302.l9.fatigue.20nov02 (1)
TRANSCRIPT
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Microstructure-Properties: II
Fatigue
27-302
Lecture 9
Fall, 2002
Prof. A. D. Rollett
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Materials Tetrahedron
Microstructure Properties
Processing
Performance
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Objective
The objective ofthis lectureisto explainthephenomenon of fatigue and also to show howresistanceto fatigue failuredepends on
microstructure. For27-302, Fall 2002: thisslidesetcontains morematerial thancan becoveredinthetime available.Slidesthatcontain material overand abovethat
expected forthiscourse are marked *.
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References
Mechanical BehaviorofMaterials (2000), T. H. Courtney,McGraw-Hill, Boston.
Phasetransformationsin metals and alloys, D.A. Porter, &K.E. Easterling, Chapman & Hall.
Materials Principles & Practice, Butterworth Heinemann,Edited by C. Newey & G. Weaver.
Mechanical Metallurgy, McGrawHill, G.E. Dieter, 3rd Ed.
Light Alloys(1996), I.J. Polmear, Wiley, 3rd Ed.
Hull, D. and D. J. Bacon(1984). Introductionto Dislocations.Oxford, UK, Pergamon.
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NotationW
a:=Alternatingstress
Wm := MeanstressR := Stressratio
I := strainNf := numberofcyclesto failureA := AmplituderatioIpl := PlasticstrainamplitudeIel := ElasticstrainamplitudeK:= Proportionalityconstant, cyclicstress-strainn:= Exponentincyclicstress-strainc := Exponentin Coffin-Manson Eq.;
also, crack lengthE := Youngsmodulusb := exponentin Basquin Eq.
m:= exponentin ParisLawK:= Stressintensity
K:=Stressintensityamplitude
a := crack length
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Fatigue
Fatigueisthenamegivento failureinresponsetoalternating loads(as opposedto monotonicstraining).
Instead of measuringtheresistanceto fatigue failurethrough anupperlimitto strain(asinductility), thetypicalmeasure of fatigueresistanceisexpressedinterms ofnumbers ofcyclesto failure. Fora givennumberofcycles(requiredin an application), sometimesthestress(thatcan besafelyendured bythe material) isspecified.
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Fatigue: general characteristics
Primarydesigncriterioninrotatingparts.
Fatigue as a name forthephenomenon based onthenotionof a material becoming tired, i.e. failing at lessthanitsnominal strength.
Cyclical strain(stress) leadsto fatigue failure. Occursin metals andpolymers butrarelyinceramics.
Also anissue forstatic parts, e.g. bridges.
Cyclic loadingstress limit
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Fatigue:general characteristics
Most applications ofstructural materialsinvolvecyclicloading; anynettensilestress leadsto fatigue.
Fatigue failuresurfaceshavethreecharacteristic features:[seenextslide, also Courtney figs. 12.1, 12.2]
A (near-)surfacedefect asthe origin ofthecrack Striationscorrespondingto slow, intermittentcrackgrowth
Dull, fibrous brittle fracturesurface(rapidgrowth).
Life ofstructural componentsgenerally limited bycyclicloading, notstaticstrength.
Mostenvironmental factorsshorten life.
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S-NCurves
S-N [stress-numberofcyclesto failure] curvedefines locusofcycles-to-failure forgivencyclicstress.
Rotating-beam fatiguetestisstandard; also alternatingtension-compression.
Plotstressversusthelog(numberofcyclesto failure), log(Nf).[seenextslide,also Courtney figs. 12.8, 12.9]
Forfrequencies< 200Hz,metals areinsensitivetofrequency; fatigue lifeinpolymersis frequency
dependent.
[Hertzberg]
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Fatigue testing, S-Ncurve
[Dieter]
Note the presence of a
fatigue limit in manysteels and its absence
in aluminum alloys.
log Nf
Wa
Wmean 1Wmean 2Wmean 3
Wmean 3 > Wmean 2 > Wmean 1Thegreaterthenumberofcyclesinthe loadinghistory,thesmallerthestressthatthe material can withstand
without failure.
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Endurance Limits
Some materialsexhibitendurance limits, i.e. astress below whichthe lifeisinfinite: [fig. 12.8] Steelstypicallyshow anendurance limit, = 40% ofyield;
thisistypically associated withthepresence of a solute
(carbon, nitrogen) thatpines dislocations andpreventsdislocation motion atsmall displacements orstrains(whichis apparentin an upperyieldpoint).
Aluminum alloys do notshow endurance limits; thisisrelatedto the absence of dislocation-pinningsolutes.
At large Nf, the lifetimeis dominated by nucleation. Thereforestrengtheningthesurface(shotpeening) is beneficial to
delay crack nucleation andextend life.
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Fatigue fracture
surface
[Hertzberg]
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Fatigue crack stages
Stage 1
Stage 2[Dieter]
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Fatigue Crack Propagation
Crack Nucleationpstressintensification atcracktip.
Stressintensitypcrackpropagation(growth);- stage I growth onshearplanes(45),stronginfluence ofmicrostructure [Courtney: fig.12.3a]- stage II growthnormal to tensile load(90)weakinfluence ofmicrostructure [Courtney: fig.12.3b].
Crackpropagationpcatastrophic, orductile failure atcrack
lengthdependent on boundaryconditions, fracturetoughness.
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Fatigue CrackNucleation
Flaws, cracks, voidscan all act ascracknucleationsites,especially atthesurface.
Therefore, smoothsurfacesincreasethetimeto nucleation;notches, stressrisersdecrease fatigue life.
Dislocation activity(slip) can also nucleate fatiguecracks.
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Dislocation Slip CrackNucleation
Dislocationslip -> tendencyto localizeslipin bands. [seeslide10, also Courtney fig. 12.3]
Persistent Slip Bands(PSBs) characteristic ofcyclicstrains.
Slip Bands -> extrusion at freesurface. [seenextslide forfig.from Murakamiet al.] Extrusions -> intrusions andcracknucleation.
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Slip steps
and thestress-strain
loop
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18Design Philosophy:Damage Tolerant
Design
S-N (stress-cycles) curves = basiccharacterization.
Old Design Philosophy = InfiniteLifedesign: acceptempirical information about fatigue life(S-N curves); apply a(large!) safety factor; retirecomponents orassemblies atthe
pre-set life limit, e.g. Nf=107. *CrackGrowth Ratecharacterization ->
*Modern Design Philosophy(AirForce, not Navycarriers!) =DamageTolerantdesign: acceptpresence ofcracksin
components. Determine life based onprediction ofcrackgrowthrate.
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Definitions: StressRatios
Alternating Stress
Meanstress| Wm = (Wmax +Wmin)/2.
Puresine wave|Meanstress=0.
Stressratio | R= Wmax/Wmin.
ForWm = 0, R=-1
Amplituderatio|
A = (1-R)/(1+R). Statistical approachshowssignificantdistributioninNf forgivenstress.
See Courtney fig. 12.6; also followingslide.
| Wa
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AlternatingStressDiagrams
[Dieter]
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Mean Stress
Alternatingstress| Wa = (Wmax-Wmin)/2. Raisingthemeanstress (Wm) decreasesNf. [seeslide19, also
Courtneyfig. 12.9]
Variousrelations between R = 0 limit andtheultimate (or
yield) stress areknown as Soderberg (linearto yieldstress),Goodman (linearto ultimate) andGerber(parabolictoultimate). [Courtney, fig. 12.10, problem12.3]
Wa
Wmeantensile strength
endurance limit at zero mean stress
Wa ! Wfat 1 Wmean
tensile strength
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Cyclic strain vs. cyclic stress
Cyclicstraincontrol complementscyclicstresscharacterization: applicableto thermal fatigue, orfixeddisplacementconditions.
Cyclicstress-straintestingdefined by a controlledstrainrange, Ipl. [seenextslide, Courtney, figs. 12.24,12.25]
Soft, annealed metalstendto harden; strengthenedmetalstendto soften.
Thus, many materialstendtowards a fixedcycle, i.e.constantstress, strain amplitudes.
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Cyclic stress-strain curve
[Courtney]
Largenumberofcyclestypicallyneededto reachasymptotichysteresis loop(~100).
Softening orhardeningpossible. [fig. 12.26]
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Cyclic stress-strain
Wavy-slip materialsgenerallyreach asymptoteincyclicstress-strain: planarslipmaterials(e.g. brass) exhibithistorydependence.
Cyclicstress-straincurvedefined bytheextrema, i.e.the tips ofthehysteresisloops. [Courtney fig. 12.27]
Cyclicstress-straincurvestendto lie below those for
monotonictensiletests. Polymerstendto softenin
cyclicstraining.
[Courtney]
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Cyclic Strain Control
Strainis a more logical independentvariable forcharacterization of fatigue. [fig. 12.11]
Define anelasticstrainrange as Iel = W/E.
Define a plasticstrainrange, Ipl. Typically observe a changeinslope betweenthe
elastic andplasticregimes. [fig. 12.12]
Low cycle fatigue(small Nf) dominated byplasticstrain: highcycle fatigue(largeNf) dominated byelasticstrain.
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Strain control
of fatigue
[Courtney]
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Cyclic Strain control: low cycle
Constitutiverelationforcyclicstress-strain:
n 0.1-0.2
Fatigue life: CoffinMansonrelation:
If
~true fracturestrain; closeto tensileductility
c -0.5to -0.7 c = -1/(1+5n); largenp longerlife.
( ! dK (I dn
(I
2! dIf 2 f
c
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Cyclic Strain control: high cycle
Forelastic-dominatedstrainsathighcycles, adaptBasquinsequation:
Intercept onstrain axis ofextrapolatedelastic line = Wf/E. Highcycle = elasticstraincontrol:
slope(inelasticregime) = b = -n/(1+5n)[Courtney, fig. 12.13]
Thehighcycle fatiguestrength, Wf, scaleswiththeyieldstress highstrengthgoodinhigh-cycle
Wa ! E(Ie2
! dWf 2 b
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Strain amplitude - cycles
[Courtney]
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Total strain (plastic+elastic) life
Low cycle = plasticcontrol: slope = c
Addtheelastic andplasticstrains.
Cross-overbetweenelastic andplasticcontrol istypically atNf= 103 cycles.
Ductilityuseful forlow-cycle; strengthforhighcycle
Examples ofMaragingsteel forhighcycleendurance,annealed4340 forlow cyclefatiguestrength.
(
2
!(Iel
2
(Ipl
2
!f2 f
b dIf 2Nf
c
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Fatigue Crack Propagation
CrackLength := a.Numberofcycles := NCrackGrowth Rate := da/dNAmplitude of Stress Intensity := K= Wc.
Definethreestages ofcrackgrowth, I, II and III,
in a plot of da/dN versus K. Stage II crackgrowth: application of linearelastic fracture mechanics.
Canconsiderthecrackgrowthrateto berelatedto the appliedstressintensity.
Crackgrowthratesomewhatinsensitiveto R (if R
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Fatigue Crack Propagation
Threestages ofcrackgrowth, I, II and III.
Stage I: transitionto afinitecrackgrowthratefrom no propagationbelow a thresholdvalue ofK.
Stage II: powerlawdependence ofcrackgrowthrate on K.
Stage III: acceleration of
growthrate with K,approachingcatastrophicfracture.
da/dN
th
c
I
IIIII
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*Paris Law
ParisLaw:
m~ 3 (steel); m~4(aluminum).
Cracknucleationignored! Threshold~ Stage I Thethresholdrepresents anendurance limit.
Forceramics, thresholdiscloseto KIC. Crackgrowthrateincreases withR (forR>0).
[fig. 12.18a]
dc
d! A((K)m
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*Striations- mechanism
Striations occurbydevelopment ofslip bandsineachcycle, followed bytip blunting, followed byclosure.
Canintegratethegrowthrateto obtaincycles asrelatedto cyclicstress-strain behavior. [Eqs. 12.6-12.8]
NII !dc
AEm (W c mc0
cf
NII !dc
dc / dNc0
cf
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*Striations, contd.
Providedthat m>2 andEisconstant, canintegrate.
Iftheinitial crack lengthis much lessthanthe final length,c0
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*Damage TolerantDesign
Calculateexpectedgrowthrates from dc/dN data. Perform NDE on all flight-critical components.
Ifcrackis found, calculatetheexpected life ofthe
component. Replace, rebuildiftoo closeto life limit.
Endurance limits.
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Geometrical effects
Notchesdecrease fatigue lifethroughstressconcentration. Increasingspecimensize lowers fatigue life. Surfaceroughness lowers life, againthroughstress
concentration.
Moderatecompressivestress atthesurfaceincreases life(shotpeening); itisharderto nucleate a crack whenthelocal stressstate opposescrack opening.
Corrosiveenvironment lowers life; corrosioneitherincreasestherate at which material isremoved from the
cracktip and/oritproduces material onthecracksurfacesthat forcesthecrack open(e.g. oxidation). Failure mechanisms
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Microstructure-FatigueRelationships
What aretheimportantissuesin microstructure-fatiguerelationships?
Answer: three majorfactors.1: geometry ofthespecimen(previousslide); anything onthesurface
thatis a site ofstressconcentration will promotecrack formation(shortenthetimerequired fornucleation ofcracks).
2: defectsinthe material; anythinginsidethe material thatcanreducethestress and/orstrainrequiredto nucleate a crack(shortenthetimerequired fornucleation ofcracks).
3: dislocationslipcharacteristics; ifdislocationglideisconfinedtoparticularslipplanes(calledplanarslip) thendislocationscanpileup at anygrain boundary orphase boundary. Thehead ofthepile-upis a stressconcentration whichcaninitiate a crack.
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Microstructure affects CrackNucleation
The maineffect ofmicrostructure(defects,surfacetreatment, etc.) isalmost all inthe low stressintensityregime, i.e. StageI. Defects, forexample,
makeiteasierto nucleatea crack, whichtranslatesinto a lowerthreshold forcrackpropagation(Kth).
Micr ostructure also affectsfracturetoughness andtherefore Stage III.
da/dN
th
c
I
IIIII
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Defects in Materials
Descriptions ofdefectsin materials atthesophomore level focuses,appropriately onintrinsicdefects(vacancies, dislocations). Forthematerialsengineer, however, defectsincludeextrinsicdefectssuch asvoids, inclusions, grain boundary films, and othertypes ofundesirablesecondphases.
Voids areintroducedeitherbygasevolutioninsolidification orbyincompletesinteringinpowderconsolidation.
Inclusions aresecondphasesentrainedin a material duringsolidification. In metals, inclusions aregenerally oxides from thesurfaceofthe metal melt, ora slag.
Grain boundary films arecommoninceramics asglassy films from
impurities. In aluminum alloys, thereis a hierachy ofnames forsecondphaseparticles; inclusions areunwanted oxides(e.g. Al2O3); dispersoids areintermetallicparticlesthat, onceprecipitated, arethermodynamicallystable(e.g. AlFeSicompounds); precipitates areintermetallicparticlesthatcan bedissolved orprecipiateddepending ontemperature(e.g.
AlCucompounds).
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Metallurgical Control: fine particles
Tendencyto localization of flow isdeleteriousto theinitiation of fatiguecracks, e.g. Al-7050 withnon-shearablevs. shearableprecipitates(Stage I in a da/dNplot). Also Al-Cu-Mg withshearableprecipitates butnon-shearable
dispersoids, vs. onlyshearableppts.
graph courtesy of J.
Staley,Alcoa
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Coarse particle effect on fatigue
Inclusionsnucleatecrackspcleanliness(w.r.t. coarseparticles) improves fatigue life, e.g. 7475improved by lowerFe+Sicomparedto 7075:0.12Fein 7475, comparedto 0.5Fein 7075;
0.1Siin 7475, comparedto 0.4Siin 7075.
graph courtesy of J.
Staley,Alcoa
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Alloy steel heat treatment
Increasinghardnesstendsto raisetheendurance limit forhighcycle fatigue. Thisis largely a function oftheresistanceto fatiguecrack formation(Stage I in a plot ofda/dN).
[Dieter]
Mobilesolutesthatpindislocationspfatiguelimit, e.g. carbon in steel
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Casting porosity affects fatigue
Castingtendsto resultinporosity. Pores areeffectivesitesfornucleation offatigue cracks. Castingsthustendto have lowerfatigueresistance(asmeasured by S-N curves) than wrought materials.
Castingtechnologies, such assqueeze casting, thatreduceporositytendtoeliminatethisdifference.
[Polmear]
Gravity castversussqueeze castversus
wroughtAl-7010
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Titanium alloys
FormanyTi alloys, theproportion ofhcp(alpha) and bcc(beta) phasesdepends
strongly ontheheattreatment. Cooling from thetwo-phaseregionresultsin a two-phasestructure, as Polmearsexample, 6.7a. Rapidcooling from abovethetransusinthesinglephase(beta) regionresultsin a two-phase microstructure with Widmanstttenlaths of(martensitic) alpha in a beta matrix, 6.7b.
The fatigueproperties ofthetwo-phasestructure aresignificantly betterthantheWidmanstttenstructure(moreresistanceto fatiguecrack formation).
The alloyinthisexampleis IM834, Ti-5.5Al-4Sn-4Zr-0.3Mo-1Nb-0.35Si-0.6C.
[Polmear]
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*Design Considerations
Ifcrackgrowthrates arenormalized bytheelastic modulus,then material dependenceis mostlyremoved![Courtney fig.12.20]
Candistinguish betweenintrinsic fatigue [use Eq. 12.4 for
combinedelastic, plasticstrainrange] forsmall cracksizesandextrinsic fatigue [use Eq. 12.6 forcrackgrowthratecontrolled] at longercrack lengths. [fig. 12.21.]
Inspection ofdesigncharts, fig. 12.22, showsthatceramicssensitiveto crackpropagation(highendurance limitinrelationto fatiguethreshold).
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*Design Considerations: 2
Metalsshow a higherfatiguethresholdinrelationtotheirendurance limit. PMMA andMg are atthelowerend ofthetoughnessrangeintheirclass.[Courtney fig. 12.22]
Also interestingto compare fracturetoughness withfatiguethreshold. [Courtney fig. 12.23]
Notethatceramics are almost onratio=1 line,
whereas metalstendto lie well below, i.e. fatigueismoresignificantcriterion.
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*Fatigue
property map
[Courtney]
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*Fatigue
property map
[Courtney]
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*Variable Stress/Strain Histories
Whenthestress/strainhistoryisstochasticallyvarying, a rule forcombiningportions of fatigue lifeisneeded.
Palmgren-MinerRuleisuseful: ni isthenumberofcycles ateachstress level, and Nfi isthe failurepoint forthatstress.[Ex. Problem 12.2]
ni
Nfi! 1
i
* Courtneys Eq. 12.9isconfusing; hehas Nfinthenumeratoralso
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*Fatigue in Polymers
Manydifferences from metals
Cyclicstress-strain behavioroftenexhibitssoftening; also affected byvisco-elasticeffects;
crazinginthetensileportionproducesasymmetries, figs. 12.34, 12.25.
S-N curvesexhibitthreeregions, withsteeplydecreasingregion II, fig. 12.31.
Nearnessto Tg resultsinstrongtemperaturesensitivity, fig. 12.42
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Fatigue: summary
Critical to practical use ofstructural materials. Fatigue affects moststructural components, even
apparentlystatically loaded ones.
Well characterizedempirically. Connection betweendislocation behaviorand
fatigue life offersexcitingresearch opportunities,i.e. physically based models are lacking!