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  • 7/28/2019 Activa s Horiba

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    Simply competitive

    Spectrometer o high quality

    Sensor or Spectroscopy

    Explore the future Automotive Test Systems | Process & Environmental | Medical | Semiconductor | ScientificExplore the future Automotive Test Systems | Process & Environmental | Medical | Semiconductor | Scientific

    ACTIVA-SIts the S inside that counts

    Offer your lab Simplicity in a high

    performance Spectrometer.

    Sotware or all

    Supplies

    ACTIVA S

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    U

    ltima

    2Simply competitive

    potential use o all ICP lines, and a Superior Semi-

    quantitative analysis oers a precise identication o

    the Samples.

    Quality

    The combination o HORIBA Scientifc high quality

    optics with the advanced eatures o the CCD detector

    is optimized to make the dierence. The ultra-low

    noise and excellent practical dynamic range o

    the CCD, associated to the constant resolution,

    aberration ree, high luminosity holographic gratings

    o the optical System, enable the instrument to t the

    needs o Simplicity, Stability and Quality.

    The high perormance CCD Sensor designed or

    Scientic Spectroscopy provides excellent analytical

    capabilities, obtained with minimal operator

    optimisation. The powerul ACTIVAnalyst Sotware

    enhances the unique capabilities o the instrumental

    conguration.

    ACTIVA-S is a CCD-based ICP-AES instrument based

    upon A Platorm or the Future, maintaining the

    Strengths o HORIBA Scientic Spectrometers while

    incorporating advanced CCD (Charge Coupled Device)

    technology to improve quality and fexibility.

    ACTIVA-S is the perect Solution to rst-time operators

    and or routine analysis with dened applications.

    Simplicity

    Both Spectrometer and Detector o ACTIVA-S oer

    the ease-o-use that every analyst wishes. Plug-&-

    Play operations and automatic optimisations help the

    user to operate the instrument at its best and achieve

    excellent analytical results.

    Flexibility

    The Total Plasma View, rom Superior vertical torch

    based radial observation, combined with a light-rich,

    high perormance optical System, allows the analyst to

    run all types o Samples. The ull wavelength coverage,

    rom 160 to 800 nm, emphasizes this fexibility: a

    unique and proprietary ICP-based Spectral database

    (rom S3-base: Single-element Spectra, Spectroscopic

    data) leads to optimum Selectivity with

    ACTIVA-S CCD-based ICP Atomic Emission SpectrometerCombines Simplicity with a high performance CCD Detector

    2

    AC

    TIVA

    S

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    Spectrometer of high quality

    The Dual back-to-back gratings (4343 / 2400 g/mm)

    oer constant Spectral resolution and ull fexibility in

    line Selection. The optical resolution is better than 12

    pm in the 160-430 nm range and less than 22 pm in

    the 430-800 nm range.

    High technology electronics with Rapid ChipTM

    components leads to ast data transer and

    processing.

    The ultra low noise CCD Solid State detector

    oers high productivity analysis o multiple elements

    at multiple wavelengths including Simultaneous

    background correction within a spectral window.

    The rst-time user rapidly becomes condent in the

    use o the instrument: optimisation operations oranalytical corrections are minimised and the plasma

    conguration is ready or all applications.

    Spacious Sample introduction area and convenient

    corrosion resistant old-down Sample tray enable

    the user to run any type o Samples with dedicated

    Sample introduction Systems.

    Quick release and quick mount torch design

    in a large and user-riendly compartment, with no

    adjustmentrequired, acilitates multi-user operation

    and provides excellent reproducibility.

    The Vertical Torch with Superior Total Plasma View

    provides optimum Sensitivity, with reduced matrix

    eects, or both aqueous and organic matrices. The

    Sheath gas device, with a large 3 mm i.d. injector tube,

    gives unique high dissolved Solids capability (up to

    30% NaCl), with excellent long-term Stability, and

    minimises memory eects.

    Smart Hood provides Sae, convenient extraction

    with reduced installation costs.

    Reliable high eciency 40.68 MHz Solid State

    generator enhances the ability to handle a wide variety

    o applications and improves the limits o detection.

    Warm-up time is also reduced (usually less than 15

    minutes).

    Excellence in Spectrometer configuration with attention to Simplicity,flexibility and quality

    3

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    productivity analysis o multiple elements at multiple

    wavelengths including background correction within a

    Spectral window. The addition o adjacent Spectral

    windows allows the System to cover the entire

    Spectrum, or ast Semi-quantitative analysis with

    multiple wavelengths.

    ACTIVA-S is equipped with an Open Electrode CCD

    (Charge Coupled Device) detector with an image area

    o 26.6 x 6.7 mm. This detector is perectly Suited

    to the Total Plasma View confguration by efciently

    collecting all the useul inormation emitted by the

    plasma. Simultaneous measurement provides high

    capability then provide a practical dynamic range

    (Signal beore saturation-to-readout noise ratio) o 107,

    with a linear response range o 5 decades minimum,

    or each line.

    Analysis o trace and major elements can be easily

    perormed with one measurement, without requiring

    dilution.

    A powerul pre-Shot algorithm automatically optimizes

    exposure time and column binning, which takes

    advantage o the ull benet o the maximum available

    dynamic range. Binning o the 256 pixel-high column

    results in a decrease in read-out time with no addition

    o readout noise and an increase in the linear dynamic

    range. The combination o ultra low noise and binning

    Sensor for Spectroscopy

    Unique CCD adapted to HORIBA Scientific quality optics

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    AC

    TIVA

    S

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    ACTIVAnalyst Sotware provides a data audit

    trail or user and instrument operation, and an online

    lab book to record daily actions perormed. Multi-level

    Security permits user access levels or viewing and

    editing.

    The wavelength library is based on the unique and

    proprietary S3-base developed by HORIBA Scientic,

    eaturing not only actual wavelengths derived rom an

    ICP Spectrometer, but also their Spectroscopic data

    such as limit o detection, line width, etc.

    Productivity is enhanced by automatic user

    programmable Start up and Shutdown, minimising

    argon usage.

    Within a method, the user gets assistancein optimisation o line Selection and acquisition

    parameters.

    Productivity is urther enhanced with automated

    analysis using a multi-method Sequence or Samples

    o various matrices requiring dierent methods.

    Barcode identication is available or Samples loaded

    in a Sequence. Automatic unattended operation is

    possible using the auto-Sampler with programmable

    re-calibrations and QC checks with user dened

    actions.

    The Simultaneous measurement provides the

    ability to visualise the Spectra o lines and their vicinityduring analysis, or ast conrmation o element

    presence or visual identication o unexpected

    Spectral intererences.

    Automatic Superior Semi-quantitative analysis

    o all elements is perormed rom ull Spectrum

    acquisition (IMAGE) and with the Total View mode or

    concentration calculation, data reporting and data re-

    processing.

    Urgent Samples can be inserted in an on-going

    Sequence, using either the current method or any

    other method.

    When required, results can be optimised, using

    various analytical correction methods. Results

    reprocessing is

    possible ater calibration or parameter changes.

    The user benets o network ready results and

    reporting with fexible export to a dened location orto a LIMS System.

    Diagnostics data reporting allows the analyst to

    control the perormance o the instrument.

    SPC (Statistical Process Control) is included

    or X, R, SD and histogram charts o user-Selected

    Solutions.

    Audit Trail Analyst or 21CFR Part 11 compliance

    with a powerul SQL Server database oers data

    Security with electronic Signatures and multi-level

    authorisation logon, and an error log le.

    TimeScan gives the possibility to have real-timeoutput o instrument Signal or troubleshooting, or or

    transient Signal acquisition (data available or export

    as a TXT le).

    Software for allPowerful ACTIVAnalyst Software extends instrument capability and fullyutilizes the unique capabilities of Solid State detection

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    Supplies

    Samples introduction systems

    Other accessories

    6

    Sample Type / Item Nebuliser Spray Chambe

    Standard

    kit P/N: 24 031 500

    Concentric, glass

    P/N: 47 929 058

    50 psi argon gas, 1 mL/min

    sample uptake

    Cyclone, glass

    P/N: 47 929 056

    High TDS / Mineral Salt

    kit P/N:

    24 072 160 (concentric / cyclo)

    24 031 510 (parallel / cyclo)

    24 031 570 (parallel / Scott)

    Concentric, glass

    P/N: 24 072 150

    30 psi argon gas, 2 mL/min

    sample uptake

    Parallel fow, PEEK/Tefon

    P/N: 47 929 024

    50 psi argon gas, 1 mL/min

    sample uptake

    Cyclone, glass

    P/N: 47 929 056

    I sensitivity is the main criteria

    Scott, glass

    P/N: 31 031 491

    I stability is the main criteria

    Requires a nebuliser adapter (P/N: 24

    Cyclone with central transer tube

    P/N: 47 929 063

    For good sensitivity and

    stability compromise

    HF

    kit P/N: 24 031 710

    Parallel fow, PEEK/Tefon

    P/N: 47 929 024

    50 psi argon gas, 1 mL/min

    sample uptake

    Cyclone, Tefon

    P/N: 47 929 031

    Limited Volume / Volatile Solvent

    kit P/N:

    24 072 030 (100 l/min

    concentric / mini-cyclo)

    Concentric, glass (limited volume)P/N: 47 929 053

    50 psi argon gas, 100 L/min

    sample uptake

    Concentric, glass (volatile solvent)

    P/N: 24 072 100

    30 psi argon gas, 0.5 mL/min

    sample uptake

    Cyclone, glassP/N: 31 031 279

    Mini-cyclone, glass

    P/N: 47 929 049

    For sensitivity at low uptake

    and very ast washout

    Cooled cyclone, glass (Peltier ee

    P/N: 24 072 210

    For optimum sensitivity

    with volatile samples

    Organics / Slurries

    kit P/N:24 031 610 (0.7 mm id nebuliser)

    24 031 600 (1 mm id nebuliser)

    Jobin Yvon, Pt needle, Zr nozzle

    P/N: 24 031 060

    0.7 mm id needle

    Jobin Yvon, Stainless Steel needle, Zr nozzle

    P/N: 24 031 050

    1 mm id needle

    (or large particulates, ie wear metals)

    Scott, glass

    P/N: 31 031 491

    Requires the JY nebuliser

    adapter (P/N: 24 031 070)

    USN nebuliser

    P/N: 24 031 650

    For aqueous solutions

    (gain in sensitivity

    by a actor o 5 to 20)

    CMA

    P/N: 24 072 140

    Kit P/N: 24 031 660 (concentric) ;

    24 031 670 (parallel)

    For simultaneous analysis o hydridesand normal elements

    AC

    TIVA

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    7

    Torch Observations

    Demountable torch

    P/N: 21 356 110

    Sheath gas system (glass)

    P/N: 21 356 040

    Specications: high sensitivity, short washout time

    Examples o application: routine applications o

    clean aqueous or organic solutions (water,)

    Demountable torch

    P/N: 21 356 110

    Sheath gas system (glass)

    P/N: 21 356 040

    Specications: suitable to high Total Dissolved Solids (TDS), high

    precision

    Examples o application: waste, sediment, sea water, metals (Cu 30

    g/l, precious metals,), alloys, NaCl 300 g/l, LiBO2

    20 g/l (usion),

    Leachates, cement, Ca sulate require preerably the concentric

    nebuliser

    Argon humidier (P/N: 24 056 810) is required with the concentric

    nebuliser

    Demountable torch

    P/N: 21 356 110

    Alumina inner (P/N: 31 032 312) and outer (P/N: 31

    032 313) tubes available i B, Na,Si to measure at

    trace levels

    Sheath gas system (inert material)P/N: 20 925 160

    Specications: suitable to hydrofuoric acid (HF)

    Examples o application: reractory samples requiring HF digestion

    (Ti base, silica, ashes, lters (air samples))

    Demountable torchP/N: 21 356 110

    Sheath gas system (glass)

    P/N: 21 356 040

    Specifcations: suitable to low volume or volatile samples, with optimumsensitivity

    Examples o application: biological or nuclear samples (small

    amount); ethanol, MIBK, gasoline, acetic acid (volatile)

    Demountable torch

    P/N: 21 356 110

    Sheath gas system (glass)

    P/N: 21 356 040

    Specifcations: robust and stable operating conditions, high precision

    Examples o application: wear metals in oil, uel, biodiesel, particulates

    Oxygen Kit (P/N: 24 056 360) is required or

    analysis o Na and K at ppb levels in organic samples

    AS-500 autosampler

    P/N: 44 820 097

    (up to 360 samples)

    Laser ablation

    For solid samples

    ax

    4 056 140 (ULTIMA 2) ;

    6 740 (ACTIVA amily)

    mples that solidiy

    m temperature (heatingample tube to spray chamber)

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    8/8Explore the future Automotive Test Systems | Process & Environmental | Medical | Semiconductor | ScientificExplore the future Automotive Test Systems | Process & Environmental | Medical | Semiconductor | Scientific

    TECHNICAL SPECIFICATIONSRadio requency, solid-state 40.68 MHz,

    water cooled

    GenCo water chiller for the generator and the coil

    direct exhaust connection or plasma

    compartment

    Fully demountable torch, 3 mm i.d; aluminainjector, 12 L/min plasma gas, 0.2 L/min

    sheath gas

    Concentric glass nebulizer, cyclonic glass

    spray chamber, 3 channels peristaltic pump

    Thermo-regulated, 0.64 meter ocal length,

    dual back-to-back gratings, 4343 g/mm and

    2400 g/mm used in the 1st order with optical

    resolution