hwbdocuments.env.nm.gov alamos national labs/ta 54/11758.pdfv~aiamos natio~~ l boratory solid waste...

v~Aiamos NATIO~~ L L BORATORY

Solid Waste Regulatory Compliance P.G. Box 1663, K490 Los Alamos, New Mexico 87545 7 -0666/F ax 7-5.224

Mr. Carl Will Permits Management Program Hazardous Waste Bureau New Mexico Environment Department 2905 Rodeo Park Drive East, Building 1 Santa Fe. New Mexico 87505-6303

Dear Mr. Will:

Date: September 26, 2002 Refer To: SWRC:02-070

SUBJECT: Transmittal of Requested Waste Characterization Data from Technical Area 54 (TA-54), Area G

The purpose of this letter is to provide NMED with review copies of waste characterization paperwork for twenty-four waste streams. This data set is being submitted in response to your request on June 11, 2002 for copies of the information that you and Steve Pullen began to review on-site.

Inc I uded is a binder containing copies of the infom1ation requested titled, "T A-54 Area G Disposal Supplemental Information as Requested by NMED" (LA-UR-02-5584). Also enclosed is a CD containing the database query that was performed on June 11, 2002, at the request of the inspectors. The data on the CD encompasses waste disposed at Area G from January 1991 through March 2001 and contains approximately 50,000 items. If you have any questions, please contact Luciana Vigil-Holterman at 665-3435.

Sincerely,

\ 0\-tyry/-)

~esL. White Solid Waste Regulatory Compliance Group

JL W IL VH/vch

Enc. a/s.

An Equal Opportunity Employer I Operated by the University o National Nuckar Security Administration of the U.S. Depart

11111111111111111111111111111111111 11758

Mr. Carl Will SWRC:02-070

Cy: w/enc.

Mr. Steve Pullen Permits Management Program Hazardous Waste Bureau

2

New Mexico Environment Department 2905 Rodeo Park Drive East, Building 1 Santa Fe, New Mexico 87505-6303

Cy: w/o cnc: G. Turner. DOE/OLASO, MS A316 R. Ramsey, LANL, RRES-DO, J519 S. French, LANL, FWO-WFM, MS 1595 L. Vigil-Holterman, LANL, RRES-SWRC, MS 490 J. Ellvinger, LANL, RRES-SWRC, MS K490 G. Bacigalupa, LANL, RRES-SWRC, MS K490 SWRC File IM-5, AlSO

September 26, 2002

An Equal Opportunity Employer I Operated by tile University of California for the National Nuclear Security Administration of tile U.S. Department of Energy

I I

T A-54 Area G Disposal Supplemental Information as Requested by NMED

Prepared by:

Los Alamos National Laboratory Waste Facility Management (FWO-WFM) Los Alamos, New Mexico 87545

LA-UR-02-5584 September 2002

LA-UR- o1.- 55~4 Approved for public release; distribution is unlimited.

Title: TA-54 Area G Disposal Supplemental Information as Requested by NMED

Author(s): Teresa K. Hofheins Sean B. French

Submitted to: NMED HWB

ALAI • os amos NATIONAL LABORATORY

Los Alamos National Laboratory, an affirmative action/equal opportunity employer, is operated by the University of California for the U.S. Department of Energy under contract W-7405-ENG-36. By acceptance of this article, the publisher recognizes that the U.S. Government relains a nonexclusive, royalty-free license to publish or reproduce the published form of this contribution, or to allow others to do so, for U.S. Government purposes. Los Alamos National Laboratory requests that the publisher identify this article as work performed under I he auspices of the U.S. Department of Energy. Los Alamos National Laboratory strongly supports academic freedom and a researcher's right to publish: as an institution, however, the Laboratory does not endorse the viewpoint of a publication or guarantee its technical correctness.

Form 836 (8/00)

Item id w_2_fno cwdrno rswd id 18772 4613 1003449

517393 2017393 S873611 517609 2017609 S820973 517638 2017638 S834560 518100 2018100 S840516 520511 2020511 S855873 520532 2020532 S820173 523929 2023929 S900150 524146 2024146 S903087 524283 2024283 S902784 524419 2024419 S902776 524522 2024522 S900951 524567 2024567 S902747 529413 5720 2029413 L93000309 530036 2943 2030036 L94000084 530780 8513 2030780 L94000407 531.097 8899 2031097 L94000596 531269 9965 2031269 L94000806

1001767 19900925141800 1008018 19900925141800 1017402 19900925141800 1017458 19900925141800 1035245 19900925141800 2045784 33037 3011359

J~~~~@~ L • I 3mos 1\!atior~al Laboratory

RECEIVED ocr I CWDRH 100344Q ~ 3mos, 1\levv Mexico 8 7 54 5 0 i992 I CHEI\~ICAL WASTE DISPOSAL REQUEST

1e all informacion requesu:d on bolh sides of chis-form in black or blue ink, inadequate informacion v/i/1 Fesult in processing delays.

Send compleled form 10 ATTN: CWDR, MS J593. Any telephone inquiries should be 'direcred 10 5--4000.

roup 2. Telephone 3. Mzil Stop 4. Tech.Are~ S. Building 6. Room I

t-7S7?'7 .:FS9'3 ~C/ ~~~ Jt--& fJ?-7 ~.>-(~ .(\_ / ~

•

.. ·_, ,, ··-' . -

'

' 10. Itemize below, by compound or chemical_ name 1. each UNUSED CHEMICAL PRODUCT destined for disposal. Check all applicable Hazard Codes.

Number Volume Weight of

Haz.ard Codea2 of of Waste and

Containers Container Container Compound or Product Name c I R T X s L G 01

02

03

04

05

06

07

08

09

10

11

12

13

14

15

16

17

18

19

20

COMPOUND OR CHEMICAL NAME = Name of single compound, names of all compounds in mixture, trade name and/or number of commercial product. For trade-name product, attach manufacturer's MSDS. YAZARD CODES: C = Corrosive, I = Ignitable, R = Radioactive, T = Toxic, X = Reactive, S = Solid, L = Liquid. G = Gas

rhis Page For EM-7 Use Only

>is position

0MAP Shaft

0Be Shaft

0PCBShaft

0 MW Storage Shaft

00ther

late Waste ieceived

,ctual Volume

)ross Weight (lbs)

·are Weight (·)

let Weight

/

>ale No. Compaction Date

(MM,OO,YY)

I l I I

I J I I

4. EM-7 A

I I

0 Low-Le H3 Shah

D High-Level H3 Shalt 0Animal1issue Shalt

0MFPShaft

D Source Shaft D Powder Shaft D Holding Shed 0MWH3Shed

ocompactor D HEPA Filter Shaft

Bale Volume (M;;)

Site Information

Vehicle Code

0Dumpster (01)

0 Dump truck (02) (ZJ F}atbed (03) 0 Pickup (04) 0 Shield cask (05) OEM-7 truck (06)

0 Other (specify below) (07)

ompact on nformation Comments

7. Disposal Location Information

L92000814

Date Approve1:;

lb·t~·tl.-

~WPit 0Asbestos Pit

0 MW Storage Dome 0 Certifiable TRU Dome D Uncertified TRU Storage

Treatment Code

Ocompaction (01)

Olncineration (02)

Oother (03) 0None (04)

l

I

Disposal Date Area Shaft Pit Transit Sequence No. Post(s) Layer Position

(MM,DD,YY)

l 10 I l I 41 9 I z G I I I I I

Storage Date Area

(MM,OD,YY)

Jirector of Disposal or ptorage Operations (Print)

(2-H~ LI:3'S A · ~ M ~ (ij2_ )crer· ·

RSl-!D

L92000814

Nasta Profile ~equest No.

·otal Waste Volume

Comments

Packa9o Codeo"

)1 • Bulk (unpacka9ed)

)2 • Wooden cute

)3 ·Drum

l6 • Steel box

17 • SI>HI cask

IB • Other ( speai'y ~low )

Radionucli de

0 Meter 0F~t3

Q ~allons

Package Code•

~units: C = Curies M = Grams

2. Hazardous Materials Transfer Form HM No.

Estimated Weight

Package Volume (Individual Package)

Amount

E +I-E +I· E +I· E +I· E +I· E +I· E +I-E +I-

Volume Units••

Units+

1. Waste Originator lnfonnatlon

C & 0 Fonn Numbers

Number ol Packages

otal Vol. ol Package Type (Pkg. Vol. X No. of Pkgs. )

Uncertainty Method++

+I- %

+I- o/o

+I- o/o

+I- o/o

+I- %

+I- %

+I- %

+I- %

HMethods: A= Analysis M = Measurement C =Calculation E =Estimation

3. Waste Certification

Volume Unit."

SS Acet

Volu.,... Unita-

G • Gallonl

Proj. Code

HERA lOR CE.RTIRCA TION STA TlME.Hl: My ai!r"''..-e ca-Uf,., thai tho_."' io .. doocribeod hen end on tho etl&ched We.oto Prolilo ~ lonn. W"""' ~~ _,leppllc.able -.ccep-1 olora{le or diopoNI criteria lloled In AQninlotnotiYI Req.JitMnent10.2, "low-lAve! Red06C1iw Solid W-ta," end In "W.-e Acoeplao"Q Critll>ria lor l.ow·!Avel Racloectiw W-to Olapc>NI8t -54. Area G."

•nerator's Name (Print)

6

I I

) /

EM-7 WASTE MANIFEST ....

**:;+

..

los ALAMOS EM-8 USE ONLY WASTE PROFILE FORM Reference Number los Alamos National laboratory

los Alamos, New Mexico 87545 .. D"/(o I 3 I,

Complete both sides of this form using a black or blue pen. Incomplete forms will be rejected. Send form to ATIN: WPF MS K490.

Division/Group Telephone Mail Stop Technical Area Building_.--../'\ Room

2.0 nC/g 0 beta ~ 0 t'n :2:. 20 yr 0 > 10.0 nC/g 0 > 100 nC/g

Oj.lamma

0 tritium WASTE GENERATOR CERTIRCATION: &sed on my knowledge of the waste and/or chemical/physical analysis, I certify that the information on this form is co~ct. I understand that this information will be made available to regulatory agencies and that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.

Wasfe Generator's Name (last, first, middle) Z Number Signature

' ~ffi'&lJQ.- 9(~ ~ 97b83 ~ If your waste management coordinator is the custodian of your waste management documentation, provide the name and mail stop of this person (optional). --->

Form 1346 (6/92)

RECEIVED 0 CT

Name (last, first, middle)

2 Cf99~ete Reverse Side .-

~ECEIVEO OCT

Date

Mail Stop

Page 1 of 2

...

.. ....

Toxic Metals (Indicate if each of ihe following heavy metals exists in your waste at the posted concentrations) arsenic 0 None 0 < 5.0 ppm 0 .:: 5.0 ppm 0 TCLP 0 Other barium tJ None 0 < 100.0 ppm 0 .::100.0 ppm 0 TCLP 0 Other cadmium [] None 0 < 1.0 ppm 0 .:: 1.0ppm 0 TCLP 0 Other chromium ~ None 0 < 5.0 ppm 0 ?. 5.0 ppm 0 TCLP 0 Other lead None 0 < 5.0 ppm 0 ?. 5.0 ppm 0 TCLP 0 Other mercury m None 0 < 0.2 ppm 0 ?. 0.2 ppm 0 TCLP 0 Other nickel

I None 0 < 134.0 ppm 0 .:: 134.0 ppm 0 TCLP 0 Other

selenium None 0 < 1.0 ppm 0 .:: 1.0ppm 0 TCLP 0 Other silver None 0 < 5.0 ppm 0 .:: 5.0 ppm 0 TCLP 0 Other thallium None 0 < 130.0 ppm 0 .::130.0 ppm 0 TCLP 0 Other

Organic Compound~ (Indicate if eacft! of the following organic compounds exists in your waste at the posted concentrations) benzene

r·~ 0 < 0.5 ppm 0 ?. 0.5 ppm 0 TCLP 0 Other carbon tetrachloride None 0 < 0.5 ppm 0 .:: 0.5 ppm 0 TCLP 0 Other chlorobe nze ne t:=

0 < 100.0 ppm 0 .::100.0 ppm 0 TCLP 0 Other chloroform 0 < 6.0 ppm 0 .:: 6.0 ppm 0 TCLP 0 Other cresol 0 < 200.00 ppm 0 .::200.0 ppm 0 TCLP 0 Other 1 ,4-dlchlorobenzene None 0 < 7.5 ppm 0 ?. 7.5 ppm 0 TCLP 0 Other 1 .2-dlchloroethane None 0 < 0.5 ppm 0 .:: 0.5 ppm 0 TCLP 0 Other 1,1 -dlchloroethylene ~\None 0 < 0.7 ppm 0 .:: 0.7 ppm 0 TCLP 0 Other 2,4-dlnhrotoluene :None 0 < 0.13 ppm 0 .:: 0.13 ppm 0 TCLP 0 Other hexachlorobenzene ID None 0 < 0.13 ppm 0 ?. 0.13 ppm 0 TCLP 0 Other hexachlorobutadlene 0 None 0 < 0.5 ppm 0 ?. 0.5 ppm 0 TCLP 0 Other hexachloroethane 0 None 0 < 3.0 ppm 0 .:: 3.0 ppm 0 TCLP 0 Other methyl ethyl ketone .. 0 None 0 < 200.0 ppm 0 .::200.0 ppm 0 TCLP 0 Other nHrobenzene 0 None 0 < 2.0 ppm 0 .:: 2.0 ppm 0 TCLP 0 Other pen1achlorophenol 0 None 0 < 100.0 ppm 0 .::100.0 ppm 0 TCLP 0 Other pyridine D None 0 < 5.0 ppn: 0 .:: 5.0 ppm 0 TCLP 0 Other tetrachloroethylenelperchloroethylene 0 None 0 < 0.7 ppm 0 ?. 0.7 ppm 0 TCLP 0 Other trichloroethylene 0 None 0 < 0.5 ppm 0 .:: 0.5 ppm 0 TCLP 0 Other 2,4 ,5-trichlorophenol 0 None 0 < 400.0 ppm 0 .::400.0 ppm 0 TCLP 0 Other 2,4,6-trichlorophenol [}] None 0 < 2.0 ppm 0 ?. 2.0 ppm 0 TCLP 0 Other vinyl chloride [}] None 0 < 0.2 ppm 0 ?. 0.2 ppm 0 TCLP 0 Other

Haz.ardous Constituents (Identify hazardous constituents for F- and K-listed wastes and substances causing waste to exhibit a characten"stic)

,t4Je,$=7

Additional Comments (Provide comments regarding the chemical or radiological nature of the waste)

Waste Classification

0 Non-RCRA waste

0 PCB 0 non-PCB TSCA waste 0 asbestos

RCRA Code 1 RCRA Code2

EM-8 Reviewer's Signature

Form 1346 (6192)

Do not write in this box - EM-8 use only

0 RCRA-regulaled solid waste 0 RCRA-regulated hazardous waste EJ Radioactive only

0 municipal refuse 0 hazardous waste 0 nonhazardous chemical waste 0 mixed low-level waste 0 administratively controlled waste 0 mixed lransuranic waste 0 sanitary/industrial sludges

RCRA Code 3 RCRA Code 4 RCRA Code 5 RCRA CodeS

'EJ low-level waste 0 transuranic waste

RCRA Code 7 RCRA Code 8

Date Cost Center/Progran1 Code for Analysis Reference Number

Page 2 of 2

I I

.,. - ..... DATEo /1)/:;/c;:J. I . To. CLmM. /)gj)~LA_f~ MS 3Sq3 FROM: Michelle Cash, HSE-8, MS K490

SUBJ: WASTE PROFILE REQUEST (WPR)

The HSE-8 Hazardous and Solid Waste Section has reviewed and Jogged the information you provided on the attached WPR(s). Based on the information you provided, your waste(s) is:

A. Non-RCRA waste

D PCB 0 non-PCB TSCA waste

0 Asbestos

B. RCRA-Regulated solid waste

0 Municipal refuse D Non-hazardous chemical wa5te

0 Administratively controlled waste 0 Sarutary /industrial sludges

C. Hazardous or Mixed

0 Hazardous waste

0 Mb:ed transuranic waste

D. Radioactive

/Low-level waste

0 Mixed low-level

D Transuranic waste

You are required to keep a copy of the WPR(s) in your files for at least 3 years. This WPR(s) is valid for one year or as long as the composition of the waste you have characteriz.ed remains the same. Should your waste change, submit a new WPR to EM-8 and attach a copy of the WPR which is being replaced.

Attachment(s)

,.. See ReveJ"M Side for Hllndling Jrutruction

.. ..

I

\

...

INSTRUCTIONS FOR HAl"IDllNG YOUR WASTE

A. Non-RCRA Wa~te

Polvchlnri=ltti Biphrnyls (PCBs)- Wast~ containing greater than SO parte per million PCB are subjl>ct to the Toxic Substance Control Act (TSCA) and m~t be managE'd in a similar manner to hazard ow wastee (see AR 10.7). Nnn-PBC TSCA W1151'- Other toxic su~tanc-ee are sut.ject to TSCA. While their management i~ not ae rE"I!Itrictive u hazardous wast~ or PCBs, they m~t be managE'd in a manner coruietent with conuoliE'd eubetancee. Asl>eslns- A~bt'!!toe removal is controliE'd by the Oean Air Act (CAA) and the Occupational Safety and Health Administration. Disposal of asb~toe is controiiE'd by the the New Mexico Solid Waste Act (NM5WA). Removal ol asMtoe or aeMt06-containing material should be performE'd only by tninE'd penonne.l from JCl. B. RCRA-RegulatHI solid wute

' -

Munidpol RLfu~- Waetee such as office, calt'teria, or rll'!!troom traeh which may be di3poeE'd at a sanitary &Oiid wute land.filL

Nonhazardous Chan it:» I W115t~- Chemical waetee not ~tE'd by RCRA 88 hazard oW! waete but which may }'OM a potential threetto human health and the environment i/ di8poee-d untreatE'd in an uncontrolJE'd land1ill.

Atiministrativdy-Contrn/Ted- WastE"!! such as nonhazardous aeh and debri!l from active ~ch fi.rins sitee, empty compre58E'd gas cylinden~, empty containers, and ueetE'd berium sanda cfupoM>d at the Laboratory's indumlaJ landfiD for segregation &om public contact and livt'!!toclr..

Sanitary/Industrial Sludges- DewaterE'd sludgee from Laboratory nonradioactiv._. wutewater treatment fllciliti• manased by EM-7.

C. RCRA-RrgulatHI solid wute

Ha:.ardous Wast~- Nonradioactivl' haz.ardoue wute.

Mi:red Low-L~I Wastr- RAdioactiv• waetll' that i.e not a transunmic waete and e:xhlbits a haz.ardoue charactmmc or contain! a component cawing it to bt> &tE'd 88 a haz.ardoue wastl'. The radioectivl' component i.e conuolJE'd by DOE Order 5820.1a and the haz.ardow component by RCRA.

Mi:rttl Transuranir Wastr- RAdioactive wa~e that contains an alpha~ tranruranium radionuclidt> with an activity of grl'ater than or &olid wa~• containins nontnuun.1ranic alpha contamination, tran1uranic alpha contamination Ieee than 100 nC/g, ~contamination (indudins tritium), or o:hibitins ~radiation.

Tran~uranir W.utr- Radioective wutt> that contAins an aJpha1!Initting tranluranium radionudide with an activity ol greater than or

-, ! I , I ; ; ' ' ~ .. ' ": I ; \ .. ' ' 'j. \ ! ' ' • ! \ t - f ~ J l I !

1. FORM NUMBE~ ---------S~BJ2lQ1l1'

LOS ALAMOS RADIOACTIVE SOLID WASTE

DISPOSAL RECORD FORM

1-J~ET-RI-E-~ AHL-l

SE f11AL NO

I t --- -~ - -~

5. WASTj CODE

A~t~

F WASTE (.!) z

lA BLDG ~ ROOM - -- -·

) .')1_2, 1ti\1Y' It I~ I I I

4. ORIGIN 0

CODE E fST!MATE -- -----l--c

~ ' L.___ ! I I I _j

! I ' I I ~~ I I ,

_:lj I

- --··--- --- -- __ _1

GROUP LEADER lAS NECESSARY) s,~,dturt.• c,•rrd,t.>t that wasre fJ.JCkd!/f' or shJpo~t•nt 15 s.Jit• to handiP and transport.

···-----~-=-=-=-=-=-=-========= --------- -

~AFT SURFACE L_ DOSE

MR/HR

PLEASE READ INSTRUCTIONS ON BACK CAREFULLY

LOS ALAMOS RADIOACTIVE SOLID WASTE DISPOSAL RECORD FORM

:l. RETRIEVABLE SERIAL NO.

I•

4.

I

ORIGIN ()F WASTE

GROUP TA BLDG.

I J111 /I~ tt~~c~s

\!) z fi

I

H-7 Waste Management Ext 6095 MS J592

ROOM

I I

5. WAST CODE

.....-----------------------6. WASTE DESCRIPTION --------·-··--- ----- -~~----.3 7. NUMBERS OF WASTE PACKAGES.

CARD PLASTIC BOARD BAGS BOXES

I I I I

DRUMS

NO. l~~~~ __ 1 8J.iS

I

s 8 4

2. DATE

Mlv1DDYY

PLEASE READ INSTRUCTIONS ON BACK CAREFULLY


DISPOSAL RECORD FORM.

J. RETRIEVABLE

SERIAL NO.

4. ORIGIN OF WASTE

GROUP TA

WI X I -15 I 4 11

BLDG.

I I t0t4

HSE -7 Waste Management

Ext 6095 MS J592

~~ tltJ t2J

I Wt ItT IH I '•

7. NUMBERS OF WASTE PACKAGES M ~ METER3 F ~ FEET3 9. PACKAG

E RADIATION AT:

CARD PLASTIC BOARD

B.t..GS BOXES

I I I I

DRUMS

NO. GAL.

I I 1 I 1

K =KILOGRAM P =POUND

WOODEN CRATES

NO. VOLUME-ft3

I I ! I _!

SURFACE 1 METER MR/HR MR/HR

8. GROSS ~ G • GALLON z

VOLUME :J

I ,1 '0 6 I I I_/ f I I l.d

10. GROSS ~~~~T====T~O~N====~------------------------------------------------------------------~

WEIGHT 5 \ 11. ADDITIONAL D~SC_£l1PTION oF PACKAGING AND PACKAG_IN __ G_M_A_T_E-:-R_IA~L_s--,..,.==~--------4

,p,u f:t: ., '7os; ; c ids-~~.···.:· . ff'_;jib?~.,-I 'r 4 K 12. RADIONUCLIDE CONTENT

C=CURIE AMOUNT DETERMINED BY: 55 MATERIALS M • GRAM

I I 1 I ' .I • > ' • • • " • ~

7. NUMBE~SOF W/\STE PACKAGES 9.PACKAGE RADIAiiON AT:

CARD- ORV~S WQOOEN CHATES PLASTIC BOARD VOLUME·ft3

BAGS BOXES NO. GA1.. NO. 8. GROSS

SURFACE t METER MAr.-tR .MAIHA ·-, J;J ~ , I I I I I I IL I I I f

I . I f 1(/, j I I K • KILOGRAM r •POUND 10. GROSS VI T•TON ... ,

WEIGHT ! . ["; :D~IT:9~AL DESCRIPTION OF PACKAGING AND PACKAGI.NG MATERIALS ,;

~j,a,o,o f ; I I 1· I I . I I I I l I I I I I 1 k. L · I j I 1 ; I ; I I I. I 'I I

ACCOVNT COOE

;.f

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I

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1. FORM NUMBER

s 8 2 017 _L...::_~-'--....L-.J

: 'U ,'\ :"'. L i\ ;_ ,; C I ~~:, T f~ U C T I 0 N S 0 f'J 8 ;:., C t< C A f~ Ef U L L 'l


DISPOSAL RECORD FORM

3-.-~-E :;-;,-, V AB l j SERIAL NO

I I '------

4. ORIGIN OF WASTE

GROUP TA

I (lkJic:.J$ I'Z

BLDG.

I I 151il

C) z i

t ,. ~ 1; ( 1 r 11 1 · ' , : , 1

ROOM

I I I

5. WASTE CODE

~- ::~~~~~~:,IP~~O~ ~ ~l D1M ~~~ --~------------~--~~---_-_-_-·-__ -__ --------------~ J M- METER 3

F • FEET3 9. PACKAGE RADIATION AT:

K KILQ(;HAM r ··POUND

tG

nOSS ~G·GALLON " z

VOLUME :J

1 ~~,.o f

SURFACE MR/HR

I I I

1 METER MR/HR

I I I I I ,o

::: __ ..LJ.Oll_ --

~J r~l~ -~\DD:;;O~~~ -D~~CRI~~~()~ ~-~-;~~':~G!_~-~-~~~ PACKA __ G_IN_G_M_A_T_E_R_IA_L_S _________ -l __ _L_,__-'-'t _ _._j l _ . ___ 1 I I I I I I _I I _1_! I I I 1 1 1 I I I I I I I I

~~-1~L~~~-4-E~~~-4-+~f-~~ ~'-+-E~-L~-l

/ ___

1

1 _', _ L~ i : 11 : .J : .~ : _: _: J~=='-------------L-. ___ J. __ ___J ~ 76fl-- ---- -~£. ./} ~..J.L '.'~ASTE GENERATOR H-f'fFfEA R~ATIVE

S1_qnatun.> certif1P.S char wast,. is 1n a.:cordc~ncr• w,rf, .111 ---"~p-pf~a_hl_e_diwo~_lr_PQuir~_"_'e_n_n._

• HS-t!7-1A(J0/81)

Siyn,Hure Ct•rtifier that waste package or shipment 1S s.1/t.' tn handle and transport.

-----------14. DISPOS.\L/STORAGE LOCATION

AREA SHAFT

< ' I ~ ': ' o .. '

GROUP LEADER (AS NECESSARY)

15.SHAFTSURFACE l DOSE

MA/HA

I I

Los Alamos Los Alamos National Laboratory Los Alamos, New Mexico 87545 1. Form Number

M

0

, •• Wooto Demlpllon

3. Retrievable Serial Number

7. Numberl of Waste Packagel

RADIOACTIVE SOLID WASTE DISPOSAL RECORD NOTE: Read instructions on back carefully before completing this form.

HSE-7 Waste Management

Ext. 6095, MS J592

5. Wa1te Code

9. Package Radiation at Card- Drums Wooden Crates

Plastic Board Bags Boxes No. Gal.

I I /JO~ I I 4 I 10. Gro11 Weight

Amount

12. Radlonucllde Content

Nuclide Amount

Waate Generator (Print Name Here)

No. Volume-f13

I I I I •

Amount Surface (mr/hr)

1 Meter (mr/hr)

11. Additional Description of Packaging and Packaging Materlall

SS Materials Write~Off

C =curie) M =gram

Error on

Amount

APPROVALS

± Amount Determined By:

( A = analysis ) M = measurement E = estimate

Account

HSE-1/-10/-11 Area Representative (Print Name Here) Additional Slgnaturea (Optional)

Signature certifies that waste package or s ipment is safe to handle and transport. (Signatur!)

15. ShaH Sur1ace Dose

Pes. mr/hr

Received £&

Logbook ~

Date Date

~-(- 9 D ~-} - 1 c_;

Project

Code

Verified

Date

I

Los Alamos Los Alamos National Laboratory Los Alamos, New Mexico 87545


1. Form Number

6. Waste Description


7. Numbers of Waste Packages Card- Drums

Plastic Board

4. Origin of Waste

Grou TA

8. Gross Volume Wooden Crates

F = foot3 Bags Boxes No. Gal. No. Volume-ft3 Amount

{M = meter3)

G =gallon

I I I I 4 1 I 4 I 1 J I I t ~,5io,o ~


Ext. 6095, MS J592

5. Waste Code

9. Package Radiation at

Surface 1 Meter (mr/hr) (mr/hr)

~ lcP·


2. Date

MMDDYY

0



7. Numbers of Waste Packages

RADIOACTIVE SOLID WASTE DISPOSAL RECORD

NOTE: Read instructions on back carefully before completing this form.

4. Origin of Waste

Grou TA

L-\GK-1


Ext. 6095, MS J592

8. Gross Volume 9. Package Radiation at Card- Drums Wooden Crates {M = meter3)

Plastic Board F = foot3 Surface 1 Meter Bags Boxes No. Gal. No. Volume-tt3 Amount G =gallon (mr/hr) (mr/hr)

I ~~o f :-;

I I l J I I I I 4 I I I + " . l I I I I I I I 10. Gross Weight 11. Additional Description of Packaging and Packaging Materials

(K = kilogram ) P =pound

Amount T = ton

~,, -

Los Alamos los Alamos National laboratory los Alamos, New Mexico 87545


NOTE: Read instructions on back carefully before completing this form. 1. Form Number



7. Numbers of Waste Packages

Card- Drums Plastic Board

4. Origin of Waste

Grou

8. Gross Volume Wooden Crates

Bags Boxes No. Gal. No. Volume-ft3 (M = meter3) F = foot3

Amount G = gallon

l J I I I I I I I I I •


Ext. 6095 MS J592

5. Waste Code

9. Package Radiation at

Surface (mr/hr)

1 Meter (mr /hr)

10. Gross Weight 11. Additional Description of Packaging and Packaging Materials

{K = kilogram ) P = ~ound

Amount T = on I I I I I I I I I I I I I I I I I I I I I I I I I I I ·- :" ..

=?I olo ~0 p ',' '· 12. Radlonucllde Content SS Materials Write,Qff

I Amount Determined By: ltc =curie) Error on

( A = analysis ) Project Nuclide Amount ±I 1

,M =gram Amount ±I M = measurement Account E = estimate Code

PI e_IB I I • I I E I -~·: ' + I I E I , .. , ~:

I




NOTE: Read instructions on back carefully before completing this form.

4. Origin of Waste

Grou TA Buildin


Ext. 6095, MS J592

5. Waste Code

, •. w .. te Demlpllon

XI 1Rit91YI lf"I!ILIA lll1IE1!v't7J 7. Numbers of Waste Packages 8. Grou Volume 9. Package Radiation at

Card- .....,_ .. ~- Wooden Crates (M = meter3) Plastic Board



1. Form Number

. Oate

MMDDYY

I'· Woote De•c•pllon


7. Numbers ol Waste Packages

4. Origin ol Waste

Grou TA Buildin

Card- Drums Wooden Crates Plastic Board Bags Boxes No. Gal. No. Volume-ft3

l I ~ J l I 13 58 I I I I t

12. Radlonucllde Content

Nuclide Amount

Waate Generator (Print Name Here)

And Signature certifies that the aste is as represented here and that ALL applicable acceptance and disposal/ storage criteria have been met. rs·gnature)

=curie) =gram

Error on

Amount

APPROVALS HSE-1/·10/·11 Area Repreaentallve (Print Name Here)

Signature certifies that waste package or shipment is safe to hand/ and transport. (Sig:atu~

- - ;Y 52>'-; __ _ a-~~ tY'--c:r-

LOS ALAMOS NATIONAL LABORATORY ~··· RSWD

I, ... --··- ·-·· .... L L93000309

RADIOACTIVE SOLID WASTE DISPOSAL (RSWD) RECORD APPLICATION FOR STORAGE/DISPOSAL

Date

)- /7- c;J Group

Jll1- G Technical Area.

1 ? Building

& Return Mail Stop

c 12 0

INSTRUCTIONS

1. Read and follow detailed instructions on last page.

2. For further assistance contact your Waste Management Coordinator.

3. Send completed form to "LLW Reviewer," EM-7, MS J595, for approval.

-, · .. ' Form 1354 (5/92) ·

~: .. ;:

--· -.'

RSWD 1. Waste Originator lnfonnatlon

L93etetet3et9

. aste 2 W Ch aracterlzatlon and Packa! Ina lnfonnatlon Waste Profile I

1517 ~10 Hazardous Materials Waste Code ~ctual Rad 0 Mixed Waste Transfer Form H M No. 0 i 3 () 7 1~15" Request No. I 0Suspect Rad 0Non-~

Total Waste Volume lJj; Meter&: Estimated Weight OKilograms Serial No.

1 I 15.0 fC Feet3 ~ tU10 0 •d ~ounds

Is this a dumpster? DYes }!QNo

If yes, 0 Compactible 0 Non-Compactible 0Gallons OTons

"' Dumpster No. I I

Waste Description ---1 i ('" I ' A) C., J?r\ / A.J J s 7)// /}i/1 (- "\ I

0Rhlr ~~~ C & D Form Numbers

II Radiation Exposure Rate • I I I I I I I I I I I I I I I I I I I I OmR/hr I I I I I I I I I I I I I I I I I I Comments

Package Cod•" Package Package Volume Volume Number of ~otal Vol. of Package Type Volume Volu,.,. 01 ·Bulk lunpackaged) Code' (Individual Package) Units•• Packag• (Pkg. Vol. X No. of Pkg ... ) Unita- unu---02 • Wooden crate ()I I I I f). (l fl/1 I d I I I I ~~· 0 jl/j

M.Met.,.3

,. ~-Drum

I I I I • I I I I I • F. F..c3 • Cardboard box G • Gellona '-" rt!' I I I I • I I I I I • ~ 05 • Plastic bag 06 • Steel box I I I I • I I I I I • 07 • Shield cask I I I I • I I I I I • 08 • Other 1 speedy below) I I I I • I I I I I • Radio nuclide Amount Units+ Uncertainty Method++ SS Acct. Proj. Code

I 1a1318"1LA

.....,

LOS ALAMOS EM-8 USE ONLY WASTE PROFILE FORM Reference Numoer Los Alamos National Laboratory

Los Alamos, New Mexico 87545 0 c:::- -:::;. ? ;:;--~ _> I '-"t_....

Complete boltl sides of this form using a black or blue pen_ Incomplete forms will be rejected. Send form to ATIN: WPF MS K 500 ppm 0 Liquid D > 200' 04 Not aqueous 0 Sulfides 0None 0 Gas cylinder or vessel .~ Not ignitable 0 Shock sensitive 0 Multilayered 0 Class A or 8 explosive 0 Suspended solids .....- 0' Nonreactive 0 Powder or ash

Waste OriQinatlon Radioactivity

A. Is ltlis waste generated in 8 radiation controlled area? 0 Yes ~ No 0 Nonradioactive lo Suspect %Radioactive Actl"'f)' .... ~ R..:lotion Type Haf't-Hte B. If yes. is ltle waste gen8f"!lted or aa::umulated in 8 property @ ~2.0 nC/g 0 alpha

~8 defined. registered radoactive materials management I-~ < 20 yr area (RMMA)? (RMMA • ) 0 Yes I)J. No tJ > 2.0 nCtg 0 beta t"~ !:_ 20 yr

C. If A is yes and you have determined ltlat your wasta is nonradioactive, provide 0 > 10.0 nCtg !X( gamma JUStification in ltle additional comments section on ltle reverse side of ltlis form. 0 > 100 nC/g 0 tritium

WASTE GENERATOR CERTIFICA noN: Based on my knowledge of the waste and/or chemJcal!physical analysis, I C8rTify that the mforma11on on this form is coaect. 1 undersrBnd that this information will be made available to regulatory agencies and that there are significant penalties lor submining false information. including the possibility of fines and imprisonment for knowing violations.

Wa~:;tcner

'""' A-54 AREA G I

...

LLW DISPOSAL CHECKLIST

EM7-RAD-F0013 Revision 1

September 17, 1992

RSWD Number q 5 0()0 .:S CJ 7 Driverw N111n111 Group & TA Arrival Date & Time l Die~aal Data & Time JU·~'-I.i C.t~lley~$ PJ-~ '{A-3 tj ..S-;g.- tj .l 2.'ff yZD-93

TruckiD No. of RSWDe Comment•

g;;L /:2 8 I /lt!t WEnlf ?

' ~. 'rJ~·/18/93 11:59 '6'5056655355 PATS

sENT gy;Xerox.Tet~r.opiP.r ?0~0 : 5-18-83 :11:3?AN ; ., laJ 002

505 6f5 52&0:~ 2

. -·-LOS· ALAMOS NATIONAL LABORATORY

RADIOACTIVE MATERIALS TRANSFER

J

No. ct Proper Ship pine Name !~em ~~-A ~ n~~ ..

ruc.r~

Hazard Cbu UttrNA Quantity Numbw l~ .... -)

' 1Th12':11' n/a. ~Form Chtomk:al Foml ~vlr1 l..al:>ol C:o~ .. 2j9 U (D~pl~ted) :ELEMENTAL 2uCl/gU~ n/a

...

~s H&rT.Uvel Weight (Swi~)

DOr o.· USNRC ldrooll~IWn NtJmber n/.a

Addilional C!EoY..riplion (&) FTTil)Jn P{)j_M l F.bx Hi

Z Numb4ir Data ~000. . ,_ /_ lbe. (J .Hq~ RadioaJwm:y F1e!>poro~~ ~08 Numt&r($) J.~J:ES C. UNG 75507 1'1-6 1.-6~Sl namA ., 62 ~rwull .,

!liW'& b If

Fonn 1~ (2./93]

~5/Utl/~3 11:34 ·. PATS

"1> >·::~.

til".·

HlALTH HUARDJ Rodiondive moteriol; de9ree of ho ircn~poflinfj. If th~rt> i~ no injury, remove and i~olo!e ,;u•peo:t~ contonuuueed clorhln51 enJ

shoe:;; o~•i$1 per~on 1o •!-.ower with ;,. no inj

~hoes; =~i6t ~ Avlhoriiy of a

Advis-e medical 1 mo1eriol.

.... , ...

17-MAY-93 RSWD# L93000309

PREAPPROVAL CLASSIFICATION SUMMARY

CLASSIFICATION SUMMARY .~ . ) TRU/LLW

NRC Class

Tritium Disposal:

DOT Type

LSA

WEIGHT AND VOLUME

Weight

{/(. OOE+03

.

.

Unit

RADIONUCLIDE INFORMATION

Nuclide Amount

/u23a ~. SOOE-09

u

SUPPORTING VALUES

Sum Adjusted Alpha (nCi/gm): 1.65E-06

GTCC Fraction 0

Sum Tritium (Ci/m3) 0

Sum Ci/A2 0

Sum Fissile (FGE) 0

Fissile Concen. (FGE/1) 0

INPUT DATA

Volume Unit

~·OOE+OO ~-

Unit Error Activated Metal

~c l.OOE+Ol

17-MAY-93 RSWD# L93000309

PREAPPROVAL CLASSIFICATION SUMMARY ADDITIONAL-INFORMATION

D WEIGHT AND VOLUMES:

Page 2

Load Weight (grams): 2.72E+06 Load Volume (m3): S.OOE+OO

INDIVIDUAL RADIONUCLIDE CLASSIFICATION:

Nuclide GFC LSA DOT Type NRC Class TRU/LLW

U238 2 ? ? N . LLW

INDIVIDUAL RADIONUCLIDE QUANTITIES:

Nuclide Total Adjusted Alpha Adjusted Total Grams Fissile Curies Total nCi/g Alpha nCi/g Grams Curies nCi/g ------- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - --U238 4.50E-09 4.50E-09 1. 65E- 06 1.65E-06 1.65E-06 1.34E-02 0

RSWD APPROVAL CHECKLIST


September 17, 1992

:equired Documentation: 1. RSWD (Form 1354) 2. WPF

Approval Criteria:

RSWD NUMBER: LY 'J;Q(X_) 3QC?J Date Entered into Database: 5- 17- Cr3

I. gJ No outstanding nonconformances

II. WPF ~ Reference number assigned by EM-8 ~ Signed by EM-8 reviewer '!)Ia Approval less than one year old unless extended by EM-8 li(J No EPA Codes indicated if for disposal 11Q Physical and chemical description meets storage/disposal WAC ~- Waste is radioactive (except Be, PCBs, or special waste) J1. Any changes on form seem appropriate and are initialed or signed by EM-8 ~Copy of WPF is in generator file

Ill. RSWD

~ Waste originator information block complete and matches WPF Enter Generator Number, Waste Stream Number, and WMC Number; check Lotus list and assign old or new numbers as needed

WPF number entry matches number on WPF Waste code is entered and appears appropriate from waste description Waste code descriptor box checked and matches WPF Load volume and weight fields complete and appear appropriate Dumpster information completed, if appropriate Waste description is complete and matches waste described on WPF Package information entered clearly and correctly; volume agrees with volume listed in load volume field

~- No drums in dumpsters ·'QJ For boxes over 50 ft3 , checklist completed and signed by EM-7 g) Radionuclide information identified and entered correctly -~· Generator signing certification statement same as on WPF. If not, call and verify that

the person is an authorized generator. If so, add to Lotus list. ';gJ WMC signed certification statement ~ Screening program run and signed printout attached to RSWD if "actual" waste E All information considered, waste meets storage/disposal WAC ~ Sign and date EM-7 approval block

~ Based on information provided, check appropriate waste disposition Affix three bar code labels to form in indicated positions Enter RSWD number, generator, and approval date in logbook

~ Time stamp form and return to mail stop on cover of RSWD or return to walk-in customer

~ If problems discovered and form not approved, copy transmittal letter and Page 1 of RSWD (with reasons for disapproval) and put in notebook

1;l Copy of Page 1 of RSWD attached to checklist li'f Any changes are initialed or signed .ZQ

Disposition: iJ!' Approved 0 Disapproved Approver Signatureu,_{['S=: 25

I

i I I I l I l I I I I I I I I I I I I I I j I I I I

l©~ A~~unru©~ los Alamos National laboratory los Alamos. New Mexico 87545

RADWASTE SCALE RECEIPT Weste Menegement

TA-54 Aree G

Tlf-3/ !l1~ ~5/1 .5.o ~ 3 =F~p~~

Time Date Vehicle ld. No.

Tare lbs.

RSWD No.

Dumpster No.

Form 14 78 (6/91) RSWD ATTACHMENT

Gross lbs.

rhis Page For EM-7 Use Only

Disposition

0MAP Shaft

0Be Shaft 0PCB Shaft

4. EM-7 A

D MW Storage Shaft OOther

D Low-Level H3 Shaft D High-Level H3 Shaft 0Animal Tissue Shaft 0MFP Shaft

D HEPA Filter Shaft

D Source Shaft D Powder Shaft D Holding Shed 0MWH3Sh&d ocompactor

5. R I I S ece v ng_ ite Information Date Wast& (MM,DD,YY) Received 01511 18'19 s - Vehicle Code Actual Volume I ,_, ~elejs ~ster (01) I I 0 Feet ump truck (02) 0 Gallons Gross Weight (lbs) 12 I 613 J o 1 o t

D Flatbed (03) D Pickup (04)

Tare Weight (·) ].2]4181° ,o. 0 Shield cask (05) 0EM-7truck (06) Net Weight

I 11 t>' I e: I () t D Other (specify below) (07) N~mber of j9>_WDs on this load I

~

RSWD

Date Approved

5-(r-li~

LOS ALAMOS RSWD NATIONAL LABORATORY

L94000084

t.J.n-..~ .... .....


Date

/-2(.)- c;y Group

J )(-I/ Technical Area

/J-Building 183

-Return Mail Stop

r'?'7'Z-

INSTRUCTIONS




Form 1354 (5/92)

r RSWD 1. Waste Originator lnfonnatlon

1 .. L94000084

Waste Profile Request No.

0Gallons

2. Hazardous Materials/Cf""l. Transfer Form ~ No. () !SJ'3

Estimated Weight 0 Kilograms Serial No. 0Pounds

0 [i]Tons

0 Mixed Waste 0Non-Rad

Is this a dumpster? Yes No

If yes, 0 Compactible 0 Non-Compactible Dumpster No.

'

Radiation Exposure Rate IOR!hr ~~~ C & 0 Form Numbers

. I I I I !DmR/h~ L...---1--L-.......L.....---'-----1 ~~--~~--~~--~~~, ~--~--~~--~~

Comments

Package Cod•" 01 • Bulk (unpackaged)

02 · Wooden aale

03· Drum

• Cardboard box

116 • Plastic bag

06-Steelbox

07 • ShiH! caak

08 • OthM (~below)

Package Code•

Package Volume (Individual Package)

Volume Units••

Number of Packeg ..

otal Vol. of Package Type Volume (Pkg. Vol. X No. of Pkg•.) Unit."

6

Radio nuclide Amount Units+ Uncertainty Method++ SS Acct.

E +I- +I- o/o

E +I- +I- o/o

E +1- +I- o/o

E +1- +1- o/o

E +1- +1- o/o

E +1- +1- o/o

E +1- +I- o/o

E +1- +I- %

++Methods: A,., Analysis M ,., Measurement C: Calculation E,., Estimation


Volu,. UnU-

G • Gallons

Proj. Code

'

GENERA lOR CE.RTIACA TIOH SlA TEMEHl: My aignat.,. certifoeo tlwt the -· io M deocribed '-e end on the en.ched w .. w Profile ~form. w .. te -• 811 ~lc.ble Keep-end otor.ge or dlopo ... crfterie llotBd In Achinlatretive Requi......,..t 10-2, ""low·l.av.l Rac:loecliw Solid w .. a, • end In "W- Acc:epl8ncll CriWria lor low·l.av.l R.dloectiw W- 018pOMI .. TA-54, ...,_ G.•

"' ~ory;a~ Print) : Waste Management Coordin

•

RSWD APPROVAL CHECKLIST.


September 17, 1992

equired Documentation: RSWD NUMBER: ( g '-fcx:::c::o 6£./-1. RSWD (Form 1354)

Date Entered into Database: OJ- ~-q tf 2. WPF Approval Criteria:

I. IS No outstanding nonconformances

II. WPF

Ill. RSWD

Reference number assigned by EM-8 Signed by EM-8 reviewer Approval less than one year old unless extended by EM-8 No EPA Codes indicated if for disposal Physical and chemical description meets storage/disposal WAC Waste is radioactive (except Be, PCBs, or special waste) Any changes on form seem appropriate and are initialed or signed by EM-8 Copy of WPF is in generator file

Waste originator information block complete and matches WPF Enter Generator Number, Waste Stream Number, and WMC Number; check Lotus list and assign old or new numbers as needed

WPF number entry matches number on WPF Waste code is entered and appears appropriate from waste description Waste code descriptor box checked and matches WPF Load volume and weight fields complete and appear appropriate Dumpster information completed, if appropriate Waste description is complete and matches waste described on WPF Package information entered clearly and correctly; volume agrees with volume listed in load volume field

No drums in dumpsters For boxes over 50 ft3 , checklist completed and signed by EM-7 Radionuclide information identified and entered correctly Generator signing certification statement same as on WPF. If not, call and verify that the person is an authorized generator. If so, add to Lotus list.

WMC signed certification statement Screening program run and signed printout attached to RSWD if "actual" waste All information considered, waste meets storage/disposal WAC Sign and date EM-7 approval block Based on information provided, check appropriate waste disposition Affix three bar code labels to form in indicated positions Enter RSWD number, generator, and approval date in logbook Time stamp form and return to mail stop on cover of RSWD or return to walk-in customer If problems discovered and form not approved, copy transmittal letter and RSWD (with reasons for disapproval) and put in notebook

Copy of Page 1 of RSWD attached to checklist Any changes are initialed or signed

Page 1 of

Disposition: Itt Approved o Disapproved Approver Signature: -+-o+~--·+}4"'--~-=----~---b'-~----

LLW DISPOSAL CHECKUST

EM7 -RAD-F0013 Revision 3

Ma.n:::n 2, • 1 9 94

RSWD 10 INo. oJSWDs Drivers Name rrTMII Date & Time Paperworx Staneo Data & Time 1foooo8Cj 4~~ /l~ud« /0·1?-9~ 9.'~Y /C-1·7-9~ /O:s:r

Group & TA Dumpster No. TruCK aD IReaay to Dispose Date & Time IDisposaJ Date & Time

]) .X -II IP-I_s-" 5~"9:2 j/)-1·?- /y //.' 0)- !C-/)·9t'( /I.' tJ.r.. IV

GY'CLw 0 PCBs 0 Beryllium 0 Asbestos 0 Other: FORMS SCALE~

a---Jruck was weighed (bulk loads only) e--10 on slip matches 10 on truck

WASTE;J?ROFILE FOAM (WPF} ~No RCRA hazard codes listed ~dioactive and low-level waste boxes checked

RADIOAJ;TJVE SOLID WASTE DISPOSAL REQUEST (RSWO) a--~rm is approved and signed by the Approval Office ~Description does not describe liquids. gases. or powders except when a notation is

Jl made by the Approval Office that the waste meets the WAC ~1- g C&O forms present and matches those listed on RSWO

11~ 13 If "actual" is indicated. signed screening program printout is attached and indicates I -level, not TAU or GTCC. Printout corresponds to RSWO.

H-1 surveyed load and signed form .< ver signed form

DUMPSTERS :::8--Aif observable waste is packaged or wrapped ,.a-Waste appears to meet WAC ~drums -a--f'ilo gas cylinders ..a-No- oil soaked boxes

--ErObservable boxes labeled ...g.-compactible/Non-Compactible a-tsA

..a-compactible/non-compactible not apparently mixed in dumpster umpster locked properiy

TR~-5'"" _Waste is containerized or wrapped in plastic Gr"'W~--trppears to meet WAC

B No gas cylinders ~if soaked boxes TRANSPOATAllON (Contact ESH-7 if any o1 these items is not correct)

B,..,TF . ~~8 If no AMTF present, a completed Excepted Package form or a Non-Radioactive

sjlitement Is present . ~~ved by BUS-6, Packaging & Transportation ~umber of packages same on RMTF(s), RSWO(s) and vehicle (not applicable to

bulk waste) 4 8 !f number of packages on any RMTF is greater than 1, completed continuation sheet ts present

PACKA~ cr ~ch package is marked and labeled correctfy (See Proper Shipping Name) e-fntegrity of the packaging is intact

VEHIC~ ~ehlde is property placarded.

POST-DISPOSAL ACTIVmES

#J# 12- C&O forms stamped and signea #;:.~- ia l~cestos. ~opy of RSWD sent to Dave Ja

rdine

B~ecord data 1n logbookS/computer

a-Transit loa sheet completed

1-vlj~B Fill dirt fo;m comp1etea. ifw} priate / _/] ~ '7

CST-7 Receiving Technician: ( /L/.,~~*

Verified by: CA-L I I-J -Cf4-Comments:

.-.. -.:-~.... . ... ~ ~·: ~:t~;.~;\; ··:;.:.-. ·: . ~-.~~~~~~!,- ':.L..C;_;,,,,

~!C~·::·/ .. . -!r. ....... ~· .. ·:· ~-

•. ~-::;j{·~ ,- - .·--:-~


o Tare VVeight Needed

No. of RSVVOSj

I

Driver's Narre

RSV\0 Number 1 .

L ?fL/ODD 0 oV I

Comments:

.RADWASTE SCALE RECEIPT

Vehicle ld. No. Tare lbs. ' .. ,:~ -.

Estimated Weight

I {J I () -~ifl_S

Waste Management TA 54 Area G

Time

' '·.:. '· . -· ... : ~ -r---

Date Gross lbs.

: ·.· i -:.- Net tbs,'. '· ,,

:; .. : .• . -~~- . . ·- ..

Converted Weight (lbs)

Total~-~--------------~

TO: MS{) 91..\tJ FRCM: Michelle Cash, EM-8, MS K490, 5-0223

SUBJECT: EXTENSION/RENEWAL OF WASTE PROFILE REQUEST FORM

This is in response to the Waste Profile Extension/Renewal Questionnaire. According to the questionnaire your waste stream has not changed from the criginal WPRF #~qy3 . This notice allows you to continue to use the above mentioned WPF number for another year or until your waste stream changes or the generator changes, and at that time a new WPF must be submitted to reflect the change. Please notify your group waste coordinator of this extension for the above WPF. Please attach this validation to the above mentioned WPF and keep it in your files for future use. If you have any questions, please give me a call.

cc: Group Waste Coordinator, MS

"

1

~0....)

7 ~~~

2. I rtlf I..IIMI TIWIIflll'l

1 ~,~,~;A.:.r,.,• H"r'""''i.J~.S,.,;~~~;" AJJ?~or,Y 1'-/.~.S. --~--------~----T-----~~.w~~~~~ cn.vwr .,...

~t~!A .N/A o.,; I ·~ ...

~002

_, __ .. · ,; 1"1 j I 9 3 • 0 9 : 5 6 'Q' 50 5 6 6 S 5 J ~ 5

RADIOACTIVE LSA FORM

Exclusive use vehicle will be loaded by the consignor, unloaded by the consignee

_.,lnd no other m·aterial will be carried in/on the cargo carrying body. Material is not to be transferred to another cargo carrying body unless directed by consignor, consignee or his authorized agent

PT-1 e.o t6/93>

·. ... .. . . ~ . . .· ... . "''. . ~-·

IIIAUII IIASAI •• ~cdiooctive mcteuai; degree of hctora wtll vort from littte to moderate.

oepenO•nt on ""o• ana Quantttv oi roo•ool:'•ve rnoter.al. Man' of thete mcnertalt mov not nave rcc•oaet••• mctet~olt labels. Some roo•oon•v• moter~ott cannot be aetenea o, common&, ovo•loble

nttrumenU. S~ull_. rodiooct••• motenalt utuotlw ••II be v•t•ltle ,f coclaottn9 fa;.la. Qunotf from fire control ot dilutton •ater mo' caute oo•lut•on.

fill 01 UPLOIIOII ~cme oi thne mcner.oia ma, burn. but none of them •gntt" reodtlw. '

Hsr-e uae ON\..,

WASTE PROFILE REQUEST I Reierei'ICe Numcer I tJ2CfL/3

- -~mplete bcnh sidu of thla fonD using • btKk 01 blue J*t~ Inadequate information. wilt result in procau&ng defay1. completed form to: Al'TJ~k ~. MS K~

/ Division/GfOUIIt I ~-

gt(Mowfectge o1 Procna 0 MSOS An.c:hed

Room

I 0 ChernQUPttysical ANivsea I Specify Below• o~~-,_A~ 0 A~e Anached Choose one or more of the itema below which best ducribea your waster

OF!~ 0 Combuetible QHign~ QOxidiz• 0P'(rOJ)~ QCyanide 0Heevv Meut QCorroeiw

0,.".,.. 0~ QA.o.toe QSo!Wfll QW-A~

oar ..... QPintnv Solu~ Q!tct..·

0 Ptlotoqrephio QSanitarv 0 Aediocherri.UV QPeimW..-0 Labornory Tr_.. 0~ 0Screp Meat·

0~

QSpencC.... QA.,...C.. 0,.....01 QPurt-.oa oc. I• a& ouu~ ...... os~ o~

QAe.tioe 0 Filter ,.... 0 Vecuum Filter Sludge Qc.n-.Pene 0 Non-S.tvege .Ole QNon.R~ 0 lluilclne Cebria ~SheCebri•

l

I ~·-d-di_ti_o"_·~· _o_~ __ "p_o_o_n_co~.p-u-·o-~--------------------------------------------------------------~----~] i General Description Of Waate (check at least one block for each columnn· I

i !

'· ~ld 0 Cemented Sludge 0 Semi·Solid/Siudoe--0 Abeorced Liquid (JUquid

OG•• O Multi-laver 0 Suspended Solid• O Powder or Aeh

FlASH POINT ("F)

OL• .. Than 100 0100to 138

O 140 to 200 QGre~er Then 200

~ne

lndica1e Known Radioactivity Of Your Waste 0Not Redioectiw (Go To Neld S.Odont

~.OnC/g 0 >2.0 nC/g 0 > 10.0 nC/g 0 > 100.0 nC/t

GENERATOR CERTlFJCATIOrt

pH

Q2.0orl._,

Q2.1 to 12.4

PCS.

O 1 2.! or Greeter i3'6t A~ceole

QUIW• tl,p ·'· 0 Reeca wtdl w.,..,_ · QCy•lid-·· .. 0 s utftdeeo.· QShocaSeueid~

QOaMAotl~ !]Mift"~~ ..

Qsoo.,...: ~Pea.-

Uat Known Radioisotopes: 0 O.terrniiiM 8y A-.y

~,» RldloiMtope 1 :..· --~~:..---- AC1Nhy1Unlt"ol ,.._.,._. ______ _

Fl~ 2. Ao1fWty,\Jnlt ef .......... ------------- -----------RidloiMtope 3;..• ------ ActNftyiUntt ef ......_ _____ _

lltediGteotope 4 AethityiUrft of MM~urw',.;;.:'---------

SuHI upon my knowl«ige ol,. .,....,., ~t~dlor clw'ltic~.J ~. I c~ m.t rM -"~ ~ r.ga ... til~~,. ~•cili•d on • .,,s 1 'orm ~ r:orr.ct. 1 und.ntMHJ th.t,. inlonn.tion will b•,.... ~ 10 ~torr _,.,o. _.. ,._,..,.. .. ~ ~ lw subm''''"'; I 'alse inform.tion. includinf til• poaibi6,., of fin• end impriMHtmenl 1M knotfllling vioMtlon&

~rint r:enerator'a Neme llut. Fim Ml)

ur Grouo'a Wnta Coordinator i1 the eustodien of your wnte TltJnegement doc:wnentltion. provide the neme end mailllot' of thi• Jtrson loptio~t.

=onn 1J4e (4/J1J

Z Number I

Oate

Pt::rr.ta tverse ':i ~'!

j Heavy M~ (indicate whettler tne follow.ng neavy metals ex1st 1n vcur waste, at tne ocsted ccncentratiOnl:

None KO~ Analv.• iCl.P Other

A,...,.. c:]' C < S.O ppm C ~ 5.0 ::om CJ 0 >0 0 a.num [3"' D < 1 00.0 ppm O ~ 1 00.0 ppm 0 0 >0 0

CaQnwurn 0 8'< 1.0 PP"' 0~ 1·0 ppm 0 0 >0 0 Chromiur!t f D < !.0 PD'ft 0 ~ !.0 ppm ODD D >0 CJ Lud 8'< !.0 PP"" 0 ~ 5.0 Pom D >0 O Mercury D

This Page For EM-7 Use Only

Disposition

0MAP Shalt

0Be Shalt

0PCB Shalt D MW Storage Shalt 00iher

Date Waste Received

Actual Volume

Gross Weight (lbs)

Tare Weight (-)

Net Weight

Bale No. Compaction Date

I (MM,DD,YY) .I I .I

I I I I

Storage Date

(MM,DD,YY)

I

I Area

G-

Area

D Low-Level H3 Shalt D High-Level H3 Shalt D Animal Tissue Shalt 0MFPShalt

D Source Shalt D Powder Shaft D Holding Shed 0MWH3Shed

ocompactor D HEPA Filter Shalt

5. Recelvln Site Information

6. c Bale Volume (M;.:~)

Vehicle Code

I:JDum~1) ~p truck (02) D Flatbed (03) 0Pickup (04)

D Shield cask (05) OEM-7 truck (06)

D Other (specify below) (07)

ompaction Information Comments

7. D1s osallocat1on lnformatron

L94000084

~LLWPit 0Asbestos Pit

0 MW Storage Dome D Certifiable TAU Dome D Uncertified TAU Storage

Treatment Code

Ocompaction (01) D Incineration (02)

I:Jolher~ ~(04)

mR!hr

mR!hr

Non-Conformance Report No.

.

Shaft Pit Transit Sequence No. Post(s) Layer Position

3'1 I w B. Stora e Location Information

Shaft Building Column Layer Row Pod Post(s) Layer Position

Date

/0-/?~Y.

Page 2

LCS'ALAMOS RSWD NATIONAL LABORATORY

L94000407

RADIOACTIVE SOLID WASTE DISPOSAL (RSWD) RECORD

APPLICATION FOR STORAGE/DISPOSAL

Date

Group

CST 13 Technical Area

5~

Return Mail Stop

Hcto '

INSTRUCTIONS




Form 1354 (5/92)

l

,

L94000407

2 • Waste Characterization and Packa! lng Information Waste Profile I Hazardous Materials

Wastj

(;//"-... t

POST-DISPOSAL ACTIVmES . lJ;tAc&o forms stamped and signed I"/ A If asbestos, copy of RSWD sent to Dave Jardine

,J tr c::r-Becord data in logbooks/computer GY'"Transit Jog sheet completed

rJ j!J~ Fill dirt form completed, if appropriate .--CST-7 Receiving Technician: C..J4-4eLES 4, Unt-MrJrJ vR Verified by:

Comments:

t ~-

I I

-..


D Tare \/Veight Needed

No. or RSV\O's

5 Dufll)Ster No. . f

/-

. ~ 14 -·JUN- 94 RSWD# L94000407

.. PREAPPROVAL CLASSIFICATION SUMMARY

CLASSIFICATION SUMMARY

TRU/LLW

NRC Class

Tritium Disposa

DOT Type

LSA

~I ~/

WEIGHT AND VOLUME

Weight Unit

/s~ ;;~:;~ ;-;--


Nuclide Amount ~;-----

~OOOE-05

SUPPORTING VALUES

Sum Adjusted Alpha (nCi/gm) : 0

GTCC Fraction 0

Sum Tritium (Ci/m3) 7.06E-04

Sum Ci/A2 4.00E-08

Sum Fissile (FGE) 0

Fissile Concen. (FGE/1) 0

INPUT DATA

Volume Unit . _/ ____ _ \..-1. OOE+OO

Unit Error Activated Metal ~--

c 0

dW

' ' . : "' 14 -·JUN- 94 RSWD# L94000407 PREAPPROVAL CLASSIFICATION SUMMARY

ADDITIONAL INFORMATION

.tu:AD WEIGHT AND VOLUMES:

Page 2

Load Weight (grams): 2.27E+04 Load Volume (m3): 5.66E-02


Nuclide GFC LSA DOT Type NRC Class TRU/LLW

H3 8 y A N ?


Nuclide Total Adjusted Alpha Adjusted Total Grams Fissile Curies Total nCi/g Alpha nCi/g Grams Curies nCi/g

------- -------- -------- -------- -------- -------- -------- --------H3 4.00E-05 0 0 0 1.76E+00 4.14E-09 0

o~"'~r l, ~ /4-~-Cz Lf

8;26/94 10:39 'a'505 665 5290

SEN! BY:Xcrox Tclccopicr 7020 : 6-26-94 PATS

10=04 5056654925-~003

5056655355:# 2

LOS ALAMOS RADIOACTIVE MATERIALS TRANSFER e NA TlONAL LA BORA TORY

~."" N&me

F Bern adtftl P INI'III T TOIII'_~'ord

R rA I!Uiidil'IQ Ro~ 0 [T•~Ilcnt Group TA e~ikllne Aoom

0 T11tphooe ~~roup · M 117-!HI .AOi _,M !3 3

~1 CST-7 "' a. 113 ~.Of Proper ShlpplnC Name Hruld Clan

UNINA Quantity

Item PI

'·•

RSWD APPROVAL CHECKLIST


September 17, 1992

~equired Documentation: RSWD NUMBER: --'=Lqc.!.-IJ...::.....:CCO~:::..t.fV.!...--..'7...!..,___ ____ _ 1 . RSWD (Form 1354) 2. WPF Date Entered into Database: /..;-11

----~------~---Approval Criteria:

I. )a No outstanding nonconformances

II. WPF Reference number assigned by EM-8 Signed by EM-8 reviewer Approval less than one year old unless extended by EM-8 No EPA Codes indicated if for disposal Physical and chemical description meets storage/disposal WAC Waste is radioactive (except Be, PCBs, or special waste) Any changes on form seem appropriate and are initialed or signed by EM-8 Copy of WPF is in generator file

Waste originator information block complete and matches WPF Enter Generator Number, Waste Stream Number, and WMC Number; check Lotus list and assign old or new numbers as needed

WPF number entry matches number on WPF Waste code is entered and appears appropriate fro!ll waste description Waste code descriptor box checked and matches WPF Load volume and weight fields complete and appear appropriate Dumpster information completed, if appropriate Waste description is c·omplete and matches waste described on WPF Package information entered clearly and correctly; volume agrees with volume listed in load volume field

No drums in dumpsters For boxes over 50 fe, checklist completed and signed by EM-7 b Radionuclide information identified and entered correctly

lp Generator signing certification statement same as on WPF. If not, call and verify that 1 the person is an authorized generator. If so, add to Lotus list. !D WMC signed certification statement \.D Screening program run and signed printout attached to RSWD if "actual" waste iD All information considered, waste meets storage/disposal WAC I=J Sign and date EM-7 approval block p Bas·ed on information provided, check appropriate waste disposition 1D Affix three par code labels to form in indicated positions r0 Enter RSWD number, generator, and approval date in logbook

~ Time stamp form and return to mail stop on cover of RSWD or return to walk-in customer

d If problems discovered and form not approved, copy transmittal letter and Page 1 of RSWD (with reasons for disapproval) and put in notebook

I Copy of Page 1 of RSWD attached to checklist

0 Any changes are initialed or signed ~

Disposition: c;{App~oved D Disapproved Approver Signature: ~~e-=--·-·------------

~ALAMOS EM-8 USE ONL:( Los Alamos National Laboratory WASTE PROFILE FORM Referena3 Number Los Alamos, New Mexico 87545

~~-\\I-S . Cmplete both 5ides of this form using a black or blue pen. Incomplete forms Wlll be reJected. c:::c C::. ' ,-?

·,·'··-· ·.

Send form to ATIN: WPF MS K490.

Division/Group Telephone Mail Stop Technical Area Building Room

esT- L3 rJ- 17d31 1-i 6::J L/ I ill-53 /f)PF-.5 -Sc.t-:;4~~¥ aJ Method of ~ Knowledge of Proa3ss (KOP) [J ChamicaJ!PhysicaJ Analysis (specify below) Characterization 0 MSDS attached (optional) -OR- 0 Request for analysis IJJ Analysis attached Waste Category (Choose one or more of the etegories below that most accurately descnbe your waste)

0 Flammable D Combustible 0 High explosive D DOT oxidizer 0 Pyrophoric 0 Cyanide O Heavy metal 0 Crrosive

Waste Description

Form

0 Solid 0 ~misolidlsludge t8J Absorbed liquid ~ Uquid 0 Gas cylinder or vessel 0 Multilayered 0 Suspended solids 0 Powder or ash

Waste Origination

0 Pesticide 0 Beryllium 0 Asbestos 0 Solvent 0 Waste rags 0 Glass 0 Plating solution 0 Etchant

lgnitability (f)

0 < 10CP 0 100° to 13 2.0 nC/g 0 > 10.0 nC/g 0 > 100 nC/g

RocJiotlon Type •

Toxic P.~tals (Indicate If each of the following heavy metals exists in your waste at the posted concentratlons)

arsenic 0 None 0 < 5.0 ppm 0 ~ 5.0 ppm 0 TCLP 0 Other barium [}] None 0 < 100.0 ppm 0 _:: 100.0 ppm [J TCLP 0 Other

0 0 0 TCL? 0 --------cadmium None 1.0 ppm ?. 1.0 ppm Other

0 0 0 TCLP 0 ------chromium None < 5.0 ppm .:: 5.0 ppm Other lead None 0 < 5.0 ppm 0 ?. 5.0 ppm 0 TCLP 0 Other mercury None 0 < 0.2 ppm 0 ?. 0.2 ppm 0 TCLP 0 Other niCl-trlchlorophenol None 0 < 400.0 ppm 0 .?. 400.0 ppm 0 TCLP 0 Other 2,4 .6-lrlchlorophenol ID None 0 < 2.0 ppm 0 .?. 2.0 ppm 0 TCLP 0 Other vinyl chloride GJ None 0 < 0.2 ppm 0 .?. 0.2 ppm 0 TCLP 0 Other

Hazardou• Constituents (ldfNltify hazardous constitufNlts for F- 8Jl0. K-list&d wastes and substances causing waste to exhibit a characteristic)

Additional Commenta (Provid6 comments ff!gBrding the chemical or radiological natuff! of the waste)

Waste Classification

0 Non-RCRA waste

0 PCB 0 non-PCB TSCA waste .0 asbestos

RCRA Code 1 RCRA Code 2

EM·B Re~iewe(s Signature

I ,-..

Fonm 1346 (6!92)

Do not write in this box - EM-8 use only

., 0 RCRA-regulated solid waste 0 RCRA·regulated hazardous waste,''f] Radioactive only

0 municipal refuse 0 nonhazardous chemical waste 0 administratively controlled waste 0 sanitary/mdustrial sludges

0 hazardous waste 0 mixed low-level waste 0 mixed tr-~nsuranic waste

RCRA Code 3 RCRA Code 4 RCRA Code 5 RCRA Code 6

~ .... ,'[] low-level waste 0 transuranic waste

RCRA Code 7 RCRA Code 8.

Date Cost Center/Program Code lor Analysis Reference Number

Page 2 ol2

WATER SAMPLE RESULTS RECORD AREA 53 BUILDING_3::___-,--ROOM .5"" ;u, "'c. rol (r'h ~ ... To.rc;d /h.cu~) w CONTROl NUMBER

ofi" (s cPl·

SAMPLE DATE 3 I;;; /q f TAKEN BY ;?J. );:;n.n.-;J·

~AMPLE LOCATION SYSTEM Jl. !/ , ALPHA BETA TRITIUM NUMBER EQUIPMENT TAKEN FROM /,/"' uCi/1 uCi/1 uCi/1

I

Cjf/-o3-P £ IH'( j-6 II.( Co/ fr-otv\ ~ TT4 A lcov--> cJ., /} ~..-7771- - /} Jc ~ v

:Los Alamos NATIONAL LABORATORY

memorandum Health & Safety Division ESH- 4 Hr,.lth Physics M~"surrmrnts

An•lytlc•llabor•rorles Section

TaiMS.·

Analyst:

Reviewer.

Phone/FAX:

Symbol:

Date:

Scott Walker, ESU-1, MS 11815 -~

John 0. Lucero, ESH-4, MS G75?-}f'

Magdalena M. Vigil, ESft-4, MS G757

5-8888/5-6071 (1\f''-\)

ESH-4-AL-REP-041

March 9, 1994

ANALYSIS REPORTS FOR SAMPLES SUBMilTED TO THE HEALTH PHYSICS

ANALYTICAL LABORATORY FROM TA-53, LAMPF

The following samples were submit1ed to ESH-4's HPAL from TA-53, LAMPF, for

analysis. The reponed activities, in J-1Ci, are the total activities on the samples and are

decay corrected to the stop date and time indicated. The samples were analyzed utilizing a

HpGe detector and ADCAM Multi-Channel Analyzer.

The analysis results are shown in the table below:

Sam pi~ Rdu-cncr CoUKil'CI

ld M D•lr Timr

ETHYL GLYCOL 9401P 3/2194 1~00

ETHYL GLYCOL 9402P 312/94 1~00

1\'DA = No Dt.1ect.able Activity

JOL mmv

Cy: J E. Salazar, ESH-1, MS H815 S. L Simmonds, ESH-1, MS H815

File

Analyu.t n.~r Timr

3nl94 0940

3n/94 1013

Art.ivity 2s

Nuclidt{s) ()10) ("/o}

NDA

NDA

-1 June 1994

Michelle Cash, ESH-8, MS-K498

From: W. A. Teasdale, P-3, MS-0442

Subject: Waste Profile Forms for Disposal of D-38, Thorium, Neptunium.

Attached are two completed ''Waste Profile Forms". I understand from personnel at CST-7 that I need to submit these to you for approval before I can send the items listed to them for disposal. If there is any additional information that you require, please let me know, I will get it to you as soon as possible.

There are two forms because the uranium and thorium are designated RSWD, while the neptunium is designated TRU waste. I ~nderstand that I need the reference number from the top R/H corner of the Waste Profile Form in order to complete the proper RSWD and TRU Waste paperwork.

When you get this, I would appreciate some communication from you regarding the assigned reference numbers, and about how long the approval process will take. I can be reached at MS-0442, Phone 7-4506, or E-mail [email protected].

Thanks.

EM-7 ~pprover's Name (

.J · M itJ-faJ ~ Disposition

0MAP Shaft

OBe Shaft

0PCB Shaft 0 MW Storage Shaft

OOther

Date Waste Received

Actual Volume

Gross Weight (lbs)

Tare Weight (·)

Bale No. Compaction Date

(MM,DD,YY)

I I I I

I I l I Disposal Date

(MM,DD,YY)

Clct lol \ I Cil4-

1 I I I I

I,

L94000407

4. EM-7 A

I

I

Area

Gr

0 Low-Level H3 Shaft

0 High-Level H3 Shaft

0Animal Tissue Shaft

0MFP Shaft

0 Source Shaft

0 Powder Shaft 0 Holding Shed 0MWH3 Shed

ocompactor 0 HEPA Filter Shaft

5. Recelvin Site Information

6 c Bale Volume (M"')

Vehicle Code

~pster (Olf#-1'/ 0 Dump truck (02) 0 Flatbed (03) 0Pickup (04) 0 Shield cask (05) 0EM-7truck (06) 0 Other (specify below) (07)

ompact1on I f n ormat on Comments

7. Disposal Location Information

Date Approved

(o-l4-Cf4

(.81LLW Pit 0Asbestos Pit

0 MW Storage Dome 0 Certifiable TAU Dome 0 Uncertified TAU Storage

Treatment Code

Ocompaction (01)

0 Incineration (02)

Qo~(o3) L....l:::tfrone (04)

'2. mR!hr

"2. mR!hr

Non-Conformance Report No.

. Shaft Pit Transit Sequence No. Post(s) Layer Position

39 oqo~ Cflfo 1 ! IO_d._111 I e:. I I I

TJ::-»-7 {)CJ()_ ~ ..,... .... torage Location Information Storage Date Area Shaft Building Column Layer Row P:ld Post(s) Layer Position (MM,DD,YY)

I I I I I I I I I I I I I I I I

9. Director of Dispos_AI Operations ,........_ / DIRECTOR OF DISPOSAL OPERATIONS CERTIACATION: My oignature certilieo that all waote rec~ngjt rage,f4'or d~ rfquire# were ..,l

Dire{ljJI Disposal or 2\ragLperations (Prin~ A I21..ES . El-l~ lHJ 12..

'Signature lUU JL';;ft~ i I Date 8'-?o-Cf4-Screened Paperwork 10. Data Management Information • ')4L S-3>-94- Date Entered in Logbook Date Entered in Database Oat Entry Verified .ial) (MM,DD,YY)

I~ I QjT·oj~q fV 01 q(t·tr·3l q, 1f Supervised Disposal o A I o I Co I q » (!~ 9-J-ql.J.- InC! Lnf lnrual A)t-; ) \ Initial ~ {lntttal) .4· M~

Pa~ '-/'

LOS ALAMOS NATIONAL LABORATORY RSWD II'

L94000596 j


Date

10 A.J.j cs 9~ Group

P-.3 Technical Area-

TA·3

Building

SM-a;.o

Return Mail Stop

't>L\'-t~

INSTRUCTIONS

1.. Read and follow detailed instructions on last page.


3. Send completed form to "LLW Reviewer," EM-7, MS JS95, for approval.

Form 1354 (5/92) ·

r , ---- -·- .... . .. ':::;:> !:1.1?. ............ - •• - 1. Waste Originator Information

L94000596

Waste Profile Request No.

Group P-a

2. Waste Characterization and P Hazardous Materials ~ -o-t Transfer Form HM No. t:' .J. /) •

Estimated Weight

~Actual Rad Osuspect Rad

0 Mixed Waste 0Non-Rad

Is this a dumpster? Yes No

If yes, 0 Com~actible 0 Non-Compactible Dumpster No.

Waste Description WASTe CONSI SlS OJ: (2.) PACKA.GES. TH6 S:IRST l S li.. ~Tea P~IJIJT C~ W~lC~ COtJT~UJ5 (~)0.,~8 MeT~L PA~S ~ l\ KG EACH. THE: SECof.JO \SA CA.RDBO~RO 60X cct-JT"'IJ.JIJ-JG

(t) THORIUa-.1 METAL RING @> o KG.

Package Codee •

01 ·Bulk (unpackaged)

02 ·Wooden crate

03· Drum

Cardboard box ,lia

05 • Plastic bag

06 · Steel box

07 • Sl>eld cask

08 • Other (specify below ) ST L P AIJ.JT CAN

Package Package Volume Code' (Individual Package)

0 '3 0 '2

C & D Form Numbers

Volume Number of otal Vol. of Package Type Unite•• Packages (Pkg. Vol. X No. of Pkgs. )

F I=

Units+ Uncertainty Method++

a..l M +I· 0/o E. 3 M +I- % E.

+I- %

+I· %

+I- %

+1- 0/o

+I- %

+I- 0/o

++Methods: A= Analysis M =Measurement C =Calculation E = Estimation


Volume Volume Units" Unita-

M • Meters3

F • Feec3

G • Gallono

SS AccL Proj. Code

12o 3?.3 \~0 ~23

GENERATOR CERTIACATION STATEMENT: My .;gna~ure certifoeo that the -II! io M deocribed here end on the enached Waoto Profile Recp.atet form. Waote n>Mio ellepplic:eble loCCepiBoce end otorage or diapoaal criteria llotld In Aaniniotnttive Requiren.nt10.2, "low·level Racioec1ive Solid w .. a,· end In -w- Acc:epiBoce c:rt1eN lor low·leWII R.doectiw W•to 01~-.« T~ ~1.~G.· ator's Name (Pn"nt)

).w'H.J..IAM A.. 'TEAS t:> A.LEz WASTE MANAGEMENT COORDINATOR STATEMENT: My .;gnaturo

Waste Management Coordinator's Name (Pn"nt) EDWARD e.. Q.o Blt-.3$0~

Z Number

82.8"77 Date

8-\0 -~'4-

Z Number .J I

EM7 -AAD-F0013 Rewuon3

Marcn 21. i 994

LLW DISPOSAL CHECKUST

RSWO 10 No. or RSWOs IOrtvera Name. ~~Amval Date & Time re.perworx Staneo Date & Time Cj ~I} d(J 5"'1~ I .)~-Jd /Jl/]~y~.- ;o-;f-i¥ /.'¥(: /v-/f-7y I:S?

Group & TA

P-3 111-3 I Ou~psrer No. rruCK 10

/72~1 IReacry ro Olspoae Date & Time

/t~l!-·7-r 2,·;o rlsposw Cate & Time ltJ-tK-i.y :J.'~tJ. ~

~W D PCBs 0 Beryilium D Asbestos D Oth~r:.:

FORMS SCALE SUP / I ~ck was weighed (bulk loads only) 1/£ £ D.s ·f4 J"'-{_ v.., 1- · 13"10 on slip matches ID on truck ....,--/q--/1.....( vJ .1- /2-~-'"--1~: /•:-l 4.- .f- 2 .'t:-tr-

' WAST§!ROFILE FORM (WPF) s--· No ACAA hazard codes listed l:rAadioactive and low-level waste boxes checked

RADIOACTIVE SOLID WASTE DISPOSAL REQUEST (ASWD) ~rm is approved and signed by the Approval Office !2r'"Description does not describe liquids, gases. or powaers except when a notation is

made by the Approval Office that the waste meets the WAC ;/ ~ 13 C&O forms present and matches those listed on ASWD

[3-1J"iactual• is indicated, signed screening program printout is attached and indicates I -level, not TAU or GTCC. Printout corresponds to RSWD.

H-1 surveyed load and signed form < ver signed form

DUMPSTERS ..a-All observable waste is packaged or wrapped __a--waste appears to meet WAC

-Q-No drums ·-B-Ne--gas cylinders ._-8--()bservable boxes labeled

i3-No oil soaked boxes

..a-compactible/Non-Compactible -e-csA -a--compactible/non-compactible not apparently mixed in dumpster a-Dumpster locked properly

TR S er--w;;ste is containerized or wrapped in plastic a-'WSste appears to meet WAC

e-f\lCgas cylinders ~soaked boxes TRANSPORTATION (Contact ESH-7 if any o1 these items is not correct)

RMTF . ~~ 9 If no RMTF present. a completed Excepted Package form or a Non-Radioactive

§tatement Is present . ~ARproved by BUS-6, Packaging & Transportation ~mber of packages same on AMTF(s), RSWO(s) and vehicle (not applicable to . bulk waste)

( @ If number of packages on any AMTF is greater than 1, completed continuation sheet · is present PACKA9.E_

a--Each package is marked and labeled correctly (See Proper Shipping Name) £Z'Integrity of the packaging is intact

VEHICw- . Et"Vehlde is property placarded. .. ~ : .~ .

.'3

POST-DISPOSAL ACTIVITIES

t/ fr 8 C&D forms stamped and signea ;Jf#- a ~oestos. copy of RSWD sent to Dave Jardine r 13"Record data in iogbookSJcomputer

g.-jfansit log sheet compieted

Jlk & Fill dirt form completed, if aopropriate CST-7 Receiving Technician:

Verified by: QAL.. 1)-J-94

Comments:

. · .. -.~::-~· . .. .

~~ .. ~~f~~~$~;: :~~-- ·: ~ ... · -~ ...: ... __ ., ..

~-~':".~ . . ~ t:~-- :. -_ : .•• ;;i· ,:;> .

. -- ... ~-~~-::..;;": ·\' :."" .. · .. : . - ... · .. - ·)··"'!


o Tare VVeight Needed

No. of RSV\Os

I DurJ1)Stecg___

Driver's Name I

Q ((u lc! ' /f'. RS\1\tD Number

t-44000S{10

Comments:

RADWASTE SCALE RECEIPT

Vehicle ld. No.

Waste Management TA 54 Area G

lime Date

Tare lbs. ~ } () {o'f{()

' ·;:: /; .· 1 C• .·' 1 ::· • ·:.r 4 ----"'---'.':....;,;,: :.::..... [__;~· c;?"Q

Gross lbs.

Net Lbs.

J

goJJ?s

Estimated Weight Converted Weight (lbs)

3lo-0

Total LI _________ ___J

RSWD

........ ·- .. AUG 25'94 11:24 No.OOS P.02 LoS-ALAMOS NATIONAL .LABORATORY

RADIOACTjVE MATERIALS TRANSFER 8 RM No. 082.0:7 SM No. Coat Code Pro;. Code/Cost AcoWVk Pkg O.te

BK03 X Sk 9 ~ Cj ~ ? '/ 9ENERAL INSTRUCTIONS: This form Is an official shipping document for transporting radioactive material within LANL boundaries. Type or print all entries. Emergency Response Guide Information must be attached to this document. Distribution of com feted forms Is Indicated below.

~~~~~~--------~----~------~--~T Bullc:llng Room 0

33Kg.

lCIIonucllde& Tn232

3 Sm40 Shipping Name

Radioactive Material, lew apeclflc activity, n.o.B.

DO~ or USNRC

0.? Radioactive

Phyalcal Form

Solid

Ch•mlcal Form

Elam•ntal

11'\mJJuorlHI Descrip!lon{a) RSWD# l94000!PS

ActiVIty

1S.9mCI

Packeglng Ulled Packaged By

STP

Chemical Form Acllvlly

0.33 mCI

Packaged By

Building

Huard Clasa

7 UN:2912 IJ'k .· Lebel Ce!egory

NA

Z Number Dale

Hazard Claaa

7

label Category

NA

Z Number Date

~esponse Guirlebook Number(s) 6:2

ItemS 62

ADDITIONAL TRANSPORTATION INFORMATION

Date , _ /O -/i -ry

HEAlTH HAZARDS

Rodiolion presenh minimal risk to lives of persons during tran

sportation

accidents. low rodiolion ho1ord when ma

terial is intide container. If material it releo1ed

from po often do not hove 'RADIOACT

IVE' lobelt.

Occo•ionolly. pockogu may hove a 'RA010ACT1VE' label and o

second

hazard label; usually the •econd hazard i• greater than the radiati

on

hazard. Some radioactive materials cann

ot be detected by commonly available

instruments.

Spilled radioactive material• uwolly will be visible if packaging

foils.

Runoff from control of cargo lire may cou1e low-level pollution.

FIRE OR EXPLOSION

Some of these materiol1. may burn. but most do not ignite read

ily.

Radioactivity doe• not change flommobility or other properties o

f the

materials.

EMERGENCY ACTION

Priority response octlons moy be performed before

toklng

rodlotlon measurements.

Priorities ore life saving, control of fire ond other

ho:.ords,

ond first old.

I-solate hazard OTeo and deny entry. Notify Rod;otion Autho

rity of occident

condition1.

Keep unnece,ory people ol least 150 feel upwind of spill; greater

di,tonce•

may be nece,.ory lor people downwind, or if odvi•ed by Radiat

ion

Authority_ Uninjured persons or equipmen

t with suspected contamination should be

detcined or i~oloted; delay cleanup until instructions are rece

ived from

Radiation Authority.

Po1.itive pre1.sure 1-elf.contoined breathing opparolu1. lSCBA) a

nd structural

firefighters' protective clothing w;ll provide odequole protec

tion.

CAll Emergency Re•ponse Telephone Number on Sh

ipping

Poper flr•t. If Shipping Paper not ovolloble c>r no on

•wer,

CAll CHEMTREC AT 1-800-424-9300.

If water potlulion occurs, notify the appropriate authorities.

fIRE Do not move damaged packag

es; ~:~ove undamaged pac"-oges ou1 of fire zone.

Smoll Fires: Dry chemical, C02, water spray or regular loom

.

Lorge Flre1: Water spray, log or regular loom.

SPILL OR LEAK Do not touch domoged co

ntainer• or 1pllled moterlol.

Smoll liquid Splll1: Cover with •and, earth or other noncom

bustible

absorbent molerial.

Dike to collect large liquid spills or cargo fire control woier.

Cover powder spill with pla\tic sheet or lorp to minimize \pr~~

?ading.

FIRST AID U1.e first aid treatment accordi

ng to the nature of the injury.

If per1.ons hove contacted released material. use standard ho

zmar procedures

for core of con1ominoted per1.ons. for transport of the injure

d, and for

notifications to authorities.

&rJ:o *~~- (/k_kr1~/ • ~ • ~ ., ••• "' • • ·--~-

1': •

16-AUG-94

ORAD CLASSIFICATION SUMMARY

CLASSIFICATION SUMMARY

TRU/LLW

NRC Class

-~ c7 No

Tritium Disposal:

DOT Type A

LSA 0

WEIGHT AND VOLUME

Weight Unit

3.60E+01 K


Nuclide

D38 TH232

SUPPORTING VALUES

Sum Adjusted Alpha (nCi/gm) : 0

GTCC Fraction

Sum Tritium (Ci/m3)

Sum Ci/A2

Sum Fissile (FGE)

Fissile Concen. (FGE/1)

INPUT DATA

Unit

M M

Volume

S.OOE-01

Error

0 0

0

0

1.62E-09

0

0

Unit

F

Activated Metal

16-ADG-94 Page 2

ADDITIONAL INFORMATION

n WEIGHT AND VOLUMES:

Load Weight (grams): 3.60E+04


Nuclide

D38 TH232

GFC

4 4

LSA

y y

DOT Type

A A


Nuclide Total Adjusted Alpha Adjusted Curies Total nCi/g Alpha

Curies nCi/g -------- -------- --------

D38 0 4.42E+02 0 TH232 0 9.08E+00 0

-

Load Volume (m3): 1.42E-02

NRC Class

N N

Total nCi/g

--------4.42E+02 9.08E+00

TRU/LLW

Grams

--------3.30E+04 3.00E+03

LLW LLW

Fissile Grams

--------0 0

I •

RADIOACTIVE LSA FORM

Exclusive use vehicle will be . loaded by the consignor, unloaded by the consignee and no other material will be

. carried in/on the cargo carrying body. Material is not to be transferred to another cargo carrying body unless directed by consignor, consignee or his authorized agent.

PT-18.0 (6/93)

Los Alamos NATIONAL LABORATORY

memorandum NUCLEAR MATERIALS AND RECONFJGURA TION TECHNOLOGY PROGRAM {NMRT) Mail Stop E524

TolfvfS: William A. Teasdale, P-3, 0442

FrorrVMS: Audrey Martinez, NMRT/NMM, E524~ Phone/FAX: 5-8999/5-8997

Symbol: NMRT/NMM:94-110

Date: August 1, 1994

SUBJECT: AUTHORIZATION TO DISCARD DEPLETED URANIUM, NEPTUNIUM, AND THORIUM

Attached is the memorandum received from DOE/AL, dated July 26, 1994, for authorization to discard the items noted in your June 8, 1994 request.

Please follow and observe all applicable laws, regulations and waste management procedures for discard of these items. ·

Contact John Cullinan, OS-2, (7-5886) prior to proceeding with discard of these items so that MC&A requirements can be addressed.

If you have any questions or ifl can of further assistance, call me at 5-7333.

AM:spg

Att: Memorandum to T.J. Trapp, from A.E. Whiteman, dated July 26, 1994. Subject: Nuclear Material Discard Authorization

cc: T.J. Trapp, NMRT, w/o., att, MS A 102 J. Cullinan, FSS-12, w/att, MS E508 J. Moses, P-3, w/o att., MS D449 Author File NMRT INMM File

lA.Jt ~ 1 .,,c;,.o ... .1# .• • -~

United States Government Department of Energy

~~emorandum Albuquerque Field Office

DATE:

REPLY TO ATINOF:

SUBJECT:

WQD:CAC

Nuclear Material Discard Authorizations ~·

ro: G.~i;.:r;; Trapp, Program Manager, ~T, LANL·'

f-3

This correspondence is provided in response to the two July 5, 1994 letters from Ms. Audrey Martinez to Mr. Corey cruz regarding the discard of several enriched uranium, depleted uranium, neptunium, and thorium items at LANL. Based upon discussion with your staff and the Lead Field Offices for these materials, the following authorizations and guidance are provided:

LANL is authorized to discard 25 kg of depleted uranium (material type 12) from Project A-GB-0103-011 and 137.2 kg of depleted uranium (89 kg of material type 12, 48.2 kg of material type 11) from Project E-GB-0103-812 in the form of partially oxidized impure metal, specification alloy parts, and impure metal with multiple alloys. The basis for this authorization is that the materials require immediate action due to their oxidation, the fact that they cannot be processed for recovery on site and the determination that it is not cost-effective to ship them off-site for recovery.

6 ...U. T-u..~.(~

LANL is authorized to discard 33 kg of high purity machined depleted uranium metal parts (material type 12) from Project A-GB-0103-011. The basis for this authorization is that the material is of no further use to this or any other LANL project and that it is not cost-effective to reprocess this material for other uses. This material was discussed with Mr. Thomas Wynn, OR (the lead office for uranium), and he concurs with the proposal to discard this material.

(·.~·H-i

~· ._:( ~u--c~·_.__~

LANL is authorized to discard 2 grams of enriched uranium impure metal (material type 35) from Project E-GB-0103-812. The basis for this authorization is that LANL cannot process this material on site and it is not cost effective to ship this material to Y-12 for recovery. Mr. Wynn concurs with the proposal to discard this material.

f>-3

T. J. Trapp -2-

LANL is authorized to discard 2 grams of impure neptunium metal (material type 82) deposited on aluminum foil from Project A-GB-0103-011. It is not cost-effective to process this material for recovery. This material was discussed with Mr. Nazir Khalil, SR (the lead office for neptunium), and he concurs with the proposal to discard this material.

LANL is authorized to discard 3 grams of neptunium scrap (material type 82) from Project A-GB-0103-011. It is not cost-effective to process this material for recovery. Mr. Khalil concurs with the proposal to discard this material.

~ ~~ ~n.~~Lt.k

LANL is authorized to discard 3 kg of high purity thorium metal in a ring used to fabricate a thorium filter from Project A-GB-0103-011. The basis for this authorization is that this material is not needed to support programmatic objectives. Mr. Wynn concurs with the proposal to discard this material.

Should you have any questions regarding these authorizations, please contact Mr. cruz of my staff on FTS (505) 845-4282.

cc: J. Newton, DP-22, HQ T. Wynn, OR N. Khalil, SR E. Bean, LAAO B. Barrett, SWEC, AL J. Baca, WQD, AL

"~ Director Weapons Quality Division

8 June 1994

o: Audrey Martinez, NM/RT, MS E524

From: W. A. Teasdale, P-3, MS D442

Subject: DISPOSAL OF NUCLEAR MATERIAL INVENTORY IN P-3 MBA ACCOUNT #120.

r Audrey, The following is a list of accountable SNM (Special Nuclear Materials) parts that are owned by P-3, have been designated NO DEFINED USE (NDU), and need to be discarded (or transferred if you can find anyone who can use them). These parts reside in P-3 Account 120, and are presently stored in the HS~4 radioactive materials vault (SM-40, W133, designated as P-3 location code AF). Per our conversation last week, please make the arrangements necessary to allow us to discard this material properly.

---I. MATERIAL TYPE 12, Depleted Uranium (U238) ·--

1. LOT ID #P3D38-1; 11kg 2. LOT ID #P3D38-2; 11kg 3. LOT ID #P3D38-3; 11kg

---=:::::---- -_____-· These are all machined metal parts, each weighing approx 11.5 kg. Each

·~em is wrapped in a zip-lock bag, so packaged weight for these is also .... 5 kg each.

----... ---~ ·---II. MATERIAL TYPE 82, Neptunium (237)

1. LOT ID #74-NP-1,2; 2g ... These are components fabricated from material that appears to have been around P3 since 1972, and consists of

f two (2) cardboard containers, each wrapped & sealed inside a plastic bag. ) The first contains 1.4 gram of Np deposited on a piece of aluminum foil 5" \ x 25" in size. Packaged weight of this container is 182 grams. The second

contains 0.8 gram of Np deposited on several smaller pieces of aluminum i -foil.-Packaged weight of this container is 100 grams. +----- -j 2. LOT ID #75-NP2372; 3g ... This is material that was split off from 1 LOT ID 75-C-237 in 1979, appears to be scrap from processing of some kind.

It is packaged in plastic containers, inside a sealed glass jar, which is, in turn, presently packaged in a metal can. The plastic containers have not been opened for more detailed examination because of the distinct possibility of contamination inside the jar. The packaged weight of this item, including the metal can, is 187 grams .

----··- ·---. ··-·· ... :. ~~ .. ;;..:.::.: .... :~ . . :·. -;::::::-::.::~.:- ----· -- ....... ·-- ... ---- ... ··-·-. ····· ~-. -----=-:--·--·~~---.............·· ~--·-- ·-·--

~ ;~ ---------

II. MATERIAL TYPE 88, Thorium - - -------~------- .

1. LOT ID #WH314/MC; 3kg

This is a thorium metal ring, 9.00" o.d. x 6.00 i.d. x .50 11 thick. It is scrap material that remained after fabrication of a thorium filter for use at WNR when P-17 was part of P-3. It is wrapped in plastic bubble-wrap, so packaged weight is also 3 kg.

Thanks for your willingness to take on this project. Once these items have been discarded, we will be able to close account 120, and be out of the accountable nuclear material business at TA-3. If I can be of further assistance, let me know!

Thanks,

Teasdale

Distribution: John Moses, P-3, MS 0429 Audrey Ulibarri, P-3, MS 0429 John Cullinan, FSS/OS-2, MS E508

' . .. !

FROM: Michelle Cash, ESH-8, MS K498, 5-0223

SUBJECT: WASTE PROFILE FORM (WPF)

The ESH-8 Hazardous and Solid Waste Section has reviewed and logged the information you provided on the attached WPF(s). Basec! on the information you provided, your waste(s) is:

A. Non-RCRA waste

0 PCB 0 non-PCB TSCA waste

0 Asbestos

B. RCRA-Regulated solid waste (non-hazardous)

0 Municipal refuse 0 Non-hazardous chemical waste

0 Administratively controlled waste 0 Sanitary /industrial sludges

C. RCRA-Regulated Hazardous or Mixed Waste

0 Hazardous waste 0 Mixed low-level

0 Mixed transuranic waste

D. Radioactive Waste

Low-level waste 0 Transuranic waste

You a!e required to keep a copy of the WPF(s) in your files for at least 3 years. This WPF(s) is vaJid for one year or as long as the composition of the waste you have characterized remains the same and the generator remains the same. Should your waste or generator change, submit a new WPF to ESH-8 and attach a copy of the WPF which is being replaced.

Attachment(s)

• See Reverse Side for Handling Instruction

4-

INSTRUCTIONS FOR HANDLING YOUR WASTE

A. Non-RCRA Waste

Polychlorin11ted Biphenyls (PCB)

Wastes containin~ greater than 50 parts per million PCB are subject to the Toxic Substance Cont

hwbdocuments.env.nm.gov alamos national labs/ta 54/11758.pdfv~aiamos natio~~ l boratory solid waste...

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