530 process

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250 g 20 g Glycerin (Glycerol) 2 g Carboxymethyl 30.31 g Alcohol (ethanol 95%) 2 g Benzoic acid 60 g Glycerin (Glycerol) 0.8 g Bromhexine HCl 0.34 g All fruit flavor 100 g Glycerin (Glycerol) 15 g Water Transf Cool down to Transf 0.14 g Sodium hydroxide pellets Adjust PH in Vess Containe Containe Vess Transf er Transf Check clarity Check & record PH (3.3- 3.6) Volume up to 1L, check & Containe Transf Containe Transf Containe

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Cool down to 3020 g Glycerin (Glycerol)2 g Carboxymethyl cellulose sodium (sodium CMC)

TransferTransferTransferTransferTransferTransfer30.31 g Alcohol (ethanol 95%)2 g Benzoic acid60 g Glycerin (Glycerol)0.8 g Bromhexine HCl0.34 g All fruit flavor20 g Glycerin (Glycerol) (Rinse the container)20 g Water(Rinse the container)

TransferContainer 5Container 4Container 3VesselContainer 2Container 1VesselAdjust PH in vessel to 3.5

Check clarityCheck & record PH (3.3-3.6)Volume up to 1L, check & record PH and filter

0.14 g Sodium hydroxide pellets5 g Water (30)15 g Water1 g Tartaric acid100 g Glycerin (Glycerol)571.4 g Sorbitol (70% solution)250 g Water

AlcoholAdd Benzoic acid, Glycerol 60gm, Bromohexidine, Fruit Flavor

Rinse with 20gm GlycerolRinse with 2gm water

250ml water at 65-70 degrees

Load 100gm Glycerol

NaOH for pH AdjustmentSorbitol for ClarityTartaric Acid + 15gms Water

Add 20gm GlycerolAdd 2gm CMC

Manufacturing Tank