

tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

ed

ra

ng

es

for

the

R

ela

tive

P

erc

en

t D

evi

atio

n

(RP

D)

of

La

bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:-

0%

- 5

0%

; R

esu

lt >

20

tim

es L

OR

:0%

- 2

0%

.

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S (Q

C L

ot:

202036)

EG

02

0A

-F:

Ca

dm

ium

74

40

-43

-90

.00

01

mg

/L0

.00

02

<0

.00

01

66

.9N

o L

imit

MW

21

E

S1

52

97

28

-00

1

EG

02

0A

-F:

Ars

en

ic7

44

0-3

8-2

0.0

01

mg

/L0

.00

10

.00

10

.00

No

Lim

it

EG

02

0A

-F:

Ch

rom

ium

74

40

-47

-30

.00

1m

g/L

<0

.00

1<

0.0

01

0.0

0N

o L

imit

EG

02

0A

-F:

Co

pp

er

74

40

-50

-80

.00

1m

g/L

0.0

01

0.0

01

0.0

0N

o L

imit

EG

02

0A

-F:

Le

ad

74

39

-92

-10

.00

1m

g/L

<0

.00

1<

0.0

01

0.0

0N

o L

imit

EG

02

0A

-F:

Nic

kel

74

40

-02

-00

.00

1m

g/L

0.0

04

0.0

04

0.0

0N

o L

imit

EG

02

0A

-F:

Zin

c7

44

0-6

6-6

0.0

05

mg

/L0

.06

60

.07

18

.28

0%

- 5

0%

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

(Q

C L

ot:

202037)

EG

03

5F

: M

erc

ury

74

39

-97

-60

.00

01

mg

/L<

0.0

00

1<

0.0

00

10

.00

No

Lim

itM

W1

9

ES

15

29

72

8-0

02

EP

074D

: F

um

igan

ts (Q

C L

ot:

203729)

EP

07

4:

1.2

-Dib

rom

oe

tha

ne

(E

DB

)1

06

-93

-45

µg

/L<

5<

50

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

07

4:

1.2

-Dic

hlo

rop

rop

an

e7

8-8

7-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

2.2

-Dic

hlo

rop

rop

an

e5

94

-20

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

cis-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

1-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

2-6

g/L

<5

<5

0.0

0N

o L

imit

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

203730)

EP

07

4E

(SIM

): V

inyl

ch

lorid

e7

5-0

1-4

g/L

<1

<1

0.0

0N

o L

imit

MW

21

E

S1

52

97

28

-00

1

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

203729)

EP

07

4:

1.1

.1.2

-Te

tra

ch

loro

eth

an

e6

30

-20

-65

µg

/L<

5<

50

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

07

4:

1.1

.1-T

rich

loro

eth

an

e7

1-5

5-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2.2

-Te

tra

ch

loro

eth

an

e7

9-3

4-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

.2-T

rich

loro

eth

an

e7

9-0

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.1

-Dic

hlo

roe

tha

ne

75

-34

-35

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.1

-Dic

hlo

roe

the

ne

75

-35

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.1

-Dic

hlo

rop

rop

yle

ne

56

3-5

8-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

.3-T

rich

loro

pro

pa

ne

96

-18

-45

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

96

-12

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.2

-Dic

hlo

roe

tha

ne

10

7-0

6-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rop

rop

an

e1

42

-28

-95

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Ca

rbo

n T

etr

ach

lorid

e5

6-2

3-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

cis-

1.2

-Dic

hlo

roe

the

ne

15

6-5

9-2

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

cis-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

47

6-1

1-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Dib

rom

om

eth

an

e7

4-9

5-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

He

xach

loro

bu

tad

ien

e8

7-6

8-3

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Iod

om

eth

an

e7

4-8

8-4

g/L

<5

<5

0.0

0N

o L

imit

Page 40: Cover - Attach C14f

4 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

C L

ot:

203729)

- c

on

tin

ued

EP

07

4:

Pe

nta

chlo

roe

tha

ne

76

-01

-75

µg

/L<

5<

50

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

07

4:

Te

tra

chlo

roe

the

ne

12

7-1

8-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.2

-Dic

hlo

roe

the

ne

15

6-6

0-5

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

tra

ns-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

10

-57

-65

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Trich

loro

eth

en

e7

9-0

1-6

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Bro

mo

me

tha

ne

74

-83

-95

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Ch

loro

eth

an

e7

5-0

0-3

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

07

4:

Ch

loro

me

tha

ne

74

-87

-35

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Dic

hlo

rod

iflu

oro

me

tha

ne

75

-71

-85

g/L

<5

0<

50

0.0

0N

o L

imit

EP

07

4:

Trich

loro

fluo

rom

eth

an

e7

5-6

9-4

50

µg

/L<

50

<5

00

.00

No

Lim

it

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds (Q

C L

ot:

203729)

EP

07

4:

1.2

.3-T

rich

loro

be

nze

ne

87

-61

-65

µg

/L<

5<

50

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

07

4:

1.2

.4-T

rich

loro

be

nze

ne

12

0-8

2-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.2

-Dic

hlo

rob

en

zen

e9

5-5

0-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

1.3

-Dic

hlo

rob

en

zen

e5

41

-73

-15

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

1.4

-Dic

hlo

rob

en

zen

e1

06

-46

-75

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

2-C

hlo

roto

lue

ne

95

-49

-85

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

4-C

hlo

roto

lue

ne

10

6-4

3-4

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Bro

mo

be

nze

ne

10

8-8

6-1

g/L

<5

<5

0.0

0N

o L

imit

EP

07

4:

Ch

loro

be

nze

ne

10

8-9

0-7

g/L

<5

<5

0.0

0N

o L

imit

EP

074G

: T

rih

alo

meth

an

es (Q

C L

ot:

203729)

EP

07

4:

Bro

mo

dic

hlo

rom

eth

an

e7

5-2

7-4

g/L

<5

<5

0.0

0N

o L

imit

MW

21

E

S1

52

97

28

-00

1

EP

07

4:

Bro

mo

form

75

-25

-25

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Ch

loro

form

67

-66

-35

µg

/L<

5<

50

.00

No

Lim

it

EP

07

4:

Dib

rom

och

loro

me

tha

ne

12

4-4

8-1

g/L

<5

<5

0.0

0N

o L

imit

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

203728)

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

203728)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

MW

21

E

S1

52

97

28

-00

1

EP

080:

BT

EX

N (Q

C L

ot:

203728)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itM

W2

1

ES

15

29

72

8-0

01

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

88

0.0

0N

o L

imit

Page 41: Cover - Attach C14f

5 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

am

ple

(L

CS

) re

fers

to

a

ce

rtifi

ed

re

fere

nce

m

ate

ria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S (Q

CL

ot:

202036)

EG

02

0A

-F:

Ars

en

ic7

44

0-3

8-2

0.0

01

mg

/L<

0.0

01

90

.80

.1 m

g/L

11

58

5

EG

02

0A

-F:

Ca

dm

ium

74

40

-43

-90

.00

01

mg

/L<

0.0

00

19

6.2

0.1

mg

/L1

15

85

EG

02

0A

-F:

Ch

rom

ium

74

40

-47

-30

.00

1m

g/L

<0

.00

19

2.3

0.1

mg

/L1

15

85

EG

02

0A

-F:

Co

pp

er

74

40

-50

-80

.00

1m

g/L

<0

.00

19

8.3

0.1

mg

/L1

15

85

EG

02

0A

-F:

Le

ad

74

39

-92

-10

.00

1m

g/L

<0

.00

18

9.4

0.1

mg

/L1

15

85

EG

02

0A

-F:

Nic

kel

74

40

-02

-00

.00

1m

g/L

<0

.00

19

4.1

0.1

mg

/L1

15

85

EG

02

0A

-F:

Zin

c7

44

0-6

6-6

0.0

05

mg

/L<

0.0

05

94

.00

.1 m

g/L

11

58

5

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

(Q

CL

ot:

202037)

EG

03

5F

: M

erc

ury

74

39

-97

-60

.00

01

mg

/L<

0.0

00

19

7.2

0.0

1 m

g/L

11

47

8

EP

074D

: F

um

igan

ts (Q

CL

ot:

203729)

EP

07

4:

1.2

-Dib

rom

oe

tha

ne

(E

DB

)1

06

-93

-45

µg

/L<

59

0.6

10

µg

/L1

17

69

EP

07

4:

1.2

-Dic

hlo

rop

rop

an

e7

8-8

7-5

g/L

<5

91

.41

0 µ

g/L

12

07

6

EP

07

4:

2.2

-Dic

hlo

rop

rop

an

e5

94

-20

-75

µg

/L<

59

0.6

10

µg

/L1

19

61

EP

07

4:

cis-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

1-5

g/L

<5

11

31

0 µ

g/L

12

06

2

EP

07

4:

tra

ns-

1.3

-Dic

hlo

rop

rop

yle

ne

10

06

1-0

2-6

g/L

<5

92

.41

0 µ

g/L

11

96

1

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

203730)

EP

07

4E

(SIM

): V

inyl

ch

lorid

e7

5-0

1-4

g/L

<1

11

41

0 µ

g/L

13

16

7

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

203729)

EP

07

4:

1.1

.1.2

-Te

tra

chlo

roe

tha

ne

63

0-2

0-6

g/L

<5

95

.11

0 µ

g/L

11

46

6

EP

07

4:

1.1

.1-T

rich

loro

eth

an

e7

1-5

5-6

g/L

<5

84

.31

0 µ

g/L

11

96

1

EP

07

4:

1.1

.2.2

-Te

tra

chlo

roe

tha

ne

79

-34

-55

µg

/L<

59

5.2

10

µg

/L1

24

70

EP

07

4:

1.1

.2-T

rich

loro

eth

an

e7

9-0

0-5

g/L

<5

10

21

0 µ

g/L

12

37

5

EP

07

4:

1.1

-Dic

hlo

roe

tha

ne

75

-34

-35

µg

/L<

59

1.9

10

µg

/L1

19

75

EP

07

4:

1.1

-Dic

hlo

roe

the

ne

75

-35

-45

µg

/L<

59

3.9

10

µg

/L1

23

69

EP

07

4:

1.1

-Dic

hlo

rop

rop

yle

ne

56

3-5

8-6

g/L

<5

90

.21

0 µ

g/L

11

97

3

EP

07

4:

1.2

.3-T

rich

loro

pro

pa

ne

96

-18

-45

µg

/L<

59

2.2

10

µg

/L1

28

74

EP

07

4:

1.2

-Dib

rom

o-3

-ch

loro

pro

pa

ne

96

-12

-85

µg

/L<

51

02

10

µg

/L1

36

66

EP

07

4:

1.2

-Dic

hlo

roe

tha

ne

10

7-0

6-2

g/L

<5

89

.01

0 µ

g/L

12

27

8

EP

07

4:

1.3

-Dic

hlo

rop

rop

an

e1

42

-28

-95

µg

/L<

59

6.7

10

µg

/L1

21

79

EP

07

4:

Bro

mo

me

tha

ne

74

-83

-95

g/L

<5

08

9.7

10

0 µ

g/L

14

05

6

EP

07

4:

Ca

rbo

n T

etr

ach

lorid

e5

6-2

3-5

g/L

<5

91

.11

0 µ

g/L

12

16

3

EP

07

4:

Ch

loro

eth

an

e7

5-0

0-3

50

µg

/L<

50

10

71

00

µg

/L1

35

63

EP

07

4:

Ch

loro

me

tha

ne

74

-87

-35

g/L

<5

06

9.7

10

0 µ

g/L

13

06

7

EP

07

4:

cis-

1.2

-Dic

hlo

roe

the

ne

15

6-5

9-2

g/L

<5

92

.01

0 µ

g/L

11

77

7

Page 42: Cover - Attach C14f

6 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

074E

: H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

203729)

- c

on

tin

ued

EP

07

4:

cis-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

47

6-1

1-5

g/L

<5

76

.91

0 µ

g/L

12

87

1

EP

07

4:

Dib

rom

om

eth

an

e7

4-9

5-3

g/L

<5

91

.61

0 µ

g/L

11

87

4

EP

07

4:

Dic

hlo

rod

iflu

oro

me

tha

ne

75

-71

-85

g/L

<5

07

2.1

10

0 µ

g/L

13

86

1

EP

07

4:

He

xach

loro

bu

tad

ien

e8

7-6

8-3

g/L

<5

91

.51

0 µ

g/L

13

25

8

EP

07

4:

Iod

om

eth

an

e7

4-8

8-4

g/L

<5

76

.31

0 µ

g/L

12

87

0

EP

07

4:

Pe

nta

chlo

roe

tha

ne

76

-01

-75

µg

/L<

51

11

10

µg

/L1

26

72

EP

07

4:

Te

tra

chlo

roe

the

ne

12

7-1

8-4

g/L

<5

79

.41

0 µ

g/L

12

47

2

EP

07

4:

tra

ns-

1.2

-Dic

hlo

roe

the

ne

15

6-6

0-5

g/L

<5

93

.61

0 µ

g/L

11

97

1

EP

07

4:

tra

ns-

1.4

-Dic

hlo

ro-2

-bu

ten

e1

10

-57

-65

µg

/L<

57

6.3

10

µg

/L1

20

60

EP

07

4:

Trich

loro

eth

en

e7

9-0

1-6

g/L

<5

87

.91

0 µ

g/L

12

07

4

EP

07

4:

Trich

loro

fluo

rom

eth

an

e7

5-6

9-4

50

µg

/L<

50

90

.11

00

µg

/L1

31

65

EP

074F

: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds (Q

CL

ot:

203729)

EP

07

4:

1.2

.3-T

rich

loro

be

nze

ne

87

-61

-65

µg

/L<

58

6.6

10

µg

/L1

25

67

EP

07

4:

1.2

.4-T

rich

loro

be

nze

ne

12

0-8

2-1

g/L

<5

87

.71

0 µ

g/L

12

66

0

EP

07

4:

1.2

-Dic

hlo

rob

en

zen

e9

5-5

0-1

g/L

<5

87

.91

0 µ

g/L

11

77

7

EP

07

4:

1.3

-Dic

hlo

rob

en

zen

e5

41

-73

-15

µg

/L<

58

9.6

10

µg

/L1

20

74

EP

07

4:

1.4

-Dic

hlo

rob

en

zen

e1

06

-46

-75

µg

/L<

58

9.8

10

µg

/L1

20

72

EP

07

4:

2-C

hlo

roto

lue

ne

95

-49

-85

µg

/L<

59

0.8

10

µg

/L1

21

71

EP

07

4:

4-C

hlo

roto

lue

ne

10

6-4

3-4

g/L

<5

92

.11

0 µ

g/L

12

17

1

EP

07

4:

Bro

mo

be

nze

ne

10

8-8

6-1

g/L

<5

90

.81

0 µ

g/L

11

67

6

EP

07

4:

Ch

loro

be

nze

ne

10

8-9

0-7

g/L

<5

90

.81

0 µ

g/L

11

88

0

EP

074G

: T

rih

alo

meth

an

es (Q

CL

ot:

203729)

EP

07

4:

Bro

mo

dic

hlo

rom

eth

an

e7

5-2

7-4

g/L

<5

92

.11

0 µ

g/L

11

86

4

EP

07

4:

Bro

mo

form

75

-25

-25

µg

/L<

51

02

10

µg

/L1

26

74

EP

07

4:

Ch

loro

form

67

-66

-35

µg

/L<

59

4.5

10

µg

/L1

18

76

EP

07

4:

Dib

rom

och

loro

me

tha

ne

12

4-4

8-1

g/L

<5

10

21

0 µ

g/L

11

56

5

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

202083)

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-91

µg

/L<

1.0

78

.65

µg

/L1

13

62

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-81

µg

/L<

1.0

84

.95

µg

/L1

14

64

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-71

µg

/L<

1.0

10

15

µg

/L1

16

64

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-31

µg

/L<

1.0

85

.25

µg

/L1

17

64

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5µ

g/L

<0

.59

7.8

5 µ

g/L

11

76

3

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

g/L

<1

.09

0.6

5 µ

g/L

11

96

2

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-21

µg

/L<

1.0

10

05

µg

/L1

18

59

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

g/L

<1

.09

3.7

5 µ

g/L

11

76

2

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

g/L

<1

.01

02

5 µ

g/L

11

66

3

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-31

µg

/L<

1.0

10

05

µg

/L1

17

61

Page 43: Cover - Attach C14f

7 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Su

b-M

atr

ix:

WA

TE

RM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

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ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

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ike R

eco

very

(%

)R

eco

very

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its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

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mp

ou

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CA

S N

um

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LO

RU

nit

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

202083)

- c

on

tin

ued

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-01

µg

/L<

1.0

10

15

µg

/L1

18

64

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-71

µg

/L<

1.0

85

.45

µg

/L1

15

64

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

g/L

<1

.01

00

5 µ

g/L

11

86

0

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

g/L

<1

.06

6.6

5 µ

g/L

11

95

9

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-81

µg

/L<

1.0

88

.15

µg

/L1

16

63

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-01

µg

/L<

1.0

10

95

µg

/L1

18

63

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

202084)

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

µg

/L<

50

95

.22

00

0 µ

g/L

12

95

9

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

g/L

<1

00

96

.63

00

0 µ

g/L

13

17

1

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

50

µg

/L<

50

92

.82

00

0 µ

g/L

12

06

2

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

203728)

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

88

.62

60

µg

/L1

27

75

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

202084)

EP

07

1:

>C

10

- C

16

Fra

ctio

n>

C1

0_

C1

61

00

µg

/L<

10

09

2.7

25

00

µg

/L1

31

59

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

µg

/L<

10

09

8.0

35

00

µg

/L1

38

74

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

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/L<

10

09

5.8

15

00

µg

/L1

27

67

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

203728)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

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09

4.2

31

0 µ

g/L

12

77

5

EP

080:

BT

EX

N (Q

CL

ot:

203728)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

18

4.0

10

µg

/L1

24

70

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

28

4.7

10

µg

/L1

20

70

EP

08

0:

me

ta-

& p

ara

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Matr

ix S

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MS

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alit

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atr

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S)

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o

f th

is

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ara

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ter

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ote

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70

Page 44: Cover - Attach C14f

8 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

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ralia

Pty

Ltd

60

43

88

40

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RR

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TR

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b-M

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ix:

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TE

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MS

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ikeR

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%)

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70

74

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inc

# N

ot

De

term

ine

d

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30

70

EG

035F

: D

isso

lved

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ury

by F

IMS

(Q

CL

ot:

202037)

MW

21

E

S1

52

97

28

-00

17

43

9-9

7-6

EG

03

5F

: M

erc

ury

93

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/L1

30

70

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds (Q

CL

ot:

203730)

MW

21

E

S1

52

97

28

-00

17

5-0

1-4

EP

07

4E

(SIM

): V

inyl

ch

lorid

e1

13

25

µg

/L1

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70

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: H

alo

gen

ate

d A

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c C

om

po

un

ds (Q

CL

ot:

203729)

MW

21

E

S1

52

97

28

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17

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5-4

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07

4:

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ne

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13

07

0

79

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74

: T

rich

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en

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25

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70

EP

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: H

alo

gen

ate

d A

rom

ati

c C

om

po

un

ds (Q

CL

ot:

203729)

MW

21

E

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52

97

28

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11

08

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74

: C

hlo

rob

en

zen

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25

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70

EP

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71:

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tal P

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um

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on

s (Q

CL

ot:

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MW

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97

28

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80

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ctio

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NE

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28

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80

: C

6 -

C1

0 F

ract

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99

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75

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70

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N (Q

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203728)

MW

21

E

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52

97

28

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17

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08

0:

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nze

ne

84

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13

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0

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ylb

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25

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70

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& p

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90

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13

07

0

Page 45: Cover - Attach C14f

Tru

e

Envir

onm

ental

QA

/QC

Co

mp

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ss

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:1

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ST

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KA

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r60438840/1

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o.

of

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lyse

d:10

Th

is r

ep

ort

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uto

mati

cally g

en

era

ted

by t

he A

LS

LIM

S t

hro

ug

h in

terp

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e A

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Qu

ality

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ep

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ce p

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rs m

easu

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LS

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his

au

tom

ate

d

rep

ort

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data

valid

ati

on

an

d is d

esig

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to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

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tlie

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Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

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hig

hlig

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ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

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ntr

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QC

) R

ep

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.

l

NO

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od

Bla

nk v

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e o

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l

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Du

plicate

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tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

Matr

ix S

pik

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exis

t -

ple

ase s

ee f

ollo

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g p

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or

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l

Fo

r all r

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Ou

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qu

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qu

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R I

G H

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S O

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|

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T

P A

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N E

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Page 46: Cover - Attach C14f

2 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

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Ltd

60

43

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40

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S I

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TR

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roje

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Ou

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Qu

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aly

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um

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term

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qu

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: W

AT

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Qualit

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ation

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am

ple

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e

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od

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te (

%)

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am

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nt

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d A

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qu

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nt

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nt

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/MS

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Th

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su

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xtra

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d

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SW

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xtra

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su

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en

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d r

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if a

ny)

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r le

ach

ate

m

eth

od

s (e

.g.

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ry

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ord

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to

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aly

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ort

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ess

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ach

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ort

est

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na

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h

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for

the

e

qu

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len

t so

il m

eth

od

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he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

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the

r m

eta

ls 1

80

da

ys.

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rea

ch d

oe

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ara

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ach

fo

r a

ll n

on

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ters

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ldin

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time

s fo

r V

OC

in

so

ils

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cco

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g

to

an

aly

tes

of

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yl

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7

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ach

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fo

r a

ll V

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na

lyte

s

an

d

sho

uld

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ve

rifie

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ca

se t

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re

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als

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Date

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2004 Id

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rea

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ho

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aly

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ratio

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Date

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od

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nD

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fo

r a

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an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

bu

lk s

am

ple

s

Sn

ap

Lo

ck B

ag

- S

ep

ara

te b

ag

receiv

ed

(E

A200)

SS

04

-FR

AG

25

-Fe

b-2

01

6--

--08-S

ep

-20

15

----

29-A

ug

-2015

----

üM

atr

ix:

WA

TE

RE

valu

atio

n: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

Page 47: Cover - Attach C14f

3 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EG

020F

: D

isso

lved

Meta

ls b

y IC

P-M

S

Cle

ar

Pla

sti

c B

ott

le -

Nit

ric A

cid

; F

ilte

red

(E

G020A

-F)

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

27

-Fe

b-2

01

6--

--03-S

ep

-20

15

----

31-A

ug

-2015

----

ü

EG

035F

: D

isso

lved

Merc

ury

by F

IMS

Cle

ar

Pla

sti

c B

ott

le -

Nit

ric A

cid

; F

ilte

red

(E

G035F

)

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

28

-Se

p-2

01

5--

--07-S

ep

-20

15

----

31-A

ug

-2015

----

ü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P071)

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

,Q

C2

01

13

-Oct-

20

15

07

-Se

p-2

01

507-S

ep

-20

15

03-S

ep

-2015

31-A

ug

-2015

üü

EP

074D

: F

um

igan

ts

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074)

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

14

-Se

p-2

01

51

4-S

ep

-20

15

05-S

ep

-20

15

05-S

ep

-2015

31-A

ug

-2015

üü

EP

074E

(SIM

): H

alo

gen

ate

d A

lip

hati

c C

om

po

un

ds

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P074E

(SIM

))

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

14

-Se

p-2

01

51

4-S

ep

-20

15

05-S

ep

-20

15

05-S

ep

-2015

31-A

ug

-2015

üü

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

Am

ber

Gla

ss B

ott

le -

Un

pre

serv

ed

(E

P075(S

IM))

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

13

-Oct-

20

15

07

-Se

p-2

01

507-S

ep

-20

15

03-S

ep

-2015

31-A

ug

-2015

üü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

MW

21

,M

W1

9,

MW

16

,M

W1

7,

MW

01

,Q

C2

01

,

TB

14

-Se

p-2

01

51

4-S

ep

-20

15

05-S

ep

-20

15

05-S

ep

-2015

31-A

ug

-2015

üü

Page 48: Cover - Attach C14f

4 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Qu

ality

Co

ntr

ol P

ara

mete

r F

req

uen

cy C

om

plian

ce

Th

e f

ollo

win

g r

ep

ort

su

mm

arise

s th

e f

req

ue

ncy

of

lab

ora

tory

QC

sa

mp

les

an

aly

sed

with

in t

he

an

aly

tica

l lo

t(s)

in

wh

ich

th

e s

ub

mitt

ed

sa

mp

le(s

) w

as(

we

re)

pro

cess

ed

. A

ctu

al r

ate

sh

ou

ld b

e g

rea

ter

tha

n o

r e

qu

al t

o

the

exp

ect

ed

ra

te.

A li

stin

g o

f b

rea

che

s is

pro

vid

ed

in t

he

Su

mm

ary

of

Ou

tlie

rs.

Ma

trix

: W

AT

ER

Eva

lua

tio

n: û

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy

no

t w

ithin

sp

eci

fica

tion

; ü

= Q

ua

lity

Co

ntr

ol f

req

ue

ncy w

ithin

sp

ecifi

ca

tion

.

Qu

alit

y C

on

tro

l Sp

ecifi

ca

tion

Qualit

y C

ontr

ol S

am

ple

Typ

e

Exp

ecte

dQ

CR

eg

ula

rA

ctu

al

Ra

te (

%)

Qualit

y C

ontr

ol S

am

ple

Typ

eC

ou

nt

Eva

lua

tio

nA

na

lytic

al M

eth

od

sM

eth

od

La

bo

rato

ry D

up

lica

tes

(DU

P)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 1

0.0

01

Dis

solv

ed

Me

rcu

ry b

y F

IMS

EG

03

5F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 1

0.0

01

Dis

solv

ed

Me

tals

by

ICP

-MS

- S

uite

AE

G0

20

A-F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

0.0

0 1

0.0

00

PA

H/P

he

no

ls (

GC

/MS

- S

IM)

EP

07

5(S

IM)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

0.0

0 1

0.0

00

10

ûT

RH

- S

em

ivo

latil

e F

ract

ion

EP

07

1

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

14.2

9 1

0.0

01

TR

H V

ola

tile

s/B

TE

XE

P0

80

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 1

0.0

01

Vin

yl C

hlo

rid

e L

ow

leve

lE

P0

74

E(S

IM)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 1

0.0

01

Vo

latil

e O

rga

nic

Co

mp

ou

nd

sE

P0

74

La

bo

rato

ry C

on

tro

l Sa

mp

les

(LC

S)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

erc

ury

by

FIM

SE

G0

35

F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

eta

ls b

y IC

P-M

S -

Su

ite A

EG

02

0A

-F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

11.1

1 5

.00

19

üP

AH

/Ph

en

ols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

10.0

0 5

.00

11

TR

H -

Se

miv

ola

tile

Fra

ctio

nE

P0

71

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

14.2

9 5

.00

17

üT

RH

Vo

latile

s/B

TE

XE

P0

80

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üV

inyl

Ch

lorid

e L

ow

leve

lE

P0

74

E(S

IM)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üV

ola

tile

Org

an

ic C

om

po

un

ds

EP

07

4

Me

tho

d B

lan

ks (

MB

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

erc

ury

by

FIM

SE

G0

35

F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

eta

ls b

y IC

P-M

S -

Su

ite A

EG

02

0A

-F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

11.1

1 5

.00

19

üP

AH

/Ph

en

ols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

10.0

0 5

.00

11

TR

H -

Se

miv

ola

tile

Fra

ctio

nE

P0

71

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

14.2

9 5

.00

17

üT

RH

Vo

latile

s/B

TE

XE

P0

80

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üV

inyl

Ch

lorid

e L

ow

leve

lE

P0

74

E(S

IM)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üV

ola

tile

Org

an

ic C

om

po

un

ds

EP

07

4

Ma

trix

Sp

ike

s (M

S)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

erc

ury

by

FIM

SE

G0

35

F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

S3

re

qu

ire

me

nt

20.0

0 5

.00

15

üD

isso

lve

d M

eta

ls b

y IC

P-M

S -

Su

ite A

EG

02

0A

-F

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

QC

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re

qu

ire

me

nt

0.0

0 5

.00

09

ûP

AH

/Ph

en

ols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)

NE

PM

20

13

S

che

du

le B

(3)

an

d A

LS

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S3

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qu

ire

me

nt

0.0

0 5

.00

01

TR

H -

Se

miv

ola

tile

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ctio

nE

P0

71

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PM

20

13

S

che

du

le B

(3)

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d A

LS

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qu

ire

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nt

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9 5

.00

17

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RH

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latile

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TE

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P0

80

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PM

20

13

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che

du

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ire

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0 5

.00

15

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inyl

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lorid

e L

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74

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13

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0 5

.00

15

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ola

tile

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an

ic C

om

po

un

ds

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07

4

Page 49: Cover - Attach C14f

5 o

f 5

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

15

29

72

8

AE

CO

M A

ust

ralia

Pty

Ltd

60

43

88

40

/1.1

BU

RR

OW

S I

ND

US

TR

IAL

:P

roje

ct

Bri

ef

Meth

od

Su

mm

ari

es

Th

e a

na

lytic

al p

roce

du

res

use

d b

y th

e E

nvi

ron

me

nta

l Div

isio

n h

ave

be

en

de

velo

pe

d f

rom

est

ab

lish

ed

in

tern

atio

na

lly r

eco

gn

ize

d p

roce

du

res s

uch

as

tho

se p

ub

lish

ed

by

the

US

EP

A,

AP

HA

, A

S a

nd

NE

PM

. In

ho

use

de

velo

pe

d p

roce

du

res

are

em

plo

yed

in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Th

e f

ollo

win

g r

ep

ort

pro

vid

es

brie

f d

esc

rip

tio

ns

of

the

an

aly

tica

l pro

ced

ure

s e

mp

loye

d f

or

resu

lts r

ep

ort

ed

in t

he

Ce

rtifi

cate

of

An

aly

sis.

So

urc

es

fro

m w

hic

h A

LS

me

tho

ds

ha

ve b

ee

n d

eve

lop

ed

are

pro

vid

ed

with

in t

he

Me

tho

d D

esc

rip

tion

s.

An

aly

tica

l Me

tho

ds

Me

tho

d D

esc

rip

tion

sM

atr

ixM

eth

od

AS

4964 -

2004 M

eth

od for

the q

ualit

ativ

e id

entific

atio

n o

f asb

est

os

in b

ulk

sam

ple

s

Analy

sis

by

Pola

rise

d L

ight M

icro

scopy

incl

udin

g d

ispers

ion s

tain

ing

Asb

est

os

Identif

icatio

n in

Soils

EA

20

0S

OIL

AS

4964 -

2004 M

eth

od for

the q

ualit

ativ

e id

entif

icatio

n o

f asb

est

os

in b

ulk

sam

ple

s

Analy

sis

by

Pola

rise

d L

ight M

icro

scopy

incl

udin

g d

ispers

ion s

tain

ing

Asb

est

os

Identif

icatio

n in

Bulk

Solid

sE

A2

00

SO

LID

In h

ouse

: R

efe

rence

d to A

PH

A 3

125; U

SE

PA

SW

846 -

6020, A

LS

QW

I-E

N/E

G020. S

am

ple

s are

0.4

5 u

m filt

ere

d

prior

to a

naly

sis.

T

he IC

PM

S tech

niq

ue u

tiliz

es

a h

ighly

effic

ient arg

on p

lasm

a to io

niz

e s

ele

cted e

lem

ents

. Io

ns

are

then p

ass

ed in

to a

hig

h v

acu

um

mass

spect

rom

ete

r, w

hic

h s

epara

tes

the a

naly

tes

base

d o

n their d

istin

ct

mass

to c

harg

e r

atio

s prior

to their m

easu

rem

ent by

a d

iscr

ete

dyn

ode io

n d

ete

ctor.

Dis

solv

ed M

eta

ls b

y IC

P-M

S -

Suite

AE

G0

20

A-F

WA

TE

R

In h

ouse

: R

efe

rence

d to A

S 3

550, A

PH

A 3

112 H

g -

B (

Flo

w-inje

ctio

n (

SnC

l2)(

Cold

Vapour

genera

tion)

AA

S)

Sam

ple

s are

0.4

5 u

m filt

ere

d p

rior

to a

naly

sis.

F

IM-A

AS

is a

n a

uto

mate

d fla

mele

ss a

tom

ic a

bso

rptio

n

tech

niq

ue. A

bro

mate

/bro

mid

e r

eagent is

use

d to o

xidis

e a

ny

org

anic

merc

ury

com

pounds

in the filt

ere

d s

am

ple

.

The io

nic

merc

ury

is r

educe

d o

nlin

e to a

tom

ic m

erc

ury

vapour

by

SnC

l2 w

hic

h is

then p

urg

ed in

to a

heate

d q

uart

z

cell.

Q

uantif

icatio

n is

by

com

paring a

bso

rbance

again

st a

calib

ratio

n c

urv

e. T

his

meth

od is

com

plia

nt w

ith

NE

PM

(2013)

Sch

edule

B(3

)

Dis

solv

ed M

erc

ury

by

FIM

SE

G0

35

FW

AT

ER

US

EP

A S

W 8

46 -

8015A

T

he s

am

ple

ext

ract

is a

naly

sed b

y C

apill

ary

GC

/FID

and q

uantif

icatio

n is

by

com

pariso

n

again

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e o

f n-A

lkane s

tandard

s. T

his

meth

od is

com

plia

nt w

ith the Q

C

requirem

ents

of N

EP

M (

2013)

Sch

edule

B(3

)

TR

H -

Sem

ivola

tile F

ract

ion

EP

07

1W

AT

ER

US

EP

A S

W 8

46 -

8260B

W

ate

r sa

mple

s are

direct

ly p

urg

ed p

rior

to a

naly

sis

by

Capill

ary

GC

/MS

and

quantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith

NE

PM

(2013)

Sch

edule

B(3

)

Vola

tile O

rganic

Com

pounds

EP

07

4W

AT

ER

(US

EP

A S

W 8

46 -

8260B

, A

LS

QW

I-O

RG

/EP

074)

Wate

r sa

mple

s are

direct

ly p

urg

ed (

ALS

QW

I-O

RG

/16)

prior

to

analy

sis

by

Capill

ary

GC

/MS

. Q

uantit

atio

n is

ach

ieve

d u

sing in

tern

al s

tandard

and a

vera

ge r

esp

onse

fact

or

quantit

atio

n tech

niq

ues

again

st a

n e

stablis

hed fiv

e p

oin

t cu

rve.

Vin

yl C

hlo

ride L

ow

leve

lE

P0

74

E(S

IM)

WA

TE

R

US

EP

A S

W 8

46 -

8270D

S

am

ple

ext

ract

s are

analy

sed b

y C

apill

ary

GC

/MS

in S

IM M

ode a

nd q

uantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. T

his

meth

od is

com

plia

nt w

ith N

EP

M (

2013)

Sch

edule

B(3

)

PA

H/P

henols

(G

C/M

S -

SIM

)E

P0

75

(SIM

)W

AT

ER

US

EP

A S

W 8

46 -

8260B

W

ate

r sa

mple

s are

direct

ly p

urg

ed p

rior

to a

naly

sis

by

Capill

ary

GC

/MS

and

quantif

icatio

n is

by

com

pariso

n a

gain

st a

n e

stablis

hed 5

poin

t ca

libra

tion c

urv

e. A

ltern

ativ

ely

, a s

am

ple

is

equili

bra

ted in

a h

eadsp

ace

via

l and a

port

ion o

f th

e h

eadsp

ace

dete

rmin

ed b

y G

CM

S a

naly

sis.

T

his

meth

od is

com

plia

nt w

ith the Q

C r

equirem

ents

of N

EP

M (

2013)

Sch

edule

B(3

)

TR

H V

ola

tiles/

BT

EX

EP

08

0W

AT

ER

Page 50: Cover - Attach C14f

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1529728

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR ALEX LATHAM Barbara Hanna

:: AddressAddress LEVEL 21, 420 George Street

SYDNEY NSW 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8555

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60438840/1.1 BURROWS

INDUSTRIAL

Page 1 of 3

:Order number 60438840/1.1 :Quote number EB2015AECOMAU0580 (EN/004/15)

:C-O-C number ---- :QC Level NEPM 2013 Schedule B(3) and ALS

QCS3 requirementSite : ----

Sampler : KATE PIGRAM

DatesDate Samples Received : Issue Date : 03-Sep-201501-Sep-2015 12:10 PM

Scheduled Reporting Date: 08-Sep-2015:Client Requested Due

Date

08-Sep-2015

Delivery DetailsMode of Delivery : :Carrier Intact.Security Seal

No. of coolers/boxes : :---- Temperature 4.2' C - Ice present

: : 11 / 10Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Sample QC200 to be forwarded to Envirolab.l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Asbestos analysis will be conducted by ALS Newcastle.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 51: Cover - Attach C14f

:Client AECOM Australia Pty Ltd

Work Order : ES1529728 Amendment 02 of 3:Page

03-Sep-2015:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exist.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

(On H

old

) S

OIL

No a

naly

sis

request

ed

SO

IL -

EA

200

Asbesto

s Id

entif

icatio

n in S

oils

-

ES1529728-008 [ 29-Aug-2015 ] SS01 ü

ES1529728-009 [ 29-Aug-2015 ] SS02 ü

ES1529728-010 [ 29-Aug-2015 ] SS03-FRAG ü

ES1529728-011 [ 29-Aug-2015 ] SS04-FRAG ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

WA

TE

R -

EP

074 V

inyl

Chlo

ride S

IM

VO

C S

IM V

inyl

Chlo

ride O

nly

WA

TE

R -

EP

074D

EF

G

VO

C -

Fum

igants

, H

al A

liphatic

s, H

al A

rom

atic

s,

WA

TE

R -

W-0

4

TR

H/B

TE

XN

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

WA

TE

R -

W-2

6

TR

H/B

TE

XN

/PA

H/8

Meta

ls

ES1529728-001 [ 31-Aug-2015 ] MW21 ü ü ü

ES1529728-002 [ 31-Aug-2015 ] MW19 ü ü ü

ES1529728-003 [ 31-Aug-2015 ] MW16 ü ü ü

ES1529728-004 [ 31-Aug-2015 ] MW17 ü ü ü

ES1529728-005 [ 31-Aug-2015 ] MW01 ü ü ü

ES1529728-006 [ 31-Aug-2015 ] QC201 ü

ES1529728-007 [ 31-Aug-2015 ] TB ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Page 52: Cover - Attach C14f

:Client AECOM Australia Pty Ltd

Work Order : ES1529728 Amendment 03 of 3:Page

03-Sep-2015:Issue Date

Requested Deliverables

ALEX LATHAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - HLAPro (HLAPro) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

AP_CUSTOMER SERVICE ANZ

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

KATE PIGRAM

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - HLAPro (HLAPro) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

Page 53: Cover - Attach C14f
Page 54: Cover - Attach C14f

CERTIFICATE OF ANALYSIS 133696

Client:

AECOM Australia Pty Ltd (Sydney)

PO Box Q410

QVB Post Office

Sydney

NSW 1230

Attention: Alex Latham, Kate Pigram

Sample log in details:

Your Reference: 60438840/1.1

No. of samples: 1 Water

Date samples received / completed instructions received 3/9/2015 / 3/9/2015

Analysis Details:

Please refer to the following pages for results, methodology summary and quality control data.

Samples were analysed as received from the client. Results relate specifically to the samples as received.

Results are reported on a dry weight basis for solids and on an as received basis for other matrices.

Please refer to the last page of this report for any comments relating to the results.

Report Details:

Date results requested by: / Issue Date: 10/09/15 / 8/09/15

Date of Preliminary Report: Not Issued

NATA accreditation number 2901. This document shall not be reproduced except in full.

Accredited for compliance with ISO/IEC 17025. Tests not covered by NATA are denoted with *.

Results Approved By:

Page 1 of 14Envirolab Reference: 133696

Revision No: R 00

Page 55: Cover - Attach C14f

Client Reference: 60438840/1.1

VHC's in water

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

Date extracted - 03/09/2015

Date analysed - 04/09/2015

Dichlorodifluoromethane µg/L <10

Chloromethane µg/L <10

Vinyl Chloride µg/L <0.3

Bromomethane µg/L <10

Chloroethane µg/L <10

Trichlorofluoromethane µg/L <10

1,1-Dichloroethene µg/L <1

Trans-1,2-dichloroethene µg/L <1

1,1-dichloroethane µg/L <1

Cis-1,2-dichloroethene µg/L <1

Bromochloromethane µg/L <1

Chloroform µg/L <1

2,2-dichloropropane µg/L <1

1,2-dichloroethane µg/L <1

1,1,1-trichloroethane µg/L <1

1,1-dichloropropene µg/L <1

Carbon tetrachloride µg/L <1

Dibromomethane µg/L <1

1,2-dichloropropane µg/L <1

Trichloroethene µg/L <1

Bromodichloromethane µg/L <1

trans-1,3-dichloropropene µg/L <1

cis-1,3-dichloropropene µg/L <1

1,1,2-trichloroethane µg/L <1

1,3-dichloropropane µg/L <1

Dibromochloromethane µg/L <1

1,2-dibromoethane µg/L <1

Tetrachloroethene µg/L <1

1,1,1,2-tetrachloroethane µg/L <1

Chlorobenzene µg/L <1

Bromoform µg/L <1

1,1,2,2-tetrachloroethane µg/L <1

1,2,3-trichloropropane µg/L <1

Bromobenzene µg/L <1

2-chlorotoluene µg/L <1

4-chlorotoluene µg/L <1

1,3-dichlorobenzene µg/L <1

1,4-dichlorobenzene µg/L <1

1,2-dichlorobenzene µg/L <1

1,2-dibromo-3-chloropropane µg/L <1

Page 2 of 14Envirolab Reference: 133696

Revision No: R 00

Page 56: Cover - Attach C14f

Client Reference: 60438840/1.1

VHC's in water

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

1,2,4-trichlorobenzene µg/L <1

Hexachlorobutadiene µg/L <1

1,2,3-trichlorobenzene µg/L <1

Surrogate Dibromofluoromethane % 97

Surrogate toluene-d8 % 93

Surrogate 4-BFB % 97

Page 3 of 14Envirolab Reference: 133696

Revision No: R 00

Page 57: Cover - Attach C14f

Client Reference: 60438840/1.1

vTRH(C6-C10)/BTEXN in Water

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

Date extracted - 03/09/2015

Date analysed - 04/09/2015

TRH C6 - C9 µg/L <10

TRH C6 - C10 µg/L <10

TRH C6 - C10 less BTEX (F1) µg/L <10

Benzene µg/L <1

Toluene µg/L <1

Ethylbenzene µg/L <1

m+p-xylene µg/L <2

o-xylene µg/L <1

Naphthalene µg/L <1

Surrogate Dibromofluoromethane % 101

Surrogate toluene-d8 % 93

Surrogate 4-BFB % 97

Page 4 of 14Envirolab Reference: 133696

Revision No: R 00

Page 58: Cover - Attach C14f

Client Reference: 60438840/1.1

svTRH (C10-C40) in Water

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

Date extracted - 04/09/2015

Date analysed - 04/09/2015

TRH C10 - C14 µg/L <50

TRH C15 - C28 µg/L <100

TRH C29 - C36 µg/L <100

TRH >C10 - C16 µg/L <50

TRH >C10 - C16 less Naphthalene

(F2)

µg/L <50

TRH >C16 - C34 µg/L <100

TRH >C34 - C40 µg/L <100

Surrogate o-Terphenyl % 84

Page 5 of 14Envirolab Reference: 133696

Revision No: R 00

Page 59: Cover - Attach C14f

Client Reference: 60438840/1.1

PAHs in Water

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

Date extracted - 04/09/2015

Date analysed - 04/09/2015

Naphthalene µg/L <1

Acenaphthylene µg/L <1

Acenaphthene µg/L <1

Fluorene µg/L <1

Phenanthrene µg/L <1

Anthracene µg/L <1

Fluoranthene µg/L <1

Pyrene µg/L <1

Benzo(a)anthracene µg/L <1

Chrysene µg/L <1

Benzo(b,j+k)fluoranthene µg/L <2

Benzo(a)pyrene µg/L <1

Indeno(1,2,3-c,d)pyrene µg/L <1

Dibenzo(a,h)anthracene µg/L <1

Benzo(g,h,i)perylene µg/L <1

Benzo(a)pyrene TEQ µg/L <5

Total +ve PAH's µg/L NIL (+)VE

Surrogate p-Terphenyl-d14 % 105

Page 6 of 14Envirolab Reference: 133696

Revision No: R 00

Page 60: Cover - Attach C14f

Client Reference: 60438840/1.1

HM in water - dissolved

Our Reference: UNITS 133696-1

Your Reference ------------- QC200

Date Sampled ------------ 31/08/2015

Type of sample Water

Date prepared - 04/09/2015

Date analysed - 04/09/2015

Arsenic-Dissolved µg/L 5

Cadmium-Dissolved µg/L <0.1

Chromium-Dissolved µg/L <1

Copper-Dissolved µg/L <1

Lead-Dissolved µg/L <1

Mercury-Dissolved µg/L <0.05

Nickel-Dissolved µg/L 2

Zinc-Dissolved µg/L 80

Page 7 of 14Envirolab Reference: 133696

Revision No: R 00

Page 61: Cover - Attach C14f

Client Reference: 60438840/1.1

Method ID Methodology Summary

Org-013 Water samples are analysed directly by purge and trap GC-MS.

Org-016 Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS.

Water samples are analysed directly by purge and trap GC-MS. F1 = (C6-C10)-BTEX as per NEPM B1

Guideline on Investigation Levels for Soil and Groundwater.

Org-003 Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by

GC-FID.

F2 = (>C10-C16)-Naphthalene as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater

(HSLs Tables 1A (3, 4)). Note Naphthalene is determined from the VOC analysis.

Org-012 subset Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by

GC-MS. Benzo(a)pyrene TEQ as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater -

2013.

Metals-022 ICP-MS Determination of various metals by ICP-MS.

Metals-021 CV-

AAS

Determination of Mercury by Cold Vapour AAS.

Page 8 of 14Envirolab Reference: 133696

Revision No: R 00

Page 62: Cover - Attach C14f

Client Reference: 60438840/1.1

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

VHC's in water Base ll Duplicate ll %RPD

Date extracted - 03/09/2

015

[NT] [NT] LCS-W2 03/09/2015

Date analysed - 04/09/2

015

[NT] [NT] LCS-W2 04/09/2015

Dichlorodifluoromethane µg/L 10 Org-013 <10 [NT] [NT] [NR] [NR]

Chloromethane µg/L 10 Org-013 <10 [NT] [NT] [NR] [NR]

Vinyl Chloride µg/L 0.3 Org-013 <0.3 [NT] [NT] [NR] [NR]

Bromomethane µg/L 10 Org-013 <10 [NT] [NT] [NR] [NR]

Chloroethane µg/L 10 Org-013 <10 [NT] [NT] [NR] [NR]

Trichlorofluoromethane µg/L 10 Org-013 <10 [NT] [NT] [NR] [NR]

1,1-Dichloroethene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Trans-1,2-

dichloroethene

µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,1-dichloroethane µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 91%

Cis-1,2-dichloroethene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Bromochloromethane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Chloroform µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 91%

2,2-dichloropropane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2-dichloroethane µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 91%

1,1,1-trichloroethane µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 90%

1,1-dichloropropene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Carbon tetrachloride µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Dibromomethane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2-dichloropropane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Trichloroethene µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 86%

Bromodichloromethane µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 88%

trans-1,3-

dichloropropene

µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

cis-1,3-dichloropropene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,1,2-trichloroethane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,3-dichloropropane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Dibromochloromethane µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 83%

1,2-dibromoethane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Tetrachloroethene µg/L 1 Org-013 <1 [NT] [NT] LCS-W2 88%

1,1,1,2-

tetrachloroethane

µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Chlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Bromoform µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,1,2,2-

tetrachloroethane

µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2,3-trichloropropane µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Bromobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

2-chlorotoluene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

4-chlorotoluene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,3-dichlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,4-dichlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2-dichlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Page 9 of 14Envirolab Reference: 133696

Revision No: R 00

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Client Reference: 60438840/1.1

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

VHC's in water Base ll Duplicate ll %RPD

1,2-dibromo-3-

chloropropane

µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2,4-trichlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Hexachlorobutadiene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

1,2,3-trichlorobenzene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Surrogate

Dibromofluoromethane

% Org-013 95 [NT] [NT] LCS-W2 88%

Surrogate toluene-d8 % Org-013 94 [NT] [NT] LCS-W2 98%

Surrogate 4-BFB % Org-013 95 [NT] [NT] LCS-W2 88%

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

vTRH(C6-C10)/BTEXN in

Water

Base ll Duplicate ll %RPD

Date extracted - 03/09/2

015

[NT] [NT] LCS-W2 03/09/2015

Date analysed - 04/09/2

015

[NT] [NT] LCS-W2 04/09/2015

TRH C6 - C9 µg/L 10 Org-016 <10 [NT] [NT] LCS-W2 87%

TRH C6 - C10 µg/L 10 Org-016 <10 [NT] [NT] LCS-W2 87%

Benzene µg/L 1 Org-016 <1 [NT] [NT] LCS-W2 89%

Toluene µg/L 1 Org-016 <1 [NT] [NT] LCS-W2 89%

Ethylbenzene µg/L 1 Org-016 <1 [NT] [NT] LCS-W2 85%

m+p-xylene µg/L 2 Org-016 <2 [NT] [NT] LCS-W2 86%

o-xylene µg/L 1 Org-016 <1 [NT] [NT] LCS-W2 87%

Naphthalene µg/L 1 Org-013 <1 [NT] [NT] [NR] [NR]

Surrogate

Dibromofluoromethane

% Org-016 101 [NT] [NT] LCS-W2 100%

Surrogate toluene-d8 % Org-016 94 [NT] [NT] LCS-W2 98%

Surrogate 4-BFB % Org-016 95 [NT] [NT] LCS-W2 88%

Page 10 of 14Envirolab Reference: 133696

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Client Reference: 60438840/1.1

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

svTRH (C10-C40) in

Water

Base ll Duplicate ll %RPD

Date extracted - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

Date analysed - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

TRH C10 - C14 µg/L 50 Org-003 <50 [NT] [NT] LCS-W1 112%

TRH C15 - C28 µg/L 100 Org-003 <100 [NT] [NT] LCS-W1 95%

TRH C29 - C36 µg/L 100 Org-003 <100 [NT] [NT] LCS-W1 97%

TRH >C10 - C16 µg/L 50 Org-003 <50 [NT] [NT] LCS-W1 112%

TRH >C16 - C34 µg/L 100 Org-003 <100 [NT] [NT] LCS-W1 95%

TRH >C34 - C40 µg/L 100 Org-003 <100 [NT] [NT] LCS-W1 97%

Surrogate o-Terphenyl % Org-003 86 [NT] [NT] LCS-W1 77%

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

PAHs in Water Base ll Duplicate ll %RPD

Date extracted - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

Date analysed - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

Naphthalene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 80%

Acenaphthylene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Acenaphthene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Fluorene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 78%

Phenanthrene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 82%

Anthracene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Fluoranthene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 80%

Pyrene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 84%

Benzo(a)anthracene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Chrysene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 80%

Benzo(b,j+k)

fluoranthene

µg/L 2 Org-012

subset

<2 [NT] [NT] [NR] [NR]

Benzo(a)pyrene µg/L 1 Org-012

subset

<1 [NT] [NT] LCS-W1 92%

Indeno(1,2,3-c,d)pyrene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Dibenzo(a,h)anthracene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Benzo(g,h,i)perylene µg/L 1 Org-012

subset

<1 [NT] [NT] [NR] [NR]

Surrogate p-Terphenyl-

d14

% Org-012

subset

95 [NT] [NT] LCS-W1 90%

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Revision No: R 00

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Client Reference: 60438840/1.1

QUALITY CONTROL UNITS PQL METHOD Blank Duplicate

Sm#

Duplicate results Spike Sm# Spike %

Recovery

HM in water - dissolved Base ll Duplicate ll %RPD

Date prepared - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

Date analysed - 04/09/2

015

[NT] [NT] LCS-W1 04/09/2015

Arsenic-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 95%

Cadmium-Dissolved µg/L 0.1 Metals-022

ICP-MS

<0.1 [NT] [NT] LCS-W1 101%

Chromium-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 96%

Copper-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 99%

Lead-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 105%

Mercury-Dissolved µg/L 0.05 Metals-021

CV-AAS

<0.05 [NT] [NT] LCS-W1 96%

Nickel-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 94%

Zinc-Dissolved µg/L 1 Metals-022

ICP-MS

<1 [NT] [NT] LCS-W1 96%

Page 12 of 14Envirolab Reference: 133696

Revision No: R 00

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Client Reference: 60438840/1.1

Report Comments:

Asbestos ID was analysed by Approved Identifier: Not applicable for this job

Asbestos ID was authorised by Approved Signatory: Not applicable for this job

INS: Insufficient sample for this test PQL: Practical Quantitation Limit NT: Not tested

NA: Test not required RPD: Relative Percent Difference NA: Test not required

<: Less than >: Greater than LCS: Laboratory Control Sample

Page 13 of 14Envirolab Reference: 133696

Revision No: R 00

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Client Reference: 60438840/1.1

Quality Control Definitions

Blank: This is the component of the analytical signal which is not derived from the sample but from reagents,

glassware etc, can be determined by processing solvents and reagents in exactly the same manner as for samples.

Duplicate : This is the complete duplicate analysis of a sample from the process batch. If possible, the sample

selected should be one where the analyte concentration is easily measurable.

Matrix Spike : A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix

spike is to monitor the performance of the analytical method used and to determine whether matrix interferences exist.

LCS (Laboratory Control Sample) : This comprises either a standard reference material or a control matrix (such as a blank

sand or water) fortified with analytes representative of the analyte class. It is simply a check sample.

Surrogate Spike: Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds

which are similar to the analyte of interest, however are not expected to be found in real samples.

Laboratory Acceptance Criteria

Duplicate sample and matrix spike recoveries may not be reported on smaller jobs, however, were analysed at a frequency

to meet or exceed NEPM requirements. All samples are tested in batches of 20. The duplicate sample RPD and matrix

spike recoveries for the batch were within the laboratory acceptance criteria.

Filters, swabs, wipes, tubes and badges will not have duplicate data as the whole sample is generally extracted

during sample extraction.

Spikes for Physical and Aggregate Tests are not applicable.

For VOCs in water samples, three vials are required for duplicate or spike analysis.

Duplicates: <5xPQL - any RPD is acceptable; >5xPQL - 0-50% RPD is acceptable.

Matrix Spikes, LCS and Surrogate recoveries: Generally 70-130% for inorganics/metals; 60-140%

for organics (+/-50% surrogates) and 10-140% for labile SVOCs (including labile surrogates), ultra trace organics

and speciated phenols is acceptable.

In circumstances where no duplicate and/or sample spike has been reported at 1 in 10 and/or 1 in 20 samples

respectively, the sample volume submitted was insufficient in order to satisfy laboratory QA/QC protocols.

When samples are received where certain analytes are outside of recommended technical holding times (THTs),

the analysis has proceeded. Where analytes are on the verge of breaching THTs, every effort will be made to analyse

within the THT or as soon as practicable.

Page 14 of 14Envirolab Reference: 133696

Revision No: R 00

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SAMPLE RECEIPT ADVICE

Client Details

Client AECOM Australia Pty Ltd (Sydney) Attention Alex Latham, Kate Pigram

Sample Login Details

Your Reference 60438840/1.1

Envirolab Reference 133696 Date Sample Received 03/09/2015 Date Instructions Received 03/09/2015 Date Results Expected to be Reported 10/09/2015

Sample Condition

Samples received in appropriate condition for analysis YES

No. of Samples Provided 1 Water Turnaround Time Requested Standard Temperature on receipt (°C) 5.7 Cooling Method Ice Sampling Date Provided YES

Comments Samples will be held for 1 month for water samples and 2 months for soil samples from date of receipt of samples

Please direct any queries to:

Aileen Hie Jacinta Hurst

Phone: 02 9910 6200 Phone: 02 9910 6200

Fax: 02 9910 6201 Fax: 02 9910 6201

Email: [email protected] Email: [email protected]

Sample and Testing Details on following page

Page 69: Cover - Attach C14f

Sample Id

VH

C's

in w

ate

r

vTR

H(C

6-

C1

0)/

BTE

XN

in

Wa

ter

svTR

H (

C1

0-C

40

) in

Wa

ter

PA

Hs

in W

ate

r

HM

in w

ate

r -

dis

solv

ed

QC200 ✓ ✓ ✓ ✓ ✓

Page 70: Cover - Attach C14f
Page 71: Cover - Attach C14f

Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

CERTIFICATE OF ANALYSIS 235771

PO Box Q410, QVB Post Office, Sydney, NSW, 1230Address

Alex LathamAttention

AECOM Australia Pty Ltd (Sydney)Client

Client Details

31/01/2020Date completed instructions received

31/01/2020Date samples received

3 SoilNumber of Samples

60623599_1.1, Burrows IEYour Reference

Sample Details

Please refer to the last page of this report for any comments relating to the results.

Results are reported on a dry weight basis for solids and on an as received basis for other matrices.

Samples were analysed as received from the client. Results relate specifically to the samples as received.

Please refer to the following pages for results, methodology summary and quality control data.

Analysis Details

Tests not covered by NATA are denoted with *Accredited for compliance with ISO/IEC 17025 - Testing.

NATA Accreditation Number 2901. This document shall not be reproduced except in full.

07/02/2020Date of Issue

07/02/2020Date results requested by

Report Details

Nancy Zhang, Laboratory Manager

Authorised By

Loren Bardwell, Senior Chemist

Josh Williams, Senior Chemist

Results Approved By

Revision No: R00

235771Envirolab Reference: Page | 1 of 15

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Client Reference: 60623599_1.1, Burrows IE

758387%Surrogate aaa-Trifluorotoluene

<3<3<3mg/kgTotal +ve Xylenes

<1<1<1mg/kgnaphthalene

<1<1<1mg/kgo-Xylene

<2<2<2mg/kgm+p-xylene

<1<1<1mg/kgEthylbenzene

<0.5<0.5<0.5mg/kgToluene

<0.2<0.2<0.2mg/kgBenzene

<25<25<25mg/kgvTPH C6 - C10 less BTEX (F1)

<25<25<25mg/kgTRH C6 - C10

<25<25<25mg/kgTRH C6 - C9

04/02/202004/02/202004/02/2020-Date analysed

04/02/202004/02/202004/02/2020-Date extracted

SoilSoilSoilType of sample

29/01/202029/01/202029/01/2020Date Sampled

QC 102QC 106QC 105UNITSYour Reference

235771-3235771-2235771-1Our Reference

vTRH(C6-C10)/BTEXN in Soil

Envirolab Reference: 235771

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708479%Surrogate o-Terphenyl

<50210140mg/kgTotal +ve TRH (>C10-C40)

<100<100<100mg/kgTRH >C34 -C40

<100210140mg/kgTRH >C16 -C34

<50<50<50mg/kgTRH >C10 - C16 less Naphthalene (F2)

<50<50<50mg/kgTRH >C10 -C16

<100120<100mg/kgTRH C29 - C36

<100120<100mg/kgTRH C15 - C28

<50<50<50mg/kgTRH C10 - C14

06/02/202006/02/202006/02/2020-Date analysed

03/02/202003/02/202003/02/2020-Date extracted

SoilSoilSoilType of sample

29/01/202029/01/202029/01/2020Date Sampled

QC 102QC 106QC 105UNITSYour Reference

235771-3235771-2235771-1Our Reference

svTRH (C10-C40) in Soil

Envirolab Reference: 235771

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919893%Surrogate p-Terphenyl-d14

<0.50.7<0.5mg/kgBenzo(a)pyrene TEQ calc(PQL)

<0.50.7<0.5mg/kgBenzo(a)pyrene TEQ calc(half)

<0.50.6<0.5mg/kgBenzo(a)pyrene TEQ calc (zero)

<0.054.51.6mg/kgTotal +ve PAH's

<0.10.4<0.1mg/kgBenzo(g,h,i)perylene

<0.1<0.1<0.1mg/kgDibenzo(a,h)anthracene

<0.10.2<0.1mg/kgIndeno(1,2,3-c,d)pyrene

<0.050.50.1mg/kgBenzo(a)pyrene

<0.20.70.2mg/kgBenzo(b,j+k)fluoranthene

<0.10.40.2mg/kgChrysene

<0.10.50.2mg/kgBenzo(a)anthracene

<0.10.60.3mg/kgPyrene

<0.10.70.3mg/kgFluoranthene

<0.10.2<0.1mg/kgAnthracene

<0.10.40.3mg/kgPhenanthrene

<0.1<0.1<0.1mg/kgFluorene

<0.1<0.1<0.1mg/kgAcenaphthene

<0.1<0.1<0.1mg/kgAcenaphthylene

<0.1<0.1<0.1mg/kgNaphthalene

04/02/202004/02/202004/02/2020-Date analysed

04/02/202004/02/202004/02/2020-Date extracted

SoilSoilSoilType of sample

29/01/202029/01/202029/01/2020Date Sampled

QC 102QC 106QC 105UNITSYour Reference

235771-3235771-2235771-1Our Reference

PAHs in Soil

Envirolab Reference: 235771

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Client Reference: 60623599_1.1, Burrows IE

34012,000450350mg/kgZinc

15023017170mg/kgNickel

0.52.80.40.4mg/kgMercury

2404,500330260mg/kgLead

54042,000110530mg/kgCopper

202601622mg/kgChromium

5.01014.4mg/kgCadmium

644127mg/kgArsenic

04/02/202004/02/202004/02/202004/02/2020-Date analysed

04/02/202004/02/202004/02/202004/02/2020-Date prepared

SoilSoilSoilSoilType of sample

29/01/202029/01/202029/01/202029/01/2020Date Sampled

QC 105 - [TRIPLICATE]

QC 102QC 106QC 105UNITSYour Reference

235771-4235771-3235771-2235771-1Our Reference

Acid Extractable metals in soil

Envirolab Reference: 235771

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241215%Moisture

04/02/202004/02/202004/02/2020-Date analysed

03/02/202003/02/202003/02/2020-Date prepared

SoilSoilSoilType of sample

29/01/202029/01/202029/01/2020Date Sampled

QC 102QC 106QC 105UNITSYour Reference

235771-3235771-2235771-1Our Reference

Moisture

Envirolab Reference: 235771

R00Revision No:

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Client Reference: 60623599_1.1, Burrows IE

Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Water samples are analysed directly by purge and trap GC-MS. F1 = (C6-C10)-BTEX as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater.

Org-016

Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Org-014

Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-MS and/or GC-MS/MS. Benzo(a)pyrene TEQ as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater - 2013. For soil results:- 1. ‘EQ PQL’values are assuming all contributing PAHs reported as <PQL are actually at the PQL. This is the most conservative approach and can give false positive TEQs given that PAHs that contribute to the TEQ calculation may not be present. 2. ‘EQ zero’values are assuming all contributing PAHs reported as <PQL are zero. This is the least conservative approach and is more susceptible to false negative TEQs when PAHs that contribute to the TEQ calculation are present but below PQL. 3. ‘EQ half PQL’values are assuming all contributing PAHs reported as <PQL are half the stipulated PQL. Hence a mid-point between the most and least conservative approaches above. Note, the Total +ve PAHs PQL is reflective of the lowest individual PQL and is therefore "Total +ve PAHs" is simply a sum of the positive individual PAHs.

Org-012/017

Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-FID. F2 = (>C10-C16)-Naphthalene as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater (HSLs Tables 1A (3, 4)). Note Naphthalene is determined from the VOC analysis. Note, the Total +ve TRH PQL is reflective of the lowest individual PQL and is therefore "Total +ve TRH" is simply a sum of the positive individual TRH fractions (>C10-C40).

Org-003

Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-FID. F2 = (>C10-C16)-Naphthalene as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater (HSLs Tables 1A (3, 4)). Note Naphthalene is determined from the VOC analysis.

Org-003

Determination of Mercury by Cold Vapour AAS. Metals-021

Determination of various metals by ICP-AES. Metals-020

Moisture content determined by heating at 105+/-5 °C for a minimum of 12 hours.

Inorg-008

Methodology SummaryMethod ID

Envirolab Reference: 235771

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Client Reference: 60623599_1.1, Burrows IE

Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Water samples are analysed directly by purge and trap GC-MS. F1 = (C6-C10)-BTEX as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater. Note, the Total +ve Xylene PQL is reflective of the lowest individual PQL and is therefore "Total +ve Xylenes" is simply a sum of the positive individual Xylenes.

Org-016

Methodology SummaryMethod ID

Envirolab Reference: 235771

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Client Reference: 60623599_1.1, Burrows IE

[NT]9868287193Org-016%Surrogate aaa-Trifluorotoluene

[NT][NT]0<1<11<1Org-0141mg/kgnaphthalene

[NT]1250<1<11<1Org-0161mg/kgo-Xylene

[NT]1240<2<21<2Org-0162mg/kgm+p-xylene

[NT]1250<1<11<1Org-0161mg/kgEthylbenzene

[NT]1190<0.5<0.51<0.5Org-0160.5mg/kgToluene

[NT]1170<0.2<0.21<0.2Org-0160.2mg/kgBenzene

[NT]1220<25<251<25Org-01625mg/kgTRH C6 - C10

[NT]1220<25<251<25Org-01625mg/kgTRH C6 - C9

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date analysed

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date extracted

[NT]LCS-13RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: vTRH(C6-C10)/BTEXN in Soil

Envirolab Reference: 235771

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[NT]9128179172Org-003%Surrogate o-Terphenyl

[NT]10833140<1001<100Org-003100mg/kgTRH >C34 -C40

[NT]88883601401<100Org-003100mg/kgTRH >C16 -C34

[NT]850<50<501<50Org-00350mg/kgTRH >C10 -C16

[NT]10879230<1001<100Org-003100mg/kgTRH C29 - C36

[NT]8846160<1001<100Org-003100mg/kgTRH C15 - C28

[NT]850<50<501<50Org-00350mg/kgTRH C10 - C14

[NT]06/02/202006/02/202006/02/2020106/02/2020-Date analysed

[NT]03/02/202003/02/202003/02/2020103/02/2020-Date extracted

[NT]LCS-12RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: svTRH (C10-C40) in Soil

Envirolab Reference: 235771

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[NT]10419293191Org-012/017%Surrogate p-Terphenyl-d14

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgBenzo(g,h,i)perylene

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgDibenzo(a,h)anthracene

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgIndeno(1,2,3-c,d)pyrene

[NT]12800.10.11<0.05Org-012/0170.05mg/kgBenzo(a)pyrene

[NT][NT]00.20.21<0.2Org-012/0170.2mg/kgBenzo(b,j+k)fluoranthene

[NT]8400.20.21<0.1Org-012/0170.1mg/kgChrysene

[NT][NT]00.20.21<0.1Org-012/0170.1mg/kgBenzo(a)anthracene

[NT]11200.30.31<0.1Org-012/0170.1mg/kgPyrene

[NT]10600.30.31<0.1Org-012/0170.1mg/kgFluoranthene

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgAnthracene

[NT]98400.20.31<0.1Org-012/0170.1mg/kgPhenanthrene

[NT]1040<0.1<0.11<0.1Org-012/0170.1mg/kgFluorene

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgAcenaphthene

[NT][NT]0<0.1<0.11<0.1Org-012/0170.1mg/kgAcenaphthylene

[NT]1120<0.1<0.11<0.1Org-012/0170.1mg/kgNaphthalene

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date analysed

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date extracted

[NT]LCS-11RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: PAHs in Soil

Envirolab Reference: 235771

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[NT]11883803501<1Metals-0201mg/kgZinc

[NT]113121501701<1Metals-0201mg/kgNickel

[NT]90220.50.41<0.1Metals-0210.1mg/kgMercury

[NT]120614902601<1Metals-0201mg/kgLead

[NT]111226605301<1Metals-0201mg/kgCopper

[NT]1142428221<1Metals-0201mg/kgChromium

[NT]109114.94.41<0.4Metals-0200.4mg/kgCadmium

[NT]1120771<4Metals-0204mg/kgArsenic

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date analysed

[NT]04/02/202004/02/202004/02/2020104/02/2020-Date prepared

[NT]LCS-13RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: Acid Extractable metals in soil

Envirolab Reference: 235771

R00Revision No:

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Not ReportedNR

National Environmental Protection MeasureNEPM

Not specifiedNS

Laboratory Control SampleLCS

Relative Percent DifferenceRPD

Greater than>

Less than<

Practical Quantitation LimitPQL

Insufficient sample for this testINS

Test not requiredNA

Not testedNT

Result Definitions

Envirolab Reference: 235771

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Guideline limits for Rinse Water Quality reported as per analytical requirements and specifications of AS 4187, Amdt 2 2019, Table7.2

The recommended maximums for analytes in urine are taken from “2018 TLVs and BEIs”, as published by ACGIH (where available).Limit provided for Nickel is a precautionary guideline as per Position Paper prepared by AIOH Exposure Standards Committee,2016.

Australian Drinking Water Guidelines recommend that Thermotolerant Coliform, Faecal Enterococci, & E.Coli levels are less than1cfu/100mL. The recommended maximums are taken from "Australian Drinking Water Guidelines", published by NHMRC & ARMC2011.

Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds whichare similar to the analyte of interest, however are not expected to be found in real samples.

Surrogate Spike

This comprises either a standard reference material or a control matrix (such as a blank sand or water) fortifiedwith analytes representative of the analyte class. It is simply a check sample.

LCS (LaboratoryControl Sample)

A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix spikeis to monitor the performance of the analytical method used and to determine whether matrix interferencesexist.

Matrix Spike

This is the complete duplicate analysis of a sample from the process batch. If possible, the sample selectedshould be one where the analyte concentration is easily measurable.

Duplicate

This is the component of the analytical signal which is not derived from the sample but from reagents,glassware etc, can be determined by processing solvents and reagents in exactly the same manner as forsamples.

Blank

Quality Control Definitions

Samples for Microbiological analysis (not Amoeba forms) received outside of the 2-8°C temperature range do not meet the idealcooling conditions as stated in AS2031-2012.

Analysis of aqueous samples typically involves the extraction/digestion and/or analysis of the liquid phase only (i.e. NOT any settledsediment phase but inclusive of suspended particles if present), unless stipulated on the Envirolab COC and/or by correspondence.Notable exceptions include certain Physical Tests (pH/EC/BOD/COD/Apparent Colour etc.), Solids testing, total recoverable metalsand PFAS where solids are included by default.

Measurement Uncertainty estimates are available for most tests upon request.

Where sampling dates are not provided, Envirolab are not in a position to comment on the validity of the analysis whererecommended technical holding times may have been breached.

When samples are received where certain analytes are outside of recommended technical holding times (THTs), the analysis hasproceeded. Where analytes are on the verge of breaching THTs, every effort will be made to analyse within the THT or as soon aspracticable.

In circumstances where no duplicate and/or sample spike has been reported at 1 in 10 and/or 1 in 20 samples respectively, thesample volume submitted was insufficient in order to satisfy laboratory QA/QC protocols.

Matrix Spikes, LCS and Surrogate recoveries: Generally 70-130% for inorganics/metals (not SPOCAS); 60-140% fororganics/SPOCAS (+/-50% surrogates) and 10-140% for labile SVOCs (including labile surrogates), ultra trace organics andspeciated phenols is acceptable.

Duplicates: >10xPQL - RPD acceptance criteria will vary depending on the analytes and the analytical techniques but is typically inthe range 20%-50% – see ELN-P05 QA/QC tables for details; <10xPQL - RPD are higher as the results approach PQL and theestimated measurement uncertainty will statistically increase.

For VOCs in water samples, three vials are required for duplicate or spike analysis.

Spikes for Physical and Aggregate Tests are not applicable.

Filters, swabs, wipes, tubes and badges will not have duplicate data as the whole sample is generally extracted during sampleextraction.

Duplicate sample and matrix spike recoveries may not be reported on smaller jobs, however, were analysed at a frequency to meetor exceed NEPM requirements. All samples are tested in batches of 20. The duplicate sample RPD and matrix spike recoveries forthe batch were within the laboratory acceptance criteria.

Laboratory Acceptance Criteria

Envirolab Reference: 235771

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Acid Extractable Metals in Soil: The laboratory RPD acceptance criteria has been exceeded for 235771-1 for Pb. Therefore a triplicate result has been issued as laboratory sample number 235771-4.

Report Comments

Envirolab Reference: 235771

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Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

SAMPLE RECEIPT ADVICE

Rebekah Panozzo, Kurtis WathenAttention

AECOM Australia Pty Ltd (Sydney)Client

Client Details

07/02/2020Date Results Expected to be Reported

31/01/2020Date Instructions Received

31/01/2020Date Sample Received

235771Envirolab Reference

60623599_1.1, Burrows IEYour reference

Sample Login Details

YESSampling Date Provided

IceCooling Method

17.0Temperature on Receipt (°C)

StandardTurnaround Time Requested

3 SoilNo. of Samples Provided

YesSamples received in appropriate condition for analysis

Sample Condition

Nil

Comments

Please direct any queries to:

Email: [email protected]: [email protected]

Fax: 02 9910 6201Fax: 02 9910 6201

Phone: 02 9910 6200Phone: 02 9910 6200

Jacinta HurstAileen Hie

Analysis Underway, details on the following page:

Page | 1 of 2

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Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

PPPPQC 102

PPPPQC 106

PPPPQC 105

Ac

id E

xtr

ac

tab

le m

eta

lsin

so

il

PA

Hs

in

So

il

sv

TR

H (

C1

0-C

40

) in

So

il

vT

RH

(C6

-C1

0)/

BT

EX

N i

n S

oil

Sample ID

The ' THIS IS NOT A REPORT OF THE RESULTS.P' indicates the testing you have requested.

TAT for Micro is dependent on incubation. This varies from 3 to 6 days.

Please contact the laboratory immediately if observed settled sediment present in water samples is to be included in the extractionand/or analysis (exceptions include certain Physical Tests (pH/EC/BOD/COD/Apparent Colour etc.), Solids testing, Total Recoverablemetals and PFAS analysis where solids are included by default.

Requests for longer term sample storage must be received in writing.

Sample storage - Waters are routinely disposed of approximately 1 month and soils approximately 2 months from receipt.

Additional Info

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Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

CERTIFICATE OF ANALYSIS 236880

PO Box Q410, QVB Post Office, Sydney, NSW, 1230Address

Alex LathamAttention

AECOM Australia Pty Ltd (Sydney)Client

Client Details

17/02/2020Date completed instructions received

17/02/2020Date samples received

1 waterNumber of Samples

60623599_1.0Your Reference

Sample Details

Results are reported on a dry weight basis for solids and on an as received basis for other matrices.

Samples were analysed as received from the client. Results relate specifically to the samples as received.

Please refer to the following pages for results, methodology summary and quality control data.

Analysis Details

Tests not covered by NATA are denoted with *Accredited for compliance with ISO/IEC 17025 - Testing.

NATA Accreditation Number 2901. This document shall not be reproduced except in full.

24/02/2020Date of Issue

24/02/2020Date results requested by

Report Details

Nancy Zhang, Laboratory Manager

Authorised By

Josh Williams, Senior Chemist

Jaimie Loa-Kum-Cheung, Metals Supervisor

Results Approved By

Revision No: R00

236880Envirolab Reference: Page | 1 of 14

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Client Reference: 60623599_1.0

<1µg/LBromobenzene

<1µg/L1,2,3-trichloropropane

<1µg/L1,1,2,2-tetrachloroethane

<1µg/LBromoform

<1µg/LChlorobenzene

<1µg/L1,1,1,2-tetrachloroethane

<1µg/LTetrachloroethene

<1µg/L1,2-dibromoethane

<1µg/LDibromochloromethane

<1µg/L1,3-dichloropropane

<1µg/L1,1,2-trichloroethane

<1µg/Lcis-1,3-dichloropropene

<1µg/Ltrans-1,3-dichloropropene

<1µg/LBromodichloromethane

<1µg/LTrichloroethene

<1µg/L1,2-dichloropropane

<1µg/LDibromomethane

<1µg/LCarbon tetrachloride

<1µg/L1,1-dichloropropene

<1µg/L1,1,1-trichloroethane

<1µg/L1,2-dichloroethane

<1µg/L2,2-dichloropropane

<1µg/LChloroform

<1µg/LBromochloromethane

<1µg/LCis-1,2-dichloroethene

<1µg/L1,1-dichloroethane

<1µg/LTrans-1,2-dichloroethene

<1µg/L1,1-Dichloroethene

<10µg/LTrichlorofluoromethane

<10µg/LChloroethane

<10µg/LBromomethane

<0.3µg/LVinyl Chloride

<10µg/LChloromethane

<10µg/LDichlorodifluoromethane

20/02/2020-Date analysed

20/02/2020-Date extracted

waterType of sample

12/02/2020Date Sampled

QC306_200212UNITSYour Reference

236880-1Our Reference

VHC's in water

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109%Surrogate 4-BFB

99%Surrogate toluene-d8

109%Surrogate Dibromofluoromethane

<1µg/L1,2,3-trichlorobenzene

<1µg/LHexachlorobutadiene

<1µg/L1,2,4-trichlorobenzene

<1µg/L1,2-dibromo-3-chloropropane

<1µg/L1,2-dichlorobenzene

<1µg/L1,4-dichlorobenzene

<1µg/L1,3-dichlorobenzene

<1µg/L4-chlorotoluene

<1µg/L2-chlorotoluene

waterType of sample

12/02/2020Date Sampled

QC306_200212UNITSYour Reference

236880-1Our Reference

VHC's in water

Envirolab Reference: 236880

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109%Surrogate 4-BFB

99%Surrogate toluene-d8

109%Surrogate Dibromofluoromethane

<1µg/LNaphthalene

<1µg/Lo-xylene

<2µg/Lm+p-xylene

<1µg/LEthylbenzene

<1µg/LToluene

<1µg/LBenzene

<10µg/LTRH C6 - C10 less BTEX (F1)

<10µg/LTRH C6 - C10

<10µg/LTRH C6 - C9

20/02/2020-Date analysed

20/02/2020-Date extracted

waterType of sample

12/02/2020Date Sampled

QC306_200212UNITSYour Reference

236880-1Our Reference

vTRH(C6-C10)/BTEXN in Water

Envirolab Reference: 236880

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112%Surrogate o-Terphenyl

<100µg/LTRH >C34 - C40

<100µg/LTRH >C16 - C34

<50µg/LTRH >C10 - C16 less Naphthalene (F2)

<50µg/LTRH >C10 - C16

<100µg/LTRH C29 - C36

<100µg/LTRH C15 - C28

<50µg/LTRH C10 - C14

19/02/2020-Date analysed

19/02/2020-Date extracted

waterType of sample

12/02/2020Date Sampled

QC306_200212UNITSYour Reference

236880-1Our Reference

svTRH (C10-C40) in Water

Envirolab Reference: 236880

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5µg/LZinc-Dissolved

1µg/LNickel-Dissolved

<0.05µg/LMercury-Dissolved

<1µg/LLead-Dissolved

<1µg/LCopper-Dissolved

<1µg/LChromium-Dissolved

<0.1µg/LCadmium-Dissolved

5µg/LArsenic-Dissolved

19/02/2020-Date analysed

19/02/2020-Date prepared

waterType of sample

12/02/2020Date Sampled

QC306_200212UNITSYour Reference

236880-1Our Reference

HM in water - dissolved

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Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Water samples are analysed directly by purge and trap GC-MS. F1 = (C6-C10)-BTEX as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater.

Org-016

Water samples are analysed directly by purge and trap GC-MS.Org-013

Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-FID. F2 = (>C10-C16)-Naphthalene as per NEPM B1 Guideline on Investigation Levels for Soil and Groundwater (HSLs Tables 1A (3, 4)). Note Naphthalene is determined from the VOC analysis.

Org-003

Determination of various metals by ICP-MS. Metals-022

Determination of Mercury by Cold Vapour AAS. Metals-021

Methodology SummaryMethod ID

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[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,4-dichlorobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,3-dichlorobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L4-chlorotoluene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L2-chlorotoluene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LBromobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2,3-trichloropropane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,1,2,2-tetrachloroethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LBromoform

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LChlorobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,1,1,2-tetrachloroethane

[NT]116[NT][NT][NT][NT]<1Org-0131µg/LTetrachloroethene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2-dibromoethane

[NT]111[NT][NT][NT][NT]<1Org-0131µg/LDibromochloromethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,3-dichloropropane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,1,2-trichloroethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/Lcis-1,3-dichloropropene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/Ltrans-1,3-dichloropropene

[NT]116[NT][NT][NT][NT]<1Org-0131µg/LBromodichloromethane

[NT]115[NT][NT][NT][NT]<1Org-0131µg/LTrichloroethene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2-dichloropropane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LDibromomethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LCarbon tetrachloride

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,1-dichloropropene

[NT]119[NT][NT][NT][NT]<1Org-0131µg/L1,1,1-trichloroethane

[NT]115[NT][NT][NT][NT]<1Org-0131µg/L1,2-dichloroethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L2,2-dichloropropane

[NT]119[NT][NT][NT][NT]<1Org-0131µg/LChloroform

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LBromochloromethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LCis-1,2-dichloroethene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,1-dichloroethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LTrans-1,2-dichloroethene

[NT]118[NT][NT][NT][NT]<1Org-0131µg/L1,1-Dichloroethene

[NT][NT][NT][NT][NT][NT]<10Org-01310µg/LTrichlorofluoromethane

[NT][NT][NT][NT][NT][NT]<10Org-01310µg/LChloroethane

[NT][NT][NT][NT][NT][NT]<10Org-01310µg/LBromomethane

[NT][NT][NT][NT][NT][NT]<0.3Org-0130.3µg/LVinyl Chloride

[NT][NT][NT][NT][NT][NT]<10Org-01310µg/LChloromethane

[NT][NT][NT][NT][NT][NT]<10Org-01310µg/LDichlorodifluoromethane

[NT]20/02/2020[NT][NT][NT][NT]20/02/2020-Date analysed

[NT]20/02/2020[NT][NT][NT][NT]20/02/2020-Date extracted

[NT]LCS-W1RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: VHC's in water

Envirolab Reference: 236880

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[NT]99[NT][NT][NT][NT]108Org-013%Surrogate 4-BFB

[NT]99[NT][NT][NT][NT]98Org-013%Surrogate toluene-d8

[NT]97[NT][NT][NT][NT]100Org-013%Surrogate Dibromofluoromethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2,3-trichlorobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LHexachlorobutadiene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2,4-trichlorobenzene

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2-dibromo-3-chloropropane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/L1,2-dichlorobenzene

[NT]LCS-W1RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: VHC's in water

Envirolab Reference: 236880

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[NT]99[NT][NT][NT][NT]108Org-016%Surrogate 4-BFB

[NT]99[NT][NT][NT][NT]98Org-016%Surrogate toluene-d8

[NT]97[NT][NT][NT][NT]100Org-016%Surrogate Dibromofluoromethane

[NT][NT][NT][NT][NT][NT]<1Org-0131µg/LNaphthalene

[NT]116[NT][NT][NT][NT]<1Org-0161µg/Lo-xylene

[NT]114[NT][NT][NT][NT]<2Org-0162µg/Lm+p-xylene

[NT]117[NT][NT][NT][NT]<1Org-0161µg/LEthylbenzene

[NT]119[NT][NT][NT][NT]<1Org-0161µg/LToluene

[NT]118[NT][NT][NT][NT]<1Org-0161µg/LBenzene

[NT]117[NT][NT][NT][NT]<10Org-01610µg/LTRH C6 - C10

[NT]117[NT][NT][NT][NT]<10Org-01610µg/LTRH C6 - C9

[NT]20/02/2020[NT][NT][NT][NT]20/02/2020-Date analysed

[NT]20/02/2020[NT][NT][NT][NT]20/02/2020-Date extracted

[NT]LCS-W1RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: vTRH(C6-C10)/BTEXN in Water

Envirolab Reference: 236880

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[NT]83[NT][NT][NT][NT]114Org-003%Surrogate o-Terphenyl

[NT]87[NT][NT][NT][NT]<100Org-003100µg/LTRH >C34 - C40

[NT]100[NT][NT][NT][NT]<100Org-003100µg/LTRH >C16 - C34

[NT]89[NT][NT][NT][NT]<50Org-00350µg/LTRH >C10 - C16

[NT]87[NT][NT][NT][NT]<100Org-003100µg/LTRH C29 - C36

[NT]100[NT][NT][NT][NT]<100Org-003100µg/LTRH C15 - C28

[NT]89[NT][NT][NT][NT]<50Org-00350µg/LTRH C10 - C14

[NT]19/02/2020[NT][NT][NT][NT]19/02/2020-Date analysed

[NT]19/02/2020[NT][NT][NT][NT]19/02/2020-Date extracted

[NT]LCS-W2RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: svTRH (C10-C40) in Water

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[NT]970551<1Metals-0221µg/LZinc-Dissolved

[NT]1000111<1Metals-0221µg/LNickel-Dissolved

[NT]96[NT]<0.051<0.05Metals-0210.05µg/LMercury-Dissolved

[NT]1020<1<11<1Metals-0221µg/LLead-Dissolved

[NT]1030<1<11<1Metals-0221µg/LCopper-Dissolved

[NT]960<1<11<1Metals-0221µg/LChromium-Dissolved

[NT]980<0.1<0.11<0.1Metals-0220.1µg/LCadmium-Dissolved

[NT]1000551<1Metals-0221µg/LArsenic-Dissolved

[NT]19/02/202019/02/202019/02/2020119/02/2020-Date analysed

[NT]19/02/202019/02/202019/02/2020119/02/2020-Date prepared

[NT]LCS-W1RPDDup.Base#BlankMethodPQLUnitsTest Description

Spike Recovery %DuplicateQUALITY CONTROL: HM in water - dissolved

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Not ReportedNR

National Environmental Protection MeasureNEPM

Not specifiedNS

Laboratory Control SampleLCS

Relative Percent DifferenceRPD

Greater than>

Less than<

Practical Quantitation LimitPQL

Insufficient sample for this testINS

Test not requiredNA

Not testedNT

Result Definitions

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Guideline limits for Rinse Water Quality reported as per analytical requirements and specifications of AS 4187, Amdt 2 2019, Table7.2

The recommended maximums for analytes in urine are taken from “2018 TLVs and BEIs”, as published by ACGIH (where available).Limit provided for Nickel is a precautionary guideline as per Position Paper prepared by AIOH Exposure Standards Committee,2016.

Australian Drinking Water Guidelines recommend that Thermotolerant Coliform, Faecal Enterococci, & E.Coli levels are less than1cfu/100mL. The recommended maximums are taken from "Australian Drinking Water Guidelines", published by NHMRC & ARMC2011.

Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds whichare similar to the analyte of interest, however are not expected to be found in real samples.

Surrogate Spike

This comprises either a standard reference material or a control matrix (such as a blank sand or water) fortifiedwith analytes representative of the analyte class. It is simply a check sample.

LCS (LaboratoryControl Sample)

A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix spikeis to monitor the performance of the analytical method used and to determine whether matrix interferencesexist.

Matrix Spike

This is the complete duplicate analysis of a sample from the process batch. If possible, the sample selectedshould be one where the analyte concentration is easily measurable.

Duplicate

This is the component of the analytical signal which is not derived from the sample but from reagents,glassware etc, can be determined by processing solvents and reagents in exactly the same manner as forsamples.

Blank

Quality Control Definitions

Samples for Microbiological analysis (not Amoeba forms) received outside of the 2-8°C temperature range do not meet the idealcooling conditions as stated in AS2031-2012.

Analysis of aqueous samples typically involves the extraction/digestion and/or analysis of the liquid phase only (i.e. NOT any settledsediment phase but inclusive of suspended particles if present), unless stipulated on the Envirolab COC and/or by correspondence.Notable exceptions include certain Physical Tests (pH/EC/BOD/COD/Apparent Colour etc.), Solids testing, total recoverable metalsand PFAS where solids are included by default.

Measurement Uncertainty estimates are available for most tests upon request.

Where sampling dates are not provided, Envirolab are not in a position to comment on the validity of the analysis whererecommended technical holding times may have been breached.

When samples are received where certain analytes are outside of recommended technical holding times (THTs), the analysis hasproceeded. Where analytes are on the verge of breaching THTs, every effort will be made to analyse within the THT or as soon aspracticable.

In circumstances where no duplicate and/or sample spike has been reported at 1 in 10 and/or 1 in 20 samples respectively, thesample volume submitted was insufficient in order to satisfy laboratory QA/QC protocols.

Matrix Spikes, LCS and Surrogate recoveries: Generally 70-130% for inorganics/metals (not SPOCAS); 60-140% fororganics/SPOCAS (+/-50% surrogates) and 10-140% for labile SVOCs (including labile surrogates), ultra trace organics andspeciated phenols is acceptable.

Duplicates: >10xPQL - RPD acceptance criteria will vary depending on the analytes and the analytical techniques but is typically inthe range 20%-50% – see ELN-P05 QA/QC tables for details; <10xPQL - RPD are higher as the results approach PQL and theestimated measurement uncertainty will statistically increase.

For VOCs in water samples, three vials are required for duplicate or spike analysis.

Spikes for Physical and Aggregate Tests are not applicable.

Filters, swabs, wipes, tubes and badges will not have duplicate data as the whole sample is generally extracted during sampleextraction.

Duplicate sample and matrix spike recoveries may not be reported on smaller jobs, however, were analysed at a frequency to meetor exceed NEPM requirements. All samples are tested in batches of 20. The duplicate sample RPD and matrix spike recoveries forthe batch were within the laboratory acceptance criteria.

Laboratory Acceptance Criteria

Envirolab Reference: 236880

R00Revision No:

Page | 14 of 14

Page 105: Cover - Attach C14f

Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

SAMPLE RECEIPT ADVICE

Alex LathamAttention

AECOM Australia Pty Ltd (Sydney)Client

Client Details

24/02/2020Date Results Expected to be Reported

17/02/2020Date Instructions Received

17/02/2020Date Sample Received

236880Envirolab Reference

60623599_1.0Your reference

Sample Login Details

YESSampling Date Provided

IceCooling Method

18Temperature on Receipt (°C)

StandardTurnaround Time Requested

1 waterNo. of Samples Provided

YesSamples received in appropriate condition for analysis

Sample Condition

Nil

Comments

Please direct any queries to:

Email: [email protected]: [email protected]

Fax: 02 9910 6201Fax: 02 9910 6201

Phone: 02 9910 6200Phone: 02 9910 6200

Jacinta HurstAileen Hie

Analysis Underway, details on the following page:

Page | 1 of 2

Page 106: Cover - Attach C14f

Envirolab Services Pty Ltd

ABN 37 112 535 645

12 Ashley St Chatswood NSW 2067

ph 02 9910 6200 fax 02 9910 6201

[email protected]

www.envirolab.com.au

PPPPQC306_200212

HM

in

wa

ter

- d

iss

olv

ed

sv

TR

H (

C1

0-C

40

) in

Wa

ter

vT

RH

(C6

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BT

EX

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ate

r

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in

wa

ter

Sample ID

The ' THIS IS NOT A REPORT OF THE RESULTS.P' indicates the testing you have requested.

TAT for Micro is dependent on incubation. This varies from 3 to 6 days.

Please contact the laboratory immediately if observed settled sediment present in water samples is to be included in the extractionand/or analysis (exceptions include certain Physical Tests (pH/EC/BOD/COD/Apparent Colour etc.), Solids testing, Total Recoverablemetals and PFAS analysis where solids are included by default.

Requests for longer term sample storage must be received in writing.

Sample storage - Waters are routinely disposed of approximately 1 month and soils approximately 2 months from receipt.

Additional Info

Page | 2 of 2

Page 107: Cover - Attach C14f
Page 108: Cover - Attach C14f

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Page 110: Cover - Attach C14f

3 o

f 1

2:

Pa

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Wo

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Clie

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76

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28

-Ja

n-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2002

766

-013

ES

20027

66-0

11

ES

2002

766

-010

ES

2002766-0

03

ES

2002766-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

)

25.4

23.6

----

15

.63

2.9

%1

.0--

--M

ois

ture

Co

nte

nt

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

Yes

Asb

esto

s D

ete

cte

d--

--N

o*

----

----

g/k

g0

.11

33

2-2

1-4

Ch

+ A

m +

Cr

Asb

esto

s T

yp

e--

--C

h--

----

----

-1

33

2-2

1-4

No

Asb

esto

s (

Tra

ce)

----

No

----

----

Fib

res

51

33

2-2

1-4

521

----

506

----

----

g0

.01

----

Sam

ple

weig

ht

(dry

)

No

----

No

----

----

g/k

g0

.1--

--S

yn

theti

c M

inera

l F

ibre

No

----

No

----

----

g/k

g0

.1--

--O

rgan

ic F

ibre

A. S

MY

LIE

----

A.

SM

YL

IE--

----

----

---

--A

PP

RO

VE

D ID

EN

TIF

IER

:

EA

200N

: A

sb

esto

s Q

uan

tifi

cati

on

(n

on

-NA

TA

)

0.1

50

øA

sb

esto

s (

Fin

es a

nd

Fib

rou

s

<7m

m)

----

0.0

090

----

----

g0

.00

04

13

32

-21

-4

0.0

29

ø--

--0

.002

----

----

% (

w/w

)0

.00

1--

--A

sb

esto

s (

Fin

es a

nd

Fib

rou

s F

A+

AF

)

<0

.1ø

Asb

esto

s C

on

tain

ing

Mate

rial

----

<0

.1--

----

--g

0.1

13

32

-21

-4

<0

.01

øA

sb

esto

s C

on

tain

ing

Mate

rial

(as 1

5%

Asb

esto

s in

AC

M >

7m

m)

----

<0

.01

----

----

% (

w/w

)0

.01

13

32

-21

-4

0.5

21

ø--

--0

.506

----

----

kg0

.00

01

----

Weig

ht

Used

fo

r %

Calc

ula

tio

n

<0

.00

04

ø--

--<

0.0

00

4--

----

--g

0.0

00

4--

--F

ibro

us A

sb

esto

s >

7m

m

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

9A

rsen

ic28

----

89

4m

g/k

g5

74

40

-38

-2

1C

ad

miu

m13

----

62

mg

/kg

17

44

0-4

3-9

16

Ch

rom

ium

241

----

29

180

mg

/kg

27

44

0-4

7-3

369

Co

pp

er

10800

----

78

5986

mg

/kg

57

44

0-5

0-8

435

Lead

3780

----

28

053

50

mg

/kg

57

43

9-9

2-1

49

Nic

kel

241

----

17

9185

mg

/kg

27

44

0-0

2-0

820

Zin

c12400

----

30

711

10

mg

/kg

57

44

0-6

6-6

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

0.4

Merc

ury

2.2

----

0.6

1.0

mg

/kg

0.1

74

39

-97

-6

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

<0

.5N

ap

hth

ale

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.59

1-2

0-3

<0

.5A

cen

ap

hth

yle

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.52

08

-96

-8

<0

.5A

cen

ap

hth

en

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

83

-32

-9

<0

.5F

luo

ren

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

86

-73

-7

<0

.5P

hen

an

thre

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.58

5-0

1-8

Page 111: Cover - Attach C14f

4 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

BH

107_1.5

-1.7

BH

107_0.5

-0.6

BH

107_0.4

-0.5

BH

109_0.9

-1.0

BH

109_0.3

-0.4

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2002

766

-013

ES

20027

66-0

11

ES

2002

766

-010

ES

2002766-0

03

ES

2002766-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s -

Co

nti

nu

ed

<0

.5A

nth

racen

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

12

0-1

2-7

<0

.5F

luo

ran

then

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

20

6-4

4-0

<0

.5P

yre

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.51

29

-00

-0

<0

.5B

en

z(a)a

nth

racen

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

56

-55

-3

<0

.5C

hry

sen

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

21

8-0

1-9

<0

.5B

en

zo(b

+j)

flu

ora

nth

en

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

20

5-9

9-2

20

5-8

2-3

<0

.5B

en

zo(k

)flu

ora

nth

en

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

20

7-0

8-9

<0

.5B

en

zo(a

)pyre

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.55

0-3

2-8

<0

.5In

den

o(1

.2.3

.cd

)pyre

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.51

93

-39

-5

<0

.5D

iben

z(a.h

)an

thra

cen

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

53

-70

-3

<0

.5B

en

zo(g

.h.i)p

ery

len

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

19

1-2

4-2

<0

.5^

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.5--

--S

um

of

po

lycyclic a

rom

ati

c h

yd

rocarb

on

s

<0

.5^

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.5--

--B

en

zo(a

)pyre

ne T

EQ

(ze

ro)

0.6

^ 0.6

----

0.6

0.6

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(h

alf

LO

R)

1.2

^ 1.2

----

1.2

1.2

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(L

OR

)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<1

0<

10

----

<1

0<

10

mg

/kg

10

----

C6 -

C9 F

racti

on

<5

0<

50

----

<5

0<

50

mg

/kg

50

----

C10 -

C14 F

racti

on

<1

00

<1

00

----

<1

00

<1

00

mg

/kg

10

0--

--C

15 -

C28 F

racti

on

110

<1

00

----

10

0<

10

0m

g/k

g1

00

----

C29 -

C36 F

racti

on

110

^ <

50

----

10

0<

50

mg

/kg

50

----

C10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

<1

0C

6 -

C10 F

racti

on

<1

0--

--<

10

<1

0m

g/k

g1

0C

6_

C1

0

<1

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<1

0--

--<

10

<1

0m

g/k

g1

0C

6_

C1

0-B

TE

X

<5

0<

50

----

<5

0<

50

mg

/kg

50

----

>C

10 -

C16 F

racti

on

160

<1

00

----

15

0<

10

0m

g/k

g1

00

----

>C

16 -

C34 F

racti

on

<1

00

<1

00

----

<1

00

<1

00

mg

/kg

10

0--

-->

C34 -

C40 F

racti

on

160

^ <

50

----

15

0<

50

mg

/kg

50

----

>C

10 -

C40 F

racti

on

(su

m)

<5

0^

<5

0--

--<

50

<5

0m

g/k

g5

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<0

.2B

en

zen

e<

0.2

----

<0

.2<

0.2

mg

/kg

0.2

71

-43

-2

<0

.5T

olu

en

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

10

8-8

8-3

<0

.5E

thylb

en

zen

e<

0.5

----

<0

.5<

0.5

mg

/kg

0.5

10

0-4

1-4

Page 112: Cover - Attach C14f

5 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

BH

107_1.5

-1.7

BH

107_0.5

-0.6

BH

107_0.4

-0.5

BH

109_0.9

-1.0

BH

109_0.3

-0.4

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

02

8-J

an

-20

20

00

:00

28

-Ja

n-2

02

0 0

0:0

0C

lien

t sa

mp

ling

da

te /

tim

e

ES

2002

766

-013

ES

20027

66-0

11

ES

2002

766

-010

ES

2002766-0

03

ES

2002766-0

01

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

ltR

esu

ltR

esult

Result

EP

080:

BT

EX

N -

Co

nti

nu

ed

<0

.5m

eta

- &

para

-Xyle

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.51

08

-38

-3 1

06

-42

-3

<0

.5o

rth

o-X

yle

ne

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.59

5-4

7-6

<0

.2^

<0

.2--

--<

0.2

<0

.2m

g/k

g0

.2--

--S

um

of

BT

EX

<0

.5^

<0

.5--

--<

0.5

<0

.5m

g/k

g0

.5--

--T

ota

l X

yle

nes

<1

Nap

hth

ale

ne

<1

----

<1

<1

mg

/kg

19

1-2

0-3

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

84.7

Ph

en

ol-

d6

81.4

----

77

.58

2.2

%0

.51

31

27

-88

-3

88.9

2-C

hlo

rop

hen

ol-

D4

86.7

----

80

.08

6.7

%0

.59

39

51

-73

-6

80.8

2.4

.6-T

rib

rom

op

hen

ol

83.5

----

73

.07

7.5

%0

.51

18

-79

-6

EP

075(S

IM)T

: P

AH

Su

rro

gate

s

97.7

2-F

luo

rob

iph

en

yl

96.6

----

98

.29

6.9

%0

.53

21

-60

-8

91.9

An

thra

cen

e-d

10

91.5

----

78

.69

3.8

%0

.51

71

9-0

6-8

94.5

4-T

erp

hen

yl-

d14

94.6

----

88

.59

3.8

%0

.51

71

8-5

1-0

EP

080S

: T

PH

(V)/

BT

EX

Su

rro

gate

s

82.8

1.2

-Dic

hlo

roeth

an

e-D

491.2

----

84

.89

1.1

%0

.21

70

60

-07

-0

85.7

To

luen

e-D

8100

----

81

.99

9.4

%0

.22

03

7-2

6-5

88.2

4-B

rom

ofl

uo

rob

en

zen

e104

----

74

.69

9.0

%0

.24

60

-00

-4

Page 113: Cover - Attach C14f

6 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

113_0.6

-0.7

BH

113_0.2

-0.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

29

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2002766-0

18

ES

2002766-0

16

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

)

13.0

12.1

----

----

----

%1

.0--

--M

ois

ture

Co

nte

nt

EA

200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

So

ils

Yes

Asb

esto

s D

ete

cte

dN

o--

----

----

--g

/kg

0.1

13

32

-21

-4

Ch

Asb

esto

s T

yp

e-

----

----

----

---

13

32

-21

-4

No

Asb

esto

s (

Tra

ce)

No

----

----

----

Fib

res

51

33

2-2

1-4

429

523

----

----

----

g0

.01

----

Sam

ple

weig

ht

(dry

)

No

No

----

----

----

g/k

g0

.1--

--S

yn

theti

c M

inera

l F

ibre

No

No

----

----

----

g/k

g0

.1--

--O

rgan

ic F

ibre

A. S

MY

LIE

A. S

MY

LIE

----

----

----

---

----

AP

PR

OV

ED

ID

EN

TIF

IER

:

EA

200N

: A

sb

esto

s Q

uan

tifi

cati

on

(n

on

-NA

TA

)

0.0

512

øA

sb

esto

s (

Fin

es a

nd

Fib

rou

s

<7m

m)

<0

.00

04

----

----

----

g0

.00

04

13

32

-21

-4

0.0

12

ø<

0.0

01

----

----

----

% (

w/w

)0

.00

1--

--A

sb

esto

s (

Fin

es a

nd

Fib

rou

s F

A+

AF

)

<0

.1ø

Asb

esto

s C

on

tain

ing

Mate

rial

<0

.1--

----

----

--g

0.1

13

32

-21

-4

<0

.01

øA

sb

esto

s C

on

tain

ing

Mate

rial

(as 1

5%

Asb

esto

s in

AC

M >

7m

m)

<0

.01

----

----

----

% (

w/w

)0

.01

13

32

-21

-4

0.4

29

ø0.5

23

----

----

----

kg0

.00

01

----

Weig

ht

Used

fo

r %

Calc

ula

tio

n

<0

.00

04

ø<

0.0

00

4--

----

----

--g

0.0

00

4--

--F

ibro

us A

sb

esto

s >

7m

m

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

46

Ars

en

ic18

----

----

----

mg

/kg

57

44

0-3

8-2

2C

ad

miu

m1

----

----

----

mg

/kg

17

44

0-4

3-9

28

Ch

rom

ium

22

----

----

----

mg

/kg

27

44

0-4

7-3

776

Co

pp

er

732

----

----

----

mg

/kg

57

44

0-5

0-8

4840

Lead

336

----

----

----

mg

/kg

57

43

9-9

2-1

69

Nic

kel

21

----

----

----

mg

/kg

27

44

0-0

2-0

1160

Zin

c752

----

----

----

mg

/kg

57

44

0-6

6-6

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

1.0

Merc

ury

0.4

----

----

----

mg

/kg

0.1

74

39

-97

-6

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

)

<0

.1--

----

----

----

--m

g/k

g0

.1--

--T

ota

l P

oly

ch

lori

nate

d b

iph

en

yls

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

)

<0

.05

alp

ha-B

HC

----

----

----

----

mg

/kg

0.0

53

19

-84

-6

<0

.05

Hexach

loro

ben

zen

e (

HC

B)

----

----

----

----

mg

/kg

0.0

51

18

-74

-1

<0

.05

beta

-BH

C--

----

----

----

--m

g/k

g0

.05

31

9-8

5-7

Page 114: Cover - Attach C14f

7 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

113_0.6

-0.7

BH

113_0.2

-0.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

29

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2002766-0

18

ES

2002766-0

16

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) -

Co

nti

nu

ed

<0

.05

gam

ma-B

HC

----

----

----

----

mg

/kg

0.0

55

8-8

9-9

<0

.05

delt

a-B

HC

----

----

----

----

mg

/kg

0.0

53

19

-86

-8

<0

.05

Hep

tach

lor

----

----

----

----

mg

/kg

0.0

57

6-4

4-8

<0

.05

Ald

rin

----

----

----

----

mg

/kg

0.0

53

09

-00

-2

<0

.05

Hep

tach

lor

ep

oxid

e--

----

----

----

--m

g/k

g0

.05

10

24

-57

-3

<0

.05

^ --

----

----

----

--m

g/k

g0

.05

----

To

tal C

hlo

rdan

e (

su

m)

<0

.05

tran

s-C

hlo

rdan

e--

----

----

----

--m

g/k

g0

.05

51

03

-74

-2

<0

.05

alp

ha-E

nd

osu

lfan

----

----

----

----

mg

/kg

0.0

59

59

-98

-8

<0

.05

cis

-Ch

lord

an

e--

----

----

----

--m

g/k

g0

.05

51

03

-71

-9

0.3

4D

ield

rin

----

----

----

----

mg

/kg

0.0

56

0-5

7-1

<0

.05

4.4

`-D

DE

----

----

----

----

mg

/kg

0.0

57

2-5

5-9

<0

.05

En

dri

n--

----

----

----

--m

g/k

g0

.05

72

-20

-8

<0

.05

beta

-En

do

su

lfan

----

----

----

----

mg

/kg

0.0

53

32

13

-65

-9

<0

.05

^ E

nd

osu

lfan

(su

m)

----

----

----

----

mg

/kg

0.0

51

15

-29

-7

<0

.05

4.4

`-D

DD

----

----

----

----

mg

/kg

0.0

57

2-5

4-8

<0

.05

En

dri

n a

ldeh

yd

e--

----

----

----

--m

g/k

g0

.05

74

21

-93

-4

<0

.05

En

do

su

lfan

su

lfate

----

----

----

----

mg

/kg

0.0

51

03

1-0

7-8

<0

.24.4

`-D

DT

----

----

----

----

mg

/kg

0.2

50

-29

-3

<0

.05

En

dri

n k

eto

ne

----

----

----

----

mg

/kg

0.0

55

34

94

-70

-5

<0

.2M

eth

oxych

lor

----

----

----

----

mg

/kg

0.2

72

-43

-5

0.3

4^

Su

m o

f A

ldri

n +

Die

ldri

n--

----

----

----

--m

g/k

g0

.05

30

9-0

0-2

/60

-57

-1

<0

.05

^ S

um

of

DD

D +

DD

E +

DD

T--

----

----

----

--m

g/k

g0

.05

72

-54

-8/7

2-5

5-9

/5

0-2

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

)

<0

.05

Dic

hlo

rvo

s--

----

----

----

--m

g/k

g0

.05

62

-73

-7

<0

.05

Dem

eto

n-S

-meth

yl

----

----

----

----

mg

/kg

0.0

59

19

-86

-8

<0

.2M

on

ocro

top

ho

s--

----

----

----

--m

g/k

g0

.26

92

3-2

2-4

<0

.05

Dim

eth

oate

----

----

----

----

mg

/kg

0.0

56

0-5

1-5

<0

.05

Dia

zin

on

----

----

----

----

mg

/kg

0.0

53

33

-41

-5

<0

.05

Ch

lorp

yri

fos-m

eth

yl

----

----

----

----

mg

/kg

0.0

55

59

8-1

3-0

<0

.2P

ara

thio

n-m

eth

yl

----

----

----

----

mg

/kg

0.2

29

8-0

0-0

<0

.05

Mala

thio

n--

----

----

----

--m

g/k

g0

.05

12

1-7

5-5

<0

.05

Fen

thio

n--

----

----

----

--m

g/k

g0

.05

55

-38

-9

<0

.05

Ch

lorp

yri

fos

----

----

----

----

mg

/kg

0.0

52

92

1-8

8-2

<0

.2P

ara

thio

n--

----

----

----

--m

g/k

g0

.25

6-3

8-2

Page 115: Cover - Attach C14f

8 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

113_0.6

-0.7

BH

113_0.2

-0.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

29

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2002766-0

18

ES

2002766-0

16

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) -

Co

nti

nu

ed

<0

.05

Pir

imp

ho

s-e

thyl

----

----

----

----

mg

/kg

0.0

52

35

05

-41

-1

<0

.05

Ch

lorf

en

vin

ph

os

----

----

----

----

mg

/kg

0.0

54

70

-90

-6

<0

.05

Bro

mo

ph

os-e

thyl

----

----

----

----

mg

/kg

0.0

54

82

4-7

8-6

<0

.05

Fen

am

iph

os

----

----

----

----

mg

/kg

0.0

52

22

24

-92

-6

<0

.05

Pro

thio

fos

----

----

----

----

mg

/kg

0.0

53

46

43

-46

-4

<0

.05

Eth

ion

----

----

----

----

mg

/kg

0.0

55

63

-12

-2

<0

.05

Carb

op

hen

oth

ion

----

----

----

----

mg

/kg

0.0

57

86

-19

-6

<0

.05

Azi

np

ho

s M

eth

yl

----

----

----

----

mg

/kg

0.0

58

6-5

0-0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

<0

.5N

ap

hth

ale

ne

<0

.5--

----

----

--m

g/k

g0

.59

1-2

0-3

<0

.5A

cen

ap

hth

yle

ne

<0

.5--

----

----

--m

g/k

g0

.52

08

-96

-8

<0

.5A

cen

ap

hth

en

e<

0.5

----

----

----

mg

/kg

0.5

83

-32

-9

<0

.5F

luo

ren

e<

0.5

----

----

----

mg

/kg

0.5

86

-73

-7

<0

.5P

hen

an

thre

ne

<0

.5--

----

----

--m

g/k

g0

.58

5-0

1-8

<0

.5A

nth

racen

e<

0.5

----

----

----

mg

/kg

0.5

12

0-1

2-7

<0

.5F

luo

ran

then

e0.8

----

----

----

mg

/kg

0.5

20

6-4

4-0

<0

.5P

yre

ne

0.7

----

----

----

mg

/kg

0.5

12

9-0

0-0

<0

.5B

en

z(a)a

nth

racen

e<

0.5

----

----

----

mg

/kg

0.5

56

-55

-3

<0

.5C

hry

sen

e<

0.5

----

----

----

mg

/kg

0.5

21

8-0

1-9

<0

.5B

en

zo(b

+j)

flu

ora

nth

en

e<

0.5

----

----

----

mg

/kg

0.5

20

5-9

9-2

20

5-8

2-3

<0

.5B

en

zo(k

)flu

ora

nth

en

e<

0.5

----

----

----

mg

/kg

0.5

20

7-0

8-9

<0

.5B

en

zo(a

)pyre

ne

<0

.5--

----

----

--m

g/k

g0

.55

0-3

2-8

<0

.5In

den

o(1

.2.3

.cd

)pyre

ne

<0

.5--

----

----

--m

g/k

g0

.51

93

-39

-5

<0

.5D

iben

z(a.h

)an

thra

cen

e<

0.5

----

----

----

mg

/kg

0.5

53

-70

-3

<0

.5B

en

zo(g

.h.i)p

ery

len

e<

0.5

----

----

----

mg

/kg

0.5

19

1-2

4-2

<0

.5^

1.5

----

----

----

mg

/kg

0.5

----

Su

m o

f p

oly

cyclic a

rom

ati

c h

yd

rocarb

on

s

<0

.5^

<0

.5--

----

----

--m

g/k

g0

.5--

--B

en

zo(a

)pyre

ne T

EQ

(ze

ro)

0.6

^ 0.6

----

----

----

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(h

alf

LO

R)

1.2

^ 1.2

----

----

----

mg

/kg

0.5

----

Ben

zo(a

)pyre

ne T

EQ

(L

OR

)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

<1

0<

10

----

----

----

mg

/kg

10

----

C6 -

C9 F

racti

on

<5

0<

50

----

----

----

mg

/kg

50

----

C10 -

C14 F

racti

on

<1

00

130

----

----

----

mg

/kg

10

0--

--C

15 -

C28 F

racti

on

<1

00

140

----

----

----

mg

/kg

10

0--

--C

29 -

C36 F

racti

on

Page 116: Cover - Attach C14f

9 o

f 1

2:

Pa

ge

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

BH

113_0.6

-0.7

BH

113_0.2

-0.3

Clie

nt

sam

ple

ID

Su

b-M

atr

ix:

SO

IL

(M

atr

ix:

SO

IL)

----

----

----

29

-Ja

n-2

02

0 0

0:0

02

9-J

an

-20

20

00

:00

Clie

nt

sam

plin

g d

ate

/ t

ime

----

----

----

----

----

----

ES

2002766-0

18

ES

2002766-0

16

Un

itL

OR

CA

S N

um

be

rC

om

po

un

d

Resu

ltR

esu

lt--

----

----

--

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s -

Co

nti

nu

ed

<5

0^

270

----

----

----

mg

/kg

50

----

C10 -

C36 F

racti

on

(su

m)

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

<1

0C

6 -

C10 F

racti

on

<1

0--

----

----

--m

g/k

g1

0C

6_

C1

0

<1

0^

C6 -

C10 F

racti

on

m

inu

s B

TE

X

(F1)

<1

0--

----

----

--m

g/k

g1

0C

6_

C1

0-B

TE

X

<5

0<

50

----

----

----

mg

/kg

50

----

>C

10 -

C16 F

racti

on

<1

00

240

----

----

----

mg

/kg

10

0--

-->

C16 -

C34 F

racti

on

<1

00

<1

00

----

----

----

mg

/kg

10

0--

-->

C34 -

C40 F

racti

on

<5

0^

240

----

----

----

mg

/kg

50

----

>C

10 -

C40 F

racti

on

(su

m)

<5

0^

<5

0--

----

----

--m

g/k

g5

0--

-->

C10 -

C16 F

racti

on

min

us N

ap

hth

ale

ne

(F2)

EP

080:

BT

EX

N

<0

.2B

en

zen

e<

0.2

----

----

----

mg

/kg

0.2

71

-43

-2

<0

.5T

olu

en

e<

0.5

----

----

----

mg

/kg

0.5

10

8-8

8-3

<0

.5E

thylb

en

zen

e<

0.5

----

----

----

mg

/kg

0.5

10

0-4

1-4

<0

.5m

eta

- &

para

-Xyle

ne

<0

.5--

----

----

--m

g/k

g0

.51

08

-38

-3 1

06

-42

-3

<0

.5o

rth

o-X

yle

ne

<0

.5--

----

----

--m

g/k

g0

.59

5-4

7-6

<0

.2^

<0

.2--

----

----

--m

g/k

g0

.2--

--S

um

of

BT

EX

<0

.5^

<0

.5--

----

----

--m

g/k

g0

.5--

--T

ota

l X

yle

nes

<1

Nap

hth

ale

ne

<1

----

----

----

mg

/kg

19

1-2

0-3

EP

066S

: P

CB

Su

rro

gate

81.8

Decach

loro

bip

hen

yl

----

----

----

----

%0

.12

05

1-2

4-3

EP

068S

: O

rgan

och

lori

ne P

esti

cid

e S

urr

og

ate

89.5

Dib

rom

o-D

DE

----

----

----

----

%0

.05

21

65

5-7

3-2

EP

068T

: O

rgan

op

ho

sp

ho

rus P

esti

cid

e S

urr

og

ate

74.5

DE

F--

----

----

----

--%

0.0

57

8-4

8-8

EP

075(S

IM)S

: P

hen

olic C

om

po

un

d S

urr

og

ate

s

76.7

Ph

en

ol-

d6

83.8

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1-0

Page 117: Cover - Attach C14f

10

of

12

:P

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e

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ES

20

02

76

6

60

62

35

99

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ject

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M A

ust

ralia

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aly

tical R

esu

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(M

atr

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Page 118: Cover - Attach C14f

11

of

12

:P

ag

e

Wo

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rde

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nt

ES

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02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

An

aly

tical R

esu

lts

----

----

----

----

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300

TB

Clie

nt

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ple

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b-M

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ix:

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TE

R

(M

atr

ix:

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TE

R)

----

----

----

----

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n-2

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0 0

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t sa

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ling

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te /

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e

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om

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lt--

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tal P

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Page 119: Cover - Attach C14f

12

of

12

:P

ag

e

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rk O

rde

r: :

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nt

ES

20

02

76

6

60

62

35

99

_1

.1:

Pro

ject

AE

CO

M A

ust

ralia

Pty

Ltd

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rro

gate

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ntr

ol L

imit

s

Reco

very

Lim

its (

%)

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Page 120: Cover - Attach C14f

Fals

e 4 4

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Tru

e

Envir

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QU

AL

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NT

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OR

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277-2

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+61 0

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:

No

. o

f sa

mp

les

an

aly

sed

8:

This

report

supers

edes

any

pre

vious

report

(s)

with

this

refe

rence

. R

esu

lts a

pply

to the s

am

ple

(s)

as

subm

itted. T

his

docu

ment sh

all

not be r

epro

duce

d, exc

ept in

full.

This

Qualit

y C

ontr

ol R

eport

conta

ins

the follo

win

g in

form

atio

n:

l

La

bo

rato

ry D

up

lica

te (

DU

P)

Re

po

rt;

Re

lativ

e P

erc

en

tag

e D

iffe

ren

ce (

RP

D)

an

d A

cce

pta

nce

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its

l

Me

tho

d B

lan

k (M

B)

an

d L

ab

ora

tory

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ntr

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po

rt;

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cove

ry a

nd

Acc

ep

tan

ce L

imits

l

Ma

trix

Sp

ike

(M

S)

Re

po

rt;

Re

cove

ry a

nd

Acc

ep

tan

ce L

imits

Sig

nato

ries

This

docu

ment has

been e

lect

ronic

ally

sig

ned b

y th

e a

uth

orize

d s

ignato

ries

belo

w. E

lect

ronic

sig

nin

g is

carr

ied o

ut in

com

plia

nce

with

pro

cedure

s sp

eci

fied in

21 C

FR

Part

11.

Sig

na

torie

sA

ccre

dita

tion

Ca

teg

ory

Po

sitio

n

Ala

na

Sm

ylie

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est

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wca

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|

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Page 121: Cover - Attach C14f

2 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

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Ltd

60

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Gen

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e

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use

d

by

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me

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h

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b

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fr

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sta

blis

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d

inte

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ally

re

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a

s th

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p

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b

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e

US

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AP

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, A

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an

d

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h

ou

se

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are

em

plo

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in t

he

ab

sen

ce o

f d

ocu

me

nte

d s

tan

da

rds

or

by

clie

nt

req

ue

st.

Wh

ere

mo

istu

re d

ete

rmin

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n h

as

be

en

pe

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lts a

re r

ep

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ry w

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ep

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less

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(<

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to

prim

ary

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est

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n a

nd

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aly

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re t

he

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f a

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po

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iffe

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nd

ard

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this

ma

y b

e d

ue

to

hig

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ois

ture

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nt,

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le (

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uce

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eig

ht

em

plo

yed

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r m

atr

ix in

terf

ere

nce

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on

ymo

us

= R

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rs t

o s

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ple

s w

hic

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re n

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cific

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rt o

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ork

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er

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t fo

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d p

art

of

the

QC

pro

cess

lot

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um

be

r =

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eg

istr

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um

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r fr

om

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acts

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rvic

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a d

ivis

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n C

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oci

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en

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iffe

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#

= I

nd

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tes

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lect

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lab

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sp

lit.

La

bo

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ry

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plic

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s

pro

vid

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info

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tion

re

ga

rdin

g

me

tho

d

pre

cisi

on

a

nd

sa

mp

le

he

tero

ge

ne

ity.

Th

e

pe

rmitt

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ra

ng

es

for

the

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ela

tive

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en

t D

evi

atio

n

(RP

D)

of

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bo

rato

ry

Du

plic

ate

s a

re

sp

ecifi

ed

in

A

LS

M

eth

od

Q

WI-

EN

/38

an

d

are

d

ep

en

de

nt

on

th

e

ma

gn

itud

e

of

resu

lts

in

com

pa

riso

n

to

the

le

vel

of

rep

ort

ing

: R

esu

lt <

1

0 t

ime

s

LO

R:

No

Lim

it; R

esu

lt b

etw

ee

n 1

0 a

nd

20

tim

es

LO

R:

0%

- 5

0%

; R

esu

lt >

20

tim

es

LO

R:

0%

- 2

0%

.

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

C L

ot:

2836485)

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

19

-00

1

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g4

04

10

.00

0%

- 2

0%

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g1

33

13

30

.00

0%

- 2

0%

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

<5

0.0

0N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g3

94

02

.80

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

5<

50

.00

No

Lim

it

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

51

52

2.4

60

% -

50

%

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

28

07

-00

6

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g6

70

.00

No

Lim

it

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g3

30

.00

No

Lim

it

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

89

20

.3N

o L

imit

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g7

70

.00

No

Lim

it

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g1

81

23

8.3

No

Lim

it

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

11

11

19

7.3

30

% -

20

%

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

) (

QC

Lo

t: 2

836488)

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

5.9

5.6

4.7

0N

o L

imit

An

on

ymo

us

ES

20

02

71

9-0

02

EA

05

5:

Mo

istu

re C

on

ten

t--

--0

.1%

15

.81

3.3

17

.20

% -

50

%A

no

nym

ou

s E

S2

00

28

07

-01

3

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

C L

ot:

2836486)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

<0

.10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

19

-00

1

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

<0

.10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

28

07

-00

6

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

834940)

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.1<

0.1

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

90

1-0

05

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.1<

0.1

0.0

0N

o L

imit

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

6

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

834939)

Page 122: Cover - Attach C14f

3 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

834939)

- c

on

tin

ued

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

90

1-0

05

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-E

nd

osu

lfa

n3

32

13

-65

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

ald

eh

yde

74

21

-93

-40

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

6

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

0.3

40

.42

22

.3N

o L

imit

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

be

ta-E

nd

osu

lfan

33

21

3-6

5-9

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

En

drin

ald

eh

yd

e7

42

1-9

3-4

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

Page 123: Cover - Attach C14f

4 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

834939)

- c

on

tin

ued

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itB

H1

13

_0

.2-0

.3

ES

20

02

76

6-0

16

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

834939)

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

itA

no

nym

ou

s E

S2

00

29

01

-00

5

EP

06

8:

De

me

ton

-S-m

eth

yl

91

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl

55

98

-13

-00

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Pirim

ph

os-e

thyl

23

50

5-4

1-1

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

it

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

itB

H1

13

_0

.2-0

.3

ES

20

02

76

6-0

16

EP

06

8:

De

me

ton

-S-m

eth

yl

91

9-8

6-8

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl

55

98

-13

-00

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Pirim

ph

os-e

thyl

23

50

5-4

1-1

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

<0

.05

0.0

0N

o L

imit

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

5<

0.0

50

.00

No

Lim

it

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.2<

0.2

0.0

0N

o L

imit

Page 124: Cover - Attach C14f

5 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

834939)

- c

on

tin

ued

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itB

H1

13

_0

.2-0

.3

ES

20

02

76

6-0

16

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

C L

ot:

2834938)

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

90

1-0

05

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

6

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

0.6

25

.3N

o L

imit

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

0.6

26

.4N

o L

imit

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

nth

en

e2

05

-99

-2

20

5-8

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(k)f

luo

ran

the

ne

20

7-0

8-9

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

07

5(S

IM):

Be

nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

Page 125: Cover - Attach C14f

6 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

C L

ot:

2834938)

- c

on

tin

ued

EP

07

5(S

IM):

Su

m o

f p

oly

cycl

ic a

rom

atic

hyd

roca

rbo

ns

----

0.5

mg

/kg

<0

.51

.28

2.4

No

Lim

itB

H1

13

_0

.2-0

.3

ES

20

02

76

6-0

16

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

TE

Q (

zero

)--

--0

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2834894)

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

71

9-0

01

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

0<

10

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

90

1-0

01

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2834937)

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

29

01

-00

5

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

itB

H1

13

_0

.2-0

.3

ES

20

02

76

6-0

16

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

0<

10

00

.00

No

Lim

it

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

<5

0<

50

0.0

0N

o L

imit

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2834894)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

19

-00

1

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

0m

g/k

g<

10

<1

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

29

01

-00

1

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2834937)

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

90

1-0

05

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

--5

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

07

1:

>C

16

- C

34

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

6

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

<1

00

<1

00

0.0

0N

o L

imit

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

--5

0m

g/k

g<

50

<5

00

.00

No

Lim

it

EP

080:

BT

EX

N (Q

C L

ot:

2834894)

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

19

-00

1

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

it

EP

08

0:

Be

nze

ne

71

-43

-20

.2m

g/k

g<

0.2

<0

.20

.00

No

Lim

itA

no

nym

ou

s E

S2

00

29

01

-00

1

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

.5m

g/k

g<

0.5

<0

.50

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

0.5

mg

/kg

<0

.5<

0.5

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

1m

g/k

g<

1<

10

.00

No

Lim

it

Page 126: Cover - Attach C14f

7 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

WA

TE

RL

ab

ora

tory

Du

pli

cate

(D

UP

) R

ep

ort

Ori

gin

al R

esu

ltR

PD

(%

)L

ab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

Du

pli

cate

Resu

ltR

eco

very

Lim

its (

%)

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

C L

ot:

2837679)

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

25

32

-00

1

EP

08

0:

C6

- C

9 F

ract

ion

----

20

µg

/L<

20

<2

00

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

71

-00

3

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

C L

ot:

2837679)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

53

2-0

01

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

02

g/L

<2

0<

20

0.0

0N

o L

imit

An

on

ymo

us

ES

20

02

77

1-0

03

EP

080:

BT

EX

N (Q

C L

ot:

2837679)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

25

32

-00

1

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

1<

10

.00

No

Lim

itA

no

nym

ou

s E

S2

00

27

71

-00

3

EP

08

0:

To

lue

ne

10

8-8

8-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

µg

/L<

2<

20

.00

No

Lim

it

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

2-3

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

ort

ho

-Xyl

en

e9

5-4

7-6

g/L

<2

<2

0.0

0N

o L

imit

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

g/L

<5

<5

0.0

0N

o L

imit

Page 127: Cover - Attach C14f

8 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Meth

od

Bla

nk (

MB

) an

d L

ab

ora

tory

Co

ntr

ol S

pik

e (

LC

S)

Rep

ort

Th

e

qu

alit

y co

ntr

ol

term

M

eth

od

/

La

bo

rato

ry

Bla

nk

refe

rs

to

an

a

na

lyte

fr

ee

m

atr

ix

to

wh

ich

a

ll re

ag

en

ts

are

a

dd

ed

in

th

e

sam

e

volu

me

s

or

pro

po

rtio

ns

as

use

d

in

sta

nd

ard

sa

mp

le

pre

pa

ratio

n.

Th

e

pu

rpo

se

o

f th

is

QC

pa

ram

ete

r is

to

m

on

itor

po

ten

tial

lab

ora

tory

co

nta

min

atio

n.

Th

e

qu

alit

y co

ntr

ol

term

L

ab

ora

tory

C

on

tro

l S

pik

e

(LC

S)

refe

rs

to

a

cert

ifie

d

refe

ren

ce

ma

teria

l, o

r a

kn

ow

n

inte

rfe

ren

ce

fre

e

ma

trix

sp

ike

d

with

ta

rge

t

an

aly

tes.

Th

e p

urp

ose

of

this

QC

pa

ram

ete

r is

to

mo

nito

r m

eth

od

pre

cisi

on

an

d a

ccu

racy

in

de

pe

nd

en

t o

f sa

mp

le m

atr

ix.

Dyn

am

ic R

eco

very

Lim

its

are

ba

sed

on

sta

tistic

al e

valu

atio

n o

f p

roce

sse

d L

CS

.

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

2836485)

EG

00

5T

: A

rse

nic

74

40

-38

-25

mg

/kg

<5

10

22

1.7

mg

/kg

12

68

6.0

EG

00

5T

: C

ad

miu

m7

44

0-4

3-9

1m

g/k

g<

19

6.2

4.6

4 m

g/k

g1

13

83

.0

EG

00

5T

: C

hro

miu

m7

44

0-4

7-3

2m

g/k

g<

21

11

43

.9 m

g/k

g1

28

76

.0

EG

00

5T

: C

op

pe

r7

44

0-5

0-8

5m

g/k

g<

59

8.9

32

mg

/kg

12

08

6.0

EG

00

5T

: L

ea

d7

43

9-9

2-1

5m

g/k

g<

59

6.7

40

mg

/kg

11

48

0.0

EG

00

5T

: N

icke

l7

44

0-0

2-0

2m

g/k

g<

21

02

55

mg

/kg

12

38

7.0

EG

00

5T

: Z

inc

74

40

-66

-65

mg

/kg

<5

10

26

0.8

mg

/kg

12

28

0.0

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

CL

ot:

2836486)

EG

03

5T

: M

erc

ury

74

39

-97

-60

.1m

g/k

g<

0.1

77

.02

.57

mg

/kg

10

57

0.0

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

834940)

EP

06

6:

To

tal P

oly

chlo

rin

ate

d b

iph

en

yls

----

0.1

mg

/kg

<0

.11

08

1 m

g/k

g1

26

62

.0

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

834939)

EP

06

8:

alp

ha

-BH

C3

19

-84

-60

.05

mg

/kg

<0

.05

84

.40

.5 m

g/k

g1

13

69

.0

EP

06

8:

He

xach

loro

be

nze

ne

(H

CB

)1

18

-74

-10

.05

mg

/kg

<0

.05

10

00

.5 m

g/k

g1

17

65

.0

EP

06

8:

be

ta-B

HC

31

9-8

5-7

0.0

5m

g/k

g<

0.0

59

5.1

0.5

mg

/kg

11

96

7.0

EP

06

8:

ga

mm

a-B

HC

58

-89

-90

.05

mg

/kg

<0

.05

93

.60

.5 m

g/k

g1

16

68

.0

EP

06

8:

de

lta-B

HC

31

9-8

6-8

0.0

5m

g/k

g<

0.0

59

5.0

0.5

mg

/kg

11

76

5.0

EP

06

8:

He

pta

chlo

r7

6-4

4-8

0.0

5m

g/k

g<

0.0

58

6.5

0.5

mg

/kg

11

56

7.0

EP

06

8:

Ald

rin

30

9-0

0-2

0.0

5m

g/k

g<

0.0

58

2.8

0.5

mg

/kg

11

56

9.0

EP

06

8:

He

pta

chlo

r e

po

xid

e1

02

4-5

7-3

0.0

5m

g/k

g<

0.0

58

9.4

0.5

mg

/kg

11

86

2.0

EP

06

8:

tra

ns-

Ch

lord

an

e5

10

3-7

4-2

0.0

5m

g/k

g<

0.0

58

9.1

0.5

mg

/kg

11

76

3.0

EP

06

8:

alp

ha

-En

do

sulfa

n9

59

-98

-80

.05

mg

/kg

<0

.05

86

.20

.5 m

g/k

g1

16

66

.0

EP

06

8:

cis-

Ch

lord

an

e5

10

3-7

1-9

0.0

5m

g/k

g<

0.0

58

1.3

0.5

mg

/kg

11

66

4.0

EP

06

8:

Die

ldrin

60

-57

-10

.05

mg

/kg

<0

.05

78

.00

.5 m

g/k

g1

16

66

.0

EP

06

8:

4.4

`-D

DE

72

-55

-90

.05

mg

/kg

<0

.05

92

.40

.5 m

g/k

g1

15

67

.0

EP

06

8:

En

drin

72

-20

-80

.05

mg

/kg

<0

.05

77

.90

.5 m

g/k

g1

23

67

.0

EP

06

8:

be

ta-E

nd

osu

lfan

33

21

3-6

5-9

0.0

5m

g/k

g<

0.0

58

3.0

0.5

mg

/kg

11

56

9.0

EP

06

8:

4.4

`-D

DD

72

-54

-80

.05

mg

/kg

<0

.05

88

.20

.5 m

g/k

g1

21

69

.0

EP

06

8:

En

drin

ald

eh

yde

74

21

-93

-40

.05

mg

/kg

<0

.05

76

.60

.5 m

g/k

g1

20

56

.0

EP

06

8:

En

do

sulfa

n s

ulfa

te1

03

1-0

7-8

0.0

5m

g/k

g<

0.0

51

08

0.5

mg

/kg

12

46

2.0

EP

06

8:

4.4

`-D

DT

50

-29

-30

.2m

g/k

g<

0.2

10

20

.5 m

g/k

g1

20

66

.0

EP

06

8:

En

drin

ke

ton

e5

34

94

-70

-50

.05

mg

/kg

<0

.05

10

00

.5 m

g/k

g1

22

64

.0

EP

06

8:

Me

tho

xych

lor

72

-43

-50

.2m

g/k

g<

0.2

92

.80

.5 m

g/k

g1

30

54

.0

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

834939)

Page 128: Cover - Attach C14f

9 o

f 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

834939)

- c

on

tin

ued

EP

06

8:

Dic

hlo

rvo

s6

2-7

3-7

0.0

5m

g/k

g<

0.0

58

4.3

0.5

mg

/kg

11

95

9.0

EP

06

8:

De

me

ton

-S-m

eth

yl9

19

-86

-80

.05

mg

/kg

<0

.05

80

.30

.5 m

g/k

g1

28

62

.0

EP

06

8:

Mo

no

cro

top

ho

s6

92

3-2

2-4

0.2

mg

/kg

<0

.27

6.8

0.5

mg

/kg

12

65

4.0

EP

06

8:

Dim

eth

oa

te6

0-5

1-5

0.0

5m

g/k

g<

0.0

58

5.5

0.5

mg

/kg

11

96

7.0

EP

06

8:

Dia

zin

on

33

3-4

1-5

0.0

5m

g/k

g<

0.0

59

2.2

0.5

mg

/kg

12

07

0.0

EP

06

8:

Ch

lorp

yrifo

s-m

eth

yl5

59

8-1

3-0

0.0

5m

g/k

g<

0.0

57

6.4

0.5

mg

/kg

12

07

2.0

EP

06

8:

Pa

rath

ion

-me

thyl

29

8-0

0-0

0.2

mg

/kg

<0

.27

7.9

0.5

mg

/kg

12

06

8.0

EP

06

8:

Ma

lath

ion

12

1-7

5-5

0.0

5m

g/k

g<

0.0

58

5.4

0.5

mg

/kg

12

26

8.0

EP

06

8:

Fe

nth

ion

55

-38

-90

.05

mg

/kg

<0

.05

80

.40

.5 m

g/k

g1

17

69

.0

EP

06

8:

Ch

lorp

yrifo

s2

92

1-8

8-2

0.0

5m

g/k

g<

0.0

58

1.4

0.5

mg

/kg

11

87

6.0

EP

06

8:

Pa

rath

ion

56

-38

-20

.2m

g/k

g<

0.2

84

.20

.5 m

g/k

g1

22

64

.0

EP

06

8:

Pirim

ph

os-

eth

yl2

35

05

-41

-10

.05

mg

/kg

<0

.05

91

.10

.5 m

g/k

g1

16

70

.0

EP

06

8:

Ch

lorf

en

vin

ph

os

47

0-9

0-6

0.0

5m

g/k

g<

0.0

58

9.6

0.5

mg

/kg

12

16

9.0

EP

06

8:

Bro

mo

ph

os-

eth

yl4

82

4-7

8-6

0.0

5m

g/k

g<

0.0

58

3.2

0.5

mg

/kg

11

86

6.0

EP

06

8:

Fe

na

mip

ho

s2

22

24

-92

-60

.05

mg

/kg

<0

.05

10

40

.5 m

g/k

g1

24

68

.0

EP

06

8:

Pro

thio

fos

34

64

3-4

6-4

0.0

5m

g/k

g<

0.0

58

4.9

0.5

mg

/kg

11

26

2.0

EP

06

8:

Eth

ion

56

3-1

2-2

0.0

5m

g/k

g<

0.0

57

9.3

0.5

mg

/kg

12

06

8.0

EP

06

8:

Ca

rbo

ph

en

oth

ion

78

6-1

9-6

0.0

5m

g/k

g<

0.0

58

4.8

0.5

mg

/kg

12

76

5.0

EP

06

8:

Azi

np

ho

s M

eth

yl8

6-5

0-0

0.0

5m

g/k

g<

0.0

59

9.1

0.5

mg

/kg

12

34

1.0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

2834938)

EP

07

5(S

IM):

Na

ph

tha

len

e9

1-2

0-3

0.5

mg

/kg

<0

.59

7.7

6 m

g/k

g1

25

77

.0

EP

07

5(S

IM):

Ace

na

ph

thyl

en

e2

08

-96

-80

.5m

g/k

g<

0.5

11

26

mg

/kg

12

47

2.0

EP

07

5(S

IM):

Ace

na

ph

the

ne

83

-32

-90

.5m

g/k

g<

0.5

96

.16

mg

/kg

12

77

3.0

EP

07

5(S

IM):

Flu

ore

ne

86

-73

-70

.5m

g/k

g<

0.5

10

0.0

6 m

g/k

g1

26

72

.0

EP

07

5(S

IM):

Ph

en

an

thre

ne

85

-01

-80

.5m

g/k

g<

0.5

10

96

mg

/kg

12

77

5.0

EP

07

5(S

IM):

An

thra

cen

e1

20

-12

-70

.5m

g/k

g<

0.5

11

26

mg

/kg

12

77

7.0

EP

07

5(S

IM):

Flu

ora

nth

en

e2

06

-44

-00

.5m

g/k

g<

0.5

10

66

mg

/kg

12

77

3.0

EP

07

5(S

IM):

Pyr

en

e1

29

-00

-00

.5m

g/k

g<

0.5

10

56

mg

/kg

12

87

4.0

EP

07

5(S

IM):

Be

nz(

a)a

nth

race

ne

56

-55

-30

.5m

g/k

g<

0.5

10

16

mg

/kg

12

36

9.0

EP

07

5(S

IM):

Ch

ryse

ne

21

8-0

1-9

0.5

mg

/kg

<0

.59

6.1

6 m

g/k

g1

27

75

.0

EP

07

5(S

IM):

Be

nzo

(b+

j)flu

ora

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en

e2

05

-99

-2

20

5-8

2-3

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mg

/kg

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.51

13

6 m

g/k

g1

16

68

.0

EP

07

5(S

IM):

Be

nzo

(k)f

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ne

20

7-0

8-9

0.5

mg

/kg

<0

.51

01

6 m

g/k

g1

26

74

.0

EP

07

5(S

IM):

Be

nzo

(a)p

yre

ne

50

-32

-80

.5m

g/k

g<

0.5

10

76

mg

/kg

12

67

0.0

EP

07

5(S

IM):

In

de

no

(1.2

.3.c

d)p

yre

ne

19

3-3

9-5

0.5

mg

/kg

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.51

17

6 m

g/k

g1

21

61

.0

EP

07

5(S

IM):

Dib

en

z(a

.h)a

nth

race

ne

53

-70

-30

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g/k

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0.5

11

56

mg

/kg

11

86

2.0

EP

07

5(S

IM):

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nzo

(g.h

.i)p

ery

len

e1

91

-24

-20

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g/k

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0.5

11

36

mg

/kg

12

16

3.0

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2834894)

EP

08

0:

C6

- C

9 F

ract

ion

----

10

mg

/kg

<1

09

6.1

26

mg

/kg

12

86

8.4

Page 129: Cover - Attach C14f

10

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILM

eth

od

Bla

nk (

MB

)

Rep

ort

Lab

ora

tory

Co

ntr

ol

Sp

ike (

LC

S)

Rep

ort

Sp

ike

Sp

ike R

eco

very

(%

)R

eco

very

Lim

its (

%)

Resu

ltC

on

cen

trati

on

Hig

hL

ow

LC

SM

eth

od:

Co

mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2834937)

EP

07

1:

C1

0 -

C1

4 F

ract

ion

----

50

mg

/kg

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09

9.6

30

0 m

g/k

g1

29

75

.0

EP

07

1:

C1

5 -

C2

8 F

ract

ion

----

10

0m

g/k

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10

01

12

45

0 m

g/k

g1

31

77

.0

EP

07

1:

C2

9 -

C3

6 F

ract

ion

----

10

0m

g/k

g<

10

01

08

30

0 m

g/k

g1

29

71

.0

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2834894)

EP

08

0:

C6

- C

10

Fra

ctio

nC

6_

C1

01

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10

96

.53

1 m

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28

68

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EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2834937)

EP

07

1:

>C

10

- C

16

Fra

ctio

n--

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50

10

93

75

mg

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57

7.0

EP

07

1:

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16

- C

34

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ctio

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/kg

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00

11

05

25

mg

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13

87

4.0

EP

07

1:

>C

34

- C

40

Fra

ctio

n--

--1

00

mg

/kg

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00

10

32

25

mg

/kg

13

16

3.0

EP

080:

BT

EX

N (Q

CL

ot:

2834894)

EP

08

0:

Be

nze

ne

71

-43

-20

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g/k

g<

0.2

96

.91

mg

/kg

11

66

2.0

EP

08

0:

To

lue

ne

10

8-8

8-3

0.5

mg

/kg

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.51

03

1 m

g/k

g1

21

67

.0

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-40

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g/k

g<

0.5

10

41

mg

/kg

11

76

5.0

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e1

08

-38

-3

10

6-4

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mg

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02

2 m

g/k

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18

66

.0

EP

08

0:

ort

ho

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5-4

7-6

0.5

mg

/kg

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.51

05

1 m

g/k

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20

68

.0

EP

08

0:

Na

ph

tha

len

e9

1-2

0-3

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11

13

1 m

g/k

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19

63

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Su

b-M

atr

ix:

WA

TE

RM

eth

od

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nk (

MB

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ort

Lab

ora

tory

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ntr

ol

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ike (

LC

S)

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ort

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ike

Sp

ike R

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very

(%

)R

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very

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its (

%)

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ltC

on

cen

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on

Hig

hL

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LC

SM

eth

od:

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mp

ou

nd

CA

S N

um

ber

LO

RU

nit

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2837679)

EP

08

0:

C6

- C

9 F

ract

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20

µg

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20

85

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60

µg

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27

75

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EP

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71:

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tal R

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vera

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rocarb

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s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2837679)

EP

08

0:

C6

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10

Fra

ctio

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C1

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09

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31

0 µ

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12

77

5.0

EP

080:

BT

EX

N (Q

CL

ot:

2837679)

EP

08

0:

Be

nze

ne

71

-43

-21

µg

/L<

18

8.2

10

µg

/L1

22

70

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EP

08

0:

To

lue

ne

10

8-8

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80

.41

0 µ

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12

36

9.0

EP

08

0:

Eth

ylb

en

zen

e1

00

-41

-42

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/L<

28

6.3

10

µg

/L1

20

70

.0

EP

08

0:

me

ta-

& p

ara

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en

e1

08

-38

-3

10

6-4

2-3

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87

.11

0 µ

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12

16

9.0

EP

08

0:

ort

ho

-Xyl

en

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5-4

7-6

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87

.61

0 µ

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12

27

2.0

EP

08

0:

Na

ph

tha

len

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g/L

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99

.21

0 µ

g/L

12

07

0.0

Matr

ix S

pik

e (

MS

) R

ep

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e

qu

alit

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ntr

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term

M

atr

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(M

S)

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rs

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an

in

tra

lab

ora

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lit

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ple

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with

a

re

pre

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e

pu

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se

o

f th

is

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p

ara

me

ter

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an

aly

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tatic

Re

cove

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imits

as

pe

r la

bo

rato

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ata

Qu

alit

y O

bje

ctiv

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Os).

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ea

l re

cove

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an

ge

s sta

ted

ma

y b

e w

aiv

ed

in t

he

eve

nt

of

sa

mp

le m

atr

ix in

terf

ere

nce

.

Su

b-M

atr

ix:

SO

ILM

atr

ix S

pik

e (

MS

) R

ep

ort

Page 130: Cover - Attach C14f

11

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

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very

Lim

its (

%)

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ike

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hL

ow

MS

Co

ncen

trati

on

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ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

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mp

ou

nd

CA

S N

um

ber

EG

005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

(Q

CL

ot:

2836485)

An

on

ymo

us

ES

20

02

71

9-0

01

74

40

-38

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G0

05

T:

Ars

en

ic9

5.6

50

mg

/kg

13

07

0.0

74

40

-43

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G0

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T:

Ca

dm

ium

89

.65

0 m

g/k

g1

30

70

.0

74

40

-47

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G0

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Ch

rom

ium

80

.75

0 m

g/k

g1

30

70

.0

74

40

-50

-8E

G0

05

T:

Co

pp

er

10

12

50

mg

/kg

13

07

0.0

74

39

-92

-1E

G0

05

T:

Le

ad

90

.22

50

mg

/kg

13

07

0.0

74

40

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-0E

G0

05

T:

Nic

kel

81

.65

0 m

g/k

g1

30

70

.0

74

40

-66

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G0

05

T:

Zin

c8

4.7

25

0 m

g/k

g1

30

70

.0

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

(Q

CL

ot:

2836486)

An

on

ymo

us

ES

20

02

71

9-0

01

74

39

-97

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G0

35

T:

Me

rcu

ry8

8.9

5 m

g/k

g1

30

70

.0

EP

066:

Po

lych

lori

nate

d B

iph

en

yls

(P

CB

) (

QC

Lo

t: 2

834940)

BH

11

3_

0.2

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E

S2

00

27

66

-01

6--

--E

P0

66

: T

ota

l Po

lych

lorin

ate

d b

iph

en

yls

84

.01

mg

/kg

13

07

0.0

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

) (

QC

Lo

t: 2

834939)

BH

11

3_

0.2

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E

S2

00

27

66

-01

65

8-8

9-9

EP

06

8:

ga

mm

a-B

HC

90

.00

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g/k

g1

30

70

.0

76

-44

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P0

68

: H

ep

tach

lor

91

.10

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g/k

g1

30

70

.0

30

9-0

0-2

EP

06

8:

Ald

rin

89

.30

.5 m

g/k

g1

30

70

.0

60

-57

-1E

P0

68

: D

ield

rin

92

.90

.5 m

g/k

g1

30

70

.0

72

-20

-8E

P0

68

: E

nd

rin

90

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mg

/kg

13

07

0.0

50

-29

-3E

P0

68

: 4

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DD

T8

0.1

2 m

g/k

g1

30

70

.0

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

) (

QC

Lo

t: 2

834939)

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

63

33

-41

-5E

P0

68

: D

iazin

on

89

.40

.5 m

g/k

g1

30

70

.0

55

98

-13

-0E

P0

68

: C

hlo

rpyr

ifo

s-m

eth

yl7

8.3

0.5

mg

/kg

13

07

0.0

23

50

5-4

1-1

EP

06

8:

Pirim

ph

os-

eth

yl8

8.2

0.5

mg

/kg

13

07

0.0

48

24

-78

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P0

68

: B

rom

op

ho

s-e

thyl

72

.60

.5 m

g/k

g1

30

70

.0

34

64

3-4

6-4

EP

06

8:

Pro

thio

fos

87

.30

.5 m

g/k

g1

30

70

.0

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s (Q

CL

ot:

2834938)

BH

11

3_

0.2

-0.3

E

S2

00

27

66

-01

68

3-3

2-9

EP

07

5(S

IM):

Ace

na

ph

the

ne

90

.21

0 m

g/k

g1

30

70

.0

12

9-0

0-0

EP

07

5(S

IM):

Pyr

en

e9

7.1

10

mg

/kg

13

07

0.0

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2834894)

An

on

ymo

us

ES

20

02

71

9-0

01

----

EP

08

0:

C6

- C

9 F

ract

ion

10

43

2.5

mg

/kg

13

07

0.0

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2834937)

BH

11

3_

0.2

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E

S2

00

27

66

-01

6--

--E

P0

71

: C

10

- C

14

Fra

ctio

n8

7.4

52

3 m

g/k

g1

37

73

.0

----

EP

07

1:

C1

5 -

C2

8 F

ract

ion

10

62

31

9 m

g/k

g1

31

53

.0

----

EP

07

1:

C2

9 -

C3

6 F

ract

ion

12

81

71

4 m

g/k

g1

32

52

.0

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2834894)

An

on

ymo

us

ES

20

02

71

9-0

01

C6

_C

10

EP

08

0:

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- C

10

Fra

ctio

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11

37

.5 m

g/k

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30

70

.0

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2834937)

Page 131: Cover - Attach C14f

12

of 12

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Su

b-M

atr

ix:

SO

ILM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

Reco

very

Lim

its (

%)

Sp

ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

EP

080/0

71:

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tal R

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vera

ble

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rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2834937)

- c

on

tin

ued

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S2

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27

66

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86

0 m

g/k

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37

73

.0

----

EP

07

1:

>C

16

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34

Fra

ctio

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32

23

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/kg

13

15

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----

EP

07

1:

>C

34

- C

40

Fra

ctio

n1

13

10

58

mg

/kg

13

25

2.0

EP

080:

BT

EX

N (Q

CL

ot:

2834894)

An

on

ymo

us

ES

20

02

71

9-0

01

71

-43

-2E

P0

80

: B

en

zen

e9

3.0

2.5

mg

/kg

13

07

0.0

10

8-8

8-3

EP

08

0:

To

lue

ne

92

.22

.5 m

g/k

g1

30

70

.0

10

0-4

1-4

EP

08

0:

Eth

ylb

en

zen

e1

09

2.5

mg

/kg

13

07

0.0

10

8-3

8-3

10

6-4

2-3

EP

08

0:

me

ta-

& p

ara

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en

e1

06

2.5

mg

/kg

13

07

0.0

95

-47

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P0

80

: o

rth

o-X

yle

ne

11

12

.5 m

g/k

g1

30

70

.0

91

-20

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P0

80

: N

ap

hth

ale

ne

12

12

.5 m

g/k

g1

30

70

.0

Su

b-M

atr

ix:

WA

TE

RM

atr

ix S

pik

e (

MS

) R

ep

ort

Sp

ikeR

eco

very

(%)

Reco

very

Lim

its (

%)

Sp

ike

Hig

hL

ow

MS

Co

ncen

trati

on

Lab

ora

tory

sam

ple

ID

Clien

t sam

ple

ID

Meth

od:

Co

mp

ou

nd

CA

S N

um

ber

EP

080/0

71:

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tal P

etr

ole

um

Hyd

rocarb

on

s (Q

CL

ot:

2837679)

An

on

ymo

us

ES

20

02

53

2-0

01

----

EP

08

0:

C6

- C

9 F

ract

ion

11

53

25

µg

/L1

30

70

.0

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s (Q

CL

ot:

2837679)

An

on

ymo

us

ES

20

02

53

2-0

01

C6

_C

10

EP

08

0:

C6

- C

10

Fra

ctio

n1

21

37

5 µ

g/L

13

07

0.0

EP

080:

BT

EX

N (Q

CL

ot:

2837679)

An

on

ymo

us

ES

20

02

53

2-0

01

71

-43

-2E

P0

80

: B

en

zen

e8

4.5

25

µg

/L1

30

70

.0

10

8-8

8-3

EP

08

0:

To

lue

ne

89

.22

5 µ

g/L

13

07

0.0

10

0-4

1-4

EP

08

0:

Eth

ylb

en

zen

e9

7.8

25

µg

/L1

30

70

.0

10

8-3

8-3

10

6-4

2-3

EP

08

0:

me

ta-

& p

ara

-Xyl

en

e9

6.7

25

µg

/L1

30

70

.0

95

-47

-6E

P0

80

: o

rth

o-X

yle

ne

94

.02

5 µ

g/L

13

07

0.0

91

-20

-3E

P0

80

: N

ap

hth

ale

ne

96

.12

5 µ

g/L

13

07

0.0

Page 132: Cover - Attach C14f

Tru

e

Envir

onm

ental

QA

/QC

Co

mp

lia

nc

e A

ss

es

sm

en

t to

as

sis

t w

ith

Qu

ali

ty R

ev

iew

Wo

rk O

rder

:E

S2002766

Pa

ge

:1

of 8

::

La

bo

rato

ryC

lient

Envi

ronm

enta

l Div

isio

n S

ydney

AE

CO

M A

ustr

alia P

ty L

td

:C

onta

ctM

R A

LE

X L

AT

HA

MT

ele

ph

on

e:+

61 2

8784 8

555

:P

roje

ct60623599_1.1

Da

te S

am

ple

s R

ece

ive

d:29-J

an-2

020

Site

:--

--Is

sue

Da

te:06-F

eb-2

020

Kurt

is W

ath

en, R

ebeka

h P

anozz

o:

Sa

mp

ler

No

. o

f sa

mp

les r

ece

ive

d:19

:O

rde

r n

um

be

r60623599_1.1

No

. o

f sa

mp

les a

na

lyse

d:8

Th

is r

ep

ort

is a

uto

mati

cally g

en

era

ted

by t

he A

LS

LIM

S t

hro

ug

h in

terp

reta

tio

n o

f th

e A

LS

Qu

ality

Co

ntr

ol R

ep

ort

an

d s

evera

l Q

uality

Assu

ran

ce p

ara

mete

rs m

easu

red

by A

LS

. T

his

au

tom

ate

d

rep

ort

ing

hig

hlig

hts

an

y n

on

-co

nfo

rman

ces, fa

cilit

ate

s f

aste

r an

d m

ore

accu

rate

data

valid

ati

on

an

d is d

esig

ned

to

assis

t in

tern

al exp

ert

an

d e

xte

rnal A

ud

ito

r re

vie

w. M

an

y c

om

po

nen

ts o

f th

is

rep

ort

co

ntr

ibu

te t

o t

he o

vera

ll D

QO

assessm

en

t an

d r

ep

ort

ing

fo

r g

uid

elin

e c

om

plian

ce.

Brief m

eth

od s

um

maries

and r

efe

rence

s are

als

o p

rovi

ded to a

ssis

t in

tra

ceabili

ty.

Su

mm

ary

of

Ou

tlie

rs

Ou

tlie

rs :

Qu

ality

Co

ntr

ol S

am

ple

s

Th

is r

ep

ort

hig

hlig

hts

ou

tlie

rs f

lag

ge

d in

th

e Q

ua

lity

Co

ntr

ol (

QC

) R

ep

ort

.

l

NO

Meth

od

Bla

nk v

alu

e o

utl

iers

occu

r.

l

NO

Du

plicate

ou

tlie

rs o

ccu

r.

l

NO

Lab

ora

tory

Co

ntr

ol o

utl

iers

occu

r.

l

NO

Matr

ix S

pik

e o

utl

iers

occu

r.

l

Fo

r all r

eg

ula

r sam

ple

matr

ices, N

O su

rro

gate

reco

very

ou

tlie

rs o

ccu

r.

Ou

tlie

rs :

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

l

NO

An

aly

sis

Ho

ldin

g T

ime O

utl

iers

exis

t.

Ou

tlie

rs :

Fre

qu

en

cy o

f Q

uality

Co

ntr

ol S

am

ple

s

l

NO

Qu

ality

Co

ntr

ol S

am

ple

Fre

qu

en

cy O

utl

iers

exis

t.

R I

G H

T

S O

L U

T I

O N

S

|

R I

G H

T

P A

R T

N E

R

Page 133: Cover - Attach C14f

2 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

An

aly

sis

Ho

ldin

g T

ime C

om

plian

ce

Ho

ldin

g

time

s fo

r V

OC

in

so

ils

vary

a

cco

rdin

g

to

an

aly

tes

of

inte

rest.

Vin

yl

Ch

lorid

e

an

d

Sty

ren

e

ho

ldin

g

tim

e

is

7 d

ays;

o

the

rs

14

da

ys.

A

re

co

rde

d

bre

ach

d

oe

s n

ot

gu

ara

nte

e

a

bre

ach

fo

r a

ll V

OC

a

na

lyte

s

an

d

sho

uld

be

ve

rifie

d in

ca

se t

he

re

po

rte

d b

rea

ch is

a f

als

e p

osi

tive

or

Vin

yl C

hlo

rid

e a

nd

Sty

ren

e a

re n

ot

key

an

aly

tes

of

inte

rest/

con

cern

.

Ho

ldin

g

time

fo

r le

ach

ate

m

eth

od

s (e

.g.

TC

LP

) va

ry

acc

ord

ing

to

th

e

an

aly

tes

rep

ort

ed

.

Ass

ess

me

nt

com

pa

res

the

le

ach

d

ate

w

ith

th

e

sho

rte

st

an

aly

te

ho

ldin

g

time

fo

r th

e

eq

uiv

ale

nt

so

il m

eth

od

. T

he

se

a

re:

org

an

ics

14

da

ys,

me

rcu

ry 2

8 d

ays

& o

the

r m

eta

ls 1

80

da

ys.

A r

eco

rde

d b

rea

ch d

oe

s n

ot

gu

ara

nte

e a

bre

ach

fo

r a

ll n

on

-vo

latil

e p

ara

me

ters

.

If s

am

ple

s a

re id

en

tifie

d b

elo

w a

s h

avi

ng

be

en

an

aly

sed

or

ext

ract

ed

ou

tsid

e o

f re

com

me

nd

ed

ho

ldin

g t

ime

s,

this

sh

ou

ld b

e t

ake

n in

to c

on

sid

era

tion

wh

en

inte

rpre

ting

re

sults

.

Th

is

rep

ort

su

mm

arize

s e

xtra

ctio

n

/ p

rep

ara

tion

a

nd

a

na

lysi

s tim

es

an

d

com

pa

res

ea

ch

with

A

LS

re

com

me

nd

ed

h

old

ing

tim

es

(re

fere

nci

ng

U

SE

PA

S

W

84

6,

AP

HA

, A

S

an

d

NE

PM

) b

ase

d

on

th

e

sa

mp

le

co

nta

ine

r

pro

vid

ed

. D

ate

s re

po

rte

d r

ep

rese

nt

first

da

te o

f e

xtra

ctio

n o

r a

na

lysi

s a

nd

pre

clu

de

su

bse

qu

en

t d

ilutio

ns

an

d r

eru

ns.

A lis

ting

of

bre

ach

es

(if

an

y)

is p

rovi

de

d h

ere

in.

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EA

055:

Mo

istu

re C

on

ten

t (D

ried

@ 1

05-1

10°C

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

A055)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Fe

b-2

02

0--

--31-J

an

-2020

----

28-J

an

-2020

----

ü

So

il G

lass J

ar

- U

np

reserv

ed

(E

A055)

BH

11

3_

0.2

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H1

13

_0

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.71

2-F

eb

-20

20

----

31-J

an

-2020

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29-J

an

-2020

----

üE

A200:

AS

4964 -

2004 Id

en

tifi

cati

on

of

Asb

esto

s in

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ils

Sn

ap

Lo

ck B

ag

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riab

le A

sb

esto

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A200)

BH

10

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H1

07

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6-J

ul-2

02

0--

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-Feb

-202

0--

--28-J

an

-2020

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üS

nap

Lo

ck B

ag

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riab

le A

sb

esto

s/P

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(E

A200)

BH

11

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13

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7-J

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02

0--

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0--

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: A

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s Q

uan

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on

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on

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TA

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ap

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esto

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(E

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BH

10

9_

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H1

07

_0

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6-J

ul-2

02

0--

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-Feb

-202

0--

--28-J

an

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----

üS

nap

Lo

ck B

ag

- F

riab

le A

sb

esto

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Bag

(E

A200N

)

BH

11

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H1

13

_0

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7-J

ul-2

02

0--

--03

-Feb

-202

0--

--29-J

an

-2020

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üE

G005(E

D093)T

: T

ota

l M

eta

ls b

y IC

P-A

ES

So

il G

lass J

ar

- U

np

reserv

ed

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BH

10

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0.3

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09

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H1

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l-2

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02

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001-F

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-20

20

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So

il G

lass J

ar

- U

np

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ed

(E

G005T

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BH

11

3_

0.2

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13

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7-J

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02

02

7-J

ul-2

02

003

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-202

001-F

eb

-20

20

29-J

an

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üü

EG

035T

: T

ota

l R

eco

vera

ble

Merc

ury

by F

IMS

So

il G

lass J

ar

- U

np

reserv

ed

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G035T

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BH

10

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09

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BH

10

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0.5

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H1

07

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25

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02

02

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20

03

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001-F

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20

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lass J

ar

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np

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26

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20

29-J

an

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EP

066:

Po

lych

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nate

d B

iph

en

yls

(P

CB

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So

il G

lass J

ar

- U

np

reserv

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P066)

BH

11

3_

0.2

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11

-Ma

r-2

02

01

2-F

eb

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20

03

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

Page 134: Cover - Attach C14f

3 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

.1:

Pro

ject

Ma

trix

: S

OIL

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

ue

fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

EP

068A

: O

rgan

och

lori

ne P

esti

cid

es (

OC

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

P068)

BH

11

3_

0.2

-0.3

11

-Ma

r-2

02

01

2-F

eb

-20

20

03

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

EP

068B

: O

rgan

op

ho

sp

ho

rus P

esti

cid

es (

OP

)

So

il G

lass J

ar

- U

np

reserv

ed

(E

P068)

BH

11

3_

0.2

-0.3

11

-Ma

r-2

02

01

2-F

eb

-20

20

03

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

EP

075(S

IM)B

: P

oly

nu

cle

ar

Aro

mati

c H

yd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P075(S

IM))

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Ma

r-2

02

01

1-F

eb

-20

20

01

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P075(S

IM))

BH

11

3_

0.2

-0.3

,B

H1

13

_0

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.71

1-M

ar-

20

20

12

-Fe

b-2

02

001

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

EP

080/0

71:

To

tal P

etr

ole

um

Hyd

rocarb

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Ma

r-2

02

01

1-F

eb

-20

20

01

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Fe

b-2

02

01

1-F

eb

-20

20

04

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

11

3_

0.2

-0.3

,B

H1

13

_0

.6-0

.71

1-M

ar-

20

20

12

-Fe

b-2

02

001

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

11

3_

0.2

-0.3

,B

H1

13

_0

.6-0

.71

2-F

eb

-20

20

12

-Fe

b-2

02

004

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Ma

r-2

02

01

1-F

eb

-20

20

01

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Fe

b-2

02

01

1-F

eb

-20

20

04

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P071)

BH

11

3_

0.2

-0.3

,B

H1

13

_0

.6-0

.71

1-M

ar-

20

20

12

-Fe

b-2

02

001

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

11

3_

0.2

-0.3

,B

H1

13

_0

.6-0

.71

2-F

eb

-20

20

12

-Fe

b-2

02

004

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

EP

080:

BT

EX

N

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

10

9_

0.3

-0.4

,B

H1

09

_0

.9-1

.0,

BH

10

7_

0.5

-0.6

,B

H1

07

_1

.5-1

.7

11

-Fe

b-2

02

01

1-F

eb

-20

20

04

-Feb

-202

031-J

an

-202

028-J

an

-2020

üü

So

il G

lass J

ar

- U

np

reserv

ed

(E

P080)

BH

11

3_

0.2

-0.3

,B

H1

13

_0

.6-0

.71

2-F

eb

-20

20

12

-Fe

b-2

02

004

-Feb

-202

031-J

an

-202

029-J

an

-2020

üü

Ma

trix

: W

AT

ER

Eva

lua

tion

: û

= H

old

ing

tim

e b

rea

ch

; ü

= W

ithin

ho

ldin

g t

ime

.

An

aly

sis

Extr

actio

n /

Pre

pa

ratio

nS

am

ple

Date

Meth

od

Eva

lua

tio

nD

ue

fo

r a

na

lysis

Date

an

aly

sed

Eva

lua

tio

nD

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fo

r e

xtr

actio

nD

ate

extr

acte

dC

on

tain

er

/ C

lien

t S

am

ple

ID

(s)

Page 135: Cover - Attach C14f

4 o

f 8

:P

ag

e

Wo

rk O

rde

r: :

Clie

nt

ES

20

02

76

6

AE

CO

M A

ust

ralia

Pty

Ltd

60

62

35

99

_1

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Pro

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Ma

trix

: W

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= H

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An

aly

sis

Extr

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Pre

pa

ratio

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ple

Date

Meth

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nD

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fo

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Date

an

aly

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ID

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EP

080/0

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To

tal P

etr

ole

um

Hyd

rocarb

on

s

Am

ber

VO

C V

ial -

Su

lfu

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cid

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QC

30

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TB

11

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02

01

1-F

eb

-20

20

05

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005-F

eb

-20

20

28-J

an

-2020

üü

EP

080/0

71:

To

tal R

eco

vera

ble

Hyd

rocarb

on

s -

NE

PM

2013 F

racti

on

s

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

QC

30

0 -

TB

11

-Fe

b-2

02

01

1-F

eb

-20

20

05

-Feb

-202

005-F

eb

-20

20

28-J

an

-2020

üü

EP

080:

BT

EX

N

Am

ber

VO

C V

ial -

Su

lfu

ric A

cid

(E

P080)

QC

30

0 -

TB

11

-Fe

b-2

02

01

1-F

eb

-20

20

05

-Feb

-202

005-F

eb

-20

20

28-J

an

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üü