+5056060864 T-782 POOI F-443Jan-1S-Z00e 0425pm From-EP TA21

-TA21 CLOSURE PROJECT

lOS ALAMOS NATIONAL LABORATORY MAIL STOP C 349

231-0727 FAX 606-1526

DATE -$ - 0 ~

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F-443 +5056060864 T-78Z P002Jan-15-2008 0425pm From-EP TAZl ~

DP Site Aggregate Area Investigation Work Plan

CJ Structure Investigation area

bull Proposed sample location

reg Proposed boreholQ location

reg FreViQU5 borehole location

Road Pipeline (surveyed location)

Pipeline (engineering drawing location)

- Fence

10-11 contour

0 30 60

FEET 993 NAO t

Borehole 21middot01678 11

- -~-- --

ScmfQO GISL8Il M2tl12S7 amp M200881 Juno 2004 modmed lor F614middot3 DP Cleanup zilo 022805 ptm

Figure 514-3 SWMU 21-024(k) proposed sample locations

June 2005 88 ER2004-04D9

F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate

SAMPLE ID RE21-07-3893

ASfLANNED AIPLANNRD AS COLIReTED

J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA

rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy

~IKI]6~7

--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----

COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA

BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______

=L-2=--~__

PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN

2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED

Explosives list ~MBERGLASS ~ rIhln

Ice y JAMPfEDESC

b ro -r~Pf-

FIELD SCREENINGIlVIEASUREMENT RESULTS shy

pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID

RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~

-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime

(Printed Name)(Printed Name)

(Signature)Signature)) -

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Sample]]) RE21-07-3893

(Jie-nt Data

Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~

Analyle Cone (pglg) DL a

2378-TCDD ND 00757

1)378-PeCDD ND 0101

J)3478-HxCDD ND 0370

123678-HxCDD ND 0413

123789-HxCDD 0367

123467S-HpCDD 863

OCDD 52~1

237Jl-TCDF 0]54

12378-PeCDF ND 23478middotPeCDF ND

123478-HxCDF 0301

123678-HxCDF 0207

234678-HxCDF 0229

123789-HxCDF ND 0174

1234678-HpCDF 357

1234789-HpCDF ND 0286

OCDF amp80

Toblls

TolalTCDD ND 00757

TolaIPeCDD middotm 0118

Total HxCDD 254

Total HpCDD 159

Total TCDF 0)78

TotalPeCDF 0729 Total HxCDF 320

Iotal HpCDF 658 ~

Analysi RAS

Project 29211

SUD pTe Data

Matrix Soil Sample SUe 100 g Solids 995

EM PCb Qualifiers

J

J 0136

0128

J J j

0993

EPA Metbod 8290

UibonliOn Data

Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA

Labeled Standard R LCL-UCLd Oualifiers

IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135

13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135

I3C-12346 78-HpCDD 100 40 -135

13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135

13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135

13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135

13C-l23789-HxCDF 102 40- [35

13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135

CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data

TEQ(Min) 0309

II Sample spaific eslimated detalOO IUn ii

b EStirowted mruciIDWll possi hie oollCWlJati01l

( Melhod detalionlirniL

d WVIeT centroT limil- upper oontroJ limit

e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)

The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy

APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843

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F-443 +5056060864 T-78Z P002Jan-15-2008 0425pm From-EP TAZl ~

DP Site Aggregate Area Investigation Work Plan

CJ Structure Investigation area

bull Proposed sample location

reg Proposed boreholQ location

reg FreViQU5 borehole location

Road Pipeline (surveyed location)

Pipeline (engineering drawing location)

- Fence

10-11 contour

0 30 60

FEET 993 NAO t

Borehole 21middot01678 11

- -~-- --

ScmfQO GISL8Il M2tl12S7 amp M200881 Juno 2004 modmed lor F614middot3 DP Cleanup zilo 022805 ptm

Figure 514-3 SWMU 21-024(k) proposed sample locations

June 2005 88 ER2004-04D9

F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate

SAMPLE ID RE21-07-3893

ASfLANNED AIPLANNRD AS COLIReTED

J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA

rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy

~IKI]6~7

--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----

COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA

BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______

=L-2=--~__

PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN

2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED

Explosives list ~MBERGLASS ~ rIhln

Ice y JAMPfEDESC

b ro -r~Pf-

FIELD SCREENINGIlVIEASUREMENT RESULTS shy

pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID

RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~

-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime

(Printed Name)(Printed Name)

(Signature)Signature)) -

r--

l

Sample]]) RE21-07-3893

(Jie-nt Data

Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~

Analyle Cone (pglg) DL a

2378-TCDD ND 00757

1)378-PeCDD ND 0101

J)3478-HxCDD ND 0370

123678-HxCDD ND 0413

123789-HxCDD 0367

123467S-HpCDD 863

OCDD 52~1

237Jl-TCDF 0]54

12378-PeCDF ND 23478middotPeCDF ND

123478-HxCDF 0301

123678-HxCDF 0207

234678-HxCDF 0229

123789-HxCDF ND 0174

1234678-HpCDF 357

1234789-HpCDF ND 0286

OCDF amp80

Toblls

TolalTCDD ND 00757

TolaIPeCDD middotm 0118

Total HxCDD 254

Total HpCDD 159

Total TCDF 0)78

TotalPeCDF 0729 Total HxCDF 320

Iotal HpCDF 658 ~

Analysi RAS

Project 29211

SUD pTe Data

Matrix Soil Sample SUe 100 g Solids 995

EM PCb Qualifiers

J

J 0136

0128

J J j

0993

EPA Metbod 8290

UibonliOn Data

Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA

Labeled Standard R LCL-UCLd Oualifiers

IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135

13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135

I3C-12346 78-HpCDD 100 40 -135

13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135

13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135

13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135

13C-l23789-HxCDF 102 40- [35

13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135

CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data

TEQ(Min) 0309

II Sample spaific eslimated detalOO IUn ii

b EStirowted mruciIDWll possi hie oollCWlJati01l

( Melhod detalionlirniL

d WVIeT centroT limil- upper oontroJ limit

e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)

The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy

APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843

ltshy

i en

I rv lt=gt lt=gt CD

lt=gt ~

en T5 3

a 3 I

rn -0

-I po

+ UI lt=gt U1 0)

cgt 0)

cgt co agt ~

-I I-

co -0

cgt cgt ~

shycgt

I ~ ~

P3pounde 6 of25

F-443+5056060864 T-782 P003Jan-15-200B 04 25pm From-EP TA21 ~- lage 1 ot

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 134 EVENT NAME 21-024(k) Dp Aggregate

SAMPLE ID RE21-07-3893

ASfLANNED AIPLANNRD AS COLIReTED

J1PDATE COLLECTED(MMIDYYYy) M)J)[A ~ 0(11)1 OxIfTgt ~ ~~O=-h-~~~-------TlME COLLECTED (H1lMM) SOBmiddotMEDIA

rTct f shyPRS W SAMlLE ftea CODE ampa-- 7(7(07 1-1amp LoeATION 11) =L--~=-=-=---__ FIELD QC TYPE tvf- ) f LOCATlON TIPE GENERlq F~Ll)~fREP amp I TOP DEP1R f~IrII~Jj ----L~-~-- SAMPilEUSAGE lliL Jshy

~IKI]6~7

--------- shyBOTIOM nEPTH fIkrnb3 (07 SCREENiPORT DESC fif FIELDMA1rux ~~ B _____ EXCAVATED YESamp-N-A~---f-~------~----

COMPOSITll TYPE COMPOSITli TIME INTERVAL - WATER FLOWING YEStsectPNA

BOREHOLpound YESampNA BOREHOLED1lCL[NATION ___~__ BOREliOLEDlRECTION ______

=L-2=--~__

PRIORI1y ORDER CNTNR PRESERVATIVE COLLECTED SPECIAL INSTRUCTIONS YIN

2 8082 125 ML GLASS Ice y 2 8290 125 ML GLASS Ice ry I NMED

Explosives list ~MBERGLASS ~ rIhln

Ice y JAMPfEDESC

b ro -r~Pf-

FIELD SCREENINGIlVIEASUREMENT RESULTS shy

pro - 0 c 10 COU-E~D BY (P~ REVIEWED BY (PRINT) ~4-u 1 Jh-t- ~-( 6 bull ~~ 11 L ~ID

RECEIVED BYDateTime DatefTimeRELINQUISHED BY P107(Printed Name) 7110(printed Name) ~~

-(SIgnature) shy(Signature)~~ t)i16CXgt RECEIVED BYDatelTlmoHELINQUISHED BY DateTime

(Printed Name)(Printed Name)

(Signature)Signature)) -

r--

l

Sample]]) RE21-07-3893

(Jie-nt Data

Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~

Analyle Cone (pglg) DL a

2378-TCDD ND 00757

1)378-PeCDD ND 0101

J)3478-HxCDD ND 0370

123678-HxCDD ND 0413

123789-HxCDD 0367

123467S-HpCDD 863

OCDD 52~1

237Jl-TCDF 0]54

12378-PeCDF ND 23478middotPeCDF ND

123478-HxCDF 0301

123678-HxCDF 0207

234678-HxCDF 0229

123789-HxCDF ND 0174

1234678-HpCDF 357

1234789-HpCDF ND 0286

OCDF amp80

Toblls

TolalTCDD ND 00757

TolaIPeCDD middotm 0118

Total HxCDD 254

Total HpCDD 159

Total TCDF 0)78

TotalPeCDF 0729 Total HxCDF 320

Iotal HpCDF 658 ~

Analysi RAS

Project 29211

SUD pTe Data

Matrix Soil Sample SUe 100 g Solids 995

EM PCb Qualifiers

J

J 0136

0128

J J j

0993

EPA Metbod 8290

UibonliOn Data

Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA

Labeled Standard R LCL-UCLd Oualifiers

IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135

13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135

I3C-12346 78-HpCDD 100 40 -135

13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135

13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135

13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135

13C-l23789-HxCDF 102 40- [35

13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135

CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data

TEQ(Min) 0309

II Sample spaific eslimated detalOO IUn ii

b EStirowted mruciIDWll possi hie oollCWlJati01l

( Melhod detalionlirniL

d WVIeT centroT limil- upper oontroJ limit

e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)

The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy

APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843

ltshy

i en

I rv lt=gt lt=gt CD

lt=gt ~

en T5 3

a 3 I

rn -0

-I po

+ UI lt=gt U1 0)

cgt 0)

cgt co agt ~

-I I-

co -0

cgt cgt ~

shycgt

I ~ ~

P3pounde 6 of25

Sample]]) RE21-07-3893

(Jie-nt Data

Narue Los Alamos National Laboratory Prajcct 07-294C Dale Collected 17-Jul-07 Tirol Collecied 1415 ~

Analyle Cone (pglg) DL a

2378-TCDD ND 00757

1)378-PeCDD ND 0101

J)3478-HxCDD ND 0370

123678-HxCDD ND 0413

123789-HxCDD 0367

123467S-HpCDD 863

OCDD 52~1

237Jl-TCDF 0]54

12378-PeCDF ND 23478middotPeCDF ND

123478-HxCDF 0301

123678-HxCDF 0207

234678-HxCDF 0229

123789-HxCDF ND 0174

1234678-HpCDF 357

1234789-HpCDF ND 0286

OCDF amp80

Toblls

TolalTCDD ND 00757

TolaIPeCDD middotm 0118

Total HxCDD 254

Total HpCDD 159

Total TCDF 0)78

TotalPeCDF 0729 Total HxCDF 320

Iotal HpCDF 658 ~

Analysi RAS

Project 29211

SUD pTe Data

Matrix Soil Sample SUe 100 g Solids 995

EM PCb Qualifiers

J

J 0136

0128

J J j

0993

EPA Metbod 8290

UibonliOn Data

Lab Sample 29211~OOJ Date Reoeived 19-Jul)7 QC Bald N(l 9210 Date Extracted 25middotulmiddot07 Date A olllyzed DB-S Date Analyzed DJ322S27-Jul-07 NA

Labeled Standard R LCL-UCLd Oualifiers

IS J3C-2378-TCDD 101 40 - 135 13C-I 2378-PeCDD 108 40 - 135

13C-l2347S-HxCDD 109 40-135 BCmiddotl 2367amp-HxCDD 895 40 - 135

I3C-12346 78-HpCDD 100 40 -135

13C-OCDD 795 40middot135 13C-237-TCDF 980 40- 135 13C-1 237amp-PeCDF 106 40- 135

13C-23478-PeCDF 103 40 - 135 Be-123478-HxCDF 114 40 - 135

13C-l23678-HxCDF 892 40 - 135 13C-234678-HxCDF 961 40 - 135

13C-l23789-HxCDF 102 40- [35

13C-I 23467 8middotHpCDF 921 40 - 135 I3C -] 2347 89-HpCDF 110 40 - 135 13CmiddotOCDF 840 40 - 135

CRS 37Cl2378-TCDD 908 40-135 eToxic EquhalcDt Quotien1 (TE-Q) Data

TEQ(Min) 0309

II Sample spaific eslimated detalOO IUn ii

b EStirowted mruciIDWll possi hie oollCWlJati01l

( Melhod detalionlirniL

d WVIeT centroT limil- upper oontroJ limit

e TEQ based on (l989) lnfemal100al To~i1 EjuLAlenl Faclors (lTE)

The results are reported In dry weight The sample size is reported in e4 veiBJlt --- -- -shy

APPnJve1 B) WiHlam J Luksernburg Ol-Aug-20070843

ltshy

i en

I rv lt=gt lt=gt CD

lt=gt ~

en T5 3

a 3 I

rn -0

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cgt 0)

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co -0

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P3pounde 6 of25

F-443 Jan-15-200S 0426pm From-EP TA21 Iigt +5056060864 T-782 P00501S ~~v~~~~~~ ~N~ORHA-~~~wNO unauthorized reproduet1on witbout ~~en pe~io1on fr~ Gg~

1_-()~4tt) High Explosives Analysts Data Sheet

Lab Name General Engineering laboratories Client Sample ID RB21-07-3S93

Lab Code GEl GELJobNo(SDG) ~

Matrb ~ GEL Sample ID 189817001

Sample AIIlount 2 Molstue 2

Date Received 19middotJOL07Amount Vnlb S

Extract-bID Type Sonioation Extraction Bakh ID 653048

Copwf1Cl-atea Extract Volumt(mL) 12 Date Extracted 25JUL07

DllutllWlFactorr a InJ~ton Volume (uL) 50

Daee Analyzed02-AUG07 2023 GEL dUII file BXS080a0J16wiff

Untts ugkg______bull _____wow _______

r ----~ ( - Cas No 1 Compound QConcentration

TATB 1000 U3058-38-6 i 2ampDiamino-4-nitrotoluene 200059229-75-3 U

35-Dinitroaniline 1000 U~_ 618-8-1 24jDiamino6-nitrotoluene 2000 U 6629-29-4 tris(ocresyl) phosphate 1000 UCmiddot 78-30~8

I ~Coln~atmtion bull

llnSrrUlDtlt X ConcentrudExtract Volume x Dilution Vahtl Ie Amoun Factor

Page 2 of 2

Page 18 of329

Jan-15-Z00a 0426pm From-EP TAZl +5056060B64 T-7B2 P0060l3 F-443 _v~ ~MV~ middotU unu=aa roproaUat10Jl wlthout 1ft bull ~n pS1lll1allion flOlII GlBL

1 High Explosives Analysis Data Sheet

Lub Name General Engineerillg Laboratories Cllent Sample ID RE21-07-3893

Lab Code GEt GEL Job No (SDG) 07-293

Matrix ~ioIL GEL Sample ID 189817001

Sample AnDllDt a MoisCure ll

Date Received Amount llhl~ g

Extraction Batch ID 653048ExtradlonType ~tion

Coneentrlllted Rxtla~Hfolulne (mL) lQ Date Extracted 25middotJUL-07

DUatlon fictor ~ bUection Volumo (nL) ~

nte Analy2tdr 30-IDL-07 1916GEL dauHlile BXm130015a

Units ugkg

I

I

I

--UasNo 18-96-7

L21-14-2

111-82-4

U~06middot51middot0

~5e1-41-0

31572middot78middot2

9-45-8Ei6-0-2 nmiddotllmiddot5

bull li8middot7zZ 11-95-3

middot1J108-1

I 993$-4

1

~)j65-0

9~J99middot0 - shy -__--_-

C03J]ound 246middotTriIIlitrotoJuene

24-pidrotoluelle

aDX

4-Amino-2ampdinitrotoluene

aMX 2-Amino-4dinitrotoluene

retryl

26-DiDitrotoluene

mTN

o-Nilrololuene

Nitr~enzene

m-Nitratoluene

135-TriniCrobcnzene

m-Dinittobenzene

p-NirrorQuene

Concentration 500

500

500

500

SOO SOO SOO 500

1000

500

i 500

500

500

SOO soo

-~

U

U

U

U

U

U

u I

U -I U

U i

U i U

U

U

~J

Concentrwon =0

Instrument X Concentllllted Bxrract Volumll X Dilution Value Sam~e Amoun Factor

Page 1 of 2

Page 17 of 329

T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r

GEL lAboratQlies LLC Report Dllte AuguSll 2007

PCB Page 1 of 1 Certificate of Analysis

Sample Summary

SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL

Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll

Batch ID 653073 lrut ECD2A1 DIlution 1

Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW

014b140~d 2CLP2

CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI

12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336

11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336

1114l-16-) Atoclor-1232 U 336 lIglkg 112 336

53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336

12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336

1I097-6H Aroclor-12S4 J 120 lIgkg 112 336

11096-82-5 Aroclar-1260 U 336 uglkg 112 336

Page 208 of329

-----

~ 2 ~ o lt0

f

o (N

~ ltll

g 01

-~ - --~

11gt319

21-353 21-485 J I Investigation area

~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I

f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)

J I I

_I I I J

I J J shylI

I -~

-

cJ Slructu ra

l- I Former slructure

Jilvestigalion area

bull Proposed sample toeation

reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion

Pipeline (surveyed location)

Pjpeline (enQineering drawjng localion)

Road

Fenoe 10-fl c1I110Uf

0 40 80

FEET 19113 HAl) t

bull 7rlltJ bull

- _shy

- ~ ~ 7050---middot

- -------- -~--~-

-

-- ~-~

- -~ --~ --- ~ - -- - -~~t= _

- - - --~~~

r050- _15 - -~- -- - - -~

---- ~ -~- _--_ -

- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~

Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn

Figure 519-3 SWMU 21-027(a) proposed sample locations

tI ll (()

ft ) ltc co ~ (0 fIl iii p a IJ)

s ~ ~ IJ)

amp 3

~ ~ J1)J

L

-

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c jgt

0 = C 5 I

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cl jo

-4

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C

= = ltXl- = cJ

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Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007

) SAMPLE ID RE21-07-SS93

ASPLANNtP

DATE COLLECfED(MMlDDIVYYV)

TIME COLLECTED (HlIMM)

PRS ID ZHIZ(JI

LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC

~~v

TOP DEPTH-fIljrid 7

BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I

i ~( ~()T COMPOSITETVPpound --

ASCQLLECTpoundll

2 ftro 7

u C bull 2( o h

R- II01d-2S lei( 4b

4 0 ft- 4 0 f 1shy

bull (

MEDIA

SUBmiddotli--shy~w

SAMPLE TECH CODE

FIELD QCTVPE

FIELD PREP

SAMlLtlJSAGE

SCREENIlOlU DESC

AS PLANNED rev

~ lJhlt77

W 11 rJ

~ 1)

amp

amp

INV

A

ASCQLLECTED

(1 h 1- 3 D tC1 A Cd t

1

tY

EXCAVATED YfSte~N--A----------------Ii

COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA

BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy

PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN

SPECIAL INSTRUCTIONS

2

2

1

8082

8290

NMED Explosives list

125MLGLASS

125MLGLASS

250 l1L AMBER GLASS

_ _-_ _shy

Ice

Ice

Ice

V y

L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH

SAMPLE COMMENTS

LOCATIONDESC Y-1lt~tLev ~k

shy

~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir

FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r

f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM

REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -

DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)

(Signature)

(Printed Name) )C20(Signature) Jo~~

RECEIVED BY Datetrime

I (Printed Name)

DateITimeRELINQUISHED BY

(Printed N arne)

(Signature)(Signature)

I I

I

T-782 POO7l013 F-443 $ +5056060864Jan-15-200S 04 26pm From-EP TA2l __r

GEL lAboratQlies LLC Report Dllte AuguSll 2007

PCB Page 1 of 1 Certificate of Analysis

Sample Summary

SDG NUlllber 07-293 Da~ Collected 07171Z0071200 Man-Ix SOIL

Lab Sample ID 189817001 Date Reccied 071l9J200709)0 Moislure 7 Client SlUllple 12 Client LANL006 Project LANLOOGOO ClientID RE2-07-3893 Method SW846)082 SOP Ref CL-OA-E-04ll

Batch ID 653073 lrut ECD2A1 DIlution 1

Run Daoo 0712712007 1258 AnaYBt JXM Inj Vol tIlL lnpDllte 071J320070800 Aliquot 30~ FInal Volume ImL Dab File 014tl401d Column 1 eLFl Level LOW

014b140~d 2CLP2

CAS No Parnmame Qualifler Result Units Ml)ULOD PQULOQ CoIWl1lI

12674-lJ-2 Aroclor-1016 U 336 uglkg Ll2 336

11104-28-2 Aroclor-1221 U 3~6 uglkg 112 336

1114l-16-) Atoclor-1232 U 336 lIglkg 112 336

53469-21-9 Arocor-1242 U 336 Ilglkg LI2 336

12672-29-lt ArocIOr-l24amp U 336 uSlkg 112 336

1I097-6H Aroclor-12S4 J 120 lIgkg 112 336

11096-82-5 Aroclar-1260 U 336 uglkg 112 336

Page 208 of329

-----

~ 2 ~ o lt0

f

o (N

~ ltll

g 01

-~ - --~

11gt319

21-353 21-485 J I Investigation area

~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I

f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)

J I I

_I I I J

I J J shylI

I -~

-

cJ Slructu ra

l- I Former slructure

Jilvestigalion area

bull Proposed sample toeation

reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion

Pipeline (surveyed location)

Pjpeline (enQineering drawjng localion)

Road

Fenoe 10-fl c1I110Uf

0 40 80

FEET 19113 HAl) t

bull 7rlltJ bull

- _shy

- ~ ~ 7050---middot

- -------- -~--~-

-

-- ~-~

- -~ --~ --- ~ - -- - -~~t= _

- - - --~~~

r050- _15 - -~- -- - - -~

---- ~ -~- _--_ -

- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~

Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn

Figure 519-3 SWMU 21-027(a) proposed sample locations

tI ll (()

ft ) ltc co ~ (0 fIl iii p a IJ)

s ~ ~ IJ)

amp 3

~ ~ J1)J

L

-

I c c 0

c jgt

0 = C 5 I

~

+ UI c UI en cl

cl jo

-4

-I ltXl

C

= = ltXl- = cJ

-n I

___

Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007

) SAMPLE ID RE21-07-SS93

ASPLANNtP

DATE COLLECfED(MMlDDIVYYV)

TIME COLLECTED (HlIMM)

PRS ID ZHIZ(JI

LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC

~~v

TOP DEPTH-fIljrid 7

BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I

i ~( ~()T COMPOSITETVPpound --

ASCQLLECTpoundll

2 ftro 7

u C bull 2( o h

R- II01d-2S lei( 4b

4 0 ft- 4 0 f 1shy

bull (

MEDIA

SUBmiddotli--shy~w

SAMPLE TECH CODE

FIELD QCTVPE

FIELD PREP

SAMlLtlJSAGE

SCREENIlOlU DESC

AS PLANNED rev

~ lJhlt77

W 11 rJ

~ 1)

amp

amp

INV

A

ASCQLLECTED

(1 h 1- 3 D tC1 A Cd t

1

tY

EXCAVATED YfSte~N--A----------------Ii

COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA

BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy

PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN

SPECIAL INSTRUCTIONS

2

2

1

8082

8290

NMED Explosives list

125MLGLASS

125MLGLASS

250 l1L AMBER GLASS

_ _-_ _shy

Ice

Ice

Ice

V y

L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH

SAMPLE COMMENTS

LOCATIONDESC Y-1lt~tLev ~k

shy

~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir

FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r

f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM

REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -

DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)

(Signature)

(Printed Name) )C20(Signature) Jo~~

RECEIVED BY Datetrime

I (Printed Name)

DateITimeRELINQUISHED BY

(Printed N arne)

(Signature)(Signature)

I I

I

-----

~ 2 ~ o lt0

f

o (N

~ ltll

g 01

-~ - --~

11gt319

21-353 21-485 J I Investigation area

~ Ifor SWMU 21-027(a) j( 4-in floor drain pipe ~ U engineerillg drawing location) I

f r I ~~ ~12~n storm drarfl cemeflt culvert _lturveyecl location)

J I I

_I I I J

I J J shylI

I -~

-

cJ Slructu ra

l- I Former slructure

Jilvestigalion area

bull Proposed sample toeation

reg Prop()Sed borehole location amp Previous sample localirm euroI Previous bOfehole localion

Pipeline (surveyed location)

Pjpeline (enQineering drawjng localion)

Road

Fenoe 10-fl c1I110Uf

0 40 80

FEET 19113 HAl) t

bull 7rlltJ bull

- _shy

- ~ ~ 7050---middot

- -------- -~--~-

-

-- ~-~

- -~ --~ --- ~ - -- - -~~t= _

- - - --~~~

r050- _15 - -~- -- - - -~

---- ~ -~- _--_ -

- ~ ~--~~ -- ~ ----- -----~-i~ ~~-~ shy ~ - ~ ~

Slu1s GISLab tA201224 061 4ll4 mgtflfied far F5193 IlPwai sile 1l3D1igt5 plrn

Figure 519-3 SWMU 21-027(a) proposed sample locations

tI ll (()

ft ) ltc co ~ (0 fIl iii p a IJ)

s ~ ~ IJ)

amp 3

~ ~ J1)J

L

-

I c c 0

c jgt

0 = C 5 I

~

+ UI c UI en cl

cl jo

-4

-I ltXl

C

= = ltXl- = cJ

-n I

___

Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007

) SAMPLE ID RE21-07-SS93

ASPLANNtP

DATE COLLECfED(MMlDDIVYYV)

TIME COLLECTED (HlIMM)

PRS ID ZHIZ(JI

LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC

~~v

TOP DEPTH-fIljrid 7

BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I

i ~( ~()T COMPOSITETVPpound --

ASCQLLECTpoundll

2 ftro 7

u C bull 2( o h

R- II01d-2S lei( 4b

4 0 ft- 4 0 f 1shy

bull (

MEDIA

SUBmiddotli--shy~w

SAMPLE TECH CODE

FIELD QCTVPE

FIELD PREP

SAMlLtlJSAGE

SCREENIlOlU DESC

AS PLANNED rev

~ lJhlt77

W 11 rJ

~ 1)

amp

amp

INV

A

ASCQLLECTED

(1 h 1- 3 D tC1 A Cd t

1

tY

EXCAVATED YfSte~N--A----------------Ii

COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA

BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy

PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN

SPECIAL INSTRUCTIONS

2

2

1

8082

8290

NMED Explosives list

125MLGLASS

125MLGLASS

250 l1L AMBER GLASS

_ _-_ _shy

Ice

Ice

Ice

V y

L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH

SAMPLE COMMENTS

LOCATIONDESC Y-1lt~tLev ~k

shy

~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir

FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r

f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM

REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -

DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)

(Signature)

(Printed Name) )C20(Signature) Jo~~

RECEIVED BY Datetrime

I (Printed Name)

DateITimeRELINQUISHED BY

(Printed N arne)

(Signature)(Signature)

I I

I

___

Jilil-IO-UUO U4QPm rrum-tr IA +bUb1i060664 T-78Z P009013 F-443 LU~ fllUllU~ rl~110nal Luoorarory Page I or

SAMPLE COLLECTION LOGFIELD CHAIN OF CUSTODY EVENT ID 198 EVENT NAME CU21-027(a) DP Site Summer]a1l2007

) SAMPLE ID RE21-07-SS93

ASPLANNtP

DATE COLLECfED(MMlDDIVYYV)

TIME COLLECTED (HlIMM)

PRS ID ZHIZ(JI

LOCATIONm ~~11u1 LOCATION TYPE GENpoundRlC

~~v

TOP DEPTH-fIljrid 7

BonOM DEPTH -r i01 FIElJlMTR1X --5- ~~~I

i ~( ~()T COMPOSITETVPpound --

ASCQLLECTpoundll

2 ftro 7

u C bull 2( o h

R- II01d-2S lei( 4b

4 0 ft- 4 0 f 1shy

bull (

MEDIA

SUBmiddotli--shy~w

SAMPLE TECH CODE

FIELD QCTVPE

FIELD PREP

SAMlLtlJSAGE

SCREENIlOlU DESC

AS PLANNED rev

~ lJhlt77

W 11 rJ

~ 1)

amp

amp

INV

A

ASCQLLECTED

(1 h 1- 3 D tC1 A Cd t

1

tY

EXCAVATED YfSte~N--A----------------Ii

COMPOSITpoundnME1NTERVAL WATER FLOWING YES~NA

BOREHOLE YES~A BOREHOLE DECLINATION ___~__ BOREHOLE DIRECTION shy

PRIOnlTY ORD~R CNTNR PRESERVATIVE COLLECTED YIN

SPECIAL INSTRUCTIONS

2

2

1

8082

8290

NMED Explosives list

125MLGLASS

125MLGLASS

250 l1L AMBER GLASS

_ _-_ _shy

Ice

Ice

Ice

V y

L _____ --_ )SAMPLE DESC t Quck I uGrvi- 15~ Gr~v TIImiddotH

SAMPLE COMMENTS

LOCATIONDESC Y-1lt~tLev ~k

shy

~c~~ 4(0 ]n Ie r fr-Dt71 (one) 113 ~r~ 1110 CIir

FIELD SCREENINGIMEASUREMENT RESULTS flO bf-c ygtY1rxi- 0 -0 r31r

f ~ I rf olcJ1f p j tJ~ Ot p17d 7-tdfM

REVIEWED BY (PRINT ___________COLLECT~DBY (pRINT) _ __---Vi shyr shy -

DateffilneDateffime RECEIVED BYRELINQUISHED BY I070 r (Printed Name)

(Signature)

(Printed Name) )C20(Signature) Jo~~

RECEIVED BY Datetrime

I (Printed Name)

DateITimeRELINQUISHED BY

(Printed N arne)

(Signature)(Signature)

I I

I

I

CL

cYgt

shy

u Sample ill RE21-07-5893 (Q

Client Data = Los Alamoo National Laboratory 0amp-347 S-Dee-07 0830

Samlc Data

Malrix Soil Sample Size t 13 g

middotSolids 894

shycgt

cgt

Name Project Date Collected Time Collected

co I Analyte Cone (pglg) DL a EWCb Qualifierst-

2378-TCDD 12378-PeCDD

l23478-HxCDD

123678-HxCDD

ltJgt CO Cgt 123789-HxCDDUgt cgt lt0 LO

1234678-HpCDD = In + OeDD

2378-TCDF

12378-PeCDF 23478-PeCDF

123478-HxCDF 12367 8-HxC DF

23 467amp-HxCDF

123789middotHxCDF

1234678-HpCDF 1234789-HpCDF

aCDF

Totals

0599 322

63amp

379

16l

1320

15200 0302

0503 L4J

492

382

692

129 [52

142

503

423

279 259 2790

643

276

205

726

435

284

699

J

I J

J B

B

EPA lVlcthod 8290

labontoa Data

Lab Sample 30042~OOl Dare Reeeind 7-Dec-07 QC Batch No 9763 Date ExlIllc[ltd 1O-Dec-07 Dale Analyzed DB-5 13-Dee-07 [)ate Analyzrd DB-225 NA

_shy

Labeled Standard R LeL-UCLd Qualifiers _ shy

IS t3C-2J78-TCDD 898 4) - 13S 13C-[2J7S-PeCDD 916 40 - 135 13C-l23478-HxCDD 935 40- 135 13C-l236 78-HltCD 0 816 40 - 135

lJC-l234678-HpCDD 104shy 40 shy 135 13C-OCDD 122 40 shy l35 13C-2378-TCDF 100 40 - 135 llC-l 2378- PeC DF [04 40- 135 13C-23478-PeCDF 109 40- fJ5 [3C-I2JA78-HKCDF 914 40 - 135

l3C- 123678-HxCDF 792 4() - lJ5 l3C-234678-HxCDP 842 40 shy 135

13C-l23789-HxCDF 9l2 40- 135 [3C-1234678-HpCDF 847 40 shy [35

13C-1234789-HpCDF 991 40 - DS L3C-QCDF 985 40 shy 135

CRS 37Cl-2378-TCDD 936 40 shy 135 eTodc Equivalent Qnotient (fEQ) Data

-lt t-CL UJ

I E o ~

LL

E n

lt0

cgt agt lt=gt cgt

I tn

I c

TotalrCDD

Total PeCDD Total HxCDD Total HpCDD Total TCDF Total PeCDF Total HxCDF

Tota[ HpCDF

Anal~st MAS

P

P

P BP

TEQ(Min) 413

a Sample specific etimated detection j iInil

b Eslilnated maximum possible cQfcenlfatioll

c Method detec1iol1lirniL

d Lo1r~oltrollimil- uppNcolltrollimit

e 7EQ based an (1989) [nternatiooal roxie EquiaIent Filltturs (ITEn

The fltlltl-Wll are repooed in dry weighl The sam pIe size is rej)lJrtild in wltt weight

AwrovedBy Martha M Maier lJ-Dec-2007 1527

T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864

1 High Explosives Analysls Data Sheet

I CalNo 118-96-7

I 121~14-2 Irshy 121-82-4

19406-51-0

2691-41middot0

35572~7g2

479-45-8

606middot20middot2 78-11-5

88-72-2

98-95-3

99-08-1 -~

9935-4

99middot65middot0 f

99w99-0l

Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893

Lab Code GEL GEL Job No (SDG) ~

Matrix SOIL GEL Sample ID 198941001

Moistm-e 103Sample Amount pound

Amoullt Units l Date Received 07~DECmiddot07

Extl8ction Type Sonicatioll Extraction Batch In 709399

COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07

PllutlOll Facto ~ Injection Volume CuLl ~

Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a

Units ugJkg __ n _

ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I

~ 24middotDinitrotolu~ene SOD I U

Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-

HMX

2-Amino-46-dinitro ojuelle

Tetryl

I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t

a

PElN 1000 U wNitrotoluellc

500 ~-1 Nitrobenzen 500 I U

i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U

ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U

____ ___-l_____ _ __ ___ L___~ - ~

_ soo U

500 U -i 500 U

-J

-----~~------------ ----- shy Concentration

Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor

Page of 2

Page 93 of344

Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443

1 High Explosives Analysis DII tn Sheet

Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893

Lab Code GEL GEL Job No (SDG) ~

Matrix SOIL GEL Sam)Je lD 198947001

Moisture 103Sample Amount 2

Date Received 07-DEC-07Amount Unitli g

Extmction Type Sonication Extractiou Batch ID 709399

Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07

Dilution Fact6r Injection Volume (uL) 50

Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff

Units ugkg

Cas No 3058middot386

59229-7S-3

Compound TATB

26-Diminc-4-nitI

- shy --- Concentnnkm -~T-0-1 1000 -~

2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U

6629--29-4

78-30-8

24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -

- ] 2000 U bull

1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I

-~-------- ---shyConcenlrarion

IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor

Page 2 of 2

Page 96 of344

-

II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443

GE~ Inboratories LLe Report Date December 15 2007

SDGNuwber 08-348 Lab Sample ill 198947001

CilelltID REZT-Ol-S893

)llltch fI) 10954l

RunDllte 1211412007 0149

Prep Date 121102007 1953

DlItli FIle 049f4901d

049b49111d

CAS No Fucmname --shy

12674-Il-2 Aruclor-l 0 16

11104-28-2 Arocior-1221

11141-16-5 AroelOr- 1232

53469-21-9 Aroclor-1242

12672-29-6 Aroclor-1248

11097-69-1 Aroclor-1254

11096-81-5 Aroclor-1260

PCB Certifieate of Analysts

Sample Summary

Date Collected 1210512007 1200

Dute Received 120712007 0930 Client LANL008

Method SW84ti8082

In8t EC02Al

Analyst JXM Aliquot 29911 Column lCLPl

2CLP2

Quulitiec Result l1nits ------ U 373 Ij1kg

U 373 uglkg

U 373 ujlkg

U 373 uglkg

U 373 u1kg

950 uglkg

690 uglkg

Page I of 1

Ma[th S

Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1

Inj Vol luI binlll Volume ImL

Level LOW

MDLtrOD PQt1OQ Column shy

124 373

124 373

124 373

124 373

24 373

124 373 2

124 373

Page 232 of 344

-

T-782 P 011013 F-443Jilll-IO-UUO U4 opm rrom-II III +5056060864

1 High Explosives Analysls Data Sheet

I CalNo 118-96-7

I 121~14-2 Irshy 121-82-4

19406-51-0

2691-41middot0

35572~7g2

479-45-8

606middot20middot2 78-11-5

88-72-2

98-95-3

99-08-1 -~

9935-4

99middot65middot0 f

99w99-0l

Lab Name General Engineering Lahorarcries Client Sample ID RE21-07-5893

Lab Code GEL GEL Job No (SDG) ~

Matrix SOIL GEL Sample ID 198941001

Moistm-e 103Sample Amount pound

Amoullt Units l Date Received 07~DECmiddot07

Extl8ction Type Sonicatioll Extraction Batch In 709399

COllcenhated Extlllct Volume (UlL) ill Dale Extracted 12middotDEC-07

PllutlOll Facto ~ Injection Volume CuLl ~

Date Analyzed 1H)EC-07 1529GEL (lata tJle EXP12l20S7a

Units ugJkg __ n _

ComJound Concentration -Q]- - 500246-Trinitrotoh Hme 1 U I

~ 24middotDinitrotolu~ene SOD I U

Rl)X 500 I u1 4-Amino-26dinibmiddoto l) illene 500 r-u-

HMX

2-Amino-46-dinitro ojuelle

Tetryl

I 26-Dlllltrotolul~ ~ lUi middot-------~------~----~-----~--t

a

PElN 1000 U wNitrotoluellc

500 ~-1 Nitrobenzen 500 I U

i m-NitrotolUefle SOD I u 135-Tdnitrober zelle 500 I U

ffi-Dinitrobenzi ne 1 500 lUi p-Nitrotoluel1e 500 I U

____ ___-l_____ _ __ ___ L___~ - ~

_ soo U

500 U -i 500 U

-J

-----~~------------ ----- shy Concentration

Instnment X ConcenUllred Extract Volume X Dilutioll Value Samele ArnouD Factor

Page of 2

Page 93 of344

Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443

1 High Explosives Analysis DII tn Sheet

Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893

Lab Code GEL GEL Job No (SDG) ~

Matrix SOIL GEL Sam)Je lD 198947001

Moisture 103Sample Amount 2

Date Received 07-DEC-07Amount Unitli g

Extmction Type Sonication Extractiou Batch ID 709399

Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07

Dilution Fact6r Injection Volume (uL) 50

Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff

Units ugkg

Cas No 3058middot386

59229-7S-3

Compound TATB

26-Diminc-4-nitI

- shy --- Concentnnkm -~T-0-1 1000 -~

2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U

6629--29-4

78-30-8

24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -

- ] 2000 U bull

1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I

-~-------- ---shyConcenlrarion

IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor

Page 2 of 2

Page 96 of344

-

II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443

GE~ Inboratories LLe Report Date December 15 2007

SDGNuwber 08-348 Lab Sample ill 198947001

CilelltID REZT-Ol-S893

)llltch fI) 10954l

RunDllte 1211412007 0149

Prep Date 121102007 1953

DlItli FIle 049f4901d

049b49111d

CAS No Fucmname --shy

12674-Il-2 Aruclor-l 0 16

11104-28-2 Arocior-1221

11141-16-5 AroelOr- 1232

53469-21-9 Aroclor-1242

12672-29-6 Aroclor-1248

11097-69-1 Aroclor-1254

11096-81-5 Aroclor-1260

PCB Certifieate of Analysts

Sample Summary

Date Collected 1210512007 1200

Dute Received 120712007 0930 Client LANL008

Method SW84ti8082

In8t EC02Al

Analyst JXM Aliquot 29911 Column lCLPl

2CLP2

Quulitiec Result l1nits ------ U 373 Ij1kg

U 373 uglkg

U 373 ujlkg

U 373 uglkg

U 373 u1kg

950 uglkg

690 uglkg

Page I of 1

Ma[th S

Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1

Inj Vol luI binlll Volume ImL

Level LOW

MDLtrOD PQt1OQ Column shy

124 373

124 373

124 373

124 373

24 373

124 373 2

124 373

Page 232 of 344

-

Jan-IO-UU~ U4pm Irom-t IAll +5056060864 T-782 P012013 F-443

1 High Explosives Analysis DII tn Sheet

Lab Name Qeneml Engineering Laboratories Client Sample llgt RE21-07-5893

Lab Code GEL GEL Job No (SDG) ~

Matrix SOIL GEL Sam)Je lD 198947001

Moisture 103Sample Amount 2

Date Received 07-DEC-07Amount Unitli g

Extmction Type Sonication Extractiou Batch ID 709399

Concentrated Extract Volume (mL) 12 Date Extracted 12-DECmiddot07

Dilution Fact6r Injection Volume (uL) 50

Date Analyzed 17middotDECmiddot07 1903 GEL data file EXS12 17035wiff

Units ugkg

Cas No 3058middot386

59229-7S-3

Compound TATB

26-Diminc-4-nitI

- shy --- Concentnnkm -~T-0-1 1000 -~

2000 1u 618middot87-1 3SmiddotDinitroaniIinc 1000 U

6629--29-4

78-30-8

24Dlamlno-6-iroii~n-trls(o-cresyl) phosphate _~___~ bull -

- ] 2000 U bull

1000 U -1I __bullbull_ bullbullbull___ ~_________ I--_~ I

-~-------- ---shyConcenlrarion

IloSlfllmem X Concanrated Etracr Volllrne Dilution L Value ~__~ Sample Amoun X Factor

Page 2 of 2

Page 96 of344

-

II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443

GE~ Inboratories LLe Report Date December 15 2007

SDGNuwber 08-348 Lab Sample ill 198947001

CilelltID REZT-Ol-S893

)llltch fI) 10954l

RunDllte 1211412007 0149

Prep Date 121102007 1953

DlItli FIle 049f4901d

049b49111d

CAS No Fucmname --shy

12674-Il-2 Aruclor-l 0 16

11104-28-2 Arocior-1221

11141-16-5 AroelOr- 1232

53469-21-9 Aroclor-1242

12672-29-6 Aroclor-1248

11097-69-1 Aroclor-1254

11096-81-5 Aroclor-1260

PCB Certifieate of Analysts

Sample Summary

Date Collected 1210512007 1200

Dute Received 120712007 0930 Client LANL008

Method SW84ti8082

In8t EC02Al

Analyst JXM Aliquot 29911 Column lCLPl

2CLP2

Quulitiec Result l1nits ------ U 373 Ij1kg

U 373 uglkg

U 373 ujlkg

U 373 uglkg

U 373 u1kg

950 uglkg

690 uglkg

Page I of 1

Ma[th S

Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1

Inj Vol luI binlll Volume ImL

Level LOW

MDLtrOD PQt1OQ Column shy

124 373

124 373

124 373

124 373

24 373

124 373 2

124 373

Page 232 of 344

-

II-IO-UUC Uflpm rrom-cr 111pound I +5056060864 T-782 P013013 F-443

GE~ Inboratories LLe Report Date December 15 2007

SDGNuwber 08-348 Lab Sample ill 198947001

CilelltID REZT-Ol-S893

)llltch fI) 10954l

RunDllte 1211412007 0149

Prep Date 121102007 1953

DlItli FIle 049f4901d

049b49111d

CAS No Fucmname --shy

12674-Il-2 Aruclor-l 0 16

11104-28-2 Arocior-1221

11141-16-5 AroelOr- 1232

53469-21-9 Aroclor-1242

12672-29-6 Aroclor-1248

11097-69-1 Aroclor-1254

11096-81-5 Aroclor-1260

PCB Certifieate of Analysts

Sample Summary

Date Collected 1210512007 1200

Dute Received 120712007 0930 Client LANL008

Method SW84ti8082

In8t EC02Al

Analyst JXM Aliquot 29911 Column lCLPl

2CLP2

Quulitiec Result l1nits ------ U 373 Ij1kg

U 373 uglkg

U 373 ujlkg

U 373 uglkg

U 373 u1kg

950 uglkg

690 uglkg

Page I of 1

Ma[th S

Moistllre 103 Project LANLOO800 SOPRlf GL-oA-E-040 Dilution 1

Inj Vol luI binlll Volume ImL

Level LOW

MDLtrOD PQt1OQ Column shy

124 373

124 373

124 373

124 373

24 373

124 373 2

124 373

Page 232 of 344

-