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NET FD Case 1856 Inorganics
Cambridge Division NATIONAL 12 Oak Park Bedforo MA 01730 ENVIRONMENTAL Tel (6171 275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TIME DATE ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 K8542 05201996 1315 05211996 GROUND WATER
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M ConroyProject Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
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I 5
M
CLF flF tur r
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0002
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Ddte Fec a i PU C-5
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1 i Igt J 0
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1 ltbull
I r
1
i tio c i
1
1
1
I
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Nshy
N
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hi
1 1 v
j (
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L
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1
h t
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i bull gt lt -
ni bull i
L 1 1 d 4 j i
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1 i
1
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-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
_t HP
I J 1 lt_ r X a t
No jEI
Lab i (4i2
Date Rec
LI
IN
IN
it M
4 J a shy
M r-l
- J jr
l e t
ore
er
CLfAR
CLEAR
T shy1 ft u reshy
0002
- C DATA SHEET
Lfr No GET G No
Lab Sample- j u - 14
Date Rr-iHC t-5
Ur iJ--5 dr-ij weight) U
f i
-
CLEAR Texture
i-LiuiL r u r CLFAR Artifact-
- u KR-gtTON
Cji I-T a l
ilaquoI ci 5AI No GEI SOL Ho
ul ~ i c CO F - TR
C bull shy TI i u bullbull a a 11 b r 3 bull r conci F gt i ) o
1 rr
1
1 1 1 bull bull
Nfc
1 1HR
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1
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90-110
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if-l
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mdash mdash - mdash mdash trade
( NK UK
Mr i i if
i INK IN- i
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ug t
CRDL E Initial
Gun
M lt I-lt bull SA-t No LgtEI 5Dj Ho
r k ~_ n ^r I r Ugt shy L or m g k g gt l-G L
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3 i ICi Prep L
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C
riiolt r i ci n
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i MR
^iT1
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i HP
raquo t Kl 1
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gt i i
IiiGj 0
ELr - - -
Contract
5n5 No GEI
j -mishy lt ori hr shy J shy C L or
G 11 inv - i 0 A f 10 fi
i ) r repa
bull n
NK MF KR r i F
- 1 pound
i NP MF
INK IN
bull HK p IH-
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INFshyIMP
I-R HF i NR
J---03 0
0009
ii rac t
jbullgt_ f- -_ -t 5 Ho CEI r o i5o-
S Source LFEt1ltN
ugL
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fi -E
gt - l l - pound
T - -ct
3 ho uEI
-- bull f W-VrT iievel do reoj _ y
1 bullbdquo bull - C shy y
V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
bull H
nr
i HF-
- 1
MR NR
bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
i rx
| MF
MR US
NF HF
NFgt
J
ltbullbull- Si gt-= HU
HO pound bull
Lew I ^ ] ~j td LL U
builds for Dopi - --bull 0 0
dTM| ISlOh ^ LI L
1T3
TV r
tK
r bullMR
HK UK
ltpoundL oAHrLE
Con t rac t
5AS No GEI iLj No
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2deg013
shy bdquo 11J I
c)i N c ^ _ - C ft3 Ho GET
^ u IC shy ii t I1 J s ugL
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ICTI At CUN AES
iLL IOhshy
gt
bull
NJ
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tr bullbull
-H-1
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Mo
Uli
GEI
Legte l
shy I bull
(Ishy
c er _ e
r i r
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bull II1IT3 (QUARTERLY
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IDL 1 L Q 1
200 i f i
0 i - 60 10
200 HR -gt 1 NK
3 1 T4X
5000 bullbull 30 irrlt
u L
100 15 0 bull 3 MR
50iU IMF-Jh bull Mft
o shy f-r-1
bulltO NK 50-0 Mr1
10 SR
10 W fO
iR
X -U H -I r ft EL 50 ICF
Ib n03 0
0016
1 - SJpoundgt EL--I NT L^-U TON FACTORS ltANNlA__
if
_ bull shy - r shy
-bullbull r
- r _
bull
EI LHK-DH
Ciishy rC
19
r-11-1
Cor- t rac t
SM- No
D c t r
GEI
04C-J95
ri A- j~igt
In f j re l rr
Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
t f ip t - j ) bull bull - - i - [ft I03 0
1 - -i
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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1 I
3 1 t bullt ugD H i
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HP NFshy
W
INK
iMR INK 1
f U Il-i 100 0
PF-T bull-bull ltN LOO
Contract bull
5AS No GEI
Ueight Moiure (gram) raquo ifiL )
05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
0 c LI
F f- PI
E pound G
H IM N K s A bull i bull r v z c U G i E bullbull- L N H
ii
lt
1 lt i
t i
-i
ii
ti
-I 2 i i bull l i i i bull bull i i i i
-1A i i t t _ bull -1 l 1 t i 1 1 1 1
gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
f
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l i
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x i bull 1 1 l 1 I
i t
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l - t -
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1
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1
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bull 1
i
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i
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t
1 i
i
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bull
i
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1 i
i
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1 i
i
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i
i
1
l r
i
I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
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t
1 1
1 bull
t
1 1
I 1
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i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
omm
ents
0 Ortn O Hshy
bull0 0 laquoa
Q 0 0 rr 0
rum rt-ts a o
A
on -fshy
a
f-
Iar iP s Oo M
r V i
I 3 -n
O 2=
(A tc IL
n
IS
o
i
_0 c PY
c C
01 en vt eo
laquoD bullO
00 ft 9
HS OO
H a
00Mr DO o
X
CO ltet O O
O 3 H-JS
0 O
M0
o rt o n a ~
ff O rrn 0 Hshy
930 c a D
O
-nJT
11 U 0 O n o
ocn ^ c BJ ortn 0 lt an-
n
H obullo 03 ft 0 S
a m
I
I
Sshy 0
9 ft O
otn ht Ca-o B) O
bull0tni lt (Dbullo
5 ltQHshyo
o o 3 II
C
0
ID
Stan
dard
vA
1 CD
Mft OO
bullr
00 ltrt 0 0 h-O
O 3
Sif bull0 n 0
Fin
al cone C
omm
ents i
olt0gt 0rfi raquoO H bullbull
shy
Hshy900 C 0 tv
c IS CD
D B ft ft
ma iB O m
0
i fl
vor O
yen 1shy
r~r^r T -
T
T
T -D C bull4)
T CN
cv
laquogtraquo
i lt ^
i
lt3
6
AQ o 0 rt O
bull0tonF lt obullu
09
H3 oa 0
CO Hft OO
O 9
00
0 3
OB
28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
t
io9deg~l-raquoS13o 1 7E7mdash 1-43ES7 -t shy rmdashl fmdash r-i i HOCO
1 H opoundS7F S 1 HoEdo 1 ~4 O Cl O i TOpound mdash 1 -i-CE-cshy1 HOpound^ -[_bullLiJV B 1H3E93 1 HoE99 1 HboOO 1 HO~deglHoHOtmdash 1 Ho~lHbHOo 17Homdash lHtaH7 1 tomdash 1 HCHOS 17HOmdash lHgHO7
rgtLK
u 1 7o mdash I HSH3o 1 oOmdash 1 H3n87 j oOmdash L H3n3o J ^ oO~lHoHO 17oOmdash IHOH-U 1771-1H35H1 1771-1H85HE
1 HoH^OFS bLK UCV pound1
1i 3SS8 l-t-5150 1 i-8pound9l l-iopound37 1 HopoundS7SE 1 -tSES7F 3
^ 1
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5 E5 11
1 1 JL
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1-)1 i 1 i
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pound 5 1 1
EO IO
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30 101 J
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i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t
I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X
Ul- bW O
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513 1-4C3
~i jr- i O
S3E11
3-7 EE5E EEoo pound55^ 34 3 d oo 3s 7o c ^lt-~ E7 1
- 9E icbo
V 3-+79 onS1 1 o37 EO 1 7 = bull41- C c5Eo iooo o 1 o 3-i- -^ raquoccoO
O 1317
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^bull43 1 359
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1 jo 835 ^c 1 1 c 1 V poundS HO ^shy
5 19o vshy37n39u
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i 7 i 1 oH V4 4 r-iC7 - i j c Ushy1 1 E9o L1 1 77lt_ pound7 Ho7
b 9oE ^ 59^0113 33pound59S-49 ^1
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1 OH o7n ^x HH003 UshyOOH51 U
-raquo C y JOH U^ 7 on7 Ushy8796^
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mdash
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mdash
~shy
mdash
mdash
shy-1C 53 OH crcshy
5su Oo 5deg sO 01 =c OO on o5 00 o7 OO
1 H-bc-bV 1 -+opound9o 1 --4opound97 BLr LCV
1 H oE93 1 4 O f~ ~ ^ tradet 0400 1 ~ o--oc5E i HC^V on poundj plusmn 1--CJ4O
i H O H f c j i C3C
1 M Oto7|- S
1 bullshy O--^O
poundgt_bullbull
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pound5 pound5
oVgt poundo 1 O
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j 1
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1 1 11 i 1i i ^ i i 1
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i_ 1 376 887
113E C1 bull 7 Io53
oo
1E15 E5C1 ^ bull
0 15o5
tv
0S oi t
ta
Vlgt
CH ^JOC x ~gt 1CT OH OCO n5 ooo ^
vj O51 V u pound pound60 lO--1 O o3 1 ~^u
58EH3V 37 999
IIOHpoundH v V 1 pound bull49-t r y]1 3deg HpoundE v Llt (gt 11 OOb 17Ho3 0 poundoo33 It O
pound17 ooo v ltj oG 12= OHO
bdquo
~v 71 ~c
^~+ ~3 7o
73 79
1 -fO-401^
raquo shy O5
i -i oS^-t i i -40OM-E 1 4tTshy
I --to -t raquoF c 1 shy1 O-t -bullbull T 3 bL
Imdash mdashE
pound5 oo [j1 o ^ L o mdash L Zio
_^ 1
rf 1i 1 1i 1 ^ 1
1 5to EoaV
onE 1 OoO ipound7 E OOO-4 O-O
1 L 3 SiT mdash bull
Vy
n =
OCj
oSEBl EE5 copound
3o o7c 1 O7 1 7-t EEo E ~3E5cE3cEZ=ooo
^ bull J C ~E oH i ) Si
n i^
r-^ a J v 7
lampjC ^- ^ J9
70011
_
CL
V sr
4 c
7001
laquoplaquofiy- Analysis EPA 300 0
Analyts
Analyst
ICVCCV True value
Job No Samle No 1
Labsys Batch
Data 0 60 -$amp
Page
A03 JL02
5shy | alaquoi i 0 20
Recovery
0oLG
O-2 G
00
41 6b svampygg OZo
loolamp
amp06V
0
0020 20020
lt
y z
Z
pound0010 I o fLy
L CO-7O
0
701 p
f I i LE
uPtRti FuJR ~Mpound v
bdquobdquobdquo 11 7E7mdash 1 M-OEB9 i-rSsea 1+SSS7_
15 1-+SE90 is-poundE9q1 bull- tgtc 9
17s-omdash1 7ot_mdash ELL bull-v
n i T 4 J
i
1
1
1
1
1
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iiiiii
ii4
i
ii
i
iiii
iiii
i11iii11iiiiiii i1
it-j n ~3opoundH
t ON
657 139u 3M-3-
(1 -t -S
O oo OgtZl
1poundpound 1 pound 1
rshy155
M-Mshy~~ ^J
3-f bull_
1 5poundoi j
5 ( E5E
11 HS 31 1^
555 bull45 19
151HC3
t sect H-6
1 f~~
3(1 j5ob pound7 SMshy
73O l_laquo ltJ
i 5o3bull i Jt-So
BOH lt_
1515i_j
t- v I Zgt
v O-o
bull_ OOMshy
O pound 1 9 u ()gt+
J 1 o O
bullJ i 1 O
o au bull_gt u i s v uov
^ ~~ ~ v raquodu r
G lt i1
bull UU5
d loOS u oGo
U I G1 O GOo U G 1 O u poundpoundpound
O i
bdquo 006 O uO3 U bull -j I 9 u ltgt 1 3 uulo J Oil 0 i j9G oGn u poundpoundG O -jOt o Oipound u lpoundt u m Jt_gtlaquo-f
bdquo poundpoundpound
(bull
kr
N _
S
7001
X
I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
irfd l ~n MKHl O M H 0^4
amp4l t^q OM^
iff 5^2 u 7^ bull ^ d$ poundLf IW- o5l HZ bull
ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
^ tiamp 1HA 7f-^ 1C1 710 (03^
I m-T
IHfraquo7 4S IX m ia 1^7 1 3 5JS U1 Ift ^ l 7Y lv Ll-S ID 21-T- Ga1 13
11 i1 2-X 41 ^ MM ltpound IX 1 11 3^5 4x TII 5H JJ SifV M 5^ SiM
W OX S3 r-4 c j9 H05 11 1 tfl bullH3 2 ltClaquo- an ( 3 ^u 3 KH 22
$7 Z
Z1V bull2H v li i XS gt-l ii G 7 IX 21-1 i Ift | ^-S 2J 22 1gtU n
3co 21 i Ill lUttgtlaquo^ i 1 Cdfc U $o $c c|
c^v t-^s ^f U-f KUftr
bull 21 pound)( St Zl U5 Ji y$gt (p 45^ ^1 l-C IX 1JJ US tfH B1 7f^ 15
i UlTK z-c L ]R I amp4 )7 raquo^1 15 Wfc L-t IX Iftl t-r a5 X is
i qlt^ H| 1 WH 7 1 laquo1 ^ IS
l IX ^ lok MlH HlG gtW iW 7rtit
r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
ooX Vn
230
1
I c o U
ou
nd
O-j
90 laquo3
VA Ni 1 11 1 31 11 1
a E
laquo^ i
c8 ii
gt mdashbulln a mdash E D bull in bull
9
abulli
Ui
Ebull a 3
3-1 O XT
O 0shyUI 4
U O
E 0 C 3 3
c C 3 3
a
r O c 3 Si Zraquo to vo
O- ashyM U) 3- 2Cr- CXS 0 C 0 3 r mdashS
0deg pound rva V3T C3- cr cr a E3 r taj
NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
bullbull
2
s -s
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1)
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g 5
Cambridge Division NATIONAL 12 Oak Park Bedforo MA 01730 ENVIRONMENTAL Tel (6171 275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TIME DATE ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 K8542 05201996 1315 05211996 GROUND WATER
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M ConroyProject Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
-1 I (1 r r ( t
u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
I
o r-r
Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
h t
- 1
- t
~
i bull gt lt -
ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
i
t
I
rshy
^ Hshyr
i
h
iN j
N
N 1-4
4f
r-NT
M
(N
N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
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No jEI
Lab i (4i2
Date Rec
LI
IN
IN
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er
CLfAR
CLEAR
T shy1 ft u reshy
0002
- C DATA SHEET
Lfr No GET G No
Lab Sample- j u - 14
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Ur iJ--5 dr-ij weight) U
f i
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CLEAR Texture
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90-110
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IFt
ugL
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bull i-ir-
bull bull HF
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CRDL E Initial
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11 15 0 LI raquo v bull F bull Mi
i MR
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Contract
5n5 No GEI
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G 11 inv - i 0 A f 10 fi
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NK MF KR r i F
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bull HK p IH-
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V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
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nr
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bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
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NF HF
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IDL 1 L Q 1
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SM- No
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GEI
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In f j re l rr
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bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
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[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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5AS No GEI
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05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
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c c i c o A R
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ii
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gt -11 i bull
xY~ t J
l
1
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1
I I
1
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1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
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l 1
1 1 1
A i i 11 l i
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l I t
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f
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A __ 1 _ 1 i bull l bull
x i bull 1 1 l 1 I
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bull 1
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bull
t
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1
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bull i bull i
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1
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1
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1 I I 1 1 t I
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1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
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bull X i t 1I
bullt
i
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l 1
1
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t 1
i j i bullbull 1 raquo t bull t 1t
1 1
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1 t
1 1
1 1
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11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
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1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
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1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
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ents
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
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531
73
bullI] 11AO
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0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
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^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
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3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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1727
la
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If
776
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701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
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602
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bull47 505i
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Analyts
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Labsys Batch
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I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
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ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
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r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
ooX Vn
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M ConroyProject Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
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CLF flF tur r
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0002
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u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
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U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
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1
1
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N
N1
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hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
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ni bull i
L 1 1 d 4 j i
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1
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-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
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v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
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20001
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Lfr No GET G No
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Ur iJ--5 dr-ij weight) U
f i
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5n5 No GEI
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V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
bull H
nr
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MR NR
bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
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NF HF
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19
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Cor- t rac t
SM- No
D c t r
GEI
04C-J95
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In f j re l rr
Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
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H1 E3 J O N C n n L r a c t
- Sraquo t iZsc 5Af No GLI I no
D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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HP NFshy
W
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f U Il-i 100 0
PF-T bull-bull ltN LOO
Contract bull
5AS No GEI
Ueight Moiure (gram) raquo ifiL )
05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
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ii
lt
1 lt i
t i
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ti
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gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
f
i l I I
l i
A __ 1 _ 1 i bull l bull
x i bull 1 1 l 1 I
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l - t -
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bull 1
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1
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bull i bull i
1
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1
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1
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1
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1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
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1 I
X ii i 1 ) l
1 bull
1 1
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1 I
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bullt
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l 1
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bull 1
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1 laquo gt
i 1 gt
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1 1
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x 11 t 4
1 1
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1 t
1 1
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1 1
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i r lt t i l X ii igt 1t
1 1
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1 1
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1 1 i i t tgt raquoi 11 i
( 1
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1 1
t 1
1 1
1 t
gt 1
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t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
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-
-
-
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-
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- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
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0 0271501 10120 476 0084L 0008
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K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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la
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776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
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pound^l 0^ J zx 3fO
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pur ^^fc -oZGgt 50
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Analyst Date Labsys Batch Supervisor
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0010 Standard Stock No
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
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-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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t- - - b e- i - tb
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Int r i e l^ rcTi - o t re^ t ion Factors fcr
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0-gt 0 0000000 o oo^oooo 000000
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FGRh XI lt F - c v pound gt - IN
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Contract
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1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
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HS
20044
2
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n a
r 0 0 5-bull -
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r IT m n
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^
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m o oD n
u
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r
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r C
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03
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pound c
a o
s laquoQ
0)laquoa n
01
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ro ltampbullmdash
bulla a n c a o
s i r
u
O
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_ -o
8 Jraquo
(I
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II
r Ji
^
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CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
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a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
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m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
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bullflO H-0
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3 O rr O m
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^
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O
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3
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amdash
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lt 0gt bullO
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Q
O 3
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ft O
Bgt 0gt
ngt OHshy
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
-1 I (1 r r ( t
u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
I
o r-r
Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
h t
- 1
- t
~
i bull gt lt -
ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
i
t
I
rshy
^ Hshyr
i
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N
N 1-4
4f
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M
(N
N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
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bull dfit- vJohri pound tlotbleshy
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Gun
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ICTI At CUN AES
iLL IOhshy
gt
bull
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tr bullbull
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100 15 0 bull 3 MR
50iU IMF-Jh bull Mft
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GEI
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Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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Contract bull
5AS No GEI
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05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
0 c LI
F f- PI
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H IM N K s A bull i bull r v z c U G i E bullbull- L N H
ii
lt
1 lt i
t i
-i
ii
ti
-I 2 i i bull l i i i bull bull i i i i
-1A i i t t _ bull -1 l 1 t i 1 1 1 1
gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
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l i
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bull
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l r
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i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
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t
1 1
1 bull
t
1 1
I 1
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i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
omm
ents
0 Ortn O Hshy
bull0 0 laquoa
Q 0 0 rr 0
rum rt-ts a o
A
on -fshy
a
f-
Iar iP s Oo M
r V i
I 3 -n
O 2=
(A tc IL
n
IS
o
i
_0 c PY
c C
01 en vt eo
laquoD bullO
00 ft 9
HS OO
H a
00Mr DO o
X
CO ltet O O
O 3 H-JS
0 O
M0
o rt o n a ~
ff O rrn 0 Hshy
930 c a D
O
-nJT
11 U 0 O n o
ocn ^ c BJ ortn 0 lt an-
n
H obullo 03 ft 0 S
a m
I
I
Sshy 0
9 ft O
otn ht Ca-o B) O
bull0tni lt (Dbullo
5 ltQHshyo
o o 3 II
C
0
ID
Stan
dard
vA
1 CD
Mft OO
bullr
00 ltrt 0 0 h-O
O 3
Sif bull0 n 0
Fin
al cone C
omm
ents i
olt0gt 0rfi raquoO H bullbull
shy
Hshy900 C 0 tv
c IS CD
D B ft ft
ma iB O m
0
i fl
vor O
yen 1shy
r~r^r T -
T
T
T -D C bull4)
T CN
cv
laquogtraquo
i lt ^
i
lt3
6
AQ o 0 rt O
bull0tonF lt obullu
09
H3 oa 0
CO Hft OO
O 9
00
0 3
OB
28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
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Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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Tr HOEN X
+ o~l IOH cr
LU N^ ~i i
CO
cr
jipbull i
O^
^
UI cc lt dWOO
z D lt N 8VUO bullyi gt XZ
XIH1VW 0 2co O o LL u
(PR
INT
NA
ME
) raquo
SIG
NA
TU
RE
^UJ LU cr 2 QD
O cr cr 3 SiQ CL
|oiI 0 O ^ ^H 0LU
FIE
LD F
ILT
ER
ED
Y
ES
N
O
gt s kiit 0 1 i^
LJ Nj
S lilh gtt p fy^ LU rr
C cr gt bullgtv
V) 0 bull0
CO ^s 0 o LU 1
en i - 0 UJ gt
li 2 C^
P O ^Sj amp pr^ It O CO UJ
UJ
sect bull
|
CO
j ^ N)
u rgtshy
$ ^ V lt LU
bullv bullDr ^shy C-JN
bullv
H
copy V
^ CL
^ UJ 15 lt Vbull5 co
bull 8 1 ^g
m gt^ gt LL omIf l
bulla 5 S ltsect - Xs10 0p suT ^shy^vj
UJ lti
_i shy 0 A1^^ IHH fN
CO
ND
I
Ifgt z UJ rh-W^ f Vrlt llt z d z m gtr ^ UJ
Klt Q 00 ^bull
1
opound LLJ W O LLJ LLJ gt cre c- ^ fm
C
fe Z U j
i_ Q ifa ^ 3 sectshy
PO
V tl s rshy
$1 LJJ O I- IB
z c
o o tr
bulls X s o0
t-N Vi)
(mdash laquo
ky- I
cc LLJ D z lt LLJ CC
lt UJ
x
Is ss c^I- c-O D lt UJ
0 P OC Z LU
LL s g y
I fQl
lt w
raquo LL o -i o
H Q
O
Sidd olt I- LLccO LLJ UJ Q t3
12glaquoUJ Q
SeSEw
zw uj
poundE D =gt O
lt C3 O Q W O LT LLJ Q Z lt
LLJ Lt LLJ
lt W
^j I
c g
^Sshy
LLJ
D
CO LL
4O O o X
UJ
^
c
g 5
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples required analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
-1 I (1 r r ( t
u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
I
o r-r
Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
h t
- 1
- t
~
i bull gt lt -
ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
i
t
I
rshy
^ Hshyr
i
h
iN j
N
N 1-4
4f
r-NT
M
(N
N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
_t HP
I J 1 lt_ r X a t
No jEI
Lab i (4i2
Date Rec
LI
IN
IN
it M
4 J a shy
M r-l
- J jr
l e t
ore
er
CLfAR
CLEAR
T shy1 ft u reshy
0002
- C DATA SHEET
Lfr No GET G No
Lab Sample- j u - 14
Date Rr-iHC t-5
Ur iJ--5 dr-ij weight) U
f i
-
CLEAR Texture
i-LiuiL r u r CLFAR Artifact-
- u KR-gtTON
Cji I-T a l
ilaquoI ci 5AI No GEI SOL Ho
ul ~ i c CO F - TR
C bull shy TI i u bullbull a a 11 b r 3 bull r conci F gt i ) o
1 rr
1
1 1 1 bull bull
Nfc
1 1HR
1 UloO -^ Ill 0 t O i v - bullbdquo- I- bull ^
i HR 1 nR HR
IF HP
bull 1
1
1
t
1
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90-110
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bull I
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if-l
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mdash mdash - mdash mdash trade
( NK UK
Mr i i if
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ug t
CRDL E Initial
Gun
M lt I-lt bull SA-t No LgtEI 5Dj Ho
r k ~_ n ^r I r Ugt shy L or m g k g gt l-G L
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bull i 1 1 1 i t i l
3 i ICi Prep L
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riiolt r i ci n
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bull I I I I
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i MR
^iT1
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raquo t Kl 1
i KR i w
gt i i
IiiGj 0
ELr - - -
Contract
5n5 No GEI
j -mishy lt ori hr shy J shy C L or
G 11 inv - i 0 A f 10 fi
i ) r repa
bull n
NK MF KR r i F
- 1 pound
i NP MF
INK IN
bull HK p IH-
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INFshyIMP
I-R HF i NR
J---03 0
0009
ii rac t
jbullgt_ f- -_ -t 5 Ho CEI r o i5o-
S Source LFEt1ltN
ugL
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fi -E
gt - l l - pound
T - -ct
3 ho uEI
-- bull f W-VrT iievel do reoj _ y
1 bullbdquo bull - C shy y
V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
bull H
nr
i HF-
- 1
MR NR
bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
i rx
| MF
MR US
NF HF
NFgt
J
ltbullbull- Si gt-= HU
HO pound bull
Lew I ^ ] ~j td LL U
builds for Dopi - --bull 0 0
dTM| ISlOh ^ LI L
1T3
TV r
tK
r bullMR
HK UK
ltpoundL oAHrLE
Con t rac t
5AS No GEI iLj No
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2deg013
shy bdquo 11J I
c)i N c ^ _ - C ft3 Ho GET
^ u IC shy ii t I1 J s ugL
1 ^bull1L L1 3 ADD
ICTI At CUN AES
iLL IOhshy
gt
bull
NJ
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tr bullbull
-H-1
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Mo
Uli
GEI
Legte l
shy I bull
(Ishy
c er _ e
r i r
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bull II1IT3 (QUARTERLY
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IDL 1 L Q 1
200 i f i
0 i - 60 10
200 HR -gt 1 NK
3 1 T4X
5000 bullbull 30 irrlt
u L
100 15 0 bull 3 MR
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o shy f-r-1
bulltO NK 50-0 Mr1
10 SR
10 W fO
iR
X -U H -I r ft EL 50 ICF
Ib n03 0
0016
1 - SJpoundgt EL--I NT L^-U TON FACTORS ltANNlA__
if
_ bull shy - r shy
-bullbull r
- r _
bull
EI LHK-DH
Ciishy rC
19
r-11-1
Cor- t rac t
SM- No
D c t r
GEI
04C-J95
ri A- j~igt
In f j re l rr
Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
t f ip t - j ) bull bull - - i - [ft I03 0
1 - -i
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
I I
1 I
3 1 t bullt ugD H i
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HP NFshy
W
INK
iMR INK 1
f U Il-i 100 0
PF-T bull-bull ltN LOO
Contract bull
5AS No GEI
Ueight Moiure (gram) raquo ifiL )
05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
0 c LI
F f- PI
E pound G
H IM N K s A bull i bull r v z c U G i E bullbull- L N H
ii
lt
1 lt i
t i
-i
ii
ti
-I 2 i i bull l i i i bull bull i i i i
-1A i i t t _ bull -1 l 1 t i 1 1 1 1
gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
f
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l i
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x i bull 1 1 l 1 I
i t
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l - t -
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1
1
1
_
bull 1
i
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t
1 i
i
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bull
i
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1 i
i
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i
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i
i
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l r
i
I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
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t
1 1
1 bull
t
1 1
I 1
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i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
omm
ents
0 Ortn O Hshy
bull0 0 laquoa
Q 0 0 rr 0
rum rt-ts a o
A
on -fshy
a
f-
Iar iP s Oo M
r V i
I 3 -n
O 2=
(A tc IL
n
IS
o
i
_0 c PY
c C
01 en vt eo
laquoD bullO
00 ft 9
HS OO
H a
00Mr DO o
X
CO ltet O O
O 3 H-JS
0 O
M0
o rt o n a ~
ff O rrn 0 Hshy
930 c a D
O
-nJT
11 U 0 O n o
ocn ^ c BJ ortn 0 lt an-
n
H obullo 03 ft 0 S
a m
I
I
Sshy 0
9 ft O
otn ht Ca-o B) O
bull0tni lt (Dbullo
5 ltQHshyo
o o 3 II
C
0
ID
Stan
dard
vA
1 CD
Mft OO
bullr
00 ltrt 0 0 h-O
O 3
Sif bull0 n 0
Fin
al cone C
omm
ents i
olt0gt 0rfi raquoO H bullbull
shy
Hshy900 C 0 tv
c IS CD
D B ft ft
ma iB O m
0
i fl
vor O
yen 1shy
r~r^r T -
T
T
T -D C bull4)
T CN
cv
laquogtraquo
i lt ^
i
lt3
6
AQ o 0 rt O
bull0tonF lt obullu
09
H3 oa 0
CO Hft OO
O 9
00
0 3
OB
28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
t
io9deg~l-raquoS13o 1 7E7mdash 1-43ES7 -t shy rmdashl fmdash r-i i HOCO
1 H opoundS7F S 1 HoEdo 1 ~4 O Cl O i TOpound mdash 1 -i-CE-cshy1 HOpound^ -[_bullLiJV B 1H3E93 1 HoE99 1 HboOO 1 HO~deglHoHOtmdash 1 Ho~lHbHOo 17Homdash lHtaH7 1 tomdash 1 HCHOS 17HOmdash lHgHO7
rgtLK
u 1 7o mdash I HSH3o 1 oOmdash 1 H3n87 j oOmdash L H3n3o J ^ oO~lHoHO 17oOmdash IHOH-U 1771-1H35H1 1771-1H85HE
1 HoH^OFS bLK UCV pound1
1i 3SS8 l-t-5150 1 i-8pound9l l-iopound37 1 HopoundS7SE 1 -tSES7F 3
^ 1
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i ^
5 E5 11
1 1 JL
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1-)1 i 1 i
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pound 5 1 1
EO IO
11 1
30 101 J
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i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t
I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X
Ul- bW O
He 5o
513 1-4C3
~i jr- i O
S3E11
3-7 EE5E EEoo pound55^ 34 3 d oo 3s 7o c ^lt-~ E7 1
- 9E icbo
V 3-+79 onS1 1 o37 EO 1 7 = bull41- C c5Eo iooo o 1 o 3-i- -^ raquoccoO
O 1317
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35E3 35E8 3533 3538 35M-E 35-47
^bull43 1 359
o E63O Eo3o 1808 2E59 3 lt=pound7S bdquo
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lt- 5 1 i 5|c
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1 jo 835 ^c 1 1 c 1 V poundS HO ^shy
5 19o vshy37n39u
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i 7 i 1 oH V4 4 r-iC7 - i j c Ushy1 1 E9o L1 1 77lt_ pound7 Ho7
b 9oE ^ 59^0113 33pound59S-49 ^1
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1 OH o7n ^x HH003 UshyOOH51 U
-raquo C y JOH U^ 7 on7 Ushy8796^
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mdash
mdash
mdash
~shy
mdash
mdash
shy-1C 53 OH crcshy
5su Oo 5deg sO 01 =c OO on o5 00 o7 OO
1 H-bc-bV 1 -+opound9o 1 --4opound97 BLr LCV
1 H oE93 1 4 O f~ ~ ^ tradet 0400 1 ~ o--oc5E i HC^V on poundj plusmn 1--CJ4O
i H O H f c j i C3C
1 M Oto7|- S
1 bullshy O--^O
poundgt_bullbull
^L-V
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pound5 pound5
oVgt poundo 1 O
io 1 j50
j 1
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1 1 11 i 1i i ^ i i 1
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i_ 1 376 887
113E C1 bull 7 Io53
oo
1E15 E5C1 ^ bull
0 15o5
tv
0S oi t
ta
Vlgt
CH ^JOC x ~gt 1CT OH OCO n5 ooo ^
vj O51 V u pound pound60 lO--1 O o3 1 ~^u
58EH3V 37 999
IIOHpoundH v V 1 pound bull49-t r y]1 3deg HpoundE v Llt (gt 11 OOb 17Ho3 0 poundoo33 It O
pound17 ooo v ltj oG 12= OHO
bdquo
~v 71 ~c
^~+ ~3 7o
73 79
1 -fO-401^
raquo shy O5
i -i oS^-t i i -40OM-E 1 4tTshy
I --to -t raquoF c 1 shy1 O-t -bullbull T 3 bL
Imdash mdashE
pound5 oo [j1 o ^ L o mdash L Zio
_^ 1
rf 1i 1 1i 1 ^ 1
1 5to EoaV
onE 1 OoO ipound7 E OOO-4 O-O
1 L 3 SiT mdash bull
Vy
n =
OCj
oSEBl EE5 copound
3o o7c 1 O7 1 7-t EEo E ~3E5cE3cEZ=ooo
^ bull J C ~E oH i ) Si
n i^
r-^ a J v 7
lampjC ^- ^ J9
70011
_
CL
V sr
4 c
7001
laquoplaquofiy- Analysis EPA 300 0
Analyts
Analyst
ICVCCV True value
Job No Samle No 1
Labsys Batch
Data 0 60 -$amp
Page
A03 JL02
5shy | alaquoi i 0 20
Recovery
0oLG
O-2 G
00
41 6b svampygg OZo
loolamp
amp06V
0
0020 20020
lt
y z
Z
pound0010 I o fLy
L CO-7O
0
701 p
f I i LE
uPtRti FuJR ~Mpound v
bdquobdquobdquo 11 7E7mdash 1 M-OEB9 i-rSsea 1+SSS7_
15 1-+SE90 is-poundE9q1 bull- tgtc 9
17s-omdash1 7ot_mdash ELL bull-v
n i T 4 J
i
1
1
1
1
1
i 1i
iiiiii
ii4
i
ii
i
iiii
iiii
i11iii11iiiiiii i1
it-j n ~3opoundH
t ON
657 139u 3M-3-
(1 -t -S
O oo OgtZl
1poundpound 1 pound 1
rshy155
M-Mshy~~ ^J
3-f bull_
1 5poundoi j
5 ( E5E
11 HS 31 1^
555 bull45 19
151HC3
t sect H-6
1 f~~
3(1 j5ob pound7 SMshy
73O l_laquo ltJ
i 5o3bull i Jt-So
BOH lt_
1515i_j
t- v I Zgt
v O-o
bull_ OOMshy
O pound 1 9 u ()gt+
J 1 o O
bullJ i 1 O
o au bull_gt u i s v uov
^ ~~ ~ v raquodu r
G lt i1
bull UU5
d loOS u oGo
U I G1 O GOo U G 1 O u poundpoundpound
O i
bdquo 006 O uO3 U bull -j I 9 u ltgt 1 3 uulo J Oil 0 i j9G oGn u poundpoundG O -jOt o Oipound u lpoundt u m Jt_gtlaquo-f
bdquo poundpoundpound
(bull
kr
N _
S
7001
X
I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
irfd l ~n MKHl O M H 0^4
amp4l t^q OM^
iff 5^2 u 7^ bull ^ d$ poundLf IW- o5l HZ bull
ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
^ tiamp 1HA 7f-^ 1C1 710 (03^
I m-T
IHfraquo7 4S IX m ia 1^7 1 3 5JS U1 Ift ^ l 7Y lv Ll-S ID 21-T- Ga1 13
11 i1 2-X 41 ^ MM ltpound IX 1 11 3^5 4x TII 5H JJ SifV M 5^ SiM
W OX S3 r-4 c j9 H05 11 1 tfl bullH3 2 ltClaquo- an ( 3 ^u 3 KH 22
$7 Z
Z1V bull2H v li i XS gt-l ii G 7 IX 21-1 i Ift | ^-S 2J 22 1gtU n
3co 21 i Ill lUttgtlaquo^ i 1 Cdfc U $o $c c|
c^v t-^s ^f U-f KUftr
bull 21 pound)( St Zl U5 Ji y$gt (p 45^ ^1 l-C IX 1JJ US tfH B1 7f^ 15
i UlTK z-c L ]R I amp4 )7 raquo^1 15 Wfc L-t IX Iftl t-r a5 X is
i qlt^ H| 1 WH 7 1 laquo1 ^ IS
l IX ^ lok MlH HlG gtW iW 7rtit
r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
ooX Vn
230
1
I c o U
ou
nd
O-j
90 laquo3
VA Ni 1 11 1 31 11 1
a E
laquo^ i
c8 ii
gt mdashbulln a mdash E D bull in bull
9
abulli
Ui
Ebull a 3
3-1 O XT
O 0shyUI 4
U O
E 0 C 3 3
c C 3 3
a
r O c 3 Si Zraquo to vo
O- ashyM U) 3- 2Cr- CXS 0 C 0 3 r mdashS
0deg pound rva V3T C3- cr cr a E3 r taj
NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
bullbull
2
s -s
^ ^ -gt
Ye
s N
o 1
c ^N gto bullmdash
1)
X bull
shy Oshy
Ngt
^gt i
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hBB|M
B|B
H||H
|
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his
wor
k be
ing
con
duct
ed lo
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gula
tory
N
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e m
onllo
nng7
Y
es
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N
o
Is t
his
wor
k be
ing
con
duct
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r re
gula
tory
s
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ent
actio
n7
US
T
Drinkm
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r
1 CO
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TS
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tin
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mdash shyg ^
LU CO 18 f-
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RE
MA
RK
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g 5
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LL
c ^ --- 0
y(shyUJ [ UJ^^N^0 vi CK UJ ^ gt| IT gtv
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1
LU cr
bull
is-o Q _-gt 15 r-
u LU z cr LU
50shy
LU
c 1
laquo
B
olt
J V ^
^
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U) LU
5 D
pound
f
D Cr)
bull IT rn ^
gt ^TI gt O
i^
N
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^ 0
|
r|O
-M^^- cyjf^^j^ bull laquo -t
^bullr-^0^ -^
TIL
ES
FR
EE
OF
HE
AD
SP
AC
E Y
ES
N
O1
i S
Ibullbull
^ TbullJ CO tLU gtJ gtr
RE
LIN
QU
ISH
ED
7Jsf
rgttf
9C^ bullv S
itfr
gt lt U V
^
s
bulllt X
CO
Qv
^x ^ lt
0bullfc HJX Zlaquo Vshy
X LU cr r-i)CO LU LU o vfi H3HJO
s -raquos
cr Q
bull
4 ^ Oti
^
^ ^ v
^ Vu gt S S li
V s gt
f an
d T
ype
of
Conta
iners
tOS2H
X
1 R
EQ
UE
ST
NE
T T
O D
ISP
OS
E O
F A
LL S
AM
PLE
RE
MA
CO
lt J56
V
7 LU EONH V s
vbull
ACO -
V
OLA
SA
MP
LE R
EM
AIN
DE
R D
ISP
OS
AL
R
ETU
RN
SA
MP
LE R
EM
AIN
DE
R T
O C
LIE
NT
JH 81
Tr HOEN X
+ o~l IOH cr
LU N^ ~i i
CO
cr
jipbull i
O^
^
UI cc lt dWOO
z D lt N 8VUO bullyi gt XZ
XIH1VW 0 2co O o LL u
(PR
INT
NA
ME
) raquo
SIG
NA
TU
RE
^UJ LU cr 2 QD
O cr cr 3 SiQ CL
|oiI 0 O ^ ^H 0LU
FIE
LD F
ILT
ER
ED
Y
ES
N
O
gt s kiit 0 1 i^
LJ Nj
S lilh gtt p fy^ LU rr
C cr gt bullgtv
V) 0 bull0
CO ^s 0 o LU 1
en i - 0 UJ gt
li 2 C^
P O ^Sj amp pr^ It O CO UJ
UJ
sect bull
|
CO
j ^ N)
u rgtshy
$ ^ V lt LU
bullv bullDr ^shy C-JN
bullv
H
copy V
^ CL
^ UJ 15 lt Vbull5 co
bull 8 1 ^g
m gt^ gt LL omIf l
bulla 5 S ltsect - Xs10 0p suT ^shy^vj
UJ lti
_i shy 0 A1^^ IHH fN
CO
ND
I
Ifgt z UJ rh-W^ f Vrlt llt z d z m gtr ^ UJ
Klt Q 00 ^bull
1
opound LLJ W O LLJ LLJ gt cre c- ^ fm
C
fe Z U j
i_ Q ifa ^ 3 sectshy
PO
V tl s rshy
$1 LJJ O I- IB
z c
o o tr
bulls X s o0
t-N Vi)
(mdash laquo
ky- I
cc LLJ D z lt LLJ CC
lt UJ
x
Is ss c^I- c-O D lt UJ
0 P OC Z LU
LL s g y
I fQl
lt w
raquo LL o -i o
H Q
O
Sidd olt I- LLccO LLJ UJ Q t3
12glaquoUJ Q
SeSEw
zw uj
poundE D =gt O
lt C3 O Q W O LT LLJ Q Z lt
LLJ Lt LLJ
lt W
^j I
c g
^Sshy
LLJ
D
CO LL
4O O o X
UJ
^
c
g 5
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
-1 I (1 r r ( t
u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
I
o r-r
Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
h t
- 1
- t
~
i bull gt lt -
ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
i
t
I
rshy
^ Hshyr
i
h
iN j
N
N 1-4
4f
r-NT
M
(N
N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
_t HP
I J 1 lt_ r X a t
No jEI
Lab i (4i2
Date Rec
LI
IN
IN
it M
4 J a shy
M r-l
- J jr
l e t
ore
er
CLfAR
CLEAR
T shy1 ft u reshy
0002
- C DATA SHEET
Lfr No GET G No
Lab Sample- j u - 14
Date Rr-iHC t-5
Ur iJ--5 dr-ij weight) U
f i
-
CLEAR Texture
i-LiuiL r u r CLFAR Artifact-
- u KR-gtTON
Cji I-T a l
ilaquoI ci 5AI No GEI SOL Ho
ul ~ i c CO F - TR
C bull shy TI i u bullbull a a 11 b r 3 bull r conci F gt i ) o
1 rr
1
1 1 1 bull bull
Nfc
1 1HR
1 UloO -^ Ill 0 t O i v - bullbdquo- I- bull ^
i HR 1 nR HR
IF HP
bull 1
1
1
t
1
HI HP i MR MF
INK i MR NTv
NF
i1 INK bull 1 1 1
90-110
0004
Ac No GET rgtJi Ho
IFt
ugL
i cj C 3 ] i i r raquo u i u bull LI 1 M r bull bull _ gt bull r GUTld 7Rlt) Fi bull J bullif bull r
gt MF
bull i-ir-
bull bull HF
t ( Hf-1 I rp
1 1
MP Mf 1
bullbull bull b08 c-o lot i i -bull- o i^ shy K i
i
i
i
1 (bullIF Mr
Hi
1
i
bull
i HR NK MFshy
bull I
J 1
t i i MR
NR | 1
if-l
L r r - - a bullt
5^r No GEi
u L
1 1
i1 Ccr iiTumig Calit iJ jjf 1 Fs jnd Ragt FoJ gt lt l bull bull bull
mdash mdash - mdash mdash trade
( NK UK
Mr i i if
i INK IN- i
i bull MF s NF-
NF i Nh
1 J J raquo J J 4 0 103 P
hf MR I
- i MK
( ( Nh | i Mf lt t INR
1 Hh lt 1 1 irihl
1 i HP SUP iP i i laquo 1 i
i 1 i
i bull P 90-110 Ci snidt
AA AMD TCP
- pound ill1 I w I j M Loo r r a ~ _ t
S4i= HO GE
ug t
CRDL E Initial
Gun
M lt I-lt bull SA-t No LgtEI 5Dj Ho
r k ~_ n ^r I r Ugt shy L or m g k g gt l-G L
I t i t i i f t
bull i 1 1 1 i t i l
3 i ICi Prep L
-^ o ij
C
riiolt r i ci n
I I I -
1
bull I I I I
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1 1 liK 1 MR nr
i i NP t i N i
i W
NR 1
1
i NK i NH
11 15 0 LI raquo v bull F bull Mi
i MR
^iT1
i HF 1 i fir-
i HP
raquo t Kl 1
i KR i w
gt i i
IiiGj 0
ELr - - -
Contract
5n5 No GEI
j -mishy lt ori hr shy J shy C L or
G 11 inv - i 0 A f 10 fi
i ) r repa
bull n
NK MF KR r i F
- 1 pound
i NP MF
INK IN
bull HK p IH-
^i^ bull NR INF Nfi
INFshyIMP
I-R HF i NR
J---03 0
0009
ii rac t
jbullgt_ f- -_ -t 5 Ho CEI r o i5o-
S Source LFEt1ltN
ugL
F i n-i L Foj Sol pound0
fi -E
gt - l l - pound
T - -ct
3 ho uEI
-- bull f W-VrT iievel do reoj _ y
1 bullbdquo bull - C shy y
V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
bull H
nr
i HF-
- 1
MR NR
bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
i rx
| MF
MR US
NF HF
NFgt
J
ltbullbull- Si gt-= HU
HO pound bull
Lew I ^ ] ~j td LL U
builds for Dopi - --bull 0 0
dTM| ISlOh ^ LI L
1T3
TV r
tK
r bullMR
HK UK
ltpoundL oAHrLE
Con t rac t
5AS No GEI iLj No
Sol id 11 ri
2deg013
shy bdquo 11J I
c)i N c ^ _ - C ft3 Ho GET
^ u IC shy ii t I1 J s ugL
1 ^bull1L L1 3 ADD
ICTI At CUN AES
iLL IOhshy
gt
bull
NJ
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o - 2 - T gt _ gt
tr bullbull
-H-1
-i bull c
Mo
Uli
GEI
Legte l
shy I bull
(Ishy
c er _ e
r i r
N Ml r-i
35 OC
-l
Ni IN
Ml
bull II1IT3 (QUARTERLY
_bull-_ bull11- jG Coi-traci
i Sn3 No GE r-DC N
IDL 1 L Q 1
200 i f i
0 i - 60 10
200 HR -gt 1 NK
3 1 T4X
5000 bullbull 30 irrlt
u L
100 15 0 bull 3 MR
50iU IMF-Jh bull Mft
o shy f-r-1
bulltO NK 50-0 Mr1
10 SR
10 W fO
iR
X -U H -I r ft EL 50 ICF
Ib n03 0
0016
1 - SJpoundgt EL--I NT L^-U TON FACTORS ltANNlA__
if
_ bull shy - r shy
-bullbull r
- r _
bull
EI LHK-DH
Ciishy rC
19
r-11-1
Cor- t rac t
SM- No
D c t r
GEI
04C-J95
ri A- j~igt
In f j re l rr
Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
t f ip t - j ) bull bull - - i - [ft I03 0
1 - -i
iiiirr-ir C C F - F L L - O N F A C T O R S lt H
H1 E3 J O N C n n L r a c t
- Sraquo t iZsc 5Af No GLI I no
D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
I I
1 I
3 1 t bullt ugD H i
_ i 3 ^NR IMF HF
HP NFshy
W
INK
iMR INK 1
f U Il-i 100 0
PF-T bull-bull ltN LOO
Contract bull
5AS No GEI
Ueight Moiure (gram) raquo ifiL )
05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
0 c LI
F f- PI
E pound G
H IM N K s A bull i bull r v z c U G i E bullbull- L N H
ii
lt
1 lt i
t i
-i
ii
ti
-I 2 i i bull l i i i bull bull i i i i
-1A i i t t _ bull -1 l 1 t i 1 1 1 1
gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
f
i l I I
l i
A __ 1 _ 1 i bull l bull
x i bull 1 1 l 1 I
i t
i )
lt1 shy
l - t -
j 4 ~ r _ _ _ _ gt _
1
1
1
_
bull 1
i
- ~~ ~ i lt
1bull
i
I
i
bull
t
1 i
i
i 1
bull
i
1
1 i
i
1
1 i
i
)
i
i
1
l r
i
I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
omm
ents
0 Ortn O Hshy
bull0 0 laquoa
Q 0 0 rr 0
rum rt-ts a o
A
on -fshy
a
f-
Iar iP s Oo M
r V i
I 3 -n
O 2=
(A tc IL
n
IS
o
i
_0 c PY
c C
01 en vt eo
laquoD bullO
00 ft 9
HS OO
H a
00Mr DO o
X
CO ltet O O
O 3 H-JS
0 O
M0
o rt o n a ~
ff O rrn 0 Hshy
930 c a D
O
-nJT
11 U 0 O n o
ocn ^ c BJ ortn 0 lt an-
n
H obullo 03 ft 0 S
a m
I
I
Sshy 0
9 ft O
otn ht Ca-o B) O
bull0tni lt (Dbullo
5 ltQHshyo
o o 3 II
C
0
ID
Stan
dard
vA
1 CD
Mft OO
bullr
00 ltrt 0 0 h-O
O 3
Sif bull0 n 0
Fin
al cone C
omm
ents i
olt0gt 0rfi raquoO H bullbull
shy
Hshy900 C 0 tv
c IS CD
D B ft ft
ma iB O m
0
i fl
vor O
yen 1shy
r~r^r T -
T
T
T -D C bull4)
T CN
cv
laquogtraquo
i lt ^
i
lt3
6
AQ o 0 rt O
bull0tonF lt obullu
09
H3 oa 0
CO Hft OO
O 9
00
0 3
OB
28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
t
io9deg~l-raquoS13o 1 7E7mdash 1-43ES7 -t shy rmdashl fmdash r-i i HOCO
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rgtLK
u 1 7o mdash I HSH3o 1 oOmdash 1 H3n87 j oOmdash L H3n3o J ^ oO~lHoHO 17oOmdash IHOH-U 1771-1H35H1 1771-1H85HE
1 HoH^OFS bLK UCV pound1
1i 3SS8 l-t-5150 1 i-8pound9l l-iopound37 1 HopoundS7SE 1 -tSES7F 3
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1 jo 835 ^c 1 1 c 1 V poundS HO ^shy
5 19o vshy37n39u
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b 9oE ^ 59^0113 33pound59S-49 ^1
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1 OH o7n ^x HH003 UshyOOH51 U
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5su Oo 5deg sO 01 =c OO on o5 00 o7 OO
1 H-bc-bV 1 -+opound9o 1 --4opound97 BLr LCV
1 H oE93 1 4 O f~ ~ ^ tradet 0400 1 ~ o--oc5E i HC^V on poundj plusmn 1--CJ4O
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vj O51 V u pound pound60 lO--1 O o3 1 ~^u
58EH3V 37 999
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pound17 ooo v ltj oG 12= OHO
bdquo
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73 79
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raquo shy O5
i -i oS^-t i i -40OM-E 1 4tTshy
I --to -t raquoF c 1 shy1 O-t -bullbull T 3 bL
Imdash mdashE
pound5 oo [j1 o ^ L o mdash L Zio
_^ 1
rf 1i 1 1i 1 ^ 1
1 5to EoaV
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1 L 3 SiT mdash bull
Vy
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lampjC ^- ^ J9
70011
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7001
laquoplaquofiy- Analysis EPA 300 0
Analyts
Analyst
ICVCCV True value
Job No Samle No 1
Labsys Batch
Data 0 60 -$amp
Page
A03 JL02
5shy | alaquoi i 0 20
Recovery
0oLG
O-2 G
00
41 6b svampygg OZo
loolamp
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0020 20020
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657 139u 3M-3-
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1poundpound 1 pound 1
rshy155
M-Mshy~~ ^J
3-f bull_
1 5poundoi j
5 ( E5E
11 HS 31 1^
555 bull45 19
151HC3
t sect H-6
1 f~~
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73O l_laquo ltJ
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1515i_j
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bull_ OOMshy
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bdquo poundpoundpound
(bull
kr
N _
S
7001
X
I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
irfd l ~n MKHl O M H 0^4
amp4l t^q OM^
iff 5^2 u 7^ bull ^ d$ poundLf IW- o5l HZ bull
ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
^ tiamp 1HA 7f-^ 1C1 710 (03^
I m-T
IHfraquo7 4S IX m ia 1^7 1 3 5JS U1 Ift ^ l 7Y lv Ll-S ID 21-T- Ga1 13
11 i1 2-X 41 ^ MM ltpound IX 1 11 3^5 4x TII 5H JJ SifV M 5^ SiM
W OX S3 r-4 c j9 H05 11 1 tfl bullH3 2 ltClaquo- an ( 3 ^u 3 KH 22
$7 Z
Z1V bull2H v li i XS gt-l ii G 7 IX 21-1 i Ift | ^-S 2J 22 1gtU n
3co 21 i Ill lUttgtlaquo^ i 1 Cdfc U $o $c c|
c^v t-^s ^f U-f KUftr
bull 21 pound)( St Zl U5 Ji y$gt (p 45^ ^1 l-C IX 1JJ US tfH B1 7f^ 15
i UlTK z-c L ]R I amp4 )7 raquo^1 15 Wfc L-t IX Iftl t-r a5 X is
i qlt^ H| 1 WH 7 1 laquo1 ^ IS
l IX ^ lok MlH HlG gtW iW 7rtit
r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
ooX Vn
230
1
I c o U
ou
nd
O-j
90 laquo3
VA Ni 1 11 1 31 11 1
a E
laquo^ i
c8 ii
gt mdashbulln a mdash E D bull in bull
9
abulli
Ui
Ebull a 3
3-1 O XT
O 0shyUI 4
U O
E 0 C 3 3
c C 3 3
a
r O c 3 Si Zraquo to vo
O- ashyM U) 3- 2Cr- CXS 0 C 0 3 r mdashS
0deg pound rva V3T C3- cr cr a E3 r taj
NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLET
AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
-1 I (1 r r ( t
u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
I
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Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
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- 1
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~
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ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
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I
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C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
_t HP
I J 1 lt_ r X a t
No jEI
Lab i (4i2
Date Rec
LI
IN
IN
it M
4 J a shy
M r-l
- J jr
l e t
ore
er
CLfAR
CLEAR
T shy1 ft u reshy
0002
- C DATA SHEET
Lfr No GET G No
Lab Sample- j u - 14
Date Rr-iHC t-5
Ur iJ--5 dr-ij weight) U
f i
-
CLEAR Texture
i-LiuiL r u r CLFAR Artifact-
- u KR-gtTON
Cji I-T a l
ilaquoI ci 5AI No GEI SOL Ho
ul ~ i c CO F - TR
C bull shy TI i u bullbull a a 11 b r 3 bull r conci F gt i ) o
1 rr
1
1 1 1 bull bull
Nfc
1 1HR
1 UloO -^ Ill 0 t O i v - bullbdquo- I- bull ^
i HR 1 nR HR
IF HP
bull 1
1
1
t
1
HI HP i MR MF
INK i MR NTv
NF
i1 INK bull 1 1 1
90-110
0004
Ac No GET rgtJi Ho
IFt
ugL
i cj C 3 ] i i r raquo u i u bull LI 1 M r bull bull _ gt bull r GUTld 7Rlt) Fi bull J bullif bull r
gt MF
bull i-ir-
bull bull HF
t ( Hf-1 I rp
1 1
MP Mf 1
bullbull bull b08 c-o lot i i -bull- o i^ shy K i
i
i
i
1 (bullIF Mr
Hi
1
i
bull
i HR NK MFshy
bull I
J 1
t i i MR
NR | 1
if-l
L r r - - a bullt
5^r No GEi
u L
1 1
i1 Ccr iiTumig Calit iJ jjf 1 Fs jnd Ragt FoJ gt lt l bull bull bull
mdash mdash - mdash mdash trade
( NK UK
Mr i i if
i INK IN- i
i bull MF s NF-
NF i Nh
1 J J raquo J J 4 0 103 P
hf MR I
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1 Hh lt 1 1 irihl
1 i HP SUP iP i i laquo 1 i
i 1 i
i bull P 90-110 Ci snidt
AA AMD TCP
- pound ill1 I w I j M Loo r r a ~ _ t
S4i= HO GE
ug t
CRDL E Initial
Gun
M lt I-lt bull SA-t No LgtEI 5Dj Ho
r k ~_ n ^r I r Ugt shy L or m g k g gt l-G L
I t i t i i f t
bull i 1 1 1 i t i l
3 i ICi Prep L
-^ o ij
C
riiolt r i ci n
I I I -
1
bull I I I I
_ 1 _ l
1 1 liK 1 MR nr
i i NP t i N i
i W
NR 1
1
i NK i NH
11 15 0 LI raquo v bull F bull Mi
i MR
^iT1
i HF 1 i fir-
i HP
raquo t Kl 1
i KR i w
gt i i
IiiGj 0
ELr - - -
Contract
5n5 No GEI
j -mishy lt ori hr shy J shy C L or
G 11 inv - i 0 A f 10 fi
i ) r repa
bull n
NK MF KR r i F
- 1 pound
i NP MF
INK IN
bull HK p IH-
^i^ bull NR INF Nfi
INFshyIMP
I-R HF i NR
J---03 0
0009
ii rac t
jbullgt_ f- -_ -t 5 Ho CEI r o i5o-
S Source LFEt1ltN
ugL
F i n-i L Foj Sol pound0
fi -E
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T - -ct
3 ho uEI
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1 bullbdquo bull - C shy y
V- a l ui - 5 gt _bull bullbullgty- l poundi dr ) teigit ^ J L
Bp^ ^ rau l 5 S bull f uU SR) c 0 n
i
bull H
nr
i HF-
- 1
MR NR
bull MR ^shy bull bull 7-000 iOC-7 bull shy bull - i F
i rx
| MF
MR US
NF HF
NFgt
J
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HO pound bull
Lew I ^ ] ~j td LL U
builds for Dopi - --bull 0 0
dTM| ISlOh ^ LI L
1T3
TV r
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Con t rac t
5AS No GEI iLj No
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2deg013
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c)i N c ^ _ - C ft3 Ho GET
^ u IC shy ii t I1 J s ugL
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ICTI At CUN AES
iLL IOhshy
gt
bull
NJ
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tr bullbull
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Mo
Uli
GEI
Legte l
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c er _ e
r i r
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Ml
bull II1IT3 (QUARTERLY
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i Sn3 No GE r-DC N
IDL 1 L Q 1
200 i f i
0 i - 60 10
200 HR -gt 1 NK
3 1 T4X
5000 bullbull 30 irrlt
u L
100 15 0 bull 3 MR
50iU IMF-Jh bull Mft
o shy f-r-1
bulltO NK 50-0 Mr1
10 SR
10 W fO
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X -U H -I r ft EL 50 ICF
Ib n03 0
0016
1 - SJpoundgt EL--I NT L^-U TON FACTORS ltANNlA__
if
_ bull shy - r shy
-bullbull r
- r _
bull
EI LHK-DH
Ciishy rC
19
r-11-1
Cor- t rac t
SM- No
D c t r
GEI
04C-J95
ri A- j~igt
In f j re l rr
Al ilg LC
bullbull - gt laquobullbull o ooooooo 0 OO-OCO u i-jOOOOO
t f ip t - j ) bull bull - - i - [ft I03 0
1 - -i
iiiirr-ir C C F - F L L - O N F A C T O R S lt H
H1 E3 J O N C n n L r a c t
- Sraquo t iZsc 5Af No GLI I no
D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
11bull ]i-T=rEiEnrNr C O ^ - K L C T T U N FACTORS (ANNUALLY
i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
^ je- lTgttsrel-jgt=i oi-rest ion Factors
FGRh XI lt F - c v pound gt - IN
_ l t i~Vr r-PLl- ( G U r i R T E H L Y )
[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
I I
1 I
3 1 t bullt ugD H i
_ i 3 ^NR IMF HF
HP NFshy
W
INK
iMR INK 1
f U Il-i 100 0
PF-T bull-bull ltN LOO
Contract bull
5AS No GEI
Ueight Moiure (gram) raquo ifiL )
05 bull-bullbull 100 100 100
_
il - IN
si -JN LOG
Contract
shy b5 Hn GEI ~L I No 5^c
Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
f w
0 c LI
F f- PI
E pound G
H IM N K s A bull i bull r v z c U G i E bullbull- L N H
ii
lt
1 lt i
t i
-i
ii
ti
-I 2 i i bull l i i i bull bull i i i i
-1A i i t t _ bull -1 l 1 t i 1 1 1 1
gt -11 i bull
xY~ t J
l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
i 1I i i 1 i bull
l 1
1 1 1
A i i 11 l i
ltl I l l
l I t
i gt i i
f
i l I I
l i
A __ 1 _ 1 i bull l bull
x i bull 1 1 l 1 I
i t
i )
lt1 shy
l - t -
j 4 ~ r _ _ _ _ gt _
1
1
1
_
bull 1
i
- ~~ ~ i lt
1bull
i
I
i
bull
t
1 i
i
i 1
bull
i
1
1 i
i
1
1 i
i
)
i
i
1
l r
i
I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
opound o n Q bullbull
0lt 9 Ortn O H-
c a 09
O-
o 9 ft O
2 ltOMshym
O O 31
n bull0
03
9
a 9
I
laquoaD
l-bO -n rt-O C o o n o
o
9
i bull
-raquo deg
(
o 0 rt o
bullo conK obullo
Otn^ c0gtO0 o rtn 2 ltQNshym o o3 n
amp
ID
andard
r 5 5 2 8 M U 5 m s g tn
Hft OO
Q
^raquo c
09 laquo ltrt o o n bullB
MO
O 3 secta0 n a
- a 0
Fin
al cono C
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ents
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
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531
73
bullI] 11AO
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0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
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^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
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3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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1727
la
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If
776
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701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
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602
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bull47 505i
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Analyts
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Labsys Batch
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I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
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ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
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r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
ooX Vn
230
1
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nd
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9
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0deg pound rva V3T C3- cr cr a E3 r taj
NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
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u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
Ddte Fec a i PU C-5
U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
i tio c i
1
1
1
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Nshy
N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
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- 1
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ni bull i
L 1 1 d 4 j i
ltbull j
1 i
1
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M
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C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
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v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
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bull dfit- vJohri pound tlotbleshy
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20001
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er
CLfAR
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0002
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Lfr No GET G No
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Ur iJ--5 dr-ij weight) U
f i
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CLEAR Texture
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
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i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
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FGRh XI lt F - c v pound gt - IN
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[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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05 bull-bullbull 100 100 100
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Contract
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Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
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ti
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gt -11 i bull
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l
1
l I
1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
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l 1
1 1 1
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l I t
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i l I I
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bull 1
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bull
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bull i bull i
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i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
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raquo t
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X ii i 1 ) l
1 bull
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bull 1
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1 laquo gt
i 1 gt
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1 1
1 1 bull
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1 t
1 1
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1 1
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1 1
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1 1 i i t tgt raquoi 11 i
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1 1
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1 1
1 t
gt 1
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i gt gt i l l i
t1 l 1
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1 1
bull l i
1 1
1 1
1
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-
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-
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-
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- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
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0 0271501 10120 476 0084L 0008
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K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
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^l AWC-^1 03 $ltst I
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r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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la
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776
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701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
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pound^l 0^ J zx 3fO
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pur ^^fc -oZGgt 50
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laquoplaquofiy- Analysis EPA 300 0
Analyts
Analyst
ICVCCV True value
Job No Samle No 1
Labsys Batch
Data 0 60 -$amp
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A03 JL02
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Recovery
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X
I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
irfd l ~n MKHl O M H 0^4
amp4l t^q OM^
iff 5^2 u 7^ bull ^ d$ poundLf IW- o5l HZ bull
ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
^ tiamp 1HA 7f-^ 1C1 710 (03^
I m-T
IHfraquo7 4S IX m ia 1^7 1 3 5JS U1 Ift ^ l 7Y lv Ll-S ID 21-T- Ga1 13
11 i1 2-X 41 ^ MM ltpound IX 1 11 3^5 4x TII 5H JJ SifV M 5^ SiM
W OX S3 r-4 c j9 H05 11 1 tfl bullH3 2 ltClaquo- an ( 3 ^u 3 KH 22
$7 Z
Z1V bull2H v li i XS gt-l ii G 7 IX 21-1 i Ift | ^-S 2J 22 1gtU n
3co 21 i Ill lUttgtlaquo^ i 1 Cdfc U $o $c c|
c^v t-^s ^f U-f KUftr
bull 21 pound)( St Zl U5 Ji y$gt (p 45^ ^1 l-C IX 1JJ US tfH B1 7f^ 15
i UlTK z-c L ]R I amp4 )7 raquo^1 15 Wfc L-t IX Iftl t-r a5 X is
i qlt^ H| 1 WH 7 1 laquo1 ^ IS
l IX ^ lok MlH HlG gtW iW 7rtit
r Sulfate EPA 3754M
Analyst te LabsyfBatch Supervisor
i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
-^ 10 Spike Stock 20 Spike prep a 25 Spike Value=
Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
fe 77 SMI 21 HIS
H7I
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230
1
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nd
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9
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0deg pound rva V3T C3- cr cr a E3 r taj
NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
M
CLF flF tur r
] e r 1 f er
0002
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u r No CEJ bull-O
r-LF L a b S a m p l e 11 x4 i
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U r i t n _ ue ign t ) U
1 i Igt J 0
(M 1 111
^ f J 1 shy
1 ltbull
I r
1
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1
1
1
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N
N1
v t
hi
1 1 v
j (
(j gtbullshy
L
( r ~ i t
bullgt
1
h t
- 1
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ni bull i
L 1 1 d 4 j i
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1 i
1
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N
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N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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End date 06079
Analytes i t
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bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
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37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
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700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
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If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
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602
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nn 10
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Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
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1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
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1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
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rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
25 -Cf^rt Spike Value= ^
i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
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i bull Calibrant lot
LCSIot LCS Prep
ValuejfrgL) Reading(ntu)
i li-4 5
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Job- sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
2X nl 213
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
i FT Lab Sample i MiiMshy
[raquoat FPC ^ 2 ii o ~ l
I 5
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CLF flF tur r
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-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
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3I2
4
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8
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11
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13
14
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Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
t
io9deg~l-raquoS13o 1 7E7mdash 1-43ES7 -t shy rmdashl fmdash r-i i HOCO
1 H opoundS7F S 1 HoEdo 1 ~4 O Cl O i TOpound mdash 1 -i-CE-cshy1 HOpound^ -[_bullLiJV B 1H3E93 1 HoE99 1 HboOO 1 HO~deglHoHOtmdash 1 Ho~lHbHOo 17Homdash lHtaH7 1 tomdash 1 HCHOS 17HOmdash lHgHO7
rgtLK
u 1 7o mdash I HSH3o 1 oOmdash 1 H3n87 j oOmdash L H3n3o J ^ oO~lHoHO 17oOmdash IHOH-U 1771-1H35H1 1771-1H85HE
1 HoH^OFS bLK UCV pound1
1i 3SS8 l-t-5150 1 i-8pound9l l-iopound37 1 HopoundS7SE 1 -tSES7F 3
^ 1
^ ^ i 1 1 1^ E c
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5 E5 11
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE NITRATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
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NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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t- - - b e- i - tb
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bull dfit- vJohri pound tlotbleshy
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Int r i e l^ rcTi - o t re^ t ion Factors fcr
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0-gt 0 0000000 o oo^oooo 000000
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FGRh XI lt F - c v pound gt - IN
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Contract
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k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
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CQ Q
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HS
20044
2
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n a
r 0 0 5-bull -
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s laquoQ
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01
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s i r
u
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8 Jraquo
(I
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II
r Ji
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CD
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aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
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a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
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a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
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u
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M01 O
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m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
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C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
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V bull=1ltMshyO 3
t i 1
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3 O rr O m
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^
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Q
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ft O
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ngt OHshy
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
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-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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FGRh XI lt F - c v pound gt - IN
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I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
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gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
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^
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C O
o
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m o oD n
u
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I ftfit
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r
cc
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r
8 i
r C
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CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
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o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
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bullo o
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b
T
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pound-kdegS~S
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raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
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3 ltHshyO 3
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bullno H-O 3 3o g M0
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ITU O Hshy
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c a D
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(D
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pound c
a o
s laquoQ
0)laquoa n
01
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ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
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CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
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01
s- a a rrr-CD bull ~ gt
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bull3
G r
S r
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9 n a
X _L
p
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7 VG ib c t c r
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03 Mtr -o
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03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
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Co
G 0 13
H-0 3 S a 3
3
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rr B
amdash
9 O
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rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
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5 ^
o
r r N 3 su
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ltP -5
X 4 61
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ID
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raquolaquoJO
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900 pound ^Ai
raquo Oshy
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B O O3 n
CD
0
a 0
1
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t ^ _D -5 -o
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_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
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bull0 0 |QO
ftgtO ^b ^3
D
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8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
= I rn No
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^ Hshyr
i
h
iN j
N
N 1-4
4f
r-NT
M
(N
N
C 1 T shy1 shy c t CLLAFv 1 t UT e
L j - o t ^ i j shy nr CLf i-iR A t i fsct
-0003
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
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FGRh XI lt F - c v pound gt - IN
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[ j i L V C o n t r a c t
5f-~ No GFi -LC Nn -S
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05 bull-bullbull 100 100 100
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Contract
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Hi hod F1
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t
1 i
i
i 1
bull
i
1
1 i
i
1
1 i
i
)
i
i
1
l r
i
I I f lt i ~~ ~~ ~
i t i i i i i i i - mdash shy mdash_ mdash _bdquo mdash mdash mdash ~
i i 1
1
i i
bull i bull i
1
i
)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
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a 1ro laquoa
Bgt
a
i
1
O
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2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
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pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
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V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
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a ~
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2
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ff-0 0 O ft B
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t
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9
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7
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T
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i
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6
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09
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CO Hft OO
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00
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28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
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NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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)
i i
1
i t
1
i
1
i i
-i 1 1 1
t i l l J i i |
1 1 bull1 T
t 1 tI l
1l 1
1
1 1
1 gt
raquo 1
f | 1 J I I
i l 1l
t
1 1
1 bull
t
1 1
I 1
il r
i 11
gt bull
1 r
t 1
) i 1
I t
1 1
I
k 1
mdash L 1 1 ( laquo gt 1 1 1 1 1
1 I I 1 1 t I
1 1 bull lt 1 t 1 1
1 I I 1 1 1 1 bull
i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
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m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
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pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
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V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
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a ~
0 0rf i 0 H-
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2
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ff-0 0 O ft B
0
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t
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9
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7
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n
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ents i
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shy
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T
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i
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6
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09
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00
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28SI MO
Ofi O B
Sshy
Dlt 0 O
900 pound ^Ai
raquo Oshy
O 0ft o
ftO 0 0 n B o
oco n c0ft00 o ftolt araquomdash
B O O3 n
CD
0
a 0
1
bullo 0
CO o
-o Hb
t ^ _D -5 -o
iof
lt3
_o pound
t lA I
1 s
5
D Bgt ft D
lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
ftgtO ^b ^3
D
-gt D bull fraquo
8 6 S 3 I 5^ bullJ laquof shyA laquo
deg ^yi bull- u ^ poundishy
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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t- - - b e- i - tb
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bull dfit- vJohri pound tlotbleshy
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FGRh XI lt F - c v pound gt - IN
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Contract
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i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
i t V A i 11 1 1 1
i 1 i
raquo t
t t
1 )
1 I
X ii i 1 ) l
1 bull
1 1
i 1 1
1 1
1 I
l 1
bull X i t 1I
bullt
i
l t shy
l 1
1
l t
t 1
i j i bullbull 1 raquo t bull t 1t
1 1
i i
I
l 1 i
l
1 t
1 1
1 1
1 )
I V bullA 1
I
11
bull 1
1 1
1 laquo gt
i 1 gt
1 1
1 1
1 l
1 1
1 1
x 11 t 4
1 1
1 1 bull
i 1
1 t
1 1
t 1
1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
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HS
20044
2
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n a
r 0 0 5-bull -
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r
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r
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pound c
a o
s laquoQ
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01
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s i r
u
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_ -o
8 Jraquo
(I
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II
r Ji
^
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CD
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aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
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a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
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bullflO H-0
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3 O rr O m
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^
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O
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3
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amdash
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raquo Oshy
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B O O3 n
CD
0
a 0
1
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t ^ _D -5 -o
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t lA I
1 s
5
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lt 0gt bullO
nrt 0
H3 oa 9
CD Hft OO
Q
O 3
D n
O ft o n Q shy
olt 9 O ftt O H-
ft O
Bgt 0gt
ngt OHshy
D o o 31
oort 0
O
O B
bull0 0 |QO
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D
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8 6 S 3 I 5^ bullJ laquof shyA laquo
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
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Analyst Date Labsys Batch Supervisor
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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1 1
1 1
i r lt t i l X ii igt 1t
1 1
1 1
1 1
i
1 1
) 1
1 1
t 1
1 1
t l
1 1 i i t tgt raquoi 11 i
( 1
1 t
1 1
t 1
1 1
1 t
gt 1
t 1
i gt gt i l l i
t1 l 1
( 1
1 1
bull l i
1 1
1 1
1
raquo 1
i 1
r r - It tLilOJ 0
-
-
-
-
-
-
- - -
JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
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3I2
4
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8
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11
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13
14
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Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
0008
Jgt
700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
-
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
Rack 2
If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
Lf7 07 0 -7
1^7^VrAfiy^f in^lt^ lt^^() 5 x
020
Cfeo
r7V
602
oil
(^|
7-7
t 20
^5
^K ^( 39
fJ
BLANK 00 fc^^ 1 ^
LCS
^00$
OM
nc^ ^C j j
^o ltWL ^7^
IT7I cc oCH IS
^1 fvLS Hi 7ltft T76 -o^l 3gtdegi I7W Z60 oft) ito f 7 f f v 73^ ^^ 1 ^^ 130
nn 10
-735shy
z^^ ftu
Li4iL
lUfo
orlaquo| )OD ^x
ygt )laquogt
35 BLANK Gft^ ^IS LCS o0eft 111
H r
NET
plusmn L-ni__jr c
FUr-4 NLJMbEn 1 CFERs-rjR N5V
i pound 3bullraquo O o T
3 7 1011 1pound 13 4
15 io 1 7 io 19 pound0c^i poundc pound3 EH pound5 poundo pound7 pound5 pound9 30 31 3pound OO 3- 35 3o 37 38 39
H Hpound HO HH
HJ bull40^7 HO
bull47 505i
j rvuL^c^ =bull_ 00 Sy loo Si oo Spound 5o(lt mdash b ( O bLK
r -i i 0 Imdash
t
io9deg~l-raquoS13o 1 7E7mdash 1-43ES7 -t shy rmdashl fmdash r-i i HOCO
1 H opoundS7F S 1 HoEdo 1 ~4 O Cl O i TOpound mdash 1 -i-CE-cshy1 HOpound^ -[_bullLiJV B 1H3E93 1 HoE99 1 HboOO 1 HO~deglHoHOtmdash 1 Ho~lHbHOo 17Homdash lHtaH7 1 tomdash 1 HCHOS 17HOmdash lHgHO7
rgtLK
u 1 7o mdash I HSH3o 1 oOmdash 1 H3n87 j oOmdash L H3n3o J ^ oO~lHoHO 17oOmdash IHOH-U 1771-1H35H1 1771-1H85HE
1 HoH^OFS bLK UCV pound1
1i 3SS8 l-t-5150 1 i-8pound9l l-iopound37 1 HopoundS7SE 1 -tSES7F 3
^ 1
^ ^ i 1 1 1^ E c
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5 E5 11
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Analyst Date Labsys Batch Supervisor
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 150 148542 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Amnonia
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 039 148542 038
mgL N mgL N
0 0
06131996 06131996
nsv nsv
BOD shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 lt20 148542 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COO 4104 mod
148541 25 148542 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3252
148541 31 148542 140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 0052 148542 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
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DIVISJOi Contract
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End date 06079
Analytes i t
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1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
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i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
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33 6 nzraquo
531
73
bullI] 11AO
ri HJ m 70-^ - shyraquo 1 1 1 1
MMmi -ft H U L |K I b yen
0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT
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700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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1727
la
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If
776
tit in
701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
Q O f t
HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
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pur ^^fc -oZGgt 50
Lf7 07 0 -7
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bull47 505i
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0010 Standard Stock No
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
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bull dfit- vJohri pound tlotbleshy
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Ur iJ--5 dr-ij weight) U
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
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C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
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FGRh XI lt F - c v pound gt - IN
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05 bull-bullbull 100 100 100
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Contract
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Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
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gt -11 i bull
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l
1
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1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
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l 1
1 1 1
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bull i bull i
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i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
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raquo t
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X ii i 1 ) l
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1 1
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1 t
1 1
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1 1
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1 1
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1 1 i i t tgt raquoi 11 i
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1 1
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1 t
gt 1
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t1 l 1
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1 1
bull l i
1 1
1 1
1
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-
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-
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JN LOG
DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
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0 0271501 10120 476 0084L 0008
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K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
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BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
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^l AWC-^1 03 $ltst I
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r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
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la
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776
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701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
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pound^l 0^ J zx 3fO
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pur ^^fc -oZGgt 50
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section One
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M MA023
TABLE OF CONTENTS
Section 1 Report Front
1A
IB
1C
ID
IE
IF
1G
1H
Table of Contents
NarrativeCover Letter
Main PageSample CrossReference
Chain of Custody Forms
Sample Receipt Logbook
Page Number
OOP
fOOOsshy
-raquo- JUUI k
JQO
fOpound_
Data QualifierFlag Descriptions pound6V o
Document Inventory Sheets COY
Control Charts fi)pound
Section 2 Metals Analysis Data 20001
Section 3 Volatiles Analysis Data No Analysis Requested
Section 4 Semi-Volatiles Analysis Data No Analysis Requested
Section 5 PesticidesPCBs Analysis Data No Analysis Requested
Section 6 Herbicide Analysis Data No Analysis Requested
Section 7 Wet Chemistry Analysis Data 70000
100J1
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
June 17 1996
Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301
RE Tinkham Garage
Dear Mr Mullin
Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)
This narrative addresses all comments for all samples as listed below
NET JOB NUMBER 9601771
SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
103
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411
All laboratory comments for the data packages have been summarized in the following tables
Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7
These narrative tables are also enclosed with each data package section
Please find enclosed a diskette of the results for this case
Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information
Sincerely
Peter M Conroy Project Manager
enclosures
TABLE 1 SAMPLE RECEIPT amp LOGIN
FD1856
GENERAL COMMENTS No comments were necessary
100
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrument run for all required elements
The value of the ICB and CCBs did not exceed the CRDL for all analytes
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
10-t- 7
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
bull103^7
TABLE AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
10
TABLE BOD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
10310
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
10112
TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT +
11 Report To Reported By
11 Mr Bob Mullin National Environmental Testing
1 GEI Consul tantsNH NET Atlantic Incorporated
1 Suffolk Building Cambridge Division
1 53 Regional Drive 12 Oak Park
1 Concord NH 03301 Bedford HA 01730
1
Report Date 06171996 NET Job Number 9601771
Project Tinkham Garage NET Client No 14755
PO No 8307 Collected By RVan Etten Shipped Via FedEx
Job Description Tinkham Airbill No
This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments
Peter M Conroy NET Project Manager
Analytical data for the following samples are included in this data report
SAMPLE NET DATE TIME DATE
ID ID TAKEN TAKEN RECD MATRIX
92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER
92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER
Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit
011
Inorganic CLP BOW 390Data Qualifier
Form I-IN includes fields for three types of result qualifiers
c Qualifier - (concentration qualifier)
laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)
Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)
Q Qualifier shy
E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN
M - Duplicate injection precision notmet
N - Spike sample recovery not within control limits
laquoS - The reported value was determined by the Method of Standard Addition (MSA)
W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance
raquobulllaquobull - Duplicate analysis not within control limits
laquoi+laquo _ Correlation coefficient for the MSA is less than 0995
X (Method) Qualifier shy
P - for ICP
A - for Flame AA
F - for Furnace AA
CV- for Manual Cold Vapor AA
CA- for Midi-Distillation spectrophotometric
NR11- if the analyte is not required to be analyzed 1031
EPA CLP 390 Deliverables Inventory
Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 2 0001
Inorganic Analysis Data Sheets 0002
OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery
22222
2222222
0004 0007 0008 0010 0011
OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges
0012 0013 0014 0015 0016 0017 0020
OC Report- Preparation Log 0021 OC Report- Analysis Run Logs
Raw Data- ICP Listings
2
2
22
0022
0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)
0042 0045
10310
ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Two Metals Analysis
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE 2 METALS NARRATIVE SUMMARY
FD1856
GENERAL COMMENT No comment necessary
HOLDING TIMES All samples were digested and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the CLP ILM030 control limits for all analytes
A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements
run
The valueanalytes
of the ICB and CCBs did not exceed the CRDL for all
The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards
DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed
Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged
All analytes that did not meet the specified criteria were flagged with an N for the associated samples
DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes
A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL
All analytes that did not meet the specified criteria were flagged with a for the associated samples
LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits
MSA No samples reguired analysis by method of standard additions for the specified furnace elements
ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes
Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL
All analytes that did not meet the specified criteria were flagged with an E for the associated samples
EPA CLP 390 Deliverables Inventory
Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856
ITEM PAGE
INORGANIC ANALYSIS DATA PACKAGE 0001
Inorganic Analysis Data Sheets 0002
OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-
Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results
OC Report-OC Report-
ICP Serial Dilutions Instrument Detection Limits
OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-
ICP Linear Ranges Preparation Log Analysis Run Logs
Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-
ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)
(Se As Tl Pb) 0024
NR NR NR NR NR NR
Raw Data-Raw Data-Raw Data-
Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)
Raw Data- Sample Preparation Log(s) 2
NR NR NR 0042
Raw Data- Working Standard Preparation Log(s) 0045
Gfc1
1 bull T _ -LI 3jrp IB ID --firI C 1-C42Cgt
t- - - b e- i - tb
- bull I i - - - - rnp I bdquo jriclt_ (itn liiE- t c r r s an - r ac t c jLJ i t -v-hi lly and for coTiplet=-ii595 s
v cn- - 3 i lcc l abc- Release of the dair- rout- bull 13 bull- -i~ri i If bullbullOinnjter-roadable ddta subiT
j ^ b-Gi s l i r - ^ d _ Ue Laboratory narigilr or G t-u - J lOU ig signature
bull dfit- vJohri pound tlotbleshy
N 3LH-
20001
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I J 1 lt_ r X a t
No jEI
Lab i (4i2
Date Rec
LI
IN
IN
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M r-l
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l e t
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er
CLfAR
CLEAR
T shy1 ft u reshy
0002
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Lfr No GET G No
Lab Sample- j u - 14
Date Rr-iHC t-5
Ur iJ--5 dr-ij weight) U
f i
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CLEAR Texture
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Cji I-T a l
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1 rr
1
1 1 1 bull bull
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90-110
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CRDL E Initial
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SM- No
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GEI
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H1 E3 J O N C n n L r a c t
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D a t e 040395
Int r i e l^ rcTi - o t re^ t ion Factors fcr
C-r f u K Ho Ni
0-gt 0 0000000 o oo^oooo 000000
2 gt - IN 1LP03 0
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i)oK DTvICiCN Contract
C-jr0 Ho poundH -C SftS Ho GEI 50^3 Ho 185i
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FGRh XI lt F - c v pound gt - IN
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05 bull-bullbull 100 100 100
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Contract
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Hi hod F1
Euo ddte 060794
Analyte
iv A bullpound f t L -z bull
c c i c o A R
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lt
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gt -11 i bull
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l
1
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1
I I
1
I
1 i
1
1
I x l i t 1 i 1 t
1 1 X ]t i
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l 1
1 1 1
A i i 11 l i
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x i bull 1 1 l 1 I
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i i 1 gt f t t t gt t 1 I r i l i raquo i 1 1 J
1 1 1 1 X ii t t
1 1 1 i t t t i
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raquo t
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X ii i 1 ) l
1 bull
1 1
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bull 1
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1 laquo gt
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1 1
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1 1
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1 1 i i t tgt raquoi 11 i
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1 1
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1 1
1 t
gt 1
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t1 l 1
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1 1
bull l i
1 1
1 1
1
raquo 1
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-
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DIVISJOi Contract
it -gt- i jSC f-u 6- -bull 5A3 No GEI
Hethod P
End date 06079
Analytes i t
__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1
1 i ) r i l t
1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l
1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt
1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-
1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t
I l lw ~ L (K- lt bullbull bull i i
raquo - i
I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade
r t i t i gt i i 1 i r
bull bull bull bull i bullgt rii bull i | i 1 i I [I
i t I 1 I raquo
I bull i 1 I bullbull bull t t ( I - _ _ _bdquo
t i i j - v gt gt i t 1 1
1 1 1 I bull bull t ii X 1 _ bdquo _ 1
-- i 1 1 1 gt bull 1 1 lt
I --^~ZLI 1 1
1
i i l i t 1 1 t -1
i I
ov bull gt - lt bull
i o gt = - 1 X 1 1
gt 1 1 1 1 (
1 1 1 i i i bull lt 1 r X 1 t 1
t ) 11 i X I t l l t raquo t
i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It
mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash
1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i
1 1 i t i t -1 i i 1 i i i
i i bull i i i i-i 1 i bull i i i - i t i bull i
i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy
) r i i i 1 I bull 1 i bull t (
i t i 1 1 t i 1 i i li r i gt t bull gt I )
i i i i 1 1 1 i t i i - gt 1 1 1
t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (
I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1
i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1
-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1
i lt t bull bull 1 t 11 1 1 1
gt - bull ( 1 I t 1 t gt 4 1 1 1
__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1
1 ( 1 1t bull i i i t i 1 1 f
1 I 1 - 1 1 t f 1
ZLfi03 0
002
A T H E N A 3 06e
Fe
Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element
Time 1607 Processing protocol 390
Sample Code Preparation Client ID Date Time Meth Batch Date
1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559
24
3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date
bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603
gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618
A T H E N A 3 06e
-e
ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390
INSTRUMENT RUN QC REPORT
CALIBRATION VERIFICATIONS
osition Sample ID Code True Value Found Value Recovery
4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036
9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39
CALIBRATION BLANKS
osition Sample ID Code CRDL Found Value Flag
5 CALB ICB 1000000 130000 U
10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B
CRDL STANDARDS
osition Sample ID Code True Value Found Value Recovery
INTERFERENCE CHECK STANDARDS
osition Sample ID Code True Value Found Value Recovery
6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875
A T H E N A 306e
3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390
F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n
BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL
_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL
9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL
A T H E N A 306e
-e
id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390
RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000
os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n
42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B
28
SFe 259940 16740 000000 00000016380 000000 000000
16740 16380
165244 52996
Results for STDCCB Measures 2 (R)
EL SIGNALsigma
Fe$ 1 6810 059
Measures STDSPEC
Elements of SIMULTANEOUS
$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212
165520 52996
Results for STDSPEC Measures -2 (R) raquo
EL SIGNALsigma
Fes 3923S 008
Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB
Measurements for SPECXshy
16810
shy
HI STDSPEC 392355
1
Elements of SIMULTANEOUS
mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083
170013 52996 Method COMM
Sampla SPECXshy shyor Simul
EL CONC sigma
SFa 9Q969 053
39365 10034 PPM 39083 99594 PPM
1 MEAS= 3 for Seq tMEAS= 2 f
Measuremants for ICV1AICV- shy 1
200
$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM
170237 52996 Method COMM
Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul
EL CONC sigma
$Fe 4S676 029
Measurements for ICAP19ICVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM
170500 52996 Method COMM
Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
laquo
EL CONS sigma
SFe 1 0272 064
Measurements for CALBICBshy shy 1
Elements of SIMULTANEOUS
SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM
170723 52996 Method COMM
Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul
EL CONC sigma
$Fe 0 00426 150
Measurements for ICSAICSAOshy shy 1
Elements of SIMULTANEOUS
^O 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il
65960 000000 000000 65960 65960 17519 PPM
bull 170946 52996 Method COMM
Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul
EL CONC sigma
$Fe 17514 004i
Measurements for ICSABICSABshy shy 1
Elements of SIMULTANEOUS
SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM
171210 52996 Method COMM
Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 17297 046
Measurements for 2XCRDLABCRshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM
171433 52996 Method COMM
Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul
EL CONC sigma
$Fe 029397 31
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM
j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i
Sample CCVllCCV- shyfor Simul
EL CONC sigma
SFe 99108 032
Measurements for CALBCCB- shy
Elements of SIMULTANEOUS
$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060
171919 52996 Method COMM
Sample CALBCCB- shyfor Simul
EL CONC sigma
SFe 001784 89
raquo raquo
Measurements for LCSHCLLCSW- shy
Elements of SIMULTANEOUS
SFe 259940 53290 000000 000000 5329053130 000000 000000 53130
172143 52996 Method COMM
Sample LCSHCLLCSW- shy= 2 for Simul
EL CONC sigma
SFe 096926 031
Measurements for PBWPBW- shy
Elements of SIMULTANEOUS
F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430
172406 52Q6 Method COMM
P5WP6W- shy
1 MEAS= 3 for Seq MEAS=shy
1
17900 002902 PPM 17060 000666 PPM
1 MEAS= 3 for Seq MEAS=
1
53290 097139 PPM 53130 096713 PPM
1 MEAS= 3 for Seq ttMEAS
1
17750 002503 PPM 17430 0 71amp51 PPM
1 jMEV5 = for 5ltc
I ltJ OilllUi
EL CONC sigma
$Fe 002077 29
Measurements for 1699-148150shy
Elements of SIMULTANEOUS
$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM
172629 52996 Method COMM
Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 5476S 041
Measurements for 1727-148287shyraquo
Elementsof SIMULTANEOUS
$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM
172852 52996 Method COMM
Sample 1727-148287- - 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 60557 041
Measurements for -148288S-
Elements of SIMULTANEOUS
SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM
173115 52996 Method COMM
Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3
EL CONC sigma
$Fe 15643 035
Measurements for -148239S-
Elements of SIMULTANEOUS
SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM
173339 52996 Method COMM
Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 4S437 023
Measurements for -148289ISOshy shy 1
Elements of SIMULTANEOUS
SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM
173602 52996 Method COMM
Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
$Fe 091334 12
Measurements for -148289PSshy shy 1
Elements of SIMULTANEOUS
259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM
173825 52996 Method COMM
Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul
EL CONC sigma
bullSFe 46540 053 amp4
Measurements for -148289DS-
Elements of SIMULTANEOUS
SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM
174048 52996 Method COMM
Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul
EL CONC sigma
SFe 54405 026
Measurements for -148290S-
Elements of SIMULTANEOUS
$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM
174312 52996 Method COMM
Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul
EL CONC sigma
SFe 35411 034
Measurements for CCV1CCV-
Elements of SIMULTANEOUS
SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM
174535 52996 Method COMM
Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul
EL CONC sigma
bullBFs 10 034 0 04
5
Elements of SIMULTANEOUS
SFe 259940 17020 000000 00000016510 000000 000000
17020 16510
17020 000559 PPM 16510-000799 PPM
174758 52996 Method COMM
Sample CALBCCBshyfor Simul
shy 1 MEAS= 3 for Seq JtMEAS
EL CONC sigma
SFe-000120 300
Measurements for -148296S- - 1
Elements of SIMULTANEOUS
$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM
175021 52996 Method COMM
Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui
EL CONC sigma
Fe 040475 12
Measurements for -148296S2- - 1
Elements of SIMULTANEOUS
SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM
175244 52996 Method COMM
Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul
EL CONC sigma
Fs 039875 1 6
Measurements for -148297S- - L n
2003S
k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V
SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM
1755=08 52996 Method COMM
Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul
EL CONG sigma
SFe 024357 083
Measurements for -148298Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM
175731 52996 Method COMM
Sample -148298Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul
EL CONC sigma
SFe 11355 041
Measurements for -148299Sshy shy 1
Elements of SIMULTANEOUS
SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM
175954 52996 Method COMM
Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul
EL CONC sigma
SFe 22429 015
Measurements for -143300Sshy shy 1
Elements of SIMULTANEOUS
36605 000000 000000 36605 36605 97025 PPM
1802-18 52996 Method COMM
Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul
EL CONC sigma
$Fe 96678 051
Measurements for 1499-147068shy shy 1
Elements of SIMULTANEOUS
SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM
130441 52996 Method COMM
Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul
EL CONC sigma
SFe 13092 024
Measurements for -1470745Sshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM
180704 52996 Method COMM
Sample -1470745S- shy= 2 for Simul
EL CONC sigma
1531I 006
Measurements for RINSEX-
Elements of SIMULTANEOUS
259940 20620 000000 00000017300 000000 OOOOGO
1 laquoMEAS= 3 for Seq ItMEAS
20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM
j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I
Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONG sigma
$Fe 005725 110
Measurements for CCV1CCVshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM
131151 52996 Method COMM
Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 10162 032
laquo
Measurements for CALBCCBshy shy 1
Elements of SIMULTANEOUS
$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM
131414 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
SFe 000772 340
Measurements for ICSAICSA1shy shy 1
Elements of SIMULTANEOUS
SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM
131637 52996 Method COMM 2003Q
Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=
ltC I O I O illlU L
EL CONC sigma
9Fe 17689 033
Measurements for ICSABICSAB-
Elements of SIMULTANEOUS
$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM
181901 52996 Method COMM
Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul
EL CONC sigma
$Fe 17634 008
Measurements for 2XCRDLABCRshyr
Elements of SIMULTANEOUS
$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM
182124 52996 Method COMM
Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul
EL CONC sigma
Fe 026868 22
Measurements for CCV1CCV- - 1
Elements of SIMULTANEOUS
35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM
132347 52 96 Method COMM
Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul
EL CCNC sigma
e 100247 0 07
Measurements for CALBCC3shy
Elements of SIMULTANEOUS
$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM
182611 52996 Method COMM
Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul
EL CONC sigma
$Fe 002064 96
SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved
PH AS RECEIVED
Sample ID Lab code PH pH(CN)
1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20
Prep code P (HN03HC1)
Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution
921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00
LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00
2004
1 i Metals Digestion
Mercury Digestio bulllaquo
Comm or ( Dj
f Client Name
i i poundpoundpoundbull
3I2
4
5
6
7
8
10 i 9
11
i 12
13
14
15
i 16
1 7
18
9
20
mdash
Comments
ICAP Opiku-
ICAP Spike
Furn bplke
AQUEOUS DIGESTION LOG
Analyst SAP Date $~fai4fc PREP BATCH i^fc^
n Analyst Date FD 5t
Supervisor page 2V
Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial
Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2
-bullraquo LCSW _^r ^~7-f -TV s^ s
~ 5V- X ix poundyen DJ T^ T ^
bullbullHHi$yen2 J-a e laquobull + laquoraquo
^shy
lUAT-tCb bullnrnroi ^
ml of Spike deg bullbull vlt M tiki
ICAP LCS
LGGmdash
o mis of
mdash ml of
LCSHCI 1 yen
LCGI ICI 2mdash
ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_
Hg Spike mis of 01 ppm Ha Hg LCS mis of 01 ppm Ha o004 3
rrr
w
CQin
W
CQ Q
H O
W Di
QO
HS
20044
2
0gtft (D
f tun X bulllt (DTJ
ft 0gt
ss M3 oaogt
n a
r 0 0 5-bull -
m Hft DO
o
r r o
9
O
gt COltft
o o MO
ltHshyO 3
r IT m n
7 r H-O
3 O ft O CQ
O bullbull
^
ttt (DftH O H-- M)
C O
o
Jfi
oca c
0gt (Drtn 5 ltOMshy
m o oD n
u
agtbullo to
I ftfit
o n a o
I
r
cc
H o O
r
8 i
r C
0 cj
ltgt
C 0 8 s
2 i _
b S 3 ^1
1^
c J7
o o
e
^ -o
bulla jr laquoMM
--OC~ bull
mdash laquo r
a O
CO rr nraquo
fH3 oc0 n a
CD M rr 00
0
caltrt o o H-O
0 o
raquolaquoIO H-O
9 3t-gtagt
Oa rr
o gshy
0 o o
e a CO
o 01 rr o
1-hOrfa o o
n en n sshyo n o lt
o 0 0
bullo o
CO laquoT o
E 9
a 1ro laquoa
Bgt
a
i
1
O
o O
2 rbull 5 JL Q 0 N o -a
c
b
T
T
pound-kdegS~S
f O o--t
raquolt (0bullo
03
SB M3 ca o
M C
03 wrr DO
0
^03 ltrr O O t-gtQyr
3 ltHshyO 3
O O
bullno H-O 3 3o g M0
n ft o o o shy
ITU O Hshy
bullbull i-b
c a D
O-
oD rr o
mo
a o n a
(D
3 a-5 O 9 ltT-t
m lt CHshy
O C O
Obullo 03 ftshy
pound c
a o
s laquoQ
0)laquoa n
01
o-s-Tl rr Bgt m r^ O
ro ltampbullmdash
bulla a n c a o
s i r
u
O
(fl
_ -o
8 Jraquo
(I
i- laquobull
II
r Ji
^
ts
Jraquo r
T
r Jl
_n
CD
D MS cctt
aHr OO
a yr
01 ltrr O O K-Q
0 3 Mff
M o O
bull=30 H-O = 5 9 3
Q rr O D
O shy
a agtmi O Hshy
SO) c amp
poundS rr 0
n o rt-3 o o ^t 0
o
laquoJ^
wl
W obulla CO
a oraquo n c m
bulla
bullc laquoc0t 2
3 O rr-t
clt2 mdashlt m
c amdash
cA -n
CD ct laquo rr rO o(5
0 -a o mdash Ul 0 u
u
Cshy opound c ao LP
M01 O
O 0 bull0 i-1
m 0f rr
0 3 H-ff
bull1o n mtvl agt t o o laquoa
H-O 3 3 0) 5 H-ffl
3O rr O ffl
Q shy
C 7
- c ca
0
QI wT prr a
a gt IDrr3o O n m
x to
Verified
11
Date R
un
w o
ltlt of^f w
CD rrffl
H3 OC
O
sect e S f tn Mrr DO - 0-
7
rraquo te lto
CDltrrO o HO
V bull=1ltMshyO 3
t i 1
ox n D O
bullflO H-0
I I t-gtagt
3 O rr O m
r r
^
Bgt ID rrn o Mshy
O
deg2gtshyo-r _O D rrir shyO ltbull-shypoundraquomdash mdash B shyO 0-
bull3
CD rr 2 S 0
r obulla
0)tS o
fO ^ O
I-SO
0 o1 D
01
s- a a rrr-CD bull ~ gt
S bulllt (0
bull3
G r
S r
o 03 rr 9
H3 CO
9 n a
X _L
p
x Ci bullbull 3 r^ o5- c
z c 2shyr lt
7 VG ib c t c r
o O
03 Mtr -o
O mdash
03 ltrr O O O bullS H-0
o
r 1deg GO 0 S a0
Q
V fe
O o 0
Co
G 0 13
H-0 3 S a 3
3
js o o
rr B
amdash
9 O
^rshy ^ C ernID Hshy
V^ sai
C r c a mdash c a
cshybullB 9
^rshy (2
rr 0
is rr-s a O n a o
f -amp -o
P usect
|J
shyJ O 1
tfl pound - 8
5 ^
o
r r N 3 su
gt0
ltP -5
X 4 61
pound_ ltbull
c
o 0rf O
Stan
dard
ID
CO MPT o o
to ltrt0 0MO
0 3 MB
o B
raquolaquoJO
5-i 0 3 M0
O B
a ~
0 0rf i 0 H-
c a O3
2
o 0 rr 0
ff-0 0 O ft B
0
ocn n c 0raquoO 0 0
B 0 0 31
M O bullO
CD cr
i0
0
aB
I I i i i
O i i
bull9 ^O
I 1 I
OOJ n c o-o rt 9 O 0
f
M
LA
QC
amp r
u raquo rgt O-
t
O C
pound
-C
djr
CD1 lt raquo
O
mft 9
H3 OQ
9
mnit oo o
7
mltrtO O MO
0 3 1mdash9
o a
H-O
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ANALYTICAL REPORT
Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301
Project Tinkham Garage
FD Case 1856
Section Seven General Chemistry
NET Job Number 9601771
National Environmental Testing Inc
Cambridge Division 12 Oak Park
Bedford MA 01730
Massachusetts Certification Number M NA023
TABLE
ALKALINITY NARATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLET AMMONIA NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was found to be within the 15 laboratory control limits The blank was less than the detection limit
TABLE BOD NARRATIVE SUMMARY
FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes
LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit
TABLE COD NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit
TABLE AQ CHLORIDE NARRATIVE SUMMARY
FD1328
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET NITRATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLE 7
SULFATE NARRATIVE SUMMARY FD 1856
GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
TABLET
TOTAL ORGANIC CARBON NARRATIVE SUMMARY
FD1856
GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number
HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times
QUALITY CONTROL
All ICVs and CCVs were within the 15 laboratory control limits
No ICBs or CCBs detected analytes greater than the detection limit
MATRIX SPIKE The spike recoveries were within the 25 control limits
DUPLICATE The result of the duplicate sample analyses were within 20 RPD
NET Cambridge Division
ANALYTICAL REPORT
Report Date 06181996
Report To GE1 ConsultantsNH
Project Tinkham Garage
NET Job No 9601771
Date Recd 05211996
Sample ID NET ID Result Units Run Batch
Analysis Date Analyst
Alkalinity
92113-NAI-H2-0596 92113-NAI-C3-0596
AQ EPA 3101
148541 148542
150 68
ppmCaC03 ppmCaC03
308 308
05301996 05301996
dec dec
Ammonia
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3501
148541 148542
039 038
mgL N mgL N
06131996 06131996
nsv nsv
BOO shy 5 day
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 4051
148541 148542
lt20 lt20
mgL mgL
501 501
05261996 05261996
dec dec
Chemical Oxygen Demand
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ COD 4104 mod
148541 148542
25 47
mgL mgL
330 330
05281996 05281996
dlw dlw
Chloride - Technicon AQ EPA 3252
92113-NAI-M2-0596
92113-NAI-C3-0596
148541
148542
31
140
mgL mgL
48 48
06101996 06101996
nsv nsv
Nitrate-calc
92113-NAI-M2-0596 92113-NAI-C3-0596
AQ EPA 3532
148541 148542
0052 lt0020
mgL N mgL N
42 42
06071996 06071996
nsv nsv
70030
NET Cambridge Division ANALYTICAL REPORT
Report Date 06181996
Report To GEI ConsultantsNH NET Job No 9601771
Project Tinkham Garage Date Recd 05211996
Run Analysis Sample ID NET ID Result Units Batch Date Analyst
Phosphate ortho AQ EPA 3653
92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw
Sulfate-Turbidimetric mod AQ EPA 3754 mod
92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu
Total Organic Carbon TOC AQ EPA 4152
92113-NAI-H2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw
700-jI
NET Cambridge Division
BATCH QUALITY CONTROL DATA
Report To GEI ConsultantsNH NET Job No 9601771
Program Tinkham Garage Report Date 06181996
LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst
Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw
Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample
LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported
Alkalinity EPA 3101
Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor
pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=
Prep_ j_ TrueValue=
pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot
Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)
Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS
0 D 385 2ZS 77
bulli Hue 71
K 3JS S40 35Zgt
00
37T
33 6 nzraquo
531
73
bullI] 11AO
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0 0271501 10120 476 0084L 0008
10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45
K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1
18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy
nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy
1 1 0110 1 0042 1 1 0024
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0008
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700
BOD EPA 4051 Labsys Batch _
Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor
Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf
2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW
p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008
Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD
Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3
SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )
fj f5
^Traquo ^9 ^LCSI a 3^f _5-7 owtf LCS II ^bullZf 3-77- ^5^ ^bull75
^l AWC-^1 03 $ltst I
1 ti^l $ amp4ol ft) ^^3 ^17- lt2
r 3d S35^ 6-1-6 lt2_ lt2lt2
pound X tiT-laquosa D ^5T 7 I ^-4 ifo 2 gM^4
poundL iv ^-f3 -if Hd ltL lt2c h o X-33
i4lt43L Hlfi-T-tt 0~$ f55^ 1 ^raquoSl^
3 3 - 3 D ^-33 ^08
5 36 ^ 3 4 41 cL ^2amp
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CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst SupervisorSpike Prep
Date
bullff
Labsys Batch gt - 7
True Value ^b j BigL
LCS Prep 7C True Value pound$ 7j rogL
Rack Number 1
531
^0-7
1727
la
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If
776
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701
NET
CHEMICAL OXYGEN DEMAND EPA 4104 Page
Analyst Date pound61T Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 600 ran wavelength
Blank otgto Correlation R = I i 10 sgto
Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx
Job No Sample No ABS mgL Dil mgL Final Rec Comments
BLANK oampo LCS
70
OH1
Ho 00^shy
BLANK 00 0 ZlS LCS
51 4 DC 05 fe
0-7
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HID 00k IK C70 700
CHEMICAL OXYGEN DEMAND EPA 4104 Page
I alyst ervisor
Date -viO Labsys Batch 7
Job No Sample No ABS mgL Oil mgL Final Rec Comments
r7(i So ozr HI BLANK
( C O O t~ amp LCS ^0 7g7
pound^l 0^ J zx 3fO
^V bull Of 9 S5
pur ^^fc -oZGgt 50
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020
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602
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bull47 505i
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Analyts
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Labsys Batch
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I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page
Analyst Date Labsys Batch Supervisor
Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt
0010 Standard Stock No
010 04C 030 Intermediate standard iLlaquo Prepared n ^gt (e-n 050 1lt 070 ICV prep A
ICV True Value mgL
Job No Sample No ABS mgL Oil mgL Final Rec Comments
ICV poundU a7i bull172 llaquo3- ICB oov gtt 5
01^
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ccv CCB
J101 r
1 Sulfa ite EPA 3754M
1 Analystj ltgt Date5 felabsvs B atch Supervise raquor
1 Cafibrant lotll^-^
LCS lot ^^0 |1ltA L ltF LCS Prep 0o LCS True Value= bull ntu laquo W^V ^jU^jW
1 Value(mgL) Reading(ntu)
04 bull1 r value= bull raquo
1 5 51
i 10 bulljJ Spike Stock
rjfc pound ft-ytf ^ 20 83-1 Spike prep (jjf~I tlaquo-3 10 ^^
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i Job- Sample Turbidity (ntu) mgL Sample Sample pH Turbidity(NTU) Dilution 1 2 3 4 mgL Final
lamp U^ f- r-i RtK LH
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NET - Dayton Total Heterotrophic Plate Counts
Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411
June 5 1996
Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301
Dear Richard
Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions
Sincerely
Peter Conroy Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05201996
JOB NUMBER
SAMPLE NO
92113-DVE-07-0596 B00733
PAGE 2
9606991
347306
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 15600 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 3 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347307
Sample Description NAI-MI-0596 B00734 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 7400 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347308
Sample Description 92113-NAI-K2-0596 B00735 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 1650 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 5 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347309
Sample Description 92113-OW2D-0596 B00736 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count 9500 CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 6 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730
SAMPLE NO 347310
Sample Description 92113-LGAW-0596 B00737 Client Project ID
Date Taken 05151996 Date Received 05161996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05161996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05251996 12 Oak Park Bedford MA 01730 NET Job Number 9607118
Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996
National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed
Reproduction of this analytical report is permitted only in its entirety
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW20-0596 B00749
PAGE 2
9607118
347716
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 540 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816
NET - CAMBRIDGE 12 Oak Park Bedford MA 01730
Sample Description Client Project ID
ANALYTICAL REPORT
05251996
JOB NUMBER
SAMPLE NO
92113-FW11D-0596 B00750
PAGE 3
9607118
347717
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 620 CFUmL 05181996 dgr
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816
PAGE 4 ANALYTICAL REPORT
05251996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607118 Bedford MA 01730
SAMPLE NO 347718
Sample Description 92113-FD01-0596 B00751 Client Project ID
Date Taken 05171996 Date Received 05181996
Parameter Result Unit Date Anal Analyst
Plate Count 600 CFUmL 05181996 dgr
NATIONAL OH 45439 ENVIRONMENTAL
Tel (513)2946856 NET Fax (513)294-7816
ANALYTICAL REPORT
NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9607058
Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis
Sample Date Date Number Sample Description Taken Received
347507 92113-ERT01-0596 B 00746 05161996 05171996
National Environmental Testing Inc certifies that the analytical results containedanalyzed
herein apply only to the specific samples
Reproductionentirety
of this analytical report is permitted only in its
Enclosure Project Coordinator
Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816
PAGE 2 ANALYTICAL REPORT
05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9607058 Bedford MA 01730
SAMPLE NO 347507
Sample Description 92113-ERT01-0596 B00746 Client Project ID
Date Taken 05161996 Date Received 05171996
Parameter Result Unit Date Anal Analyst
Plate Count CFUmL 05171996 kkh
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