net: fd case 1856 inorganicssection. please find enclosed a diskette of the results for this case....

NET FD Case 1856 Inorganics

Cambridge Division NATIONAL 12 Oak Park Bedforo MA 01730 ENVIRONMENTAL Tel (6171 275-3535 NET TESTING INC Fax (617) 275-7411

June 17 1996

Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional DriveConcord NH 03301

RE Tinkham Garage

Dear Mr Mullin

Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1856 NET job number 9601771)

This narrative addresses all comments for all samples as listed below

NET JOB NUMBER 9601771

SAMPLE NET DATE TIME DATE ID ID TAKEN TAKEN RECD MATRIX

92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 K8542 05201996 1315 05211996 GROUND WATER

Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING INC Fax (617) 275-7411

All laboratory comments for the data packages have been summarized in the following tables

Sample Receipt and Login TABLE 1 Metals and Cyanide Analysis TABLE 2 Volatile Organics Analysis No Analysis Requested Semi-Volatile Organics Analysis No Analysis Requested PesticidePCB Organics Analysis No Analysis Requested Herbicides Analysis No Analysis RequestedWet Chemistry Analysis Requested TABLE 7

These narrative tables are also enclosed with each data package section

Please find enclosed a diskette of the results for this case

Thank you for this opportunity to be of service to you Please do not hesitate to call or write if you have any questions or require further information

Sincerely

Peter M ConroyProject Manager

enclosures

TABLE 1 SAMPLE RECEIPT amp LOGIN

FD1856

GENERAL COMMENTS No comments were necessary

TABLE 2 METALS NARRATIVE SUMMARY

FD1856

GENERAL COMMENT No comment necessary

HOLDING TIMES All samples were digested and analyzed within contractual holding times

QUALITY CONTROL

All ICVs and CCVs were within the CLP ILM030 control limits for all analytes

A CRDL standard was analyzed for each AA and ICP instrument run for all required elements

The value of the ICB and CCBs did not exceed the CRDL for all analytes

The ICP interference check sample was analyzed according to CLP ILM030 protocol The results were within the control limits of 20 of the true value for analytes included in the interference check standards

DIGESTION SPIKE The digestion spike recoveries were within the 25 control limits for all analytes analyzed

Exceptions are granted in a situation where the sample concentration exceeds the spike concentration by a factor of four or more In this case the data is reported unflagged

All analytes that did not meet the specified criteria were flagged with an N for the associated samples

DUPLICATE The result of the duplicate sample analysis was within 20 RPD for all analytes

A control limit of 20 RPD is not used when either the original or duplicate sample values are less than 5X the CRDL Control limits are not applicable when both values are below the CRDL

All analytes that did not meet the specified criteria were flagged with a for the associated samples

LCS and PREPARATION BLANK The LCS and preparation blank analyzed were found to be within the acceptable limits

MSA No samples required analysis by method of standard additions for the specified furnace elements

ISD The ICP serial dilution was analyzed according to the CLP ILM030 protocol The five fold dilution values were within 10 difference for all ICP analytes

Exceptions are granted in a situation where the sample concentration is less than fifty times the IDL

All analytes that did not meet the specified criteria were flagged with an E for the associated samples

TABLE

ALKALINITY NARATIVE SUMMARY

FD1856

GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number

HOLDING TIMES All samples were digesteddistilled and analyzed within contractual holding times

DUPLICATE The result of the duplicate sample analyses were within 20 RPD for all analytes

LCS and PREPARATION BLANK The LCS was found to be within the 20 laboratory control limits The blank was less than the detection limit

TABLET

AMMONIA NARRATIVE SUMMARY

FD1856

GENERAL COMMENTS Sample duplicate was identified as S2 preceded by the sample number Sample spike was identified as DS preceded by the sample number


QUALITY CONTROL

All ICVs and CCVs were within the 15 laboratory control limits

No ICBs or CCBs detected analytes greater than the detection limit

MATRIX SPIKE The spike recoveries were within the 25 control limits

DUPLICATE The result of the duplicate sample analyses were within 20 RPD


TABLE BOD NARRATIVE SUMMARY

FD 1856





TABLE COD NARRATIVE SUMMARY

FD1856

GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by sample number Sample spike will be identified with DS preceded by sample number


QUALITY CONTROL





LCS and PREPARATION BLANK The LCS was within the 15 laboratory control limit The blank was less than the detection limit

TABLE AQ CHLORIDE NARRATIVE SUMMARY

FD1328

GENERAL COMMENTS Sample duplicate will be identified with S2 preceded by the sample number Sample spike will be identified with PS preceded by the sample number


QUALITY CONTROL



MATRIX SPIKE Spike recoveries were within the 25 laboratory control limits


TABLE NITRATE NARRATIVE SUMMARY

FD 1856



QUALITY CONTROL





TABLE ORTHO PHOSPHATE NARRATIVE SUMMARY

FD 1856

GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with PS preceded by the sample number


QUALITY CONTROL





TABLE 7

SULFATE NARRATIVE SUMMARY FD 1856



QUALITY CONTROL



MATRIX SPIKE The spike recoveries were within 25 control limits


TABLE

TOTAL ORGANIC CARBON NARRATIVE SUMMARY

FD1856

GENERAL COMMENTS Sample duplicate was identified with S2 preceded by the sample number Sample spike was identified with DS preceded by the sample number


QUALITY CONTROL





= I rn No

i FT Lab Sample i MiiMshy

[raquoat FPC ^ 2 ii o ~ l

I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O

r-LF L a b S a m p l e 11 x4 i

Ddte Fec a i PU C-5

U r i t n _ ue ign t ) U

1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

I

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Nshy

N

N1

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hi

1 1 v

j (

(j gtbullshy

L

( r ~ i t

bullgt

1

h t

- 1

- t

~

i bull gt lt -

ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N

C 1 T shy1 shy c t CLLAFv 1 t UT e

L j - o t ^ i j shy nr CLf i-iR A t i fsct

-0003

NET Cambridge Division ANALYTICAL REPORT

Report Date 06181996

Report To GEI ConsultantsNH

Project Tinkham Garage

NET Job No 9601771

Date Recd 05211996

Sample ID NET ID Result Units Run Batch

Analysis Date Analyst

Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec

Chemical Oxygen Demand

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw

Chloride - Technicon

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

NET Cambridge Division

ANALYTICAL REPORT


Report To GE1 ConsultantsNH NET Job No 9601771

Project Tinkham Garage Date Recd 05211996

Run Analysis Sample ID NET ID Result Units Batch Date Analyst

Phosphate ortho AQ EPA 3653

92113-NAI-H2-0596 148541 011 mgL 92 05211996 dlu 92113-NAI-C3-0596 148542 0044 mgL 92 05211996 dlw

Sulfate-Turbidimetric mod AQ EPA 3754 mod

92113-NAI-H2-0596 148541 36 mgL 25 05241996 dlw 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlw

Total Organic Carbon TOC AQ EPA 4152

92113-NAI-M2-0596 148541 53 mgL 251 05291996 dlw 92113-NAI-C3-0596 148542 67 mgL 251 05291996 dlw

ANALYTICAL REPORT

Report To Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional Drive Concord NH 03301


FD Case 1856

Section One

NET Job Number 9601771

National Environmental Testing Inc

Cambridge Division 12 Oak Park

Bedford MA 01730

Massachusetts Certification Number M MA023

TABLE OF CONTENTS

Section 1 Report Front

1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents

NarrativeCover Letter

Main PageSample CrossReference

Chain of Custody Forms

Sample Receipt Logbook

Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_

Data QualifierFlag Descriptions pound6V o

Document Inventory Sheets COY

Control Charts fi)pound

Section 2 Metals Analysis Data 20001

Section 3 Volatiles Analysis Data No Analysis Requested

Section 4 Semi-Volatiles Analysis Data No Analysis Requested

Section 5 PesticidesPCBs Analysis Data No Analysis Requested

Section 6 Herbicide Analysis Data No Analysis Requested

Section 7 Wet Chemistry Analysis Data 70000

100J1

Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617)275-3535 NET TESTING INC Fax (617) 275-7411

June 17 1996

Mr Bob Mullin GEI ConsultantsNHSuffolk Building53 Regional DriveConcord NH 03301

RE Tinkham Garage

Dear Mr Mullin




SAMPLE NET DATE TINE DATE 10 to TAKEN TAKEN RECO MATRIX

92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER

103







Sincerely

Peter M Conroy Project Manager

enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7



MSA No samples reguired analysis by method of standard additions for the specified furnace elements




TABLE


FD1856





bull103^7

TABLE AMMONIA NARRATIVE SUMMARY

FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +

11 Report To Reported By

11 Mr Bob Mullin National Environmental Testing

1 GEI Consul tantsNH NET Atlantic Incorporated

1 Suffolk Building Cambridge Division

1 53 Regional Drive 12 Oak Park

1 Concord NH 03301 Bedford HA 01730

1

Report Date 06171996 NET Job Number 9601771

Project Tinkham Garage NET Client No 14755

PO No 8307 Collected By RVan Etten Shipped Via FedEx

Job Description Tinkham Airbill No

This report has been approved and certified for release by the following staff Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments

Peter M Conroy NET Project Manager

Analytical data for the following samples are included in this data report

SAMPLE NET DATE TIME DATE

ID ID TAKEN TAKEN RECD MATRIX

92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER

92113-NAI-C3-0596 148542 05201996 1315 05211996 GROUND WATER

Note Where a compound or analyte is not detected the result is reported as less than (lt) the laboratory reporting limit

011

Inorganic CLP BOW 390Data Qualifier

Form I-IN includes fields for three types of result qualifiers

c Qualifier - (concentration qualifier)

laquoB - If the reported value is less that the Contract required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL)

Un - Analyte was not detected The result of the analyte is less than the Instrument Detection Limit (IDL)

Q Qualifier shy

E - The reported value is estimated because of the presence of interference If the 5-fold dilution analysis for one or more analytes is not within 10a chemical or physical interference effect must be suspected and the data for all affected analytes in the samples received associated with that serial dilution must be flagged with an E on Form IX-IN and Form I-IN

M - Duplicate injection precision notmet

N - Spike sample recovery not within control limits

laquoS - The reported value was determined by the Method of Standard Addition (MSA)

W - Postdigested spike for Furnace AA analysis is out of control limits (85-115) while sample absorbance is less than 50 of spike absorbance

raquobulllaquobull - Duplicate analysis not within control limits

laquoi+laquo _ Correlation coefficient for the MSA is less than 0995

X (Method) Qualifier shy

P - for ICP

A - for Flame AA

F - for Furnace AA

CV- for Manual Cold Vapor AA

CA- for Midi-Distillation spectrophotometric

NR11- if the analyte is not required to be analyzed 1031

EPA CLP 390 Deliverables Inventory

Project Name GEI ConsultantsNH Tinkham Garacre NET Job Numbers 9601771 FD Number FD 1856

ITEM PAGE

INORGANIC ANALYSIS DATA PACKAGE 2 0001

Inorganic Analysis Data Sheets 0002

OC Report- Initial and Continuing Calibration OC Reoort- CRDL Standards OC Reoort- Blanks OC Report- ICP Interference Check Sample OC Report- Spike Sample Recovery

22222

2222222

0004 0007 0008 0010 0011

OC Report- Post Digest Spike Recovery NR OC Reoort- Duplicates OC Repprt- Laboratory Control Sample OC Report- Standard Addition Results OC Report- ICP Serial Dilutions OC Reoort- Instrument Detection Limits OC Report- Interelement Correction Factors OC Report- ICP Linear Ranges

0012 0013 0014 0015 0016 0017 0020

OC Report- Preparation Log 0021 OC Report- Analysis Run Logs

Raw Data- ICP Listings

2

2

22

0022

0024 Raw Data- Combined Compounds (Se As Tl Pb) NR Raw Data- Sb Worksheet (s) NR Raw Data- As Worksheet (s) NR Raw Data- Cd Worksheet (s) NR Raw Data- Pb Worksheet (s) NR Raw Data- Se Worksheet (s) NR Raw Data- Tl Worksheet (s) NR Raw Data- Ha Worksheet (s) NR Raw Data- CN Worksheet (s) NR Raw Data- Sample Preparation Log(s) Raw Data- Working Standard Preparation Log(s)

0042 0045

10310

ANALYTICAL REPORT



FD Case 1856

Section Two Metals Analysis




Bedford MA 01730

Massachusetts Certification Number M NA023


FD1856



QUALITY CONTROL


A CRDL standard was analyzed for each AA and ICP instrumentfor all required elements

run

The valueanalytes

of the ICB and CCBs did not exceed the CRDL for all














Project Name GET ConsultantsNH Tinkham Garage NET Job Numbers _JL6_ 01771 FD Number FD 1856

ITEM PAGE

INORGANIC ANALYSIS DATA PACKAGE 0001


OC Report-OC Report-OC Report-OC Report-QC Report-OC Report-OC Report-OC Report-OC Report-

Initial and Continuing Calibration CRDL Standards Blanks ICP Interference Check Sample Spike Sample Recovery Post Digest Spike RecoveryDuplicatesLaboratory Control Sample Standard Addition Results

OC Report-OC Report-

ICP Serial Dilutions Instrument Detection Limits

OC Report- Interelement Correction Factors OC Report-QC Report-QC Report-

ICP Linear Ranges Preparation Log Analysis Run Logs

Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-Raw Data-

ICP Listings Combined Compounds Sb Worksheet(s) As Worksheet(s) Cd Worksheet(s) Pb Worksheet(s) Se Worksheet(s)

(Se As Tl Pb) 0024

NR NR NR NR NR NR

Raw Data-Raw Data-Raw Data-

Tl Worksheet(s) Hg Worksheet(s) CN Worksheet(s)

Raw Data- Sample Preparation Log(s) 2

NR NR NR 0042

Raw Data- Working Standard Preparation Log(s) 0045

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Lfr No GET G No

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l

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1 1 1

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j 4 ~ r _ _ _ _ gt _

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1

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1

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1

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t 1 tI l

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1 1

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1 1

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1 1

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1 r

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1 1

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k 1

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1 1 bull lt 1 t 1 1

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1 1 1 i t t t i

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raquo t

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1 )

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X ii i 1 ) l

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1 1

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1 1

1 I

l 1

bull X i t 1I

bullt

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l 1

1

l t

t 1

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1 1

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l 1 i

l

1 t

1 1

1 1

1 )

I V bullA 1

I

11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

1 1

x 11 t 4

1 1

1 1 bull

i 1

1 t

1 1

t 1

1 1

1 1

i r lt t i l X ii igt 1t

1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

t l

1 1 i i t tgt raquoi 11 i

( 1

1 t

1 1

t 1

1 1

1 t

gt 1

t 1

i gt gt i l l i

t1 l 1

( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract

it -gt- i jSC f-u 6- -bull 5A3 No GEI

Hethod P

End date 06079

Analytes i t

__ in bull - 7 i IT fe bull r A ^ i A t bull i c s c C C c F P M 11 H N iK s A ri T 2 C i [bull - - iD A R 0 (J E R G H O i l i E - S l H i L H S N 1 t i i t bull i ( 1

1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l

1 I 1 1 1 i 1 1IT- i 00 i ]bull 1 1 1 X 1 1 I bull I 1 lt

1 i f l 1 _ 1 1 5raquoO p - i _ _ _ bdquo _ 1 1-

1 1 1 1 -bull l C^1 rlt5 - t bull - bdquo _ _ _ _ _ _ bull _ 1 I i ( t

I l lw ~ L (K- lt bullbull bull i i

raquo - i

I raquo 1 i i i i t t it - 1 bull i 0gt r ^ ___trade

r t i t i gt i i 1 i r

bull bull bull bull i bullgt rii bull i | i 1 i I [I

i t I 1 I raquo

I bull i 1 I bullbull bull t t ( I - _ _ _bdquo

t i i j - v gt gt i t 1 1

1 1 1 I bull bull t ii X 1 _ bdquo _ 1

-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I

ov bull gt - lt bull

i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1

t ) 11 i X I t l l t raquo t

i i 1 1 1 1 bull 1 I f 11 1 i 0 - -i 1 1 J bull I I It

mdash mdash mdash 1 I I i gt t I bull V u i ij i bullbull X _ 1 1 1 I _ 1 _ -- ~~ mdash mdash

1 1 ) S 1 1 - 1 t l r - 0 bull iu i X t t l i t -1 i i

1 1 i t i t -1 i i 1 i i i

i i bull i i i i-i 1 i bull i i i - i t i bull i

i i i 1 ( 1 i 1 t i i i i i I i i bull i 1 t i - _ _ _ bull shy

) r i i i 1 I bull 1 i bull t (

i t i 1 1 t i 1 i i li r i gt t bull gt I )

i i i i 1 1 1 i t i i - gt 1 1 1

t t gt i i ) I t i gt 1 1 1 l i t bull i t 1 1 (

I I I ) i t l i gt i I 1 1 t l 1 i t i t 1 i l i i i 1 1 1

i i t 1 i bull i i gt i i 1 1 1 i t i i t i t 1 1 I 1 I 1 1 1

-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1

i lt t bull bull 1 t 11 1 1 1

gt - bull ( 1 I t 1 t gt 4 1 1 1

__ 1 __ ^ ^ f _ ) iijrri_ _ _ bdquo _ _ _ i i bull t i l lt 1 1

1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe

Run id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Element Multi-Element

Time 1607 Processing protocol 390

Sample Code Preparation Client ID Date Time Meth Batch Date

1 BLANK X P 041696 ZZZZZZ 060796 1432 2 SPEC X P 042396 ZZZZZZ 060796 1434 3 ICV1A ICV P 041696 ICV 060796 1437 4 ICAP19 ICV P 042296 ICV 060796 1439 5 CALB ICB P 091295 ICB 060796 1441 6 ICSA ICSAO P 042896 ICSA 060796 1443 7 ICSAB ICSABO P 042396 ICSAB 060796 1445 8 2XCRDLAB CRIO P 042396 CRI 060796 1447 9 STD1 CCV P 042696 CCV 060796 1449 10 CALB CCB P 091295 CCB 060796 1451 11 LCSHCL X P 6422CW 032494 ZZZZZZ 060796 1454 12 PBW X P 6422CW ZZZZZZ 060796 1456 13 1760-148486 X P 6422CW ZZZZZZ 060796 1458 14 1760-148487 X P 6422CW ZZZZZZ 060796 1500 15 1760-148488 X P 6422CW ZZZZZZ 060796 1502 16 1760-148488 X P 6422CW ZZZZZZ 060796 1504 17 1760-148489 X P 6422CW ZZZZZZ 060796 1506 18 1760-148489 X P 6422CW ZZZZZZ 060796 1508 19 1760-148489 X P 6422CW ZZZZZZ 060796 1510 20 1760-148489 X P 6422CW ZZZZZZ 060796 1512 21 STD1 CCV P 042696 CCV 060796 1514 22 CALB CCB P 091295 CCB 060796 1516 23 1760-148490 X P 6422CW ZZZZZZ 060796 1518 24 LCSHCL LCSW P 6424CW 052996 LCSW 060796 1520 25 PBW PBW P 6424CW 052996 PBW 060796 1522 26 1771-148541 S P 6424CW 052996 92113-NAI-M2 060796 1524 27 1771-148541 ISD P 6424CW 92113-NAI-M2L060796 1526 28 1771-148541 PS P 6424CW 92113-NAI-M2A060796 1528 29 1771-148541 DS P 6424CW 052996 921 13-NAI-M2S060796 1531 30 1771-148542 S P 6424CW 052996 92113-NAI-C3 060796 1533 31 1771-148542 S2 P 6424CW 052996 92113-NAI-C3D060796 1535 32 LCSHCL LCSW P 6416CW 052396 LCSW 060796 1537 33 STD1 CCV P 042696 CCV 060796 1539 34 CALB CCB P 091295 CCB 060796 1541 35 PBW PBW P 6416CW 052396 PBW 060796 1543 36 1746-148405 S P 6416CW 052396 92113-FW05-O5060796 1545 37 1746-148406 S P 6416CW 052396 92113-ERT01-0060796 1547 38 1746-148406 ISD P 6416CW 92113-ERT01-0060796 1549 39 1746-148406 PS P 6416CW 921 13-ERT01-0060796 1551 40 1746-148406 DS P 6416CW 052396 92113-ERT01-0060796 1553 41 1746-148406 S2 P 6416CW 052396 92113-ERT01-0060796 1555 42 1746-148407 S P 6416CW 052396 92113-FW04-05060796 1557 43 1746-148408 S P 6416CW 052396 92113-ERT02-0060796 1559

24

3 3 Sample Code Preparation Client ID Date Time _ Meth Batch Date

bullM 1746-148409 S P 6416CW 052396 92113-FW08D-0060796 1601 5 STD1 CCV P 042696 CCV 060796 1603

gt CALB CCB P 091295 CCB 060796 1605 47 1746-148410 S P 6416CW 052396 92113-FW21D-0060796 1608 3 ICSA ICSA1 P 042896 ICSA 060796 1610 9 ICSAB ICSAB1 P 042396 ICSAB 060796 1612 50 2XCRDLAB CRI1 P 042396 CRI 060796 1614 L STD1 CCV P 042696 CCV 060796 1616 gt CALB CCB P 091295 CCB 060796 1618

A T H E N A 3 06e

-e

ltun id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM analytical method P Time 1607 Element Fe Processing protocol 390

INSTRUMENT RUN QC REPORT

CALIBRATION VERIFICATIONS

osition Sample ID Code True Value Found Value Recovery

4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036

9 STD1 CCV 100000000 101600000 1016 21 STD1 CCV 100000000 102090000 1021 33 STD1 CCV 100000000 105080000 1O51 45 STD1 CCV 100000000 104320000 1043 51 STD1 CCV 10000OOOO 103940000 1O39

CALIBRATION BLANKS

osition Sample ID Code CRDL Found Value Flag

5 CALB ICB 1000000 130000 U

10 CALB CCB 1000000 213000 B 22 CALB CCB 1000000 56000 U 34 CALB CCB 1000000 103000 U 46 CALB CCB 1000000 11 1000 U 52 CALB CCB 1000000 221000 B

CRDL STANDARDS


INTERFERENCE CHECK STANDARDS


6 ICSA ICSAO 2000000000 1704100000 852 48 ICSA ICSA1 2000000000 1750500000 875 7 ICSAB ICSABO 2000000000 1707700000 854 49 ICSAB ICSAB1 2000000000 1750600000 875

A T H E N A 306e

3un id 19 9615930 Acquired 060796 by GMP JP3IN WON MODEL 50 ICP Crunched 061196 by JEM M ilytical method p Time 1607 E-rement Fe Processing protocol 390

F_laquoL 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000

3c Sample Code Dil M Prep P Solution Final Units Flags Batch C meas mgL Cone n

BLANK X 100 P 00000 ugL Z -L SPEC X 100 P 00000 ugLZ 3 ICV1A ICV 100 P 517890 5178 9000 ugL bull ICAP19 ICV 100 P 106280 10628000 ugL

_ CALB ICB 100 P 001300 13 0000 ugL U 6 ICSA ICSAO 100 P 17041000 1704100000 ugL ICSAB ICSABO 100 P 170 77000 1707700000 ugL 2XCRDLAB CRIO 100 P 027375 2737500 ugL

9 STD1 CCV 100 P 10 16000 10160 0000 ugL 3O CALB CCB 100 P 002129 21 3000 ugL B 1 LCSHCL X 100 w 6422CW P 103180 1031 8000 ugL t= PBW X 100 w 6422CW P 012435 124 3500 ugL 13 1760-148486 X 100 w 6422CW P 15 71400 15714 0000 ugL 1 1760-148487 X 100 w 6422CW P 35 90300 35903 OOOO ugL 1_ 1760-148488 X 100 w 6422CW P 10 20200 10202 0000 ugL 16 1760-148488 X 100 w 6422CW P 10 68300 10683 0000 ugL 1 1760-148489 X 100 w 6422CW P 16 68600 16686 0000 ugL 1 1760-148489 X 500 w 6422CW P 340080 17004 0000 ugL R 1 1760-148489 X 100 w 6422CW P 16 70500 16705 0000 ugL 20 1760-148489 X 100 w 6422CW P 17 74800 17748 OOOO ugL 2 STD1 CCV 100 P 10 20900 10209 0000 ugL 2= CALB CCB 100 P 000556 56000 ugL U 23 1760-148490 X 100 w 6422CW P 48 96200 48962 0000 ugL 2 LCSHCL LCSW 100 w 6424CW P 103140 1031 4000 ugL 2_ PBW PBW 100 w 6424CW P 003874 38 7400 ugL B 26 1771-148541 S 100 w 6424CW P 16 32200 16322 OOOO ugL 2 1771-148541 ISD 500 w 6424CW P 339700 16985 0000 ugL 2 1771-148541 PS 100 w 6424CW P 16 45400 16454 OOOO ugL 29~ 1771-148541 DS 100 w 6424CW P 17 67600 17676 0000 ugL 30 1771-148542 S 100 w 6424CW P 091832 918 3200 ugL 3 1771-148542 S2 100 w 6424CW P 087462 874 6200 ugL 3= LCSHCL LCSW 100 w 6416CW P 111230 1112 3000 ugL 33 STD1 CCV 100 P 10 50800 10508 0000 ugL 3 CALB CCB 100 P 001026 10 3000 ugL U 3_ PBW PBW 100 w 6416CW P 005482 54 8200 ugL B 36 1746-148405 S 100 w 6416CW P 29 02100 29021 0000 ugL 3 1746-148406 S 100 w 6416CW P 021106 211 0600 ugL 3 1746-148406 ISD 500 w 6416CW P 004421 221 0500 ugL B 39 1746-148406 PS 100 w 6416CW P 041221 412 2100 ugL 40 1746-148406 DS 100 w 6416CW P 119440 1194 4000 ugL 4 1746-148406 S2 100 w 6416CW P 039801 398 0100 ugL

A T H E N A 306e

-e

id 19 9615930 Acquired 060796 by GMP JOBIN WON MODEL 50 ICP Crunched 061196 by JEM Analytical method P Time 1607 ilement Fe Processing protocol 390

RDI_ 10000 IDL 1500 Default wavelength 2599400 _inear range 50000000

os Sample Code Oil M Prep P Solution Final Units Flags Batch c meas mgL Cone n

42 1746-148407 S 1 00 U 6416CW P 40 64000 40640 0000 ugL 43 1746-148408 S 1 00 W 6416CW P 10 93500 10935 OOOO ugL 44 1746-148409 S 100 W 6416CW P 19 89200 19892 0000 ugL 45 STD1 CCV 100 P 10 43200 10432 0000 ugL 46 CALB CCB 100 P 001112 11 1000 ugL U 47 1746-148410 S 1 00 W 6416CU P 305680 3056 8000 ugL 48 ICSA ICSA1 100 P 175 05000 175050 0000 ugL 49 ICSAB ICSAB1 100 P 175 06000 175060 0000 ugL 50 2XCRDLAB CRI1 100 P 031292 312 9200 ugL 51 STD1 CCV 1 00 P 10 39400 10394 0000 ugL 52 CALB CCB 100 P 002206 22 1000 ugL B

28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996

Results for STDCCB Measures 2 (R)

EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC

Elements of SIMULTANEOUS

$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996

Results for STDSPEC Measures -2 (R) raquo

EL SIGNALsigma

Fes 3923S 008

Intensities for Recalibration El Wave LOUFe$ 259940 STDCCB

Measurements for SPECXshy

16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083

170013 52996 Method COMM

Sampla SPECXshy shyor Simul

EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM

1 MEAS= 3 for Seq tMEAS= 2 f

Measuremants for ICV1AICV- shy 1

200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM


Sample ICV1AICV- shy 1 MEAS= 3 for Seq 2 for Simul

EL CONC sigma

$Fe 4S676 029

Measurements for ICAP19ICVshy shy 1


$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM


Sample ICAP19ICVshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul

laquo

EL CONS sigma

SFe 1 0272 064

Measurements for CALBICBshy shy 1


SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM


Sample CALBICB- shy 1 MEAS= 3 for Seq MEAS for Simul

EL CONC sigma

$Fe 0 00426 150

Measurements for ICSAICSAOshy shy 1


Ô 7 7 + J O ^ 7 bull mdash -3 VWWWVv1^- V - W W-A- OQ 7 _ O O raquo 7 laquo_ O X bullraquogt V 7 f J~ Il

65960 000000 000000 65960 65960 17519 PPM

bull 170946 52996 Method COMM

Sample ICSAJlCSAOshy shy 1 MEA3= 3 for Seq ttrtEAS= 2 for Simul

EL CONC sigma

$Fe 17514 004i

Measurements for ICSABICSABshy shy 1


SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM


Sample ICSABICSABshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul

EL CONC sigma

$Fe 17297 046

Measurements for 2XCRDLABCRshy shy 1


$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM


Sample 2XCRDLABCRshy shy 1 MEAS= 3 for Seq SMEAS = 2 for Simul

EL CONC sigma

$Fe 029397 31

Measurements for CCV1CCVshy shy 1


bull-EF-e 25994O 23315 000000 000000 38315 33315 93880 PPM 33986 000000 OCOOOO 38986 33986 9933ft PPM

j 10-UD U^7 70 -~ - - I ici-i igt^v-i bull v-wi n i

Sample CCVllCCV- shyfor Simul

EL CONC sigma

SFe 99108 032

Measurements for CALBCCB- shy


$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060


Sample CALBCCB- shyfor Simul

EL CONC sigma

SFe 001784 89

raquo raquo

Measurements for LCSHCLLCSW- shy


SFe 259940 53290 000000 000000 5329053130 000000 000000 53130


Sample LCSHCLLCSW- shy= 2 for Simul

EL CONC sigma

SFe 096926 031

Measurements for PBWPBW- shy


F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430

172406 52Q6 Method COMM

P5WP6W- shy

1 MEAS= 3 for Seq MEAS=shy

1

17900 002902 PPM 17060 000666 PPM

1 MEAS= 3 for Seq MEAS=

1

53290 097139 PPM 53130 096713 PPM

1 MEAS= 3 for Seq ttMEAS

1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29

Measurements for 1699-148150shy


$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM


Sample 1699-148150- - 1 MEAS= 3 for Seq MEAS = 2 for Simul

EL CONC sigma

$Fe 5476S 041

Measurements for 1727-148287shyraquo

Elementsof SIMULTANEOUS

$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041

Measurements for -148288S-


SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM


Sample -1482385shy shy MEAS= 3 for Seq MEAS 2 for Simul 20Q3

EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM


Sample -148289Sshy shy 1 MEAS= 3 for Seq MEAS 2 for Simul

EL CONC sigma

SFe 4S437 023

Measurements for -148289ISOshy shy 1


SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM


Sample -148289ISOshy shy 1 MEAS= 3 for Seq MEAS = 2 for Simul

EL CONC sigma

$Fe 091334 12

Measurements for -148289PSshy shy 1


259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM


Sample -148289PSshy shy 1 raquoMEAS= 3 for 5eq MEAS= 2 for Simul

EL CONC sigma

bullSFe 46540 053 amp4

Measurements for -148289DS-


SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM


Sample -148289DSshy 1 MEAS= 3 for Seq ttMEAS= 2 for Simul

EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM


Sample -148290Sshy 1 MEAS= 3 for Seq 8MEAS 2 for Simul

EL CONC sigma

SFe 35411 034

Measurements for CCV1CCV-


SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM


Sample CCVUCCV- 1 MEAS= 3 for Seq laquoMEAS= 2 for Simul

EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM


Sample CALBCCBshyfor Simul

shy 1 MEAS= 3 for Seq JtMEAS

EL CONC sigma

SFe-000120 300

Measurements for -148296S- - 1


$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM


Sample -148296S- - 1 MEAS= 3 for Seq MEAS 2 for Simui

EL CONC sigma

Fe 040475 12

Measurements for -148296S2- - 1


SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM


Sample -148296S2- - 1 MEAS = 3 for Seq MEAS 2 for Simul

EL CONC sigma

Fs 039875 1 6

Measurements for -148297S- - L n

2003S

k_ A CTtllO I I L-O W I ^ A I IWImdash I 111 1L_ V

SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM

1755=08 52996 Method COMM

Sample -143297Sshy shy 1 JMEAS= 3 for Seq ttMEAS 2 for Simul

EL CONG sigma

SFe 024357 083

Measurements for -148298Sshy shy 1


SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM


Sample -148299 Sshy shy 1 traquoMEAS= 3 for Seq tfMEAS 2 for Simul

EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM

1802-18 52996 Method COMM

Sample -148300Sshy shy 1 tMEA5= 3 for Seq MEAS 2 for Simul

EL CONC sigma

$Fe 96678 051

Measurements for 1499-147068shy shy 1


SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM


Sample 1499-147068- shy 1 MEAS= 3 for Seq MEAS = 2 for Simul

EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM


Sample -1470745S- shy= 2 for Simul

EL CONC sigma

1531I 006

Measurements for RINSEX-


259940 20620 000000 00000017300 000000 OOOOGO

1 laquoMEAS= 3 for Seq ItMEAS

20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM

j_oV7-iO Ui7 70 MCi-MWVj- -~^l II I

Sample RINSEXshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul

EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM


Sample CCV1CCVshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul

EL CONC sigma

$Fe 10162 032

laquo

Measurements for CALBCCBshy shy 1


$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM


Sample CALBCCBshy shy 1 MEAS= 3 for Seq MEAS= 2 for Simul

EL CONC sigma

SFe 000772 340

Measurements for ICSAICSA1shy shy 1


SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q

Sample ICSAICSAI- - 1 ttMEAS = 3 for 5laquosq raquoMpoundAS=

ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033

Measurements for ICSABICSAB-


$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM


Sample ICSABICSAB- - 1 MEAS= 3 for Seq ttMEASshy= 2 for Simul

EL CONC sigma

$Fe 17634 008

Measurements for 2XCRDLABCRshyr


$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM


Sample 2XCRDLABCR- - 1 MEAS= 3 for Seq ttMEAS = 2 for Simul

EL CONC sigma

Fe 026868 22

Measurements for CCV1CCV- - 1


35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM

132347 52 96 Method COMM

Sample CCV1CCV- - 1 liMEAS = 3 for Seq BMEVi = C^ for Simul

EL CCNC sigma

e 100247 0 07

Measurements for CALBCC3shy


$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96

SAMPLE PREPARATION REPORT AQUEOUS Prep batch 6424CW Date 053O96 Printed by SRM Approved

PH AS RECEIVED

Sample ID Lab code PH pH(CN)

1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20

Prep code P (HN03HC1)

Client ID Sample ID Lab Initial Final Date Ana- Overall Code vol ml vol ml Prep lyst Dilution

921 13-NAI-M2 1771-148541 DS 100 100 052996 0800 SRM 100 921 13-NAI-M2 1771-148541 S 100 100 052996 0800 SRM 1 00 921 13-NAI-C3 1771-148542 S 100 100 052996 0800 SRM 100 921 13-NAI-C3 1771-148542 S2 100 100 052996 0800 SRM 1 00

LCSHCL LCSW 100 100 052996 0800 SRM 100 PBW PBW 100 100 052996 0800 SRM 1 00

2004

1 i Metals Digestion

Mercury Digestio bulllaquo

Comm or ( Dj

f Client Name

i i poundpoundpoundbull

3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke

AQUEOUS DIGESTION LOG

Analyst SAP Date $~fai4fc PREP BATCH i^fc^

n Analyst Date FD 5t

Supervisor page 2V

Furnace Volumes ICAPV olumes Hg Vol Initial Final Initial Final Initial

Client ID mis mis mis mis mis pH PBW ^^^^^^Q^^^^V ^^^^^^^^^^^^^^^P 100 100 lt2

-bullraquo LCSW _^r ^~7-f -TV s^ s

~ 5V- X ix poundyen DJ T^ T ^

bullbullHHi$yen2 J-a e laquobull + laquoraquo

^shy

lUAT-tCb bullnrnroi ^

ml of Spike deg bullbull vlt M tiki

ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash

ml of l-urn L)b Furn-tGS mis gf~~FaTn- LGS-mdash_

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ANALYTICAL REPORT



FD Case 1856

Section Seven General Chemistry




Bedford MA 01730


TABLE


FD1856





TABLET AMMONIA NARRATIVE SUMMARY

FD1856



QUALITY CONTROL







FD 1856






FD1856

GENERAL COMMENTS Sample duplicate will be identified with 52 preceded by sample number Sample spike will be identified with DS preceded by sample number


QUALITY CONTROL







FD1328



QUALITY CONTROL





TABLET NITRATE NARRATIVE SUMMARY

FD1856



QUALITY CONTROL





TABLET ORTHO PHOSPHATE NARRATIVE SUMMARY

FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT


Report To GE1 ConsultantsNH


NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw

Chloride - Technicon AQ EPA 3252

92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030



Report To GEI ConsultantsNH NET Job No 9601771




92113-NAI-M2-0596 148541 011 mgL 92 05211996 dlw 92113-NA1-C3-0596 148542 0044 mgL 92 05211996 dlw


92113-NAI-M2-0596 148541 36 mgL 25 05241996 dlu 92113-NAI-C3-0596 148542 25 mgL 25 05241996 dlu



700-jI


BATCH QUALITY CONTROL DATA


Program Tinkham Garage Report Date 06181996

LCS Method Spike Sample Duplicate Parameter X Recovery Blank Recovery (Run 1) (Run 2) RPD Analyst

Alkalinity AQ 1054 lt20 dec BOD shy 5 day AO 1159 lt20 lt20 lt20 dec Chemical Oxygen Demand AQ 942 lt15 913 37 37 00 dlw Chemical Oxygen Demand AO 979 41 39 50 Chloride - Technicon AQ 957 lt010 800 220 230 44 nsv Chloride - Technicon AQ 880 12 12 00 Chloride - Technicon AQ 800 100 100 00 Nitrate-calc AQ 1095 lt0020 1030 lt0020 lt0020 nsv Nitrate-calc AQ 1090 lt0020 lt0020 Phosphate ortho AO 1033 lt0015 1080 0044 0049 108 dlw Sulfate-Turbidimetric mod AO 1029 lt040 2000 15 15 00 dlw Sulfate-Turbidimetric mod AO 3000 45 45 00 Total Organic Carbon TOC AO 1006 lt030 1050 18 19 54 dlw

Please note that the data reported for the Duplicates and Spikes were analyzed in the same batch but may not necessarily be that of your sample

LCS - Laboratory Control Sample For analyses not requiring sample digestionpreparation independent control check sample result is reported

Alkalinity EPA 3101

Analyst Date 5]lfG_ Labsys Batch amplt2 Supervisor

pH Calibration V-1lt OD2NH2S04lot_ pH LCS Value ^7o 010NH2SO4lot_ LCS REC=

Prep_ j_ TrueValue=

pH4 Buffer lot L^P pH7 Buffer lot ^- P pH 10 Buffer lot

Alkafinrty as (ml H2SO4) fN H2SO4) 50000 MoL CaCOa (ml Sample)

Job Number Sample ID mis Sample Initial pH NAcid Initm Final m Total m mgL CaCO3 REC Blank 50 bull01 oo OU LCS 50 n-0 1SS

0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

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73

bullI] 11AO

ri HJ m 70-^ - shyraquo 1 1 1 1

MMmi -ft H U L |K I b yen

0 0271501 10120 476 0084L 0008

10 Q^H12 f 0s1U-148541 1 B 0008 fe 11-148542 034 03 90 820 i4 1amp^2J-147966 03841 73 1amp2-147967 1 0041 57 1672-147969 1 45

K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1

18 Ifcg5-I48073 1 388 0163 3398 ltgt05 -148074 19 1 3400 M Campgt 40 22 148075 23 1 ^ 0008 148076 993 1 V 0463 148077 94 1 ]_ 0051 148078 3412 K1 i 1572shy

nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024

34 j 1140338 36 1 0008 148339 36 1 1 0014 148340 j7 1 0089 148341 3374 38 1554mdashi148342 3364 039 1 1 1550mdash 148343 349 040 0163 148342S2 i 1 3323 K203 1 440 1 i 0209 3260 1 1 1506 0 0008A HT

0008

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700

BOD EPA 4051 Labsys Batch _

Initial Analyst P^C Date^f276^ TimeJ Final Analyst Date Time_ Supervisor

Bar Press inrtial(mmHg)=_2 DO inttial(mgl)=jpound-_j2ltf

2-T -W BOD mot=(DO initial-DO finalM LCS Lot poundpound f^Preo ampJZW

p True Valuer n^^fmoA P(oHuten factor)=mls sample300ml Ret overy= ) t f(seed correction)=(seed initial DO - seedfinal DO) x 008

Job Number Sample ID Vol(ml) mtesMd Initial DO(mgL) Final DO(mgL) DO diff t P mgL BOD Avg BOD

Blank 1 300 0 TampQ jLtlt Blank II 300 0 57^D 8-t3

SEED 25 ^31 i-2gt ^ ^)^ bullfZM SEED II 25 ^-y ^1)3- )

fj f5

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CHEMICAL OXYGEN DEMAND EPA 4104 Page

Analyst SupervisorSpike Prep

Date

bullff

Labsys Batch gt - 7

True Value ^b j BigL

LCS Prep 7C True Value pound$ 7j rogL

Rack Number 1

531

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tit in

701

NET


Analyst Date pound61T Labsys Batch Supervisor

Std Value (mgL) Absorbance ABS 600 ran wavelength

Blank otgto Correlation R = I i 10 sgto

Standard Stock No 50 - oil 100 0 6 250 fM 500 T^Tx

Job No Sample No ABS mgL Dil mgL Final Rec Comments

BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor

Date -viO Labsys Batch 7

Job No Sample No ABS mgL Oil mgL Final Rec Comments

r7(i So ozr HI BLANK

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I I TOTAL PHOSPHATE CcORTHOPHOSP EPA 3653 Page

Analyst Date Labsys Batch Supervisor

Std Value (mgL) Absorbance ABS 660 run wavelength tttfltiBlank Correlation R = lt

0010 Standard Stock No

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ICV True Value mgL


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NET - Dayton Total Heterotrophic Plate Counts

Cambridge Division NATIONAL 12 Oak Park Bedford MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET Ireg TESTING INC Fax (617) 275-7411

June 5 1996

Mr Richard Van Etten rmdash i~ f- imdash t bullgt mdash ~ GEI Consultants Suffolk Building 53 Regional Drive 1 7 1V96 Concord NH 03301

Dear Richard

Enclosed is your Plate Count data from NET-Dayton Also enclosed is a copy of the method used as well as their Quality Assurance Plan Please feel free to call me with any questions

Sincerely

Peter Conroy Project Coordinator

Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax (513) 294-7816

ANALYTICAL REPORT

NET - CAMBRIDGE 05201996 12 Oak Park Bedford MA 01730 NET Job Number 9606991

Enclosed is the analytical report for the following sample(s) submitted to the Dayton Division of NET Inc for analysis

Sample Date Date Number Sample Description Taken Received

347306 92113-DVE-07-0596 B00733 05151996 05161996 347307 NAI-MI-0596 B00734 05151996 05161996 347308 92113-NAI-K2-0596 B00735 05151996 05161996 347309 92113-OW2D-0596 B00736 05151996 05161996 347310 92113-LGAW-0596 B00737 05151996 05161996

National Environmental Testing Inc certifies that the analytical results containedanalyzed

herein apply only to the specific samples

Reproductionentirety

of this analytical report is permitted only in its

Enclosure Project Coordinator


NET - CAMBRIDGE 12 Oak Park Bedford MA 01730

Sample Description Client Project ID

ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306

Date Taken 05151996 Date Received 05161996

Parameter Result Unit Date Anal Analyst

Plate Count 15600 CFUmL 05161996 dgr


PAGE 3 ANALYTICAL REPORT

05201996 NET - CAMBRIDGE 12 Oak Park JOB NUMBER 9606991 Bedford MA 01730

SAMPLE NO 347307

Sample Description NAI-MI-0596 B00734 Client Project ID




Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET Ireg TESTING INC Fax (513) 294-7816



SAMPLE NO 347308

Sample Description 92113-NAI-K2-0596 B00735 Client Project ID







SAMPLE NO 347309

Sample Description 92113-OW2D-0596 B00736 Client Project ID







SAMPLE NO 347310

Sample Description 92113-LGAW-0596 B00737 Client Project ID



Plate Count CFUmL 05161996 dgr


ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996

National Environmental Testing Inc certifies that the analytical results contained herein apply only to the specific samples analyzed

Reproduction of this analytical report is permitted only in its entirety





ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716




Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET TESTING INC Fax- (513) 294-7816



ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717




Dayton Division NATIONAL 3601 South Dixie Drive Dayton OH 45439 ENVIRONMENTAL Tel (513) 294-6856 NET |reg TESTING INC Fax (513) 294-7816



SAMPLE NO 347718

Sample Description 92113-FD01-0596 B00751 Client Project ID




NATIONAL OH 45439 ENVIRONMENTAL

Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT


Enclosed is the analytical report for the following sample (s) submitted to the Dayton Division of NET Inc for analysis


347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507

Sample Description 92113-ERT01-0596 B00746 Client Project ID



Plate Count CFUmL 05171996 kkh

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Cambridge Division NATIONAL 12 Oak Park Bedforo MA 01730 ENVIRONMENTAL Tel (6171 275-3535 NET TESTING INC Fax (617) 275-7411

June 17 1996

Mr Bob Mullin GEI ConsultantsNH Suffolk Building 53 Regional DriveConcord NH 03301

RE Tinkham Garage

Dear Mr Mullin




SAMPLE NET DATE TIME DATE ID ID TAKEN TAKEN RECD MATRIX

92113-NAI-M2-0596 148541 05201996 1010 05211996 GROUND WATER 92113-NAI-C3-0596 K8542 05201996 1315 05211996 GROUND WATER







Sincerely


enclosures


FD1856



FD1856



QUALITY CONTROL
















TABLE


FD1856





TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



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TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

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NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











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1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96

SAMPLE PREPARATION REPORT AQUEOUS Page 1 Prep batch 6424CW Date 053O96 Printed by SRM Approved

PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

-nJT

11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

^5

^K ^( 39

fJ

BLANK 00 fc^^ 1 ^

LCS

^00$

OM

nc^ ^C j j

ô ltWL ^7^

IT7I cc oCH IS


nn 10

-735shy

z^^ ftu

Li4iL

lUfo

orlaquo| )OD ^x

ygt )laquogt


H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

E b 5

E5 pound5 5

1-)1 i 1 i

O1 pound5 pound5

pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

- bulllaquo mdash c

Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

O oo OgtZl


rshy155

M-Mshy~~ ^J

3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

555 bull45 19

151HC3

t sect H-6

1 f~~


73O l_laquo ltJ

i 5o3bull i Jt-So

BOH lt_

1515i_j

t- v I Zgt

v O-o

bull_ OOMshy

O pound 1 9 u ()gt+

J 1 o O

bullJ i 1 O


^ ~~ ~ v raquodu r

G lt i1

bull UU5

d loOS u oGo


O i



(bull

kr

N _

S

7001

X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

Ngt

^gt i


hBB|M

B|B

H||H

|

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

N

^ co

mpl

ianc

e m

onllo

nng7

Y

es

_ gt

N

o

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

s

enlo

rcem

ent

actio

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lt W

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c g

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D

CO LL

4O O o X

UJ

^

c

g 5







Sincerely


enclosures


FD1856



FD1856



QUALITY CONTROL
















TABLE


FD1856





TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

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1

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1

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hi

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j (

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L

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ni bull i

L 1 1 d 4 j i

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1 i

1

i

t

I

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^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

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NR NR NR 0042


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1 1

1

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-

-

-

-

-

-

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JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




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1 I 1 - 1 1 t f 1

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002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

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LCGI ICI 2mdash



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w

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W Di

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20044

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f tun X bulllt (DTJ

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ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

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gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

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cc

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o 0 0

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i

1

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c

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raquolt (0bullo

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3 ltHshyO 3

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c a D

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01


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ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




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Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


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i li-4 5



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a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

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s N

o 1

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FD1856



FD1856



QUALITY CONTROL
















TABLE


FD1856





TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

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1 ltbull

I r

1

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ni bull i

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1 i

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t

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rshy

^ Hshyr

i

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iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


t- - - b e- i - tb





N 3LH-

20001

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hf MR I

- i MK


1 Hh lt 1 1 irihl


i 1 i


AA AMD TCP


S4i= HO GE

ug t

CRDL E Initial

Gun



I t i t i i f t


3 i ICi Prep L

-^ o ij

C

riiolt r i ci n

I I I -

1

bull I I I I

_ 1 _ l

1 1 liK 1 MR nr

i i NP t i N i

i W

NR 1

1

i NK i NH


i MR

îT1

i HF 1 i fir-

i HP

raquo t Kl 1

i KR i w

gt i i

IiiGj 0

ELr - - -

Contract

5n5 No GEI


G 11 inv - i 0 A f 10 fi

i ) r repa

bull n

NK MF KR r i F

- 1 pound

i NP MF

INK IN

bull HK p IH-

î^ bull NR INF Nfi

INFshyIMP

I-R HF i NR

J---03 0

0009

ii rac t


S Source LFEt1ltN

ugL


fi -E

gt - l l - pound

T - -ct

3 ho uEI





i

bull H

nr

i HF-

- 1

MR NR


i rx

| MF

MR US

NF HF

NFgt

J


HO pound bull



dTM| ISlOh ^ LI L

1T3

TV r

tK

r bullMR

HK UK

ltpoundL oAHrLE

Con t rac t

5AS No GEI iLj No

Sol id 11 ri

2deg013

shy bdquo 11J I



1 ^bull1L L1 3 ADD

ICTI At CUN AES

iLL IOhshy

gt

bull

NJ

i -c

o - 2 - T gt _ gt

tr bullbull

-H-1

-i bull c

Mo

Uli

GEI

Legte l

shy I bull

(Ishy

c er _ e

r i r

N Ml r-i

35 OC

-l

Ni IN

Ml



i Sn3 No GE r-DC N

IDL 1 L Q 1

200 i f i

0 i - 60 10

200 HR -gt 1 NK

3 1 T4X


u L

100 15 0 bull 3 MR


o shy f-r-1

bulltO NK 50-0 Mr1

10 SR

10 W fO

iR


Ib n03 0

0016


if

_ bull shy - r shy

-bullbull r

- r _

bull

EI LHK-DH

Ciishy rC

19

r-11-1

Cor- t rac t

SM- No

D c t r

GEI

04C-J95

ri A- j~igt

In f j re l rr

Al ilg LC



1 - -i




D a t e 040395


C-r f u K Ho Ni

0-gt 0 0000000 o ooôooo 000000

2 gt - IN 1LP03 0









I I

1 I

3 1 t bullt ugD H i

_ i 3 ^NR IMF HF

HP NFshy

W

INK

iMR INK 1

f U Il-i 100 0


Contract bull

5AS No GEI



_

il - IN

si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

0 c LI

F f- PI

E pound G


ii

lt

1 lt i

t i

-i

ii

ti


-1A i i t t _ bull -1 l 1 t i 1 1 1 1

gt -11 i bull

xY~ t J

l

1

l I

1

I I

1

I

1 i

1

1

I x l i t 1 i 1 t

1 1 X ]t i

i 1I i i 1 i bull

l 1

1 1 1

A i i 11 l i

ltl I l l

l I t

i gt i i

f

i l I I

l i


x i bull 1 1 l 1 I

i t

i )

lt1 shy

l - t -

j 4 ~ r _ _ _ _ gt _

1

1

1

_

bull 1

i

- ~~ ~ i lt

1bull

i

I

i

bull

t

1 i

i

i 1

bull

i

1

1 i

i

1

1 i

i

)

i

i

1

l r

i

I I f lt i ~~ ~~ ~


i i 1

1

i i

bull i bull i

1

i

)

i i

1

i t

1

i

1

i i

-i 1 1 1

t i l l J i i |

1 1 bull1 T

t 1 tI l

1l 1

1

1 1

1 gt

raquo 1

f | 1 J I I

i l 1l

t

1 1

1 bull

t

1 1

I 1

il r

i 11

gt bull

1 r

t 1

) i 1

I t

1 1

I

k 1


1 I I 1 1 t I

1 1 bull lt 1 t 1 1

1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

i 1 1

1 1

1 I

l 1

bull X i t 1I

bullt

i

l t shy

l 1

1

l t

t 1


1 1

i i

I

l 1 i

l

1 t

1 1

1 1

1 )

I V bullA 1

I

11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

1 1

x 11 t 4

1 1

1 1 bull

i 1

1 t

1 1

t 1

1 1

1 1


1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

t l


( 1

1 t

1 1

t 1

1 1

1 t

gt 1

t 1

i gt gt i l l i

t1 l 1

( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

-nJT

11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

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Labsys Batch

Data 0 60 -$amp

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June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

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FD1856



QUALITY CONTROL
















TABLE


FD1856





TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

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u r No CEJ bull-O


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M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


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4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


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A T H E N A 306e







A T H E N A 306e

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28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

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CD cr

i0

0

aB

I I i i i

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bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

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djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

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c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

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X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

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11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

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9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

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fJ

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^00$

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nc^ ^C j j

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nn 10

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H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

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E5 pound5 5

1-)1 i 1 i

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pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

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Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

O oo OgtZl


rshy155

M-Mshy~~ ^J

3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

555 bull45 19

151HC3

t sect H-6

1 f~~


73O l_laquo ltJ

i 5o3bull i Jt-So

BOH lt_

1515i_j

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v O-o

bull_ OOMshy

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J 1 o O

bullJ i 1 O


^ ~~ ~ v raquodu r

G lt i1

bull UU5

d loOS u oGo


O i



(bull

kr

N _

S

7001

X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

Ngt

^gt i


hBB|M

B|B

H||H

|

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

N

^ co

mpl

ianc

e m

onllo

nng7

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es

_ gt

N

o

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his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

s

enlo

rcem

ent

actio

n7

US

T

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a W

ate

r

1 CO

MM

EN

TS

-^

-

-

-1

U

r

lt

-lt

Vf

7

lt

H

tjtfO

Gt

PR

OJE

CT

NA

ME

LO

CA

TIO

N

1

L f

~(H

f1

1

-r

fslfft

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L

on

tin

(mdash Z CL

mdash shyg ^

LU CO 18 f-

1V 1 rshy

e o K LU cr O

LU O gt a XLU

RE

MA

RK

S

^

g 5

UJ Vcr c- ~ gt O

LL

c ^ --- 0


JD -x

1

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bull

is-o Q _-gt 15 r-

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50shy

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c 1

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^

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N

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ES

FR

EE

OF

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AD

SP

AC

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ES

N

O1

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RE

LIN

QU

ISH

ED

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itfr

gt lt U V

^

s

bulllt X

CO

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s -raquos

cr Q

bull

4 ^ Oti

^

^ ^ v

^ Vu gt S S li

V s gt

f an

d T

ype

of

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iners

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1 R

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NE

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OS

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PLE

RE

MA

CO

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AIN

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AIN

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R T

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LIE

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JH 81

Tr HOEN X

+ o~l IOH cr

LU N^ ~i i

CO

cr

jipbull i

O^

^

UI cc lt dWOO



(PR

INT

NA

ME

) raquo

SIG

NA

TU

RE

ÛJ LU cr 2 QD

O cr cr 3 SiQ CL

|oiI 0 O ^ ^H 0LU

FIE

LD F

ILT

ER

ED

Y

ES

N

O

gt s kiit 0 1 i^

LJ Nj


C cr gt bullgtv

V) 0 bull0

CO ^s 0 o LU 1

en i - 0 UJ gt

li 2 C^


UJ

sect bull

|

CO

j ^ N)

u rgtshy

$ ^ V lt LU


bullv

H

copy V

^ CL


bull 8 1 ^g

m gt^ gt LL omIf l


UJ lti


CO

ND

I


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1


C

fe Z U j


PO

V tl s rshy

$1 LJJ O I- IB

z c

o o tr

bulls X s o0

t-N Vi)

(mdash laquo

ky- I


lt UJ

x


0 P OC Z LU

LL s g y

I fQl

lt w

raquo LL o -i o

H Q

O


12glaquoUJ Q

SeSEw

zw uj

poundE D =gt O


LLJ Lt LLJ

lt W

^j I

c g

^Sshy

LLJ

D

CO LL

4O O o X

UJ

^

c

g 5







TABLE


FD1856





TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

I

o r-r

Nshy

N

N1

v t

hi

1 1 v

j (

(j gtbullshy

L

( r ~ i t

bullgt

1

h t

- 1

- t

~

i bull gt lt -

ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


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N 3LH-

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1 - -i




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il - IN

si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

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ii

lt

1 lt i

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-i

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gt -11 i bull

xY~ t J

l

1

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1

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1

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i i 1

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)

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1

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t 1 tI l

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k 1


1 I I 1 1 t I

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1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

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1 1

1 I

l 1

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i

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1 1

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11

bull 1

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i 1 gt

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1 1

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1 1

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1 1

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1 1

1 1


1 1

1 1

1 1

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1 1

) 1

1 1

t 1

1 1

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1 t

1 1

t 1

1 1

1 t

gt 1

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( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


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gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

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a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

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01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

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8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

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ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




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Analyst

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Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


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June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

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TABLET


FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

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1

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i

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iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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5AS No GEI



_

il - IN

si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

0 c LI

F f- PI

E pound G


ii

lt

1 lt i

t i

-i

ii

ti


-1A i i t t _ bull -1 l 1 t i 1 1 1 1

gt -11 i bull

xY~ t J

l

1

l I

1

I I

1

I

1 i

1

1

I x l i t 1 i 1 t

1 1 X ]t i

i 1I i i 1 i bull

l 1

1 1 1

A i i 11 l i

ltl I l l

l I t

i gt i i

f

i l I I

l i


x i bull 1 1 l 1 I

i t

i )

lt1 shy

l - t -

j 4 ~ r _ _ _ _ gt _

1

1

1

_

bull 1

i

- ~~ ~ i lt

1bull

i

I

i

bull

t

1 i

i

i 1

bull

i

1

1 i

i

1

1 i

i

)

i

i

1

l r

i

I I f lt i ~~ ~~ ~


i i 1

1

i i

bull i bull i

1

i

)

i i

1

i t

1

i

1

i i

-i 1 1 1

t i l l J i i |

1 1 bull1 T

t 1 tI l

1l 1

1

1 1

1 gt

raquo 1

f | 1 J I I

i l 1l

t

1 1

1 bull

t

1 1

I 1

il r

i 11

gt bull

1 r

t 1

) i 1

I t

1 1

I

k 1


1 I I 1 1 t I

1 1 bull lt 1 t 1 1

1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

i 1 1

1 1

1 I

l 1

bull X i t 1I

bullt

i

l t shy

l 1

1

l t

t 1


1 1

i i

I

l 1 i

l

1 t

1 1

1 1

1 )

I V bullA 1

I

11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

1 1

x 11 t 4

1 1

1 1 bull

i 1

1 t

1 1

t 1

1 1

1 1


1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

t l


( 1

1 t

1 1

t 1

1 1

1 t

gt 1

t 1

i gt gt i l l i

t1 l 1

( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

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c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

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11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

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9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

^5

^K ^( 39

fJ

BLANK 00 fc^^ 1 ^

LCS

^00$

OM

nc^ ^C j j

ô ltWL ^7^

IT7I cc oCH IS


nn 10

-735shy

z^^ ftu

Li4iL

lUfo

orlaquo| )OD ^x

ygt )laquogt


H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

E b 5

E5 pound5 5

1-)1 i 1 i

O1 pound5 pound5

pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

- bulllaquo mdash c

Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

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$7 Z








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i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

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a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

Ngt

^gt i


hBB|M

B|B

H||H

|

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his

wor

k be

ing

con

duct

ed lo

r re

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tory

N

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mpl

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e m

onllo

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es

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his

wor

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ing

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ent

actio

n7

US

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r

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MM

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TS

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-1

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FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

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Nshy

N

N1

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hi

1 1 v

j (

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L

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1

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ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


t- - - b e- i - tb





N 3LH-

20001

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Date Rec

LI

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0002

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Lfr No GET G No


Date Rr-iHC t-5


f i

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CLEAR Texture


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1 rr

1

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1 - -i




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_

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si -JN LOG

Contract


Hi hod F1

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Analyte


c c i c o A R

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ii

lt

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1 1 1 i t t t i

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1 1

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bull 1

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i 1 gt

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1 1

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1 1

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1 1

1 1

1 1

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1 1

) 1

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1 t

1 1

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1 1

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gt 1

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1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


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gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


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1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

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QO

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20044

2

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f tun X bulllt (DTJ

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ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

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r IT m n

7 r H-O

3 O ft O CQ

O bullbull

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ttt (DftH O H-- M)

C O

o

Jfi

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m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

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a O

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fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

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a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

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raquolt (0bullo

03

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M C

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0


3 ltHshyO 3

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n ft o o o shy

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bullbull i-b

c a D

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mo

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3 a-5 O 9 ltT-t

m lt CHshy

O C O

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pound c

a o

s laquoQ

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01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

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(I

i- laquobull

II

r Ji

^

ts

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T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

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0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

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M01 O

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m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

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Q shy

C 7

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0

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a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

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r r

^

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O


bull3

CD rr 2 S 0

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01


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bull3

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S r

o 03 rr 9

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9 n a

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p


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o O

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o

r 1deg GO 0 S a0

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H-0 3 S a 3

3

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9 O


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rr 0

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P usect

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o

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c

o 0rf O

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dard

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to ltrt0 0MO

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a ~

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c a O3

2

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f

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QC

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t

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H3 OQ

9

mnit oo o

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H-O


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c a 09

O-

o 9 ft O

2 ltOMshym

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n bull0

03

9

a 9

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9

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-raquo deg

(

o 0 rt o

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amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

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al cono C

omm

ents

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Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

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n

IS

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i

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00 ft 9

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n

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5 ltQHshyo

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C

0

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dard

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c IS CD

D B ft ft

ma iB O m

0

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vor O

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r~r^r T -

T

T

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cv

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i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

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lt3

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t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

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olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

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51 4 DC 05 fe

0-7

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I alyst ervisor





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Lf7 07 0 -7


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NET

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3 7 1011 1pound 13 4


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t



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^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

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1-)1 i 1 i

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11 1

30 101 J

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i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

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35E3 35E8 3533 3538 35M-E 35-47

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fc r

R

F

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c

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JD


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5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

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mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

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^L-V

^j

S5 Io 1 1 i

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io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

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0 15o5

tv

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ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

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n =

OCj

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n i^

r-^ a J v 7

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70011

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4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

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it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

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3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

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151HC3

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1 f~~


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J 1 o O

bullJ i 1 O


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bull UU5

d loOS u oGo


O i



(bull

kr

N _

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X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

Ngt

^gt i


hBB|M

B|B

H||H

|

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

N

^ co

mpl

ianc

e m

onllo

nng7

Y

es

_ gt

N

o

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

s

enlo

rcem

ent

actio

n7

US

T

Drinkm

a W

ate

r

1 CO

MM

EN

TS

-^

-

-

-1

U

r

lt

-lt

Vf

7

lt

H

tjtfO

Gt

PR

OJE

CT

NA

ME

LO

CA

TIO

N

1

L f

~(H

f1

1

-r

fslfft

rC

L

on

tin

(mdash Z CL

mdash shyg ^

LU CO 18 f-

1V 1 rshy

e o K LU cr O

LU O gt a XLU

RE

MA

RK

S

^

g 5

UJ Vcr c- ~ gt O

LL

c ^ --- 0


JD -x

1

LU cr

bull

is-o Q _-gt 15 r-

u LU z cr LU

50shy

LU

c 1

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^

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pound

f

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i^

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N

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|

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ES

FR

EE

OF

HE

AD

SP

AC

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N

O1

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RE

LIN

QU

ISH

ED

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itfr

gt lt U V

^

s

bulllt X

CO

Qv

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cr Q

bull

4 ^ Oti

^

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f an

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ype

of

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X

1 R

EQ

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ST

NE

T T

O D

ISP

OS

E O

F A

LL S

AM

PLE

RE

MA

CO

lt J56

V

7 LU EONH V s

vbull

ACO -

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OLA

SA

MP

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AIN

DE

R D

ISP

OS

AL

R

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SA

MP

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EM

AIN

DE

R T

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LIE

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CO

cr

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(PR

INT

NA

ME

) raquo

SIG

NA

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RE

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N

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bullv

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copy V

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m gt^ gt LL omIf l


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ND

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fe Z U j


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bulls X s o0

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ky- I


lt UJ

x


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LL s g y

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lt w

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H Q

O


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SeSEw

zw uj

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lt W

^j I

c g

^Sshy

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D

CO LL

4O O o X

UJ

^

c

g 5


FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

I

o r-r

Nshy

N

N1

v t

hi

1 1 v

j (

(j gtbullshy

L

( r ~ i t

bullgt

1

h t

- 1

- t

~

i bull gt lt -

ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


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c c i c o A R

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lt

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1 1

1

raquo 1

i 1

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-

-

-

-

-

-

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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




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1 I 1 - 1 1 t f 1

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A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



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w

CQin

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H O

W Di

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HS

20044

2

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f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

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r IT m n

7 r H-O

3 O ft O CQ

O bullbull

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I ftfit

o n a o

I

r

cc

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n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

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a 1ro laquoa

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i

1

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c

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T

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pound-kdegS~S

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raquolt (0bullo

03

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n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

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mo

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3 a-5 O 9 ltT-t

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ro ltampbullmdash

bulla a n c a o

s i r

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II

r Ji

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T

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CD

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aHr OO

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0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

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a oraquo n c m

bulla

bullc laquoc0t 2

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c amdash

cA -n


0 -a o mdash Ul 0 u

u

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M01 O

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m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

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C 7

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0

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a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

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3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

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fO ^ O

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0 o1 D

01


S bulllt (0

bull3

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S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

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o

r 1deg GO 0 S a0

Q

V fe

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Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

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f -amp -o

P usect

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5 ^

o

r r N 3 su

gt0

ltP -5

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pound_ ltbull

c

o 0rf O

Stan

dard

ID

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to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

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ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

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CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

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LA

QC

amp r

u raquo rgt O-

t

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pound

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djr

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O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

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H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

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n bull0

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9

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-raquo deg

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o 0 rt o

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amp

ID

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r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

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al cono C

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ents

0 Ortn O Hshy

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rum rt-ts a o

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a

f-

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n

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n

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bull0tni lt (Dbullo

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C

0

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dard

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c IS CD

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ma iB O m

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T

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AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

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00

0 3

OB

28SI MO

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Dlt 0 O

900 pound Âi

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B O O3 n

CD

0

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1

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t ^ _D -5 -o

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-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




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A03 JL02


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June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





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FD1328



QUALITY CONTROL






FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

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-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











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-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

-nJT

11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

^5

^K ^( 39

fJ

BLANK 00 fc^^ 1 ^

LCS

^00$

OM

nc^ ^C j j

ô ltWL ^7^

IT7I cc oCH IS


nn 10

-735shy

z^^ ftu

Li4iL

lUfo

orlaquo| )OD ^x

ygt )laquogt


H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

E b 5

E5 pound5 5

1-)1 i 1 i

O1 pound5 pound5

pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

- bulllaquo mdash c

Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

O oo OgtZl


rshy155

M-Mshy~~ ^J

3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

555 bull45 19

151HC3

t sect H-6

1 f~~


73O l_laquo ltJ

i 5o3bull i Jt-So

BOH lt_

1515i_j

t- v I Zgt

v O-o

bull_ OOMshy

O pound 1 9 u ()gt+

J 1 o O

bullJ i 1 O


^ ~~ ~ v raquodu r

G lt i1

bull UU5

d loOS u oGo


O i



(bull

kr

N _

S

7001

X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

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NE

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LL S

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PLE

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MA

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lt J56

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NA

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RE

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m gt^ gt LL omIf l


UJ lti


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ND

I


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1


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fe Z U j


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o o tr

bulls X s o0

t-N Vi)

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ky- I


lt UJ

x


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LL s g y

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lt w

raquo LL o -i o

H Q

O


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lt W

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D

CO LL

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^

c

g 5


FD 1856



QUALITY CONTROL






FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

I

o r-r

Nshy

N

N1

v t

hi

1 1 v

j (

(j gtbullshy

L

( r ~ i t

bullgt

1

h t

- 1

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~

i bull gt lt -

ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

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ii

lt

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gt -11 i bull

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l

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k 1


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1 I I 1 1 1 1 bull


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1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

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1 bull

1 1

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1 1

1 I

l 1

bull X i t 1I

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i

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l 1

1

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1 1

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l

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bull 1

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i 1 gt

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1 1

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1 1

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1 1

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1 1


1 1

1 1

1 1

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1 1

) 1

1 1

t 1

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1 t

1 1

t 1

1 1

1 t

gt 1

t 1

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( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




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I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


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gt 1 1 1 1 (

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1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




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gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

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e

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bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

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o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

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ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




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Analyst

ICVCCV True value

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Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


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i li-4 5



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a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

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FD 1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

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1

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i

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iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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N 3LH-

20001

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if-l

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5^r No GEi

u L

1 1



( NK UK

Mr i i if

i INK IN- i

i bull MF s NF-

NF i Nh


hf MR I

- i MK


1 Hh lt 1 1 irihl


i 1 i


AA AMD TCP


S4i= HO GE

ug t

CRDL E Initial

Gun



I t i t i i f t


3 i ICi Prep L

-^ o ij

C

riiolt r i ci n

I I I -

1

bull I I I I

_ 1 _ l

1 1 liK 1 MR nr

i i NP t i N i

i W

NR 1

1

i NK i NH


i MR

îT1

i HF 1 i fir-

i HP

raquo t Kl 1

i KR i w

gt i i

IiiGj 0

ELr - - -

Contract

5n5 No GEI


G 11 inv - i 0 A f 10 fi

i ) r repa

bull n

NK MF KR r i F

- 1 pound

i NP MF

INK IN

bull HK p IH-

î^ bull NR INF Nfi

INFshyIMP

I-R HF i NR

J---03 0

0009

ii rac t


S Source LFEt1ltN

ugL


fi -E

gt - l l - pound

T - -ct

3 ho uEI





i

bull H

nr

i HF-

- 1

MR NR


i rx

| MF

MR US

NF HF

NFgt

J


HO pound bull



dTM| ISlOh ^ LI L

1T3

TV r

tK

r bullMR

HK UK

ltpoundL oAHrLE

Con t rac t

5AS No GEI iLj No

Sol id 11 ri

2deg013

shy bdquo 11J I



1 ^bull1L L1 3 ADD

ICTI At CUN AES

iLL IOhshy

gt

bull

NJ

i -c

o - 2 - T gt _ gt

tr bullbull

-H-1

-i bull c

Mo

Uli

GEI

Legte l

shy I bull

(Ishy

c er _ e

r i r

N Ml r-i

35 OC

-l

Ni IN

Ml



i Sn3 No GE r-DC N

IDL 1 L Q 1

200 i f i

0 i - 60 10

200 HR -gt 1 NK

3 1 T4X


u L

100 15 0 bull 3 MR


o shy f-r-1

bulltO NK 50-0 Mr1

10 SR

10 W fO

iR


Ib n03 0

0016


if

_ bull shy - r shy

-bullbull r

- r _

bull

EI LHK-DH

Ciishy rC

19

r-11-1

Cor- t rac t

SM- No

D c t r

GEI

04C-J95

ri A- j~igt

In f j re l rr

Al ilg LC



1 - -i




D a t e 040395


C-r f u K Ho Ni

0-gt 0 0000000 o ooôooo 000000

2 gt - IN 1LP03 0









I I

1 I

3 1 t bullt ugD H i

_ i 3 ^NR IMF HF

HP NFshy

W

INK

iMR INK 1

f U Il-i 100 0


Contract bull

5AS No GEI



_

il - IN

si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

0 c LI

F f- PI

E pound G


ii

lt

1 lt i

t i

-i

ii

ti


-1A i i t t _ bull -1 l 1 t i 1 1 1 1

gt -11 i bull

xY~ t J

l

1

l I

1

I I

1

I

1 i

1

1

I x l i t 1 i 1 t

1 1 X ]t i

i 1I i i 1 i bull

l 1

1 1 1

A i i 11 l i

ltl I l l

l I t

i gt i i

f

i l I I

l i


x i bull 1 1 l 1 I

i t

i )

lt1 shy

l - t -

j 4 ~ r _ _ _ _ gt _

1

1

1

_

bull 1

i

- ~~ ~ i lt

1bull

i

I

i

bull

t

1 i

i

i 1

bull

i

1

1 i

i

1

1 i

i

)

i

i

1

l r

i

I I f lt i ~~ ~~ ~


i i 1

1

i i

bull i bull i

1

i

)

i i

1

i t

1

i

1

i i

-i 1 1 1

t i l l J i i |

1 1 bull1 T

t 1 tI l

1l 1

1

1 1

1 gt

raquo 1

f | 1 J I I

i l 1l

t

1 1

1 bull

t

1 1

I 1

il r

i 11

gt bull

1 r

t 1

) i 1

I t

1 1

I

k 1


1 I I 1 1 t I

1 1 bull lt 1 t 1 1

1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

i 1 1

1 1

1 I

l 1

bull X i t 1I

bullt

i

l t shy

l 1

1

l t

t 1


1 1

i i

I

l 1 i

l

1 t

1 1

1 1

1 )

I V bullA 1

I

11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

1 1

x 11 t 4

1 1

1 1 bull

i 1

1 t

1 1

t 1

1 1

1 1


1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

t l


( 1

1 t

1 1

t 1

1 1

1 t

gt 1

t 1

i gt gt i l l i

t1 l 1

( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

-nJT

11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


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Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

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i li-4 5



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a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

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^gt i


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his

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TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

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I r

1

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i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

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4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

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CD cr

i0

0

aB

I I i i i

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bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

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djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

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O 2=

(A tc IL

n

IS

o

i

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c C

01 en vt eo

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00 ft 9

HS OO

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X

CO ltet O O

O 3 H-JS

0 O

M0

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ff O rrn 0 Hshy

930 c a D

O

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11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

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9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

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fJ

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nc^ ^C j j

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nn 10

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H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

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1-)1 i 1 i

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pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

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Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

O oo OgtZl


rshy155

M-Mshy~~ ^J

3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

555 bull45 19

151HC3

t sect H-6

1 f~~


73O l_laquo ltJ

i 5o3bull i Jt-So

BOH lt_

1515i_j

t- v I Zgt

v O-o

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J 1 o O

bullJ i 1 O


^ ~~ ~ v raquodu r

G lt i1

bull UU5

d loOS u oGo


O i



(bull

kr

N _

S

7001

X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

Ngt

^gt i


hBB|M

B|B

H||H

|

Is t

his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

N

^ co

mpl

ianc

e m

onllo

nng7

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es

_ gt

N

o

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his

wor

k be

ing

con

duct

ed lo

r re

gula

tory

s

enlo

rcem

ent

actio

n7

US

T

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a W

ate

r

1 CO

MM

EN

TS

-^

-

-

-1

U

r

lt

-lt

Vf

7

lt

H

tjtfO

Gt

PR

OJE

CT

NA

ME

LO

CA

TIO

N

1

L f

~(H

f1

1

-r

fslfft

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L

on

tin

(mdash Z CL

mdash shyg ^

LU CO 18 f-

1V 1 rshy

e o K LU cr O

LU O gt a XLU

RE

MA

RK

S

^

g 5

UJ Vcr c- ~ gt O

LL

c ^ --- 0


JD -x

1

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bull

is-o Q _-gt 15 r-

u LU z cr LU

50shy

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c 1

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^

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N

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|

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ES

FR

EE

OF

HE

AD

SP

AC

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ES

N

O1

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Ibullbull


RE

LIN

QU

ISH

ED

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rgttf

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itfr

gt lt U V

^

s

bulllt X

CO

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s -raquos

cr Q

bull

4 ^ Oti

^

^ ^ v

^ Vu gt S S li

V s gt

f an

d T

ype

of

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iners

tOS2H

X

1 R

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NE

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ISP

OS

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AM

PLE

RE

MA

CO

lt J56

V

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MP

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AIN

DE

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AIN

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R T

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LIE

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JH 81

Tr HOEN X

+ o~l IOH cr

LU N^ ~i i

CO

cr

jipbull i

O^

^

UI cc lt dWOO



(PR

INT

NA

ME

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SIG

NA

TU

RE

ÛJ LU cr 2 QD

O cr cr 3 SiQ CL

|oiI 0 O ^ ^H 0LU

FIE

LD F

ILT

ER

ED

Y

ES

N

O

gt s kiit 0 1 i^

LJ Nj


C cr gt bullgtv

V) 0 bull0

CO ^s 0 o LU 1

en i - 0 UJ gt

li 2 C^


UJ

sect bull

|

CO

j ^ N)

u rgtshy

$ ^ V lt LU


bullv

H

copy V

^ CL


bull 8 1 ^g

m gt^ gt LL omIf l


UJ lti


CO

ND

I


Klt Q 00 ^bull

1


C

fe Z U j


PO

V tl s rshy

$1 LJJ O I- IB

z c

o o tr

bulls X s o0

t-N Vi)

(mdash laquo

ky- I


lt UJ

x


0 P OC Z LU

LL s g y

I fQl

lt w

raquo LL o -i o

H Q

O


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SeSEw

zw uj

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LLJ Lt LLJ

lt W

^j I

c g

^Sshy

LLJ

D

CO LL

4O O o X

UJ

^

c

g 5

TABLE


FD1856



QUALITY CONTROL





= I rn No



I 5

M

CLF flF tur r

] e r 1 f er

0002

-1 I (1 r r ( t

u r No CEJ bull-O


Ddte Fec a i PU C-5


1 i Igt J 0

(M 1 111

^ f J 1 shy

1 ltbull

I r

1

i tio c i

1

1

1

I

o r-r

Nshy

N

N1

v t

hi

1 1 v

j (

(j gtbullshy

L

( r ~ i t

bullgt

1

h t

- 1

- t

~

i bull gt lt -

ni bull i

L 1 1 d 4 j i

ltbull j

1 i

1

i

t

I

rshy

^ Hshyr

i

h

iN j

N

N 1-4

4f

r-NT

M

(N

N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


t- - - b e- i - tb





N 3LH-

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LI

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CLEAR Texture


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1

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1 - -i




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il - IN

si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

f w

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ii

lt

1 lt i

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-i

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ti


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gt -11 i bull

xY~ t J

l

1

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1

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1

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)

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t 1 tI l

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k 1


1 I I 1 1 t I

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1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

i 1 1

1 1

1 I

l 1

bull X i t 1I

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i

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l 1

1

l t

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1 1

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1 t

1 1

1 1

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11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

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1 1

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1 1

1 1


1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

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1 t

1 1

t 1

1 1

1 t

gt 1

t 1

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( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


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gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

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bulla jr laquoMM

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mdash laquo r

a O

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fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

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8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

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ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




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June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





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-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











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A i i 11 l i

ltl I l l

l I t

i gt i i

f

i l I I

l i


x i bull 1 1 l 1 I

i t

i )

lt1 shy

l - t -

j 4 ~ r _ _ _ _ gt _

1

1

1

_

bull 1

i

- ~~ ~ i lt

1bull

i

I

i

bull

t

1 i

i

i 1

bull

i

1

1 i

i

1

1 i

i

)

i

i

1

l r

i

I I f lt i ~~ ~~ ~


i i 1

1

i i

bull i bull i

1

i

)

i i

1

i t

1

i

1

i i

-i 1 1 1

t i l l J i i |

1 1 bull1 T

t 1 tI l

1l 1

1

1 1

1 gt

raquo 1

f | 1 J I I

i l 1l

t

1 1

1 bull

t

1 1

I 1

il r

i 11

gt bull

1 r

t 1

) i 1

I t

1 1

I

k 1


1 I I 1 1 t I

1 1 bull lt 1 t 1 1

1 I I 1 1 1 1 bull


1 1 1 1 X ii t t

1 1 1 i t t t i

i t V A i 11 1 1 1

i 1 i

raquo t

t t

1 )

1 I

X ii i 1 ) l

1 bull

1 1

i 1 1

1 1

1 I

l 1

bull X i t 1I

bullt

i

l t shy

l 1

1

l t

t 1


1 1

i i

I

l 1 i

l

1 t

1 1

1 1

1 )

I V bullA 1

I

11

bull 1

1 1

1 laquo gt

i 1 gt

1 1

1 1

1 l

1 1

1 1

x 11 t 4

1 1

1 1 bull

i 1

1 t

1 1

t 1

1 1

1 1


1 1

1 1

1 1

i

1 1

) 1

1 1

t 1

1 1

t l


( 1

1 t

1 1

t 1

1 1

1 t

gt 1

t 1

i gt gt i l l i

t1 l 1

( 1

1 1

bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


i o gt = - 1 X 1 1

gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

o o

e

^ -o

bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

-nJT

11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

^5

^K ^( 39

fJ

BLANK 00 fc^^ 1 ^

LCS

^00$

OM

nc^ ^C j j

ô ltWL ^7^

IT7I cc oCH IS


nn 10

-735shy

z^^ ftu

Li4iL

lUfo

orlaquo| )OD ^x

ygt )laquogt


H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

E b 5

E5 pound5 5

1-)1 i 1 i

O1 pound5 pound5

pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

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Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

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01^


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$7 Z








r Sulfate EPA 3754M



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i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

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230

1

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nd

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3-1 O XT

O 0shyUI 4

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E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

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N



-0003





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


Gfc1


t- - - b e- i - tb





N 3LH-

20001

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1 1

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-

-

-

-

-

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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




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A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

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13

14

15

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ICAP Opiku-

ICAP Spike

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ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

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Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

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i li-4 5



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fe 77 SMI 21 HIS

H7I

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230

1

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nd

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E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

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his

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g 5





NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 150 148542 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Amnonia

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 039 148542 038

mgL N mgL N

0 0

06131996 06131996

nsv nsv

BOD shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 lt20 148542 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COO 4104 mod

148541 25 148542 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3252

148541 31 148542 140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 0052 148542 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv


ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

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NR NR NR 0042


Gfc1


t- - - b e- i - tb





N 3LH-

20001

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Date Rec

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1 rr

1

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bull i-ir-

bull bull HF

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si -JN LOG

Contract


Hi hod F1

Euo ddte 060794

Analyte


c c i c o A R

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lt

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1 1 1 i t t t i

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1 1

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1 1

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gt 1

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bull l i

1 1

1 1

1

raquo 1

i 1

r r - It tLilOJ 0

-

-

-

-

-

-

- - -

JN LOG

DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




i t I 1 I raquo




-- i 1 1 1 gt bull 1 1 lt

I --^~ZLI 1 1

1

i i l i t 1 1 t -1

i I


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gt 1 1 1 1 (

1 1 1 i i i bull lt 1 r X 1 t 1





1 1 i t i t -1 i i 1 i i i





i i i i 1 1 1 i t i i - gt 1 1 1




-raquo t ) bull ) 1 1 1 1 ( 1 1 1 1


gt - bull ( 1 I t 1 t gt 4 1 1 1


1 ( 1 1t bull i i i t i 1 1 f

1 I 1 - 1 1 t f 1

ZLfi03 0

002

A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

HS

20044

2

0gtft (D

f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

ltgt

C 0 8 s

2 i _

b S 3 ^1

1^

c J7

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bulla jr laquoMM

--OC~ bull

mdash laquo r

a O

CO rr nraquo

fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

T

pound-kdegS~S

f O o--t

raquolt (0bullo

03

SB M3 ca o

M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

Obullo 03 ftshy

pound c

a o

s laquoQ

0)laquoa n

01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

(fl

_ -o

8 Jraquo

(I

i- laquobull

II

r Ji

^

ts

Jraquo r

T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

01 ltrr O O K-Q

0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

Cshy opound c ao LP

M01 O

O 0 bull0 i-1

m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

3O rr O ffl

Q shy

C 7

- c ca

0

QI wT prr a

a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

I I t-gtagt

3 O rr O m

r r

^

Bgt ID rrn o Mshy

O


bull3

CD rr 2 S 0

r obulla

0)tS o

fO ^ O

I-SO

0 o1 D

01


S bulllt (0

bull3

G r

S r

o 03 rr 9

H3 CO

9 n a

X _L

p


z c 2shyr lt

7 VG ib c t c r

o O

03 Mtr -o

O mdash


o

r 1deg GO 0 S a0

Q

V fe

O o 0

Co

G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


V^ sai

C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

is rr-s a O n a o

f -amp -o

P usect

|J

shyJ O 1

tfl pound - 8

5 ^

o

r r N 3 su

gt0

ltP -5

X 4 61

pound_ ltbull

c

o 0rf O

Stan

dard

ID

CO MPT o o

to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

CD cr

i0

0

aB

I I i i i

O i i

bull9 Ô

I 1 I


f

M

LA

QC

amp r

u raquo rgt O-

t

O C

pound

-C

djr

CD1 lt raquo

O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


0lt 9 Ortn O H-

c a 09

O-

o 9 ft O

2 ltOMshym

O O 31

n bull0

03

9

a 9

I

laquoaD


o

9

i bull

-raquo deg

(

o 0 rt o

bullo conK obullo


amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

O 3 secta0 n a

- a 0

Fin

al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

Q 0 0 rr 0

rum rt-ts a o

A

on -fshy

a

f-

Iar iP s Oo M

r V i

I 3 -n

O 2=

(A tc IL

n

IS

o

i

_0 c PY

c C

01 en vt eo

laquoD bullO

00 ft 9

HS OO

H a

00Mr DO o

X

CO ltet O O

O 3 H-JS

0 O

M0

o rt o n a ~

ff O rrn 0 Hshy

930 c a D

O

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11 U 0 O n o


n

H obullo 03 ft 0 S

a m

I

I

Sshy 0

9 ft O

otn ht Ca-o B) O

bull0tni lt (Dbullo

5 ltQHshyo

o o 3 II

C

0

ID

Stan

dard

vA

1 CD

Mft OO

bullr

00 ltrt 0 0 h-O

O 3

Sif bull0 n 0

Fin

al cone C

omm

ents i


shy

Hshy900 C 0 tv

c IS CD

D B ft ft

ma iB O m

0

i fl

vor O

yen 1shy

r~r^r T -

T

T

T -D C bull4)

T CN

cv

laquogtraquo

i lt ^

i

lt3

6

AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

O 9

00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

bullo 0

CO o

-o Hb

t ^ _D -5 -o

iof

lt3

_o pound

t lA I

1 s

5

D Bgt ft D

lt 0gt bullO

nrt 0

H3 oa 9

CD Hft OO

Q

O 3

D n

O ft o n Q shy

olt 9 O ftt O H-

ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

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Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


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a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

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ANALYTICAL REPORT











ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

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4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


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A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



ICAP LCS

LGGmdash

o mis of

mdash ml of

LCSHCI 1 yen

LCGI ICI 2mdash



rrr

w

CQin

W

CQ Q

H O

W Di

QO

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20044

2

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f tun X bulllt (DTJ

ft 0gt

ss M3 oaogt

n a

r 0 0 5-bull -

m Hft DO

o

r r o

9

O

gt COltft

o o MO

ltHshyO 3

r IT m n

7 r H-O

3 O ft O CQ

O bullbull

^

ttt (DftH O H-- M)

C O

o

Jfi

oca c

0gt (Drtn 5 ltOMshy

m o oD n

u

agtbullo to

I ftfit

o n a o

I

r

cc

H o O

r

8 i

r C

0 cj

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2 i _

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1^

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e

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mdash laquo r

a O

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fH3 oc0 n a

CD M rr 00

0

caltrt o o H-O

0 o

raquolaquoIO H-O

9 3t-gtagt

Oa rr

o gshy

0 o o

e a CO

o 01 rr o

1-hOrfa o o

n en n sshyo n o lt

o 0 0

bullo o

CO laquoT o

E 9

a 1ro laquoa

Bgt

a

i

1

O

o O


c

b

T

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f O o--t

raquolt (0bullo

03

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M C

03 wrr DO

0


3 ltHshyO 3

O O


n ft o o o shy

ITU O Hshy

bullbull i-b

c a D

O-

oD rr o

mo

a o n a

(D

3 a-5 O 9 ltT-t

m lt CHshy

O C O

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pound c

a o

s laquoQ

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01


ro ltampbullmdash

bulla a n c a o

s i r

u

O

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(I

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II

r Ji

^

ts

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T

r Jl

_n

CD

D MS cctt

aHr OO

a yr

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0 3 Mff

M o O

bull=30 H-O = 5 9 3

Q rr O D

O shy

a agtmi O Hshy

SO) c amp

poundS rr 0

n o rt-3 o o ^t 0

o

laquoJ^

wl

W obulla CO

a oraquo n c m

bulla

bullc laquoc0t 2

3 O rr-t

clt2 mdashlt m

c amdash

cA -n


0 -a o mdash Ul 0 u

u

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M01 O

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m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

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Q shy

C 7

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0

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a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

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r r

^

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O


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01


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o 03 rr 9

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p


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o O

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o

r 1deg GO 0 S a0

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H-0 3 S a 3

3

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9 O


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t

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9

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7

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c a 09

O-

o 9 ft O

2 ltOMshym

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n bull0

03

9

a 9

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o

9

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-raquo deg

(

o 0 rt o

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amp

ID

andard

r 5 5 2 8 M U 5 m s g tn

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Q

^raquo c


MO

O 3 secta0 n a

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al cono C

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ents

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rum rt-ts a o

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a

f-

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n

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bull0tni lt (Dbullo

5 ltQHshyo

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C

0

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dard

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c IS CD

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ma iB O m

0

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vor O

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i

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09

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CO Hft OO

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00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

ftO 0 0 n B o


B O O3 n

CD

0

a 0

1

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t ^ _D -5 -o

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t lA I

1 s

5

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nrt 0

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CD Hft OO

Q

O 3

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ft O

Bgt 0gt

ngt OHshy

D o o 31

oort 0

O

O B

bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

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51 4 DC 05 fe

0-7

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I alyst ervisor





pound^l 0^ J zx 3fO

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pur ^^fc -oZGgt 50

Lf7 07 0 -7


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NET

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3 7 1011 1pound 13 4


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t



rgtLK




^ 1

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i ^

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11 1

30 101 J

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I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

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c

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5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

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mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

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^j

S5 Io 1 1 i

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io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

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0 15o5

tv

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ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

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n =

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n i^

r-^ a J v 7

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70011

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4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

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it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

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3-f bull_

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5 ( E5E

11 HS 31 1^

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1 f~~


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bullJ i 1 O


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d loOS u oGo


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(bull

kr

N _

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X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

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^gt i


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|

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his

wor

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duct

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es

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his

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n7

US

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ate

r

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MM

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UJ

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c

g 5

ANALYTICAL REPORT



FD Case 1856

Section One




Bedford MA 01730


TABLE OF CONTENTS


1A

IB

1C

ID

IE

IF

1G

1H

Table of Contents





Page Number

OOP

fOOOsshy

-raquo- JUUI k

JQO

fOpound_










100J1


June 17 1996


RE Tinkham Garage

Dear Mr Mullin






103







Sincerely


enclosures


FD1856


100


FD1856



QUALITY CONTROL










10-t- 7







TABLE


FD1856





bull103^7


FD1856



QUALITY CONTROL






10


FD1856






FD1856



QUALITY CONTROL






10310


FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL





10112


FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLE


FD1856



QUALITY CONTROL






ANALYTICAL REPORT +







1













011






Q Qualifier shy









P - for ICP

A - for Flame AA

F - for Furnace AA






ITEM PAGE




22222

2222222

0004 0007 0008 0010 0011


0012 0013 0014 0015 0016 0017 0020



2

2

22

0022


0042 0045

10310

ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730



FD1856



QUALITY CONTROL



run

The valueanalytes
















ITEM PAGE











(Se As Tl Pb) 0024

NR NR NR NR NR NR




NR NR NR 0042


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-

-

-

-

-

-

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DIVISJOi Contract


Hethod P

End date 06079

Analytes i t


1 i ) r i l t

1 1 1 1 1 1 1 1 i 1 1I bull i U i~^ 1 X 1 t l





raquo - i




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A T H E N A 3 06e

Fe





24




A T H E N A 3 06e

-e





4 ICAP19 ICV 10000000 10628000 1063 3 ICV1A ICV 50000000 51789000 1036


CALIBRATION BLANKS


5 CALB ICB 1000000 130000 U


CRDL STANDARDS





A T H E N A 306e







A T H E N A 306e

-e





28

SFe 259940 16740 000000 00000016380 000000 000000

16740 16380

165244 52996


EL SIGNALsigma

Fe$ 1 6810 059

Measures STDSPEC


$Fe 259940 39259 000000 000000 39259 39212 000000 000000 39212

165520 52996


EL SIGNALsigma

Fes 3923S 008



16810

shy

HI STDSPEC 392355

1


mdash SFe 259940 39365 000000 000000 3936539083 000000 000000 39083



EL CONC sigma

SFa 9Q969 053

39365 10034 PPM 39083 99594 PPM



200

$Fe 259940 19924 000000 000000 19924 19924 4857 PPM 19998 000000 000000 19996 19998 48774 PPM



EL CONC sigma

$Fe 4S676 029



$Fe 259940 55560 000000 000000 55560 55560 10318 PPM 55210 000000 000000 55210 55210 10225 PPM



laquo

EL CONS sigma

SFe 1 0272 064



SFe 259940 17140 000000 000000 17140 17140 000879 PPM 16800 000000 000000 16800 16800-000027 PPM



EL CONC sigma

$Fe 0 00426 150




65960 000000 000000 65960 65960 17519 PPM



EL CONC sigma

$Fe 17514 004i



SFe 259940 64918 000000 000000 64918 64913 17241 PPM 65338 000000 000000 65338 65338 17353 PPM



EL CONC sigma

$Fe 17297 046



$Fe 259940 30240 000000 0 OOOOO 30240 30240 035761 PPM 25460 000000 000000 25460 25460 023033 PPM



EL CONC sigma

$Fe 029397 31






EL CONC sigma

SFe 99108 032



$Fa 259940 17900 000000 000000 1790017060 000000 000000 17060



EL CONC sigma

SFe 001784 89

raquo raquo



SFe 259940 53290 000000 000000 5329053130 000000 000000 53130



EL CONC sigma

SFe 096926 031



F-^ 259940 1T750 0 OOOOO 000000 1775017430 000000 000000 17430


P5WP6W- shy


1

17900 002902 PPM 17060 000666 PPM


1

53290 097139 PPM 53130 096713 PPM


1

17750 002503 PPM 17430 0 71amp51 PPM

1 jMEV5 = for 5ltc

I ltJ OilllUi

EL CONC sigma

$Fe 002077 29



$Fe 259940 20677 000000 000000 20677 20677 54610 PPM 20795 000000 000000 20795 20795 54926 PPM



EL CONC sigma

$Fe 5476S 041



$Fe 259940 22843 000000 000000 22843 22843 60380 PPM 22977 000000 000000 22977 22977 60735 PPM



EL CONC sigma

$Fe 60557 041



SFe 259940 60282 000000 000000 60282 60282 15604 PPM 60571 000000 000000 60571 60571 15631 PPM



EL CONC sigma

$Fe 15643 035



SFe 259940 18791 000000 000000 18791 18791 45560 PPM 18736 000000 000000 18736 13736 45414 PPM



EL CONC sigma

SFe 4S437 023



SFe 259940 51410 000000 000000 51410 51410 092133 PPM 50810 000000 000000 50810 50810 090535 PPM



EL CONC sigma

$Fe 091334 12



259940 19224 000000 000000 19224 19224 46713 PPM 19094 000000 000000 19094 19094 46367 PPM



EL CONC sigma




SFe 259940 22075 000000 000000 22075 22075 54305 PPM 22150 000000 000000 22150 22150 54505 PPM



EL CONC sigma

SFe 54405 026



$Fe 259940 13434 000000 000000 13434 13434 35325 PPM 13499 000000 000000 13499 13499 35497 PPM



EL CONC sigma

SFe 35411 034



SFe 259940 39353 000000 000000 39353 39353 10031 PPM 39376 000000 000000 39376 39376 10037 PPM



EL CONC sigma

bullBFs 10 034 0 04

5


SFe 259940 17020 000000 00000016510 000000 000000

17020 16510

17020 000559 PPM 16510-000799 PPM




EL CONC sigma

SFe-000120 300



$Fe 259940 32140 000000 000000 32140 32140 040821 PPM 31830 000000 000000 31880 31880 040128 PPM



EL CONC sigma

Fe 040475 12



SFe 259940 31610 000000 000000 31610 31610 039409 PPM 31960 000000 000000 31960 31960 040341 PPM



EL CONC sigma

Fs 039875 1 6


2003S


SFe 259940 26090 000000 000000 26090 26090 024711 PPM 26200 000000 000000 26200 26200 025004 PPM



EL CONG sigma

SFe 024357 083



SFe 259940 44202 000000 000000 44202 44202 11322 PPM 44443 000000 000000 44448 44448 11388 PPM



EL CONC sigma

SFe 11355 041



SFe 259940 10095 000000 000000 10095 10095 22405 PPM 10113 000000 000000 10113 10113 22453 PPM



EL CONC sigma

SFe 22429 015



36605 000000 000000 36605 36605 97025 PPM



EL CONC sigma

$Fe 96678 051



SFe 259940 49251 000000 000000 49251 49251 13070 PPM 49416 000000 000000 49416 49416 13114 PPM



EL CONC sigma

SFe 13092 024



$Fe 259940 57693 000000 000000 57693 57693 15318 PPM 57642 000000 000000 57642 57642 15304 PPM



EL CONC sigma

1531I 006



259940 20620 000000 00000017300 000000 OOOOGO


20620 2 Otgt20 010145 PPM 17300 17300 001305 PPM



EL CONG sigma

$Fe 005725 110



$Fe 259940 39929 000000 000000 39929 39929 10185 PPM 39756 000000 000000 39756 39756 10139 PPM



EL CONC sigma

$Fe 10162 032

laquo



$Fe 259940 17790 000000 000000 17790 17790 002610 PPM 16410 000000 000000 16410 16410-001065 PPM



EL CONC sigma

SFe 000772 340



SFe 259940 6o753 000000 000000 6o753 66753 17730 PPM 66440 000000 000000 66440 66440 I6a7 PPM

131637 52996 Method COMM 2003Q


ltC I O I O illlU L

EL CONC sigma

9Fe 17689 033



$Fe 259940 66429 000000 000000 66429 66429 17644 PPM 66354 000000 000000 66354 66354 17624 PPM



EL CONC sigma

$Fe 17634 008



$Fe 259940 28500 000000 000000 28500 28500 031128 PPM 25300 000000 000000 25300 25300 022607 PPM



EL CONC sigma

Fe 026868 22



35Fe 259940 39308 000000 000000 3 308 39303 10019 PPM 39343 000000 000000 39343 39343 10029 PPM



EL CCNC sigma

e 100247 0 07



$Fe 259940 18110 000000 000000 18110 18110 003462 PPM 17060 000000 000000 17060 17060 000666 PPM



EL CONC sigma

$Fe 002064 96


PH AS RECEIVED


1771-148541 S 20 1771-148542 S 20 1771-148542 S2 20





2004



Comm or ( Dj

f Client Name


3I2

4

5

6

7

8

10 i 9

11

i 12

13

14

15

i 16

1 7

18

9

20

mdash

Comments

ICAP Opiku-

ICAP Spike

Furn bplke




Supervisor page 2V






^shy



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LGGmdash

o mis of

mdash ml of

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n a

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m Hft DO

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9

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gt COltft

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3 O ft O CQ

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0 3 Mff

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bull=30 H-O = 5 9 3

Q rr O D

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poundS rr 0

n o rt-3 o o ^t 0

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laquoJ^

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cA -n


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u

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m 0f rr

0 3 H-ff


H-O 3 3 0) 5 H-ffl

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0

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a gt IDrr3o O n m

x to

Verified

11

Date R

un

w o

ltlt of^f w

CD rrffl

H3 OC

O


7

rraquo te lto

CDltrrO o HO

V bull=1ltMshyO 3

t i 1

ox n D O

bullflO H-0

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3 O rr O m

r r

^

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O


bull3

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fO ^ O

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01


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bull3

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o 03 rr 9

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9 n a

X _L

p


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7 VG ib c t c r

o O

03 Mtr -o

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o

r 1deg GO 0 S a0

Q

V fe

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G 0 13

H-0 3 S a 3

3

js o o

rr B

amdash

9 O


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C r c a mdash c a

cshybullB 9

^rshy (2

rr 0

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f -amp -o

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5 ^

o

r r N 3 su

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pound_ ltbull

c

o 0rf O

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dard

ID

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to ltrt0 0MO

0 3 MB

o B

raquolaquoJO

5-i 0 3 M0

O B

a ~

0 0rf i 0 H-

c a O3

2

o 0 rr 0

ff-0 0 O ft B

0

ocn n c 0raquoO 0 0

B 0 0 31

M O bullO

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i0

0

aB

I I i i i

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bull9 Ô

I 1 I


f

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LA

QC

amp r

u raquo rgt O-

t

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pound

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djr

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O

mft 9

H3 OQ

9

mnit oo o

7

mltrtO O MO

0 3 1mdash9

o a

H-O


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c a 09

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o 9 ft O

2 ltOMshym

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n bull0

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9

a 9

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o

9

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-raquo deg

(

o 0 rt o

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amp

ID

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r 5 5 2 8 M U 5 m s g tn

Hft OO

Q

^raquo c


MO

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al cono C

omm

ents

0 Ortn O Hshy

bull0 0 laquoa

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rum rt-ts a o

A

on -fshy

a

f-

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n

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o

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HS OO

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n

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a m

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bull0tni lt (Dbullo

5 ltQHshyo

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dard

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bullr

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al cone C

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c IS CD

D B ft ft

ma iB O m

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r~r^r T -

T

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T -D C bull4)

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cv

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AQ o 0 rt O

bull0tonF lt obullu

09

H3 oa 0

CO Hft OO

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00

0 3

OB

28SI MO

Ofi O B

Sshy

Dlt 0 O

900 pound Âi

raquo Oshy

O 0ft o

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B O O3 n

CD

0

a 0

1

bullo 0

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t ^ _D -5 -o

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lt3

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t lA I

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5

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Q

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D o o 31

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bull0 0 |QO

ftgtO ^b ^3

D

-gt D bull fraquo



ANALYTICAL REPORT



FD Case 1856





Bedford MA 01730


TABLE


FD1856






FD1856



QUALITY CONTROL







FD 1856






FD1856



QUALITY CONTROL







FD1328



QUALITY CONTROL






FD1856



QUALITY CONTROL






FD1856



QUALITY CONTROL





TABLE 7




QUALITY CONTROL





TABLET


FD1856



QUALITY CONTROL






ANALYTICAL REPORT




NET Job No 9601771

Date Recd 05211996



Alkalinity

92113-NAI-H2-0596 92113-NAI-C3-0596

AQ EPA 3101

148541 148542

150 68

ppmCaC03 ppmCaC03

308 308

05301996 05301996

dec dec

Ammonia

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3501

148541 148542

039 038

mgL N mgL N

06131996 06131996

nsv nsv

BOO shy 5 day

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 4051

148541 148542

lt20 lt20

mgL mgL

501 501

05261996 05261996

dec dec


92113-NAI-M2-0596 92113-NAI-C3-0596

AQ COD 4104 mod

148541 148542

25 47

mgL mgL

330 330

05281996 05281996

dlw dlw


92113-NAI-M2-0596

92113-NAI-C3-0596

148541

148542

31

140

mgL mgL

48 48

06101996 06101996

nsv nsv

Nitrate-calc

92113-NAI-M2-0596 92113-NAI-C3-0596

AQ EPA 3532

148541 148542

0052 lt0020

mgL N mgL N

42 42

06071996 06071996

nsv nsv

70030












700-jI









Alkalinity EPA 3101



Prep_ j_ TrueValue=




0 D 385 2ZS 77

bulli Hue 71

K 3JS S40 35Zgt

00

37T

33 6 nzraquo

531

73

bullI] 11AO



0 0271501 10120 476 0084L 0008


K 162-147968 0034 1 0028 11 1605-148072 K 0022 17 1


nV06-148214 3415 1 1 1573 shy106-148215 1 0 0045 1706-148216 1 0107 1U -W 6 1577shy

1 1 0110 1 0042 1 1 0024


0008

Jgt

700









fj f5



1 ti^l $ amp4ol ft) ^^3 ^17- lt2

r 3d S35^ 6-1-6 lt2_ lt2lt2




3 3 - 3 D ^-33 ^08

5 36 ^ 3 4 41 cL ^2amp

-



Date

bullff

Labsys Batch gt - 7



Rack Number 1

531

^0-7

1727

la

Rack 2

If

776

tit in

701

NET







BLANK oampo LCS

70

OH1

Ho 00^shy

BLANK 00 0 ZlS LCS

51 4 DC 05 fe

0-7

Q O f t

HID 00k IK C70 700


I alyst ervisor





pound^l 0^ J zx 3fO

^V bull Of 9 S5

pur ^^fc -oZGgt 50

Lf7 07 0 -7


020

Cfeo

r7V

602

oil

(^|

7-7

t 20

^5

^K ^( 39

fJ

BLANK 00 fc^^ 1 ^

LCS

^00$

OM

nc^ ^C j j

ô ltWL ^7^

IT7I cc oCH IS


nn 10

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z^^ ftu

Li4iL

lUfo

orlaquo| )OD ^x

ygt )laquogt


H r

NET

plusmn L-ni__jr c



3 7 1011 1pound 13 4


H Hpound HO HH

HJ bull40^7 HO

bull47 505i


r -i i 0 Imdash

t



rgtLK




^ 1

^ ^ i 1 1 1^ E c

i ^

5 E5 11

1 1 JL

E b 5

E5 pound5 5

1-)1 i 1 i

O1 pound5 pound5

pound 5 1 1

EO IO

11 1

30 101 J

E pound E

i i i i 1 1 1 1 1 1 1 1 1 1 1 1 i 11 i mdash 1 1 1i j1 1 1 -t

I1 1 i i 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 X

Ul- bW O

He 5o

513 1-4C3

~i jr- i O

S3E11


- 9E icbo


O 1317


35E3 35E8 3533 3538 35M-E 35-47

^bull43 1 359


O

fc r

R

F

O

R R

0

c

R R R R R R O

JD


3 U


1 O1-


lt- 5 1 i 5|c

- bulllaquo mdash c

Oo 175^ 3575

C ~ bull wJO i_JO





5 19o vshy37n39u



b 9oE ^ 59^0113 33pound59S-49 ^1




~mdash

mdash

mdash

mdash

~shy

mdash

mdash

shy-1C 53 OH crcshy




i H O H f c j i C3C

1 M Oto7|- S

1 bullshy O--Ô

poundgt_bullbull

^L-V

^j

S5 Io 1 1 i

pound5 pound5

oVgt poundo 1 O

io 1 j50

j 1

A

1 1 11 i 1i i ^ i i 1

T 1 1

cVoo 20O6 272Si_ 133C

i_ 1 376 887

113E C1 bull 7 Io53

oo

1E15 E5C1 ^ bull

0 15o5

tv

0S oi t

ta

Vlgt



58EH3V 37 999



bdquo

~v 71 ~c

^~+ ~3 7o

73 79

1 -fO-401^

raquo shy O5



Imdash mdashE


_^ 1

rf 1i 1 1i 1 ^ 1

1 5to EoaV



Vy

n =

OCj

oSEBl EE5 copound



n i^

r-^ a J v 7

lampjC ^- ^ J9

70011

_

CL

V sr

4 c

7001


Analyts

Analyst

ICVCCV True value

Job No Samle No 1

Labsys Batch

Data 0 60 -$amp

Page

A03 JL02


Recovery

0oLG

O-2 G

00

41 6b svampygg OZo

loolamp

amp06V

0

0020 20020

lt

y z

Z

pound0010 I o fLy

L CO-7O

0

701 p

f I i LE





n i T 4 J

i

1

1

1

1

1

i 1i

iiiiii

ii4

i

ii

i

iiii

iiii

i11iii11iiiiiii i1

it-j n ~3opoundH

t ON

657 139u 3M-3-

(1 -t -S

O oo OgtZl


rshy155

M-Mshy~~ ^J

3-f bull_

1 5poundoi j

5 ( E5E

11 HS 31 1^

555 bull45 19

151HC3

t sect H-6

1 f~~


73O l_laquo ltJ

i 5o3bull i Jt-So

BOH lt_

1515i_j

t- v I Zgt

v O-o

bull_ OOMshy

O pound 1 9 u ()gt+

J 1 o O

bullJ i 1 O


^ ~~ ~ v raquodu r

G lt i1

bull UU5

d loOS u oGo


O i



(bull

kr

N _

S

7001

X






ICV True Value mgL



01^


amp4l t^q OM^


ccv CCB

J101 r







1 5 51






^ tiamp 1HA 7f-^ 1C1 710 (03^

I m-T




$7 Z








r Sulfate EPA 3754M



LCSIot LCS Prep


i li-4 5



2X nl 213

fe 77 SMI 21 HIS

H7I

ooX Vn

230

1

I c o U

ou

nd

O-j

90 laquo3

VA Ni 1 11 1 31 11 1

a E

laquo^ i

c8 ii


9

abulli

Ui

Ebull a 3

3-1 O XT

O 0shyUI 4

U O

E 0 C 3 3

c C 3 3

a






June 5 1996


Dear Richard


Sincerely



ANALYTICAL REPORT













ANALYTICAL REPORT

05201996

JOB NUMBER

SAMPLE NO

92113-DVE-07-0596 B00733

PAGE 2

9606991

347306







SAMPLE NO 347307








SAMPLE NO 347308








SAMPLE NO 347309








SAMPLE NO 347310






ANALYTICAL REPORT




347716 92113-FW20-0596 B00749 05171996 05181996 347717 92113-FW11D-0596 B00750 05171996 05181996 347718 92113-FD01-0596 B00751 05171996 05181996







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW20-0596 B00749

PAGE 2

9607118

347716







ANALYTICAL REPORT

05251996

JOB NUMBER

SAMPLE NO

92113-FW11D-0596 B00750

PAGE 3

9607118

347717







SAMPLE NO 347718






Tel (513)2946856 NET Fax (513)294-7816

ANALYTICAL REPORT




347507 92113-ERT01-0596 B 00746 05161996 05171996









SAMPLE NO 347507





bullbull

2

s -s

^ ^ -gt

Ye

s N

o 1

c ^N gto bullmdash

1)

X bull

shy Oshy

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^gt i


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B|B

H||H

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his

wor

k be

ing

con

duct

ed lo

r re

gula

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es

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his

wor

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r

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LL

c ^ --- 0


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bull

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bulllt X

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f an

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of

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PLE

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cr

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(PR

INT

NA

ME

) raquo

SIG

NA

TU

RE

ÛJ LU cr 2 QD

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ED

Y

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N

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LJ Nj


C cr gt bullgtv

V) 0 bull0

CO ^s 0 o LU 1

en i - 0 UJ gt

li 2 C^


UJ

sect bull

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CO

j ^ N)

u rgtshy

$ ^ V lt LU


bullv

H

copy V

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bull 8 1 ^g

m gt^ gt LL omIf l


UJ lti


CO

ND

I


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1


C

fe Z U j


PO

V tl s rshy

$1 LJJ O I- IB

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t-N Vi)

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ky- I


lt UJ

x


0 P OC Z LU

LL s g y

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raquo LL o -i o

H Q

O


12glaquoUJ Q

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zw uj

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LLJ Lt LLJ

lt W

^j I

c g

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LLJ

D

CO LL

4O O o X

UJ

^

c

g 5

net: fd case 1856 inorganicssection. please find enclosed a diskette of the results for this case....

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