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SMITH ANALYTICAL, LLC

PO Box 278 Seabrook, Texas 77580‐0278 (281) 667‐6463 www.SmithAnalytical.com

2018 PROCESS ANALYZER TRAINING CATALOG

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Overview Analyzer technicians are highly skilled technologists that install, calibrate and maintain some of the most sophisticated instrumentation in the world. Analyzers are used in all types of refining, petrochemical and manufacturing industries, and are valuable for the control of processes and environmental compliance. Most analyzer technicians start out as instrumentation technicians who, because of their aptitude and attitude, have moved to a higher level of technology.

There is a shortage of analyzer technicians throughout the United States and abroad, and the shortage will only increase as many analyzer technicians retire in the next five to ten years. Analyzer technicians enjoy excellent a starting salaries and with experience, have the potential to earn annual salaries exceeding $100,000 per year.

The analyzer training programs offered by Smith Analytical, LLC are designed to provide the highest level of insight into the subject matter being presented.

Why Use Smith Analytical, LLC For Your Process Analyzer Training Needs?

Smith Analytical, LLC was founded for the sole purpose of providing value added products and services to the hydrocarbon processing industry. During the past thirty six years, the staff of Smith Analytical, LLC has conducted hundreds of training programs covering analytical instrumentation in the US, Far East, Middle East, Canada, China, Europe and Africa.

The Smith Analytical, LLC Instruction Staff

The Instruction Staff at Smith Analytical, LLC has years of hands-on, practical experience with all aspects of analytical instrumentation. Unlike Instructors that other organizations may employ, our training staff is regularly involved in all aspects analytical technology, to ensure that we can convey in a practical manner, the information our Student / Client needs to know. All Instructors have 10+ years of engineering, project, or field experience and are considered industry experts in their field of study.

Where Will The Class Be Held?

Training programs can either be conducted at the offices of Smith Analytical, LLC located at 5318 FM 517 West, Alvin, Texas or at your plant site.

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What is the Minimum and Maximum Class Size?

This will vary from program to program, but as a rule, the minimum class size is 3 students for most courses and the maximum is 10 students. Smith Analytical, LLC will rarely conduct training programs with more than 10 students, as this does not allow enough time for individual questions or hands-on, that is an essential part of all programs.

What Does the Course Fee Cover?

The course fee includes attendance to the course and training materials. All courses attended at the offices of Smith Analytical also include a daily continental breakfast and lunch every day of the course.

How Can I Register For a Training Class?

This can be done on-line (www.smithanalytical.com) or by calling Smith Analytical at (281) 667-6463. Smith Analytical accepts PO’s and Credit Cards for payment.

SMITH ANALYTICAL TRAINING FACILITY FM 517, ALVIN, TEXAS

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Owners and Principals of Smith Analytical, LLC

The Owners and Principals of Smith Analytical have over 100 years of experience in the field of process analytical instrumentation. We pride ourselves on providing our Clients with an exceptional service experience.

Steve Smith – Owner, Consultant and Sr. Instructor

Thirty-seven years working in the field of analytical instrumentation in a variety of positions. Of this time, twenty years handling day to day operations for three different analyzer organizations Steve has owned or held ownership interest in. Steve is the founder of Advanced Analytical Solutions, LLC (1993-1997) and most recently Smith Analytical, LLC (2012 – Current). Prior to the sale of Process Analytical Applications, Inc. (PAAI) to Cameron in 2008, Steve had ownership interest in PAAI. Steve had been directly involved in handling over $125M USD in analytical projects, in addition to twenty-five years of experience teaching analytical instrumentation courses at the college level and to Clients all over the world. Steve can be reached at (281) 667-6463 or [email protected]

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Annie Crabtree-Smith – Owner and Sales Manager Sixteen years of technical and sales experience working in the oil, gas, chemical and refining sector supporting process analytical equipment sales. Annie is the former Owner of Alliance Business Services (1997-2003), Process Analytical Sales (2007-2008) and was one of the Owners of Process Analytical Applications, Inc (PAAI). After the sale of PAAI to Cameron, Annie served at the Sales Manager first for Cameron Process Analytics and then Horiba Instruments Incorporated. Annie can be reached at (832) 275-5298 or [email protected]

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Justin Smith – Sr. Analyzer Specialist

Associates degree in Chemistry and Business Management. Ten years of experience working with process analyzers, sample systems and the ancillary equipment for these systems in both chemical plant and refinery settings. Proficient in numerous types of analytical equipment including; ABB Magnos and UrasAmetek 900,910,921 Sulfur Analyzer Ametek WDG IV, Applied Automation Gas Chromatographs Siemens Maxum I and II, Thermo ccientific SOLA I and II Rosemount Oxymitter 4000, Rosemount pH, ORP, DO, and Conductivity, GE, Panametrics hydrogen, oxygen, and moisture, Horiba, Enda 7000, Yokogawa Gas Chromatographs, Sick Maihak GM 31,32, 35, Flow Sic systems, Mettler Toledo, and Optical Scientific flow meters. Well versed in analytical software and Data acquisition software including Maxum EZchrom, Portal and system manager, APC, Aspen and PI trending software, Vivicom Data acquisition systems Works daily with EPA regulations regarding CEMS analyzers, downtime and uptime.

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Bob Scraper – Sr. Instructor / Analyzer Specialist

Has worked in the petro-chemical industry for over 30 years for most of the major companies in the US and many abroad maintaining online Gas Chromatographs and continuous type analyzers. Especially skilled at training technicians in the use of sample systems, Siemens/AAI GCs, ABB GCs, Yokogawa GCs and Rosemount/Daniels analyzers.

Mark O’Pry – Sr. Instructor / Analyzer Specialist

A.A.S. Degree in Instrumentation, Lee College, Baytown TX. Completed A.A.S analyzer training levels I, II, and III. These classes include Chemistry, Process Analyzer Fundamentals, Sample Systems, Basic Chromatography, ABB Extrel Mass Spec, Continuous Emissions Monitoring Systems and Advanced Chromatography. Manufacturer certified for Prima Mass Spectrometers, Siemens Advanced Optichrom Operation and Maintenance / Chromatography Technology, Compur Monitox and Statox Monitors, Ametek Photometric UV Analyzers, Sola II Total Sulfur, ABB Magnos-Limas-Uras, Honeywell Cirrus Version 6, Thermo 42I and 48I, Triconex PLC, Rosemount Smart Transmitters, Nuclear gauge certified, Fisher Digital Valves Yokogawa Analyzer Best Practices and Honeywell Systems Operations.

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TABLE OF CONTENTS

Technical Training Ladder Pg. 9

2018 Training Priced Training Schedule Pg. 12

Ametek WDG-IV Oxygen Analyzer Syllabus Pg. 16

Analyzer Communications and Network Syllabus Pg. 19

Basic Chemistry Course Syllabus Pg. 23

Basic Gas Chromatograph Syllabus Pg. 27

Continuous Emissions Monitoring Systems Course Syllabus Pg. 31

Advanced Gas Chromatograph Troubleshooting Syllabus Pg. 35

Practical Gas Chromatograph Skills Syllabus Pg. 39

Gas Detection Training and Self Certification Pg. 44

Analyzer Key Performance Indicator Syllabus Pg. 47

Process Analyzer Engineering Course Syllabus Pg. 52

Process Analyzer Fundamentals Course Syllabus Pg. 56

Process Sample System Theory and Maintenance Syllabus Pg. 60

Practical Skills Sample System Syllabus Pg. 66

Siemens Advance Gas Chromatograph Syllabus Pg. 70

Siemens Maxum Gas Chromatograph Syllabus Pg. 74

Thermo-Scientific Model 42i and 48i Analyzer Training Pg. 78

Analyzer Certification Level 2 Syllabus Pg. 81

Analyzer Certification Level 1 Syllabus Pg. 82

Map to Smith Analytical and Area Hotels Pg. 83

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Training Progression Plan

The following is the recommend training track for companies who plan on using Smith Analytical, LLC to provide training services to their staff. There are currently two training tracks. One is designed for Analyzer Professionals (Engineers, Designers or Environmental Professionals) and the second is for Analyzer Technicians who are looking to gain additional insight into this discipline.

ANALYZER PROFESSIONAL TRAINING LADDER

Analyzer Engineer /Designer /

Environmental Professional Basic Chemistry – BC-101 Sample System – PSS- 101

Process Analyzer Fundamentals – PAF- 101

Analyzer Project Management & Engineering – PAE- 101

Analyzer Communication – AC-101

Key Performance Indicators –PAE-103 CEMS Training – CEMS-101

Advanced Sample Systems – PSS-102

Advanced GC Troubleshooting – GC-102 or Practical Skills GC

Training-GC-103

Advanced Analyzer Project Management & Engineering –

PAE- 102

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ANALYZER TECHNICIAN TRAINING LADDER

Analyzer Technician Basic Chemistry – BC-101 Sample System – PSS-101

Process Analyzer Fundamentals – PAF-101

Basic Chromatography – GC-101

Analyzer Communication – AC-101

Key Performance Indicators –PAE-103

CEMS Training – CEMS-101

TCEQ Reg 115 Cooling Tower and Flare Monitoring System

Training – CEMS 102

Advanced GC Troubleshooting –GC-102

Practical GC Skills – GC-103

GC Practical Skills Training –GC-103

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Note:

1. Students should be Level 3 proficient in English. Level 3 includes the student understands and

speaks conversational and academic English with decreasing hesitancy and difficulty. The

student is post‐emergent, developing reading comprehension and writing skills in English. The

students English literacy skills allow the student to demonstrate academic knowledge in content

areas with assistance.

2. Students should have at least a High School education

3. Students should have good math skills

4. Students should have a basic understanding or knowledge with basic test equipment including

flow meters and digital volt meters

5. Students must have basic PC skills

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PO Box 278 Seabrook, Texas 77580‐0278 (281) 667‐6463 www.SmithAnalytical.com 2018 TRAINING SCHEDULE

CLASS INSTRUCTOR START END PRICING PER

STUDENT

AMETEK WDG-IV TRAINING (2 DAY CLASS)

SMITH CALL FOR INFO

CALL FOR INFO

$1,000.00

ANALYZER COMMINICATIONS (AC-101)

ARNOLD CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

BASIC CHEMISTRY (BC-101)

SMITH 2-6-2018 2-8-2018 $1,450.00


SMITH 6-5-2018 6-7-2018 $1,450.00


SMITH 9-18-2018 9-20-2018 $1,450.00

BASIC GAS CHROMATOGRAPHY TRAINING (BGC-101)

SMITH OR SCRAPER

3-6-2018 3-8-2018 $1,450.00


SMITH OR SCRAPER

6-12-2018 6-14-2018 $1,450.00


SMITH OR SCRAPER

10-16-2018 10-18-2018 $1,450.00

CONTINUOUS EMISSIONS MONITORING SYSTEM TRAINING COURSE – (CEMS 101)

SMITH OR SCRAPER

4-3-2018 4-5-2018 $1,450.00


SMITH OR SCRAPER

11-7-2018 11-8-2018 $1,450.00

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2018 TRAINING SCHEDULE


STUDENT GAS CHROMATOGRAPH TROUBLESHOOTING TRAINING COURSE – (GC-102)

SCRAPER, O’PRY OR

SMITH

4-9-2018

4-12-2018

$1,750.00

GAS CHROMATOGRAPH TROUBLESHOOTING TRAINING COURSE – (GC-102)

SCRAPER, O’PRY OR

SMITH

11-12-2018

11-14-2018

$1,750.00

GAS CHROMATOGRAPH PRACTICAL SKILL TRAINING COURSE – (GC-103)

SCRAPER, O’PRY OR

SMITH

4--16-2018 4-19-2018 $1,450.00

GAS CHROMATOGRAPH PRACTICAL SKILL TRAINING COURSE – (GC-103)

SCRAPER, O’PRY OR

SMITH

10-15-2018 10-18-2018 $1,450.00

GAS DETECTION FUNDAMENTALS (GD-101)

SMITH 2-28-2018 2-29-2018 $1,000.00

GAS DETECTION FUNDAMENTALS (GD-101)

SCRAPER, O’PRY OR

SMITH

9-12-2018 9-13-2018 $1,000.00

KEY PERFORMANCE INDICATORS

CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

PROCESS ANALYZER ENGINEERING TRAINING COURSE (PAE-101)

SMITH CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

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PO Box 278 Seabrook, Texas 77580‐0278 (281) 667‐6463 www.SmithAnalytical.com 2018 TRAINING SCHEDULE


STUDENT PROCESS ANALYZER FUNDAMENTALS TRAINING COURSE – (PAF-101)

SMITH 4-23-2018 4-26-2018 $1,750.00

PROCESS ANALYZER FUNDAMENTALS TRAINING COURSE – (PAF-101)

SMITH 12-3-2018 12-6-2018 $1,750.00

SAMPLE SYSTEM MAINTENANCE (PSS-101)

SMITH OR SCRAPER

2-20-2018 2-22-2018 $1,450.00


SMITH OR SCRAPER

6-19-2018 6-21-2018 $1,450.00


SMITH OR SCRAPER

10-2-2018 10-4-2018 $1,450.00

SAMPLE SYSTEM PRACTICAL SKILL TRAINING COURSE – (PSS-102)

SMITH OR SCRAPER

CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

SIEMENS ADVANCE GC TRAINING 4 DAY COURSE (SA-101)

SMITH OR SCRAPER

5-7-2018 5-10-2018 $2,450

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2018 TRAINING SCHEDULE


STUDENT SIEMENS MAXUM TRAINING (SM-101)

SCRAPER, O’PRY OR

SMITH

3-19-2018 3-22-2018 $1,750.00

SIEMENS MAXUM TRAINING (SM-101)

SCRAPER, O’PRY OR

SMITH

5-21-2018 5-24-2018 $1,750.00

SIEMENS MAXUM TRAINING (SM-101)

SCRAPER, O’PRY OR

SMITH

10-22-2018

10-25-2018

$1,750.00

THERMOX 42I NOX AND 48I CO ANALYZER TRAINING (MIN CLASS SIZE 4)

SCRAPER, O’PRY OR

SMITH

5-15-2018 5-16-2018 $1,750.00

THERMOX 42I NOX AND 48I CO ANALYZER TRAINING (MIN CLASS SIZE 4)

SCRAPER, O’PRY OR

SMITH

9-12-2018 9-13-2018 $1,750.00

ANALYZER TECHNICIAN LEVEL 1 CERTIFICATION (ATL1C)

CALL FOR INFO CALL FOR INFO

CALL FOR INFO

CALL FOR INFO


CALL FOR INFO CALL FOR INFO

CALL FOR INFO

CALL FOR INFO

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AMETEK WDG-IV OXYGEN ANALYZER

TRAINING COURSE

PURPOSE

The purpose of the Ametek WDG-IV Training Course is to cover fundamental concepts of oxygen in gas measurement, overview of the Ametek WDG-IV, software overview of the Ametek WDG-IV, calibration and hands-on labs with this analyzer.

AUDIENCE

The course is designed for engineers or analyzer technicians who are seeking a better understanding of high temperature zirconia oxygen measurements, the WDG-IV Analyzer and how to approach specific problems when dealing with this technology.

COURSE OBJECTIVES

1. Introduce participants to fundamentals of oxygen in gas measurement. 2. Review Ametek WDG-IV hardware. 3. Review of Ametek WDG-IV software and User Parameters. 4. Calibration of the WDG-IV Oxygen Analyzer. 5. Troubleshooting the WDG-IV Oxygen Analyzer. 6. Help participants develop a better understanding of how this information is used to

maintain and troubleshoot the equipment.

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METHODOLOGY

The training approach is based on principles of adult learning with a focus on peer review during all the steps of the training/learning event. The course models a variety of effective training methodologies including demonstration, practice, discussion, brain-storming, buzz groups, case studies, visualization and presentation. Once students have gained the concepts explained and demonstrated in this class, they can begin to apply their knowledge when maintaining or troubleshooting sample conditioning systems.

STRUCUTRE: 7 sessions, labs, a baseline exam and final exam

MATERIALS AND TOOLS: Each session includes an introduction, learning objectives, participatory methodologies, and activities. A pre/post course assessment and peer feedback form on practice sessions are included.

TIME: 16 hours technical content.

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Training Detail

During the one week course there are a total of 15 Training Sessions. The following is the material which

will be covered in each session.

Session 1 – Overview of Oxygen in Gas Measurement

• Paramagnetic measurement

• High Temperature Zirconia measurement

Session 2 – Analyzer Hardware Overview

• Ametek WDG‐IV hardware overview

• Combustible and Methane Detector overview

Session 3 – Analyzer Software Overview

• Entering User defined parameters

Session 4 – Analyzer Calibration Lab‐#1

• Students will be required to calibrate the analyzer using Low and High Standard O2 Gas (20.95%)

Session 5 – – Analyzer Calibration Lab‐#2

• Students will be required to calibrate the analyzer using Low and High Standard O2 Gas (10.00%

Session 6 – Analyzer Troubleshooting Lab‐#1

• Troubleshooting 101 and ways to make fault finding more efficient

Session 7 – Analyzer Troubleshooting Lab 2

• Lab 2 – Troubleshooting Lab. The Instructor will introduce several problems into the equipment

(hardware and software) which must be corrected. Students must identify the problems with

the analyzer.

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ANALYZER COMMUNICATIONS

TRAINING COURSE

PURPOSE

The purpose of the Analyzer Communications Training Course is to cover fundamental concepts of analyzer networks and communication protocols used to transmit measurement data to a distributive control system (DCS) or programmable logic controller (PLC).

AUDIENCE

The course is designed for engineers or analyzer specialist who are seeking a better understanding of analyzer communications, networks and how to approach specific problems when dealing with this technology.

COURSE OBJECTIVES

7. Introduce participants to fundamentals of communication networks. 8. Review various types of communication protocols. 9. Number Systems used in computers. 10. Details for some of the common Protocols. 11. Help participants develop a better understanding of how this information is used to


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METHODOLOGY





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Training Detail



Session 1 – Overview of Analyzer Communications

• History of communication, leading up to digital communication

Session 2 – Analyzer Communications Part 1

• OSI 7 Layer Model (Overview then detail)


• Introduction to Physical Layer (RS232, 485, Fiber Optics, etc)


• Introduction to protocols and the OSI layers they represent (Modbus, Profibus, Foundation

Fieldbus)

Session 5 – Analyzer Communications Lab 1

• Lab 1 – Generation of Modbus Addresses. Students are required to develop various Modbus

map addresses which will contain specific analytical data.


• Review Lab 1



• Lab 2 – Troubleshooting Lab. Students will be presented with a analyzer communications

drawing and a Modbus map and must identify the problems with the proposed system.


• Lab 2 Review

• Number Systems used in computers (Binary, Hex & conversion between each base)

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• Lab 3 – Students are required to demonstrate they understand and can properly convert Binary

and Hexadecimal numbers


• Lab 3 Review

• Detailed setup of a Honeywell Experion Modbus link (Ethernet and Serial)


• Lab 4 – Using hardware provided as part of the class, Students working in groups must

demonstrate basic understanding of analyzer communications.

Session 12 – Analyzer Communications Fundamentals Part 7

• Lab 4 Review

• Details of common Physical layer component

• Setup of a communications link demo (Kepware to Phoenix Contact bus module. Wonderware

as an HMI)


• Sniffing the communication link with Wireshark

• Deconstruct the network packet to show the encapsulated Modbus Information


• Detailed setup of a n AB PLC to communicate Modbus


• Review of Real World Problems Raised by the Class

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BASIC ANALYZER CHEMISTRY

TRAINING COURSE – (BC-101)

PURPOSE

The purpose of the Process Analyzer Chemistry Training Course is to strengthen the understanding of those individuals who work with or support process analyzers on a daily basis.

AUDIENCE

The course is designed for individuals who work with process sample conditioning systems and analyzers. This course is designed for lab and analyzer technicians and other process analyzer professionals seeking a better understanding or refresher course in basic chemistry.

BASIC CHEMISTRY COURSE OBJECTIVES

1. Introduce participants to principles and concepts of basic chemistry. 2. Develop participants’ capacity to read and understand basic chemical equations. 3. Equip participants with knowledge so they understand empirical formulas and can draw

molecules in long hand structure. 4. Identify how basic chemistry concepts apply to process sample conditioning systems and

analyzers. 5. Help participants develop a better understanding of how this information is used in their

daily task.

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METHODOLOGY

The training approach is based on principles of adult learning with a focus on peer review during all the steps of the training/learning event. The course models a variety of effective training methodologies including demonstration, practice, discussion, brain-storming, buzz groups, case studies, visualization and presentation. Once students have gained an understanding of inorganic and organic chemistry, they can begin to apply their knowledge to learning the methods used in chemical analysis. Among these are spectroscopy, gas chromatography, continuous analyzers and sample conditioning systems.

STRUCUTRE: Formal training sessions which also include a baseline and final exam.


TIME: Twenty-four (24) hours technical content presented in the formal training session.

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Basic Chemistry Training Detail – (BC-101)

During the one week Basic Chemistry Training Course, there are a total of 15 Training Sessions. The

following is the material which will be covered in each session.

Session 1 – Basic Chemistry Part 1

• Explanation on the Role of Basic Chemistry as it Relates to Process Analyzers


• Atom Symbols

• Chemical Formula


• Atomic Structure

• Energy and Bond Formation


• Molecular Geometry and Polarity

• The Octet Rule

• Properties of Ionic and Covalent Compounds


• Chemical Equilibrium

• Common Charges

• Mole and Formula Weights


• Calibration Standards (Liquid Volume, Weight Percent, Mole Percent)

• Making up solutions / Concentration

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• Alkanes


• Unsaturated Hydrocarbons


• Aromatics

• Isomers


• Alcohols, Phenols and Ethers

• Aldehydes and Ketones

• Carboxylic acids and Esters

• Amines and Amides


• Acids and Bases

• Activity and Ionic Strength


• Alkane Covalent Compounds Naming


• Alkene Covalent Compounds Naming


• Alkyne Covalent Compounds Naming


• Physical Properties

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BASIC CHROMATOGRAPHY TRAINING COURSE (BGC-101)

PURPOSE

The purpose of the Basic Chromatography Training Course is to strengthen the understanding of those individuals who work with or support process gas chromatograph analyzers.

AUDIENCE

The course is designed for individuals who work with process gas chromatographs. This course is designed for engineers, supervisors and analyzer technicians seeking a better understanding of the operational theory of this technology. Students attending this training must have an understanding of basic chemistry or attended the Introduction to Basic Chemistry Training Class.

PRACTICAL CHROMATOGRAPHY COURSE OBJECTIVES

1. Introduce participants to principles and concepts of basic chromatography. 2. Develop participants’ capacity to read and understand valve diagrams. 3. Equip participants with knowledge so they understand basic operational and

troubleshooting concepts. 4. Explain the operational theory of peak integration, baseline correction and calibration. 5. Help participants develop a better understanding of how this information is used in their

daily task. 6. Demonstrate basic understanding of these concepts by using the Smith Analytical GC

Simulator Software.

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METHODOLOGY

The training approach is based on principles of adult learning with a focus on peer review during all the steps of the training/learning event. The course models a variety of effective training methodologies including demonstration, practice, discussion, brain-storming, buzz groups, case studies, visualization and presentation. Once students have gained an understanding of basic chromatography concepts, they can begin to apply their knowledge to this analysis technique.

STRUCUTRE: 15 sessions, calibration and troubleshooting labs plus a baseline and final exam


TIME: Twenty-four (24) hours technical content.

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Training Detail

During the program there are a total of 15 Training Sessions. The following is the material which will be

covered in each session.

Session 1 – Basic Chromatography Part 1

• Overview of a Gas Chromatograph


• Sample Valve Overview

• Slider, Rotor and Plunger Valves


• Column Types

• Adsorption Columns


• Absorption Columns

• Boiling Point Columns

• Polar Columns

• Capillary Columns


• Detector Overview

• Thermo Conductivity Detectors


• Flame Ionization Detectors


• Flame Photo Metric Detectors

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• Back Flush Application


• Heartcut ‐ Back Flush Application


• Peak Integration

• Calibration of a Gas Chromatograph


• Lab #1 – Perform a Basic Calibration of a Gas Chromatograph Using the Smith Analytical Peak

Simulator GC. Lab is design to test Students understanding of GC calibration.


• Lab #2 – Perform a Basic Calibration of a Gas Chromatograph Using the Smith Analytical Peak

Simulator GC. Lab is design to test Students understanding of GC calibration.


• Lab #3 – Troubleshoot the Gas Chromatograph Simulator Using the Smith Analytical GC

Simulator. Lab is design to test Students understanding on peak integration and calibration.


• Lab #4 – Troubleshoot the Gas Chromatograph Simulator Using the Smith Analytical GC

Simulator. Lab is design to test Students understanding on peak integration and calibration.


• Lab #5 – Set‐up a Method (Gate Times, Response Factors and Calibration) Using the Smith

Analytical GC Simulator. Lab is design to test Students understanding of basic GC concepts.

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PURPOSE

The purpose of the Continuous Emissions Monitoring System (CEMS) Training Course is to introduce the Student to a variety of concepts and measurement techniques used when working with stationary emissions monitoring systems. This course covers stationary systems used on furnaces, boilers, waste water discharge, cooling towers and flares.

AUDIENCE

The course is designed for analyzer engineers, supervisors, analyzer specialist, environmental or analyzer technicians who are seeking a better understanding of continuous emissions monitoring systems. Individuals attending this course should have attended the Basic Chemistry Training Course prior to taking the CEMS Course.

PROCESS SAMPLE SYSTEM, PROCESS ANALYZER FUNDAMENTAL AND ANALYZER SHELTER MAINTENANCE COURSE OBJECTIVES

1. Overview of Why CEMS Are Used. 2. Overview of stationary stack furnace or boiler CEMS. 3. Overview of stationary Waste Water CEMS. 4. Overview of stationary Cooling Tower CEMS. 5. Overview of stationary Flare CEMS. 6. Detailed explanation of the function of the hardware used in the various CEMS. 7. Detailed explanation of performance and calibration specifications. 8. CEMS Reporting requirements. 9. Help participants develop a better understanding of how this information is used when

working with process analytical instrumentation.

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METHODOLOGY


STRUCUTRE: formal training class consist of fifteen (15) sessions, and includes labs, a baseline exam and final exam.


TIME: Twenty-four (24) hours of on-line and formal class room technical content.

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Continuous Emissions Monitoring Training Detail – (CEMS 101)

During the one‐week course there are a total of 15 Training Sessions. The following is the material which


Session 1 – Overview of Why CEMS Are Used

• Discussion on Why Process CEMS Are Used and Needed

• Diluent and Pollutants

• Overview of Emissions Sources

Session 2 – CEMS Part 1

• Boiler and Furnace Stationary CEMS Overview

• Sample Probe

• Sample Line

• Sample System


• Oxygen Analyzer Measurement Theory

• Infrared Analyzer Measurement Theory


• NOx Analyzer Measurement Theory

• UV Analyzer Measurement Theory

Session 5 – CEMS Lab 1

• Lab 1 – Identify the function of the hardware used in stationary CEMS


• Review Lab 1

• Data Acquisition System

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• Overview of Cooling Tower CEMS

• Sparger Sample System Overview

• Overview of Gas Chromatograph Measurement Technique Using Flame Ionization Detection


• Overview of Flare CEMS

• Heated Sample System Overview

• Overview of Gas Chromatograph Measurement Technique Thermo Conductivity Detection


• Lab 2 – Students will be required to select analytical methods for a variety of CEMS

measurements and then review lab


• Calibration Requirements

• Seven Day Drift Test

• EPA Performance Specification 9

• Quarterly Cylinder Gas Audits

• Annual RATA


• Data Reporting Requirements


• Lab 3 – Students will have to demonstrate they can read and properly identify common

hardware found in any CEMS. Additionally, the lab will require Students to identify reasons why

particular problems with any of the CEMS covered in this course may occur

• Open Discussion

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GAS CHROMATOGRAPH TROUBLESHOOTING

TRAINING COURSE – (GC-102)

PURPOSE

The purpose of the Gas Chromatograph Troubleshooting Training Course is to cover fundamental and advanced concepts of gas chromatograph troubleshooting.

AUDIENCE

The course is designed for analyzer specialist or analyzer technicians who are seeking a better understanding or want to develop additional gas chromatograph troubleshooting skills. Individuals attending this course must have five plus years of experience working with gas chromatographs. Recommended classes before taking this course include Basic Chemistry and Basic Chromatography or Practical Skills Gas Chromatograph Training Programs. This is not an entry level course.

GAS CHROMATOGRAPH TROUBLESHOOTING COURSE OBJECTIVES

1. Basic Chromatography Review. 2. Troubleshooting various hardware components of a gas chromatograph. 3. Baseline correction methods. 4. Explanation and demonstration of peak integration. 5. Explanation and demonstration of converting peak integration into a concentration 6. Help participants develop a better understanding of how this information is used to


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METHODOLOGY





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Advanced Gas Chromatograph Troubleshooting Training Detail – (GC-102)



Session 1 – Basic Chromatography Review

• Review of Basic Chromatography

Session 2 – Gas Chromatograph Troubleshooting Part 1

• Integration and Baseline Correction


• Troubleshooting Sample and Column Valves


• Troubleshooting Packed and Capillary Columns

Session 5 – Gas Chromatograph Troubleshooting Lab 1

• Lab 1 – Identify possible reasons for problem seen with chromatograms presented for this lab

exercise


• Review Lab 1

• Detector Overview

• Thermo Conductivity Detector (TCD) Overview and Troubleshooting


• Lab 2 – Troubleshooting Lab. Students will be presented with TCD troubleshooting exercise in

this lab


• Lab 2 Review

• Flame Ionization Detector (FID) Overview and Troubleshooting

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• Lab 3 – Troubleshooting Lab. Students will be presented with FID troubleshooting exercise in

this lab


• Lab 3 Review

• Flame Photometric Detector (FPD) Overview and Troubleshooting


• Lab 4 – Students will be required to troubleshoot an analytical method using the Smith

Analytical Gas Chromatograph Simulator Software


• Lab 4 Review

• Iso‐Thermal and Programmable Ovens

• Affect of Carrier Pressure and Temperature


• Typical Gas Chromatograph Applications

• Back Flush Application

• Heartcut‐Back Flush Application


• Lab 5 – Students will be required to demonstrate they understand how to read and troubleshoot

using a GC valve diagram


• Lab 5 Review

• Open Discussion

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GAS CHROMATOGRAPH PRACTICAL SKILL

TRAINING COURSE – (GC-103)

PURPOSE

The purpose of the Gas Chromatograph Troubleshooting Training Course is to cover fundamental and advanced concepts of gas chromatography. This course utilizes a one of a kind gas chromatograph simulator which allows the Student to learn and demonstrate understanding in method development, GC gating and calibration. Additionally, the simulator can be set-up to run in backflush or heatcut backflush mode to test the Students comprehension of this subject matter.

AUDIENCE

The course is designed for analyzer specialist or analyzer technicians who are seeking a better understanding of how to set-up a gas chromatograph. This program is 20-30% lecture and 70-80% lab. Individuals attending this course must have one year of experience working with gas chromatographs or have completed the Basic Chemistry and Basic Chromatography Training Course. This is not an entry level training course.

GAS CHROMATOGRAPH PRACTICAL SKILLS COURSE OBJECTIVES

1. Basic Chromatography Review. 2. Explanation and demonstration of peak integration. 3. Baseline correction methods. 4. Explanation and demonstration of converting peak integration into a concentration using

standard calculations that are found in ABB, Siemens, Yokogawa and Emerson gas chromatographs.

5. Setting up a method for a gas chromatograph. 7. Setting peak times using the GC simulation software. 8. Setting backflush valve timing using the GC simulation software 9. Setting heartcut-backflush valve timing using the GC simulation software 10. Setting dual heartcut-backflush valve timing using the GC simulation software 11. Help participants develop a better understanding of how this information is used to


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METHODOLOGY




TIME: Thirty-two (32) hours technical content.

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Practical Skills Gas Chromatograph Training Detail – (GC-103)



Session 1 – Basic Chromatography Review

• Review of Basic Chromatography

Session 2 – Gas Chromatograph Practical Skills

• Integration and Baseline Correction

Session 3 – Gas Chromatograph Practical Skills Lab 1

• Perform Basic Calibration of a Gas Chromatograph Using the Smith Analytical GC Simulation

Software

• Review Lab 1


• Baseline Correction Techniques are covered in this session including front to back height

correction, front height correction, Back Height Correction and Tangent Skims.


• Lab 2 – Setting peak times for an analytical method using the GC Simulation software

• Review Lab 2


• How Peak Values are Converted into Concentrations


• Lab 3 – Troubleshooting Lab. Students have to identify issues with GC Simulation program

• Lab 3 Review

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• BackFlush Application Review

• Detailed explanation of how the Back Flush Application works and its use in Gas

Chromatography

• Detailed review of a Back Flush Application Drawing

• Development of a Step Sequence Summary for this application


• Lab 4 – Set‐up a GC with a Back Flush Application using the GC Simulation software

• Review Lab 4


• Lab 5 – Students will have to demonstrate understanding of the Back Flush Application by

setting up a Back Flush Application using various method requirements. All work will be done

using the GC Simulation software

• Review Lab 5


• Lab 4 – Students will be required to troubleshoot a Back Flush analytical method using the Smith

Analytical Gas Chromatograph Simulator Software

• Set Peak Times after resolving the issue with the simulator

• Calibrate the equipment using the simulator

• Review Lab 6


• Heartcut / BackFlush Application Review

• Detailed explanation of how the Back Flush Application works and its use in Gas

Chromatography

• Detailed review of a Heartcut / Back Flush Application Drawing


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• Revrse Column Step Application Review

• Detailed explanation of how the Reverse Column Step works and its use in Gas Chromatography

• Detailed review of a Reverse Column Step Application Drawing



• Lab 7 – Students will be required to demonstrate they understand how to read and troubleshoot

using a GC heartcut / backflush application valve diagram

• Students will have to set‐up a heartcut / backflush application using the GC simulator software

• Review Lab 7


• Lab 8 ‐ Heartcut / Backflush Application troubleshooting lab using the GC simulator software

• Review Lab 8

44



GAS DETECTION FUNDAMENTALS

TRAINING COURSE

PURPOSE

The purpose of the Ametek WDG-IV Training Course is to cover fundamental concepts of gas detection and to allow for Stake Holders to self-certify their technicians in the use and calibration of this safety equipment. Both area monitors and analyzer shelter gas detection systems are covered. This class consists of formal lecture and hands-on training.

AUDIENCE

The course is designed for engineers or analyzer technicians who are seeking a better understanding of oxygen deficiency, LEL and toxic gas detection and how to approach specific problems when dealing with this technology.

COURSE OBJECTIVES

1. Introduce participants to fundamentals of oxygen gas measurement. 2. Introduce participants to fundamentals of Lowe Explosive Level gas measurement. 3. Introduce participants to fundamentals of toxic gas measurement. 4. Review gas detection hardware. 5. Review of software and User Parameters. 6. Calibration of Oxygen, LEL and Toxic Gas Analyzer. 7. Troubleshooting the Area Gas Monitor Analyzer. 8. Help participants develop a better understanding of how this information is used to


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METHODOLOGY





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Training Detail



Session 1 – Overview of Gas Measurement and Alarm Systems

• Electrochemical Sensors for Oxygen and other compounds

• LEL measurement using Infra‐red

• Overview of a basic Analyzer Shelter Alarm System


• Gas detection hardware overview


• Entering User defined parameters into the gas detector

Session 4 – Oxygen Analyzer Calibration Lab‐#1

• Students will be required to calibrate the analyzer using Low (Zero) and High Standard O2 Gas

(20.95%)

Session 5 – – LEL / Toxic Gas Analyzer Calibration Lab‐#2

• Students will be required to calibrate the analyzer(s) using Low (zero) and high cal gas






the analyzer.

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KEY PERFORMANCE INDICATOR (KPI) TRAINING COURSE

PURPOSE

The purpose of the Key Performance Indicator (KPI) Training Course is to introduce or strengthen the importance of performance metrics used in conjunction with process analytical systems.

AUDIENCE

The course is designed for individuals who work with process analyzers. This course is designed for engineers, supervisors, lab and analyzer technicians who are seeking a better understanding of Key Performance Indicators.

KPI COURSE OBJECTIVES

1. Introduce participants to principles and concepts of KPI. 2. Develop participants’ capacity to understand concepts of KPI, Statistical Quality Control

and Gage Test. 3. Equip participants with knowledge so they understand how performance metrics can be

used to improve equipment performance. 4. Identify how these concepts apply to process sample conditioning systems and analyzers. 5. Help participants develop a better understanding of how this information is used in their

daily task.

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METHODOLOGY

The training approach is based on principles of adult learning with a focus on peer review during all the steps of the training/learning event. The course models a variety of effective training methodologies including demonstration, practice, discussion, brain-storming, buzz groups, case studies, visualization and presentation. Once students have gained the concepts explained and demonstrated in this class, they can begin to apply their knowledge to improve analytical system performance.

STRUCUTRE: 15 sessions, 12 Labs, a baseline and final exam


TIME: Twenty-four (24) hours technical content.

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Key Performance Indicator Training Detail



Session 1 – Introduction to KPI

• Explanation of Key Performance Indicators (KPI) as it Relates to Process Analyzers

Session 2 – Lab 1 & 2

• Lab 1 – Brain storming exercise listing requirements for a “Successful Analyzer System”

• Lab 2 ‐ Generate list of products or services that are of consistent quality

Session 3 – KPI

• Continued discussion of KPI

• Lab 3 – Selection of Measurement System

• Lab 4 – Defining a Vision

Session 4 – Performance Measurement

• Discussion of the Fundamentals of Performance Measurement

• Design Practices

• Operating Practices

• Maintenance Practices

Session 5 – Performance Measurement (Continued)

• Manufacturing Performance Requirements

• Customer Needs

Session 6 – Best Operating Practices

• Overview of how to select and implement “Better” Practices

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Session 7 – KPI and Process Analyzers

• Ten Year Cost of Ownership

• Lab 5 – Identity Cost of Ownership for a Variety of Process Analyzers

• Lab 6 ‐ Provide your estimated cost for an analysis

Session 8 – KPI and the Details

• Key Performance Indicators

• Performance Indicators

Session 9 – KPI and the Details (Continued)

• Result Indicators

• Key Result Indicators


• Quantitative Indicators

• Practical Indicators

• Directional Indicators

• Actionable Indicators

• Financial Indicators


• Characteristics of a KPI

• Lab 7 – Select two most important Key Performance Indicators (KPI’s) or Critical Success Factors

(CSF) when dealing with process analyzer measurements

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Session 12 – Review of KPI and Labs

• Review of the information presented in Sessions 8‐11

• Lab 8 ‐ review Appendix V: SABIC Maintenance Key Performance Indicators and properly classify

each item as either a KRI, RI, PI or KPI

• Lab 9 ‐ List every item your group deems important required to have a successful analyzer

system. Review your ideas from the “Brain Storming” lab and use those items you still deem important.

Session 13 – Analyzer Performance Specifications and Testing

• NIST programs

• SRM program

• Certificate of Traceability

• Precision

• Repeatability

• Reproducibility Conditions

• Site Precision Conditions

• EPA Performance Specification 9

• Sample Line Loss Test

Session 14 – Development and Use of Gage R&R Test for Process Analyzers

• ANOVA gauge R&R

• Measuring instruments

• Test Methods

Session 15 – Statistical Quality Control (SQC)

• Control Charts

• Use of Statistical Process Control Information

• Development of SQC Charts

52



PROCESS ANALYZER ENGINEERING TRAINING COURSE (PAE-101)

PURPOSE

The purpose of the Process Analyzer Engineering Course is to strengthen the understanding of those individuals who work with or support process analyzers on a daily basis.

AUDIENCE

The course is designed for individuals who work with process chromatographs. This course is designed for engineers or analyzer specialist seeking a better understanding of project methodologies and the project execution cycle. Individuals attending this training course should have previous work experience with process analytical instrumentation or lab analyzers.

PROCESS ANALYZER ENGINEERING COURSE OBJECTIVES

1. Introduce participants to principles and concepts of process analyzer engineering. 2. Explanation of lag time, dew point and bubble point calculations. 3. Cover in detail additional calculations which are typically done during an analyzer

project including shelter wind, roof, floor loading, heat loading and HVAC sizing, sample line pressure loss, Reynolds Number, power loading and the development of the power loading schedule, heated sample line and thermo-well fail calculations.

4. Develop participants’ capacity to read and understand shelter mechanical and electrical drawings, sample system drawings and other project related drawings.

5. Equip participants with knowledge so they understand datasheets. 6. Explain a typical project cycle. 7. Help participants develop a better understanding of how this information is used during

the project engineering cycle. 8. Demonstrate basic understanding of these concepts by completing various lab exercises

during the training.

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METHODOLOGY


STRUCUTRE: 15 sessions, labs plus a baseline and final exam



54



Process Analyzer Engineering Training Detail (PAE-101)

During the one week training course there are a total of 15 Training Sessions. The following is the

material which will be covered in each session.

Session 1 – Analyzer Project Engineering Part 1

• Overview of a typical analyzer project


• Design Fundamentals Overview

• General Specifications


• Process Analyzer Datasheets

Session 4 – Analyzer Project Engineering 4

• Dew Point Calculations

• Bubble Point Calculations


• Sample Probes

• Sample Line


• Lag Time Calculations

• Electrical Load Calculations

• Area Classification


• Lab 1 – Calculate Dew and Bubble Point for the Sample System that the details provided for

• Lab 2 – Calculate Lag Time for the for the Sample System that the details provided for

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• Lab 3 – Review datasheets to determine if there are problems or missing information the project

would require


• Shelter Drawing Review


• Electrical System Drawing Review


• Sample System Drawing Review


• HVAC Sizing

• NFPA 496 Purge Systems


• Process Analyzer Networks


• Factory Acceptance Test Procedures


• Lab 4 – Review Sample System Drawing to demonstrate understanding of drawing symbols and

review concepts

• Lab 5 – Review Shelter Design Drawing to demonstrate understanding of drawing symbols and

review concepts

56



PROCESS ANALYZER FUNDAMENTALS TRAINING COURSE – (PAF-101)

PURPOSE

The purpose of the Process Analyzer Fundamentals Course is to strengthen the understanding of those individuals who work with or support process analyzers on a daily basis.

AUDIENCE

The course is designed for individuals who work with process analyzers. This course is designed for engineers, supervisors, analyzer specialist or technicians seeking a better understanding of the operating principles of process analyzers.

PROCESS ANALYZER COURSE OBJECTIVES

1. Introduce participants to principles and concepts of process analyzers. 2. Explanation of in situ and extractive measurements. 3. Develop participants’ capacity to understanding basic measurement techniques including

conductivity, pH, gas chromatography, spectroscopy and continuous analyzers.

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METHODOLOGY


STRUCUTRE: 15 sessions plus a baseline and final exam

MATERIALS AND TOOLS: Each session includes an introduction, learning objectives, participatory methodologies, and activities. A pre/post course assessment and peer feedback form on practice sessions are included. Each student will receive a copy of the latest edition of the Process Measurement and Analysis by Bela Liptak. TIME: Thirty-two (32) hours technical content.

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Process Analyzer Fundamentals Training Detail – (PAF-101)

During the one week training course there are a total of 15 Training Sessions. The following is the

material which will be covered in each session.

Session 1 – Analyzer Fundamentals Part 1

• Why Process Analyzers are Used

• In Situ Analyzers

• Extractive Analyzers


• Analyzer Selection


• Sample System Overview

Session 4 – Analyzer Fundamentals 4

• Water Measurement Principles

• Conductivity Analyzers


• pH Analyzers


• Turbidity Analyzers


• TOC Analyzers


• Overview of Spectroscopy

• Infrared Measurement Theory

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• Infrared Measurement Theory Continued


• Infrared Measurement Theory Continued


• Ultra Violet and Laser Analyzers


• Oxygen in Gases


• Oxygen in Gases Continued


• Gas Chromatography


• Gas Chromatography Continued

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SAMPLE SYSTEM MAINTENANCE TRAINING COURSE – (PSS-101)

PURPOSE

The purpose of the Sample System Training Course is to introduce the basic concepts and hardware found in process sample conditioning systems and how this hardware is used in conjunction with process analytical systems.

AUDIENCE

The course is designed for individuals who work with process analyzers. This course is designed for engineers, supervisors and analyzer technicians who are seeking a better understanding of sample conditioning systems.

SAMPLE SYSTEM COURSE OBJECTIVES

1. Introduce participants to fundamentals, principles and concepts of sample conditioning. 2. Explain and demonstrate to the students the three major types of sample conditioning

systems. 3. Explain and demonstrate to the students the hardware used in the various sample

conditioning systems. 4. Equip participants with knowledge so they understand how sample conditioning systems

operate and the steps required improve equipment performance. 5. Identify how these concepts apply to process sample conditioning systems. 6. Help participants develop a better understanding of how this information is used to


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METHODOLOGY


STRUCUTRE: Formal training sessions which also include a baseline and final exam.


TIME: Twenty-four (24) hours technical content presented in the formal training session.

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Process Sample System Training Detail – (PSS-101)



Session 1 – Overview of Process Analyzer Sample Systems

• Explanation of sample system fundamentals

• In Situ versus Extractive Systems

Session 2 – Sample Systems Fundamentals

• Isokinetic Samples

• Non‐Isokinetic Samples

• Fast Loop

• Lag‐time Definition and Calculation

Session 3 – The Sample Tap and Transport Line

• Sample Probes Types

• Probe Location and Installation

• Sample Probe Egress

• Sample Line Construction

• Non‐Heated Sample Line

• Heated Sample Line

• Specially Coated Sample Line

Session 4 – Extractive Sample Systems – Vapor Sample System

• Discussion of the Fundamentals of Vapor Sample System

• Vapor Sample System Drawing Review

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Session 5 – Extractive Sample Systems – Vapor Sample System




Session 6 – Extractive Sample Systems – Liquid Sample System

• Discussion of the Fundamentals of Liquid Sample System

• Liquid Sample System Drawing Review

Session 7 – Extractive Sample Systems – Liquid Sample System




Session 8 – Extractive Sample Systems – Liquid / Vaporizing Sample System

• Discussion of the Fundamentals of Liquid / Vaporizing Sample System

• Liquid / Vaporizing Sample System Drawing Review




Session 9 – Identify Hardware Used in a Sample Conditioning System

• Students must be able to identify hardware used in a vapor, liquid and liquid/vaporzing sample

system

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Session 10 – Extractive Sample Systems – Sparger Sample System

• Discussion of the Fundamentals of a Sparger Sample System

• Sparger Sample System Drawing Review




Session 11 – Extractive Sample Systems – Vacuum Sample System

• Discussion of the Fundamentals of a Vacuum Sample System

• Vacuum Sample System Drawing Review




Session 12 – Lab #2 – Identify Hardware Used in Sparger and Vacuum Sample System

• Students must be able to identify hardware used in a sparger and vacuum sample system

Session 13 – Equipment: Regulators and Valves

• Pressure Reducing Regulators

• Back Pressure Regulators

• Single State Regulators

• Dual Stage Regulators

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Session 14 – Equipment: Filters and Phase Separators

• Filter Types

• Coalescing Filters

• Edge and Surface Area Filters

• Guard Filters

• Pygas Samplers

Session 15 – Sample System Safety

• Design Considerations

• Egress

• Safety Precautions During Start‐up

• Safety Precautions During Routine Maintenance

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SAMPLE SYSTEM PRACTICAL SKILL

TRAINING COURSE – (PSS-102)

PURPOSE

This course is designed to provide “Hands-on” experience with process sample conditioning systems. This training program is 30% lecture and 70% lab. Students will work with actual process sample conditioning hardware and the Smith Analytical Sample System Simulator during this course. Each Student will be required to review a vapor and liquid sample system drawing and then construction the system using the equipment and tools which are provided with this program. Students should attend the Basic Sample System Course PSS-101 or the Advance Sample System Course PSS-102 before attending this course. This is not an entry level training program.

AUDIENCE

The course is designed for analyzer specialist or analyzer technicians who are seeking a better understanding of process analyzer sample systems. This program is 20-30% lecture and 70-80% lab. Individuals attending this course must have one year of experience working with process sample systems or have completed the Basic Chemistry and Process Sample System Training Course. This is not an entry level training course.

SAMPLE SYSTEM PRACTICAL SKILLS COURSE OBJECTIVES

1. Sample System Review 2. Troubleshooting Labs 3. Vapor Sample System Lab 4. Liquid Sample System Lab 5. Liquid Vaporizing Sample System Lab

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METHODOLOGY





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Practical Sample System Training Detail – (PSS-103)



Session 1 – Practical Skills Sample System Training

• Review of Sample Systems


• Review of Sample Systems


• Troubleshooting Lab #1


• Troubleshooting Lab #2


• Vapor Sample System Design Lab






• Vapor Sample System Layout Lab


• Vapor Sample System Layout Lab


• Liquid Sample System Design Lab

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• Liquid Sample System Design Lab


• Liquid Sample System Layout Lab


• Liquid Sample System Layout Lab


• Liquid‐Vaporizing Sample System Design Lab


• Liquid‐Vaporizing Sample System Layout Lab


• Liquid‐Vaporizing Sample System Layout Lab

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SIEMENS ADVANCE™ CHROMATOGRAPHY TRAINING COURSE (SA-101)

PURPOSE

The purpose of the Siemens Advance Chromatography Training Course is to strengthen the understanding of those individuals who work with or support process gas chromatograph analyzers on a daily basis. This course is generally attended by individuals who desire a better understanding of this gas chromatograph or want to understand specific troubleshooting techniques . The course is designed to cover in detail all aspects of the Siemens Advance Gas Chromatograph. During this course, the Instructor will cover the hardware and software used in the Advance Gas Chromatograph, calibration of the GC and common troubleshooting techniques.

AUDIENCE

The course is designed for individuals who work with the Siemens process gas chromatographs. This course is designed for engineers, supervisors and analyzer technicians seeking a better understanding of the operational theory of this technology.


1. Introduce participants to principles and concepts of basic chromatography. 2. Overview of Siemens Advance GC Hardware 3. Troubleshooting the Siemens Advance GC 4. Develop participants’ capacity to read and understand valve diagrams. 5. Equip participants with knowledge so they understand basic Siemens operational and

troubleshooting concepts. 6. Explain the operational theory of peak integration, baseline correction and calibration. 7. Demonstrate basic understanding of these concepts by using the Siemens GC software.

(APC)

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METHODOLOGY





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Training Detail

During the one week there are a total of 15 Training Sessions. The following is the material which will be


Session 1 – Siemens Advance Part 1

OVERIVEW & ROLE OF THE GAS CHROMATOGRAPH

Session 2 – Siemens Sample Advance Part 2



• Column Types



BASIC GC HARDWARE OVERVIEW


• APC SOFTWARE OVERVIEW


• SETTING PARAMETERS (GATE TIMES, CALINRATION CONCENTRATIONS, ETC)


• REVIEWING A CHROMATOGRAM USING APC


• HOW TO CALIBRATE THE ADVANCE GC


• HOW TO SAVE AND LOAD AN AMD FILE


• TROUBLESHOOTING THE ADVANCE GC

73




• TROUBLESHOOTING THE TCD LAB #2


• TROUBLESHOOTING THE FID LAB #3

74



SIEMENS MAXUM CHROMATOGRAPHY TRAINING COURSE (SM-101)

PURPOSE

The purpose of the Siemens Maxum Chromatography Training Course is to strengthen the understanding of those individuals who work with or support process gas chromatograph analyzers on a daily basis. This course is generally attended by individuals who desire a better understanding of this gas chromatograph or want to understand specific troubleshooting techniques . The course is designed to cover in detail all aspects of the Siemens Maxum Gas Chromatograph. During this course, the Instructor will cover the hardware and software used in the Maxum Gas Chromatograph, calibration of the GC and common troubleshooting techniques.

AUDIENCE

The course is designed for individuals who work with the Siemens process gas chromatographs. This course is designed for engineers, supervisors and analyzer technicians seeking a better understanding of the operational theory of this technology.


8. Introduce participants to principles and concepts of basic chromatography. 9. Overview of Siemens Maxum GC Hardware 10. Troubleshooting the Siemens Maxum GC 11. Develop participants’ capacity to read and understand valve diagrams. 12. Equip participants with knowledge so they understand basic Siemens operational and

troubleshooting concepts. 13. Explain the operational theory of peak integration, baseline correction and calibration. 14. Demonstrate basic understanding of these concepts by using the Siemens Maxum GC EZ

Chrom and Portal Software.

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METHODOLOGY





76



Training Detail

During the one week there are a total of 15 Training Sessions. The following is the material which will be


Session 1 – Siemens Maxum Part 1

OVERIVEW & ROLE OF THE GAS CHROMATOGRAPH




• Column Types



BASIC MAXUM GC HARDWARE OVERVIEW


• MAXUM EZ CHROM OVERVIEW

• MAXUM PORTAL OVERVIEW


• SETTING PARAMETERS IN EZ CHROM (GATE TIMES, CALINRATION CONCENTRATIONS, ETC)


• REVIEWING A CHROMATOGRAM USING EZ CHROM


• HOW TO CALIBRATE THE MAXUM GC


• HOW TO SAVE AND LOAD AN AMD FILE


• TROUBLESHOOTING THE MAXUM GC

77




• TROUBLESHOOTING THE TCD LAB #2


• TROUBLESHOOTING THE FID LAB #3

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THERMO-SCIENTIFIC 42I (NOX) AND 48I (CO) ANALYZER TRAINING COURSE

PURPOSE

The purpose of the Thermo-Sceintific 42//48 Analyzer Training Course is to cover fundamental concepts of carbon monoxide and NOx in gas measurement, provide an overview of the analyzers in addition to calibration and hands-on labs with this equipment.

AUDIENCE

The course is designed for engineers or analyzer technicians who are seeking a better understanding of CEMS or process measurements using the Thermo 421/48i Analyzers and how to approach specific problems when dealing with this technology.

COURSE OBJECTIVES

1. Introduce participants to fundamentals of oxygen in gas measurement. 2. Review Thermo 42i NOx analyzer hardware. 3. Thermo 48i NOx analyzer hardware. 4. Review of User Parameters. 5. Calibration of the 42i NOx Analyzer. 6. Calibration of the 48i CO Analyzer. 7. Troubleshooting the 42i and 48i Analyzers. 8. Help participants develop a better understanding of how this information is used to


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METHODOLOGY





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Training Detail



Session 1 – Measurement Overview of 42i CO and 48i NOx in Gas Measurement

• Measuring CO with Infrared

• Chemiluminescence measurement technique for NOx


• 42i hardware overview

• 48i hardware overview


• Entering User defined parameters

Session 4 – Analyzer Calibration Lab‐#1

• Students will be required to calibrate the 48i CO analyzer using Low and High Standard Cal Gases

Session 5 – – Analyzer Calibration Lab‐#2

• Students will be required to calibrate the 42i NOx analyzer using Low and High Standard Cal

Gases


• Troubleshooting 101 for both the 421 and 48i and ways to make fault finding more efficient




the analyzer.

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Currently no certification organization (ISA, NCCER) offers any type of Analyzer Technician Certification Program. Smith Analytical has developed a comprehensive written and hands-on program, which allows our Clients to “Self-Certify” their Analyzer Technicians.

Students who attend the Analyzer Technician Level 1 Certification Program should have attended formal training programs on the subject matter and have hands-on, field experience. This is NOT a training program, but a Certification Program.

The Analyzer Technician Level 1 Certification Program evaluates the Students understanding of Basic Chemistry, Basic Chromatography, Process Analyzer Fundamentals and Sample System Theory and Maintenance.

The Level 1 Certification consist of:

1. Fifty (50) question multiple choice test covering Basic Chemistry 2. Fifty (50) question multiple choice test covering Basic Gas Chromatography 3. Fifty (50) question multiple choice test covering Process Analyzer Fundamentals 4. Fifty (50) question multiple choice test covering Sample System Theory and

Maintenance

Students must score 80% or better on each of the individual exams to obtain a passing score. A certificate will be issued for each individual exam passed. Those Students passing all four individual test will be awarded the Analyzer Technician Level 1 Certification Certificate.

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Currently no certification organization (ISA, NCCER) offers any type of Analyzer Technician Certification Program. Smith Analytical has developed a comprehensive written and hands-on program, which allows our Clients to “Self Certify” their Analyzer Technicians.

Students who attend the Analyzer Technician Level 2 Certification Program should have attended formal training programs on the subject matter and have hands-on, field experience. This is NOT a training program, but a Certification Program.

The Analyzer Technician Level 2 Certification Program evaluates the Students understanding of Continuous Emissions Monitoring Systems, Practical Gas Chromatography and Process Analyzer Troubleshooting skills.

The Level 2 Certification consist of:

1. Fifty (50) question multiple choice test covering Continuous Emissions Monitoring Systems (CEMS)

2. Fifty (50) question multiple choice test covering Practical Gas Chromatography 3. Fifty (50) question multiple choice test covering Process Analyzer Troubleshooting 4. Hands on test setting up a gas chromatograph method including setting up a back-flush

and heart cut. Students will use the Smith Analytical GC Simulator to complete this portion of the training

Students must score 80% or better on each of the individual exams to obtain a passing score. A certificate will be issued for each individual exam passed. Those Students passing all four individual test will be awarded the Analyzer Technician Level 2 Certification Certificate.

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GENERAL AREA MAP SHOWING SMITH ANALYTICAL OFFICE LOCATION 5318 FM 517 WEST, ALVIN, TEXAS

AREA HOTELS

All hotels listed below are 15-30 minutes from the Smith Analytical office.

1. Holiday Inn Alvin, Texas (281) 331-8800 2. Holiday Inn Webster, Texas (281) 335-6272 3. Hampton Inn League City, Texas (281) 614-5437 4. South Shore Harbour Resort (281) 334-1000 5. Hilton Houston NASA Clear Lake (281) 333-9300 6. Boardwalk Inn (281) 334-9880 7. Holiday Inn Kemah (NEAR BOARDWALK) (281) 334-0003 8. The San Luis Hotel (409) 744-1500

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