bloci< environmental · 2012-03-08 · 2.0 vapor extraction pilot testing in order to evaluate...

BLOCI< ENVIRONMENTAL

March 8, 2012

Mr. Kris Eric Olsen Vice President of Campus Plmu1ing & Operation Chapman University One Un iversity Drive Orange, CA 92866

SUBJECT: VAPOR EXTRACTION PILOT TEST REPORT

SITE: FILMMAKER'S VILLAGE PROJECT 220,228,264, & 296 NORTH CYPRESS STREET ORANGE, CALIFORNIA

Dear Mr. Olsen:

Enclosed please find two copies of the Vapor Extraction Pilot Test Repol1 and final invoice for the above-mentioned property. In addition, a electronic PDF version of the final report will be sent to you via email. If you have any questions please cal l me at (949) 455-0325.

Sincerely,

BLOCK ENVIRONMENTAL

Erik M. Block, PG, REA President

Enclosures

cc: Mr Luis Lodregueza, OCHCA (1 copy)

23 MUSICk, Ste 100' IrVIne CA 92618 ·1676 ' TEL 949'455'0325 FAX 949'455'1958

VAPOR EXTRACTION PILOT TEST REI>ORT

FILlVll\-1AKER'S VILLAGE PH.OJECT 220, 228, 264, & 296 NORTH CYPRESS STREET

ORANGE, CALIFORNIA

March 8, 2012

Prepared For:

Mr. Kris Eric Olsen Vice President of CaInpus Planning & Operation

Chapman University One University Drive

Orange, CA 92866

Prepared By:

BLOCK ENVIRONMENTAL 23 Musick, Suite 100

Irvine, California 92618 (949) 455-0325

TABLE OF CONTENTS

Section

1.0 INTRODUCTION

1.1 Objectives

1.2 Site Description

1.3 Description of Contmninants

2.0 V APOR EXTRACTION PILOT TESTfNG

2.1 Testing Procedures

2.2 Laboratory Analysis

3.0 FINDINGS AND CONCLUSIONS

2.1 Laboratory Analysis Results

2.2 Vapor Extraction Testing Results

4.0 REPORT LIMIT A TIONS

Figures

Index Map 2 Site Plan 3 Site Plan Showing Estilnated Area of Vacuum Influence

Tables

Vapor Extraction Test Well Influent Concentrations, January 26,2012

Appendices

A General Field Procedures B Vapor Extraction Test Field Data Sheets C Laboratory Analysis Results

2 "I .)

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4

5

March 8, 2012

1.0 INTRODUCTION

Vapor Extraction Pilot Testing Report Filmmaker's Village Project. Orange, California

Block Environmental No. 30-333-03

This report describes the vapor extraction pilot test activities prepared on behalf of Chaplnan

University for the Filmlnaker's Village Project, located at 220, 228, 264, and 296 North Cypress

Street in the City of Orange, California (the "Site"). Refer to Figure 1 for an Index map showing

the subject property location.

1.1 Objectives

A vapor extraction test was conducted to evaluate subsurface soil characteristics which may

affect the application of this relnedial technology beneath the subject property. Volatile Organic

Compounds (VOCs) such as tetrachloroethene (PCE) may be recovered from the subsurface by

inducing volatilization of the contan1inants to vapor-phase in the vadose zone.

1.2 Site Description

The Site, cOlnprising approxilnately 3 acres, is bounded by West Paltn Avenue to the north,

North Cypress Street to the east, \Vest Maple Avenue to the south and railroad tracks to the \Nest.

The Site consists of several large industrial buildings \vith 4 separate street addresses. The

building addressed 220 North Cypress Street is currently occupied by Chapn1an University. The

relnaining 3 addresses (228, 264, and 296 North Cypress Street) are currently unoccupied. The

Site is further defined by the County of Orange Assessor Parcel NUI11ber 039-160-03. A Site

plan showing the site details is included as Figure 2.

1.3 Description of Contaminants

Soil Gas - Elevated concentrations of VOCs above the California I-IUI11an Health Screening

Levels (CHHSLs) for residential land use \""ere detected in soil gas samples collected on the

north central and east central portions of the subject property. Chlorinated VOCs exceeding its

residential CHHSL include: PCE, TCE. Carbon Tetrachloride, and Vinyl Chloride. Detectable

concentrations below the residential CHHSLs include: 1,I,I-TCA. Toluene, cis-I)-DeE, and

r-,·1arch 8, 2012 Vapor Extraction Pilot Testing Report

Filmmaker's Village Project, Orange, California Block Environmental

)Jo.30-333-03

Xylenes. Detectable concentrations of Chloroforn1 and Trichlorotluoromethane (Freon 113)

were also present but no CHHSLs for these compounds have been established. The results

suggest that these soil gas in1pacts are relatcd to a VOC release fron1 previous Site operations at

the 264 and 296 North Cypress Street buildings. PCE concentrations above residential CHHSLs

extend to a depth of 85 fbg (maximum depth explored) in both potential source areas and may

pose a risk to groundwater.

Soil - VOCs including Chlorofonn, PCE, TCE, and Napthalene were detected in soil sa1nplcs

collected on the north central and east central portions of the subject property. Concentrations of

PCE above PRGs for residential land use were detected south and southeast of the 264 North

Cypress Street building. Elevated concentrations (below PRGs) of Chlorofonn, PCE, and TCE

extend to a depth of 85 fbg (maxirnUln depth explored) in both potential SOUl-c.e areas and may

pose a risk to groundwater.

2.0 VAPOR EXTRACTION PILOT TESTING

In order to evaluate the ren1edial options for reducing VOCs in the soil beneath the site, a vapor

extraction pilot test was conducted to determine the air ilo\v characteristics of the soils beneath

the site. The results have becn used to evaluate the radius of influence and optin1al extraction

rate and vaCUUln. Three, 2-inch diatneter, dual-nested Vapor Extraction \\' ells (VE\V -1, VEVv -2,

and YEW -3) \vere installed as part of the vapor extraction testing activities. Each \vell is

screened through permeable soil layers in a shallow zone (10-15 fbg) and deep zone (33 to 45

fbg). The teclmology involves applying a relatively high vacuun1 to the subsurface by operating a

vacuum pUlnp connected to one of the extraction wells. This creates a pressure gradient and thus

induces radial air flow. As air flo\vs past in1pacted media the contan1inants transfer into vapor

phase and rnigrate with the air stremn. The influent air is conveyed from the extraction well to

the treatn1ent equiprnent. Activated carbon adsorption \vas employed to treat extracted vapors.

The success of vapor extraction is influenced by many factors including the penneability of the

soil, moisture content, distance to the surface, or \vhether the surface is capped or unpaved.

2

1'v1arch 8, 2012

2.1 Testing Procedures

Vapor Extraction Pilot Testing Report Fiitnmaker's Village Project, Orange, California

Block Environmental No. 30-333-03

On January 26, 2012, Block Environn1cntal conducted vapor extraction pilot testing at the site.

Vapor extraction testing \vas performed using South Coast Air Quality tvlanagement District

(SCAQMD) approved equiplnent to create a vaCUUln in the extraction well. Pressure drawdown

\vas monitored in the extraction and observation wells using Inagnehelic gauges connected to

\vell heads using air tight caps, and recorded in inches of water (in. H20). The vapor flow rate

frOln the extraction well was ll1easured using an electronic instnllnent and recorded in standard

cubic feet per Ininute (scfn1). Vapor concentrations were monitored in the extraction well using a

calibrated photoionization detector (PID). A description of general tield procedures and copies

of the field testing data are also included in Appendix A and Appendix B, respectively.

2.2 Laboratonr Analysis

During the vapor extraction test six inf1uent and one efl1uent vapor san1ples \vere collected and

analyzed for VOCs using EPA ~1ethod 8260B. The samples \vere collected in Tedlar bags using

a vaCUUln pump. Satnples were transported in a chilled cooler under chain-of-custody protocol to

Associated Laboratories, Inc., a California Departn1ent of Health Services (DHS)-certified

laboratory. Results of laboratory analysis are listed on Table 1. The Official Laboratory Reports

and Chain of Custody Record are included in Appendix C.

3.0 FINDINGS AND CONCLUSIONS

Analy1ical results of vapor san1ples and pilot testing results are based on field data collected on

January 26, 2012.

3.1 Analytical Results

All of the compounds reported in the laboratory analysis results were non-detcct with the

exception of peE, \vhich \vas detected in all 6 well inilucnt smnples at concentrations ranging

from 33,783 ).lg/n13 to 1,241,030 I-lg/mJ. The California I-Iuman Health Screening Level

3

March 8, 2012 Vapor Extraction Pilot Testing Report

filmmaker's Village Project, Orange, California Block Environmental

No. 30-333-03

(CHHSL) for PCE is 180 Ilg/m3. The carbon adsorption unit effluent smnple was non-detcct for

all C0111pounds \vith the exception of 14.0 Vppb toluene, which is lnost likely not fr01n the test

Site (none detected in any of the 6 influent samples), but possibly fro111 a previous canister use.

3.2 Vapor Extraction Test Results

Measured tlO\V rates ranged froln approxin1ately 4 to 80 cubic feet per Ininute (ctln) at vacuum

pressures as high as 9.75 inches of mercury. The vacuum radius of influence in the shallow and

deep zone testing levels \-vas calculated using a sen1i logarithn1ic graphical Inethod which yielded

a radius of influence of approximately 50 feet at the highest vaCUUlns tested. The radius of

influence is defined as the distance at \vhich an induced vaccum of 0.1 inches of water is

predicted. Refer to Figure 3 for a Site Plan showing the Estilnated Area of Vacuum Intluence.

Graphs of vaCUUln response vs. distance with a best fit line yielding the average radius of

influence are included in Appendix D.

Subsequent to the installation of these extraction \vells deeper subsurface testing revealed the

presence of VOCs in soil do\vn to a depth of 95-1 00 fbg, \vhere ground"water is present. Equal or

higher penneability soil present belo\v depth the depths evaluated during this vapor extraction

test should yield an equal or larger radius of influence.

Based on the results of this investigation, vapor extraction appears to be a feasibile technology to

remediate VOC-ilnpacted soil in the vadose zone beneath the site. Using a predicted radius of

influence of 50 feet, a well field of 17 nested vapor extraction \vells should be sufficient to

effectively capture PCE vapors w'ithin the estilnated contaminated zones. This assumes thc

lateral extent of vapor contmnination in the deeper zones (45 to 100 fbg) is approxin1ately the

same as in shallo\v zones (0 to 45 fgb).

Vapor extraction systems typically have a high initial efficiency rates which drop off drmnaticaUy

as influent concentrations decrease. The removal efficiency rates usually declines to an

asymptotic level. Treatlnent of the extracted vapors \vill be required in order to Ineet the

requirelnents set by the SCAQMD.

4

:vtarch 8. 2012 Vapor E:-..traction Pilot Test ing Report

Filmmaker' s Village Project. Orange. California

4.0 REPORT LIMITATIONS

Block Environmental No. 30·333-03

This document was prepared so lely for Chapman University in accordance with the standards of

the environmental consulting industry at the time the services we re pe rformed and in acco rdance

with the contract betwecn Chapman University and Block Envi ronmen tal. This report is

governed by the speci fi c scope of wo rk autho ri zed by Chapman Uni ve rsity and is not intended to

be reli ed upon by any other party. We have reli ed on information or instruction provided by

Chapman Uni versity and other part ies and, unless otherwi se expressly indicated. have made no

independent investigation as to the va lidity, completeness. o r accuracy of such informatio n. This

report makes no representation or warranty that environmental contaminat ion does not cx ist at

this Site beyond that desc ribed in thi s report.

BLOCK I~NVlRONMENTAL

Paul Breen, Jr.

Project Geologist

Erik M. Block, P.G.

Pres ident

5

FIGURES

Map crealed with TOPO!f) ClDJ2 Ne.bnel Oeogre.~ (WWW.Mtionalgeographic.cOml.topo)

Filmmaker's Village Project 220, 228, 264 & 296 North Cypress Street Orange, California

INDEX MAP FIGURE 1

13LOCI< ENVIRONMENTAL 23 Musick, Suite 100 Irvine, California 92618

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TABLES

TABLE 1 VAPOR EXTRACTION TEST WELL INFLUENT CONCENTRATIONS

Fih11111aker's Village Project 220, 228, 264, and 296 N. Cypress St., Orange, Califo111ia

January 26, 2012

'Vell Screen Anaylsis by EPA l\'lcthod 8260B

~umber Interval peE peE

(fbg) (Vppb) (~lg/m3)

VEW-l 10-25 4,900 33,783

VE\V-l 33-45 71,000 489517

VE\V-2 10-25 38,000 261,995

VE\V-2 33-45 85,000 586,042

VE\V-3 10-25 62,000 427,466

VEW-3 33-45 180,000 1,241,030

Residential CHI-JSLs 26 Vppb 180 !-lg/m3

Commercial CHHSLs 87 Vppb 603 pg/m3

Notes:

tbg = Feel BelO\v Grade

Vppb = vapor in palts per billion

~lg/m3= micrograms per cubic meter

PCE = Tetrachloroethylene

CHHSL = California \-iuman Health Screening Level

APPENDIX A

APPENDIX A GENERAL FIELD PROCEDURES

In order to evaluate the relnedial options for reducing VOCs in the soil a vapor extraction pilot

tests was conducted to detern1ine the air flow characteristics of the soils beneath the site. The

resu1ts will be used to evaluate the radius of influence, and optin1al extraction rate and vaCUUln.

The vapor extraction test ,vas perforn1ed using a n10bile treatnlent system to extract vapors f)'om

one of the three dual-nested Vapor Extraction Wells at the Site (VEW-I, VE\V-2, and VEW-3).

Eaeh well contains 2 well casings screened at two different intervals (shallow zone from 10 to 25

feet below grade [fbgJ/deep zone fron1 33 to 45 tbg).

The extraction was perf01111ed on one well and one zone at a time (e.g. YE\V -1 shallow zone).

The relnaining two wells were used for observation of induced vaCUUln (e.g. VE\V -2 and YEW-3

shallow zone). A separate test \-vas performed on each of the three \-vells in both shallow and

deep zones (6 tests total).

At vanous titnes during the extraction test the air flow and vaCUU111 was recorded at the

extraction well. In addition, tield lneasurelnents of influent vapor concentrations were taken at

the extraction well using a rID. During the extraction tests, transient VaCUU111 responses were

n10nitored in the observation wells at various tilnes to assess vacuun1 propagation and steady

state conditions. Soil gas sanlples were collected in Tedlar bags during testing for analysis of

VOC concentrations.

APPENDIX B

Time

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VAPOR EXTRACTION TEST FIELD DATA SHEET

Site: Filmmaker's Village Project Proj ect Ad d res s· --'--''':'2'''674 7N~C"-yp":r"'e"'ss"'S~t:":r e':::'eL:t =-- City: Orange

Cl ient· Chapman

VEW -1

Well Screen Interval (Shallow Zone) 10-25 fbg

Well Screen Interval (Deep Zone) 33-45 fbg

Extraction Well System Extraction Well Extraction Well Wellhead Vacuum (" Hg) Vacuum (" Hg) Flowrate (scfm) Inlet Conc. (ppm v) Vacuum (" H2O)

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Date: 1/26/2012 Page 1 of 1

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Date: 1/26/2012 Page' 1 of 1

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Site: Filmmaker's Village Project Project Address' -...:....::';';2:;::6477iN=:C~Yc.,pc::re:':s""-s ""S7:tre':.::e"::t:'::':""-


VEW-1



Extraction Well System Extraction Well Extraction Well Wellhead Vacuum (" Hg) Vacuum (" Hg) Flowrate (scfm) Inlet Cone. (ppm v) Vacuum (" H2O)

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Date: 1/26/2012 Page' 1 of 1

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Date: 1/26/2 01 2 Page' 1 of 1

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Site: _...:F...:;il.:::-m7m.:.:a",k=er-=,·s...:Vc::i l.:.:la",-ge7'-P:..:ro~je:..::c,-t _ Project Address· 264 N Cypress Street

City: Orange Cl ient· Chapman

VEW-1



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;.g ./.0 5·0 y?/ 19·0

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Date: 1/26/2012 Page· 1 of 1

VEW-2 VEW -3

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33-45 fbg 33-45 fbg


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comments: __ .r;7~..:;J.J..:.k::..t1....1...-..:Si,,-,~-,-v:....::-r"--..:;$.l<..O,,::;w.:;.:;/\....:...........::;«k.LC-"O""V.<::lr0",-~"--_tz>_-,,-5c....:/'...:.i'-""'-----,,-____________ _

BLOCK ENVI RONMENTAL

APPENDIX C

Client: Address:

Attn:

Associated Laboratories 806 N. Batavia - Orange, CA 92868 Tel (714)771-6900 Fax (714)538-1209 www.associatedlabs.com [email protected]

Block Environmental 23 Musick Suite #100 Irvine, CA 92618 Erik Block

Comments: #30-333-03 Filmmaker's Village Project 264 N. Cypress St., Orange

Lab Request: 298455 Report Date: 02/01/2012 Date Received: 01/26/2012

Client 10: 12211

This laboratory request covers the following listed samples which were analyzed for the parameters indicated on the attached Analytical Result Report. All analyses were conducted using the appropriate methods indicated on the attached report and all NELAC criteria. This cover letter is an integral part of the final report.

SamQle# Client Sam~le ID

298455-001 VEW-3-S 298455-002 VEW-3-D 298455-003 VEW-1-S 298455-004 VEW-1-D 298455-005 VEW-2-S 298455-006 VEW-2-D 298455-007 System Effluent

Thank you for the opportunity to be of service to your company. Please feel free to call if there are any questions regarding this report or if we can be of further service.

ASS rED L:~R7~ Edward S. Beh e, ~D. -Lab Director NOTE: Unless notified in writing. all samples will be discarded by appropriate disposal protocol 45 days from date reported.

The reports of the Associated Laboratories are confidential property of our clients and may not be reproduced or used for publication in part or in full without our written permission. This is for the mutual protection of the public, our clients, and ourselves.

Page 1 of 8

TESTING & CONSUL TING

Chemical

Microbiological

Environmental

Sample #: 298455-001

Matrix: Air

Collect Date: 01/26/12

Collect Time: 11 :46 AM

Client: Block Environmental

Client Sample #: VEW-3-S

Site:

Collector: Client

_-.:::C=-=o=m~p~o=u.:...:n-=d ______ .. __ ~_. __ ._._ .. ____ Resu!t .. __ OF. ROL Units Analysi~ Dat~}·\!!a.Jy_~t Method: EPA 8260B Prep Method: Method QCBatchlO: QC1122815

---- _ .. _ ... _ ... _ .... _-_.- ----- ...

1,1.1-Trichloroethane NO 5000 5000 Vppb 01127/12 nicollez

1,1.2,2-Tetrachloroethane

1,1.2-Trichloroethane ... - . ~ .. - - - - - - - - - - - - - - - .. .. 1,1,2-Trichlorotrifluoroethane

.. _----------_ .. _-_ ........ . 1,1-0ichloroethane

1,1-0ichloroethene

1,2,4-Trichlorobenzene + • - ~ - - - - - - • - .... - - ..... - - •••••••

1,2,4-Trimethylbenzene .. _------_ ... _-_ ............. . 1,2-Dibromoethane

NO -. --NO

5000

5000

NO 5000

NO 5000

NO 5000 .... ---_ .... _------_.

NO 5000

... -_ ... _---+-_.+. 5000 Vppb 01/27/12 nicollez

+-+.+ --_ •••••• .... _ ... _------_ .... 5000 Vppb 01/27/12 nicollez

5000 Vppb 01/27/12 nicollez ....... - . - .. - . - . ~ - . ~ .. - .....

5000 Vppb 01/27/12 nicollcz

5000 Vppb 01/27/12 nicollez

5000 Vppb 01/27/12 nicollcz __ ••• _____ • + • _ •• _ • __ ••••••••••••••••••••• _ •••• __ • • ... • ••••• ~ ... M •••••••• _ ••••• _ ••••• __ ••••••• ~ •••

NO 5000 5000 Vppb 01/27/12 nicollez ~ .. __ •• ~ __ •• _____ • • • • •• _______ • _ • • •••••••• _ •• _____ ••• __ •• ~ .. H ••• _

NO 5000 5000 Vppb 01/27/12 nicollez · ~ --- ..... - - - - . -- - - . -- - . - ................... -.. - ...... - ... - - -- - - .. - .. -"" -. - . ---..... _. . ... -. -.... -. -........ - ...... ----- .. -- - . -. --. -... - .. -... ----... - ... -..... -.. --..... -... . 1,2-0ichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez

..•.. ______________ .. _ .. __ . _____ . _________ ..... 0-·-- __ --_.-- ._._. ______________ ._ ................................... _ ......• _ •••......... _ .• _ •. __ ._ .. ____ ......... .

1.2-0ichloroethane NO 5000 5000 Vppb 01/27/12 nicollez ._ .. _---_ ....... _-_ ... ---- ............ ---------_. __ ._._ ..

1 ~~~~~~~.I?r.~~!~~~~~ ............... _ ............................ . NO 5000 5000 Vppb 01/27/12 nicollez

~ ~3~?-!~i.~~~~XI.~~.~~~~~ ........................................................ ~~ ...... ?~~.~.... ...... . ...... ?~~.~ ...... _ y~~.~ ......... ~~!~!~:.~ ..... ~!~~I!~~ .. . 1.3-0ichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez ·1:4~Dich·lc;roi:;e~ze~e············ ............................................ ···NO······S·OOO·················· ·S·OC)O······· ·Vppb········ ·o1"t2"7i1·2······~ic~liez··· • __ ..... _ .. _ •••••• _ ..... _ • _ ..... _ • _ .......... _ ••• ~ ______________ ••• _ ••••••• _ •••••••• H _ •• _______________ ... ___ •• _ •• __ •• _ • _ • __ • ________ ••••• ~ __ •• __ • _ • _ H ••••• __ •• ___________ • __ • ____ ••••

. ~~~t.~~!~~I~~n~ .................................................................. ~~ ...... ?~~.~ .................. ~.~~.~ ........ ':'.~~.~ ......... ~~!~!~:.~ ..... ~!~~I!~~ .. . Benzene NO 5000 5000 Vppb 01/27/12 nicollez · --. - . - --. - - - .... ----- --- - -- - - ... - - . - - - - --- -- -- . - . - - - . -- . ~ ... - .. _. . .. - .. - . - . - - .. - -- ---- - - . - - . - - --... - . - - . . . . . .. . .. -- - - .. - - --- ... -.. - ---. -........ - . - ... --- . ---- -- -- - -- - - - - - - - - - - .. Bromodichloromethane NO 5000 5000 Vppb 01/27/12 nicollez ..... _ ...... -... - .. _------_ ............... _ .. - ....... -- .. __ .. _--_ ... - ... _- -_. __ ._--_ ...... - .... -_.- ... -- ........ __ .... __ .... _.- ..... _ ........... -.----_ ..... _----_._ .. __ ...... . Bromoform NO 5000 5000 Vppb 01/27/12 nicollez

Bromomethane NO 5000 5000 Vppb 01127/12 nicollez ... __ .. _---------_ .. _-------_._ ...... - .. -.------------_._ .. _ .... _-_ ... _.- ._ .. _ ... _.- ............ __ .- .. _ ... - ... _ ....... -_ ... --.-_._._- ...... -_ ....... _ ........ -............ -- .... -. Carbon Tetrachloride NO 5000 5000 Vppb 01/27/12 nicollez .. - ........... ----------------------_._-----------------_ ..... __ .... _ ... __ ............. -._.-.----._--._ ... -....... _ ..... _----_._-----.- .. _._.,_ ......... -.- ... __ .... _ .... _ ....... . Chlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez .... _--_._-_._----_ ... _-----_ ...... _ .. _ ..... __ ..... __ ._* ...... __ ...... _-- ... _ .. _--.----_._. __ .. _- •........ _. __ .. --.---------_.-_._._- .... -...•... _ .... _ ....... _.-_ .•.. _._ .... . Chlorodibromomethane NO 5000 5000 Vppb 01/27/12 nicollez · - ..... -... ---.. --. -..... - .. --.. - ........... - ........ - .... -...... - ~ .. -- - - - . - - - - - . - ~ -. - . - - .. - . - - - - . --- -.. - ..... --.... - ....... - - - - ..... ---- .. - - -- ......... ~ ..... -.. - . .. . . - . - - - --......... -. -- - .... - ... .. Chloroethane NO 5000 25000 Vppb 01/27/12 nicollez · ..... - -_ ... -.... - . -... -.. -----. _ .. _. --. -..... ~ -.. -... - - ... -- ---- - - - _ ... - _ ......... - ...... -- - . -.. - . --...... -.. - -................. - ... - - .... ---- - . -.. - ... --. . .. . .. . ... - - - - - - - -- .. - . -........ - ...... - . Chloroform NO 5000 5000 Vppb 01/27/12 nicollez .. _- .... _-.- ..... _-------_ .. --._- .... __ .- ... -.---------------_ ...... _ ............... _ .. _ ............. -.................. -.. __ .. _-- ........ _ .. _ ........... _-------.-.-.-._.- ....... . Chloromethane NO 5000 25000 Vppb 01/27/12 nicollez - - - - - -- --- -- - -- ----------.. -. ----.. - -. ---... -. --. ---... --...... --........ -- - ... -.......... -----. - - - ..... ---... --- --- -- -- .... ~ ....... --. --.. ~ .. -. -.. -.... -............ -. ----- ----- ... - --.. --.. . cis-1.2-0ichloroethene NO 5000 5000 Vppb 01/27/12 nicollez - -. -_ .. ---- _. - ------ --- -_ .. -- -- --- _ ... --_. _ .. -- - _. --- _ .. _. -_ ....... -.. _ ......... -........ - .. - -'. -_ ........... _ ..... -_ ............ _.,.,." - ---.- .... _ ............ -----_ .. -_ ... - - -- - -- -.--_ ..... -.......... - ..

cis-1,3-dichloropropene NO 5000 5000 Vppb 01/27/12 nicollez · .. _ .. _ .... -_ .. --_ ...... ----- -. -.... _. --..... _ ...... - - _. - -_. - - - - - _ .... _ .... _ .. _ ... _. _. _. - _. _ .. - - ....... -- _. -" . _ .. _. - _. - - - - - - _. --- -- - _ .. - _. - - --. _ .. _ .......... _ .. _. -- -_. _ .. -- _. - - ..... .. Oichlorodifluoromethane NO 5000 5000 Vppb 01127/12 nicollez .-_._---------------------_ .. _._-_._ ......... _._----_ .. __ .. _ ........ -_ ... _ .. -_ ... _ .. - ... _ ........ ..- .............. - .......... -_.- ....... _-_._ .. _-_ ...... _._ ...... _ ... __ .... _------.-- ..... _ .... _ ....... . Oi-isopropyl ether (OIPE) NO 5000 5000 Vppb 01/27/12 nicoliez ._ ..... --.--_._-----------------_._---_ .. ---------------_._---_._ ........... _ .. _._ ... _---_ ... _ ..... _--_ ........ __ ._ .... -.--_.--------_.-- ...... _ .................. _------------.---- .. .

. ~~~Xl.~~.~~~~~ ................................................ _ .................. ~~ ...... ?~~.~ ................... ?~?~ ........ ':'~P.~ ......... ~~!~!(~.~ ..... ~!~~I!~~ .. .

. ~!~Xl._~~.~~~~~!~!~.~~ .~~!~~) ....... _ ... .. . ...... .... . . . .. .. . . . . . . . . . . . -..... ~~ ...... ?~~.~ .................... ?~?~ ....... .':'~~.~ ..... _ ... ~ :!~! ~~.~ ..... ~ !?~I!~~ .. . m and p-Xylene NO 5000 5000 Vppb 01/27/12 nicollez -_ ................ -_.--_._-_ .... ---.. .-._---.------_ ..... _ ..... __ .. . ... __ ._-----_ ..... _....... -_ .. _---- .. ---------_ .. -_ ... _- .. - ................. _-_._----------- .. Methylene chloride NO 5000 5000 Vppb 01/27/12 nicollez · -............. -.. - --- --- . - --.. -. . . . . . . . ~ . - . - . - . - - .. --- - - - --- ... ---............. - - .. --. -. - - - - .. - - -- . --....... - .. . Methyl-t-butyl Ether (MTBE) NO 5000 5000 Vppb 01/27/12 nicollez · ... -... -.......... ----... - . -. -..... -... _. . .. -................... - -- - " .... --.. - . . . . . - .... - ... - . -- - .. - .... - - ...... - .. - - ..... -... - -.... ~ .... . o-Xylene NO 5000 ._-_._----_._ .. _. __ .............. - .. _ ...... _ .. _--------- ...... _- ... __ .... _ ..... _ .... __ ... Styrene NO 5000

_ .. _._-_. __ .. _---------_ ....... - ........... __ ._-- .. ---------_ .. _-_.- .

t-Butyl alcohol (TBA) NO 5000 .- .... - .. ------------------_ .. -.... - ... -- .. -- .. _.---------------_._-_ .......... -_._._-----_._._-------.

5000

5000

10000

Vppb

Vppb

Vppb

Tert-amylmethylether (TAME) NO 5000 5000 Vppb ........ _-----------------_ .... _. __ ._-_ .... -.... -.... _._.------.- .. _ .. ---- ... - ...... - .. __ ._-- .... _----.------ ..... _-_.- ....... ------_._--Tetrachloroethene 62000 5000 5000 Vppb -.............. -_ .. -... -.------ ................... -._ ... -....... _-_.- .... -- ........... - ... _-- ..... _ .......... _._- ...... - ... _. ._-_._ .. -_ .... . Toluene ......... ~~ ...... ?~~.~ .................. ?~~.~ ....... .':'~~? trans-1,2-dichloroethene NO 5000 5000 Vppb

trans-1,3-dichloropropene NO 5000 5000 Vppb ....... -.-- ... ---------_.-.---._ ...... _ .. -.- ........ - ...... -.---------._.- ..... - ... -._----- .... - ... _--- ...... _ .... . Trichloroethene NO 5000 5000 Vppb

.... __ .. _-_ ........... _ .. _ .. -

01/27/12 nicollez

01/27/12 nicollez

01/27/12 nicollez . . __ .... - ....... __ .... _.

01/27/12 nicollez

01/27/12 nicollez .. __ ._.-.- ....... __ ..

01/27/12 nicollez

01/27/12 nicollez

01/27/12 nicollez

01/27/12 nicollez Trichlorofluoromethane NO 5000 5000 Vppb 01/27/12 nicollez ·Vi~YI·6;1~~i~£~····························· ..................................... ·NO····· ·5'000 ................. ··S·OO·O······ ··Vppb········ ·o1i27i12···· ·~icolie~ _ .. _ ... -.. _. __ .. _ ..... _._-----_ .................. _ .................... _ .. _.-._ .............. _._ ......... _ ............. _ ..... , .. -------- .... -.... _ ................. __ .- ......... _-_ ....... .

. ~y.I~~~~.~~~t.~~) .................................................................. ~~ ...... ?~~.~ .................. ?~~.~ ........ ':'~~? ......... ~:!~!~~~ ..... ~!??I!~~ .. .

NO = Not Deteced or < ROL ROL = Reporting Detection Limit OF = Dilution Factor

ASSOCIA TED LABORA TORIES Analytical Results Report

Lab Request 298455 Page 2 of 8

Sample#: 298455-002

Matrix: Air


Collect Time: 12:46 PM

Compound Method: EPA 8260B

1 ,1 ,i-Trichloroethane


Client Sample #: VEW-3-D

Site:

Collector: Client

__ ----=R'-'-c=s=-=u::..:.lt=----_D=o..:.-F ________ 8Ql~ ___ J! nits Ana lysis Date Ana Iyst Prep Method: Method QCBatchlD: QC1122815

ND 10000 10000 Vppb 01/27/12 nicollez ------------_ .................................... --00-··.- .......... __ . ___ .... __ . __ ...................... _. _________ .... __ ... - .... -.......... __ .- ... - .. ,. __ .... -.- __ ............... . 1,1,2,2-Tetrachloroethane ND 10000 10000 Vppb 01/27/12 nicollez .... _. ___ .... 0 ........................................ _., .•...•.•.. _0 ____ 0_ .. __ ._ .......... _ ................ _ ....... _._ ••••.•...... ' ..... _._0. _., ........... _·_.c· •• ___ •. _ ••••• _ ........... .

1,1,2-Trichloroethane NO 10000 10000 Vppb 01/27/12 nicollez .......... -............. - ... - .............. __ .... __ .. _------1,1,2-Trichlorotrifluoroethane NO 10000 10000 Vppb 01/27/12 nicollez ----------- .. - ..... _--_ .................................. - .................. . ........... ________ ............................. ·0· ............ . .... _-_ ... _----_. __ .... _------_ .. 1,1-Dichloroethane NO 10000 10000 Vppb 01/27/12 nicollez ---_ .. __ ._-_ ..... __ .... _----- ......... - .. - ..... .

1,1-Dichloroethene NO 10000 10000 Vppb 01/27/12 nicollez ...................................... __ .---.-_ ... -----_ ...... _--- ........ __ . __ ........ _- ........................... _-- ..... - ............... --.. . ............................... _-_. __ ._-----_ .. 1,2,4-Trichlorobenzene NO 10000 10000 Vppb 01/27/12 nicollez

................ - .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. • .. .. .. .. .. .. .. .. .. .. .. .... .. ................. ~ .. .. .. .. • .... .. .. .. .. ... .. .............. - .................................................................. * .. .. .. .. .. .. .... • - ........... , ...... ..

_~~~~~_-!~i_r:!~!~XI_~~_~~~_~~ __________ . _._ .. _ ... _. _.. .. _____ ~~. ____ ~~_~~_~_ _ _ 10000 01/27/12 nicollez ....... __ ._-.---_._.--- .......... -

Vppb

1,2-Dibromoethane NO 10000 10000 Vppb 01/27/12 nicollez ................ _._._-------_._--_._ ....... . . ........ - .... ~ . --........ - . . .. . . . . .. .. . .. . ... -.. - ... -..... - - . -- - .. - . - - .. -- -1,2-Dichlorobenzene NO 10000 10000 Vppb 01/27/12 nicollez -- . -- -- - - - - - .. - - .. -- .. --- .. --. - .. - . -... , ...................... " . .. . --......... - . .. .. - . - - ... - - .. - ... -... -... -........ ~ . ........... _ • • • •• • ..... _ ... _ • __ 0 • __ ~ k • _ .. __ • _ ••• _ 4 __

1,2-Dichloroethane NO 10000 10000 Vppb 01/27/12 nicollez .. _-----------_._--------------_.......................... .------_._------ ...... _._ ........ . .... - .......... _. __ .... --- ...... _._------_._--------_. __ .-

10000 Vppb 01/27/12 nicollez . __ .. __ .. _ ... _-_ .. _._---_ .... _._---------------.----._._---_~~~~~~~~!~r_~~!~~~~~ _______________________ . ____ . ________ . ___ . __ . __ .... _____ . _~~ _____ ~~_~~_~ _______ _

_~~~~~_-!~i_~~!~XI~~_~~~~? ____________________ . __ . __________ . __________ . _ .. _. _____ ~~ ____ ~~_~~_~ _________ . _____ . __ ~~_~~_~ ________ y?p_~ _. ______ ~~!~~~~_~ _____ ~!:~I!~_~ __ _ 1,3-Dichlorobenzene ND 10000 10000 Vppb 01/27/12 nicollez

- - • - - - - - - - - - - - - - - - - - - - - - ............... - ........ - •• - ........ ~ • • ... • .......... - • - - •• - - • - - - - - • 0 _ •• _ ••• _ ............... _ .......... _ .... _ ..... __ • _ • • • • • • • • • .. • • • • • • • •• • ....... ~ ~ ...... _ • _ ........... _ • _ .... _

1 A-Dichlorobenzene ND 10000 10000 Vppb 01/27/12 nicollez - .. -- -- -- .... - . -----.. -. - .. --........................... -......... - ...... - - -- --- - ... - . - - - . - - . - ......... - ........ -. -..... - - .. ~ .. -....... - ....... -.............................................................. - ..... ..

-~~~~~¥!~~~~~~~------- --- -- ---_ .. -- -- -- --- -- -- ------------- ----- ------- ---- ------~~-- ---~~-~~-~----- -- --- -- --- --~~-~~-~- ---- --y?~-~ . __ .- ---~~!~~~:-~- -- __ ~!~~I!~~ __ _ Benzene ND 10000 10000 Vppb 01/27/12 nicollez -----------------_ ... _ .................................................... -- .. -------_ ..... _ ........................ '--"." ........................ - ....... -. __ ..... _ ......... __ .

Bromodichloromethane ND 10000 10000 Vppb 01/27/12 nicollez -B-r~~(;f~~~------------------------ ------- --- -. -----. -.. -- ------. --- --. -. -- -----NO-----10-0C)0---· ------ - ----- -1600-0 -- --- -\ipp-6- ------ -01i27i1-2---- -~i~~li~~---

...... - _ ............. - - .. - - - .. - _. - - - - - - - • - - - - - • - .... - - - - ...... - • - ........ - •• - ...... - - ................ _ ...... - _. - • - - - - ••• - - - - • - .......... - ......... - - - _ .. - •• .... •• 0 .. _ .. _ _.. • _________ • _ ....................... __ ~

Bromomethane NO 10000 10000 Vppb 01/27/12 nicollez - .. _ ... -_ ............. -... _ .... -----_ ...... _ ... - _ .... _ .... _ ......... _ .. - ..... - .. _... .. ~ ..... - .. -..... _ ............. - ....... -_ ... -- ~. - . - - .. - - - _ ....... -..... _ ..................... - . . . .. " ... -. -- ........ -. -_ ................. . Carbon Tetrachloride NO 10000 10000 Vppb 01/27/12 nicollez · .. --.............................. -.. -......... -.... -................... - - ... - . - _ .. - ................ --............................. - .... - .. .. .. .. . .. .. . ............................................. -.. ~ .......... - ... ---- .. - - -- - - - - . -Chlorobenzene ND 10000 10000 Vppb 01/27/12 nicollez

_ ••• ______ ................ _ ......... __ .... _ .............. _ .......... _ •••••• ___ ._._ ••. _ •• _ • __ • ______ •• _ ••• ___ ....... _ •• _ ••••• , .•• __ ............. _, • ••• • ••••••••••••• - ••• 0 ______ --_._---------_.-.-

Chlorodibromomethane ND 10000 10000 Vppb 01/27/12 nicollez • .. - - - - - • - - - .... - - - - - .... - .... - .......... - ......................................... - - ... - • - • 0 ~ _ .. + _ • + _ ... __ ...... ___ •• ___ • 0 __ •• ___ •• _ • • • • .. • • • ... • .... _ & • _ ... _ _ + .... ___ .... __ •• ____ •• _ .. __ • _ .. __ ........................... .

Chloroethane ND 10000 50000 Vppb 01/27/12 nicollez ...... _ .. _ ... __ • ___ • __ ......... _ ............................ _ ................... _ ....... ~ ............... ___ • __ ... ____ .... __ .. ___ ..... _ ........... __ 4 ••••••••• ~ ~ ....... & ......... _ ••• _ • _ ....... _ + _ • _ .. ____ ~ _____ .... _ ...................... .

Chloroform ND 10000 10000 Vppb 01/27/12 nicollez .... _. - - - ___ .............. _ .............................................. "" ..... _ ..... - • - ~ ....... - _. - - + - _ •• - - - _. - _. ___ • _0 _.0 ••• _ ... _ ..................................... _ •.•. _ . _. _________ . _ • ____ ... _ .. _ ......................... __ Chloromethane ND 10000 50000 Vppb 01/27/12 nicollez ___ ........ __ ................. _. __ ..... __ .. _ ............... ___ ........ ___ • __ ~ ...... __ •• & .. _____ .. ____ • _ ................ _ ..................................... 0- •••• 0 ............ _ ............................. _____ ... ______ • ____ • _ .. _ ....... _ ..... ..

cis-1.2-Dichloroethene ND 10000 10000 Vppb 01/27/12 nicollez .. _ .. - - _ .. _ .. _ .......... _ .. - - __ - - - - - _ ............... """ _ .... - - .. _ .... ~ .. _. - - - .......... _ .... _. - - _ ...... - • _ ••••• 4o"''' ...... ~ .... ____ .. - __ .... - - ..... - ........... - ..... - ............. - _ ........ - - 0 0 _ • __ • _______ .. __ ..... _ ............... .

cis-1,3-dichloropropene ND 10000 10000 Vppb 01/27/12 nicollez ........ _ ... 4o _____ ......... .- __________ ....... _ ••• _ .... - _. _ ........... _. _. & _ .... - - - __ .. - - - - _ ...... _ ....... _ ... __ ..... 4o .... _ ............. - _ ............... _ ........ - _ ... - - - - - _ .. _ .. _. - - ____ •• ___ .......................... .

Dichlorodifluoromethane ND 10000 10000 Vppb 01/27/12 nicollez - .. - - .... - - .. - .... - - .... - •• - ............ - .. - ......................................... - ..... - ... - • ~ •• 0 • ____ ....... _ .. _____ .. _ 0 __ .... ___ • ____ ... __ ... _ .. ___ • ___ .............. _ ............. _ ..... ~ .... _ .... _ .. _ .... ______ .. ___ • ___ .. _ .. __

Di-isopropyl ether (DIPE) ND 10000 10000 Vppb 01/27/12 nicollez • ... - - - - _ .. - - • - - • - - - - - - - - .. - - ... - - - • - • - - - .. - - .. - ... - - • - - .......... - .. - ..... 0 .. ____ • ___ .. _ .. _ ...... _ ..................... _ ......... ___ ................ _ .......... ~ ••••• _ •••••• 0 ______________ .. ___ •• _ .. _ ............ ~ ... .

_~~~X~~~~~~~~ ____________________ _______________________________________________ ~~_ .. --~~_~~_~_ --- __ -_______ . _. -~~_~~_~ ____ . __ y?~_~ _________ ~~!~?~~_~ __ . __ ~!~~I!~~ __ _ _ ~!~XI_-!~_~~~~~!~!~_~~_(~!~9 ___________________________________________________ ~~ _____ ~~_~~_~. ____________ . ____ ~~_~~_~. ______ y?~_~ _. _. ____ .~~!~~(!_~ _____ ~!9~1!~~ __ _ _ ~_~~_~_~~~~~~~~ ______________________________________ . __________________________ ~~ _____ ~~_~~_~ _______________ . __ ~~_~~_~_. ______ y?~~ _________ ~:!~~~:_~ _____ ~!9?_1!~~ __ _ _ ~~!~X'~~~_~~!9_~?_~ ______________ _______________________________________________ ~~ _____ ~~_~~_~ __________ -______ ~~_~~_~_. _____ y?~_~ ____ ... _~:!~?~~_~ _____ ~!9~1!~~ ___ _ Methyl-t-butyl Ether (MTBE) ND 10000 10000 Vppb 01/27/12 nicollez ••• _ ........... - ••• -~- -_ •• - ••• __ •• _-. _e •• _._ ....... ~ •• ~ •••• _ ••• _ •• _ ••• _______ - __ • ______ • ____ ._. _. ___________ - _. - - ___ ••• + ........ __ •• ~ ............ ~ _ ........... _. _________ ._._ •••• _. __ ••

_~~~~I_:~_: _________________________ . -___________________ . ___________ -________ -_____ ~~ __ -__ ~~_~~_~ ______ -___________ ~~_~~_~ ____ . ___ y?~_~ _________ ~!!~?~~_~ _____ ~!9~1!~~ __ . Styrene NO 10000 10000 Vppb 01/27/12 nicollez -t~But};I-~-I~~h~f(TBA)----- ---- -- ------- ---- -- -.. ----- -. ---- --- ------ ---- --------NO-- -- -10-00-0--- ---- --- ---- . --20-000- -. -----vpp-6 --. --- -- -o1i27/12- -- --nic~li~~ ---............ -..... -- ........................................................ ~ . ~ .... -~ ......... - - ....... -.. - .... - -.... --.. - -..... -... --- ............. --. - ........................ - - . -- . --. - .. - . - -. -.. -.. -...... - .... _ .. - - . ~ . --- -Tert-amylmethylether (TAME) ND 10000 10000 Vppb 01/27/12 nicollez .... _____ .. _.0 .................. _ .................... _ .................... k .. __ ....................... _ ................................. _ .............. _._ .... __ . __ ................ _._ ........ ___ .. _ ..... ____ ...• _ ... . Tetrachloroethene 180000 10000 10000 Vppb 01/27/12 nicollez T~-I;;~~-~---- ------------------ -------. ---- -- --- -. --- .. -.. -. ----- -- --- -- --- --. ---- -NO-- ---10-0C)0- ----- --- --- ------10-00-0 ---- ----Vppb' ----- ---01i27i12 ----'~i~~li~~ -.. -t~~~~---_i:2~~ii~-hl-~roeth~-~~-- ---- ---- -- ----- -- ------. -----. -------- --- --- ----- --- -ND--- --10-00-0-- ---- ----- --- .. --10"00-0- -----. -V-ppb -----. -. -01i27i1-i -----ni~~li~~' --

:t!~:~~:-:~,:~~~:i?:~I:~~~?~~p:~~:~:::::::::: ::: :::::::::::::::::::: ::: ::::::::-: :::::: :~~::: ::~~:~~:~:::::::::::::: -:: :~O:~?:~::::::: :Y?P:~ -:::: -.: :~~!~~?1~::: ::~~~~I!~~: -. _~:!~~_I?_r_~~~~:~_: ____________ . _____ ._ .. ___________ . _. __ .. _. _ .. _. ___ . ______________ ~~ _____ ~~_~~_~_ .... _. _____ . _. _19_~?_~ _______ y~~_~. _. _ ... __ ~1!~?~~_~_. ___ ~!~?I!~~ _~~~~~}?_r_~!I~~:?_r:!~~~_~~_:_ . _____________________ . _______________________________ ~~ ___ : _~9_~~_~ _______ . ____ . ___ .~~_~~_~ _______ y?~_~ _________ ~}!~~~~~_ ... __ ~!:~I~~~ __ _

_ y!~XI_~~}?_r!?_: _______________ . _____ . __ . ____ . ____ .. ___ . __________________ . ______ ~~ _____ ~~_~~_~ _______________ . __ ~~_~~_~ ______ . y?~_~ _____ . __ ~:!~~~!_~ _____ ~!~?_I!~~. __ _ ~y_I~~~_~_r._~t_~9 _________________ . __ . _____________ . _______________________________ ~~ _____ ~~_~~_~ __________________ ~~_~~_~. __ . ___ y?~_~ __ _______ ~~!~~(!_~ _____ ~!~~I!~~

NO = Not Oeteced or < RDL ROL = Reporting Detection Limit DF =: Dilution Factor


:.:\: /:/ ,./{_ .. _- ..


Sample #: 298455-003 Client: Block Environmental

Matrix: Air

Collect Date: 01126/12


CHen! Sample #: VEW-1-S

Site:

Collector: Client

Compound Result DF .~_ .... __ J~.DL Units Analysis Date Analyst Method: EPA 8260B Prep Method: Method QCBatchlD: QC1122815

1,1.1-Trichloroethane NO 1250 .... ~.~?~ ....... . '!p.~~ ........ . ~~!~~~~.~ ..... ~!~?I!~~. ·1:1~2'.2~Tetrachl~~~;;th~ne· ..... , .. "" ....................................... ·NO .. · .. '1'25'ci' -- ... '.... .. ... ~.~?~ ........ '!?~.~ ....... ~}!~~~}.~ ..... ~!~?I!~~. :~;~ ~?~-j~i~~~?!~~!~~~~~~~::~::::::::::::~ ~~::::.:.:::: .. :::.:.:~:::':::::.:' ::::: ~~::.:.: ~:~~:~:::::: ............ ~.~?~ ....... . '!p.~.~ .... .... ~!!~~(~.~ .... ~!~?I!~~ .

. ~ ~~ :?-!~i.~~!~!~t.r.i!I.~~~?~!~.~~:: .............................................. ~~ ...... }.~?~ .......... ' ....... !.~?~ ...... . '!p.~.~ ..... .... ~!!~?(}.~ .... ~!??I.I~.~ .~ ~~ ~~~~~.I?r.~~~~.~~:.... ........................ ..... .... ........ . ..... ~~ ... }.~?~. ........... ... }~?~. ...'!?~~ ........ ~!!~7~!.~ .... r~~~?I!~~ .~ ~~~~~~~.I?~~~~h.:~: ........................................................... ~~ ..... }.~?~ ................... !.~?~ ...... '!?~.~ ......... ~!!~~(~.~ ..... ~!~?I!~.~ ... 1,2.4-Trichlorobenzene NO 1250 1250 Vppb 01/27/12 nicollez '1 :2~4'-Trfmett;ylbe'~~erie"""'''''''''''''''''''''''''''' ..................... NO'" . ·1·25·0 .. · ...... · ...... "1'25'0'" .... Vpp·b .. · .... "01'/27i1'2'" "riic~lie~'"

1:2~D~~~~~~~~~~~~~~::::::::::·.:::::: :~~::.::::.: .. :::::::: ." ::::::.::::.:::: :~~ .... ~:~~:~::::': ............. ~.~~.~ .. ::::. :Y?P:~: .::.:. ::~~!~~(~:~:' .. :~!~~I!~~·:. 1,2-0ichlorobenzene · .. ~ - - - .. - ...... - . - ~ - - - - -- - - - ........ - .... --- - - - - - - . - - - - ... ~ . 1,2-Dichloroethane ... _-_ .. _--------------_ .. __ .... ------_._----------_.

NO 1250 1250 Vppb 01/27/12 nicollez . -- . - - . - . - ~ - ............. - .. _. -... - .. - ~ ... - -- - - - - - . - - - .. - - - - - - - - . - - .. - .... - .. -......... - ..... -.. -................................. .

NO 1250 1250 Vppb 01/27/12 nicollez • _ •••• ____ • ~ _ •• • ............ _ • • ..... _ • __ • _ _ ___ • ____ • __ • _______ • __ • __ • __ '" .. __ • _ .................. __ ••• ~ _ ............ u ... _ ••

,1 !~~~~~~.I?~~~!~~~~~ ........................................................ ~~ ...... ~.~~.~ ................... ~.~~.~ ....... y?~.~ ........ ~~!~~(~.~ .... ~!~~I~~.~ .. . ~~~~~.-!~i.r::~!~XI.~~~~~.~~ .............................................. " ........ ~~ ..... ~.~~.~ .................. !.~~.~ ........ '!?~.~ ......... ~!!~~~:~ ..... ~!~?I!~~ .. . ~ ~~~~~~~!?~~~::~::~~.: ................................................... " ..... ~~.... :.~~.~ ................... ~.~~.~ ........ ':'.~~.~ ......... ~!!~~~~.~ ..... ~!~~I!~~ ... . ~!~~~~~~.I~~~~.~~.~~~.: ............................................................ ~~ ...... }.~?_~ ................... :?~.~ ........ ,!p.p,~ ......... ~~!~:~!~ ..... ~~~?I!~~ .. . . 4~~t.~~!~~!~~~~ ........ , .... , .................................................... ,~~ ...... :.~?~ .................... :.~~.~ ....... ':'?~.~ ........ ~}!~~~! .~ ..... ~~~?I!~~ .. . Benzene NO 1250 1250 Vppb 01127/12 nicollez .-_ ... -_._--------_._---_._-_._ ... - ..... -.-.-- .... ---_ .. - .... _._----_. __ ._- .. _--_. __ .. __ .. _ .... _ ........... _._ .. _ ........ _ ...... - ... __ .... __ ._-_ .. __ .... _._._ .. __ ..... _----_. __ ..

Bromodichloromethane NO 1250 1250 Vppb 01/27/12 nicollez ... _ ..... -._- ... ----._---------------_. __ ... _----_._ .... _ .. __ .- ............. -......... -.- .. ----.--- .. __ .- .. - .. -._---_ .. _.-----_._._-- .. _----- .. _-_._ ... -----_ ...... _.-- .... __ .- ...... _-_ .... _-

.~!?~~.f?~~ ........... _._ ........................................................ ~~ ...... :.~?~, .................. :.~~.~ ....... yp.P.~ ......... ~:!~?~:~ ..... ~~~?I!~~ .. . Bromomethane NO 1250 1250 Vppb 01/27/12 nicollez ----- -- - ---- - --- ------ -- ------ --_ .. _. - -_ ........ --_ ............... _ ............... -_ .... --. _ .... _. -_. -- - ----- - - _ .. _. - .. --- - - - - _. _ .. - - -_ .. -- - - -- ----- -- _. -.- .. -- -- .. ----- -. - - ......... -..... - ........... _ ....... . Carbon Tetrachloride NO 1250 1250 Vppb 01/27/12 nicollez .---_._----_._---_ .. _-_._._._- .. -.............. -_ ... --.-_.-.- ... __ . __ ._----_. __ ._-_ ... _--_ ..... --_ ... _._-----_ ... _.- .. ----_._ .. __ ._--_ .... _------------------_.------_ .. _.- ........... _ ... _-_. Chlorobenzene NO 1250 1250 Vppb 01/27/12 nicollez

- _ ... - - - - - _ •• __ .... - - _ ......................... - _ ...... _. _ .. _ ....... _ ••• _. - _ •• - - - • __ • - - _. - - •• _.' _. ___ 0__ .... __ • ___________ • _. _. _______ • _ •• _. ______ •• _ ....... ___ •• , •• _ ........... __ ... _ ... _. _________ • __ •

<?~I.~~?~i.~~o~.~~,~~~~.~~ ........................................................ ~~ ...... ~.~?~ ................... :.~~.~ ........ ':'?~.~ ......... ~!!~?~~~ .... ~!~?I!~~ .. . . <?~~~~?~~~~.~~ .................................................................... ~~ ...... ~.~?~ ................... ~.~~.~ ........ ,!p'p~ ......... ~~!~?~~.~ ..... ~~~?I!~.~ ... . <?~I.~~?~~~ ...................................................................... ~~ ...... !.~?~ ................... :,~~.~ ...... .':'?p,~ ......... ~:!~~(~~ ..... ~!~?I!~:: ... Chloromethane NO 1250 6250 Vppb 01/27/12 nicollez · - - - -- .. - -- - -- . - - --- -- - - -- ~ ---- - .. - - . -- ... - - - - -- - . - - - -- - - - - .. - - -- - .. - .. -.............. - -.............................. _ ....... -..... - ...... -- . - . -.. - - ... - -- - - . -- ---...... -..... -- .. - .................... - - . - - - - . - ..... - - .. -cis-1,2-0ichloroethene NO 1250 1250 Vppb 01/27/12 nicollez ._------------_ .. _. __ ._------_._-------------_._ .. _._--_._----_ .. __ ................................... _--_ .. _ ... _ .. _-_ ...... ----_ .. _--------------._--------- .............. _--------_._._. __ ._--cis-1.3-c1ichloropropene NO 1250 1250 Vppb 01/27/12 nicollez · . - . - . - . - - ... - - .. - . - - - ----- .. --- - -- --- - - - - - - - - - . - - . - - - - . - - .. - . - - ... -- - - - .. - - .. - ... - . - .............. - - ... - - - .. - ..... - - - - .. - . - . - . - - - - .. - - - - - -- -- ..................... - ~ ... -............ - - - .. - ............... .

O!~~I.~~?~i~!~?~~~~~~~.~~ ....................................................... ~~ ...... !.~~.~ ................... ~ .~~.~ ........ ,!p.P.~ ......... ~!!~?~] ~ ...... ~~~~I!~~ .. . Oi-isopropyl ether (OIPE) NO 1250 1250 Vppb 01/27/12 nicollez ....... ______ •••••••••••• __ ....... __ • ___ •• __ .... __ ......... _____ • ___ • __ ._ •• ___ ••••• __ • __ • _____ • ______ •• ___________ ••• _ ••• _r __ .............. ___ ..... ____ ._._. _________ ............ 0.' ___ •• _

Ethylbenzene NO 1250 1250 Vppb 01/27/12 nicollez ............................... --.... - ...... -.................... --............... - -.. - . - - - .. - ...... - ... - ....... - . - - --......... - .... - .. - -. - .... -......... -- .. - ...... - .. - ......... - - ... _ .. -- . - - --- -- - ... ~ ............... - -_ .. - - - - - - - .. -Ethyl-tertbutylether (ETBE) NO 1250 1250 Vppb 01/27/12 nicollez ----- - - .. - -.... - ~ ................................................. - .. -....... - ......................... - . - .. - ................. - - ....... -.......... - .... - ... - - ... - . ----- . - - - . --.. -.. --.. -... - ..... - .................. - . -... - - - . -.......... - .. .

m and p-Xylene NO 1250 1250 Vppb 01/27/12 nicollez .. --_. -- ~ --- ---- - - - -. - ---. -.... - -...... - . - .. -- .... -. -- .. - ...... -- - - . - - ..... - - . - . - .. - - . -. - -----_ .. _ .. - -. --- .. _. -., ... -...................... _ .... - - -.. - .. - - . - . - - - - - . - - .. - - - - - . -............... _ ... --- - - .. - .. -Methylene chloride NO 1250 1250 Vppb 01/27/12 nicollez

:~~!~yl~!~~~~~~~~!~~~:(:0.t~~~::::::::::::: :::::: ~:::.::::: .::::::::::::: :::::::~~:: ::::~:~~~: :::::.::::::::: :::~:~~:~:::: ::::Y~P~. :::::: ::~~!~~?~~::: ::~~~?I!~~':' .~:~~I.~~.~ ....................................................................... ~~ ...... }.~~.~ .................. ~.~?~ ...... .. '!p.~~ ........ . ~:!~~~~.~ ..... ~!~?I!~~ .. . ~~~.r~~~.............. ................................ .. .......... ~~ ..... }~?~ ................... ~.~?~ ....... '!?~.~ ........ ~:!~?~1.~ ... ~~~?I~~~ . . t~~~~~.I.~!9.~~~I.~~.~! ......................................................... ~~ ...... :.~~.~ .................. .?~?~ ....... yp.p~ ....... .. ~:!~~!~~ ..... ~!~?I!~~ .. . ~~,~~~.~~!~:~.t.~~!~~~.~~.\~~~~L ................................... ......... ~~ ...... }.~~.~ ................... ~.~?~ ....... yp.p~ ......... ~:!~?~!.~ ..... ~~~~I!~~ .. . T ~t!~?~,I~~~~.t~~~: ................................................... , . .. ... ~.~?~.. .. .: ?~.~. . . . . . .. . . .. .. .... : .~?~. .. . .. yp.P.~. . ... . .. ~ :!~7 ~~.~ ..... ~!~~I!~~ .. . . ~ ?I~:~.~ ...................................................................... ~~ ..... :.~?~ ................... :.~~.~ ....... '!?P.~ ......... ~ :!~~~!.~ ..... ~~~?I!~~ .. . . t!~~~,-.~ •. ~~?!~.~I.~~~~~~~.~~ ....................................................... ~~ ...... ~.~~.~ ................... :.~?~ ........ '!?~.~ ......... ~!!~?~~.~ ..... ~!~?I!~~ ... trans-1,3~dichloropropene NO 1250 1250 Vppb 01/27/12 nicollez 'T~i~h·I~·r-~~th~~'~·""'''''·''''''''''·''''''''''···''''·''·''·''··''''··''···''··· NO .... · ·1·2!{O· .... · .. ·· ........ '1'2!5ci' .. · .. V·pp·b ...... ·· 'o1i27/12" "'~i~~li~~'" 'Trich-I(;roiluo;'ometh'a~ie"""" ................................................ NO· .. ·· ·1·2t50 .. · ...... · .. · .. · .. ·1·25·0······ .. v·pp'ti .. · .. ··· 'o1iz7i1'2' .... rijcolie~··· 'vinyl' Ct;I~'ri~:je" .... , .......................................................... "NO'" · .. 1·2!50· ...... ·· .. ····· .. ·1·2!50· .. ·· · .. V·pp·b ........ ·o1i27/1·i .... 'rii;~lie~'"

~y:I~~~~:(t~~~~)::: :::::::::::::::::: ::::::::::::::.::::::: :::::::::: :::::: :::::::~~: ::::: ~~~~:~::~ ::~:::: ::.::: .:: ~:~~:~~ :::::: y~~:~ :~:::::: :~~!~~?~:~:: :::~!~?I!~~ ... ND = Not Deteced or < RDL RDL = Reporting Detection Limit OF = Dilution Factor




Matrix: Air


Collect TIme: 02:51 PM

Client Sample #: VEW-1-D

Site:

Collector: Client

Result DF _~C::..=o::..!m.!..!.l!p:..:::o:..:::u:..:..n-=-=d~ ____________ . __ Method: EPA 82608 Prep Method: Method

NO 5000 _~~ ~ =~_-!~i_~~~?!~~!~_~~_~ ____________ . _________ . ________ . __ _

_~ ~~=~_,~-_~~t_r~~~_I~~~~t_~~!:~ _______ . __________ . _____ ... NO 5000

1,1,2-Trichloroethane -_ ....... _- .... -------_ ................. -- ... __ ... . NO 5000

-. ~ - ... - .. -.. . -. -. -..... ~ .... --...... -- - . -............ -NO 5000

..... -- .. -----_ ............... __ .-1,1,2-Trichlorotrifluoroelhane -----------_ .................... --- ................ . 1,1-Dichloroethane NO 5000 -_ .. _ ......... -_ ....... -.--- ......................... . 1,1-Dichloroethene NO 5000

_._ • • _ .... u •• _. __ •• _____ • ___ •••• _ •• • ••

1,2,4-Trichlorobenzene NO 5000 _ • _ ...... ~ a- ....... - ••• __ •••••••••• .... - .. - ..... _ ....... - ............... _ .......... _.

1,2,4-Trimethylbenzene NO 5000 _____ • __ .. ____ .. _ .... ____ .4 ........ • ••• • •• . . . . - . ~ ....... - . - .

1,2-Dibromoethane NO 5000 ... -._ .. -._ .. - .. -_ .. _._---_ ............... -....... _ .... .

1,2-Dichlorobenzene NO 5000 ... - ... _------_ ..... __ ................................. - .. -1,2-Dichloroethane NO 5000

1,2-Dichloropropane NO 5000 _. ____ .. ___ •• _ ... ___ •• _ •• 4 •••••••••• • ••• •••• .. _··

1,3,5-Trimethylbenzene NO 5000

RDL

5000

5000

5000

5000

. Units Analysis Date Analyst QCBatchlD: QC1122815

Vppb 01/27/12 nicollez ... _-_._---_ ......... ----.--.---------_ ... .

Vppb 01127/12 nicollez - , ___ '.0. __ ..•.. --. ____ ._. ___________ ..•.

Vppb 01/27/12 nicollez .... _ ........ . . ~ .............. - .. - . ~ . -...... - ... .

01/27/12 nicollez - ... -.. ---_ .... Vppb

Vppb 5000

5000 ............ __ ...

5000

5000

5000

5000

5000

01/27/12 nicollez

Vppb 01/27/12 nicollez .. --- .... _ .. _ .. _ .. _-_ .. __ .... _-_. Vppb 01/27/12 nicollez

....... _ ....... - ... -.... - .......... -. Vppb

Vppb ......... ,.- .. -Vppb

Vppb

01/27/12 nicollez .................... - . ..- .... 01/27/12 nicollez

01/27/12 nicollez

01/27/12 nicollez ............ _ .... _ ............ _ ...... .

Vppb 01127/12 nicollez

Vppb 01127/12 nicollez ..... ---- .. ----_ .... _------ ... -................... -....... -. ......................................................... _ ... _ ...

5000

5000

5000 1 ,3-Dichlorobenzene NO 5000 Vppb 01/27/12 nicollez .................

1,4-Dichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez .... _ .. __ ..... _____ ..................... _ ................. _.......... ............... • _ ............ " ...................... _ ........ _... .., • _ ........ _ ................ _ ... _ •• 4 ••••• 4 ••••• _. ___ • _. ____ ....... _ .... _

_ ~:~t_~¥!~~!~~~~ _________________ . _______________ ... ___ . _. _______ . ____ . __________ ~~ ______ ~_~9_~ _________ .... ___ ?_~9_~ ______ ':'?~_~ _________ ~~!~!~~_~ _____ ~!~~I!~!: _._ Benzene NO 5000 5000 Vppb 01/27/12 nicollez __ .. _ ... ____ • _ • __ • _ •• _____ .. " _ .................. _ ••• ~ _ ••• _ •••••••••••••••• _ •••• ~ ...... _ ... _ •• _ .... __ •••• ___ .... ___ • _ 4 _ •• _ ••• ,, ___ ... • • •• • •••••••••• ___ • •• __ ••• _ ....... _ ...... 4 ................ ..

Bromodichloromethane NO 5000 5000 Vppb 01/27/12 nicollez ..... - .. -................ -.. -...... -.... _ ............................ - . _. . ........ -...... - ... - ... - .... -... -----..... -..... ~ ........... ~ ...... - . . . . . ................... - . . . .. .. .. .. . . ... . ... - ... -- ... --.. - - . -.......... - .... - .

Bromoform NO 5000 5000 Vppb 01/27/12 nicollez •• ___ ...... _ .............. ___ .. ___ ........................................ _ ••••• __ ....... _._ ..... __ .. __ ........... _ .................. " •••• _ ._._ •• _ •• ___ ........... • ........ • ..................... 4 ...... .

Bromomethane NO 5000 5000 Vppb 01/27/12 nicollez ................ '"' ... _ .. _ '"' • _ .. __ .. _ •• __ .... _ .. __ .................... ~ .... _ •••••••••••• _ •• _ • _ •• • _ ............. 4 __ ..... " .. _ ... 4 ........... _ •• _ 4- •• • _ ................... _ ................ __ .................... 4 ..... 4 _ ••• _ ........ .

Carbon Tetrachloride NO 5000 5000 Vppb 01/27/12 nicollez - .. - ..... - . -- _ ... ------..... _ ...... _ .... - .......... - ... -..................... - .... - . -...... - .. ... . ... ~ . -. . .. .... . .. . . . .. . . . .. . .. .. . ... . . . . . . . . . . - ............. - ............. - ............. -.................... _ ... - . Chlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez

• _ .... __ ... ____ .. __ ........... _ ............ _ •••••••••••••••••• __ •• •• 4 •• _ _ •• __ • " ........... " .... 4 .......... - •• _ , ......... ~ .. ~ •• - • • • • • .. - • .. .. .. • .. • • .. • • • • •••• ~. • - ...... - - • - •• _ - _ ...... _ ...... _ .... _ ••••

Chlorodibromomethane NO 5000 5000 Vppb 01/27/12 nicollez _. _ ... _ ...................................... _. -...... -........... _ .... - .. .. .. .." ... - -...... _ .... -_. -... " --_ .. - .............. - ~ ........... - ............ - .. _. . .. - , .................................... _. _ .. -_. - - -_. _ .... _ .... -........ -....... - -. -

_<?_~I_~:?_~~~~-~~--------- _________ -__ ---________ ----_. -_. - ------__ - _. --___________ .. ~~ ______ ~_~~_~ ________ . ___ . -_. __ ~~_~~_~ _______ .':'.~~~_ -_______ ~~!~?:~~ ___ -_~!~~I~~!: -__ Chloroform NO 5000 5000 Vppb 01127/12 nicollez

• ..... _ ............... _ .............. _ ..... _ ........... __ ........ _ ••••• _ _ _ ...... __ ........... _ • __ ••• _ • _ ....... ~ ................... _ ....................... _ .......... _ .......... _ • _ w _ ..... _ ....... ~ _ .......... _ .............. _ .. _ • _ ... _ • ~

Chloromethane NO 5000 25000 Vppb 01/27/12 nicoJlez •••• _ ............. _ ........... _ .................................... _ ........... " ••••••••••• __ •• _ .......... __ ,.._ .... __ .. _. __ .... _ ••• ____ .... ••• •• ··_ ................... ____ ...... _·.·._ ............... 4 ••••• __ •• _ •• _ ••

cis-1,2-Dichloroethene NO 5000 5000 Vppb 01/27/12 nicollez .......................................... _ ....... -.............................. - - - ........ - ....... -.. - .... -.... - ~ .... '" -"' ............ - _ ....... _ .... _ ....... ~ ... - .. -.......... -.. -..... -... - ....... _ .............................. _ ..... - --- - - . - ...... . cis-1,3-dichloropropene NO 5000 5000 Vppb 01/27112 nicollez

• _ .... _. _ ... _ .. _. ___ • __ ... __ • __ ~. _ .............. _ ............ 4 •••••••• ~ .. _ ..... __ ••• , .......................... _ ...................... T __ ... _ •••• , _ ... _ .. __ ..... ___ ......... _ ........... ~ ...... _ .. __ ..... _ • ___ ••••••••• '

_~!~_~I_~~?~i!~~~~~~~~~~_~~ _________________________ ... ___________________________ ~~ ______ ~~~~ ______________ . ____ ~_~9_~ ________ ':'?~~ _________ ~~!~?~~~ _____ ~!~?_I~~!: __ _

_ ~!~i_~?~~?~~~~~~~_~~~~~_~L _________________ " __ . ___ .. _______________ . _________ ~~ ______ ?_~9_~ ___________________ ?_~~_~ ___ . ___ ':'?~_~ _________ ~~!~?~~_~ ____ .~!~~I!~!:_._ Ethylbenzene NO 5000 5000 Vppb 01/27/12 nicollez

• ....... _ .. _ ..................... _ .. __ ............ ~ .. • • • • • • • .. .. • .. .. • • • .. • •• • •••••• ~. _ •• ~ 4 ••••••••• _ .......... _ ..... 4 ................ _ • _ ••• ~ •••• _ ....... _ • _ •••• _ ........... __ • _ ..... __ .. _ ... __ • _

Ethyl-tertbutylether (ETBE) NO 5000 5000 Vppb 01/27/12 nicollez _ •• __ • __ ........... ____ .............................. 4 .... _ .... _ ••• 4._ ••• __ •••••• _ ......... 4." ................... _.· ............ ·._.· .............................. 4 ..... _____ • __ "' .......... .

_~ _~~_~_~~~~~:~: ___________________________ .. _. __ . ____ . ________________ . _______ ~~ ______ ?_~~_~ __________________ ~_~9_~ __ .. _ .. _':'~~_~ _________ ~~!~!~~_~ _____ ~~~~I!~!: __ _

_ ~_~~~y.I~~~.~~_I?r!~_~ ________________________ .. ______ .. _. _____________ . _________ ~~ ______ ?_~~_~ ___________ .. _. _ ~_~~_~ __ . ___ ':'?~_~ _________ ~!!~?:!_~ _____ ~!~~I!~_z _. _

_ ~~~~y.I~~~~_~~~~~!~~~ _(~_~~~)_______ _ _ _ __ _ _ __ _ _ _ _ _ _ __ _ . _. ________ ~~ ___ . __ ?_~9_~ ___________ . ___ ~_~~_~ .. _ . __ .':'?~_~ _________ ~~!~?~~_~ _____ ~!~~I!~!: __ _

_ ~~~~I_~~_~ __ - __________________ -__ . __ ----- __ . -- ----- __ -__________ . _______ ~~ ______ ~_~~_~_ ------ __ .. --_. _. _~_~~_~. _. - -__ ':'~~_~ ___ -----_~!!~!~~_~ __ -__ ~!~?_I~~!: -_.

_~~y!~~~ ______ . ___________________ . _____________ . _. _ . __ .. _. __ . _____________ ~~ ______ ~_~~_~ ___ . ____ . .. _~_~9_~ __ .. " _':'?~_~ _________ ~!!~~~~~ ____ ~~~?_I!~!: _t~~~_ty_I_~~~~~~I_~~~~ ______________________ . _ __ _ _ __ . _____________________ ~~ ______ ?_~9_~ ___ . ___ . ________ .~?_~?_~ .. ___ .':'?~? _________ ~!!~!(~_~ _____ ~!~~I!~!: _.' Tert-amylmethylether (TAME) NO 5000 · .......................... --......... -..... . . .. . . . .. . . . .. . .. . . . . . . . . . . . . . .. . ..... - ~ ..... - ..... - - .... -_. - _ ....... _. _ ... _. - . - - - .. _____ ?_~9_~ _______ .':'?~? _________ ~:!~!(~_~ _____ ~!~~I~~!:. _. Tetrachloroethene 71000 5000 5000 Vppb 01/27/12 nicollez

....... _ • _. • ........................ _ •••• _ •• ___ • ~ • 4 •••••••••••

_~?I~:~_: _____________________________ .. ______ ._ .... _____ . _____________ .. _________ ~~ _____ ?_~~_~_ ._. ___ . _. _ .. __ ... ?_~9_~ ___ . ___ .':'?~_~_. _ . _____ ~:!~!(~~ ___ ._r_l!~?I!~!:. trans-1,2-dichloroethene NO 5000 5000 Vppb 01/27/12 nicollez

:t~~~~:-:1)~~!9~(~~??'~~~~~:~:::'::::: ::::::: -::::::::: -:::::: _: :::::::::: -::: -::: ~~:::::: ~:~~:~:::::::::: .. --: -::: ~:~~:~:::::: ::Y?~:~:::--:: _ :~~!~t~~~:: :::~!~~I!~~::-Trichloroethene NO 5000

_~~~~~_I?_r_~~I~?:?_~~!~_~~_~ ______________________ . _... _. __ . _____ ... __ . ____ ~~_. ____ ~_~~_~ .. ____ . _ .. ____ . _. __ ?_~~~ _ _ . _ .':'?~_~ _________ ~~!~?~~_~. __ . _~~~?_I~:!: _. _

_ ':'l~y'I_~~_I?_r_i?_~ _____________________ . __________ '" _... ____ . ____ . _. __ . ____ ~~. ___ .. ~_~~_~. _ _ _ _ _ _ _ _ _ ... ?_~?_~ _ .. ___ .':'?~_~ _____ ... _~:!~?~~_~ .. ___ ~!~~I!~!: ... _~y'I~~~~_(~~t_~~ ______________________ . _____________________________ . _____________ ~~ ______ ?_~~_~ _______ . __ . _____ . _?_~?_~ __ . __ . __ ':'?~_~ __ . ______ ~:!~?~~_~ _____ ~!~~I!~!: __ .

ND = Not Deteced or < RDL RDL = Reporting Detection Limit OF;::: Dilution Factor




Matrix: Air

Called Date: 01/26/12


Compound

Client Sample #: VEW-2-S

Site:

Collector: Client

Result DF RDL Units Analysis Da!~8.nalyg Method: EPA 8260B Prep Method: Method QCBatchlD: QC1122815 ----_._- - .. _--_ .. _--

1.1,1-Trichloroethane NO 5000 5000 Vppb . 01/27/12 nicollez ___ .. ________________ .. ____ ...... ___ ......... _._. ____ .. _ •. ___ +._-------------- _____ .0 __ •• ___ • ___ 0 •• ____ ---------_ •• ___ • ________ •• _. ________ .. _______________ • _______ ........... _ •••••

1.1.2,2-Tetrachloroethane NO 5000 5000 Vppb 01127/12 nicollez •• __ .. ________ ... _ ......... _ ............... ___ ......... ___ ••••• _____ •••• ___ _ ••• __ 0 .. _.·.- _. ________ •• , ••• ___ ......... _._ ...... ______ .. _____ ••••• _________ 0_ ... __ .......... .

1.1,2-Trichloroethane NO 5000 5000 Vppb 01/27/12 nicollez .......... - ........ - ..................................................................... -..... ~ - - - . - . - - - . - , - - - . - ... - . . - - . - .. - . - . - .. .' - -- . -- - .. - - . . ....... - - - . - - .. - .... - - - --- ... - .. -.. - - - - - . . .. . ... .. . ... -...... . 1,1.2-Trichlorotrifluoroethane NO 5000 5000 Vppb 01/27/12 nicollez · - - --........... - - . - - --.......... - --- --........ - --- - -. - -. - - - - - - - - - - - - - . - - - - - . - .. -- - - - . - - - - . - .. - - - . -. . .. .. -. - - -.. -- . - . - . - - - --- - - - - - ~ - - - . - - - . ---. -.... - - - .. -. -- ....... - - - . - .. -- . - - .. - - ... . 1,1-Dichloroethane NO 5000 5000 Vppb 01/27/12 nicollez ----------_ .. __ ... _-----_ ..... _--_._._-------_¥_----_._.- .. _- .. -_ .. __ . . ...... _ ...... -_.--_. __ ._. . .---------_ .. -._._-- .. _._- .-- ..... -.- ..... __ ... - ._-_._- .... . 1.1-Dichloroethene NO 5000 5000 Vppb 01/27/12 nicollez

... _-------- ..... _-----_. __ . __ .. -.--- ........... -------_ .. -_. 1,2.4-Trichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez

..... _-----_ .... _. __ . __ ._--._ ............... . 1.2.4-Trimethylbenzene NO 5000 5000 Vppb 01/27/12 nicollez ._ ....... _ ....................... - ............. - .. . ........... _---_ ...... -._----_ .. . 1,2-Dibromoethane NO 5000 5000 Vppb 01/27/12 nicollez .......... _-_ .. _-_. __ ... _ .. _----_ ................. . 1,2-0ichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez . _ ................................................. --- ............ " ... _- .. . ....... -._--_._. __ .. ....... _ .. __ .......... _-----------_ .. _------- .. - ........ _---_ .. 1.2-Dichloroethane NO 5000 5000 Vppb 01127/12 nicollez ...... _-_ ... __ .. _._ .... _----------_ ... _-- ........... _ .. _._-----_ .. -1,2-Dichloropropane NO 5000 5000 Vppb 01/27/12 nicollez

- - - - - - - - - - - - - .. - - - - - - - - - - • - - - - - • - - •• - - ••• - • - - _. - - - - - ••• - • - - - ..... - - • _. • ••••• - ........ - ......... ¥ ••••• - - ~ • - - • - - ~ - - _. - - - - - - + - • - - - - - - - • - ••• - • - - ....... - • - - - •••••••••• <+ - - - - ••••• - - - • - • - • - -

1,3,5-Trimethylbenzene NO 5000 5000 Vppb 01/27/12 nicollez - .. ---- ----- . - - .... - - - ------- - - -- - - . - -- .... - - - . - -.... - . - - - .. - . - - . - - - . - - - .... , .. - - - ... - .. -. -- ............ -...... _ ...... - - - . - .... - . - . - . - - ----.. - .. - ... - - - . --. ~ - --- . - ~ ........... -. - - . - -- - . - .. - . - -. --1,3-Dichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez

• _____________ .. _ .... __________________ ... ______ •• ___ • _ • ____ • _ • ___ ~ ___ ••• _ •••• _. •• _ k • _ ............ ___ •• ___ • _ .. _ • ____ • __ ~ _ ••• ___ .. ________ • _ • ___ • _ ... __ • __ •• _ • ___ •• _ ~ .. __ ~ • _ .. __ • _ • __ • _ •••• _

1 A-Dichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez ____ .. _ .. _ .. _ .... _ .. _____________________ .. _ • ______________ • ____ • ___ .... __ ••• _ • __ •• _ ................................... ____ .... _ • ~ ___ • __ ... __ .... _ .... __ • _ •• ___ .... _ .... _ .. _ • _ .... _ .... ~ ...... _ 4 __ • __ • ___ .. _ ••• __

_ ~~~t_~~~~~~~~~~ ______________________________________________________ .. __ .. __ ... __ ~~. __ . __ ~_~~_~ ___________________ ~_~~_~ __ .. ____ ':'?~_~ ______ . __ ~!!~?~!~ .. _. __ ~~~?I!~~ __ _ Benzene NO 5000 5000 Vppb 01127/12 nicollez __________ .. __________ ..... ____ •• __ .. _ • _ ........... _ ••• _ .. _ ••••• # • • •• • •• _ ~ ... <+' ................. _ .... _ ••• _ ••• _ ..... _ • _ .... _ # •••••••• _ ~ ........ _ ..... 4 • _____ .. __________ .. _ •• ____ .. _ • _ ..... _ ............ __ •

Bromodichloromethane NO 5000 5000 Vppb 01/27/12 nicollez ...... ___ ... ___ • ___ .. ___ .. _____________ .. _____ • _____ • _____ 4 ••• _. ___ • _______ • ________ ._. __ .. _. ___ ••••• _._. ___ • __ • _________ • __ .. _. __ .. _____ • ______ ._ ........ _ .... __ ••• _ ........ __ • _____ .. _____ • ___ _

Bromoform NO 5000 5000 Vppb 01/27/12 nicollez ..... -.. -.. _---_.- ......... --.---_.- ... ---_._------ .. ------- .. --_. __ ._------ .. ----- ._-------_._-_ .... _--------------_._---- ... __ ._-- .... --_ ... _._- .. -.... - .. -... - ............ _--------_._._-_ .... -Bromomethane NO 5000 5000 Vppb 01/27/12 nicollez

- .. - - - - .. - ....... - <+ .. - - ... - - ... - ..... - ... - ................................. - •••••••••••• - • • •• •• - - •• - ..... - • - - .. - - - - - ...... - - ............... - ......... - - • - ~ - ....... -' - - .. - • - - • - • - - - - ~ ~ • - • - - .. - - - - - • " ..... - ............... -

Carbon Tetrachloride NO 5000 5000 Vppb 01/27/12 nicollez _________ • ___ .. _ ...... _ • __ .. __ .. _ .. __ .. _ .... _ •• _ .... ~ .... _ ...... ,.. _ •• • ••• ~ • _ • _ .... _ •••••• _ •••• _ • ____ ........ _ •••• _ ...... _ •• __ •• _ ....... _ • _ ..... u • _ ••••••• __ .... _____ • _ • _________ ............. ___ ~ ~ _ • _

Chlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez · - . - - - - -- -- . ---. ----... --. -... -- ............. ~ .. -. - .. ~ ... -. ~ ... ~ ...... - . _.. .... - ..... - -- - " - - ....... -. . . .............. - ... - .......... - .... ----.. - . ~ . -. -- --- -- . - - -- - - -- - -- ~ ... - -........ -. -... -- - .. . Chlorodibromomethane NO 5000 5000 Vppb 01/27/12 nicollez · -------.. - ......... -............ -" ...... -....... - - .................. - ................. --.. -- .. - .. - - . - - --- ~ - - - -- - - - -- . - - - - -- .... -.... - ...... -.. --.... - - - ................. - . -. -- ... - - - ... --- .. ----- .. - - ...... , .. ~ -- . - -... -Chloroethane NO 5000 25000 Vppb 01/27/12 nicollez

.. -.......... - ... _--.--.-- .. ------_ .. ------ ... -------.--_ .. --- .. ------ .. -------------------------------.-----_ .. -.- .. --._ ... _--_ ... -.... -- ............... __ .. __ ._--_ .. _----- ... -- ...... _--------Chloroform ND 5000 5000 Vppb 01/27/12 nicollez

.. - .... -- .. -- ... ---- - - - --- - -- - -- -- -- - -- - - - - -- --- --- -- -- -_. - - - - --- -. - - -_ ... - _. - - _. - ----- --- - - -- - - - -- - -- --- - - - - - - _. - _. - - - - --- - - -_.-.'" - --... - .......... - .......... -_ .. -- -_. _. -. -...... -- .. -Chloromethane NO 5000 25000 Vppb 01/27/12 nicollez ------------- - -- _._----- ._- -- -_. --- - - -- -_ .. ---- -- -- - _ .. - _. -. _. -- - --- - -- _. - -- # •• -_ .. - .. _ ........ _.- --_ .. _----- --- -- - - -- -- - --- - .--- - ----- - -- - -- -- --_ ....... - _ ............. _. - -_. _ .. - ..... - .......... _ ••

cis-1,2-Dichloroethene NO 5000 5000 Vppb 01/27/12 nicollez ---_ .. _ .. _--_ .... _._._--_ .. _ ........ __ .. _ .... __ ._-_ ... _---- ... -_ .. _._._-_._._ ........... _ ..... _--_ .. _-_ .. __ ..... _----_ .. _-_ .. --_._------- .. -------.--- ...... _---- ........... _-_._-_ .. _-.-- ......... - .. .- ... .

_~~:~~~~:~i~~~?!~~~?_~~_~~ ___ .. __________ . ____________ . ___________________________ ~~ ______ ~_~~_~ ___________________ ~_~~_~. ____ ... ':'~~_~ _______ . _~:!~?~!? ____ .. ~~~~I!~!: __ _ Dichlorodifluoromethane NO 5000 5000 Vppb 01/27/12 nicollez

:~!=~~??~~~~~:~~~~rj~~~:~f::: :::: ::::::::: :::::::::::::: :::::::::::::: ::::::::~~:: ::::~:~~:~:::::::::::::::::: :~:~~:~:::::: ::Y?P~:::::~:: :~~!~~?~:~::: ::~~~~I!~~::: Ethylbenzene NO 5000 5000 Vppb 01/27/12 nicollez

:~~~:~~-!~:~~~!y~~!~:~~:($i~~~:::::: ::::::: ::::::::::: ::::::: ::::::: -:::::::::: ::~~:::: ::~:~~:~: ::::::::::::::::: :~:~~:~::::: :::Y?P~:::::::: :~~!~??~:~:: _ ::~}~?I!~~::: _~_~~_~_~~~¥~~!l.~ ______________________________________ . _______ . ____ .. ___ .. _______ ~~_. ___ .~_~~_~_. _____________ . ___ ~_~~_~ __ . __ . _y?p_~ __ . __ .. __ ~:!~?(}_~ ___ ._~!~?I!~~ __ _ Methylene chloride NO 5000 5000 Vppb 01/27/12 nicollez -M~thyl~t~b~iyIEth~;:-(M-T8E)----- ---- ------- --- ---. -.. -. -.. --- --- .-- --. -. -- -- -NO" --- -S-OClO---- -- -- --. --- -'---£500-0- -- -.-. \ippb"-- --- -o1i27i12 -'- --l~i~olie~ ---

:~=~~(~~~::::::::::::::::::::::::::::::::::::: ::::::: :::::::: -::::::::: ::::::::: ::~~::::- :~:~~:~: ::::::::: :::::::::~:~~:~: --::.: :Y?P~::: ::::: :~~!~??~~:::::~~~~I!~~ _:-Styrene NO 5000 5000 Vppb 01/27/12 nicollez -t~B~ty-l-a·lcohol-(TBA)----· ------ ----- ----- .. --. -- ..... -. --. -.. -- .... --- . --. --. -NO'" - '!50cio- --- ---. ----- -- -- -1cioclo -- .. -. \ipp-b-----· --01"27i12-- ---~i~olie~'-

:t~:~~~0.y!~~t:~~!~!~~~:(t~~~~:::::::::::::: ::::: :::::: -:::::::::::: :::: ::::::~~::::: :~:~?:~:::: ::::::: ::::: :::~~?:~_:::::::Y?~~::::::.: :~~!~?(~~: ::::~~~~I!~~::: Tetrachloroethene 38000 5000 5000 Vppb 01/27/12 nicollez iolu-~~~' ---- --. -.--. -. ----. -- ----.- ---------.- -.. ------ --- --- ----- ----- --. -- -- --NO -- -.. -s-ocio- -.... -. -. -------- -5cio-o~" -. -. '\ippi;---- --- 'o1i27i12' .-- -~i~oli~i"-

:t~~~~:-:~,:~~~!?~I:~~~~(~~:~~:::: :::: :::::::::::::::: ::::::::::: ::::::.::: :::::: ::: :~~ :::.:: ~:~~:~:::::::::: :::::::::~:~?:~::: -:: :y~p~:: ::::: -:~~!~t~~~:: :::~!~?:I!~~-.t!~~~_-_~._~~?_i~_~I_~~?p'~~P_~~_~. ___ .. _. ______ . _______ . _. _________ ._ ... ___ .'_' __ ._ .. ~~ ____ . ~_~~_~_._ .. ______________ ?_~~_~ ___ . __ . .':'.~~~ _______ . _~~!~?(J.~ __ ___ ~i~?I!~~. !:~~~_I?_~~~_t~~~_~ _________________ .. __ . _________ . __ . _. _ ... ____ . __ . _. ____ . _. ____ . _~~. _____ ?_~~_~ ____________ . _____ .?_~~_~ ________ ':'_~~_~ .. ____ ___ ~J!~?(!_~ ____ ~!~~I!~~ __ _ ~:~~~_I~r_~!I~~~?~~_t~_~~~ _________ ._._. ________ . __ ... _. __ . ________ .. ____ . _______ ~~ _____ . ?_~9_~ _____________ . _ .. _. ?_~~_~ __ . ____ .':'p.~_~ __ _ . _. _. _~~!~?(!_~_. ___ ~!~?I!~~ __ _ _ ':'!~~I_~~_I?_~i?_~ __________________ . _______ . ___ . _ ........... ___ ... ____ . _ _. ____ ... _~~ _____ ?_~~_~ _____ . __ . ___ ... ____ ?_~?_~ __ . _. ___ ':'~~_~ ___ . _ .. _~}!~?(~~._. __ ~!~?I!~~ __ _ ~y_I~~~_: _(~~t_~9 ___________________________ . ___ ... ___ ..... _ .. _____ . _ .. _ .. _. _. __ ., _~~ ______ ?_~9_~ __________ .. _ .. ____ ?_~?_~ ______ _ y?~_~ __ . _._. __ ~:!~?~!~_. ___ ~~~~I~~~ __ _

ND = Not Deteced or < RDL RDL = Reporting Detection Limit DF = Dilution Factor




Matrix: Air



Client Sample #: VEW-2-0

Site:

Collector: Client

Comp:.:::o:.!:u~n!..!:d=----_____________ --"Rc.=.e=-su!::..l:..=.t_--=D:...:.F_ ..... _. __ --BP_'=._. __ Units AnillYs is Date An_~y_~t Method: EPA 8260B Prep Method: Method QCBatchlD: QC1122815

.~~~~~._!~~~~!?!~~~~.~~.~ .............. _._... .... "._. _ .. ~~ ..... 5000 .. ___ . ____ . 5000 . \!.~p_~ .. _ .... _~1!~?(~.~ .. ___ ~!~?I!~_~ _ 1.1.2.2-Tetrachloroethane -... ---. ----- .... --... -- .. -......... - - - - - . ----.... ~ ... - . 1.1.2-Trichloroethane •••••• _____ ........................... _______ •• - ••••••• _0"-'-

1.1.2-Trichlorotrifluoroethane

1.1-0ichloroethane

NO 5000 . - .............. -.-.--.-

NO 5000 _.- ....... - .. -.-._--_ .. --------_.-NO 5000

5000

5000

5000 - ~ - - - ~ .... - - - - ..................... - - - .. - - - - - - - - .. .. ... ..

NO 5000 5000

Vppb .++ _ ••••• * •

Vppb -----_ ... _-_ .. -.-Vppb

01/27/12 . ..... - ..... 01127/12

01127/12

nicollez

nicollez

nicollez ... _----------- ... _--------------------_ ..

Vppb 01/27/12 nicollez __ ........ _ • _ _ ~. _ .. ___ ... _ • _ • _ • •• • ••••••• w __ •••••• ~ ............ ~ ................................... .

_~ ~~~~~~~~?_r_~~!~_~~~. __ ._. _. ___ . _______ . ____________ . ____ .. ________ . _. ________ . __ ~~ ______ ~_~~_~ __ .. ________________ ?_~~.~ ______ .'!~~_~ .. ___ . __ .~:!~?(:.~ ____ .. ~!~?I!~_~ __ . 1.2,4-Trichlorobenzene NO 5000 - .... _---_.-._---_. __ ...... _ ... _ ................ ----- .......... _--_._. 1.2,4-Trimethylbenzene NO 5000 ... -..... _--_ ................... _ ........... _---_.-. 1.2-Dibromoethane NO 5000 ...... _ ...... _ ..................... -................ _-------_ ... _ .... . ..... .... -......... _ .. __ .. . 1.2-Dichlorobenzene NO 5000 -_.- ... ---_ ... _ .. _ ............................. _._----_ ............. __ ._._ .. . 1.2-Dichloroethane NO 5000

5000

5000

5000

5000

5000

Vppb 01/27/12 nicollez . _._--------- ......... _-----_ .. _._-.-.

Vppb 01/27/12 nicollez --_._ .. - ... _ ......... _._ ... _._. __ ._--_ .. Vppb 01127/12 nicollez ._-_. __ .... _ ..................... _._ .......... . Vppb 01/27/12 nicollez

.. - . - - ---............ -. - ---- --_. - -- - - . -~ .. -Vppb 01/27/12 nicollez

_ ........... __ .................................. --_._--_.- ..... _. __ ... _-_ ... _ .... . •• n •• " .. ____ • ___ ••• ___ • _ •••• ____ • ___ • _ •• - _ • _ ~ ... __ •• - ••••• _____ • • • • •• • ••••• - - - - - - - - •• - - ..... - _ ....

1.2-Dichloropropane NO 5000 5000 Vppb 01/27/12 nicollez ............ _--_ ................. -..................... --_ ... -----_.- ..... _. __ .. . • • • • • •• • ............................ p ~ • p ... _ • + ___ ••• _ ........... 4 • • ••••••• _ ......... ____ .......... _ •••• _ ... _ ....... _ ....... _ ••

1.3.5-Trimethylbenzene NO 5000 5000 Vppb 01/27/12 nicollez .. _ .......... _ .... _ ......... -_ .............................. ------_ .. __ .... -_ .. __ ._---_ .. . ..... - . - ... - .. -......................... - .. -.... - -.. - .. - .. -. -....... - .. . ............... -.. - . - - .......... - ~ ....... ~ - ............... . 1.3-Dichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez

..... _ .. ---_ ........... _-.---------- ............ . 1,4-Dichlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez .............................. -.. _ ... _-_.- ........ -------------_._ ...... _-_. __ . __ ...... _ ...................... -.......... _ ................ _-_ .. - .. _-- ....... -...... - ......... -.-.- ................ _._ ................ . _~~~_t_~~!t .. ~~~~ .. ~~ ... _ . ____ . _ ... _ ..... __ . ________ .... _______ . __________ .. ___ . __ ._ ._ .. _~~_. _ .. _ ?_~~_~. ______________ .. _ .?_~~ .. ~ _______ \(~p_~ _______ .O!!~?~~_~ .. _ .. _~!~~I!~~ Benzene NO 5000 5000 Vppb 01/27/12 nicollez .- ... _ .. _ .............................. ,._ ... ,.. . .. _._--_ ........ _ .... _ .. _._ .... --- .. - .............. - ...... . Bromodichloromethane ------~~--.- --?~~-~ --. -_._. -- -_ .. -... _. ?-~~.~ - .. ---\(~p~---. -. --.~}!~?(~-~ -. _ .. ~~~?I!~~ - __ Bromoform NO 5000 5000 Vppb 01/27/12 nicollez

......... _- ... - ............. __ ... _ .................. _ ••..... _ .. _-.------_.-.+ .. - ... __ ... - ................. . Bromomethane NO 5000 5000 Vppb 01/27/12 nicollez ....... _ .... _ ............... - .. --_ ....................... -..... _-- .. - ................... _---.- ..... - ... _ ....... -....... _ ...... -.--_ ....................... _ .. _------_ ... _- .. -._ ......... --- ........... . Carbon Tetrachloride NO 5000 5000 Vppb 01/27/12 nicollez ...... -.................................. - ........... -..... - ... - ...... - ................. - .. ~ - .............. -........... -........... - . ..................... . - - --- ... -...... - - - ... - - . - - - ................. - .... - - .. - .. - .

Chlorobenzene NO 5000 5000 Vppb 01/27/12 nicollez ..... -..... -............ -..... -- ... -.............. - ............... - .. .. .. . - ... -. . . . . . . . . . . . . . - ............ -.. -. -............ - . . .. . ................. - - .. - - ... -- . -.. - ...... ~ ... ~ .... ~ ... - .. - . -... --- ....... .

Chlorodibromomethane NO 5000 5000 Vppb 01/27/12 nicollez

:¢~~~~~~~~~:~~~~~:~:~:~::::::: :::::: ::::~:::: ::.::: :-:::: ::: .. :::::::::::::':::: :::~~::::.: ~~~:~::: ::::: ::::::: :::~~:~~:~:::::: ::~?p:~:::: ::: ::~~!~?~~~: ::::~]~~I!~~.:: .<?-~~~~?!?-~~-------.- .. --- ...... -_. -._._._ ... -_ ... --_ ..... -.. _.- ----- -------- ------~~---- --~-~~-~ --_. -- _. -- --- ...... ?-~~.~-- _ .. ---.'!~~-~--- --- --~!!~?~:-~- -- -_~!~?I!~~- __ Chloromethane NO 5000 25000 Vppb 01/27/12 nicollez

:~~~:~ ;?:~~~~I~~~~(~~~~~::: ::::::::::::::: :::::: ::::::::: ::::~:~::::. -:::: .:::::~~::::::~~~~:~:::::::: :::::::: :::~:~~:~::::: :::~?~:~::::::: ::~~!~??~~:::::~~~~I!~~ ::: .~i.~~~!~~~i_~~!?!~~~??~_~~ .. _ . ___ . ________ .... __ .. _. ________________________ . _____ ~~. _____ ~.~~ .. ~. _ .. ____ . __ .... _ .... ?~~_~_. ___ . _ y?~.~ __ . __ ... _ .~}!~?~~_~ _____ ~!~?I!~_~. __ Dichlorodifluoromethane NO 5000 5000 Vppb 01/27/12 nicollez "6i:i-sopropy iether-(OiF)E)"'- ---- '-'-'--'-'''-'' --.- .. -... ------- ... ---- ---.. -- '"--NO----- -5'00-0' -.... -.. ---'-' .---- .. !{ooo ---.- '''V-pp'b -- -.. -'--61i27i12"-"'ni~~lie~ ---'Eth'yibe-~z~ne-'--"'--"--'" --------------- ---. ---- .. --. -.. -.. ------ -.-. --. -.. -. "NO"--" 5'00-0" .. ---- ------------s-oi)o·-· -----V-pp-b------ ·--01i27i12-- .... -nic~lie~· -.. "Eth-yi-te-rtb~iyieti'-~~'(ETBE-)""" ... -.... --'- -.. --- --. -- --------- ---- -- --- ---" NO-- --- ·5-00-0-······ - -' -- ------s-oi)o-' ---.. -V .. pp-b-· .. · --. 'o1i27i12- ---'ri[c~lie~ - -.~ -~~-d 'p~Xyie~e""" .-.- ... -------------------- -.-. --.. -- ------- ---- ---. --' ---"NO'-" '-5'00-0- --.... --- -- ----- -'--!50()O" -. -- --Vpp-b-- ----- -·01i27i12-----ni~~lie~· 'Meihylene-chic;rid-~---"-" -- -.. --. -- .. --. --- .... --.- -.. -. -- ..... -. -.. -... -- -------NO-- ----5-0C)0 -.- -... -.. -.- .... --. -!50cio-" ---- '"V·pp-b· .. ···· "o1i27i12- ---'~ic~lie~-

:~~~~Xl~!~~~~~~~!~~~~~:t~~~:::: ::::::::::::.::::::: :::::::::::: -: _ _ . ::::~~::::. :~:~?:~::::::::: :::::::::: ~:~?:~::: :::::~?~:~ ::: :::: ::~~!~??~~::: ::~!?~I!~~. __

.~~~~~~~.~ .. -' --... _._ .. _ ..... -- ---_ ... ---- ._-----. ---_. --. -._- ----- -- -_ ... ---_ .... _. ~~.- ---? .. ~?-~. ------. ----- -_ .. _ ... ?~~-~-- -- ----\(?~-~.- ....... ~!!~?~:~- .. __ ~!~~I!~~. __

.~~Y!~~~ __ . _. __ ... _. ____ .. __ ... __ _ _ _ ________ _ __ _ .. _ ......... _. ___ . __ .. __ .... _ ~~. ____ ?_~~_~ _ .. _________ '" __ .? .. ~~_~ ______ y?~_~ ... _. __ ... ~!!~?~:~ __ ... ~!~?I!ez

.t~~~_ty}_~_I?~~~IJI~~~~_ ........ ___ .. _____________ .. __ .. ___ " __ ....... ______ . __ . __ . __ .. __ ~~ _____ ?_~~_~_. _ .... _. _. _. _. ___ ~~ .. ~~.~ _____ . y?~_~ ___ . _ ... ~!!~?(:_~ .. __ ~!??I!~~_ Tert-amylmethylether (TAME) NO 5000 5000 Vppb 01/27/12 nicollez

!~(r~~~I~~~~:t~~~~:::::::::::' ::: :::::::::-:::::: -:::::: -:: :::::-:::::::. -: ::~~:~~§::::: ~:~~:~::. -:::. ::::::::::: ~~?:~::: _::: :~?p~:::::: -:~~!~??~~:-:: :~~?~I!~~. _ _ ~?I~~~~ ... __ ................. ____ .. ________ . __ ._ ... _. _. __ ... _. __ ..... __ . NO 5000 5000 Vppb 01/27/12 nicollez

_t~~_~~_-_1:.~~?!~~~~~?~~~~_~~ ... __ ..... ___________ . __ . __ ... ___________ .... ::: -:::: ::~~::::.: ~:~~:~ ..... --. -----:::::: :~:~~:~::::::. :~?~:~ ::::-::: :~~!~??j~:: :::~!?~I!~~: _: trans-1.3-dichloropropene ...... -- - - -... -- ... ~ -~ .. -- .................... - ............. - .. Trichloroethene

NO

NO 5000 _ _ _ . _. ?_~~_~ _. _ . _ .. '!?~?. _ _ _ _O~!~.?~~ .. ~ .. __ .~~~?I!~z -?-~~-~. -... ------ --- -----?-~~.~. -------\(?~-~- ---- --.~!/~?(:_~ --- .. ~!~?I!~~

_~~~~~~?_r~~I~~~?_~~~~.~~_~ .... ____ . _____________ ... ___ ..... ______ ... _____ . _ .. __ . ___ . ~~ __ . _ .. ?_~~~. __ . __ . ____________ ?_~~~_ .. _____ y~~? ______ .. ~:!~?~:_~ ____ .~!~?I~~~ Vinyl Chloride NO 5000 5000 Vppb 01/27/12 nicollez -Xy-(e~es '(T~tai)"'" -..... --.. ---------- ---- .. -. --.... -. ---. --' -.. -- .... -... --- -.. --NO- --- -i,.,ooo -. -. -. ------ ---- ---iioo'o .. --- --V-ppb -... -. --o1i27/12"- -- '~i~~li~~ -............ ~ ........... ~ ... ~ .... ~ ....... - . - .... - ........ -.................... - - . - -- - .......................................... - - .. - - - ......... - - - ........ - - - - - - ... - .............. - - - - ............... .

NO = Not Deteced or < RDL RDL = Reporting Detection Limit OF = Dilution Factor



Sample#: 298455-007

Matrix: Air




Client Sample #: System Effluent

Site:

Collector: Client

Compou nd _____ ...!..R~e~s:..=::u:..:..:lt~ __ D=_=___F _____ RD L Units Analysis Date An~..!yst QCBatchlD: QC1122815 Method: EPA 8260B Prep Method: Method ----------------

1,1,1-Trichloroethane NO 7

:~~~;~,~~~~~r~~~I~~~~t~~~~:':::::: ::::::::::.:::::::: :::: :::.':: ::::. ::::':::::~~::::.:: ::::~ :::: :: .. -... _~:! ~?_-!~i_~~!~!~~!~_~~_~ _ ........................................................ ~~ .......... ? .~: !~?.-!~i.~~!?!~t.r!~.~?!~:~~.~~~............................ ............... NO ..... ? ................... _ .. ? ..... . \(p-~~ .... _ ... . ~~!~~(~ ~ ..... ~!~?I!~~ .\~~~~~~}?~~~.t~~~: ............................................ _ .............. ~~ ..... ? ................... J... Vppb ..... ~:!~~!1.~ ..... ~!~?I!~~ .. . ~ :~~~~~~.I?r.~~.t~.:~: .. _ ......................................... __ ............... ~~ ......... ~ ....................... ~ ....... . \(p-~~ __ ... __ ._~!!~~(!.~ ..... ~!~?I!~~ .. .

.......... -~ ....... y~~.~ ......... ~~ !~~[].~ ..... ~ !~?I !~~ .. . 7 Vppb 01/28/12 nicollez

... - ... -_ .... _-----------------.-------------_. Vppb 01/28/12 nicollez ---_. __ .. _---_._-_ .... - ..... ----------_ ...... -... -.. _--. __ ..... -- .. -_.-7

7 Vppb 01/28/12 nicollez - - . - - - - .. - .... - - . - ....... --..... -...... - - - .. - - - - .. - - - --- - - .. - - ~ .. - - .. - - -- - - .

7 Vppb 01/28/12 nicollez . - - .. - _ .. - .. - - - _ .. - - . --~ ...

01/28/12 nicollez ._ ..... --- ................... -... -_ .. .

1,2-Dichlorobenzene NO 7 01/28/12 nicollez 4 ......... _ .......... _ ......... __ ...... __ • ~ ••••• 4 ........ - .. - - _ -. - .. - - - - - - - - ..... - .. - .. -. - • - - - ••• - .... - ... - ...... _.,

.~~~~~~~~.I?~~~~~.~~_: ___ ..................... __ ................... _ .............. ~~. . ...... _~....... . ... . ... _.? .... . y.~~~ .. ..... O~!~~!!.~ .... ~!~?I!~!: .. .

. ~ :~~~~~~.I?_~~p!~~~~~ ........................ _ .. __ ............................. ~~ ......... J ............... .. _ .... . X ... __ .. . ~P-~_~ .. _ .. __ .~~!~~!~.~ .... ~!~?I!~!: .. .

. ~~~:~:!~i_~~!~XI_~~_~~~~~_ ................. ___ ............... ,_ .................. ~~ ....... . J ..................... .. X ...... . Y.~~.~ ... .. _ ... ~~!~~(~.~ ..... ~1!~~1!~~ .. 1,3-Dichlorobenzene ND 7 7 Vppb 01/28/12 nicollez - ........ -............ -...... --.. -- ---- - .... -. - .. - .............. ~ ... - . -- - - --- - - - - . - .. - - . - ............ - .... - - .. - ... - .. -........ -. .. . ............... - .. - . - . - - ...... - .... . - - . - - - -- -- - - - - . - . - ........ - ... - - - - . - - .. - .... - ...... - .. 1,4-Dichlorobenzene NO 7 7 Vppb 01/28/12 n icollez - -- -- -_ .. -_ ...... - .. -...... -- -- ---- --- -- - - --_. - _ ................ " ......... -- _. - - _. -- - --. _ ........... - ...... _ .. -_ .. _ .. - _ ... _ .. _ ....... , ..... _. -..... - - .......................... _. -. - - -_. - -. - - - _ ..... -.. - ..... _ ...... _ .......... .

_~~~t_~~!~?~~~~~ .................... _ ............. __ ........... _ .............. ___ .~~ ......... _~ ...................... ? .... _ .. ~P-P.~ ......... ~~!~~!}.~ .... _~!??I!~.~ .. . Benzene NO 7 7 Vppb 01/28/12 nicolJez ......... -............. - - --- --- ----- -............................... - - . - --- - .. - - - - - ... - ---- ... '.. .... . - . - -- - ....... - - - ..... - - - .. - ...... - - . - ... - . - - - ". ~ ........ ,- ... - -................ ' .............. - . ~ .. ~ - - ..... - ..... - - . - . - -Bromodichloromethane NO 7 7 Vppb 01/28/12 nicollez

~ ........... __ • __ ._ .. ___ • ___ .... ______ ........................ 0 .~ __ ••• _ .... ______ • __ • _. _ .................. 0 ....... • .. - ... _ .... - ... - •• ___ .. _ ••• ~.- • ______ • -.- ••• ___ .. ___ •• ---. -.----- ... _ ... _. _ ... _. ~ ........... ~.

Bromoform NO 7 7 Vppb 01/28/12 nicollez .......... -........ ------- - .. - .... - -- ... _ .... - .. - ....... ~ ......................... - .... - - . - .. - . - ... - - . - . - . - --... -.............................. - . ...... .. . ......... ~. .. ................. - ..... ~ ........ -........... - . - . --- - . - .. - . - - .

Bromomethane NO 7 7 Vppb 01/28/12 nicollez ............................... -...... - .. - - .. - --. - -- ..... -- .. ---- - .... ~ ...... - ~ ........... , ..... - - .. - .. - - - . - . -- .. - . - --- .. ---- . - - - ..... - .. - .. - ................ - _. . .... ' - - ~ .. - .. - . ~ - - -.. ~ .. .. ... . - .................... - - - - - - .. - . - -- .. --- - - . - -Carbon Tetrachloride NO 7 7 Vppb 01/28/12 nicollez ------_ .. __ ................. -................ _--_ .... _-------.--------_.-_._ .. _ ....................... _._ ... _--_ .. -------_. __ .. _----_.---_._------_._-----------------_._ .. _--------------------- .. _----- .. Chlorobenzene NO 7 7 Vppb 01/28/12 nicollez

Chlorodibromomethane NO 7 7 Vppb 01/28/12 nicollez ............... __ ...... ___ ......... ____ .... ______ • ____________ • ____________ ....... _._. ____________ •• _. ____ •• __ • __ ._. ____ • __ .. _____ • __ • __ ._. __ • ____________________ • __ • _____________ ... _0 ................. .

. '?~~~:?~~~~.~~ __ .. _____ ......... _._ ....... ___ .............. _ ..................... ~~ ........ _.? _ ... _ .......... _ ..... ~.~ .... _._ YP-P.~._ ...... . ~!!~~~].~ ..... ~~~?I!~~ .. . -'?~I.~~~!?~~ _ .......................... _ .. __ ..... _ ........ __ .... __ ...... _ ........ _~~ .......... X_ .............. _ ....... ? .... Y?P.~ .......... ~!!~~~}.~ __ ... ~~~~I!~!: .. . . <?_~I_~:~_~.:~~~~~ ..... ____ ............ _ .................. ____ .... _. _ .......... __ .. ~~. _ ...... . _L ... _ .. ' .............. ~.~ ... .... y?p_~ ........ . ~!!~~~!.~ .. _ .. ~!~?I~~~ .. . . ~i.~:~ ~?~~!~~l?~?~.t~~~: __ ..... _. __ .............. __ ........... _ ... _ ........ __ ... ~~ ......... . L ...................... ? ....... YP-~.~ 01/28/12 nicollez

.~i.~:~~~.-~i.~~!?~?~~?_~~_~~ .......... _ ........ _ ................................... ~~ ....... __ .X ....... ................ ? ... _ . Y.~~.~. 01/28/12 nicollez

Dichlorodifluoromethane NO 7 7 Vppb 01/28/12 nicollez

:~~~~??~~P.~~~~~~~~~~~~~)::::::: :::::::::::::: :::::::::::: ::::::::::::::::: ::: :~~:: :::::: :::~::::::::: :::::: ::::: ::::~::::::: :Y?P~:::::::: :~~!~~?~~: ::::~~?~I~~~::' Ethylbenzene NO 7 7 Vppb 01/28/12 nicollez ·Eih·Yi-t~rtb~tYieit;er-(ETBE·)·················· .................. -............... No········ .. ·y-······ .... ········ .... ? ...... \i"ppb········ ·o1i28i1·2···· 'ni~oliez'" '~'~~'d 'p~Xyi~ne"-"'-"-" ............... -....................... -............ ·-NO·········· 7" ...... -............. ? ....... \ipp·b··· .. ··· 'o1i28i12'" "n;~oliez'"

·M~ihyl~~~·~h·I~·rid·~·· ...... -.. ···-····--·-· .. ·· ............... -- .......... ····NO······ ··7··········· ............. 7" · .. ·· .. 'ippb·· .... ···01i28i12···· 'nlcoliez"

:~~~~Xl~!~~:~~~( ~!~~~~(~:~~~~::: ::::: ::::: .:::::::.: :::::::: :::::: :::::: :::::: :~~:::""'. ::~:::::'::::'::.::-""" 7'::'.:: :y~~~::'::::: :~~!~~?~~:::: :~!?~I!~~ .. a-Xylene ND 7 7 Vppb 01/28/12 nicollez

• _ 8 _ H ~ .... __ • __ • _ • ________ • _ • 4 •• __ .. __ ...... _ ...... ~ ••• _ ~ ........ _ •• ___ • __ .. __ • __ •••••

Styrene ND 7 7 Vppb 01/28/12 nicollez

:t~~~~y):~!~~~~(~~~): :::: ::::: :::: ::::::::::::::::: -: .::::::: :::: ::::::: :::::::~~:::: ::: :::!: .:::.:::':: .':. :-:::~~:. -'.: .:Y~~~::.::: :::~~!~$~~~.:: ::~!~~l!~:~' . . ~~~~~~¥!~~.t.~~~:!~_~~ .(.~ ~~~L ............................................. __ ~~ ........... ~......... .. . . . . 7 Vppb

... - . - . - ------ -- . - . - - - - . - -- - ..... , . ~ ..... - .... -01/28/12 nicollez

Tetrachloroethene NO 7 7 Vppb 01/28/12 nicollez ...... - .. - ~ -- .. _. . ... - - - . - - - . - ..... " . - .... - . - . ~ ....

Toluene 14.0 7 7 Vppb 01/28/12 nicollez

:t!~~~:-:1)~~}~~(~~?~~~~:~~::::::: :::::::: :::::::::::::::. :::::::.:'::':. :::::::::~~:::.::: '::!-::::::::.':.:.: ....... ~ ... : ::y~~~:::::: :::~~!~~~~:~::. ::~!~~I!~~':: .t!~.~~.-_1.'.~~~!?~I_~~~p-~~P.~~~ .............................. _ .................... __ ~~ .......... !.. ...... ............ ? ..... Y~P~ ......... ~1(~~~~.~ ..... ~!~?I!~~ .. . . ~~~~~.I?~~~.t~~~.~ .. __ ._ .... ___ ..... _ ........................................... _~~ .......... !. __ . __ .. ..... 7 Vppb 01/28/12 nicollez Trichlorofluaromethane NO 7 ......... . j .... '" ·Vppb··· .. ··· ·o1i2Si1-i···· 'nic~I'lez" Vinyl-ct;l~'ri~i~"--"'--"'--"""'" ... -..................................... -. -NO···· .. ··· --7· .... ···· -., ···········7······· ·V·ppb··· .. ··· ·01·/28i1-i···· 'nic~liez'"

~y~I~~~~:(t~t:~~:::::::::::::::::::::::::: :::::::::::::.::::::: :::::::::::: ::: ::::~~:: :::::::::~::::::.:'::: ... :::::: ::!.::::': :Y?~~::::: ::: :~~!~~!~.~:::: :0~?~1!~~.:. ND = Not Deteced or < RDL RDL = Reporting Detection Limit OF = Dilution Factor



ASSOCIATED LABORATORIES QC SUMMARY FOR LAB REQUEST 298455

QCBatchlD: QC1122815 Created By: nicollez Method: EPA 8260B

Matrix: Air Created Date: 01/27/12 Instrument VOA-MS (group)

1.1-Dichloroethane ND Vppb .. - .. .. .. .. .. .. - .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. . .. .. .. .. .. .. .. .. . .. .. .. .. .. .. .. .. .. .. . ~ .. .. .. .. .. .. .. .. .. .. .. .. .. . . .. .. .. .. .. .. .. .. . .. .. .. .. .. .. .. .. .. .

1.1-Dichloroethene N D Vppb : 1.2.4-T~i~hio-robenzen~ - - - - - - - - - - - - - - - - - - - - . NO - - - - - - .. - . - - - - - - - -Vppb - - - - - . - . - - .. - - - . - - - - - - - - - - - -. - - - - ......... - . _. _ ... - .... - - ... - - ..... - - . - - ........ - .. _ ..... - .... _ ..... -. - ... _. _. - - ..

I ~ ,~.~-:r~im~t~~I~e_n~e.n~ _ 580 560 Vppb 3.5

t 1,2-Dibromoethane ND __ Y?pb

~ .~-~~c~l~r.o?~n~~n.e. _ _ ND Vppb 1.2-Dichloroethane ND Vppb

.. .... . ..................... ..

1.2-Dichloropropane ND Vppb ........................................ 1.3,5-Trimethylbenzene 280 270 Vppb 3.6 .............................................................................................................................................................................. " .. 1,3-Dichlorobenzene ND Vppb ................................................................................................................................................................................... 1,4-Dichlorobenzene ND Vppb

....................

4-Ethyltoluene 700 680 Vppb ....................... Benzene 170 160 Vppb ........................... Bromodichloromethane NO Vppb Bromofon1l ND Vppb Bromomethane ND Vppb .............................. - . - - - - . Carbon Tetrachloride ND Vppb Chlorobenzene ND Vppb Chlorodibromomethane ND . - . - .... - - - - - - - - ........ _ .. - .. - - - ... Chloroethane ND

Chloroform ND

Vppb

Vppb

Vppb . - ........... - - ... - _ .... - . Chloromethane ND Vppb

- - .. _ .... - - - - . - ....... - - ...... - .......... - - ... - .. - . cis-1.2-Dichloroethene ND Vppb cis-1.3-dichloropropene ND Vppb

2.9

6.1 0-20

- .............................. - ........... - .... - .. _ .. - - - .......... - - - - ............... - - .. - ........ - - - - ..... - ....... - ...... _ .. - ........ - ....... - .. -

!?i9~I~r~~if~u?~o:n.e~h~~e .... ___ .. _ . _ .. _ . _ .... ~~ .... ___ .......... y?~~ __ . ___ . _ ..... __ ... _ ... ____ ... __ Ethylbenzene 230 220 Vppb 4.4 0-20 o ~a~~ ~-~~I~~e~ : : : : : : : ~ : : : - .. - - .... - - : : ~?~O~ ~ . -. -. -2600- - . : : ~ :V?~~ : -. ------3.8' .. - - ....... '0:2'0' . - . -

~~t~~I~n~ _c~l?r!d_e .. _ . __ .... ____ ..... _ ND . __ ... _____ Y?~~ _ L ~~t~~I-~-?~t~1 .E!h.e~ <,M.T~~~ _ . . . . . _ . _ ... ~~ _ _ _ . _ . ~~ __ .. _ . Y?~~ . ! o-Xylene 1200 1200 Vppb

t ~Z;~~~IDr~ettien~ • • • • . • • • • • . . . . • • . . • • • ~~ • . . • . . • • 570 . • • . • • .~:~~ • ~ ~~I~e~~ : : : : : : : : : : : : : : : : : : : : - - - - . - : : : : 1:6~ : : - - - : : ~ : 1~6~: - - . - . 'Vppb' _. - - . - - 0.0

! trans-1.2-dichloroethene ND _ .. _ . _ .. __ .. y?~~

f ~~:~;~;~~~t:;OP;Dpe~e • ~~ NO <:~~ ....... 0.0

I t,:~t~~~~:·melhane : : : • : • : . : : : : • : •...••• ~~ •• • . • • • • • • ..•.••• ;:: .• : : : • : : •

0.0 0-20

0.0 0-20

3.4

0-20

NO = Not Deteced or < RDL MOL = Method Detection Limit RDL = Reporting Detection Limit OF = Dilution Factor




QCBatchlD: QC1122815

Matrix: Air

I Xylenes (Total)

I QCLabID: QC1122815MB1

, Analysis Date: 01/27/12 i

Created By: nicollez

Created Date: 01/27/12

3900

Method: EPA 8260B

Instrument VOA-MS (group)

3800 Vppb 2.6

BLANK SUMMARY

Blank J . _________ A_n_a~ly~te _______________ ~ ______ ._R_e_su_l_ts~----.J-----U--ni-ts ___ .. __________ __

All Analytes are NO

NO = Not Deteced or < RDL MDL = Method Dotection Limit RDL = Reporting Detection Limit OF = Dilution Factor



.'/ .;':\ .. /L ___ _

ASSOCIATED LABORATORIES ~ 806 North &:rtavia • Orange. CA 92868 Phone: (714) 771·6900 • Fax: (714) 538·1209

CUSTOMER INFORMATION

COMPANY ~'oG~ ~\I\,..o~oA SEND REPORl TO: £ r-;~ fio tk..

Chain of Custody Record

PROJECT INFORMATION

PROJECT NAME:h'/JIJ~'&} V;//Wf?-; frJ,u1 NUMBER: :3 0 ---3:S~ _0.3 if \I

Lab Job No.

Page /

REQUIRED TURN AROUND TIME: Standard: Xl'\fJ 72 Hours: 48 Hours: 24 Hours: ~

-

EMAIL: ~b J:..-oJ b/o"k..cu1v :('O~ ~\ ..{"~tI\ ADDRESS: d'_'fJ!l~_C~~. JtI ADDRESS: 1.; M. v1 rdL, ~ (00 r;ntltb t:rl ~ l'>

:C.t"\tjl\.Jt I VA qt,brB p.o.#: r.I

~~~ PHONE: q1CJ- </ ~r -- D}l'S'" SAMPLED BY: ~J}loJc-_

~ ~ lJ" Sample 10 Date Time Matrix Container Pres.

~ 0 Number/Size ~

Test Instructions & Comments 1 ~lSW.J3-5 j-;;'b -/2 I(:L{~ lhJb.", / -reP//~ Xli 2 \Jt,\JJ-3---o (l:~ I )tJ 3 \jew .. 1- s .2;~~ I '101 4 V~w---I---- D J:sl J ~ 5 V~-J-S '(:2"-' ~ 6 V~\N--:l"" D 3 :2--> .. ~ 7 s~~ £R::hJ«"Q- '(:"5 1'lJ 8 ~

,

9

10

11

12

13

11\

15

Total No. of Sam~les: .7 Method of Shipment: 1)(0 ~ ~ Preservative: 1 = Ice 2 =HCI 3 =HN0:3 4 =~S04 5 =NaOH 6 =Other Relinquished by ~ 1. Recelve~ 1. Relinquished by 2. Received By: 2. Relinquished by 3. Received By:

r.=.~~ ---- .. Signature: AT Signature:

t' ... - Signature: Signature: Signature: Signature:

n Printed Namd, t,l" S 'la=> ~ printedName:~"l ~,.. ~rinted Name: Printed Name: Printed Name: Printed Name:

1-"

Date: {6. Time:!'"'_(O D(~ t 6'-'(2-- Ti/),)O Date: Time: Date: -z- -rb ~."

Time: Date: Time: Date: Time:

I

Dlstrlbullon: White· Laboratory Canary - laboratory Pink - Project/Account Manager Goldenrod· Sampler/Originator

3.

ASSOCIATED LABORATORIES 806 North Batavia - Orange, California 92868 - 714-771-6900 FAX 714-538-1209

SAMPLE ACCEPTANCE CHECKLIST

Section 1 ,....... Client: B I vcl b::'l \//0./ (ii-y-"e_""'-~4 I Project: ___________ _

Date Received: \ I 2&11 2 Sample(s) received in cooler: Yes Ship ing Intonnation:

Section 2

. Sampler's Nam.e: ' @ @(Skip Section 2)

No

Was the cooler packed with: Ice Ice Packs _ Bubble Wrap _ Styrofoam __ Paper __ None Other ________ _

Cooler or box temperature: ___________ _

(Acceptance range is 2 to 6 Deg. C.)

Section 3 Was a COC received? Is it properly completed? (IDs, sampling date and time, signature, test) Were custody seals present? If Yes - were they intact? Were all samples sealed in plastic bags? Did all samples arrive intact? If no, indicate below. Did all bottle labels agree with COC? (ill, dates and times) Were correct containers used for the tests required? Was a sufficient amount of sample sent for tests indicated? Was there headspace in VOA vials? \Vere the containers label ed with COITect preservati ves? Was total residual chlorine measured (Fish Bioassay satnples only)? * *: If the answer is no, please infom1 Fish Bioassay Dept. ilnmediately.

I Section 4· Explanations/Comments

Section 5 'Vas Project Manager notified of discrepancies: YIN N/A

Completed By: Date: t /2/;:;( /.?

YES NO v \.,/

V-

v v v if

V

N/A

"\/

V

V V

Client: Address:

Attn:

Associated Laboratories 806 N. Batavia - Orange, CA 92868 Tel (714)771-6900 Fax (714)538-1209 www.associatedlabs.com [email protected]

Block Environmental 23 Musick Suite #100 Irvine, CA 92618 Erik Block

Comments: #30-319-03, Filmaker's Village 204 N. Cypress St., Orange, CA

~~ \ \"' ~: GOt:ro-9"

{hel~tc\ Lab Req uest: 298544 Report Date: 02/07/2012 Date Received: 01/27/2012

Client 10: 12211

This laboratory request covers the following listed samples which were analyzed for the parameters indicated on the attached Analytical Result Report. All analyses were conducted using the appropriate methods indicated on the attached report and all NELAC criteria. This cover letter is an integral part of the final report.

Sample #

298544-001

Client Sample ID

CARB-1

Thank you for the opportunity to be of service to your company. Please feel free to call if there are any questions regarding this report or if we can be of further service.

NOTE: Unless notified in writing, all samples will be discarded by appropriate disposal protocol 45 days from date reported.

The reports of the Associated Laboratories are confidential property of our clients and may not be reproduced or used for publication in part or in full without our written permission. This is for the mutual protection of the public, our clients, and ourselves.

Page 1 of 3

TESTING & CONSUL TlNG

Chemical

Microbiological

Environmental

Sample #: 298544-001

Matrix: Solid


Collect Time:

Client:

Client Sample #:

Site:

Collector:

~~rnp=o~u~n=d~ ________________ _ Method: EPA 8260B

Carbon Disulfide

1,1-Dichloroethene

1,2-Dichloroethane

1 A-Dichlorobenzene

Benzene

Carbon Tetrachloride

Chlorobenzene +-+-++--+++ -+ -- - ----+++ -

Chloroform

2-Butanone (MEK)

Tetrachloroethene ------+-+-- -++--

Trichloroethene

Vinyl Chloride

1,1-Dichloropropene

1,2,3-Trichlorobenzene

1,2,3-Trichloropropane

1,2,4-Trichlorobenzene

1,2,4-Trimethylbenzene --+.+++ - ••• -++++-------------

1,2-Dibromo-3-chloropropane ++++

1,2-Dibromoethane

1,2-Dichlorobenzene

1,1,1,2-Tetrachloroethane

1,1, i-Trichloroethane

1,1,2,2-Tetrachloroethane

1,1.2-Trichloroethane

1,1,2-Trichlorotrifluoroethane

1.1-Dichloroethane

1.2-Dichloropropane

1.3,5-Trimethylbenzene

1.3-Dichlorobenzene -+----------- -------1.3-Dichloropropane

2-Chloroethyl Vinyl Ether -++-++---+-+

2-Chlorotoluene

4-Chlorotoluene -- - +-- -+-

4-lsopropyltoluene ---+-- -- ----. -

4-Methyl-2-pentanone (MIBK)

Acetone

Allyl Chloride ._.----+-

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Bromomethane - +-+--+---

2,2-Dichloropropane

Chlorodibromomethane

Chloroethane

Chloromethane

cis-1,2-Dichloroethene ------ - -+++--

cis-1,3-dichloropropene

NO = Not Oeteced or < RDL

Block Environmental

CARB-1

Client

Result OF Prep Method: 1311/5030

NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO

ROL J.Jl1itsAnalysis DateAn~_lyst QCBatchlD: QC1123021

5

5

5

5

5

5

5

5

100

5

5

5 --5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

100

5

5

5

5

5

5

5

5

5

5

5

5

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L -+-+--

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp - .---+-02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp -++-

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp -- -

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp --+-+--

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp --

02/02/12 ryanp

02/02/12 ryanp - - --+-

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp - - .. --

02/02/12 ryanp

02/02/12 ryanp ----- -

02/02/12 ryanp

02/02/12 ryanp -++-

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp -- -+---

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp ---+-+

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

02/02/12 ryanp

RDL = Reporting Detection Limit OF = Dilution Factor

ASSOCIA TED LABORATORIES Analytical Results Report

Lab Request 298544 Page 2 of 3 i\


Matrix: Solid Client Sample #: CARB-1

Collect Date: 01/27/12 Site:

Collect Time: Collector: Client

Result OF ~ompound ROL NO cis-1,4-dichloro-2-butene 5

NO Dibromomethane 5

NO Dichlorodifluoromethane 5

NO Ethylbenzene 5 --

NO Hexachlorobutadiene 5

NO Isopropylbenzene 5

NO m and p-Xylene 5

NO Methyl-t-butyl Ether (MTBE) 5

NO Methylene chloride 5

NO N-butylbenzene 5

NO N-propylbenzene 5

NO Naphthalene 5

NO o-Xylene 5 - ....

NO Sec-butylbenzene 5

NO Styrene 5

NO Tert-butylbenzene 5

NO Toluene 5

NO trans-1,2-dichloroethene 5

NO trans-1,3-dichloropropene 5

NO trans-1,4-dichloro-2-butene 5

NO Trichlorofluoromethane 5

NO Xylenes (Total) 5 -- ----

Surrogates for Method EPA 8260B By Prep Method1311/5030

Analytes

1,2-Dichloroethane-d4 (SUR)

4-Bromofluorobenzene (SUR)

Dibromodifluoromethane (SUR)

Toluene-d8 (SUR)

ND = Not Deteced or < RDL

ASSOCIA TED LAB ORA TORIES

Percent Recove!y Control Limits

110 70-145

103 70-145

100 70-145

103 70-145

RDL = Reporting Detection Limit

Analytical Results Report


LJni~Analy~is Date Analy§t ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp -+++--

ug/L 02/02/12 ryanp

ug/L 02102112 ryanp •••• +-

ug/L 02/02/12 ryanp ++---+

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

ug/L 02/02/12 ryanp

l

_J

OF = Dilution Factor

QCBatchlD: QC1123021

Matrix: Solid


Created By: ryanp

Created Date: 02/03/12

Method: EPA 8260B

Instrument VOA-MS (group)

Matrix Spike/Matrix Spike Duplicate Summary

QCLablD QC1123021MS1. QC1123021MSD1 Source Sam pie #: 298710-004 Analysis Date:

Analyte

1.1-Dichloroethene

Benzene

Chlorobenzene

Methyl-t-butyl Ether (MTBE)

Toluene

Trichloroethene

QCLabID: QC1123021LCS1

1.1-Dichloroethene

Benzene

Analyte

Chlorobenzene

Methyl-t-butyl Ether (MTBE)

Toluene

Trichloroethene

I

Samplei

Amount

24

ND

ND

ND

ND

40

Spike Amount

MS MSD -

50 50

50 50

50 50

50 50

50 50

50 50

Spike Result

MS MSD

76 75

49 48

51 51

57 57

50 48

86 82

% Recoveries

Units %MS %MSD RPD

ug/L 104 102 1.9

ug/L 98 96 2.1

ug/L 102 102 0.0

ug/L 114 114 0.0

ug/L 100 96 4.1

ug/L 92 84 9.1 -----

Lab Control Spike/ Lab Control Spike Duplicate Summary

-----

Analysis Date: ----

Spike Amount Spike Result % Recoveries

LCS LCSD LCS LCSD Units %LCS %LCSD RPD

50 49 ug/L 98

50 48 ug/L 96

50 49 ug/L 98

50 53 ug/L 106

50 47 ug/L 94

50 45 ug/L 90

02/03/12

Acceptance Criteria

%Rec %RPD

59-172 0-22

62-137 0-24

60-133 0-24

62-137 0-21

59-139 0-21

66-142 0-21

02/03/12

Acceptance Criteria

%Rec %RPD

59-172

62-137

60-133

62-137

59-139

66-142 - - - - - - - - - - - -- - - - - - - - - - - - - - ~ - - - - - -- -- - - - - - - - - -

QCLabID: QC1123021 MB1 BLANK SUMMARY Analysis Date: 02/03/12

Analyte

Blank

Results Units 1_ All Analytes are ND

NO = Not Deteced or < RDL MOL = Method Detection Limit RDL = Reporting Detection Limit OF = Dilution Factor

ASSOCIA TED LABORA TORIES Analytical Results Report -- ---


.. ~. ,c \

Dale: ' / ?.-3·/1 2-

Page -.Lot L BLOCK ENVIRONMENTAL .., 3 Vlv5>IIY~JJ. £9£65 Soulh "IMe OlIVa, Suil816tl-""':;:'" v ..J b r_" C:o(;:) CHAIN OF CUSTODY RECORD Lagb"Ci Adls, CalifOrnia §26SJ=- -L..( v I I V"r""'I -l1J, It:, TEL (949) 45!;-0325 • FAX (949) 455-1958

Project Number: "30- ~I ~ - 0 3 Project Manager: ~ . 01 c>~1e.-- ANALYSES

£~~~~~ Project Name: 'f; \ - _ .... Ik.,r, \}.~ Sampler!s) : E. (2,1.., ,,,L..- #. ~ 0" ,.,. '#'0 v:; Slle Address: '2-& --I ii_ C{}!,-"SS , ~~<&o+~ ~"~~v.

C.SSO: ~ ..k(? $' ~ 6~~,p ~ ~~~ " Q~c.".t:- ( A LaboralOrl! ; It-~OoQ ~0~"t- <t (p<S> , ~~ .~~ ,#0 ~ '#-~ '<If. ~. . ~~~'V~#~~~ ~ ~0~~U ~/' ~ Sample Cl Sample Identification Date Time Type

No. of oJ/~ ~~#~a~:#.V~ , No. U Field Point Name ConlainersfType Notes

CAR..8.- J I II '2i' I I"z. c.~.l '3. """SA. A . < 'L

-

~~~re) ~\~\ ~1L );iV~ :r;;raIUre) Date Tore Instructions to Laboratory:

\~ . 1-?7- 2 J~ e-

o 2 I Relinquished by: (Signature) Date Time Received ~ (Signature) Dale Tore

Global 10 #:

Relinquished by: (Signature) Date Time Received by: (Signature) Date T ..... Method' 01 Shipment: ReqU~ed Turnaround: \l.~.", ~"l) D b. '--\, \i '->/1-- 't>~~~

ASSOCIA TED LABORATORIES 806 N orth Batavia - Orange, California 92868 - 714-771-6900 FAX 714-538-1209

SAMPLE ACCEPTANCE CHECKLIST

Section 1 Client: (3[vc.1:. E"v,~"'rr-c"-+QI I Date Received: U'l7(1Z-

Proj ect:---:---:-:::-_----:=-o::-_---=-=--_ _ _ Sampler's Name: ® No

<§)Skip Section 2) Sample(s) received in cooler: Yes Ship ing lnfonnation:

Section 2 Was the cooler packed with: Ice Ice Packs _ Bubble Wrap _ Styrofoam

_ _ Paper __ None ather ___ _____ _ Cooler or box temperature: __________ _

(Acceptance range is 2 to 6 Deg. C.)

Section 3 YES NO Was a cac received? · f

Is it properly completed? (IDs, sampling date and time, signature, test) ./ Were custody seals present? / If Yes - were they intact? Were all samples sealed in plastic bags? \/

Did all samples arrive intact? Ifno, indicate below. J Did all bottle labels agree with COC? (ID, dates and times) V'

Were correct containers used for the tests required? v Was a sufficient amount of sample sent for tests indicated? ,/

Was there headspace in VOA vials? \Vere the containers labeled wi th C01Tt~ct preservatives? Was total residual chlorine measured (Fish Bioassay samples only)? * * . .. If the answer IS no, please mforrn Fish BIOassay Dept. ImmedIately.

Explanations/Comments I Stttion 4

Section 5 Was Project Manager notified of discrepancies: YIN NIA

r/J ' Completed By: r;/~ ~ Date: \ ( ,}7/1 z.

-----------

N/A

, .....

V v V

APPENDIX D

100 ~~-

:IE 10 :0 :0

r-- ' ~ 6 N

C J: --

1---'

W • ~ • jj 1 w ~ <J) m 0

0.1

I---

0.Q1 --+--, , a

obs. Well

VEW-1. VEW-2. VEW-3.

Obs. Wen

VEW-1. VEW-2a VEW-3a

Obs. Well

VEW-1a VEW-2a VEW-3.

c-

' ..... ,

_L--.

. t-

FILMMAKER'S VILLAGE PROJECT VAPOR EXTRACTION TEST

January 26, 2012

OBSERVED VACUUM vs DISTANCE

--- I -

- r---- -- -

~

'~ c-- ~ ,.-

- ,-- - - " - I- -

-, , ~'

,

-

"-- - ~

r--~

~ , , I I , --+-

10 20 30 40 50 DISTANCE TO EXTRACTIoN WELL

(feel)

Extraction Well = VEW·1 a

Flow Distance Obs Vac Rate

(feet) (In H2O) (SCFM) 0 122.4 36 32 0.045 63 0.02


(feet) (In H2O) (SCFM) a 85 21

32 0.05 63 0.01

Flow DIstance Obs Vac Rate

(feet) (In H2O) (SCFM) a 51 14.4 32 0.02 63 a

-

.. H ,

60 70

100

:!; 10 ::J ::J 0 « > -02 ~ J:

'" . • 1 w ii ., g m

0

0.1

0.01

~

"'-" --

'~


January 26, 2012


,- -

-

- .

- !- --f-- 1- .... ~~-

~ --

-~

" - r- ----"., -

-I

1 cf I !

, , I , I , I , -0 10 20 30 40

DISTANCE TO EXTRACTION WELL (feet)

Extraction Well = VEW-1 b

Flow Obs. Distance Obs Vac Rate Well (feot) (In H2O) (SCFM)

V8N-1 0 136 1. V8N-2 32 0.04 VEW-3 63 0.02

Flow Obs. Distance Obs Vae Rato Well (feot) (In H20) (SCFM)

V8N-1 0 112.2 6.6 V8N-2 32 0.03 VEW-3 63 0.01

Flow Obs. Distance Obs Vae Rate Well (foot) (In H2O) (SCFM)

VEW-1 0 85 5.3 VEW-2 32 0.02 VEW-3 63 0.01

-I

-

--r-

-, I -

-r-- -== .-

- --~

--+- -

" I

-1--.. 1 , ~ ! , ' ll , ,

50 60 70

100

:E 10 :::> :::> 0 .. > -02 W J:

ii; ~ 1 W 1j In §.

'" 0

0.1

0.01

.. '-- ' -

~

-- -


January 26, 2012


T ~

-_._.-

" , -r-

-

---

---- --- ---",

-

- - -f-.~

~ ... ,

• r- -~-

- - - -- -.- - .- - ~ I

,~ t .I-o-+-+- ,- --t '~I--' .. , ·I--+---+--I---'t---I

0 10 20 30 40 50 60 DISTANCE TO EXTRACTION WELL

(feel)

Extraction Well = VEW-2a

Flow Obs. Distance Obs Vac Rate Well (feet) (In H2O) (SCFM)

VEW-2a 0 136 80.5 VEW-1a 32 0,08 VEW-3a 70 0.02


VEW-2a 0 75 38.4 VEW-1a 32 0.045 VEW~3a 70 0


VEW-2a 0 47.6 22.5 VEW-1a 32 0.02 VEW-3a 70 0

-

- L- -

r--- -

-

- - --I

-

- --

70 80

100 t I

f-

~

f-

0_1 I

~ 0_01 , T

0 10

Obs_ Well

VEW-2b VEW-lb VEW-3b

Obs. Well


Obs_ Well



January 26, 2012


,

, , ,

-- ~

-

II

" -

, - --

, , , -I , , ~ ~ , , , >--

20 30 40 50

DISTANCE TO EXTRACTION WELL (feet)

Extraction Well = VEW-2b


(foot) (In H20) (SCFM) 0 136 33 32 0_2 70 0-07


(foot) (In H2O) (SCFM) 0 122.4 27_7 32 0_16 70 0_05


(foot) (In H20) (SCFM) 0 102 18.8

32 0_11 70 0_03

-

-

--

- --T =-C-,-

- --+-1---t--4--~-=1 60 70 80

-

100 •

"

-, , ~ 10 ::J ::J 0

~ 6 c N

~ r . • 1 w ;;

'" g In 0

0.1

+

0.01 , , I , , 0 10

Obs. Well

VEW-3a VEW-1a VEW~2a

Obs. Woll

VEW-3a VEW-1a VEW-2a

Obs. Well

VEW-Ja VEW-1a VEW-2a

-


January 26, 2012


r I I I

t-

I I

~ - -

-

t .. - -

f-- '" ,----I ,

" . -

, ~ -I I ~ 1 1 1 j 1 C 1

20 30 40 SO DISTANCE TO EXTRACTION WELL

(feet)

Extraction Well = VEW-3a

Flow Distance Obs Vac Rato

(foot) (In H2O) (SCFM) 0 115.6 51 63 0.01 70 0.05


(foot) (In H20) (SCFM) 0 85 34.4

63 0.01 70 0.04

Flaw Distance Obs Vac Rate

(foot) (In H2O) (SCFM) 0 51 20.6

63 0.01 70 0.015

- r- ==; -

.. -

- -

-

.-

)--=-0...--- , • ~ ... 1 L,*C-4~)-1

60 70 80

100

:E 10 ::> ::> 0 .. > -02 !:! I

'" • • 1 w £ rn :§.

"' 0

0.1

0.01

r >If--L

FILMMAKER'S VI LLAGE PROJECT V APOR EXTRACTION TEST

January 26, 20 12


I - ,----

I ~ -

~

- :::::::-, -

---

-~

f- ~-

'"" c- - --

C--._- > ---f--- -

, - -

-~ - I- --p.. -

I

-.

-r--- -- ~ r- • - ----""-

I-- - I- - c-f-+ ,-+-+-I-+-->

-x ,- '---l~ ->-- ,- I ,-f-' -;---+--1" -w-t.1---l I

0 10 20 30 40 50 60 70 DISTANCE TO EXTRACTION WEll

(feet)

Extraction Well = VEW-3b


VEW-3b 0 115.6 50 VEW-lb 63 0.06 VEW-2 b 70 0.05

Flow Obs. Distance Obs Vac Rat. Well (feet) (In H2O) (SCFM)

VEW-3a 0 78.2 25.4 VEW-1a 63 0.03 VEW-2a 70 0.045


VEW-3b 0 51 11.3 VEW-lb 63 0.01 VEW-2b 70 0.015

----

--

-

--

-

-

I

80

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