certificate of analysis · certificate of analysis order #: 30605 order name: gelato 350mg batch#:...

*Total CBD = CBD + CBDA x 0.877

CERTIFICATE OF ANALYSISOrder #: 30605Order Name: Gelato 350mgBatch#: GEL9135Completed: 05/06/2019

Arise Bioscience Inc.4855 Technology Way Suite 500Boca Raton Florida, 33431(866) 407-1164

Sample

0.000% D9-THC

35.267% Total CBD

Cannabinoids Testcannabinoids weight(%) mg/gDELTA-9-TETRAHYDROCANNABINOL D9-THC N/D N/DTETRAHYDROCANNABINOLIC ACID THCA N/D N/DCANNABIDIOL CBD 35.267% 352.673CANNABIDIOLIC ACID CBDA N/D N/DCANNABIDIVARIN CBDV 0.100% 0.998CANNABICHROMENE CBC 0.351% 3.510CANNABINOL CBN 0.298% 2.978CANNABIGEROL CBG 0.020% 0.201CANNABIGEROLIC ACID CBGA N/D N/DDELTA-8-TETRAHYDROCANNABINOL D8-THC N/D N/DTETRAHYDROCANNABIVARIN THCV N/D N/D

TOTAL D9-THC N/D N/DTOTAL CBD* 35.267% 352.673TOTAL CANNABINOIDS 36.036% 360.360

4001 SW 47th Avenue Suite 207Davie, FL [email protected]

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.



TERPENES: TOTAL (1.950%)GC-Headspace - Shimadzu GCMS QP2020 with HS20

Terpene Results (%)(1R)-ENDO-(+)-FENCHYL ALCOHOL 0.072%ALPHA-BISABOLOL 0.007%ALPHA-CEDRENE 0.005%ALPHA-PINENE 0.152%BETA-MYRCENE 0.258%BORNEOL (MIX OF ISOMERS) 0.006%CAMPHENE 0.015%CARYOPHYLLENE 0.282%CARYOPHYLLENE OXIDE 0.026%CIS-BETA-OCIMENE 0.037%GERANIOL 0.011%GERANYL ACETATE 0.030%HUMULENE 0.126%ISOBORNEOL 0.007%LIMONENE 0.488%LINALOOL 0.283%PULEGONE 0.007%TERPINEOL (MIX OF ISOMERS) 0.075%TRANS-BETA-OCIMENE 0.047%TRANS-NEROLIDOL 0.016%

Terpenes Breakdown

Top Terpenes Results:

Tested for but not present:

3-CARENE, ALPHA-TERPINENE, ALPHA.-PHELLANDRENE, BETA-PINENE, CAMPHOR, CAMPHOR (MIX OF ISOMERS), CEDROL, CIS-NEROLIDOL, EUCALYPTOL, FENCHONE, FENCHONE (ISOMER),GAMMA-TERPINEOL, GAMMA.-TERPINENE, GUAIOL, ISOPULEGOL, MENTHOL, NEROL, SABINENE, SABINENE HYDRATE, TERPINOLENE, VALENCENE



N/D = Not Detected, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level



PESTICIDE ANALYSIS:GC QQQ - Shimadzu GCMS-TQ8040

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

ABAMECTIN B1A 0.100 N/D 0.003 0.001ACEPHATE 0.100 N/D 0.003 0.001ACEQUINOCYL 0.100 N/D 0.003 0.001ACETAMIPRID 0.100 N/D 0.003 0.001ALDICARB 0.100 N/D 0.003 0.001AZOXYSTROBIN 0.100 N/D 0.003 0.001BIFENAZATE 0.100 N/D 0.003 0.001BIFENTHRIN 3.000 N/D 0.003 0.001BOSCALID 0.100 N/D 0.003 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.003 0.001CHLORANTRANILIPROLE 10.000 N/D 0.003 0.001CHLORPYRIFOS 0.100 N/D 0.003 0.001CLOFENTEZINE 0.100 N/D 0.003 0.001DAMINOZIDE 0.100 N/D 0.003 0.001DIAZANON 0.100 N/D 0.003 0.001DICHLORVOS 0.100 N/D 0.003 0.001DIMETHOATE 0.100 N/D 0.003 0.001DIMETHOMORPH 2.000 N/D 0.003 0.001ETHOPROPHOS 0.100 N/D 0.003 0.001ETOFENPROX 0.100 N/D 0.003 0.001ETOXAZOLE 0.100 N/D 0.003 0.001FENHEXAMID 0.100 N/D 0.003 0.001FENOXYCARB 0.100 N/D 0.003 0.001FENPYROXIMATE 0.100 N/D 0.003 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 0.100 N/D 0.003 0.001FLUDIOXONIL 0.100 N/D 0.003 0.001HEXYTHIAZOX 0.100 N/D 0.003 0.001

PESTICIDE ANALYSIS:GC QQQ - Shimadzu LCMS-8060

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

IMAZALIL 0.100 N/D 0.003 0.001IMIDACLOPRID 5.000 N/D 0.003 0.001KRESOXIM-METHYL 0.100 N/D 0.003 0.001MALATHION 0.500 N/D 0.003 0.001METALAXYL 2.000 N/D 0.003 0.001METHIOCARB 0.100 N/D 0.003 0.001METHOMYL 1.000 N/D 0.003 0.001MEVINPHOS 0.100 N/D 0.003 0.001MYCLOBUTANIL 0.100 N/D 0.003 0.001NALED 0.100 N/D 0.003 0.001OXAMYL 0.500 N/D 0.003 0.001PACLOBUTRAZOL 0.100 N/D 0.003 0.001PERMETHRINS 0.500 N/D 0.003 0.001PHOSMET 0.100 N/D 0.003 0.001PIPERONYLBUTOXIDE

3.000 0.009 0.003 0.001

PRALLETHRIN 0.100 N/D 0.003 0.001PROPICONAZOLE 0.100 N/D 0.003 0.001PROPOXUR 0.100 N/D 0.003 0.001PYRETHRINS(PYRETHRIN I)

0.500 N/D 0.003 0.001

PYRIDABEN 0.100 N/D 0.003 0.001SPINETORAM 0.100 N/D 0.003 0.001SPINOSAD 0.100 N/D 0.003 0.001SPIROMESIFEN 0.100 N/D 0.003 0.001SPIROTETRAMAT 0.100 N/D 0.003 0.001SPIROXAMINE 0.100 N/D 0.003 0.001TEBUCONAZOLE 0.100 N/D 0.003 0.001THIACLOPRID 0.100 N/D 0.003 0.001THIAMETHOXAM 5.000 N/D 0.003 0.001TRIFLOXYSTROBIN 0.100 N/D 0.003 0.001





RESIDUAL SOLVENTS:GC-Headspace - Shimadzu GCMS QP2020 with HS20

Residual Solvent Action Level (ppm) Results (ppm)ACETONE 5,000.000 N/DACETONITRILE 410.000 N/DBENZENE 1.000 N/DBUTANE 5,000.000 N/DCHLOROFORM 1.000 N/DDICHLOROETHANE 1.000 N/DDICHLOROMETHANE 1.000 N/DETHANOL 5,000.000 N/DETHYL ACETATE 5,000.000 N/DETHYL ETHER 5,000.000 N/DISOPROPYL ALCOHOL 5,000.000 N/DMETHANOL 3,000.000 N/DN-HEPTANE 5,000.000 N/DN-HEXANE 290.000 N/DPENTANE 5,000.000 N/DPROPANE 5,000.000 N/DTOLUENE 890.000 N/DTRICHLOROETHANE 1.000 N/DXYLENES 2,170.000 N/D





Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060

Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20.000 N/DAFLATOXIN B2 20.000 N/DAFLATOXIN G1 20.000 N/DAFLATOXIN G2 20.000 N/DOCHRATOXIN A 20.000 N/D

Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030

Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200.000 2.630CADMIUM (CD) 200.000 < LOQMERCURY (HG) 100.000 6.230LEAD (PB) 500.000 4.770

*Lower Limit of Quantitation (LOQ) is 1 ppb

Microbial Analysis:PCR - Agilent AriaMX

Test Test MethodUsed Device Used LOD Allowable Amount Actual

Result Pass/Fail

STEC E. COLI* USP 61/62† ARIAMX PCR 2 COPIES OF DNA PRESENCE / ABSENTBELOW

LODPASS

SALMONELLA* USP 61/62† ARIAMX PCR 5 COPIES OF DNA PRESENCE / ABSENTBELOW

LODPASS

ASPERGILLUS USP 61/62† ARIAMX PCR ASP_LOD*** PRESENCE / ABSENTBELOW

LODPASS

† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex *** Flavus = 2 Copies of DNA / Fumigatis = 2 Copies of DNA Niger = 20 Copies of DNA / Terrus = 10 copies of DNA



certificate of analysis · certificate of analysis order #: 30605 order name: gelato 350mg batch#:...

Documents