analytical report 6 · page 5 of 15 6/16/2016 1 2 3 4 5 6 7 8 9 10 11 12 procedure hdp-pr-qa-006,...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-17741-1Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

For:Westinghouse Electric Company LLC3300 State Road PFestus, Missouri 63028

Attn: Mr. Martin Swanson

Authorized for release by:6/16/2016 4:33:49 PMRhonda Ridenhower, Manager of Project [email protected] forIvan Vania, Project Manager II(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of ContentsClient: Westinghouse Electric Company LLCProject/Site: HDP RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-17741-1

of 15TestAmerica St. Louis

6/16/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

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Case NarrativeClient: Westinghouse Electric Company LLC TestAmerica Job ID: 160-17741-1Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-17741-1

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Westinghouse Electric Company LLC

Project: HDP RFP-CBA-022 (7 DAY TAT)

Report Number: 160-17741-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data

have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the

client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT

The sample was received on 6/9/2016 11:30 AM; the sample arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 3.4º C.

TECHNETIUM-99 (ICPMS)Sample L09-02-06-P-E-S-00 (160-17741-1) was analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A.

The samples were prepared on 06/13/2016 and analyzed on 06/14/2016.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDS

Sample L09-02-06-P-E-S-00 (160-17741-1) was analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 06/10/2016.

Batch 255888:

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Case NarrativeClient: Westinghouse Electric Company LLC TestAmerica Job ID: 160-17741-1Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-17741-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

The following samples could not be thoroughly homogenized before sub-sampling was performed due to sample matrix:

L09-02-06-P-E-S-00 (160-17741-1) and (160-17741-A-1 DU). The sample was very fine powder and small rocks.

Batch 255888:

Percent Moisture exceeded the RPD limit for the duplicate of sample 160-17741-1. The initial result was 20.9 % moisture and the duplicate result was 13.6 % moisture yielding an RPD of 42% (30%).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)Sample L09-02-06-P-E-S-00 (160-17741-1) was analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE

GA-01-R. The samples were dried on 06/09/2016, and prepared and analyzed on 06/10/2016.

Preparation Batch 160-256004:

Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. L09-02-06-P-E-S-00 (160-17741-1), (LCS 160-256004/2-A), (MB 160-256004/1-A) and (160-17741-A-1-D DU)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.


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Procedure HDP-PR-QA-006, Chain of Custody

Page 1 of! Hematite Decommissioning Project !Revision: 4 I I Westinghouse Non-Proprietary Class 3

FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY

Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that !he sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-060916-01 Pa!!e 111 Project Name:

Westinghouse Electric Company

Contact Person: Clark Evers

Phone Number: 314-810-3336 Sampler Name John Michel

Sample ID Date Time !Matrix

L09-02-06-P-E-S-OO 5/2712016 14:40 I s

Relinquished by: ~

Company Name: VJ·C.C-

Received bv:

Company Name:

~~15

Date/Time

(,,.,.-ct-1-t.c c'ioo

Date/Time

Date/Time

0...-cz - (p \\ · -~~

Company Name:

Laboratory Name: TA-MO

Laboratory Address: 13715 Rider Trail North

~ 1--~~~~~~~~~~~~~~~~~~--t ·§ PhoneNo. 8 314-298-8566 ]I Laboratory Contact Person: ~ Ivan Vania

Phone No. 708-870-8453

Turn Around Time Rush (7 days)

Remarks l ILSA09-02

1l Hill II \~ I l l 11 II 160-177 41 Ch;;1in of Custody

--,.d<'-- ---------1

Total I Cooler Temperatun::: 1 Ambient

Cooler ID: I Shipper and Number: 0608-01

Date/Time I Comments: NIA

Verified By:

Login Sample Receipt Checklist

Client: Westinghouse Electric Company LLC Job Number: 160-17741-1

Login Number: 17741

Question Answer Comment

Creator: Dedner, Connie L

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Definitions/GlossaryTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC

Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Qualifiers

Rad

Qualifier Description

U Result is less than the sample detection limit.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

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Method SummaryTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Method Method Description LaboratoryProtocol

SW8466020A Metals (ICP/MS), Tc-99 TAL SL

EPAMoisture Percent Moisture TAL SL

SW8466020A Metals (ICP/MS), Tc-99 in Activity TAL SL

DOEGA-01-R Cesium-137 & Other Gamma Emitters (GS) TAL SL

Protocol References:

DOE = U.S. Department of Energy

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


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Sample SummaryTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-17741-1 L09-02-06-P-E-S-00 Solid 05/27/16 14:40 06/09/16 11:30


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Client Sample ResultsTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Lab Sample ID: 160-17741-1Client Sample ID: L09-02-06-P-E-S-00Matrix: SolidDate Collected: 05/27/16 14:40

Date Received: 06/09/16 11:30

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte

Actinium 228 0.953

(2σ+/-)

0.147

(2σ+/-)

106/10/16 17:0206/10/16 13:50pCi/g0.0696

RL MDC

0.111

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

pCi/g 06/10/16 13:50 06/10/16 17:02 10.1520.09170.0916U-0.0347Americium 241

pCi/g 06/10/16 13:50 06/10/16 17:02 10.3440.4340.4111.33Bismuth 212

pCi/g 06/10/16 13:50 06/10/16 17:02 10.05530.1080.08080.693Bismuth 214

pCi/g 06/10/16 13:50 06/10/16 17:02 10.05090.1450.06411.01Lead 212

pCi/g 06/10/16 13:50 06/10/16 17:02 10.07180.1190.07960.848Lead 214

pCi/g 06/10/16 13:50 06/10/16 17:02 10.2982.000.99816.9Potassium 40

pCi/g 06/10/16 13:50 06/10/16 17:02 11.880.3550.355U0.000Protactinium 231

pCi/g 06/10/16 13:50 06/10/16 17:02 10.05531.000.1080.08080.693Radium 226

pCi/g 06/10/16 13:50 06/10/16 17:02 10.6501.000.4420.4261.15Thorium 234

pCi/g 06/10/16 13:50 06/10/16 17:02 10.4580.1310.131U0.0531Uranium 235

pCi/g 06/10/16 13:50 06/10/16 17:02 16.783.833.83U2.38Protactinium 234m

pCi/g 06/10/16 13:50 06/10/16 17:02 10.06960.1470.1110.953Thorium 232

Tl-208 0.337 0.0447 0.0567 0.0327 pCi/g 06/10/16 13:50 06/10/16 17:02 1

(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Lab Sample ID: 160-17741-1Client Sample ID: L09-02-06-P-E-S-00Matrix: SolidDate Collected: 05/27/16 14:40

Percent Solids: 79.1Date Received: 06/09/16 11:30

Method: 6020A - Metals (ICP/MS), Tc-99RL MDL

Technetium 99 0.00026 0.000068 0.000021 mg/Kg ☼ 06/13/16 09:12 06/14/16 15:49 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity

Analyte

Technetium 99 4.38

(2σ+/-)

0.432

(2σ+/-)

106/14/16 15:4906/13/16 09:12pCi/g0.2341.37

RL MDC

0.155

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

06/13/16 09:12 06/14/16 15:49 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

92


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QC Sample ResultsTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Method: 6020A - Metals (ICP/MS), Tc-99

Client Sample ID: Method BlankLab Sample ID: MB 160-256106/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256398 Prep Batch: 256106

RL MDL

Technetium 99 ND 0.000053 0.000016 mg/Kg 06/13/16 09:12 06/14/16 15:40 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-256106/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256398 Prep Batch: 256106

Technetium 99 0.00119 0.00121 mg/Kg 102 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: L09-02-06-P-E-S-00Lab Sample ID: 160-17741-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256398 Prep Batch: 256106

Technetium 99 0.00026 0.00150 0.00178 mg/Kg 101 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: L09-02-06-P-E-S-00Lab Sample ID: 160-17741-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256398 Prep Batch: 256106

Technetium 99 0.00026 0.00150 0.00172 mg/Kg 97 75 - 125 3 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity


Technetium 99

Analyte

U 106/14/16 15:4006/13/16 09:12pCi/g0.181

MDC

1.05

RL

0.02180.0210

(2σ+/-) (2σ+/-)

MB

0.06321

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total

Carrier

Re 30 - 110 06/13/16 09:12 06/14/16 15:40 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

95

MB MB


Technetium 99

Analyte

120-8010220.7420.4 1.94 1.05 0.180

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

LCS

Qualifier Limits%Yield

95

LCS


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Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: L09-02-06-P-E-S-00Lab Sample ID: 160-17741-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256399 Prep Batch: 256106

Technetium 99

Analyte

125-7510130.4225.74.38 2.91 1.43 0.244

RL MDC(2σ+/-)

MS MS

pCi/g


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

MS


89

MS

Client Sample ID: L09-02-06-P-E-S-00Lab Sample ID: 160-17741-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256399 Prep Batch: 256106

Technetium 99

Analyte

10.18125-759729.4025.74.38 2.74 1.40 0.239

RL MDC(2σ+/-)

MSD MSD

pCi/g

UnitResult Qual %Rec LimitAdded

Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

RER

RER

Re

Carrier

30 - 110

MSD


91

MSD

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)


Actinium 228

Analyte

U 106/12/16 17:1906/10/16 13:50pCi/g0.0559

MDCRL

0.03050.0305

(2σ+/-) (2σ+/-)

MB

0.01254

MB


Uncert.

Count

Uncert.

Total

106/12/16 17:1906/10/16 13:50pCi/g0.02700.01820.0182U-0.004577Americium 241

106/12/16 17:1906/10/16 13:50pCi/g0.3090.07180.0718U-0.01231Bismuth 212

106/12/16 17:1906/10/16 13:50pCi/g0.08060.06510.0651U-0.01247Bismuth 214

106/12/16 17:1906/10/16 13:50pCi/g0.02120.01260.0126U0.006006Lead 212

106/12/16 17:1906/10/16 13:50pCi/g0.05510.03400.0339U-0.02222Lead 214

106/12/16 17:1906/10/16 13:50pCi/g0.3220.2380.238U0.03194Potassium 40

106/12/16 17:1906/10/16 13:50pCi/g0.6430.2700.270U0.1069Protactinium 231

106/12/16 17:1906/10/16 13:50pCi/g0.08061.000.06510.0651U-0.01247Radium 226

106/12/16 17:1906/10/16 13:50pCi/g0.2401.000.07640.0760U0.07467Thorium 234

106/12/16 17:1906/10/16 13:50pCi/g0.1370.06100.0609U-0.03246Uranium 235

106/12/16 17:1906/10/16 13:50pCi/g4.340.4660.466U0.0000Protactinium 234m

106/12/16 17:1906/10/16 13:50pCi/g0.05590.03050.0305U0.01254Thorium 232

Other Detected

Radionuclide

None

MB

(2σ+/-) (2σ+/-) MDCRL

pCi/g 06/10/16 13:50 06/12/16 17:19 1

MB


Uncert.

Count

Uncert.

Total

Radionuclides

Other Detected


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Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)


Americium 241

Analyte

116-879999.57101 10.4 0.492

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Cesium 137 33.9 32.90 3.44 0.200 0.158 pCi/g 97 87 - 120

Cobalt 60 30.9 29.58 2.98 0.120 pCi/g 96 87 - 115

Client Sample ID: L09-02-06-P-E-S-00Lab Sample ID: 160-17741-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 256042 Prep Batch: 256004

Actinium 228

Analyte

10.171.0050.953 0.162 0.145

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

Americium 241 -0.0347 U -0.04368 U 0.110 0.183 pCi/g 0.04 1

Bismuth 212 1.33 1.348 0.432 0.350 pCi/g 0.02 1

Bismuth 214 0.693 0.8010 0.144 0.0852 pCi/g 0.43 1

Lead 212 1.01 1.014 0.154 0.0673 pCi/g 0.03 1

Lead 214 0.848 0.7945 0.120 0.0754 pCi/g 0.23 1

Potassium 40 16.9 18.57 2.33 0.259 pCi/g 0.38 1

Protactinium 231 0.000 U -0.5237 U 1.67 2.79 pCi/g 0.26 1

Radium 226 0.693 0.8010 0.144 1.00 0.0852 pCi/g 0.43 1

Thorium 234 1.15 1.184 0.581 1.00 0.889 pCi/g 0.04 1

Uranium 235 0.0531 U 0.08394 U 0.204 0.340 pCi/g 0.09 1

Protactinium

234m

2.38 U 3.552 U 5.26 9.54 pCi/g 0.13 1

Thorium 232 0.953 1.005 0.162 0.145 pCi/g 0.17 1

Tl-208 10.010.33820.337 0.0718 0.0492

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

RER

RER

Total

Other Detected

Radionuclides


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QC Association SummaryTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Metals

Prep Batch: 256106

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid None160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid None160-17741-1 MS L09-02-06-P-E-S-00 Total/NA

Solid None160-17741-1 MSD L09-02-06-P-E-S-00 Total/NA

Solid NoneLCS 160-256106/2-A Lab Control Sample Total/NA

Solid NoneMB 160-256106/1-A Method Blank Total/NA

Analysis Batch: 256398


Solid 6020A 256106160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid 6020A 256106160-17741-1 MS L09-02-06-P-E-S-00 Total/NA

Solid 6020A 256106160-17741-1 MSD L09-02-06-P-E-S-00 Total/NA

Solid 6020A 256106LCS 160-256106/2-A Lab Control Sample Total/NA

Solid 6020A 256106MB 160-256106/1-A Method Blank Total/NA

General Chemistry

Analysis Batch: 255888


Solid Moisture160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid Moisture160-17741-1 DU L09-02-06-P-E-S-00 Total/NA

Rad

Leach Batch: 255856


Solid Dry and Grind160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid Dry and Grind160-17741-1 DU L09-02-06-P-E-S-00 Total/NA

Prep Batch: 256004


Solid Fill_Geo-0 255856160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid Fill_Geo-0 255856160-17741-1 DU L09-02-06-P-E-S-00 Total/NA

Solid Fill_Geo-0LCS 160-256004/2-A Lab Control Sample Total/NA

Solid Fill_Geo-0MB 160-256004/1-A Method Blank Total/NA

Prep Batch: 256106


Solid None160-17741-1 L09-02-06-P-E-S-00 Total/NA

Solid None160-17741-1 MS L09-02-06-P-E-S-00 Total/NA

Solid None160-17741-1 MSD L09-02-06-P-E-S-00 Total/NA

Solid NoneLCS 160-256106/2-A Lab Control Sample Total/NA

Solid NoneMB 160-256106/1-A Method Blank Total/NA


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Tracer/Carrier SummaryTestAmerica Job ID: 160-17741-1Client: Westinghouse Electric Company LLC


Method: 6020A - Metals (ICP/MS), Tc-99 in ActivityPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-110)

Re

92160-17741-1

Percent Yield (Acceptance Limits)

L09-02-06-P-E-S-00

89160-17741-1 MS L09-02-06-P-E-S-00

91160-17741-1 MSD L09-02-06-P-E-S-00

95LCS 160-256106/2-A Lab Control Sample

95MB 160-256106/1-A Method Blank

Tracer/Carrier Legend

Re = Re


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analytical report 6 · page 5 of 15 6/16/2016 1 2 3 4 5 6 7 8 9 10 11 12 procedure hdp-pr-qa-006,...

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