analytical summary report

April 13, 2021

APPL Inc908 N Temperance Ave.Clovis CA, 93611-8606

Work Order: B21032068 Quote ID: 5675

Project Name: Not Indicated

Energy Laboratories Inc Billings MT received the following 2 samples from APPL Inc on 3/29/2021 for analysis.

Lab ID Client Sample ID Collect Date Received Date Matrix Test

B21032068-001 BA29552 ERH1294 03/24/21 12:15 03/29/2021 Drinking Water DRO-Liquid-Liquid Extraction SW3520CDiesel Range Organics SW8015C

B21032068-002 BA29553 ERH1295 03/24/21 12:55 03/29/2021 Drinking Water Same As Above

The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. Any issues encountered during sample receipt are documented in the Work Order Receipt Checklist.

The results as reported relate only to the item(s) submitted for testing. This report shall be used or copied only in its entirety. Energy Laboratories, Inc. is not responsible for the consequences arising from the use of a partial report.

If you have any questions regarding these test results, please contact your Project Manager.

Report Approved By:

ANALYTICAL SUMMARY REPORT

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CLIENT: APPL Inc

Project: Not Indicated Report Date: 4/13/2021

Work Order: B21032068 CASE NARRATIVEGeneral Comments:

For any question please contact your Project Manage at (406) 252-6325 or [email protected].

All analyses have been performed in accordance with DOD QSM Version 5.3 unless otherwise noted below. The specific methodologies used in obtaining the enclosed analytical results are indicated on the Analytical Summary Report and the Laboratory Analytical Report. The samples were received at the appropriate temperature and in accordance with the chain of custody unless otherwise noted in the Work Order Receipt Checklist.

The tests listed below are accredited and meet the requirements of DoD QSM Version 5.3 as verified by ANSI-ASQ National Accreditation Board (ANAB) certificate number ADE-2588. Exceptions to this require client authorization and records documenting this approval are attached in the Sample Management Records. Accreditation may not be offered or required for all methods and analytes reported in this package. Refer to the certificate and scope of accreditation located at https://www.energylab.com/whyus/certifications-quality-control/ or contact your project manager.

Project specific matrix quality control samples may not be reported if site specific samples were not submitted. Matrix quality control samples were performed on project samples where adequate volume was available. All quality control measures met criteria unless otherwise noted in the Analytical QC Exceptions report and in the Analysis Specific Comments below. Where available, sample management records are attached.

The Level IV Validation Package includes data reports for all analyses associated with the instrument calibration, quality control (QC) sample analysis, and sample analysis. All analytical data is within method specifications except as noted in the Analytical QC Exceptions report or the Analysis Specific Comments below. The analytical report identifies preparation batch and analytical run IDs associated with each result for a sample. Only the raw data associated with the parameters listed on this report should be validated.

Analysis Specific Comments:

An Analytical QC Exceptions Report has been attached, summarizing all qualified QC results. All quality control measures met criteria; therefore there were no analytical QC exceptions on this report.

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Work Order Receipt Checklist

APPL Inc B21032068

Shipping container/cooler in good condition?

Custody seals intact on all shipping container(s)/cooler(s)?

Custody seals intact on all sample bottles?

Chain of custody present?

Chain of custody signed when relinquished and received?

Chain of custody agrees with sample labels?

Samples in proper container/bottle?

Sample containers intact?

Sufficient sample volume for indicated test?

All samples received within holding time?(Exclude analyses that are considered field parameterssuch as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)

Container/Temp Blank temperature:

Water - VOA vials have zero headspace?

Water - pH acceptable upon receipt?

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

No

No

No

No

No

No

No

No

No

No

No

No

R £

£

£

R

R

R

R

R

R

R

£

£

£

£

£

£

£

£

£

£

£

£

£

Not Present

Not Present

Not Present

£

R

R

Not Applicable

Not Applicable R

R

0.6°C On Ice

3/29/2021Taylor K. Burris

FedEx

gda

Date Received:

Received by:

Login completed by:

Carrier name:

BL2000\tedwards

3/30/2021

Reviewed by:

Reviewed Date:

Contact and Corrective Action Comments:The state the sample was collected in was not provided. The sample was collected in Hawaii per phone conversation with Paul Henige on 3/30/21.

The collection time indicated on the Chain of Custody for all samples is in Hawaii-Aleutian Standard Time. The collection time has been converted to Mountain Standard Time.

Temp Blank received in all shipping container(s)/cooler(s)? Yes NoR £ Not Applicable £

Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.

Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis.

Standard Reporting Procedures:

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Qualifiers and AbbreviationsQualifier Qualifier Description

## Limit of Quantitation (LOQ) for this analyte exceeds the Maximum Contaminant Level (MCL)

* Result exceeds the Maximum Contaminant Level (MCL)

A The analyte level was greater than four times the spike level - in accordance with the method, percent recovery is not calculated

B Analyte detected in the method blank

C Continuing calibration verification was outside of the quality control advisory limits

D Limit of Quantitation (LOQ) increased due to sample matrix

E Estimated value - result exceeds the instrument upper quantitation limit

H Analysis performed past the method holding time

J The reported result is an estimated value

L Lowest Limit of Quantitation (LOQ) available for the analytical method used

N Analyte concentration was not sufficiently high to calculate a Relative Percent Difference (RPD) for the serial dilution test

O Diluted out

P Poor method performance - method validations have shown no recoveries at low concentrations or method performance was erratic

Q Values reported below the Limit of Quantitation (LOQ) are statistically invalid

R Relative Percent Difference (RPD) exceeds advisory limit

S Spike recovery outside of advisory limits

T Analyte detected in the associated trip blank

U Not detected at the Limit of Detection (LOD)

V The RPD value for this duplicate represents the RER value and the RPDLimit of 2 is the RER upper limit.

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Qualifiers and AbbreviationsAbbreviation

Reporting Explanation of Abbreviation

DF Dilution Factor

DL Detection Limit

LOD Limit of Detection

LOQ Limit of Quantitation

MCL Maximum Contaminant Level

MDC Minimum Detectable Concentration

ND Not detected at the Limit of Quantitaton (LOQ)

RBSL Risk-Based Screening Levels

REC Recovery

RER Relative Error Ratio

RPD Relative Percent Difference

SPK Spike

Sample Types Explanation of Abbreviation

CCB Continuing Calibration Blank

CCV Continuing Calibration Verification Standard

DUP Sample Duplicate

ICSA Interference Check Sample A

ICSAB Interference Check Sample AB

ICV Initial Calibration Verification Standard

LCS Laboratory Control Sample

LCSD Laboratory Control Sample Duplicate

LFB Laboratory Fortified Blank

LRB Laboratory Reagent Blank

MBLK Method Blank

MS Sample Matrix Spike

MSD Sample Matrix Spike Duplicate

PDS Post Digestion/Distillation Spike

QCS Quality Control Sample

SD Serial Dilution

SRM Standard Reference Material

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LABORATORY ANALYTICAL REPORTPrepared by Billings, MT Branch

Lab ID: B21032068-001Client: APPL Inc Collection Date: 03/24/2021 12:15Client Sample ID: BA29552 ERH1294 Date Received: 03/29/2021Project: Not Indicated Report Date: 04/13/2021Matrix: Drinking Water

Analyses Result Units DF Qual LOQ LOD DL MCL Method Analysis Date / By RunID : Run Order BatchID

PETROLEUM HYDROCARBONS-SEMI-VOLATILEDiesel Range Organics (DRO) ND mg/L 1 U 0.30 0.11 0.037 SW8015C 03/31/2021 17:04/amn GCFID-HP5-B_210331A : 5 154020C10 to C25 Hyrocarbons ND mg/L 1 U 0.29 0.11 0.037 SW8015C 03/31/2021 17:04/amn GCFID-HP5-B_210331A : 5 154020C8 to C18 Hydrocarbons ND mg/L 1 U 0.29 0.11 0.048 SW8015C 03/31/2021 17:04/amn GCFID-HP5-B_210331A : 5 154020Total Extractable Hydrocarbons ND mg/L 1 U 0.30 0.11 0.048 SW8015C 03/31/2021 17:04/amn GCFID-HP5-B_210331A : 5 154020 Surr: o-Terphenyl 107 %REC 1 50-150 SW8015C 03/31/2021 17:04/amn GCFID-HP5-B_210331A : 5 154020

- Note 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28.- Note 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time.

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LABORATORY ANALYTICAL REPORTPrepared by Billings, MT Branch

Lab ID: B21032068-002Client: APPL Inc Collection Date: 03/24/2021 12:55Client Sample ID: BA29553 ERH1295 Date Received: 03/29/2021Project: Not Indicated Report Date: 04/13/2021Matrix: Drinking Water

Analyses Result Units DF Qual LOQ LOD DL MCL Method Analysis Date / By RunID : Run Order BatchID

PETROLEUM HYDROCARBONS-SEMI-VOLATILEDiesel Range Organics (DRO) ND mg/L 1 U 0.30 0.12 0.039 SW8015C 03/31/2021 19:52/amn GCFID-HP5-B_210331A : 8 154020C10 to C25 Hyrocarbons ND mg/L 1 U 0.30 0.12 0.039 SW8015C 03/31/2021 19:52/amn GCFID-HP5-B_210331A : 8 154020C8 to C18 Hydrocarbons ND mg/L 1 U 0.30 0.12 0.049 SW8015C 03/31/2021 19:52/amn GCFID-HP5-B_210331A : 8 154020Total Extractable Hydrocarbons ND mg/L 1 U 0.30 0.12 0.049 SW8015C 03/31/2021 19:52/amn GCFID-HP5-B_210331A : 8 154020 Surr: o-Terphenyl 106 %REC 1 50-150 SW8015C 03/31/2021 19:52/amn GCFID-HP5-B_210331A : 8 154020

- Note 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28.- Note 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time.

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Analytical QC Summary Report

Prepared by Billings, MT Branch

Client: APPL Inc

Workorder: B21032068


Run ID: Run Order: GCFID-HP5-B_210331A: 4 SampType: Method Blank Batch ID: 154020

Method: SW8015C Analysis Date: 03/31/2021 16:22 Prep Date: 03/30/2021 15:20

Lab ID: MB-154020 Units: mg/L Prep Method: SW3520C

Analytes Result LOQ Spk value Spk RefVal %REC LowLimit HighLimit RPD RefVal %RPD RPDLimit Qual

Diesel Range Organics (DRO) ND 0.15

C10 to C25 Hyrocarbons ND 0.15

C8 to C18 Hydrocarbons ND 0.15

Total Extractable Hydrocarbons ND 0.15

Surr: o-Terphenyl 0.21 0.0020 0.20 104.0 50 150

Associated Samples: B21032068-001A, B21032068-002A

Run ID: Run Order: GCFID-HP5-B_210331A: 3 SampType: Laboratory Control Sample Batch ID: 154020


Lab ID: LCS-154020 Units: mg/L Prep Method: SW3520C


Diesel Range Organics (DRO) 16 0.30 15 107.0 36 132

Total Extractable Hydrocarbons 17 0.30 15 112.0 60 132

Surr: o-Terphenyl 0.22 0.0020 0.20 107.0 56 125


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Analytical QC Summary Report

Prepared by Billings, MT Branch

Client: APPL Inc

Workorder: B21032068


Run ID: Run Order: GCFID-HP5-B_210331A: 6 SampType: Sample Matrix Spike Batch ID: 154020


Lab ID: B21032068-001AMS Units: mg/L Prep Method: SW3520C


Diesel Range Organics (DRO) 31 0.60 30 0.00 104.0 36 132

Total Extractable Hydrocarbons 33 0.60 30 0.00 108.0 60 132

Surr: o-Terphenyl 0.42 0.0040 0.40 0.00 105.0 56 125


Run ID: Run Order: GCFID-HP5-B_210331A: 7 SampType: Sample Matrix Spike Duplicate Batch ID: 154020


Lab ID: B21032068-001AMSD Units: mg/L Prep Method: SW3520C


Diesel Range Organics (DRO) 32 0.60 30 0.00 108.0 36 132 31 3.5 20.0

Total Extractable Hydrocarbons 34 0.60 30 0.00 112.0 60 132 33 3.3 20.0

Surr: o-Terphenyl 0.44 0.0040 0.40 0.00 109.0 56 125 0.00


Run ID: Run Order: GCFID-HP5-B_210331A: 2 SampType: Continuing Calibration Verification Standard Batch ID: R358548

Method: SW8015C Analysis Date: 03/31/2021 14:16 Prep Date:

Lab ID: CCV_0331HP504r Units: mg/L Prep Method:


Total Extractable Hydrocarbons 16 0.30 15 107.0 80 120

Surr: o-Terphenyl 0.20 0.0020 0.20 99.0 80 120


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Analytical QC Exceptions Report

Prepared by Billings, MT BranchClient: APPL IncWorkorder: B21032068Project: Not Indicated Report Date: 04/13/2021

All quality control measures met criteria; there were no Analytical QC Exceptions.

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Lab ID Client Sample ID Collection Date Matrix Test Name TCLP Date PrepMethod Prep Date Prep

BatchAnalysis Method Analysis Date

001A BA29552 ERH1294 03/24/2021 12:15 Drinking Water Diesel Range Organics SW3520C 03/30/2021 15:20 154020 SW8015C 03/31/2021 17:04

002A BA29553 ERH1295 03/24/2021 12:55 Drinking Water Diesel Range Organics SW3520C 03/30/2021 15:20 154020 SW8015C 03/31/2021 19:52

Preparation and Analysis Dates Report

4/13/2021

APPL Inc

Not IndicatedProject Name: Report Date:

Client:

Work Order: B21032068

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Chemical Abstracts Service (CAS) Registry NumbersPrepared by Billings, MT Branch

Client: APPL IncWorkorder: B21032068Project: Not Indicated Report Date: 04/13/2021

Analyses CAS No

Petroleum Hydrocarbons-Semi-VolatileDiesel Range Organics (DRO)C10 to C25 HyrocarbonsC8 to C18 HydrocarbonsTotal Extractable Hydrocarbons

4/13/2021 1:51:09 PM of 75

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BA29552 ERH1294 Batch ID: 154020

DIESEL RANGE ORGANICS CHROMATOGRAM REPORT

Sample Name: B21032068-001A ;0331HP5 , $HC-8015-DRO-W,

Raw File: G:\org\HP5\DAT\HP5033121_b\0331HP5.0008.RAW

Date & Time Acquired: 3/31/2021 5:04:34 PM

Method File: G:\Org\HP5\Methods\DR_8015-HG-L%.met

Calibration File: G:\Org\HP5\Cals\SW8015C_DRO210108HG.CAL

Sample Weight: 1040 Dilution: 1 S.A.: 1

Mean RF for TEH: 29457.33

Rt range for Diesel Range Organics: 6.439 to 15.702

SURROGATE COMPOUND RT ACTUAL MEASURED %REC

*o-Terphenyl_____________12.094 .192 .206 107.01 -

*1-Chlorooctadecane______12.901 .192 .162 84.3 -

DRO Area:563246.1 DRO Amount: 1.838533E-02

TEH Area:1378570 TEH Amount: 4.499892E-02

G:\org\HP5\dat\HP5033121_b\Review\008_B21032068-001A_DR_8015-HG-L%.xls

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BA29552 ERH1294 Batch ID: 154020





Method File: G:\Org\HP5\Methods\DR_C10-C25-HG-L%.met

Calibration File: G:\Org\HP5\Cals\SW8015C_DRO210108-C10-C25-HG.CAL





*o-Terphenyl_____________12.094 .192 .206 107.01 -


(C10-C25) DRO Area:615766.9 (C10-C25) DRO Amount: 2.069672E-02


G:\org\HP5\dat\HP5033121_b\Review\008_B21032068-001A_DR_C10-C25-HG-L%.xls

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Batch ID: 154020

RESIDUAL RANGE ORGANICS CHROMATOGRAM


Raw File: G:\Org\HP5\DAT\HP5033121_b\0331HP5.0008.RAW



Calibration File: G:\Org\HP5\Cals\SW8015C_DRO210108-C8-C18-HGb.CAL


Mean RF for for Residual TEH Range Organics Calculations: 29457.33

Rt range for Residual (C8-C18) Range Organics: 4.33 to 11.58


RRO (C8-C18) Area:1037235 RRO (C8-C18) AMOUNT: 3.385714E-02 AMN 04/01/2021


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10.1

0

10.2

7

10.3

6

10.5

0

10.5

6

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

1

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.6

0

12.6

4

12.7

4

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.1

9

14.3

8

14.5

7

14.8

0

14.9

5

15.3

1

15.5

0

15.6

2

15.7

8

16.2

2

16.3

2

16.6

7

16.8

6

17.3

0

17.3

3

17.4

2

17.7

5

18.1

6

18.6

1

19.2

1

20.4

8

*C

al D

iesel

C8

C18

G:\Org\HP5\DAT\HP5033121_b\0331HP5.0008.RAW B21032068-001A ;0331HP5 , $HC-8015-DRO-W,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

BA29553 ERH1295 Batch ID: 154020











*o-Terphenyl_____________12.095 .198 .209 105.76 -



TEH Area:3019305 TEH Amount: 0.1014827


3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

BA29553 ERH1295 Batch ID: 154020











*o-Terphenyl_____________12.095 .198 .209 105.76 -


(C10-C25) DRO Area:615766.9 (C10-C25) DRO Amount: 2.069672E-02



3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020













3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1

*C

al D

iesel

C8

C18


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

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5000

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ANALYTICAL RUN Summary

12-Jan-21

Run ID GCFID-HP5-B_210108B

Energy Laboratories Inc

Std ID Std Name Std Amount Std Units Samp Amount Samp Units SampType Expiration Date

DRO200917B Diesel Fuel #2 50,000 ug/mL in DCM CALS 12/31/2021

DRO201210A #2 Diesel in Acetone 150,000 ug/mL SECOND S 6/10/2021

DRO210105B EPH (4) SURR-1000 ug/mL ea. in Hexane SURRS 5/31/2022

Run Start Date: 1/8/2021

Comments: NEW ICAL SW8015C_DRO210108HA.CAL

Column ID:

Ical:

Analyst: Ann Nebel

14154799 CCV_0108HP51 HC-8015-DRO- CAL1 1/8/2021 2:21:25 1 0 0R354713

Seq No Lab ID Test Code Sample Typ File ID Analysis Date DF Prep Date SPKref RPDrefBatch ID pmoist

Analyte T Units SpikeRAW Final SPKref RPDref PQLMDL UQL %REC LOW HIGH %RPD QText

Total Extractable Hydrocarbons A mg/L 0.150.1350772 0 0 0.30 50 90% 0%80 120

14154800 CCV_0108HP51 HC-8015-DRO- CAL2 1/8/2021 3:03:30 1 0 0R354713



Total Extractable Hydrocarbons A mg/L 3.753.865478 0 0 0.30 50 103% 0%80 120

14154801 CCV_0108HP51 HC-8015-DRO- CAL3 1/8/2021 3:45:32 1 0 0R354713



Total Extractable Hydrocarbons A mg/L 1515.3786 0 0 0.30 50 103% 0%80 120

1

of 75

14154802 CCV_0108HP51 HC-8015-DRO- CAL4 1/8/2021 4:27:38 1 0 0R354713



Total Extractable Hydrocarbons A mg/L 37.539.10215 0 0 0.30.0499 50 104% 0%80 120

14154803 CCV_0108HP51 HC-8015-DRO- CAL5 1/8/2021 5:09:49 1 0 0R354713



Total Extractable Hydrocarbons A mg/L 5050.03634 0 0 0.30.0499 50 100% 0%80 120

14154804 CCV_0108HP50 HC-8015-DRO- CAL1 1/8/2021 5:52:15 1 0 0R354713



o-Terphenyl S mg/L 0.0020.00201784 0 0 0.0020 0 101% 0%80 120

14154805 CCV_0108HP50 HC-8015-DRO- CAL2 1/8/2021 6:34:45 1 0 0R354713



o-Terphenyl S mg/L 0.050.04980491 0 0 0.0020 0 100% 0%80 120

14154806 CCV_0108HP50 HC-8015-DRO- CAL3 1/8/2021 7:17:18 1 0 0R354713



o-Terphenyl S mg/L 0.20.2027571 0 0 0.0020 0 101% 0%80 120

14154807 CCV_0108HP50 HC-8015-DRO- CAL4 1/8/2021 7:59:52 1 0 0R354713



o-Terphenyl S mg/L 0.50.4989882 0 0 0.0020.000327 0 100% 0%80 120

2

of 75

14154808 CCV_0108HP51 HC-8015-DRO- CAL5 1/8/2021 8:42:33 1 0 0R354713



o-Terphenyl S mg/L 10.9852039 0 0 0.0020.000327 0 99% 0%80 120

14154809 CCV_0108HP51 HC-8015-DRO- ICV 1/8/2021 9:25:08 1 0 0R354713




3

of 75

Data File Sample Name Method Weight Dil Factor Amt Inj. IS Cal ID

G:\org\HP5\DAT\HP5010821_b\0108HP5.04r CCV_0108HP504r, DRO ;0108HP5 , DRO201215A G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0

G:\org\HP5\DAT\HP5010821_b\0108HP5.05r DCM-Baseline Check-V05 G:\Org\HP5\Methods\DR_8015-GX-LEXP.met 1 1 1 1 0

G:\org\HP5\DAT\HP5010821_b\0108HP5.06r

CCV_0108HP511r, CAL1 ;0108HP5 , 150 ug per mL Diesel (20 uL of Cal3 + 980 uL

DCM(13322), then 100 uL of that + 100 uL of DCM (13322)) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0


CCV_0108HP512r, CAL2 ;0108HP5 , 3750 ug per mL Diesel (100 uL Cal4 + 900 uL of

DCM(13322) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0


CCV_0108HP513r, CAL3 ;0108HP5 , 15000 ug per mL Diesel (300 uL of DRO20917B

+ 700 uL DCM(13322) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0


CCV_0108HP514r, CAL4 ;0108HP5 , 37500ug per mL Diesel (750 uL of DRO20917B


G:\org\HP5\DAT\HP5010821_b\0108HP5.10r CCV_0108HP515r, CAL5 ;0108HP5 , 50000 ug per mL Diesel (200 uL of DRO20917B) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0


CCV_0108HP506r, CAL1 ;0108HP5 , 2 ug per mL OTP (10 uL of Cal3 + 990 uL

DCM(13322) G:\Org\HP5\Methods\DS_8015-HA-L#.met 1 1 1 1 0


CCV_0108HP507r, CAL2 ;0108HP5 , 50 ug per mL OTP (100 uL Cal4 + 900 uL of



CCV_0108HP508r, CAL3 ;0108HP5 , 200 ug per mL OTP (100uL of Cal5 + 400 uL






CCV_0108HP510r, CAL5 ;0108HP5 , 1000 ug per mL OTP (250 uL 4000 ug/mL OTP

DRO210105B + 750 DCM(13322) G:\Org\HP5\Methods\DS_8015-HA-L#.met 1 1 1 1 0


CCV_0108HP516r, Second Source ;0108HP5 , 15000 ug per mL (100uL of

DRO201210A + 900uL DCM(13322) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0

Write Sequence Insert Entries(Have the first cell for entries selected

of 75

Chrom Perfect Calibration File

Printed on 1/11/2021 9:47:38 AM Page 1 of 2

File Name: G:\Org\HP5\Cals\SW8015C_DRO210108HA.CAL

Version: 5

Creator: AMN 1/11/2021

Description: DRO-8015. New ICal Per 0108HP5 (2021)-2 uL Inj.; COD added using OTP RFs

Reason for change:

External standard calibration

Standard injection volume: 1

Standard sample weight: 1

Area reject threshold: 500

Reference peak area reject threshold: 500

Amount units: nanograms

No default component

Method of calculating data point averages: Equal weight for all updates

No calibration update report

All levels are normal data points.

of 75



1 DRO Range Start

0 20000 40000

Amount

0

999999900

Are

a

Expected retention time: 6.82 minutes

Search window: 0.05 minutes

No retention time reference component

Group number: 0

High alarm limit: 0

Low alarm limit: 0

Component constant: 0

Single peak quantification by area

Y = 29457.33 X + 0

Average CF fit with equal weighting, forced to origin

Coefficient of determination: 0.9985872

Average error: 3.979%

Average CF: 29457.33

RSD: 5.768%

Level Amount Response Cal Factor Error, % Source Date and time

1 150 3979014 26526.76 -9.949 Manual 1/11/2021 9:46:00 AM

2 3750 1.138667E+08 30364.46 3.079 Manual 1/11/2021 9:46:09 AM

3 15000 4.530125E+08 30200.83 2.524 Manual 1/11/2021 9:46:18 AM

4 37500 1.151845E+09 30715.87 4.272 Manual 1/11/2021 9:46:27 AM

5 50000 1.473937E+09 29478.74 0.073 Manual 1/11/2021 9:46:39 AM

of 75



2 *o-Terphenyl

0 200 400 600 800 1000

Amount

0

9999999

20000000

30000000

Are

a




Group number: 0

High alarm limit: 0

Low alarm limit: 0



Y = 35071.26 X + 0





RSD: 1.097%


1 2 70648.41 35324.2 0.721 G:\Org\HP5\DAT\HP5010821_b\0108HP5.0011.BND 1/11/2021 9:44:43 AM

2 50 1746406 34928.12 -0.408 G:\Org\HP5\DAT\HP5010821_b\0108HP5.0012.BND 1/11/2021 9:44:50 AM

3 200 7110604 35553.02 1.374 G:\Org\HP5\DAT\HP5010821_b\0108HP5.0013.BND 1/11/2021 9:44:58 AM

4 500 1.749965E+07 34999.3 -0.205 G:\Org\HP5\DAT\HP5010821_b\0108HP5.0014.BND 1/11/2021 9:45:02 AM

5 1000 3.455164E+07 34551.64 -1.482 G:\Org\HP5\DAT\HP5010821_b\0108HP5.0015.BND 1/11/2021 9:45:07 AM

of 75



3 *1-Chlorooctadecane

0 200 400 600 800 1000

Amount

0

9999999

20000000

30000000

Are

a




Group number: 0

High alarm limit: 0

Low alarm limit: 0



Y = 35071.26 X + 0





RSD: 1.097%


1 2 70648.41 35324.2 0.721 Manual 1/11/2021 9:45:13 AM

2 50 1746406 34928.12 -0.408 Manual 1/11/2021 9:45:15 AM

3 200 7110604 35553.02 1.374 Manual 1/11/2021 9:45:17 AM

4 500 1.749965E+07 34999.3 -0.205 Manual 1/11/2021 9:45:19 AM

5 1000 3.455164E+07 34551.64 -1.482 Manual 1/11/2021 9:45:21 AM

of 75


Sample Name: CCV_0108HP504r, DRO ;0108HP5 , DRO201215A



Method File: G:\Org\HP5\Methods\DC_8015-HA-L%.met

Calibration File: G:\Org\HP5\Cals\SW8015C_DRO210108HA.CAL





*o-Terphenyl_____________12.572 200. 197.718 98.86 -

*1-Chlorooctadecane______13.364 200. 156.111 78.06 -

DRO Area:8.880706E+07 DRO Amount: 3014.77

TEH Area:1.082932E+08 TEH Amount: 3676.273

_

CONTINUING CALIBRATION REPORT: G:\Org\HP5\DAT\HP5010821_b\0108HP5.0004.RAW

COMPOUND ACTUAL(NG) MEASURED(NG) %RECOVERY LIMITS

TOTAL DRO________________15000. 3676.27 24.51 85-115

SURROGATE COMPOUND RT ACTUAL MEASURED %REC LIMITS

*o-Terphenyl_____________12.572 200. 197.718 98.86 85-115

*1-Chlorooctadecane______13.364 200. 156.111 78.06 85-115

G:\org\HP5\dat\HP5010821_b\Review\004_CCV_0108HP504r_DC_8015-HA-L%.xls

3.6

8

4.0

1

4.1

8

4.2

3

4.3

0

4.4

9

4.5

5

4.6

2

4.6

9

4.7

8

5.0

0

5.1

3

5.2

2

5.2

8

5.5

5

5.7

9

5.8

7

5.9

4

6.0

6

6.1

1

6.2

6

6.3

1

6.4

0

6.4

6

6.5

3

6.6

6

6.7

5

6.8

2

6.9

7

7.0

4

7.1

5

7.2

3

7.3

0

7.3

6

7.5

1

7.5

8

7.6

4

7.7

0

7.8

2

8.0

0

8.1

2

8.1

7

8.3

8

8.4

8

8.5

9

8.6

7

8.7

1

8.8

6

8.9

4

9.0

6

9.1

4

9.2

1

9.2

9

9.4

2

9.4

8

9.5

3

9.6

1

9.7

1

9.8

1

9.9

2

9.9

9

10.0

6

10.1

0

10.1

7

10.3

4

10.5

3

10.5

9

10.6

2

10.6

8

10.7

3

10.9

0

11.0

8

11.1

8

11.2

5

11.3

4

11.4

4

11.6

7

11.7

5

11.8

2

11.8

7

11.9

7

12.0

7

12.2

8

12.4

0

12.4

7 1

2.5

7

12.6

6

12.7

1

12.8

1

12.9

4

13.0

6

13.1

0

13.3

6

13.5

3

13.5

7

13.6

3

13.7

7

13.8

4

13.9

6

14.1

7

14.2

5

14.3

1

14.4

1

14.5

5

14.6

6

14.9

0

15.0

5

15.1

4

15.1

9

15.2

8

15.3

3

15.4

3

15.7

8

15.9

1

16.0

5

16.1

4

16.4

7

16.6

4

16.7

2

16.8

0

17.1

2

17.4

4

17.5

5

17.7

6

18.2

5

18.7

3

19.3

2

19.6

3

19.9

7

20.7

7

21.1

2

21.2

6

21.4

3

21.5

5

21.7

3

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\Org\HP5\DAT\HP5010821_b\0108HP5.0004.RAW CCV_0108HP504r, DRO ;0108HP5 , DRO201215A

4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

7000

of 75


Sample Name: DCM-Baseline Check-V05



Method File: G:\Org\HP5\Methods\DR_8015-GX-LEXP.met

Calibration File: G:\Org\HP5\Cals\SW8015C_DRO200123GX.CAL





*o-Terphenyl_____________29.787 200. . . -

*1-Chlorooctadecane______29.787 200. . . -

DRO Area:48911.73 DRO Amount: 1.688754

TEH Area:90991.55 TEH Amount: 3.141625

G:\org\HP5\dat\HP5010821_b\Review\005_DCM-Baseline Chec_DR_8015-GX-LEXP.xls

3.0

6

4.7

1

4.8

3

4.9

9

5.3

8

5.4

2

5.4

6

5.6

2

5.7

1

5.9

3

6.0

8

6.2

0

6.3

1

6.3

5

6.3

8

6.5

0

6.5

8

6.6

8

6.8

1

6.8

9

7.0

3

7.1

1

7.3

1

7.3

6

7.4

8

7.5

3

7.6

1

7.6

4

7.6

8

7.7

7

7.8

2

7.9

3

8.0

0

8.0

4

8.3

8

8.5

6

8.7

0

8.7

9

9.1

6

9.2

3

9.3

8

9.7

2

10.8

6 1

7.4

6

17.6

5

18.4

7

19.3

1

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5010821_b\0108HP5.0005.RAW DCM-Baseline Check-V05

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

10

20

30

40

50

60

70

80

90

100

110

120

130

140

150

of 75


Sample Name: CCV_0108HP511r, CAL1 ;0108HP5 , 150 ug per mL Diesel









*o-Terphenyl_____________12.568 200. .738 .37 -

*1-Chlorooctadecane______13.399 200. .796 .4 -

DRO Area:3854036 DRO Amount: 130.8345


_

CONTINUING CALIBRATION REPORT: G:\org\HP5\DAT\HP5010821_b\0108HP5.0006.RAW


TOTAL DRO________________15000. 135.08 .9 85-115


*o-Terphenyl_____________12.568 200. .738 .37 85-115

*1-Chlorooctadecane______13.399 200. .796 .4 85-115


3.5

5

3.9

6

4.2

4

4.3

3

4.4

1

4.7

0

5.0

7

5.1

4

5.1

8

5.3

2

5.3

6

5.4

0

5.4

8

5.5

6

5.6

3

5.7

4

5.7

6

5.8

2

5.8

7

5.9

7

6.0

7

6.1

1

6.2

1

6.2

9

6.3

8

6.4

3

6.4

8

6.5

1

6.5

7

6.6

2

6.6

8

6.8

2

6.9

6

7.0

2

7.0

7

7.1

6

7.3

0

7.3

6

7.4

3

7.5

3

7.5

8

7.6

4

7.7

2

7.7

7

7.8

2

7.8

6

7.9

6

8.0

2

8.0

5

8.1

2

8.1

7

8.2

1

8.2

6

8.3

4

8.3

8

8.4

4

8.4

9

8.5

4

8.6

0

8.6

3

8.6

7 8

.72

8.7

9

8.8

3

8.8

9

9.0

3

9.0

7

9.1

6

9.2

9

9.3

6 9.4

1

9.4

8 9

.57

9.6

7

9.7

1

9.8

1

9.8

8

9.9

8

10.1

0

10.2

1

10.2

6

10.3

2

10.3

9

10.4

8

10.6

4

10.7

0 1

0.7

5

10.8

4

10.9

0

10.9

5

11.0

3

11.0

6

11.1

7

11.2

6

11.3

9

11.4

5

11.6

2

11.6

6

11.8

1

11.9

7

12.0

2

12.0

8

12.1

5

12.2

2

12.2

6

12.3

3

12.4

7

12.5

4

12.5

7

12.6

5

12.6

8

12.7

8

12.9

4

13.0

3

13.1

3

13.1

7

13.2

2

13.3

1

13.4

0

13.4

6

13.5

7

13.6

4

13.7

2

13.8

4

13.9

3

14.0

0

14.1

0

14.2

6

14.4

1

14.5

0

14.6

6

14.7

6

14.8

0

15.0

5

15.1

7

15.2

9

15.4

3

15.7

9

16.1

4

16.3

4

16.6

4

16.8

1

17.4

4

17.5

8

17.7

7

18.0

4

19.3

2

21.5

1

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5010821_b\0108HP5.0006.RAW CCV_0108HP511r, CAL1 ;0108HP5 , 150 ug per mL Diesel

4 6 8 10 12 14 16 18 20 22

10

20

30

40

50

60

70

80

of 75











*o-Terphenyl_____________12.54 200. 26.506 13.25 -




_



TOTAL DRO________________15000. 3865.48 25.77 85-115


*o-Terphenyl_____________12.54 200. 26.506 13.25 85-115



3.5

6

3.7

1

3.8

3

3.9

6

4.0

5

4.1

4

4.2

5

4.3

3

4.4

1

4.5

4

4.5

9

4.7

0

4.7

8

4.8

4

4.9

0

4.9

9

5.0

7

5.1

4

5.1

8

5.3

2

5.3

6

5.4

0

5.4

8

5.5

6

5.6

3

5.7

4

5.7

6

5.8

2

5.8

7

5.9

7

6.0

6

6.1

1

6.2

1

6.2

9

6.3

8

6.4

3

6.4

8

6.5

1

6.5

7

6.6

2

6.6

8

6.8

2

6.9

6

7.0

2

7.0

7

7.1

6

7.3

0

7.3

5

7.4

3

7.5

2

7.5

8

7.6

4

7.7

7

7.8

6

7.9

6

8.0

5

8.1

2

8.1

7

8.2

1

8.2

6

8.3

4

8.3

8

8.4

3

8.4

8

8.6

3

8.6

7 8

.72

8.7

9

8.8

3

8.8

9

9.0

3

9.0

7

9.1

6

9.2

9

9.4

1

9.4

8

9.5

4

9.5

7

9.6

7

9.7

2

9.8

1

9.8

8 9

.98

10.1

0

10.2

1

10.2

6

10.3

2

10.3

9

10.4

8

10.6

1

10.6

4

10.6

9 1

0.7

5

10.8

4

10.9

0

10.9

5

11.0

3

11.0

6

11.1

7

11.2

6

11.3

3

11.3

9

11.4

5

11.6

1

11.6

6

11.8

1

11.9

7

12.0

2

12.0

7

12.1

5

12.2

1

12.2

6

12.3

3

12.4

6

12.5

4

12.6

5

12.6

8

12.7

8 1

2.9

4

13.0

0

13.0

3

13.1

3

13.1

7

13.2

2

13.3

1

13.4

0

13.4

6

13.5

6

13.6

4

13.7

1

13.8

4

13.9

2

14.0

0

14.1

0

14.2

5

14.4

0

14.5

0

14.6

0

14.6

6

14.7

5

14.8

0

14.8

9

15.0

5

15.1

7

15.2

8

15.4

2

15.5

4

15.6

5

15.7

8

15.9

1

16.0

1

16.1

4

16.2

6

16.3

4

16.4

7

16.5

9

16.8

0

17.0

4

17.1

2

17.2

7

17.4

5

17.5

8

17.7

7

18.0

3

18.2

4

18.7

4

19.3

1

20.2

6

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


4 6 8 10 12 14 16 18 20 22

0

200

400

600

800

1000

1200

1400

1600

1800

of 75











*o-Terphenyl_____________12.545 200. 101.663 50.83 -




_



TOTAL DRO________________15000. 15378.6 102.52 85-115


*o-Terphenyl_____________12.545 200. 101.663 50.83 85-115



3.5

5

3.7

1

3.8

3

3.9

6

4.0

5

4.1

4

4.2

5

4.3

3

4.4

1

4.5

4

4.5

9

4.7

0

4.7

8

4.8

4

4.9

0

4.9

9

5.0

7

5.1

4

5.1

8

5.3

2

5.3

6

5.4

0

5.4

8

5.5

6

5.6

3

5.7

6

5.8

3

5.8

7

5.9

7

6.0

6

6.1

1

6.2

1

6.3

0

6.3

8

6.4

3

6.4

8

6.5

1

6.5

7

6.6

2

6.6

8

6.7

1

6.8

2

6.9

6

7.0

2

7.0

7

7.1

6

7.3

0

7.3

6

7.4

3

7.5

3

7.5

8

7.6

5

7.7

2

7.7

7

7.8

3

7.8

6

7.9

6

8.0

3

8.0

6

8.1

2

8.1

8

8.2

1

8.2

6

8.3

4

8.3

9

8.4

9

8.6

3

8.7

2

8.8

0

8.8

3

8.8

9

9.0

3

9.0

8

9.1

7

9.2

9

9.4

1

9.4

9 9.5

8

9.6

7

9.7

3

9.8

1

9.8

9 9

.99

10.1

1

10.2

1

10.2

7

10.3

3

10.4

0

10.4

9

10.5

6

10.6

5

10.7

0 1

0.7

6

10.8

5

10.9

1

10.9

6

11.0

3

11.0

7

11.1

8

11.2

6

11.3

4

11.3

9

11.4

6

11.6

2

11.6

7

11.8

2

11.9

8

12.0

3

12.0

8

12.1

6

12.2

2

12.2

7

12.3

3

12.4

7

12.5

5

12.6

6

12.6

8

12.7

8 1

2.9

5

13.0

1

13.0

3

13.1

3

13.1

7

13.2

3

13.3

1

13.4

0

13.4

7

13.5

7

13.6

4

13.7

2

13.8

4

14.0

0

14.1

0

14.2

6

14.4

0

14.5

0

14.6

6

14.8

0

14.9

0

15.0

5

15.1

7

15.2

8

15.4

2

15.5

4

15.6

5

15.7

8

15.9

0

16.0

0

16.1

3

16.2

5

16.3

4

16.4

7

16.5

9

16.6

9

16.8

0

16.9

0

16.9

8

17.1

2

17.2

7

17.4

5

17.5

7

17.7

6

17.8

2

17.9

7

18.2

4

18.7

4

19.3

2

20.7

7

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

7000

of 75


Sample Name: CCV_0108HP514r, CAL4 ;0108HP5 , 37500ug per mL Diesel









*o-Terphenyl_____________12.557 200. 266.864 133.43 -




_



TOTAL DRO________________15000. 39102.15 260.68 85-115


*o-Terphenyl_____________12.557 200. 266.864 133.43 85-115



3.5

6

3.7

2

3.8

3

3.9

6

4.0

5

4.1

4

4.2

5

4.3

3

4.4

1

4.5

5

4.5

9

4.7

0

4.7

8

4.8

4

4.9

0

4.9

9

5.0

7

5.1

5

5.3

2

5.3

6

5.4

1

5.4

8

5.5

7

5.6

4

5.7

7

5.8

3

5.8

8

5.9

7

6.0

6

6.1

1

6.2

2

6.3

0

6.4

3

6.4

8

6.5

1

6.5

7

6.6

3

6.6

9

6.8

2

6.9

6

7.0

3

7.0

8

7.1

6

7.3

0

7.3

6

7.4

3

7.5

3

7.5

8

7.6

6

7.7

3

7.7

8

7.8

3

7.8

7

7.9

7

8.0

3

8.0

6

8.1

3

8.2

2

8.2

7

8.3

5

8.4

0

8.4

5

8.5

0

8.6

4 8.7

3

8.8

0

8.8

4

8.9

0

9.0

4

9.0

9

9.1

8

9.3

0

9.3

7 9.4

2

9.5

0 9.5

9

9.7

4

9.8

3

9.9

0

10.0

1

10.1

2

10.2

3

10.2

8

10.3

5

10.4

1

10.5

1

10.6

3

10.6

7

10.7

2 10.7

7

10.8

7

10.9

3

10.9

8

11.0

5

11.0

8

11.1

9

11.2

8

11.3

5

11.4

1

11.4

7

11.6

4 11.6

9

11.8

3

11.9

9

12.0

4

12.1

0

12.1

7

12.2

3

12.2

8

12.3

4

12.4

8

12.5

6

12.6

7

12.7

0

12.8

0

12.9

6

13.0

4

13.1

4

13.1

8

13.2

4

13.3

2

13.4

1

13.4

8

13.5

8

13.6

5

13.7

2

13.8

4

13.9

3

14.0

0

14.1

0

14.2

6

14.4

0

14.5

0

14.6

1

14.6

6

14.7

5

14.9

0

15.0

5

15.1

7

15.2

8

15.4

2

15.5

4

15.6

5

15.7

9

15.9

1

16.0

1

16.1

3

16.2

5

16.3

4

16.4

7

16.5

9

16.6

8

16.8

0

16.9

0

16.9

7

17.1

2

17.2

7

17.4

5

17.5

7

17.8

2

17.9

6

18.2

4

18.7

4

18.8

9

19.3

2

19.9

8

20.3

8

20.7

6

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5010821_b\0108HP5.0009.RAW CCV_0108HP514r, CAL4 ;0108HP5 , 37500ug per mL Diesel

4 6 8 10 12 14 16 18 20 22

0

2000

4000

6000

8000

10000

12000

14000

16000

of 75











*o-Terphenyl_____________12.561 200. 341.952 170.98 -




_



TOTAL DRO________________15000. 50036.34 333.58 85-115


*o-Terphenyl_____________12.561 200. 341.952 170.98 85-115



3.5

6

3.7

1

3.8

3

3.9

6

4.0

5

4.1

4

4.2

5

4.3

3

4.4

1

4.5

5

4.5

9

4.7

0

4.7

8

4.8

4

4.9

0

4.9

9

5.0

7

5.1

5

5.3

2

5.3

6

5.4

1

5.4

8

5.5

7

5.6

4

5.7

7

5.8

3

5.8

8

5.9

7

6.0

6

6.1

2

6.2

2

6.3

0

6.4

4 6.5

1

6.5

8

6.6

3

6.6

9

6.7

2

6.8

3

6.9

6

7.0

3

7.0

8

7.1

6

7.3

0

7.3

6

7.4

4

7.5

3

7.5

9

7.6

6

7.7

3

7.7

8

7.8

4

7.8

7

7.9

8

8.0

7

8.1

3

8.2

2

8.2

7

8.4

0

8.5

0

8.6

4 8.7

3

8.8

1

8.8

4

8.9

1

9.0

4

9.1

0

9.1

8

9.3

1

9.4

3

9.5

0 9.5

9

9.7

5

9.8

3

9.9

1

10.0

2

10.1

3

10.2

3

10.2

8

10.3

6

10.4

2

10.5

1

10.6

4

10.6

7

10.7

8

10.8

7

10.9

3

10.9

8

11.0

9

11.2

0

11.2

8

11.3

6

11.4

1

11.4

8

11.6

4 11.6

9

11.8

4

12.0

0

12.0

5

12.1

0

12.1

7

12.2

0

12.2

4

12.2

9

12.3

5

12.4

9

12.5

6

12.7

0

12.8

0

12.9

6

13.0

5

13.1

4

13.1

9

13.2

4

13.3

3

13.4

1

13.4

8

13.5

8

13.6

5

13.7

3

13.8

4

13.9

4

14.0

0

14.1

0

14.2

6

14.4

0

14.5

0

14.6

6

14.9

0

15.0

5

15.1

7

15.2

8

15.4

2

15.5

4

15.6

5

15.7

8

15.9

1

16.0

0

16.1

3

16.2

5

16.3

4

16.4

7

16.6

8

16.8

0

16.8

9

17.1

2

17.2

7

17.4

5

17.5

7

17.8

2

17.9

6

18.2

4

18.3

8

18.7

4

19.3

0

19.4

4

19.9

8

20.3

8

20.7

7

21.4

9

21.6

8

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


4 6 8 10 12 14 16 18 20 22

0

5000

10000

15000

20000

of 75


Sample Name: CCV_0108HP506r, CAL1 ;0108HP5 , 2 ug per mL OTP



Method File: G:\Org\HP5\Methods\DS_8015-HA-L#.met






*o-Terphenyl_____________12.569 200. 2.018 1.01 -




_



TOTAL DRO________________15000. . . 85-115


*o-Terphenyl_____________12.569 200. 2.018 1.01 85-115


G:\org\HP5\dat\HP5010821_b\Review\011_CCV_0108HP506r_DS_8015-HA-L#.xls

12.0

2

12.0

8

12.1

3

12.4

7

12.5

7

12.8

3

12.9

4

13.3

9

13.7

2

13.8

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=2.0

178

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

212

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N

G:\org\HP5\DAT\HP5010821_b\0108HP5.0011.RAW CCV_0108HP506r, CAL1 ;0108HP5 , 2 ug per mL OTP

12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

15

20

25

30

35

40

45

50

55

60

65

70

75

of 75











*o-Terphenyl_____________12.567 200. 49.805 24.9 -




_



TOTAL DRO________________15000. . . 85-115


*o-Terphenyl_____________12.567 200. 49.805 24.9 85-115

*1-Chlorooctadecane______15.793 200. . . 85-115


12.0

2

12.0

7

12.4

6

12.5

7

12.9

4

13.0

0

13.7

2

13.7

8

13.8

4

13.9

7

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=49.8

049

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N


12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

200

400

600

800

1000

1200

1400

of 75











*o-Terphenyl_____________12.572 200. 202.757 101.38 -




_



TOTAL DRO________________15000. 27.47 .18 85-115


*o-Terphenyl_____________12.572 200. 202.757 101.38 85-115



12.0

7

12.1

2

12.4

4

12.5

7

12.8

8

12.9

4

13.0

0

13.0

6

13.3

6

13.4

6

13.7

2

13.7

8

13.8

3

13.9

6

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=202.7

571

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

15

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N


12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

-500

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75











*o-Terphenyl_____________12.583 200. 498.988 249.49 -




_



TOTAL DRO________________15000. 39.54 .26 85-115


*o-Terphenyl_____________12.583 200. 498.988 249.49 85-115



12.0

7

12.4

4

12.5

8

12.7

1

12.7

8

12.8

8

12.9

4

13.0

0

13.0

5

13.3

6

13.7

2

13.7

7

13.9

6

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=498.9

882

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

182

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N


12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

2000

4000

6000

8000

10000

12000

14000

of 75











*o-Terphenyl_____________12.594 200. 985.204 492.6 -




_



TOTAL DRO________________15000. 46.56 .31 85-115


*o-Terphenyl_____________12.594 200. 985.204 492.6 85-115



12.0

2

12.0

7

12.4

4

12.5

9

12.7

1

12.7

8

12.8

8

12.9

4

13.0

0

13.0

5

13.4

0

13.7

7

13.9

6

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=985.2

039

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

224

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N


12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

5000

10000

15000

20000

25000

of 75


Sample Name: CCV_0108HP516r, Second Source ;0108HP5 , 15000 ug per mL









*o-Terphenyl_____________12.532 200. 148.336 74.17 -




_



TOTAL DRO________________15000. 14941.95 99.61 85-115


*o-Terphenyl_____________12.532 200. 148.336 74.17 85-115



3.5

5

3.7

4

3.8

3

3.9

5

4.0

5

4.1

4

4.2

4

4.3

3

4.4

1

4.5

4

4.5

8

4.6

9

4.7

8

4.8

5

4.9

9

5.0

7

5.1

4

5.2

4

5.3

2

5.3

6

5.4

0 5.4

9 5.5

6

5.6

4

5.7

6

5.8

2

5.8

7

5.9

7

6.0

6

6.1

1 6.2

1

6.2

9

6.3

8

6.4

3

6.5

0

6.5

7

6.6

2

6.6

8

6.7

1

6.8

2

6.9

5

7.0

2

7.0

7

7.1

6

7.3

0

7.3

6

7.4

2

7.5

2

7.5

8

7.6

4

7.7

2

7.7

7

7.8

2

7.8

6

7.9

6

8.0

2

8.0

6

8.1

2

8.1

8 8.2

1

8.3

4

8.3

9

8.4

9

8.5

4

8.6

3

8.6

7 8.7

2

8.7

6

8.8

0

8.8

3

8.8

9

8.9

5

9.0

7

9.1

5

9.1

9

9.3

1

9.4

1

9.4

9

9.5

4 9

.57

9.6

7

9.7

2

9.7

9

9.8

9

9.9

6 1

0.0

3

10.1

1

10.2

7

10.3

3

10.4

9

10.6

1

10.6

4

10.6

9

10.8

4

10.9

1

10.9

6

11.0

5

11.1

8

11.2

5

11.3

4

11.3

9

11.4

5

11.5

9

11.6

9

11.7

9

11.8

2

11.8

9

11.9

7

12.0

3

12.1

9

12.2

7

12.3

3

12.4

7

12.5

3

12.6

7

12.7

7

12.8

2

12.9

4

13.0

2

13.1

3

13.2

2

13.2

9

13.4

0

13.5

7

13.6

7

13.7

1 1

3.8

3

14.0

0

14.1

0

14.2

5

14.3

4

14.4

1

14.5

0

14.6

6

14.7

4

14.8

0

14.8

9

14.9

4

15.0

5

15.1

8

15.2

8

15.4

2

15.5

5

15.6

4

15.7

8

15.9

0

16.0

0

16.1

3

16.2

5

16.3

3

16.4

7

16.5

8

16.8

0

16.9

0

16.9

9

17.1

2

17.4

5

17.5

6

17.7

6

18.0

4

18.2

4

18.7

2

19.3

0

20.3

6

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5010821_b\0108HP5.0016.RAW CCV_0108HP516r, Second Source ;0108HP5 , 15000 ug per mL

4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

of 75

Data File Sample Name Method Weight Dil Factor Amt Inj. IS Cal ID Manual Integration

G:\org\HP5\DAT\HP5010821_b\0108HP5.04r CCV_0108HP504r, DRO ;0108HP5 , DRO201215A G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0

Integration is valley to valley. Assigned Set Baseline All

Valley on at 17.5.

G:\org\HP5\DAT\HP5010821_b\0108HP5.05r DCM-Baseline Check-V05 G:\Org\HP5\Methods\DR_8015-GX-LEXP.met 1 1 1 1 0 No integration.


CCV_0108HP511r, CAL1 ;0108HP5 , 150 ug per mL Diesel (20 uL of Cal3 + 980 uL

DCM(13322), then 100 uL of that + 100 uL of DCM (13322)) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0

The integration of Diesel Range Organics

and Total Extractable Hydrocarbons is the

hydrocarbon response with reference to the

basline. Assigned Set Baseline All Valley on at 17.5


CCV_0108HP512r, CAL2 ;0108HP5 , 3750 ug per mL Diesel (100 uL Cal4 + 900 uL of

DCM(13322) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0






CCV_0108HP513r, CAL3 ;0108HP5 , 15000 ug per mL Diesel (300 uL of DRO20917B







CCV_0108HP514r, CAL4 ;0108HP5 , 37500ug per mL Diesel (750 uL of DRO20917B






G:\org\HP5\DAT\HP5010821_b\0108HP5.10r CCV_0108HP515r, CAL5 ;0108HP5 , 50000 ug per mL Diesel (200 uL of DRO20917B) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0






CCV_0108HP506r, CAL1 ;0108HP5 , 2 ug per mL OTP (10 uL of Cal3 + 990 uL


Surrogates are integrated using a valley to

valley integration using Set Basline Now

placed slight before at 12.4 and slightly

after the surrogate peak at 12.66 and scaling showing

surrogaete peak from 12-14.


CCV_0108HP507r, CAL2 ;0108HP5 , 50 ug per mL OTP (100 uL Cal4 + 900 uL of
























CCV_0108HP510r, CAL5 ;0108HP5 , 1000 ug per mL OTP (250 uL 4000 ug/mL OTP

DRO210105B + 750 DCM(13322) G:\Org\HP5\Methods\DS_8015-HA-L#.met 1 1 1 1 0







CCV_0108HP516r, Second Source ;0108HP5 , 15000 ug per mL (100uL of

DRO201210A + 900uL DCM(13322) G:\Org\HP5\Methods\DC_8015-HA-L%.met 1 1 1 1 0





Write Sequence Insert Entries(Have the first cell for entries selected)

Page 1 of 1

Digitally signed byAnn NebelDate: 2021.01.27 15:17:17 -07:00

of 75

Prep Batch 154020

Prep Start Date: 3/30/2021 3:20:20 PMPrep Code: HC-3520-DRO

Sample ID pHFinal

Vol (mL)

Initial

Samp Amt Factor

PREP BATCH REPORTTechnician: Ann Nebel

Prep End Date: 3/31/2021 1:01:00 PM

Page:1 of 1

Sol

Added

Sol

Recovered MatrixPrep

Start Date

Prep

End Date

Batch Units: ML

Balance

Prep Temp NA °C

3/31/20213/30/20210.001

Start time: 3:15 PM on 03/30/2021. End time: 9:20 AM on 03/31/2021

MB-154020 1000 1.000 0

3/31/20213/30/20210.001

All bottles used in the prep batch were used completely and then disposed of.

LCS-154020 1000 1.000 0

3/31/20213/30/20210.000962

Bottle 1/2 Clear no sediment.

B21032068-001A 1040 1.002 0 0Drinking Water

3/31/20213/30/20210.002


B21032068-001AMS 500 1.002 0 0Drinking Water

3/31/20213/30/20210.002


B21032068-001AMSD 500 1.002 0 0Drinking Water

3/31/20213/30/20210.00198

Bottle 1/2 Turbid with light sediment. DCM turned yellow in color. Blew down to 1.3mL bottled to 2mL.

B21031979-001A 1010 2.002 0 0Aqueous

3/31/20213/30/20210.000971

Bottle 1/2 Turbid no sediment.

B21031997-001D 1030 1.002 0 0Aqueous

3/31/20213/30/20210.003

Bottle 1/2 Grayish color liquid, very turbid with heavy sediment and DCM turned yellow in color. Blew down to 2.9mL, bottled to 3mL.

B21031999-001D 1000 3.006-2 0 0Aqueous

3/31/20213/30/20210.00099


B21032068-002A 1010 1.002 0 0Drinking Water

Spk ID Spike Name SampType AmtAdd Exp Date

DRO210105A OTP/COD SURR 2000 ug/mL all 100ul 9/30/2024

FP210225 13301 DCM RINSED FILTER PAPER all 1 7/22/2021

Sulfate 03/08/21 ( Baked Sodium Sulfate all Varies 9/28/2025

DRO201210A #2 Diesel in Acetone 150,000 ug/mL LCS, LCSD, MS, 100ul 6/10/2021

Number Reagent Name Exp Date AmtAdd

11 Carbon Filter Water 1/1/2023

11684 PTFE Boiling Stones 24928241 7/18/2024

13019 Sulfuric Acid 2020050559 5/1/2022

13273 pH-indicator Strips 0-14 HC025486 9/30/2024

13680 Dichloromethane EA567 12/19/2022

of 75

ANALYTICAL RUN Summary

01-Apr-21

Run ID GCFID-HP5-B_210331A

Energy Laboratories Inc

Std ID Std Name Std Amount Std Units Samp Amount Samp Units SampType Expiration Date

DRO210204A Carbon Scan STD MARKER 3/5/2028

DRO210311C ALASKA MARKER-200ug/mL MARKER 9/30/2021

DRO210319C 8015 CCV-15,000ug/mL + 200 OTP CCV 8/8/2021

Run Start Date: 3/31/2021

Comments: DRO-8015-ICAL information is in Index GCFID-HP5-B_210108C

Column ID:

Ical:

Analyst: Ann Nebel

14285727 MARKER_0331 HC-8015-DRO- SAMP 3/31/2021 1:34:1 1 0 0R358548



Diesel Range Organics (DRO) A mg/L 03.212108 0 0 0.30.0389 50 0% 0%0 0


o-Terphenyl S mg/L 0.20.2134707 0 0 0.0020.00053 0 107% 0%50 150

Diesel Range Organics (C10 to C24) X mg/L 03.212108 0 0 0.30.15 0 0% 0%0 0

14285728 CCV_0331HP50 HC-8015-DRO- CCV 3/31/2021 2:16:1 1 0 0R358548




o-Terphenyl S mg/L 0.20.1986519 0 0 0.0020.00053 0 99% 0%80 120

14285729 LCS-154020 HC-8015-DRO- LCS-DOD 3/31/2021 3:40:3 1 3/30/2021 3: 0 0154020



1

of 75

14285729 LCS-154020 HC-8015-DRO- LCS-DOD 3/31/2021 3:40:3 1 3/30/2021 3: 0 0154020





o-Terphenyl S mg/L 0.20.2146244 0 0 0.0020.00053 0 107% 0%56 125


14285730 MB-154020 HC-8015-DRO- MBLK 3/31/2021 4:22:3 1 3/30/2021 3: 0 0154020



C10 to C25 Hyrocarbons A mg/L 00 0 0 0.30.0389 0 0% 0%0 0

C8 to C18 Hydrocarbons A mg/L 00 0 0 0.30.0499 0 0% 0%0 0

Diesel Range Organics (DRO) A mg/L 00 0 0 0.30.0389 50 0% 0%0 0

Total Extractable Hydrocarbons A mg/L 00 0 0 0.30.0499 50 0% 0%0 0

o-Terphenyl S mg/L 0.20.2082983 0 0 0.0020.00053 0 104% 0%50 150

Diesel Range Organics (C10 to C24) X mg/L 00 0 0 0.30.15 0 0% 0%0 0

14285731 B21032068-001 HC-8015-DRO- SAMP 3/31/2021 5:04:3 1 3/30/2021 3: 0 0154020



C10 to C25 Hyrocarbons A mg/L 00 0 0 0.28860.0374218 0 0% 0%0 0 U

C8 to C18 Hydrocarbons A mg/L 00 0 0 0.28860.0480038 0 0% 0%0 0 U

Diesel Range Organics (DRO) A mg/L 00 0 0 0.30.0374218 50 0% 0%0 0 U

Total Extractable Hydrocarbons A mg/L 00 0 0 0.30.0480038 50 0% 0%0 0 U

o-Terphenyl S mg/L 0.19240.2057819 0 0 0.0020.0005099 0 107% 0%50 150

14285732 B21032068-001 HC-8015-DRO- MS-DOD 3/31/2021 5:46:3 1 3/30/2021 3: 1E+07 0154020





o-Terphenyl S mg/L 0.40.4209306 0 0 0.0040.00106 0 105% 0%56 125


2

of 75

14285733 B21032068-001 HC-8015-DRO- MSD-DOD 3/31/2021 6:28:2 1 3/30/2021 3: 1E+07 1E+07154020



Diesel Range Organics (DRO) A mg/L 3032.28234 0 31.18094 0.60.0778 50 108% 3%36 132

Total Extractable Hydrocarbons A mg/L 3033.6459 0 32.54864 0.60.0998 50 112% 3%60 132

o-Terphenyl S mg/L 0.40.4371331 0 0 0.0040.00106 0 109% 0%56 125

Diesel Range Organics (C10 to C24) X mg/L 3032.28234 0 31.18094 0.60.3 0 108% 3%36 132

14285734 B21032068-002 HC-8015-DRO- SAMP 3/31/2021 7:52:2 1 3/30/2021 3: 0 0154020



C10 to C25 Hyrocarbons A mg/L 00 0 0 0.2970.038511 0 0% 0%0 0 U

C8 to C18 Hydrocarbons A mg/L 00 0 0 0.2970.049401 0 0% 0%0 0 U

Diesel Range Organics (DRO) A mg/L 00 0 0 0.30.038511 50 0% 0%0 0 U

Total Extractable Hydrocarbons A mg/L 00 0 0 0.30.049401 50 0% 0%0 0 U

o-Terphenyl S mg/L 0.1980.2094215 0 0 0.0020.0005247 0 106% 0%50 150

14285735 MARKER_0331 HC-8015-DRO- SAMP 3/31/2021 9:16:4 1 0 0R358548





o-Terphenyl S mg/L 0.20.2163709 0 0 0.0020.00053 0 108% 0%50 150


14285736 CCV_0331HP51 HC-8015-DRO- CCV 3/31/2021 9:58:5 1 0 0R358548




o-Terphenyl S mg/L 0.20.2024086 0 0 0.0020.00053 0 101% 0%80 120

3

of 75

Data File Sample Name Method Weight Dil Factor Amt Inj. IS Cal ID

G:\org\HP5\DAT\HP5033121_b\0331HP5.01r DCM-Baseline Check-01 G:\Org\HP5\Methods\DR_8015-HG-LEXP.met 1 1 1 1 0

G:\org\HP5\DAT\HP5033121_b\0331HP5.02r MARKER_0331HP502r, CSCAN ;0331HP5 , DRO210204A g:\org\HP5\Methods\\CSC210331.met 1 1 1 1 0

G:\org\HP5\DAT\HP5033121_b\0331HP5.03r MARKER_0331HP503r, DRO AK;0331HP5 , DRO210311C G:\Org\HP5\Methods\DC_8015-HG-L%.met 1000 1 1 1 0

G:\org\HP5\DAT\HP5033121_b\0331HP5.04r CCV_0331HP504r, DRO 8015;0331HP5 , DRO210319C G:\Org\HP5\Methods\DC_8015-HG-L%.met

G:\Org\HP5\Methods\DS_8015-HG-L#.met 1 1 1 1 0


G:\org\HP5\DAT\HP5033121_b\0331HP5.06r LCS-154020 ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033106-HG-L%.met


G:\org\HP5\DAT\HP5033121_b\0331HP5.07r MB-154020 ;0331HP5 , G:\Org\HP5\Methods\DR_8015-HG-L%.met

G:\Org\HP5\Methods\DR_C8-C18-HG-L%.met

G:\Org\HP5\Methods\DR_C10-C25-HG-L%.met 1000 1 1 1 0

G:\org\HP5\DAT\HP5033121_b\0331HP5.08r B21032068-001A ;0331HP5 , $HC-8015-DRO-W, G:\Org\HP5\Methods\DR_8015-HG-L%.met



G:\org\HP5\DAT\HP5033121_b\0331HP5.09r B21032068-001AMS ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033106-HG-L%.met


G:\org\HP5\DAT\HP5033121_b\0331HP5.10r B21032068-001AMSD ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033110-HG-L%.met






G:\org\HP5\DAT\HP5033121_b\0331HP5.13r MARKER_0331HP513r, CSCAN ;0331HP5 , DRO210204A g:\org\HP5\Methods\\CSC210331.met 1 1 1 1 0

G:\org\HP5\DAT\HP5033121_b\0331HP5.14r MARKER_0331HP514r, DRO AK;0331HP5 , DRO210311C G:\Org\HP5\Methods\DC_8015-HG-L%.met 1000 1 1 1 0




of 75


Sample Name: DCM-Baseline Check-01



Method File: G:\Org\HP5\Methods\DR_8015-HG-LEXP.met






*o-Terphenyl_____________12.087 200. .616 .31 -

*1-Chlorooctadecane______12.948 200. 1.054 .53 -



G:\org\HP5\dat\HP5033121_b\Review\001_DCM-Baseline Chec_DR_8015-HG-LEXP.xls

4.7

4

4.8

8

4.9

8

5.0

9

5.1

7

5.2

6

5.3

7

5.4

6

5.5

0

5.5

8

5.7

4

5.8

5

5.9

6

6.0

1

6.0

4

6.1

6

6.2

5

6.3

9

6.4

4

6.6

7

6.6

9

6.8

1

7.0

9

7.2

8

7.3

2

7.4

1

7.4

9

7.5

9

7.6

6

7.8

8

7.9

3

8.0

1

8.0

5

8.2

4

8.3

5

8.4

3

8.5

6

8.6

0

8.6

8

8.7

5

8.7

9

8.8

4

9.1

0

9.2

3

9.3

2

9.5

7

9.6

9

9.9

0

10.4

8

10.8

3

11.0

2

11.2

6

11.3

4

11.5

3

11.7

5

11.8

4

11.8

8

12.0

2

12.0

9

12.2

2

12.3

2

12.3

7

12.4

9

12.6

7

12.8

1

12.9

5

13.0

6

13.1

2

13.1

9

13.6

1

17.9

3

20.7

9

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0001.RAW DCM-Baseline Check-01

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

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30

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50

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G:\

org

\HP

5\d

at\

HP

50

33

12

1_

b\R

evi

ew

\00

2_

MA

RK

ER

_0

33

1H

P5

02

r_C

SC

21

03

31

.xls

0.8

4

0.9

2

1.0

1

1.0

4

1.1

0

1.2

0

1.2

4

1.3

8

1.5

3

1.6

3

1.8

6

2.0

2

2.2

0

2.3

4

2.5

0

2.5

4

2.7

0

3.1

0

3.4

3

3.5

2

3.5

6

3.9

9

4.1

8

4.2

6

4.3

0

4.3

8

4.5

1

4.9

8

5.4

3

5.5

6

6.0

2

6.1

4

6.2

4

6.4

1

6.5

0

6.6

9

6.8

1

6.8

9

6.9

7

7.0

4

7.1

5

7.3

0

7.3

7

7.5

5

7.6

6

7.7

0

7.7

5

7.8

2

7.8

5

8.0

2

8.3

3

8.4

8

8.5

8

8.6

9

8.8

2

8.9

4

9.0

3

9.1

4

9.3

2

9.6

0

9.7

0

9.7

7

9.9

2

10

.06

1

0.1

8

10

.21

1

0.3

2

10

.48

1

0.7

2

10

.82

1

1.0

2

11

.15

1

1.1

7

11

.25

1

1.2

9

11.3

9

11

.53

1

1.7

5

11

.87

1

2.0

3

12

.22

1

2.2

6

12

.36

1

2.5

0

12

.66

1

2.7

7

12

.82

1

2.9

5

13

.06

1

3.1

2

13.1

6

13

.26

1

3.3

8

13

.53

1

3.6

3

13

.65

1

3.7

9

13

.93

1

4.1

9

14

.43

1

4.5

8

14

.81

1

4.8

5

14.9

5

15

.17

1

5.3

1

15

.52

1

5.6

6

15

.82

1

5.9

9

16

.19

1

6.3

2

16.5

1

16

.62

1

6.9

4

17.0

8

17.2

3

17

.57

1

7.9

4

18

.38

1

8.6

1

18.8

8

19.4

9

20.1

8

21

.02

21

.46

21.9

9

23.9

8

24.6

0

c-5

c-6

c-7

c-8

c-9

c-1

0

c-1

1

c-1

2

c-1

3

c-1

4

c-1

5

c-1

6

c-1

7

c-1

8

c-1

9

c-2

0

c-2

1

c-2

2

c-2

3

c-2

4

c-2

5

c-2

6

c-2

7

c-2

8

c-2

9

c-3

0

c-3

2

c-3

4

c-3

6

c-3

8

c-4

0

G:\

org

\HP

5\D

AT

\HP

50

331

21

_b\0

33

1H

P5

.00

02.R

AW

MA

RK

ER

_0

33

1H

P50

2r,

CS

CA

N ;

03

31H

P5

, D

RO

21

02

04A

05

00

10

00

15

00

20

00

250

03

000

35

00

40

00

45

00

500

05

500

60

00

65

00

70

00

0 2 4 6 8

10

12

14

16

18

20

22

24

26

28

30

of 75


Sample Name: MARKER_0331HP503r, DRO AK;0331HP5 , DRO210311C



Method File: G:\Org\HP5\Methods\DC_8015-HG-L%.met






*o-Terphenyl_____________12.095 .2 .213 106.74 -




G:\org\HP5\dat\HP5033121_b\Review\003_MARKER_0331HP503r_DC_8015-HG-L%.xls

3.6

6

3.8

3

3.8

8

3.9

7

4.1

6

4.2

4

4.3

3

4.4

0

4.6

9

4.8

2

4.8

9

4.9

6

5.1

7

5.2

4

5.4

6

5.5

5

5.6

4

5.7

5

5.8

1

5.9

3

6.0

1

6.0

9

6.2

1

6.3

5

6.4

3

6.4

9

6.6

4

6.8

1

6.9

0

7.0

2

7.1

5

7.2

3

7.2

9

7.6

0

7.6

6

7.6

9

7.7

6

7.8

1

7.9

5

8.0

2

8.2

1

8.2

8

8.3

3

8.4

8

8.5

4

8.6

8

8.8

3

9.0

2

9.0

9

9.1

9

9.3

2

9.4

1

9.5

1

9.6

0

9.6

4

9.6

9

9.7

6

9.8

9

10.1

0

10.2

1

10.3

2

10.4

8

10.7

5

10.8

1

10.9

1

11.0

1

11.2

4

11.3

2

11.3

8

11.4

3

11.5

3

11.7

4

11.8

4

11.9

5

12.0

2

12.1

0

12.2

2

12.2

6

12.3

6

12.4

9

12.6

4

12.9

0

13.1

0

13.1

8

13.2

8

13.3

7

13.5

7

13.6

9

13.7

7

13.9

4

14.0

8

14.1

9

14.4

3

14.5

8

14.7

1

14.8

1

14.8

5

14.9

5

15.3

0

15.4

3

15.6

5

15.7

8

15.9

8

16.3

1

16.6

2

16.9

2

17.2

4

17.4

5

17.5

6

17.9

3

18.3

8

18.6

1

18.8

7

19.4

7

21.0

0

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0003.RAW MARKER_0331HP503r, DRO AK;0331HP5 , DRO210311C

4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

of 75


Sample Name: CCV_0331HP504r, DRO 8015;0331HP5 , DRO210319C









*o-Terphenyl_____________12.102 200. 322.798 161.4 -




_



TOTAL DRO________________15000. 16034.62 106.9 85-115


*o-Terphenyl_____________12.102 200. 322.798 161.4 85-115


G:\org\HP5\dat\HP5033121_b\Review\004_CCV_0331HP504r_DC_8015-HG-L%.xls

3.5

8

3.6

8

3.7

7

3.8

9

3.9

8

4.0

6

4.2

1

4.2

5

4.3

7

4.4

4

4.5

1

4.5

7

4.6

7

4.7

5

4.8

1

4.9

2

4.9

9

5.0

3

5.0

8

5.1

5

5.2

4

5.4

3

5.5

0

5.5

5

5.6

4

5.7

3

5.7

7

5.8

2

5.8

9

5.9

7

6.0

4

6.1

0 6.1

7

6.2

3

6.2

8

6.3

4

6.4

9

6.6

1

6.6

8

6.7

2

6.7

9

6.8

1

6.9

4

7.0

0

7.0

7

7.1

6

7.2

2

7.2

9

7.3

6

7.4

5

7.5

0

7.6

0

7.6

5

7.7

4

7.8

2

7.8

8 7

.95

8.0

2

8.1

1

8.2

4

8.3

3

8.3

9

8.4

4

8.5

1

8.6

3

8.6

9

8.7

5

8.8

1

8.8

7

9.0

1

9.0

7

9.1

5

9.1

8

9.3

2

9.3

9

9.4

6

9.5

6

9.7

0

9.7

7

9.9

2

10.0

5

10.1

2

10.2

1

10.3

1

10.4

0

10.4

9

10.6

0 1

0.7

5

10.8

2

10.8

7

10.9

4

11.0

3

11.1

5

11.2

0

11.2

5

11.3

4

11.4

6

11.5

4

11.5

9

11.7

5

11.8

9

11.9

6

12.0

3

12.1

0

12.1

6

12.1

9

12.3

0

12.4

4

12.4

9

12.6

7

12.7

2

12.8

1

12.9

4

13.0

6

13.1

2

13.2

0

13.2

9

13.3

7

13.5

3

13.6

2

13.7

9

13.9

4

14.0

3

14.1

9

14.2

7

14.3

3

14.4

2

14.5

7

14.7

0

14.7

9

14.9

4

15.0

6

15.1

6

15.3

0

15.4

2

15.5

1

15.6

4

15.7

6

15.8

5

15.9

8

16.2

2

16.3

1

16.4

2

16.4

9

16.6

2

16.7

0

16.9

3

17.0

4

17.2

3

17.5

5

17.9

3

18.3

6

18.8

6

20.9

7

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0004.RAW CCV_0331HP504r, DRO 8015;0331HP5 , DRO210319C

4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

7000

of 75





Method File: G:\Org\HP5\Methods\DS_8015-HG-L#.met






*o-Terphenyl_____________12.102 200. 198.652 99.33 -




_



TOTAL DRO________________15000. 8881.19 59.21 85-115


*o-Terphenyl_____________12.102 200. 198.652 99.33 85-115


G:\org\HP5\dat\HP5033121_b\Review\004_CCV_0331HP504r_DS_8015-HG-L#.xls

11.5

4

11.5

9

11.7

5

11.8

9

11.9

6

12.0

3

12.1

0

12.1

6

12.1

9

12.2

3

12.3

0

12.4

4

12.4

9

12.6

7

12.7

2

12.8

1

12.9

4

13.0

6

13.1

2

13.2

0

13.2

9

13.3

7

13.5

3

13.6

2

13.7

9

13.9

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=198.6

519

C=0.0

C

=0.0

C

=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=35.7

574

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N S

BN

SB

N

SB

N


11.6 11.8 12.0 12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

1000

2000

3000

4000

5000

6000

7000

of 75











*o-Terphenyl_____________12.094 200. .026 .01 -





3.9

9

4.0

9

4.2

7

4.3

9

4.5

8

4.6

5

4.8

0

4.8

6

4.9

2

4.9

6

5.0

2

5.0

6

5.1

1

5.1

4

5.2

0

5.3

7

5.5

4

5.5

8

5.6

6

5.7

3

5.8

7

5.9

6

6.0

4

6.4

4

6.4

7

6.9

0

7.2

9

7.3

7

7.4

6

7.6

8

8.0

8

8.3

3

8.5

5

8.7

9

8.8

4

9.3

4

9.7

1

9.8

9

10.1

4

10.5

1

12.0

9

12.3

8

12.4

9

12.7

2

12.9

4

17.8

7

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

10

20

30

40

50

60

70

80

90

100

110

120

130

140

150

of 75

Batch ID: 154020


Sample Name: LCS-154020 ;0331HP5 ,



Method File: G:\Org\HP5\Methods\D3_8015-033106-HG-L%.met






*o-Terphenyl_____________12.1 .2 .363 181.67 -




G:\org\HP5\dat\HP5033121_b\Review\006_LCS-154020_D3_8015-033106-HG-L%.xls

2.8

6

3.1

2

3.3

2

3.4

4

3.5

9

3.6

7

3.7

8

3.9

0

3.9

9

4.0

6

4.2

5

4.3

8

4.4

5

4.5

2

4.5

8

4.6

1

4.6

7

4.7

5

4.8

2

4.9

1

5.0

0

5.0

3

5.0

9

5.1

7 5.2

4

5.3

1

5.3

5

5.4

3

5.5

0 5

.56

5.6

4

5.6

7

5.7

4

5.7

7

5.8

1

5.8

9

5.9

7

6.0

2

6.0

4

6.1

0

6.1

7

6.2

4

6.2

8

6.3

4

6.3

8

6.4

3

6.4

9

6.6

1

6.6

8

6.7

2

6.7

9

6.8

2

6.9

4 6.9

9

7.0

7

7.1

6

7.2

2

7.2

4

7.2

9

7.3

6

7.4

2

7.4

5

7.5

0

7.5

8

7.6

0

7.6

5

7.7

3

7.7

6

7.8

2

7.9

5

8.0

2

8.0

7

8.1

2

8.1

7

8.2

1

8.2

4

8.2

7 8

.33

8.3

9

8.4

5 8

.51

8.5

5

8.6

3

8.6

9

8.7

4

8.8

1

8.9

0

8.9

5

9.0

1

9.0

7

9.0

9 9.1

4

9.1

8

9.2

6

9.3

2

9.3

8

9.4

6

9.4

8

9.5

5

9.5

7 9.6

2

9.6

5

9.7

0

9.7

5

9.8

1

9.9

2

9.9

7

10.0

5

10.0

8

10.1

1

10.1

9

10.2

5

10.2

9

10.4

0

10.4

9

10.6

0

10.7

5

10.8

2

10.8

7

10.9

6

11.0

3

11.1

5

11.1

9

11.2

6

11.2

9

11.3

5

11.3

9

11.4

5

11.4

8

11.5

4

11.5

9

11.6

7

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.1

6

12.2

3

12.3

1

12.3

7

12.4

2

12.4

9

12.5

7

12.6

8

12.7

7

12.8

3

12.9

1

12.9

4

13.0

1

13.1

2

13.2

1

13.2

6

13.3

8

13.5

4

13.6

3

13.6

7 13.7

9

13.8

5

13.9

4

14.0

3

14.1

9

14.2

8

14.3

3

14.4

2

14.5

7

14.7

0

14.7

9

14.9

4

15.0

7

15.1

6

15.3

0

15.4

2

15.5

1

15.6

5

15.7

6

15.8

5

15.9

8

16.0

9

16.1

8

16.3

1

16.4

1

16.6

2

16.8

5

16.9

3

17.0

0

17.0

2

17.0

3

17.0

7

17.1

2

17.1

3

17.1

7

17.2

3

17.2

9

17.3

2

17.3

9

17.4

2

17.4

4

17.5

5

17.5

6

17.6

4

17.6

6

17.7

2

17.7

5

17.8

1

17.8

3

17.8

5

17.9

3

18.0

0

18.0

3

18.0

7

18.1

4

18.1

6

18.1

8

18.2

1

18.2

2

18.3

5

18.3

6

18.3

7

18.3

9

18.4

3

18.4

5

18.4

8

18.6

1

18.7

0

18.7

3

18.7

6

18.7

7

18.7

9

18.8

0

18.8

2

18.8

8

18.9

0

18.9

1

18.9

3

18.9

4

18.9

6

18.9

8

19.0

0

19.0

1

19.0

4

19.0

9

19.1

1

19.1

3

19.1

7

19.1

8

19.2

0

19.2

1

19.2

4

19.2

5

19.2

7

19.2

9

19.3

6

19.4

1

19.4

4

19.4

8

19.5

0

19.5

1

19.5

3

19.5

5

19.5

7

19.5

8

19.6

1

19.6

2

19.6

5

19.6

7

19.6

9

19.7

1

19.7

2

19.7

4

19.7

6

19.7

7

19.7

9

19.8

2

19.8

5

19.8

8

19.9

2

19.9

5

19.9

7

19.9

8

20.0

0

20.0

2

20.0

4

20.0

6

20.0

8

20.0

9

20.1

5

20.1

7

20.1

9

20.2

2

20.2

4

20.2

6

20.3

0

20.3

2

20.3

3

20.3

5

20.3

7

20.3

9

20.4

3

20.4

5

20.4

6

20.4

8

20.4

9

20.5

0

20.5

3

20.5

5

20.5

6

20.5

8

20.6

0

20.6

3

20.6

4

20.6

6

20.7

0

20.7

2

20.7

4

20.7

7

20.7

8

20.8

0

20.8

3

20.8

5

20.8

8

20.9

1

20.9

4

20.9

5

20.9

6

20.9

8

21.0

0

21.0

1

21.0

4

21.0

7

21.0

8

21.1

0

21.1

1

21.1

3

21.1

5

21.2

0

21.2

1

21.2

3

21.2

5

21.2

8

21.3

1

21.3

2

21.3

4

21.3

7

21.4

0

21.4

2

21.4

4

21.4

5

21.4

7

21.5

0

21.5

4

21.5

5

21.5

8

21.6

0

21.6

1

21.6

4

21.6

5

21.6

6

21.7

1

21.7

4

21.7

5

21.7

9

21.8

0

21.8

2

21.8

6

21.8

8

21.9

0

21.9

2

21.9

4

21.9

9

22.0

1

22.0

2

22.0

5

22.0

6

22.0

8

22.1

3

22.1

6

22.1

9

22.2

1

22.2

3

22.2

5

22.2

8

22.2

9

22.3

0

22.3

2

22.3

4

22.3

6

22.3

7

22.3

9

22.4

3

22.4

5

22.4

9

22.5

1

22.5

3

22.5

5

22.5

9

22.6

1

22.6

3

22.6

4

22.6

8

22.7

0

22.7

2

22.7

5

22.7

7

22.7

9

22.8

1

22.8

6

22.8

7

22.8

9

22.9

2

22.9

3

22.9

5

22.9

9

23.0

1

23.0

3

23.0

5

23.0

7

23.0

9

23.1

1

23.1

3

23.1

4

23.1

8

23.2

0

23.2

2

23.2

3

23.2

4

23.2

6

23.2

7

23.2

9

23.3

1

23.3

3

23.3

4

23.3

6

23.4

0

23.4

3

23.4

4

23.4

6

23.4

7

23.5

0

23.5

2

23.5

3

23.5

5

23.5

8

23.6

2

23.6

4

23.6

6

23.6

9

23.7

2

23.7

5

23.7

8

23.7

9

23.8

1

23.8

4

23.8

7

23.8

8

23.9

0

23.9

2

23.9

4

23.9

6

23.9

7

23.9

9

24.0

0

24.0

2

24.0

4

24.0

7

24.0

8

24.1

0

24.1

3

24.1

6

24.1

9

24.2

0

24.2

2

24.2

4

24.2

5

24.2

7

24.2

8

24.3

2

24.3

4

24.3

6

24.3

7

24.3

8

24.4

0

24.4

2

24.4

7

24.4

8

24.4

9

24.5

1

24.5

3

24.5

4

24.5

7

24.5

9

24.6

1

24.6

2

24.6

4

24.6

5

24.6

7

24.6

8

24.7

0

24.7

2

24.7

5

24.7

9

24.8

3

24.8

5

24.8

7

24.9

0

24.9

2

24.9

4

24.9

6

24.9

8

25.0

1

25.0

4

25.0

6

25.0

8

25.0

9

25.1

1

25.1

3

25.1

4

25.1

6

25.1

9

25.2

1

25.2

4

25.2

5

25.2

7

25.2

9

25.3

1

25.3

2

25.3

4

25.3

6

25.3

9

25.4

3

25.4

4

25.4

8

25.5

0

25.5

2

25.5

5

25.5

7

25.5

8

25.5

9

25.6

2

25.6

4

25.6

7

25.6

9

25.7

0

25.7

5

25.7

6

25.7

8

25.8

2

25.8

4

25.8

6

25.8

8

25.9

0

25.9

2

25.9

3

25.9

6

26.0

0

26.0

2

26.0

3

26.0

7

26.1

0

26.1

3

26.1

5

26.1

7

26.1

9

26.2

1

26.2

4

26.2

5

26.2

8

26.2

9

26.3

1

26.3

4

26.3

8

26.4

0

26.4

2

26.4

6

26.4

8

26.5

1

26.5

2

26.5

4

26.5

6

26.5

8

26.6

0

26.6

2

26.6

4

26.6

6

26.6

8

26.7

0

26.7

2

26.7

4

26.7

5

26.7

8

26.8

0

26.8

3

26.8

4

26.8

7

26.9

0

26.9

5

26.9

7

27.0

0

27.0

2

27.0

5

27.0

7

27.0

9

27.1

0

27.1

2

27.1

5

27.1

7

27.1

8

27.2

0

27.2

2

27.2

4

27.2

6

27.2

8

27.3

1

27.3

5

27.3

7

27.4

0

27.4

2

27.4

4

27.4

6

27.4

8

27.5

0

27.5

1

27.5

3

27.5

5

27.5

6

27.5

9

27.6

3

27.6

6

27.6

9

27.7

1

27.7

3

27.7

8

27.8

0

27.8

3

27.8

4

27.8

7

27.8

9

27.9

0

27.9

2

27.9

4

27.9

7

27.9

9

28.0

3

28.0

5

28.0

9

28.1

1

28.1

3

28.1

6

28.2

0

28.2

4

28.2

6

28.3

1

28.3

5

28.3

8

28.4

0

28.4

3

28.4

7

28.5

1

28.5

3

28.6

3

28.7

2

28.8

3

28.8

5

28.8

9

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0006.RAW LCS-154020 ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020


Sample Name: LCS-154020 ;0331HP5 ,









*o-Terphenyl_____________12.1 .2 .215 107.31 -




G:\org\HP5\dat\HP5033121_b\Review\006_LCS-154020_DS_8015-HG-L#.xls

11.5

4

11.5

9

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.3

1

12.3

7

12.4

9

12.5

7

12.6

8

12.7

7

12.8

3

12.9

1

13.1

2

13.2

1

13.2

6

13.3

8

13.5

4

13.6

3

13.7

9

13.9

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.2

146

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.2

207

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N

SB

N

G:\org\HP5\DAT\HP5033121_b\0331HP5.0006.RAW LCS-154020 ;0331HP5 ,

11.6 11.8 12.0 12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

1000

2000

3000

4000

5000

6000

7000

of 75

Batch ID: 154020


Sample Name: MB-154020 ;0331HP5 ,









*o-Terphenyl_____________12.094 .2 .208 104.15 -




G:\org\HP5\dat\HP5033121_b\Review\007_MB-154020_DR_8015-HG-L%.xls

3.1

1

3.2

6

3.3

2

3.4

7

3.5

8

3.6

6

3.8

0

3.8

4

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

7

4.7

0

4.7

5

4.8

2

4.8

7

4.9

1

5.0

9

5.1

4

5.2

4

5.2

9

5.3

8

5.5

1

5.5

9

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

6

6.4

2

6.4

6

6.5

6

6.6

6

6.7

1

7.0

1

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.8

2

7.8

8

7.9

8

8.0

7

8.1

9

8.3

4

8.4

1

8.4

7

8.7

0

8.7

6

8.8

0

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.3

9

9.5

5

9.5

9

9.7

2

9.7

7

9.9

1

9.9

7

10.1

1

10.2

8

10.3

5

10.5

0

10.5

6

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.5

9

12.6

4

12.7

5

12.9

0

13.1

0

13.2

1

13.2

8

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.2

0

14.3

8

14.5

8

14.8

0

15.3

1

15.5

0

15.6

2

15.7

9

16.8

6

18.6

1

19.3

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0007.RAW MB-154020 ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020











*o-Terphenyl_____________12.094 .2 .208 104.15 -


(C10-C25) DRO Area:615766.9 (C10-C25) DRO Amount: 2.069672E-02 AMN 04/01/2021TEH Area:1240178 TEH Amount: 4.210082E-02

G:\org\HP5\dat\HP5033121_b\Review\007_MB-154020_DR_C10-C25-HG-L%.xls

3.1

1

3.2

6

3.3

2

3.4

7

3.5

8

3.6

6

3.8

0

3.8

4

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

7

4.7

0

4.7

5

4.8

2

4.8

7

4.9

1

5.0

9

5.1

4

5.2

4

5.2

9

5.3

8

5.5

1

5.5

9

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

6

6.4

2

6.4

6

6.5

6

6.6

6

6.7

1

7.0

1

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.8

2

7.8

8

7.9

8

8.0

7

8.1

9

8.3

4

8.4

1

8.4

7

8.7

0

8.7

6

8.8

0

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.3

9

9.5

5

9.5

9

9.7

2

9.7

7

9.9

1

9.9

7

10.1

1

10.2

8

10.3

5

10.5

0

10.5

6

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.5

9

12.6

4

12.7

5

12.9

0

13.1

0

13.2

1

13.2

8

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.2

0

14.3

8

14.5

8

14.8

0

15.3

1

15.5

0

15.6

2

15.7

9

16.8

6

18.6

1

19.3

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0007.RAW MB-154020 ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75












G:\org\HP5\dat\HP5033121_b\Review\007_MB-154020_DR_C8-C18-HG-L%.xls

3.1

1

3.2

6

3.3

2

3.4

7

3.5

8

3.6

6

3.8

0

3.8

4

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

7

4.7

0

4.7

5

4.8

2

4.8

7

4.9

1

5.0

9

5.1

4

5.2

4

5.2

9

5.3

8

5.5

1

5.5

9

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

6

6.4

2

6.4

6

6.5

6

6.6

6

6.7

1

7.0

1

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.8

2

7.8

8

7.9

8

8.0

7

8.1

9

8.3

4

8.4

1

8.4

7

8.7

0

8.7

6

8.8

0

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.3

9

9.5

5

9.5

9

9.7

2

9.7

7

9.9

1

9.9

7

10.1

1

10.2

8

10.3

5

10.5

0

10.5

6

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.5

9

12.6

4

12.7

5

12.9

0

13.1

0

13.2

1

13.2

8

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.2

0

14.3

8

14.5

8

14.8

0

15.3

1

15.5

0

15.6

2

15.7

9

16.8

6

18.6

1

19.3

1

*C

al D

iesel

C8

C18

G:\Org\HP5\DAT\HP5033121_b\0331HP5.0007.RAW MB-154020 ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

BA29552 ERH1294 Batch ID: 154020











*o-Terphenyl_____________12.094 .192 .206 107.01 -





3.0

9

3.2

5

3.3

2

3.4

6

3.5

8

3.6

6

3.7

9

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

6

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

4

5.2

7

5.3

8

5.5

1

5.5

9

5.6

4

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

3

6.4

5

6.5

5

6.6

6

6.7

4

6.9

7

7.0

0

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.7

9

7.9

7

8.1

9

8.3

3

8.4

1

8.4

6

8.6

9

8.7

6

8.8

0

8.8

4

9.0

1

9.1

0

9.2

1

9.3

2

9.3

9

9.4

2

9.5

5

9.6

6

9.7

2

9.7

7

9.9

1

9.9

9

10.0

4

10.1

0

10.2

7

10.3

6

10.5

0

10.5

6

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

1

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.6

0

12.6

4

12.7

4

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.1

9

14.3

8

14.5

7

14.8

0

14.9

5

15.3

1

15.5

0

15.6

2

15.7

8

16.2

2

16.3

2

16.6

7

16.8

6

17.3

0

17.3

3

17.4

2

17.7

5

18.1

6

18.6

1

19.2

1

20.4

8 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

BA29552 ERH1294 Batch ID: 154020











*o-Terphenyl_____________12.094 .192 .206 107.01 -


(C10-C25) DRO Area:615766.9 (C10-C25) DRO Amount: 2.069672E-02 AMN 04/01/2021TEH Area:1378570 TEH Amount: 4.499892E-02


3.0

9

3.2

5

3.3

2

3.4

6

3.5

8

3.6

6

3.7

9

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

6

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

4

5.2

7

5.3

8

5.5

1

5.5

9

5.6

4

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

3

6.4

5

6.5

5

6.6

6

6.7

4

6.9

7

7.0

0

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.7

9

7.9

7

8.1

9

8.3

3

8.4

1

8.4

6

8.6

9

8.7

6

8.8

0

8.8

4

9.0

1

9.1

0

9.2

1

9.3

2

9.3

9

9.4

2

9.5

5

9.6

6

9.7

2

9.7

7

9.9

1

9.9

9

10.0

4

10.1

0

10.2

7

10.3

6

10.5

0

10.5

6

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

1

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.6

0

12.6

4

12.7

4

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.1

9

14.3

8

14.5

7

14.8

0

14.9

5

15.3

1

15.5

0

15.6

2

15.7

8

16.2

2

16.3

2

16.6

7

16.8

6

17.3

0

17.3

3

17.4

2

17.7

5

18.1

6

18.6

1

19.2

1

20.4

8 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020













3.0

9

3.2

5

3.3

2

3.4

6

3.5

8

3.6

6

3.7

9

3.8

9

3.9

8

4.1

2

4.1

8

4.3

7

4.5

1

4.6

6

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

4

5.2

7

5.3

8

5.5

1

5.5

9

5.6

4

5.7

4

5.8

6

5.9

6

6.0

2

6.0

4

6.2

4

6.3

3

6.4

5

6.5

5

6.6

6

6.7

4

6.9

7

7.0

0

7.0

9

7.1

6

7.3

0

7.3

6

7.6

6

7.7

9

7.9

7

8.1

9

8.3

3

8.4

1

8.4

6

8.6

9

8.7

6

8.8

0

8.8

4

9.0

1

9.1

0

9.2

1

9.3

2

9.3

9

9.4

2

9.5

5

9.6

6

9.7

2

9.7

7

9.9

1

9.9

9

10.0

4

10.1

0

10.2

7

10.3

6

10.5

0

10.5

6

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.3

6

11.4

9

11.5

9

11.7

1

11.7

6

11.9

5

12.0

2

12.0

9

12.3

0

12.4

3

12.5

0

12.6

0

12.6

4

12.7

4

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

4

14.0

7

14.1

9

14.3

8

14.5

7

14.8

0

14.9

5

15.3

1

15.5

0

15.6

2

15.7

8

16.2

2

16.3

2

16.6

7

16.8

6

17.3

0

17.3

3

17.4

2

17.7

5

18.1

6

18.6

1

19.2

1

20.4

8

*C

al D

iesel

C8

C18


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020


Sample Name: B21032068-001AMS ;0331HP5 ,









*o-Terphenyl_____________12.1 .4 .702 175.56 -




G:\org\HP5\dat\HP5033121_b\Review\009_B21032068-001AMS_D3_8015-033106-HG-L%.xls

2.8

6

3.1

1

3.3

3

3.4

4

3.5

9

3.6

7

3.7

9

3.9

0

3.9

9

4.0

6

4.2

5

4.3

8

4.4

5

4.5

2

4.5

8

4.6

7

4.7

5

4.8

2

4.9

1

5.0

0

5.0

3

5.0

9

5.1

7

5.2

4

5.3

1

5.3

5

5.4

3

5.5

0 5

.56

5.6

4

5.6

7

5.7

4

5.7

7

5.8

0

5.8

9

5.9

6

6.0

2

6.0

4

6.1

0

6.1

7

6.2

4

6.2

8

6.3

4

6.3

7

6.4

3

6.4

9

6.6

1

6.6

8

6.7

2

6.7

9

6.8

2

6.9

4 6.9

9

7.0

7

7.1

6

7.2

2

7.2

4

7.2

9

7.3

6

7.4

2

7.4

5

7.5

0

7.5

8

7.6

0

7.6

5

7.7

3

7.7

6

7.8

2

7.9

5

8.0

2

8.1

1

8.1

7

8.2

1

8.2

4

8.2

7 8

.33

8.3

9

8.4

5 8

.51

8.5

5

8.6

2

8.6

9

8.7

4

8.8

0

8.9

0

8.9

5

9.0

1

9.0

7

9.0

9 9.1

4

9.1

8

9.2

6

9.3

2

9.3

8

9.4

6

9.5

5

9.5

6 9.6

2

9.6

5

9.7

0

9.7

5

9.8

1

9.9

2

9.9

7

10.0

5

10.0

8

10.1

1

10.1

9

10.2

5

10.2

9

10.4

0

10.4

9

10.6

0

10.7

5

10.8

2

10.8

7

10.9

6

11.0

2

11.1

5

11.1

9

11.2

5

11.2

9

11.3

5

11.3

9

11.4

8

11.5

4

11.5

9

11.6

8

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.1

6

12.2

3

12.3

1

12.3

7

12.4

2

12.4

9

12.5

6

12.5

7

12.6

8

12.7

7

12.8

3

12.9

1

12.9

4

13.0

1

13.1

2

13.2

1

13.2

6

13.3

7

13.5

3

13.6

3

13.6

7 1

3.7

9

13.8

5

13.9

4

14.0

4

14.0

8

14.1

9

14.2

8

14.3

3

14.4

2

14.5

7

14.7

0

14.8

0

14.9

4

15.0

6

15.1

6

15.3

0

15.4

2

15.5

1

15.6

5

15.7

6

15.8

5

15.9

8

16.0

9

16.1

8

16.2

2

16.3

1

16.4

2

16.6

2

16.7

9

16.8

2

16.8

4

16.9

3

17.0

4

17.1

1

17.2

3

17.2

8

17.3

2

17.4

4

17.4

5

17.5

6

17.6

3

17.6

5

17.6

8

17.7

1

17.7

3

17.7

4

17.8

1

17.8

4

17.9

3

18.0

1

18.0

4

18.0

6

18.1

2

18.1

8

18.2

2

18.2

4

18.2

8

18.2

9

18.3

0

18.3

3

18.3

5

18.3

7

18.3

9

18.4

1

18.4

4

18.4

7

18.4

8

18.6

1

18.7

1

18.7

4

18.7

6

18.7

9

18.8

2

18.8

4

18.8

6

18.8

9

18.9

1

18.9

4

18.9

6

18.9

9

19.0

1

19.0

3

19.0

6

19.1

7

19.2

0

19.2

4

19.2

5

19.2

9

19.3

9

19.4

1

19.4

4

19.4

8

19.5

1

19.5

3

19.5

5

19.5

9

19.6

1

19.6

3

19.6

5

19.6

6

19.6

8

19.7

0

19.7

4

19.7

6

19.7

9

19.8

0

19.8

2

19.8

7

19.8

9

19.9

1

19.9

4

19.9

5

19.9

9

20.0

0

20.0

2

20.0

5

20.0

9

20.1

1

20.1

2

20.1

4

20.1

7

20.1

8

20.2

0

20.2

3

20.2

4

20.2

5

20.2

7

20.2

9

20.3

2

20.3

5

20.3

7

20.4

1

20.4

3

20.4

4

20.4

6

20.4

8

20.5

0

20.5

2

20.5

3

20.5

5

20.5

7

20.6

0

20.6

3

20.6

5

20.6

7

20.6

8

20.7

1

20.7

5

20.7

8

20.8

0

20.8

2

20.8

3

20.8

6

20.9

0

20.9

2

20.9

3

20.9

5

20.9

7

20.9

9

21.0

1

21.0

4

21.0

6

21.1

1

21.1

5

21.1

7

21.1

9

21.2

1

21.2

3

21.2

6

21.3

0

21.3

2

21.3

4

21.3

6

21.3

8

21.3

9

21.4

1

21.4

4

21.4

6

21.4

8

21.4

9

21.5

0

21.5

2

21.5

4

21.5

7

21.5

9

21.6

0

21.6

3

21.6

4

21.6

5

21.6

7

21.7

1

21.7

2

21.7

6

21.7

7

21.8

0

21.8

1

21.8

5

21.8

7

21.8

8

21.9

0

21.9

1

21.9

3

21.9

5

21.9

7

22.0

0

22.0

6

22.0

8

22.1

0

22.1

1

22.1

4

22.1

5

22.1

7

22.1

9

22.2

1

22.2

3

22.2

5

22.2

8

22.3

0

22.3

3

22.3

5

22.3

9

22.4

4

22.4

5

22.4

8

22.5

1

22.5

2

22.5

5

22.5

7

22.6

0

22.6

1

22.6

3

22.6

4

22.6

6

22.6

7

22.6

9

22.7

0

22.7

2

22.7

5

22.7

8

22.7

9

22.8

2

22.8

5

22.8

6

22.8

7

22.8

9

22.9

2

22.9

4

22.9

5

22.9

8

22.9

9

23.0

1

23.0

3

23.0

4

23.0

7

23.0

8

23.1

1

23.1

3

23.1

7

23.1

9

23.2

0

23.2

3

23.2

4

23.2

6

23.2

9

23.3

1

23.3

3

23.3

4

23.3

5

23.3

7

23.3

9

23.4

0

23.4

2

23.4

5

23.4

8

23.5

0

23.5

3

23.5

4

23.5

7

23.5

9

23.6

2

23.6

5

23.6

7

23.7

0

23.7

2

23.7

4

23.7

6

23.7

8

23.8

0

23.8

2

23.8

3

23.8

5

23.8

9

23.9

1

23.9

3

23.9

5

23.9

8

24.0

1

24.0

3

24.0

5

24.0

8

24.1

0

24.1

2

24.1

4

24.1

5

24.1

7

24.1

8

24.1

9

24.2

2

24.2

5

24.2

6

24.2

8

24.3

0

24.3

2

24.3

3

24.3

5

24.3

8

24.4

0

24.4

1

24.4

2

24.4

6

24.4

9

24.5

1

24.5

3

24.5

5

24.5

7

24.5

9

24.6

0

24.6

2

24.6

4

24.6

6

24.6

8

24.6

9

24.7

1

24.7

3

24.7

5

24.7

7

24.8

0

24.8

2

24.8

4

24.8

6

24.8

6

24.8

9

24.9

0

24.9

2

24.9

4

24.9

4

24.9

6

24.9

8

25.0

0

25.0

3

25.0

5

25.0

6

25.0

8

25.1

0

25.1

1

25.1

4

25.1

6

25.1

7

25.1

8

25.2

0

25.2

2

25.2

4

25.2

5

25.2

9

25.3

0

25.3

2

25.3

3

25.3

6

25.3

8

25.3

9

25.4

2

25.4

3

25.4

6

25.4

9

25.5

2

25.5

5

25.5

7

25.5

9

25.6

1

25.6

2

25.6

4

25.6

8

25.7

0

25.7

1

25.7

3

25.7

5

25.7

7

25.8

0

25.8

2

25.8

6

25.8

7

25.8

9

25.9

1

25.9

4

25.9

5

25.9

8

26.0

0

26.0

2

26.0

4

26.0

7

26.0

8

26.1

0

26.1

2

26.1

5

26.1

6

26.1

7

26.1

9

26.2

1

26.2

3

26.2

5

26.2

7

26.2

8

26.3

0

26.3

2

26.3

3

26.3

5

26.3

9

26.4

2

26.4

3

26.4

5

26.4

6

26.4

7

26.5

0

26.5

2

26.5

4

26.5

6

26.5

9

26.6

1

26.6

2

26.6

4

26.6

7

26.6

8

26.7

0

26.7

2

26.7

4

26.7

6

26.7

9

26.8

0

26.8

3

26.8

5

26.8

7

26.8

9

26.9

1

26.9

2

26.9

6

26.9

8

26.9

9

27.0

1

27.0

3

27.0

4

27.0

6

27.0

7

27.0

9

27.1

1

27.1

2

27.1

5

27.1

6

27.1

9

27.2

1

27.2

3

27.2

5

27.3

0

27.3

1

27.3

6

27.3

8

27.4

0

27.4

4

27.4

6

27.4

8

27.5

1

27.5

2

27.5

5

27.5

7

27.6

1

27.6

4

27.6

5

27.6

8

27.7

0

27.7

2

27.7

4

27.7

6

27.7

8

27.8

0

27.8

2

27.8

5

27.8

7

27.9

0

27.9

2

27.9

7

27.9

8

28.0

2

28.0

5

28.0

7

28.1

0

28.1

3

28.1

6

28.1

9

28.2

5

28.2

7

28.2

9

28.3

1

28.4

1

28.4

4

28.4

8

28.5

2

28.5

5

28.6

3

28.6

6

28.6

9

28.8

0

28.8

9

28.9

3

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0009.RAW B21032068-001AMS ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020


Sample Name: B21032068-001AMS ;0331HP5 ,









*o-Terphenyl_____________12.1 .4 .421 105.23 -




G:\org\HP5\dat\HP5033121_b\Review\009_B21032068-001AMS_DS_8015-HG-L#.xls

11.5

4

11.5

9

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.3

1

12.3

7

12.4

9

12.6

8

12.7

7

12.8

3

12.9

1

13.1

2

13.2

1

13.2

6

13.3

7

13.5

3

13.6

3

13.7

9

13.9

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.4

209

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.4

524

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N

SB

N

G:\org\HP5\DAT\HP5033121_b\0331HP5.0009.RAW B21032068-001AMS ;0331HP5 ,

11.6 11.8 12.0 12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

1000

2000

3000

4000

5000

6000

7000

of 75

Batch ID: 154020


Sample Name: B21032068-001AMSD ;0331HP5 ,









*o-Terphenyl_____________12.101 .4 .729 182.31 -




G:\org\HP5\dat\HP5033121_b\Review\010_B21032068-001AMSD_D3_8015-033110-HG-L%.xls

2.8

6

3.1

1

3.3

2

3.4

4

3.5

9

3.6

7

3.7

9

3.9

0

3.9

9

4.0

6

4.2

5

4.3

8

4.4

4

4.5

2

4.5

8

4.6

7

4.7

5

4.8

2

4.9

1

5.0

0

5.0

3

5.0

9

5.1

7

5.2

4

5.3

1

5.3

5

5.4

3

5.5

0 5

.56

5.6

4

5.6

7

5.7

4

5.7

7

5.8

1

5.8

9

5.9

6

6.0

2

6.0

4

6.1

0

6.1

7

6.2

4

6.2

8

6.3

4

6.3

7

6.4

3

6.4

9

6.6

1

6.6

8

6.7

2

6.7

9

6.8

2

6.9

4 6.9

9

7.0

7

7.1

6

7.2

2

7.2

4

7.2

9

7.3

6

7.4

2

7.4

5

7.5

0

7.6

0

7.6

5

7.7

3

7.7

6

7.8

2

7.9

5

8.0

2

8.1

2

8.1

7

8.2

1

8.2

4

8.2

7 8

.33

8.3

9

8.4

5 8

.51

8.5

5

8.6

3

8.6

9

8.7

4

8.8

1

8.9

0

8.9

5

9.0

1

9.0

7

9.0

9 9.1

4

9.1

8

9.2

6

9.3

2

9.3

8

9.4

6

9.5

5

9.5

7 9

.62

9.6

5

9.7

0

9.7

5

9.8

1

9.9

2

9.9

7

10.0

5

10.0

8

10.1

1

10.1

9

10.2

5

10.2

9

10.4

0

10.4

9

10.6

0

10.7

5

10.8

2

10.8

7

10.9

6

11.0

3

11.1

5

11.1

9 11.2

5

11.2

9

11.3

5

11.3

8

11.4

7

11.5

4

11.5

9

11.6

8

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.1

6

12.2

3

12.3

1

12.3

6

12.4

2

12.5

0

12.5

6

12.6

8

12.7

7

12.8

3

12.9

1

12.9

4

13.0

1

13.1

2

13.2

1

13.2

6

13.3

8

13.5

3

13.6

3

13.6

8 13.7

9

13.8

5

13.9

4

14.0

3

14.1

9

14.2

7

14.3

3

14.4

2

14.5

7

14.7

0

14.8

0

14.9

4

15.0

7

15.1

6

15.3

0

15.4

2

15.5

1

15.6

5

15.7

6

15.8

5

15.9

8

16.0

9

16.1

8

16.3

1

16.4

1

16.6

2

16.7

0

16.8

1

16.8

5

16.9

3

17.0

4

17.1

1

17.2

3

17.3

3

17.4

4

17.5

5

17.5

6

17.6

5

17.7

1

17.7

3

17.9

2

18.0

3

18.0

5

18.1

4

18.1

7

18.2

0

18.2

9

18.3

2

18.3

4

18.3

7

18.4

0

18.4

7

18.4

9

18.5

1

18.6

1

18.7

7

18.7

9

18.8

2

18.8

4

18.8

6

18.8

8

18.9

1

18.9

5

18.9

6

18.9

8

19.0

1

19.1

5

19.1

7

19.1

8

19.2

0

19.2

6

19.2

8

19.3

1

19.3

5

19.3

7

19.4

0

19.4

2

19.4

3

19.4

5

19.4

8

19.4

9

19.5

1

19.5

4

19.5

6

19.5

9

19.6

0

19.6

3

19.6

6

19.6

9

19.7

4

19.7

7

19.7

8

19.8

1

19.8

2

19.8

5

19.8

8

19.9

5

19.9

7

19.9

9

20.0

2

20.0

3

20.0

5

20.0

8

20.1

0

20.1

2

20.1

4

20.1

7

20.2

0

20.2

3

20.2

5

20.2

9

20.3

1

20.3

4

20.3

6

20.3

9

20.4

0

20.4

2

20.4

4

20.4

6

20.4

8

20.5

1

20.5

3

20.5

7

20.6

0

20.6

2

20.6

5

20.6

8

20.7

1

20.7

2

20.7

5

20.7

7

20.8

0

20.8

3

20.8

5

20.8

7

20.8

9

20.9

1

20.9

3

20.9

6

20.9

8

21.0

0

21.0

2

21.0

5

21.0

7

21.2

0

21.2

6

21.3

2

21.3

4

21.4

0

21.4

5

21.4

9

21.5

2

21.5

6

21.5

8

21.6

1

21.6

3

21.6

5

21.6

8

21.7

0

21.7

3

21.7

6

21.7

9

21.8

1

21.8

3

21.8

5

21.8

7

21.9

1

21.9

3

21.9

8

21.9

9

22.0

2

22.0

4

22.0

9

22.1

5

22.1

8

22.1

9

22.2

4

22.2

7

22.2

9

22.3

2

22.3

4

22.3

8

22.4

1

22.4

5

22.4

7

22.5

2

22.5

4

22.5

9

22.6

3

22.6

6

22.6

8

22.6

9

22.7

1

22.7

5

22.7

7

22.8

0

22.8

1

22.8

4

22.8

8

22.9

2

22.9

5

22.9

6

22.9

8

23.0

1

23.0

4

23.0

7

23.1

1

23.1

2

23.1

5

23.1

7

23.2

0

23.2

2

23.2

3

23.2

7

23.3

0

23.3

2

23.3

4

23.3

8

23.4

1

23.4

4

23.4

8

23.5

1

23.5

4

23.5

6

23.5

9

23.6

2

23.6

4

23.6

6

23.6

8

23.6

9

23.7

2

23.7

4

23.7

6

23.8

0

23.8

3

23.8

6

23.8

9

23.9

1

23.9

3

23.9

8

24.0

1

24.0

3

24.0

6

24.0

9

24.1

3

24.1

5

24.1

7

24.1

8

24.2

2

24.2

5

24.2

7

24.3

0

24.3

5

24.3

6

24.3

8

24.4

3

24.4

6

24.4

8

24.5

0

24.5

3

24.5

7

24.6

1

24.6

4

24.6

5

24.6

7

24.7

0

24.7

4

24.7

5

24.7

7

24.7

9

24.8

0

24.8

3

24.8

5

24.8

8

24.8

9

24.9

1

24.9

4

24.9

7

24.9

9

25.0

2

25.0

4

25.0

9

25.1

1

25.1

4

25.1

7

25.1

8

25.2

0

25.2

1

25.2

2

25.2

5

25.2

9

25.3

1

25.3

4

25.3

6

25.3

8

25.4

2

25.4

5

25.4

6

25.4

8

25.5

1

25.5

2

25.5

5

25.5

7

25.6

0

25.6

2

25.6

4

25.6

6

25.6

8

25.7

1

25.7

4

25.7

5

25.7

7

25.7

9

25.8

1

25.8

2

25.8

8

25.9

1

25.9

5

25.9

7

25.9

9

26.0

3

26.0

5

26.0

7

26.0

9

26.1

4

26.1

6

26.1

8

26.2

1

26.2

2

26.2

4

26.2

8

26.3

2

26.3

4

26.3

5

26.3

7

26.4

0

26.4

3

26.4

5

26.4

6

26.4

8

26.4

9

26.5

1

26.5

4

26.5

7

26.5

9

26.6

1

26.6

2

26.6

6

26.6

9

26.7

0

26.7

4

26.8

0

26.8

2

26.8

4

26.8

6

26.8

8

26.9

1

26.9

3

26.9

6

26.9

9

27.0

1

27.0

4

27.0

6

27.1

0

27.1

1

27.1

4

27.1

8

27.2

1

27.2

3

27.2

5

27.3

1

27.3

4

27.3

5

27.3

8

27.4

1

27.4

5

27.4

8

27.5

0

27.5

2

27.5

4

27.5

8

27.6

2

27.6

5

27.6

8

27.6

9

27.7

1

27.7

5

27.7

7

27.7

9

27.8

1

27.8

5

27.8

8

27.9

2

27.9

6

28.0

1

28.0

4

28.0

6

28.0

8

28.1

0

28.1

4

28.1

8

28.2

0

28.2

2

28.2

5

28.3

1

28.3

8

28.4

0

28.4

3

28.4

7

28.4

8

28.5

4

28.5

7

28.5

9

28.6

1

28.6

6

28.7

0

28.7

5

28.7

8

28.8

7

28.9

0

28.9

6

28.9

8

29.1

8

29.2

5

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0010.RAW B21032068-001AMSD ;0331HP5 ,

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020


Sample Name: B21032068-001AMSD ;0331HP5 ,









*o-Terphenyl_____________12.101 .4 .437 109.28 -




G:\org\HP5\dat\HP5033121_b\Review\010_B21032068-001AMSD_DS_8015-HG-L#.xls

11.5

4

11.5

9

11.7

5

11.8

4

11.8

9

11.9

4

12.0

3

12.1

0

12.3

1

12.3

6

12.5

0

12.6

8

12.7

7

12.8

3

12.9

1

13.1

2

13.2

1

13.2

6

13.3

8

13.5

3

13.6

3

13.7

9

13.9

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.4

371

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.4

673

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N

SB

N

G:\org\HP5\DAT\HP5033121_b\0331HP5.0010.RAW B21032068-001AMSD ;0331HP5 ,

11.6 11.8 12.0 12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

1000

2000

3000

4000

5000

6000

7000

of 75











*o-Terphenyl_____________12.096 200. .017 .01 -





4.0

9

4.3

6

4.5

2

4.6

2

4.7

5

4.7

8

4.8

2

4.8

7

4.9

3

5.0

6

5.1

4

5.1

9

5.2

5

5.3

3

5.3

8

5.5

1

5.5

8

5.6

8

5.7

4

5.8

8

5.9

7

6.0

2

6.0

4

6.4

5

6.4

8

6.5

9

6.6

4

7.2

8

7.3

3

7.4

0

7.4

8

7.6

9

7.9

3

8.0

1

8.1

0

8.2

3

8.3

4

8.6

1

8.7

3

8.8

4

9.0

3

9.1

0

9.2

3

9.3

4

9.4

8

9.5

9

9.7

8

9.8

9

10.2

2

10.2

9

10.5

0

10.8

4

12.1

0

12.3

9

12.5

0

12.7

3

12.8

5

13.0

8

17.4

7

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

10

20

30

40

50

60

70

80

90

100

110

120

130

140

150

of 75

BA29553 ERH1295 Batch ID: 154020











*o-Terphenyl_____________12.095 .198 .209 105.76 -





3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

BA29553 ERH1295 Batch ID: 154020











*o-Terphenyl_____________12.095 .198 .209 105.76 -


(C10-C25) DRO Area:615766.9 (C10-C25) DRO Amount: 2.069672E-02 AMN 04/01/2021TEH Area:3019305 TEH Amount: 0.1014827


3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1 D

RO

Range S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

Batch ID: 154020













3.2

6

3.3

3

3.5

9

3.6

7

3.8

2

4.0

2

4.1

2

4.2

1

4.3

8

4.5

1

4.6

2

4.7

5

4.8

2

4.8

7

4.9

1

5.0

8

5.1

4

5.2

7

5.3

4

5.5

1

5.5

8

5.7

0

5.7

5

5.8

6

5.9

6

6.0

2

6.0

5

6.2

4

6.3

7

6.4

5

6.5

3

6.5

6

6.6

6

6.7

1

6.7

4

6.8

1

6.8

7

6.9

7

7.0

1

7.0

9

7.1

5

7.3

0

7.3

6

7.5

7

7.6

1

7.6

6

7.7

5

7.8

4

7.9

3

7.9

7

8.0

7

8.1

4

8.3

3

8.4

1

8.4

7

8.6

5

8.7

0

8.7

6

8.8

4

8.9

9

9.1

0

9.2

2

9.3

2

9.4

2

9.5

6

9.5

9

9.6

7

9.7

2

9.7

8

9.8

8

9.9

1

10.0

0

10.0

4

10.1

0

10.2

6

10.3

6

10.5

0

10.5

7

10.6

5

10.7

5

10.8

2

10.9

1

11.0

1

11.1

2

11.2

0

11.2

8

11.3

3

11.4

5

11.5

2

11.5

9

11.6

5

11.7

6

11.9

5

12.0

2

12.0

9

12.1

8

12.2

2

12.3

0

12.4

3

12.4

9

12.6

0

12.6

5

12.9

0

13.1

1

13.2

1

13.2

7

13.4

6

13.5

7

13.7

0

13.7

7

13.9

7

14.0

7

14.1

9

14.3

0

14.3

8

14.5

7

14.7

9

14.9

5

15.0

2

15.3

2

15.5

0

15.6

3

15.6

8

15.7

8

16.2

2

16.6

7

16.8

6

17.3

2

17.4

5

18.6

1

*C

al D

iesel

C8

C18


0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

6000

of 75

G:\

org

\HP

5\d

at\

HP

50

33

12

1_

b\R

evi

ew

\01

3_

MA

RK

ER

_0

33

1H

P5

13

r_C

SC

21

03

31

.xls

0.8

4

0.9

2

1.0

1

1.0

4

1.1

0

1.2

0

1.2

2

1.2

4

1.3

8

1.5

3

1.6

2

1.8

5

2.1

1

2.1

9

2.3

3

2.5

0

2.6

9

3.1

0

3.4

2

3.5

3

3.8

3

3.9

0

3.9

9

4.1

7

4.2

2

4.2

5

4.2

7

4.3

8

4.5

0

4.8

8

5.0

3

5.4

6

5.5

6

6.0

4

6.1

4

6.2

4

6.4

3

6.4

9

6.6

9

6.8

1

6.8

9

6.9

7

7.0

4

7.1

5

7.2

9

7.3

8

7.6

6

7.6

9

7.7

5

7.8

1

7.8

5

8.0

2

8.0

5

8.2

5

8.3

2

8.3

6

8.4

8

8.5

9

8.7

0

8.8

3

8.9

4

9.0

3

9.1

4

9.3

2

9.4

1

9.5

5

9.6

0

9.6

5

9.7

0

9.9

2

10

.06

1

0.1

8

10

.21

1

0.3

2

10.4

8

10

.72

1

0.8

2

11

.02

1

1.1

7

11

.25

1

1.2

8

11.3

8

11

.53

1

1.6

6

11

.71

1

1.7

4

11

.86

1

2.0

2

12.2

2

12.2

6

12

.36

1

2.4

9

12

.77

1

2.8

2

12

.94

1

3.1

2

13.1

6

13

.26

1

3.3

8

13

.53

1

3.6

9

13

.79

1

3.9

3

14

.19

1

4.4

3

14

.58

1

4.8

0

14.8

5

14

.95

1

5.1

7

15

.31

1

5.5

2

15

.65

1

5.8

0

15

.82

1

5.9

9

16.1

9

16

.31

1

6.5

1

16

.62

1

6.9

3

17.0

8

17.2

3

17.5

7

17.9

3

18

.38

1

8.6

0

18.8

8

19

.48

20.1

8

20.5

0

21.0

2

21

.46

21.9

8

22.4

8

23.3

7

c-5

c-6

c-7

c-8

c-9

c-1

0

c-1

1

c-1

2

c-1

3

c-1

4

c-1

5

c-1

6

c-1

7

c-1

8

c-1

9

c-2

0

c-2

1

c-2

2

c-2

3

c-2

4

c-2

5

c-2

6

c-2

7

c-2

8

c-2

9

c-3

0

c-3

2

c-3

4

c-3

6

c-3

8

c-4

0

G:\

org

\HP

5\D

AT

\HP

50

331

21

_b\0

33

1H

P5

.00

13.R

AW

MA

RK

ER

_0

33

1H

P51

3r,

CS

CA

N ;

03

31H

P5

, D

RO

21

02

04A

05

00

10

00

15

00

20

00

250

03

000

35

00

40

00

45

00

500

05

500

60

00

65

00

70

00

0 2 4 6 8

10

12

14

16

18

20

22

24

26

28

30

of 75


Sample Name: MARKER_0331HP514r, DRO AK;0331HP5 , DRO210311C









*o-Terphenyl_____________12.095 .2 .216 108.19 -




G:\org\HP5\dat\HP5033121_b\Review\014_MARKER_0331HP514r_DC_8015-HG-L%.xls

3.6

6

3.8

8

3.9

6

4.0

4

4.1

6

4.2

3

4.3

6

4.4

6

4.6

9

4.8

2

4.8

9

4.9

4

4.9

6

5.1

7

5.2

4

5.4

6

5.5

5

5.6

3

5.8

0

5.9

3

6.0

1

6.0

9

6.2

1

6.3

0

6.4

3

6.4

9

6.6

4

6.8

1

6.9

0

7.0

2

7.1

5

7.2

3

7.2

9

7.6

5

7.7

6

7.8

1

8.0

1

8.2

7

8.3

2

8.4

8

8.5

4

8.6

8

8.8

3

9.0

2

9.0

9

9.1

9

9.3

2

9.4

1

9.5

0

9.6

4

9.6

9

9.7

6

9.8

9

10.1

0

10.2

1

10.3

1

10.4

8

10.7

5

10.8

2

10.9

1

11.0

1

11.2

4

11.3

2

11.3

8

11.4

3

11.5

3

11.7

4

11.8

4

11.9

5

12.0

2

12.0

9

12.2

2

12.2

6

12.3

6

12.4

9

12.6

4

12.9

0

13.1

0

13.1

8

13.2

8

13.3

7

13.6

9

13.7

7

13.9

4

14.0

8

14.1

9

14.4

3

14.5

8

14.7

1

14.8

0

14.8

5

14.9

4

15.3

0

15.4

3

15.6

5

15.7

8

15.9

8

16.3

1

16.6

2

16.9

2

17.0

4

17.5

5

17.9

3

18.3

7

18.6

0

18.8

7

19.4

6

20.9

9

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd

G:\org\HP5\DAT\HP5033121_b\0331HP5.0014.RAW MARKER_0331HP514r, DRO AK;0331HP5 , DRO210311C

4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

of 75











*o-Terphenyl_____________12.101 200. 328.872 164.44 -




_



TOTAL DRO________________15000. 16347.83 108.99 85-115


*o-Terphenyl_____________12.101 200. 328.872 164.44 85-115


G:\org\HP5\dat\HP5033121_b\Review\015_CCV_0331HP515r_DC_8015-HG-L%.xls

3.5

8

3.6

8

3.7

8

3.9

0

3.9

9

4.0

6

4.2

5

4.3

7

4.4

4

4.5

2

4.5

8

4.6

7

4.7

5

4.8

1

4.9

2

4.9

9

5.0

3

5.0

8

5.1

5

5.2

4

5.4

3

5.5

0

5.5

5

5.6

4

5.7

3

5.7

7

5.8

2

5.8

9

5.9

7

6.0

4

6.1

0 6.1

7

6.2

3

6.2

8

6.3

4

6.4

9

6.6

1

6.6

8

6.7

2

6.7

9

6.8

1

6.9

4

7.0

0

7.0

7

7.1

6

7.2

2

7.2

9

7.3

6

7.4

5

7.5

0

7.6

0

7.6

5

7.7

4

7.8

2

7.9

5

8.0

2

8.1

1

8.2

4

8.3

3

8.3

9

8.4

4

8.5

1

8.6

3

8.6

9

8.7

5

8.8

0

8.8

7

9.0

1

9.0

7

9.1

5

9.1

8

9.3

2

9.3

9

9.4

6

9.5

5

9.7

0

9.7

7

9.9

2

10.0

5

10.1

2

10.2

0

10.3

1

10.4

0

10.4

9

10.6

0 1

0.7

5

10.8

2

10.8

7

11.0

2

11.1

5

11.1

9

11.2

5

11.3

4

11.4

6

11.5

4

11.5

9

11.6

8

11.7

5

11.8

9

11.9

6

12.0

3

12.1

0

12.1

6

12.1

9

12.3

0

12.4

4

12.4

9

12.6

7

12.7

2

12.8

1

12.9

4

13.0

5

13.1

2

13.2

0

13.2

9

13.3

7

13.5

3

13.6

2

13.7

8

13.9

4

14.0

4

14.1

8

14.2

7

14.4

1

14.5

7

14.7

0

14.7

9

14.9

4

15.0

6

15.1

5

15.3

0

15.4

1

15.5

1

15.6

4

15.7

6

15.8

5

15.9

8

16.2

3

16.3

1

16.4

2

16.4

9

16.6

2

16.7

0

16.9

3

17.0

3

17.2

2

17.5

5

17.9

3

18.3

6

19.1

4

19.4

5

20.9

7

DR

O R

ange S

tart

*o-T

erp

henyl

*1-C

hlo

roocta

decane

DR

O R

ange E

nd


4 6 8 10 12 14 16 18 20 22

0

1000

2000

3000

4000

5000

6000

7000

of 75











*o-Terphenyl_____________12.101 200. 202.409 101.2 -




_



TOTAL DRO________________15000. 9048.29 60.32 85-115


*o-Terphenyl_____________12.101 200. 202.409 101.2 85-115


G:\org\HP5\dat\HP5033121_b\Review\015_CCV_0331HP515r_DS_8015-HG-L#.xls

11.5

4

11.5

9

11.6

8

11.7

5

11.8

9

11.9

6

12.0

3

12.1

0

12.1

6

12.1

9

12.3

0

12.4

4

12.4

9

12.6

7

12.7

2

12.8

1

12.9

4

13.0

5

13.1

2

13.2

0

13.2

9

13.3

7

13.5

3

13.6

2

13.7

8

13.9

4

*o-T

erp

henyl

*1-C

hlo

roocta

decane

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=202.4

086

C=0.0

C

=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=35.5

124

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

C=0.0

SB

N

SB

N

SB

N

SB

N


11.6 11.8 12.0 12.2 12.4 12.6 12.8 13.0 13.2 13.4 13.6 13.8 14.0

0

1000

2000

3000

4000

5000

6000

7000

of 75

Data File Sample Name Method Weight Dil Factor Amt Inj. IS Cal ID Manual Integrations

G:\org\HP5\DAT\HP5033121_b\0331HP5.01r DCM-Baseline Check-01 G:\Org\HP5\Methods\DR_8015-HG-LEXP.met 1 1 1 1 0 No integration

G:\org\HP5\DAT\HP5033121_b\0331HP5.02r MARKER_0331HP502r, CSCAN ;0331HP5 , DRO210204A g:\org\HP5\Methods\\CSC210331.met 1 1 1 1 0 No integration

G:\org\HP5\DAT\HP5033121_b\0331HP5.03r MARKER_0331HP503r, DRO AK;0331HP5 , DRO210311C G:\Org\HP5\Methods\DC_8015-HG-L%.met 1000 1 1 1 0 No integration


G:\Org\HP5\Methods\DS_8015-HG-L#.met

1 1 1 1 0

The integration of Diesel Range Organics and Total Extractable

Hydrocarbons is the hydrocarbon response with reference to the

basline. Assigned Set Baseline All Valley on at 16.27.

Surrogates are integrated using a valley to valley integration using Set

Basline Now placed slight before at 12.01 and slightly after the surrogate

peak at 12.23 and scaling showing surrogate peak from 11.5-14.


G:\org\HP5\DAT\HP5033121_b\0331HP5.06r LCS-154020 ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033106-HG-L%.met


1000 1 1 1 0



basline. Peak width adjusted.




G:\org\HP5\DAT\HP5033121_b\0331HP5.07r MB-154020 ;0331HP5 , G:\Org\HP5\Methods\DR_8015-HG-L%.met



The integration of Diesel Range Organics, Total Extractable Hydrocarbons,

C8-C18 range, C10-C25 range is the hydrocarbon response with reference to

the basline.






the basline.

G:\org\HP5\DAT\HP5033121_b\0331HP5.09r B21032068-001AMS ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033106-HG-L%.met


500 1 1 1 0







G:\org\HP5\DAT\HP5033121_b\0331HP5.10r B21032068-001AMSD ;0331HP5 , G:\Org\HP5\Methods\D3_8015-033110-HG-L%.met


500 1 1 1 0













the basline.

G:\org\HP5\DAT\HP5033121_b\0331HP5.13r MARKER_0331HP513r, CSCAN ;0331HP5 , DRO210204A g:\org\HP5\Methods\\CSC210331.met 1 1 1 1 0 No integration

G:\org\HP5\DAT\HP5033121_b\0331HP5.14r MARKER_0331HP514r, DRO AK;0331HP5 , DRO210311C G:\Org\HP5\Methods\DC_8015-HG-L%.met 1000 1 1 1 0 No integration



1 1 1 1 0



basline. Assigned Set Baseline All Valley on at 16.27.





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