1 2 3 4 5 analytical report 6 - naperville park district · 2017-12-07 · analytical report...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200

TestAmerica Job ID: 500-46374-1TestAmerica Sample Delivery Group: 500-46374-1Client Project/Site: Naperville Sportsman Club

For:Shaw Environmental & Infrastructure, Inc1607 East Main StreetSuite ESaint Charles, Illinois 60174

Attn: Jeffrey Cademartori

Authorized for release by:5/24/2012 4:50:47 PMCindy PritchardProject Mgmt. [email protected]

Designee for

Richard WrightProject Manager [email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Shaw Environmental & Infrastructure, IncProject/Site: Naperville Sportsman Club

TestAmerica Job ID: 500-46374-1SDG: 500-46374-1

of 39TestAmerica Chicago

5/24/2012

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

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Case NarrativeClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1

Project/Site: Naperville Sportsman Club SDG: 500-46374-1

Job ID: 500-46374-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-46374-1

Comments

No additional comments.

Receipt

The samples were received on 5/16/2012 7:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 4.0º C.

GC/MS Semi VOA

Method(s) 8270C: The following sample was diluted due to the abundance of target analytes: G19 (0-6") (500-46374-5). Elevated

reporting limits (RLs) are provided.

No other analytical or quality issues were noted.

Metals

Method(s) 7471A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for 500-46374-1 were outside control limits for Hg. The

associated laboratory control sample (LCS) recovery met acceptance criteria.


General Chemistry

No analytical or quality issues were noted.

Organic Prep


TestAmerica Chicago of 39 5/24/2012

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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc

SDG: 500-46374-1Project/Site: Naperville Sportsman Club

Client Sample ID: E24 (0-6") Lab Sample ID: 500-46374-1

☼Benzo[b]fluoranthene

RL

0.043 mg/Kg

MDL

0.0084

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

8270C Total/NA1J0.011

☼Chrysene 0.043 mg/Kg0.0098 Total/NA8270C10.020 J

☼Arsenic 1.2 mg/Kg0.26 Total/NA6010B123

☼Barium 1.2 mg/Kg0.14 Total/NA6010B161

☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.36

☼Chromium 1.2 mg/Kg0.20 Total/NA6010B120

☼Copper 1.2 mg/Kg0.33 Total/NA6010B136

☼Lead 0.60 mg/Kg0.21 Total/NA6010B119

☼Selenium 1.2 mg/Kg0.35 Total/NA6010B10.47 J

☼Zinc 2.4 mg/Kg0.83 Total/NA6010B165

☼Mercury 0.021 mg/Kg0.0064 Total/NA7471A10.035

pH 0.200 SU0.200 Total/NA9045C17.76

Client Sample ID: G9 (0-6") Lab Sample ID: 500-46374-3

☼Benzo[a]pyrene

RL

0.045 mg/Kg

MDL

0.0083



☼Benzo[b]fluoranthene 0.045 mg/Kg0.0088 Total/NA8270C10.014 J


☼Antimony 2.6 mg/Kg0.34 Total/NA6010B11.7 J B

☼Arsenic 1.3 mg/Kg0.28 Total/NA6010B16.3


☼Cadmium 0.26 mg/Kg0.064 Total/NA6010B10.23 J






pH 0.200 SU0.200 Total/NA9045C17.22


☼Acenaphthene

RL

0.51 mg/Kg

MDL

0.15



☼Anthracene 0.51 mg/Kg0.12 Total/NA8270C50.29 J

☼Benzo[a]anthracene 0.51 mg/Kg0.11 Total/NA8270C53.1

☼Benzo[a]pyrene 0.51 mg/Kg0.093 Total/NA8270C54.7

☼Benzo[b]fluoranthene 0.51 mg/Kg0.099 Total/NA8270C56.0

☼Benzo[g,h,i]perylene 0.51 mg/Kg0.17 Total/NA8270C52.6

☼Benzo[k]fluoranthene 0.51 mg/Kg0.12 Total/NA8270C52.2

☼Chrysene 0.51 mg/Kg0.11 Total/NA8270C53.9

☼Dibenz(a,h)anthracene 0.51 mg/Kg0.14 Total/NA8270C50.66

☼Fluoranthene 0.51 mg/Kg0.21 Total/NA8270C53.9

☼Fluorene 0.51 mg/Kg0.12 Total/NA8270C50.13 J

☼Indeno[1,2,3-cd]pyrene 0.51 mg/Kg0.17 Total/NA8270C52.5

☼Phenanthrene 0.51 mg/Kg0.21 Total/NA8270C51.2

☼Pyrene 0.51 mg/Kg0.18 Total/NA8270C53.9








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Client Sample ID: G19 (0-6") (Continued) Lab Sample ID: 500-46374-5

☼Lead

RL

1.6 mg/Kg

MDL

0.55


6010B Total/NA1190



☼Mercury 0.049 mg/Kg0.015 Total/NA7471A10.045 J

pH 0.200 SU0.200 Total/NA9045C17.63

Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7

☼Benzo[a]anthracene

RL

0.055 mg/Kg

MDL

0.012



☼Benzo[a]pyrene 0.055 mg/Kg0.010 Total/NA8270C10.022 J


☼Benzo[k]fluoranthene 0.055 mg/Kg0.013 Total/NA8270C10.015 J


☼Fluoranthene 0.055 mg/Kg0.023 Total/NA8270C10.034 J

☼Pyrene 0.055 mg/Kg0.020 Total/NA8270C10.030 J

☼Antimony 2.9 mg/Kg0.39 Total/NA6010B133 B










pH 0.200 SU0.200 Total/NA9045C17.55



RL

0.047 mg/Kg

MDL

0.010
















pH 0.200 SU0.200 Total/NA9045C18.21

Client Sample ID: J4 (0-6") Lab Sample ID: 500-46374-11


RL

0.069 mg/Kg

MDL

0.015






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Client Sample ID: J4 (0-6") (Continued) Lab Sample ID: 500-46374-11

☼Chrysene

RL

0.069 mg/Kg

MDL

0.016
















pH 0.200 SU0.200 Total/NA9045C17.78



RL

0.068 mg/Kg

MDL

0.014


8270C Total/NA10.081







☼Indeno[1,2,3-cd]pyrene 0.068 mg/Kg0.023 Total/NA8270C10.064 J










☼Selenium 1.8 mg/Kg0.52 Total/NA6010B12.3

☼Silver 0.91 mg/Kg0.11 Total/NA6010B10.48 J



pH 0.200 SU0.200 Total/NA9045C17.72


☼Acenaphthene

RL

0.062 mg/Kg

MDL

0.019



☼Anthracene 0.062 mg/Kg0.015 Total/NA8270C10.047 J








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☼Dibenz(a,h)anthracene

RL

0.062 mg/Kg

MDL

0.017


8270C Total/NA10.16




☼Naphthalene 0.062 mg/Kg0.012 Total/NA8270C10.012 J














pH 0.200 SU0.200 Total/NA9045C17.76


☼Antimony

RL

2.5 mg/Kg

MDL

0.33


6010B Total/NA1J B0.39










pH 0.200 SU0.200 Total/NA9045C17.70

Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19


RL

0.075 mg/Kg

MDL

0.016








☼Phenanthrene 0.075 mg/Kg0.032 Total/NA8270C10.046 J










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Client Sample ID: K7 (0-6") (Continued) Lab Sample ID: 500-46374-19

☼Zinc

RL

4.6 mg/Kg

MDL

1.6


6010B Total/NA173


pH 0.200 SU0.200 Total/NA9045C17.77


☼Antimony

RL

2.9 mg/Kg

MDL

0.39


6010B Total/NA1J B1.6










pH 0.200 SU0.200 Total/NA9045C17.71

Client Sample ID: L5 (0-6") Lab Sample ID: 500-46374-23


RL

0.052 mg/Kg

MDL

0.010













pH 0.200 SU0.200 Total/NA9045C18.27


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Method SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Method Method Description LaboratoryProtocol

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CHI

SW8466010B Metals (ICP) TAL CHI

SW8467471A Mercury (CVAA) TAL CHI

SW8469045C pH TAL CHI

EPAMoisture Percent Moisture TAL CHI

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200


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Sample SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

500-46374-1 E24 (0-6") Solid 05/09/12 10:31 05/16/12 07:00

500-46374-3 G9 (0-6") Solid 05/09/12 12:20 05/16/12 07:00

500-46374-5 G19 (0-6") Solid 05/09/12 16:08 05/16/12 07:00

500-46374-7 I9 (0-6") Solid 05/09/12 13:22 05/16/12 07:00

500-46374-9 I18 (0-6") Solid 05/07/12 15:45 05/16/12 07:00

500-46374-11 J4 (0-6") Solid 05/09/12 14:40 05/16/12 07:00

500-46374-13 J13 (0-6") Solid 05/07/12 13:40 05/16/12 07:00

500-46374-15 J15 (0-6") Solid 05/07/12 13:00 05/16/12 07:00

500-46374-17 J24 (0-6") Solid 05/09/12 11:00 05/16/12 07:00

500-46374-19 K7 (0-6") Solid 05/07/12 16:30 05/16/12 07:00

500-46374-21 K11 (0-6") Solid 05/07/12 14:25 05/16/12 07:00

500-46374-23 L5 (0-6") Solid 05/09/12 15:20 05/16/12 07:00


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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Lab Sample ID: 500-46374-1Client Sample ID: E24 (0-6")Matrix: SolidDate Collected: 05/09/12 10:31

Percent Solids: 74.2Date Received: 05/16/12 07:00

Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL

Acenaphthene <0.043 0.043 0.013 mg/Kg ☼ 05/18/12 07:14 05/20/12 20:37 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Acenaphthylene <0.043

0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Anthracene <0.043

0.043 0.0091 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[a]anthracene <0.043

0.043 0.0079 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[a]pyrene <0.043

0.043 0.0084 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[b]fluoranthene 0.011 J

0.043 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[g,h,i]perylene <0.043

0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[k]fluoranthene <0.043

0.043 0.0098 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Chrysene 0.020 J

0.043 0.012 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Dibenz(a,h)anthracene <0.043

0.043 0.018 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Fluoranthene <0.043

0.043 0.0099 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Fluorene <0.043

0.043 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Indeno[1,2,3-cd]pyrene <0.043

0.043 0.0084 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Naphthalene <0.043

0.043 0.018 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Phenanthrene <0.043

0.043 0.016 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Pyrene <0.043

2-Fluorobiphenyl 78 30 - 119 05/18/12 07:14 05/20/12 20:37 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Nitrobenzene-d5 76 05/18/12 07:14 05/20/12 20:37 130 - 115

Terphenyl-d14 96 05/18/12 07:14 05/20/12 20:37 136 - 134

Method: 6010B - Metals (ICP)RL MDL

Antimony <2.4 2.4 0.32 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:24 1


1.2 0.26 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Arsenic 23

1.2 0.14 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Barium 61

0.24 0.060 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Cadmium 0.36

1.2 0.20 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Chromium 20

1.2 0.33 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Copper 36

0.60 0.21 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Lead 19

1.2 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Selenium 0.47 J

0.60 0.072 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Silver <0.60

2.4 0.83 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Zinc 65

Method: 7471A - Mercury (CVAA)RL MDL

Mercury 0.035 0.021 0.0064 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:12 1


General ChemistryRL MDL

pH 7.76 0.200 0.200 SU 05/16/12 16:39 1



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Lab Sample ID: 500-46374-3Client Sample ID: G9 (0-6")Matrix: SolidDate Collected: 05/09/12 12:20






0.045 0.011 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Anthracene <0.045


0.045 0.0083 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[a]pyrene 0.0089 J




0.045 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Chrysene 0.011 J



0.045 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Fluorene <0.045




0.045 0.016 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Pyrene <0.045

2-Fluorobiphenyl 66 30 - 119 05/18/12 07:14 05/20/12 20:53 1


Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 20:53 130 - 115

Terphenyl-d14 90 05/18/12 07:14 05/20/12 20:53 136 - 134


Antimony 1.7 J B 2.6 0.34 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:31 1


1.3 0.28 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Arsenic 6.3

1.3 0.15 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Barium 94

0.26 0.064 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Cadmium 0.23 J

1.3 0.22 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Chromium 15

1.3 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Copper 20

0.65 0.22 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Lead 47

1.3 0.37 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Selenium <1.3

0.65 0.078 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Silver <0.65

2.6 0.89 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Zinc 51


Mercury 0.040 0.021 0.0063 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:23 1



pH 7.22 0.200 0.200 SU 05/16/12 16:41 1



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Acenaphthene 0.19 J 0.51 0.15 mg/Kg ☼ 05/18/12 07:14 05/20/12 21:10 5



0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Anthracene 0.29 J

0.51 0.11 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[a]anthracene 3.1

0.51 0.093 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[a]pyrene 4.7

0.51 0.099 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[b]fluoranthene 6.0

0.51 0.17 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[g,h,i]perylene 2.6

0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[k]fluoranthene 2.2

0.51 0.11 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Chrysene 3.9

0.51 0.14 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Dibenz(a,h)anthracene 0.66

0.51 0.21 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Fluoranthene 3.9

0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Fluorene 0.13 J

0.51 0.17 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Indeno[1,2,3-cd]pyrene 2.5


0.51 0.21 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Phenanthrene 1.2

0.51 0.18 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Pyrene 3.9

2-Fluorobiphenyl 71 30 - 119 05/18/12 07:14 05/20/12 21:10 5


Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 21:10 530 - 115

Terphenyl-d14 96 05/18/12 07:14 05/20/12 21:10 536 - 134


Antimony 4.2 J B 6.4 0.85 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:37 1


3.2 0.70 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Arsenic 13

3.2 0.38 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Barium 85

0.64 0.16 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Cadmium 0.64

3.2 0.54 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Chromium 15

3.2 0.87 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Copper 1600

1.6 0.55 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Lead 190

3.2 0.92 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Selenium 1.2 J

1.6 0.19 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Silver <1.6

6.4 2.2 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Zinc 810


Mercury 0.045 J 0.049 0.015 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:25 1



pH 7.63 0.200 0.200 SU 05/16/12 16:43 1



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Lab Sample ID: 500-46374-7Client Sample ID: I9 (0-6")Matrix: SolidDate Collected: 05/09/12 13:22






0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Anthracene <0.055

0.055 0.012 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[a]anthracene 0.017 J




0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[k]fluoranthene 0.015 J

0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Chrysene 0.024 J


0.055 0.023 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Fluoranthene 0.034 J

0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Fluorene <0.055




0.055 0.020 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Pyrene 0.030 J

2-Fluorobiphenyl 64 30 - 119 05/18/12 07:14 05/20/12 21:27 1


Nitrobenzene-d5 57 05/18/12 07:14 05/20/12 21:27 130 - 115

Terphenyl-d14 83 05/18/12 07:14 05/20/12 21:27 136 - 134


Antimony 33 B 2.9 0.39 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:43 1


1.5 0.32 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Arsenic 39

1.5 0.17 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Barium 100

0.29 0.073 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Cadmium 0.32

1.5 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Chromium 15

1.5 0.40 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Copper 21

0.73 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Lead 5400

1.5 0.42 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Selenium 0.89 J

0.73 0.088 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Silver <0.73

2.9 1.0 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Zinc 64


Mercury 0.050 0.027 0.0081 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:27 1



pH 7.55 0.200 0.200 SU 05/16/12 16:46 1



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0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Anthracene <0.047






0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Chrysene 0.032 J



0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Fluorene <0.047




0.047 0.017 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Pyrene 0.019 J

2-Fluorobiphenyl 76 30 - 119 05/18/12 07:14 05/20/12 21:44 1


Nitrobenzene-d5 70 05/18/12 07:14 05/20/12 21:44 130 - 115

Terphenyl-d14 102 05/18/12 07:14 05/20/12 21:44 136 - 134


Antimony 0.70 J B 2.9 0.38 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:49 1


1.4 0.31 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Arsenic 2.2

1.4 0.17 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Barium 72

0.29 0.071 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Cadmium 0.25 J

1.4 0.24 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Chromium 15

1.4 0.39 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Copper 18

0.71 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Lead 69

1.4 0.41 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Selenium <1.4

0.71 0.086 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Silver <0.71

2.9 0.98 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Zinc 49


Mercury 0.027 0.022 0.0069 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:28 1



pH 8.21 0.200 0.200 SU 05/16/12 16:48 1



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Lab Sample ID: 500-46374-11Client Sample ID: J4 (0-6")Matrix: SolidDate Collected: 05/09/12 14:40






0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Anthracene <0.069






0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Chrysene 0.032 J



0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Fluorene <0.069




0.069 0.025 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Pyrene 0.039 J

2-Fluorobiphenyl 69 30 - 119 05/18/12 07:14 05/20/12 22:00 1


Nitrobenzene-d5 62 05/18/12 07:14 05/20/12 22:00 130 - 115

Terphenyl-d14 97 05/18/12 07:14 05/20/12 22:00 136 - 134


Antimony 1.6 J B 4.2 0.55 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:55 1


2.1 0.45 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Arsenic 11

2.1 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Barium 110

0.42 0.10 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Cadmium 0.23 J

2.1 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Chromium 18

2.1 0.56 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Copper 24

1.0 0.36 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Lead 40

2.1 0.60 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Selenium 0.70 J

1.0 0.13 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Silver <1.0

4.2 1.4 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Zinc 99


Mercury 0.049 0.034 0.010 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:30 1



pH 7.78 0.200 0.200 SU 05/16/12 16:50 1



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0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Anthracene <0.068






0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Chrysene 0.12



0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Fluorene <0.068

0.068 0.023 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Indeno[1,2,3-cd]pyrene 0.064 J



0.068 0.025 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Pyrene 0.14

2-Fluorobiphenyl 60 30 - 119 05/18/12 07:14 05/20/12 22:17 1


Nitrobenzene-d5 49 05/18/12 07:14 05/20/12 22:17 130 - 115

Terphenyl-d14 86 05/18/12 07:14 05/20/12 22:17 136 - 134


Antimony 46 B 3.6 0.48 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:02 1


1.8 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Arsenic 92

1.8 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Barium 70

0.36 0.090 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Cadmium 1.1

1.8 0.30 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Chromium 510

1.8 0.49 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Copper 580

0.91 0.31 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Lead 6400

1.8 0.52 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Selenium 2.3

0.91 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Silver 0.48 J

3.6 1.2 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Zinc 67


Mercury 0.040 0.032 0.0099 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:32 1



pH 7.72 0.200 0.200 SU 05/16/12 16:52 1



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Acenaphthene 0.050 J 0.062 0.019 mg/Kg ☼ 05/18/12 07:14 05/20/12 22:34 1









0.062 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Chrysene 0.77



0.062 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Fluorene 0.026 J


0.062 0.012 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Naphthalene 0.012 J


0.062 0.022 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Pyrene 0.82

2-Fluorobiphenyl 59 30 - 119 05/18/12 07:14 05/20/12 22:34 1


Nitrobenzene-d5 53 05/18/12 07:14 05/20/12 22:34 130 - 115

Terphenyl-d14 89 05/18/12 07:14 05/20/12 22:34 136 - 134


Antimony 15 B 3.6 0.48 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:08 1


1.8 0.40 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Arsenic 30

1.8 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Barium 57

0.36 0.090 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Cadmium 0.67

1.8 0.30 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Chromium 27

1.8 0.49 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Copper 27

0.91 0.31 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Lead 3000

1.8 0.52 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Selenium 1.3 J

0.91 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Silver 0.31 J

3.6 1.2 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Zinc 53


Mercury 0.040 0.028 0.0084 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:34 1



pH 7.76 0.200 0.200 SU 05/16/12 16:54 1



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0.044 0.011 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Anthracene <0.044



0.044 0.0087 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[b]fluoranthene <0.044



0.044 0.010 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Chrysene <0.044



0.044 0.010 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Fluorene <0.044




0.044 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Pyrene <0.044

2-Fluorobiphenyl 69 30 - 119 05/18/12 07:14 05/20/12 22:51 1


Nitrobenzene-d5 64 05/18/12 07:14 05/20/12 22:51 130 - 115

Terphenyl-d14 89 05/18/12 07:14 05/20/12 22:51 136 - 134


Antimony 0.39 J B 2.5 0.33 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:14 1


1.3 0.27 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Arsenic 7.6

1.3 0.15 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Barium 110

0.25 0.062 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Cadmium 0.16 J

1.3 0.21 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Chromium 24

1.3 0.34 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Copper 29

0.63 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Lead 20

1.3 0.36 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Selenium 0.82 J

0.63 0.076 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Silver <0.63

2.5 0.86 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Zinc 63


Mercury 0.063 0.021 0.0064 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:36 1



pH 7.70 0.200 0.200 SU 05/16/12 16:56 1



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Lab Sample ID: 500-46374-19Client Sample ID: K7 (0-6")Matrix: SolidDate Collected: 05/07/12 16:30






0.075 0.018 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Anthracene <0.075






0.075 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Chrysene 0.050 J



0.075 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Fluorene <0.075



0.075 0.032 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Phenanthrene 0.046 J

0.075 0.027 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Pyrene 0.068 J

2-Fluorobiphenyl 60 30 - 119 05/18/12 07:14 05/20/12 23:07 1


Nitrobenzene-d5 51 05/18/12 07:14 05/20/12 23:07 130 - 115

Terphenyl-d14 98 05/18/12 07:14 05/20/12 23:07 136 - 134


Antimony 2.2 J B 4.6 0.61 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:35 1


2.3 0.50 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Arsenic 15

2.3 0.28 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Barium 120

0.46 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Cadmium <0.46

2.3 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Chromium 85

2.3 0.63 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Copper 320

1.2 0.40 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Lead 1900

2.3 0.66 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Selenium 2.2 J

1.2 0.14 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Silver <1.2

4.6 1.6 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Zinc 73


Mercury 0.052 0.038 0.011 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:41 1



pH 7.77 0.200 0.200 SU 05/16/12 16:59 1



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0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Anthracene <0.047






0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Chrysene <0.047



0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Fluorene <0.047




0.047 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Pyrene <0.047

2-Fluorobiphenyl 62 30 - 119 05/18/12 07:14 05/20/12 23:24 1


Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 23:24 130 - 115

Terphenyl-d14 88 05/18/12 07:14 05/20/12 23:24 136 - 134


Antimony 1.6 J B 2.9 0.39 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:41 1


1.5 0.32 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Arsenic 7.0

1.5 0.17 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Barium 150

0.29 0.072 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Cadmium 0.073 J

1.5 0.24 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Chromium 23

1.5 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Copper 21

0.73 0.25 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Lead 38

1.5 0.42 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Selenium 0.62 J

0.73 0.088 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Silver <0.73

2.9 1.0 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Zinc 59


Mercury 0.060 0.024 0.0073 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:43 1



pH 7.71 0.200 0.200 SU 05/16/12 17:01 1



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Lab Sample ID: 500-46374-23Client Sample ID: L5 (0-6")Matrix: SolidDate Collected: 05/09/12 15:20






0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Anthracene <0.052






0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Chrysene 0.012 J



0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Fluorene <0.052




0.052 0.019 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Pyrene <0.052

2-Fluorobiphenyl 73 30 - 119 05/18/12 07:14 05/20/12 23:41 1


Nitrobenzene-d5 66 05/18/12 07:14 05/20/12 23:41 130 - 115

Terphenyl-d14 98 05/18/12 07:14 05/20/12 23:41 136 - 134


Antimony 0.66 J B 3.0 0.40 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:47 1


1.5 0.33 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Arsenic 3.8

1.5 0.18 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Barium 78

0.30 0.075 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Cadmium 0.24 J

1.5 0.25 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Chromium 15

1.5 0.41 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Copper 23

0.75 0.26 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Lead 30

1.5 0.43 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Selenium <1.5

0.75 0.091 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Silver <0.75

3.0 1.0 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Zinc 49


Mercury 0.045 0.025 0.0076 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:45 1



pH 8.27 0.200 0.200 SU 05/16/12 17:03 1



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Definitions/GlossaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Qualifiers

GC/MS Semi VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

Metals



Qualifier

F MS or MSD exceeds the control limits

B Compound was found in the blank and sample.

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample

EDL Estimated Detection Limit

EPA United States Environmental Protection Agency

MDL Method Detection Limit

ML Minimum Level (Dioxin)

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RL Reporting Limit

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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QC Association SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


GC/MS Semi VOA

Prep Batch: 150126

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3541500-46374-1 E24 (0-6") Total/NA

Solid 3541500-46374-3 G9 (0-6") Total/NA

Solid 3541500-46374-5 G19 (0-6") Total/NA

Solid 3541500-46374-7 I9 (0-6") Total/NA

Solid 3541500-46374-9 I18 (0-6") Total/NA

Solid 3541500-46374-11 J4 (0-6") Total/NA

Solid 3541500-46374-13 J13 (0-6") Total/NA

Solid 3541500-46374-15 J15 (0-6") Total/NA

Solid 3541500-46374-17 J24 (0-6") Total/NA

Solid 3541500-46374-19 K7 (0-6") Total/NA

Solid 3541500-46374-21 K11 (0-6") Total/NA

Solid 3541500-46374-23 L5 (0-6") Total/NA

Solid 3541LCS 500-150126/2-A Lab Control Sample Total/NA

Solid 3541MB 500-150126/1-A Method Blank Total/NA

Analysis Batch: 150266


Solid 8270C 150126500-46374-1 E24 (0-6") Total/NA

Solid 8270C 150126500-46374-3 G9 (0-6") Total/NA

Solid 8270C 150126500-46374-5 G19 (0-6") Total/NA

Solid 8270C 150126500-46374-7 I9 (0-6") Total/NA

Solid 8270C 150126500-46374-9 I18 (0-6") Total/NA

Solid 8270C 150126500-46374-11 J4 (0-6") Total/NA

Solid 8270C 150126500-46374-13 J13 (0-6") Total/NA

Solid 8270C 150126500-46374-15 J15 (0-6") Total/NA

Solid 8270C 150126500-46374-17 J24 (0-6") Total/NA

Solid 8270C 150126500-46374-19 K7 (0-6") Total/NA

Solid 8270C 150126500-46374-21 K11 (0-6") Total/NA

Solid 8270C 150126500-46374-23 L5 (0-6") Total/NA

Solid 8270C 150126LCS 500-150126/2-A Lab Control Sample Total/NA

Solid 8270C 150126MB 500-150126/1-A Method Blank Total/NA

Metals

Prep Batch: 149954


Solid 7471A500-46374-1 E24 (0-6") Total/NA

Solid 7471A500-46374-1 DU E24 (0-6") Total/NA

Solid 7471A500-46374-1 MS E24 (0-6") Total/NA

Solid 7471A500-46374-1 MSD E24 (0-6") Total/NA

Solid 7471A500-46374-3 G9 (0-6") Total/NA

Solid 7471A500-46374-5 G19 (0-6") Total/NA

Solid 7471A500-46374-7 I9 (0-6") Total/NA

Solid 7471A500-46374-9 I18 (0-6") Total/NA

Solid 7471A500-46374-11 J4 (0-6") Total/NA

Solid 7471A500-46374-13 J13 (0-6") Total/NA

Solid 7471A500-46374-15 J15 (0-6") Total/NA

Solid 7471A500-46374-17 J24 (0-6") Total/NA

Solid 7471A500-46374-19 K7 (0-6") Total/NA

Solid 7471A500-46374-21 K11 (0-6") Total/NA

Solid 7471A500-46374-23 L5 (0-6") Total/NA

Solid 7471ALCS 500-149954/8-A Lab Control Sample Total/NA


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Metals (Continued)

Prep Batch: 149954 (Continued)


Solid 7471AMB 500-149954/7-A Method Blank Total/NA

Prep Batch: 150013


Solid 3050B500-46374-1 E24 (0-6") Total/NA

Solid 3050B500-46374-3 G9 (0-6") Total/NA

Solid 3050B500-46374-5 G19 (0-6") Total/NA

Solid 3050B500-46374-7 I9 (0-6") Total/NA

Solid 3050B500-46374-9 I18 (0-6") Total/NA

Solid 3050B500-46374-11 J4 (0-6") Total/NA

Solid 3050B500-46374-13 J13 (0-6") Total/NA

Solid 3050B500-46374-15 J15 (0-6") Total/NA

Solid 3050B500-46374-17 J24 (0-6") Total/NA

Solid 3050B500-46374-19 K7 (0-6") Total/NA

Solid 3050B500-46374-21 K11 (0-6") Total/NA

Solid 3050B500-46374-23 L5 (0-6") Total/NA

Solid 3050BLCS 500-150013/2-A Lab Control Sample Total/NA

Solid 3050BMB 500-150013/1-A Method Blank Total/NA



Solid 6010B 150013500-46374-1 E24 (0-6") Total/NA

Solid 6010B 150013500-46374-3 G9 (0-6") Total/NA

Solid 6010B 150013500-46374-5 G19 (0-6") Total/NA

Solid 6010B 150013500-46374-7 I9 (0-6") Total/NA

Solid 6010B 150013500-46374-9 I18 (0-6") Total/NA

Solid 6010B 150013500-46374-11 J4 (0-6") Total/NA

Solid 6010B 150013500-46374-13 J13 (0-6") Total/NA

Solid 6010B 150013500-46374-15 J15 (0-6") Total/NA

Solid 6010B 150013500-46374-17 J24 (0-6") Total/NA

Solid 6010B 150013500-46374-19 K7 (0-6") Total/NA

Solid 6010B 150013500-46374-21 K11 (0-6") Total/NA

Solid 6010B 150013500-46374-23 L5 (0-6") Total/NA

Solid 6010B 150013LCS 500-150013/2-A Lab Control Sample Total/NA

Solid 6010B 150013MB 500-150013/1-A Method Blank Total/NA



Solid 7471A 149954500-46374-1 E24 (0-6") Total/NA

Solid 7471A 149954500-46374-1 DU E24 (0-6") Total/NA

Solid 7471A 149954500-46374-1 MS E24 (0-6") Total/NA

Solid 7471A 149954500-46374-1 MSD E24 (0-6") Total/NA

Solid 7471A 149954500-46374-3 G9 (0-6") Total/NA

Solid 7471A 149954500-46374-5 G19 (0-6") Total/NA

Solid 7471A 149954500-46374-7 I9 (0-6") Total/NA

Solid 7471A 149954500-46374-9 I18 (0-6") Total/NA

Solid 7471A 149954500-46374-11 J4 (0-6") Total/NA

Solid 7471A 149954500-46374-13 J13 (0-6") Total/NA

Solid 7471A 149954500-46374-15 J15 (0-6") Total/NA

Solid 7471A 149954500-46374-17 J24 (0-6") Total/NA

Solid 7471A 149954500-46374-19 K7 (0-6") Total/NA

Solid 7471A 149954500-46374-21 K11 (0-6") Total/NA


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Metals (Continued)

Analysis Batch: 150190 (Continued)


Solid 7471A 149954500-46374-23 L5 (0-6") Total/NA

Solid 7471A 149954LCS 500-149954/8-A Lab Control Sample Total/NA

Solid 7471A 149954MB 500-149954/7-A Method Blank Total/NA

General Chemistry



Solid Moisture500-46374-1 E24 (0-6") Total/NA

Solid Moisture500-46374-3 G9 (0-6") Total/NA


Solid Moisture500-46374-7 I9 (0-6") Total/NA


Solid Moisture500-46374-11 J4 (0-6") Total/NA




Solid Moisture500-46374-19 K7 (0-6") Total/NA


Solid Moisture500-46374-23 L5 (0-6") Total/NA



Solid 9045C500-46374-1 E24 (0-6") Total/NA

Solid 9045C500-46374-3 G9 (0-6") Total/NA

Solid 9045C500-46374-5 G19 (0-6") Total/NA

Solid 9045C500-46374-7 I9 (0-6") Total/NA

Solid 9045C500-46374-9 I18 (0-6") Total/NA

Solid 9045C500-46374-11 J4 (0-6") Total/NA

Solid 9045C500-46374-13 J13 (0-6") Total/NA

Solid 9045C500-46374-15 J15 (0-6") Total/NA

Solid 9045C500-46374-17 J24 (0-6") Total/NA

Solid 9045C500-46374-19 K7 (0-6") Total/NA

Solid 9045C500-46374-21 K11 (0-6") Total/NA

Solid 9045C500-46374-23 L5 (0-6") Total/NA

Solid 9045C500-46374-23 DU L5 (0-6") Total/NA


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Surrogate SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-119) (30-115) (36-134)

FBP NBZ TPH

78 76 96500-46374-1

Percent Surrogate Recovery (Acceptance Limits)

E24 (0-6")

66 60 90500-46374-3 G9 (0-6")

71 60 96500-46374-5 G19 (0-6")

64 57 83500-46374-7 I9 (0-6")

76 70 102500-46374-9 I18 (0-6")

69 62 97500-46374-11 J4 (0-6")

60 49 86500-46374-13 J13 (0-6")

59 53 89500-46374-15 J15 (0-6")

69 64 89500-46374-17 J24 (0-6")

60 51 98500-46374-19 K7 (0-6")

62 60 88500-46374-21 K11 (0-6")

73 66 98500-46374-23 L5 (0-6")

83 80 88LCS 500-150126/2-A Lab Control Sample

79 76 109MB 500-150126/1-A Method Blank

Surrogate Legend

FBP = 2-Fluorobiphenyl

NBZ = Nitrobenzene-d5

TPH = Terphenyl-d14


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QC Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc


Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 500-150126/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 150266 Prep Batch: 150126

RL MDL

Acenaphthene <0.033 0.033 0.0099 mg/Kg 05/18/12 07:14 05/20/12 17:31 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

<0.033 0.00760.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Acenaphthylene

<0.033 0.00780.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Anthracene

<0.033 0.00700.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[a]anthracene

<0.033 0.00610.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[a]pyrene

<0.033 0.00650.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[b]fluoranthene

<0.033 0.0110.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[g,h,i]perylene

<0.033 0.00790.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[k]fluoranthene

<0.033 0.00750.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Chrysene

<0.033 0.00930.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Dibenz(a,h)anthracene

<0.033 0.0140.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Fluoranthene

<0.033 0.00760.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Fluorene

<0.033 0.0110.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Indeno[1,2,3-cd]pyrene

<0.033 0.00640.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Naphthalene

<0.033 0.0140.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Phenanthrene

<0.033 0.0120.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Pyrene

2-Fluorobiphenyl 79 30 - 119 05/20/12 17:31 1

MB MB

Surrogate

05/18/12 07:14

Dil FacPrepared AnalyzedQualifier Limits%Recovery

76 05/18/12 07:14 05/20/12 17:31 1Nitrobenzene-d5 30 - 115

109 05/18/12 07:14 05/20/12 17:31 1Terphenyl-d14 36 - 134

Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-150126/2-A



Acenaphthene 1.67 1.35 mg/Kg 81 67 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Acenaphthylene 1.67 1.38 mg/Kg 83 67 - 110

Anthracene 1.67 1.35 mg/Kg 81 67 - 112

Benzo[a]anthracene 1.67 1.48 mg/Kg 89 68 - 117

Benzo[a]pyrene 1.67 1.48 mg/Kg 89 64 - 118

Benzo[b]fluoranthene 1.67 1.67 mg/Kg 100 60 - 118

Benzo[g,h,i]perylene 1.67 1.17 mg/Kg 70 66 - 130

Benzo[k]fluoranthene 1.67 1.38 mg/Kg 83 56 - 129

Chrysene 1.67 1.38 mg/Kg 83 66 - 118

Dibenz(a,h)anthracene 1.67 1.30 mg/Kg 78 62 - 126

Fluoranthene 1.67 1.49 mg/Kg 89 68 - 121

Fluorene 1.67 1.41 mg/Kg 84 66 - 112

Indeno[1,2,3-cd]pyrene 1.67 1.26 mg/Kg 76 67 - 127

Naphthalene 1.67 1.32 mg/Kg 79 65 - 110

Phenanthrene 1.67 1.41 mg/Kg 84 66 - 118

Pyrene 1.67 1.40 mg/Kg 84 66 - 119

2-Fluorobiphenyl 30 - 119

Surrogate

83

LCS LCS

Qualifier Limits%Recovery

80Nitrobenzene-d5 30 - 115

88Terphenyl-d14 36 - 134


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Method: 6010B - Metals (ICP)




RL MDL

Antimony 0.280 J 2.0 0.27 mg/Kg 05/17/12 08:40 05/18/12 17:02 1

MB MB


<1.0 0.221.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Arsenic

<1.0 0.121.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Barium

<0.20 0.0500.20 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Cadmium

<1.0 0.171.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Chromium

<1.0 0.271.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Copper

<0.50 0.170.50 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Lead

<1.0 0.291.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Selenium

<0.50 0.0600.50 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Silver

<2.0 0.692.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Zinc




Antimony 50.0 44.9 mg/Kg 90 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 10.0 8.85 mg/Kg 88 80 - 120

Barium 200 189 mg/Kg 95 80 - 120

Cadmium 5.00 4.67 mg/Kg 93 80 - 120

Chromium 20.0 19.3 mg/Kg 96 80 - 120

Copper 25.0 24.0 mg/Kg 96 80 - 120

Lead 10.0 9.89 mg/Kg 99 80 - 120

Selenium 10.0 8.10 mg/Kg 81 80 - 120

Silver 5.00 4.62 mg/Kg 92 80 - 120

Zinc 50.0 47.0 mg/Kg 94 80 - 120

Method: 7471A - Mercury (CVAA)




RL MDL

Mercury <0.017 0.017 0.0051 mg/Kg 05/16/12 14:41 05/18/12 10:09 1

MB MB





Mercury 0.167 0.201 mg/Kg 120 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 MS



Mercury 0.035 0.0986 0.181 F mg/Kg 149 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


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Method: 7471A - Mercury (CVAA) (Continued)

Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 MSD



Mercury 0.035 0.105 0.188 F mg/Kg 146 75 - 125 3 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 DU



Mercury 0.035 0.0387 mg/Kg 10 20☼

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: 9045C - pH

Client Sample ID: L5 (0-6")Lab Sample ID: 500-46374-23 DU



pH 8.27 8.300 SU 0.4

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD


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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1


Client Sample ID: E24 (0-6") Lab Sample ID: 500-46374-1Matrix: SolidDate Collected: 05/09/12 10:31


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8270C 1 150266 05/20/12 20:37 DA TAL CHITotal/NA

Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA

Analysis 6010B 1 150123 05/18/12 18:24 TDS TAL CHITotal/NA

Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA

Analysis 7471A 1 150190 05/18/12 10:12 PFK TAL CHITotal/NA

Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA

Analysis 9045C 1 149927 TAB TAL CHITotal/NA

05/16/12 16:39

05/16/12 16:41

(Start)

(End)

Client Sample ID: G9 (0-6") Lab Sample ID: 500-46374-3Matrix: SolidDate Collected: 05/09/12 12:20


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:41

05/16/12 16:43

(Start)

(End)



Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:43

05/16/12 16:46

(Start)

(End)


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Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7Matrix: SolidDate Collected: 05/09/12 13:22


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:46

05/16/12 16:48

(Start)

(End)



Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:48

05/16/12 16:50

(Start)

(End)

Client Sample ID: J4 (0-6") Lab Sample ID: 500-46374-11Matrix: SolidDate Collected: 05/09/12 14:40


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:50

05/16/12 16:52

(Start)

(End)


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Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:52

05/16/12 16:54

(Start)

(End)



Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:54

05/16/12 16:56

(Start)

(End)



Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:56

05/16/12 16:59

(Start)

(End)


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Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19Matrix: SolidDate Collected: 05/07/12 16:30


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 16:59

05/16/12 17:01

(Start)

(End)



Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 17:01

05/16/12 17:03

(Start)

(End)

Client Sample ID: L5 (0-6") Lab Sample ID: 500-46374-23Matrix: SolidDate Collected: 05/09/12 15:20


Prep 3541 05/18/12 07:14 STW150126 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








05/16/12 17:03

05/16/12 17:05

(Start)

(End)




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Certification SummaryClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1


Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago R-194A2LAA2LA

TestAmerica Chicago 40461State ProgramAlabama 4

TestAmerica Chicago 01132CANELACCalifornia 9

TestAmerica Chicago E871072NELACFlorida 4

TestAmerica Chicago 939State ProgramGeorgia 4

TestAmerica Chicago N/AState ProgramGeorgia 4

TestAmerica Chicago N/AState ProgramHawaii 9

TestAmerica Chicago 100201NELACIllinois 5

TestAmerica Chicago C-IL-02State ProgramIndiana 5

TestAmerica Chicago 82State ProgramIowa 7

TestAmerica Chicago E-10161NELACKansas 7

TestAmerica Chicago 90023State ProgramKentucky 4

TestAmerica Chicago 66State ProgramKentucky (UST) 4

TestAmerica Chicago L2304DoD ELAPL-A-B

TestAmerica Chicago L2304ISO/IEC 17025L-A-B

TestAmerica Chicago 30720NELACLouisiana 6

TestAmerica Chicago M-IL035State ProgramMassachusetts 1

TestAmerica Chicago N/AState ProgramMississippi 4

TestAmerica Chicago 291State ProgramNorth Carolina DENR 4

TestAmerica Chicago R-194State ProgramNorth Dakota 8

TestAmerica Chicago 8908State ProgramOklahoma 6

TestAmerica Chicago 77001State ProgramSouth Carolina 4

TestAmerica Chicago T104704252-09-TXNELACTexas 6

TestAmerica Chicago P330-12-00038FederalUSDA

TestAmerica Chicago 460142NELACVirginia 3

TestAmerica Chicago 999580010State ProgramWisconsin 5

TestAmerica Chicago 8TMS-QState ProgramWyoming 8

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's

current list of certified methods and analytes.


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of 39 5/24/2012

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Login Sample Receipt Checklist

Client: Shaw Environmental & Infrastructure, Inc Job Number: 500-46374-1

SDG Number: 500-46374-1

Login Number: 46374

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

TrueRadioactivity either was not measured or, if measured, is at or below background

N/AThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice. 4.0

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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TestAmerica Job ID: 500-46374-3TestAmerica Sample Delivery Group: 500-46374-1Client Project/Site: Naperville Sportsman Club



Authorized for release by:6/14/2012 1:17:47 PM





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Table of Contents


TestAmerica Job ID: 500-46374-3SDG: 500-46374-1

Page 2 of 43TestAmerica Chicago

6/14/2012

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1


Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3


Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9


Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26



Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35


Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40


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Job ID: 500-46374-3


Narrative

Job Narrative

500-46374-3

Comments


Receipt

The samples were received on 5/16/2012 7:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 4.0º C.

GC/MS Semi VOA

Method(s) 8270C: The following samples were prepared outside the method defined holding time because the request for the test was

made after the holding time for the sample expired. G19 (6-12") (500-46374-6), I9 (6-12") (500-46374-8), J13 (6-12") (500-46374-14), J15

(6-12") (500-46374-16), K7 (6-12") (500-46374-20)


Metals

Method(s) 7471A: The following sample(s): 500-46374-6, 8, 14, 16, and 20 were prepared and/or analyzed outside the method defined

holding time for Hg because the request for the test was made after the holding time for the sample expired.

Method(s) D2974-87: A correction factor of 0.58 was applied to the calculation of FOC by Nelson and Sommers.


General Chemistry


Organic Prep


TestAmerica ChicagoPage 3 of 43 6/14/2012

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Barium

RL

0.50 mg/L

MDL

0.010


6010B TCLP1J0.44

Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0029 J

Lead 0.0075 mg/L0.0050 TCLP6010B10.66

Organic Matter at 440 Deg(C)

RL

0.10 %

RL

0.10


D2974-87 Total/NA13.9

FOC by Nelson and Sommers (0.58

factor)

0.058 %0.058 Total/NAD2974-8712.3


☼Antimony

RL

2.2 mg/Kg

MDL

0.29


6010B Total/NA1J0.43






☼Lead 0.54 mg/Kg0.19 Total/NA6010B19.0


Barium 0.50 mg/L0.010 TCLP6010B11.2

Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0052

Lead 0.0075 mg/L0.0050 TCLP6010B10.0065 J

pH 0.200 SU0.200 Total/NA9045C17.60


Arsenic

RL

0.050 mg/L

MDL

0.010


6010B TCLP10.066

Barium 0.50 mg/L0.010 TCLP6010B10.70


Lead 0.0075 mg/L0.0050 TCLP6010B19.0


RL

0.10 %

RL

0.10


D2974-87 Total/NA15.5


factor)

0.058 %0.058 Total/NAD2974-8713.2


☼Benzo[a]pyrene

RL

0.050 mg/Kg

MDL

0.0092


8270C Total/NA1J H0.016

☼Benzo[b]fluoranthene 0.050 mg/Kg0.0098 Total/NA8270C10.022 J H

☼Chrysene 0.050 mg/Kg0.011 Total/NA8270C10.020 J H

☼Fluoranthene 0.050 mg/Kg0.021 Total/NA8270C10.027 J H

☼Pyrene 0.050 mg/Kg0.018 Total/NA8270C10.021 J H

☼Antimony 3.0 mg/Kg0.39 Total/NA6010B10.45 J










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Client Sample ID: I9 (6-12") (Continued) Lab Sample ID: 500-46374-8

Barium

RL

0.50 mg/L

MDL

0.010


6010B TCLP1J0.43


Lead 0.0075 mg/L0.0050 TCLP6010B10.022

☼Mercury 0.025 mg/Kg0.0076 Total/NA7471A10.046 H

pH 0.200 SU0.200 Total/NA9045C17.68


Arsenic

RL

0.050 mg/L

MDL

0.010


6010B TCLP10.10

Barium 0.50 mg/L0.010 TCLP6010B10.59


Lead 0.0075 mg/L0.0050 TCLP6010B134


RL

0.10 %

RL

0.10


D2974-87 Total/NA17.0


factor)

0.058 %0.058 Total/NAD2974-8714.1


☼Acenaphthene

RL

0.054 mg/Kg

MDL

0.016



☼Anthracene 0.054 mg/Kg0.013 Total/NA8270C10.055 H

☼Benzo[a]anthracene 0.054 mg/Kg0.011 Total/NA8270C10.33 H

☼Benzo[a]pyrene 0.054 mg/Kg0.0098 Total/NA8270C10.46 H

☼Benzo[b]fluoranthene 0.054 mg/Kg0.011 Total/NA8270C10.63 H

☼Benzo[g,h,i]perylene 0.054 mg/Kg0.018 Total/NA8270C10.32 H

☼Benzo[k]fluoranthene 0.054 mg/Kg0.013 Total/NA8270C10.22 H

☼Chrysene 0.054 mg/Kg0.012 Total/NA8270C10.49 H

☼Dibenz(a,h)anthracene 0.054 mg/Kg0.015 Total/NA8270C10.072 H

☼Fluoranthene 0.054 mg/Kg0.022 Total/NA8270C10.75 H

☼Fluorene 0.054 mg/Kg0.012 Total/NA8270C10.038 J H

☼Indeno[1,2,3-cd]pyrene 0.054 mg/Kg0.018 Total/NA8270C10.27 H

☼Phenanthrene 0.054 mg/Kg0.023 Total/NA8270C10.11 H

☼Pyrene 0.054 mg/Kg0.020 Total/NA8270C10.57 H

☼Antimony 2.9 mg/Kg0.39 Total/NA6010B1480






☼Lead 73 mg/Kg25 Total/NA6010B100120000


☼Silver 0.73 mg/Kg0.088 Total/NA6010B11.7


Arsenic 0.050 mg/L0.010 TCLP6010B10.067

Barium 0.50 mg/L0.010 TCLP6010B10.81


Lead 0.75 mg/L0.50 TCLP6010B100120

☼Mercury 0.028 mg/Kg0.0085 Total/NA7471A10.026 J H

pH 0.200 SU0.200 Total/NA9045C17.08



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Arsenic

RL

0.050 mg/L

MDL

0.010


6010B TCLP1J0.012

Barium 0.50 mg/L0.010 TCLP6010B10.57


Lead 0.0075 mg/L0.0050 TCLP6010B18.4


RL

0.10 %

RL

0.10


D2974-87 Total/NA14.9


factor)

0.058 %0.058 Total/NAD2974-8712.8


☼Acenaphthene

RL

0.053 mg/Kg

MDL

0.016



☼Anthracene 0.053 mg/Kg0.013 Total/NA8270C10.027 J H

☼Benzo[a]anthracene 0.053 mg/Kg0.011 Total/NA8270C10.39 H

☼Benzo[a]pyrene 0.053 mg/Kg0.0098 Total/NA8270C10.62 H

☼Benzo[b]fluoranthene 0.053 mg/Kg0.010 Total/NA8270C10.72 H

☼Benzo[g,h,i]perylene 0.053 mg/Kg0.018 Total/NA8270C10.46 H

☼Benzo[k]fluoranthene 0.053 mg/Kg0.013 Total/NA8270C10.35 H

☼Chrysene 0.053 mg/Kg0.012 Total/NA8270C10.48 H

☼Dibenz(a,h)anthracene 0.053 mg/Kg0.015 Total/NA8270C10.11 H

☼Fluoranthene 0.053 mg/Kg0.022 Total/NA8270C10.50 H

☼Fluorene 0.053 mg/Kg0.012 Total/NA8270C10.020 J H

☼Indeno[1,2,3-cd]pyrene 0.053 mg/Kg0.018 Total/NA8270C10.40 H

☼Phenanthrene 0.053 mg/Kg0.023 Total/NA8270C10.13 H

☼Pyrene 0.053 mg/Kg0.019 Total/NA8270C10.48 H

☼Antimony 3.0 mg/Kg0.40 Total/NA6010B19.1









Arsenic 0.050 mg/L0.010 TCLP6010B10.023 J

Barium 0.50 mg/L0.010 TCLP6010B10.94


Lead 0.0075 mg/L0.0050 TCLP6010B123

Mercury 0.00020 mg/L0.000020 TCLP7470A10.000020 J H

☼Mercury 0.024 mg/Kg0.0073 Total/NA7471A10.034 H

pH 0.200 SU0.200 Total/NA9045C17.31


Arsenic

RL

0.050 mg/L

MDL

0.010


6010B TCLP1J0.021

Barium 0.50 mg/L0.010 TCLP6010B10.72


Lead 0.0075 mg/L0.0050 TCLP6010B12.7


RL

0.10 %

RL

0.10


D2974-87 Total/NA14.7


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Client Sample ID: K7 (0-6") (Continued) Lab Sample ID: 500-46374-19


factor)

RL

0.058 %

RL

0.058


D2974-87 Total/NA12.7


☼Benzo[a]pyrene

RL

0.041 mg/Kg

MDL

0.0075



☼Benzo[b]fluoranthene 0.041 mg/Kg0.0080 Total/NA8270C10.014 J H









Barium 0.50 mg/L0.010 TCLP6010B10.65


Lead 0.0075 mg/L0.0050 TCLP6010B10.026

☼Mercury 0.020 mg/Kg0.0060 Total/NA7471A10.014 J H

pH 0.200 SU0.200 Total/NA9045C17.64


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ASTMD2974-87 Ash Content TAL CHI



ASTM = ASTM International






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500-46374-5 G19 (0-6") Solid 05/09/12 16:08 05/16/12 07:00

500-46374-6 G19 (6-12") Solid 05/09/12 16:08 05/16/12 07:00

500-46374-7 I9 (0-6") Solid 05/09/12 13:22 05/16/12 07:00

500-46374-8 I9 (6-12") Solid 05/09/12 13:22 05/16/12 07:00

500-46374-13 J13 (0-6") Solid 05/07/12 13:40 05/16/12 07:00

500-46374-14 J13 (6-12") Solid 05/07/12 13:40 05/16/12 07:00

500-46374-15 J15 (0-6") Solid 05/07/12 13:00 05/16/12 07:00

500-46374-16 J15 (6-12") Solid 05/07/12 13:00 05/16/12 07:00

500-46374-19 K7 (0-6") Solid 05/07/12 16:30 05/16/12 07:00

500-46374-20 K7 (6-12") Solid 05/07/12 16:30 05/16/12 07:00


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Date Received: 05/16/12 07:00

Method: 6010B - Metals (ICP) - TCLPRL MDL

Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Barium 0.44 J

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:26 1Cadmium 0.0029 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:26 1Lead 0.66

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:26 1Silver <0.025

Method: 7470A - Mercury (CVAA) - TCLPRL MDL

Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:05 1


General ChemistryRL RL

Organic Matter at 440 Deg(C) 3.9 0.10 0.10 % 06/07/12 09:34 1


0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers

(0.58 factor)

2.3


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Acenaphthene <0.039 H 0.039 0.012 mg/Kg ☼ 06/07/12 07:07 06/08/12 12:52 1


0.039 0.0091 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Acenaphthylene <0.039 H

0.039 0.0093 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Anthracene <0.039 H

0.039 0.0083 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[a]anthracene <0.039 H

0.039 0.0072 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[a]pyrene <0.039 H

0.039 0.0077 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[b]fluoranthene <0.039 H

0.039 0.013 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[g,h,i]perylene <0.039 H

0.039 0.0095 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[k]fluoranthene <0.039 H

0.039 0.0090 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Chrysene <0.039 H

0.039 0.011 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Dibenz(a,h)anthracene <0.039 H

0.039 0.016 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Fluoranthene <0.039 H

0.039 0.0090 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Fluorene <0.039 H

0.039 0.013 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Indeno[1,2,3-cd]pyrene <0.039 H

0.039 0.0077 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Naphthalene <0.039 H

0.039 0.017 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Phenanthrene <0.039 H

0.039 0.014 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Pyrene <0.039 H

2-Fluorobiphenyl 53 30 - 119 06/07/12 07:07 06/08/12 12:52 1


Nitrobenzene-d5 47 06/07/12 07:07 06/08/12 12:52 130 - 115

Terphenyl-d14 71 06/07/12 07:07 06/08/12 12:52 136 - 134


Antimony 0.43 J 2.2 0.29 mg/Kg ☼ 06/06/12 10:14 06/06/12 21:52 1


1.1 0.24 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Arsenic 5.7

1.1 0.13 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Barium 60

0.22 0.054 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Cadmium 0.48

1.1 0.18 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Chromium 11

1.1 0.29 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Copper 21

0.54 0.19 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Lead 9.0

1.1 0.31 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Selenium <1.1

0.54 0.065 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Silver <0.54

2.2 0.74 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Zinc 35


Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Barium 1.2

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:30 1Cadmium 0.0052

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:30 1Lead 0.0065 J

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:30 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:06 1



Mercury <0.018 H 0.018 0.0054 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:03 1



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pH 7.60 0.200 0.200 SU 06/11/12 14:22 1



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Arsenic 0.066 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Barium 0.70

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:50 1Cadmium 0.0036 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:50 1Lead 9.0

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:50 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:08 1






(0.58 factor)

3.2


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0.050 0.0092 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[a]pyrene 0.016 J H

0.050 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[b]fluoranthene 0.022 J H



0.050 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Chrysene 0.020 J H


0.050 0.021 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Fluoranthene 0.027 J H

0.050 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Fluorene <0.050 H




0.050 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Pyrene 0.021 J H

2-Fluorobiphenyl 47 30 - 119 06/07/12 07:07 06/08/12 13:10 1


Nitrobenzene-d5 45 06/07/12 07:07 06/08/12 13:10 130 - 115

Terphenyl-d14 57 06/07/12 07:07 06/08/12 13:10 136 - 134


Antimony 0.45 J 3.0 0.39 mg/Kg ☼ 06/06/12 10:14 06/06/12 21:58 1


1.5 0.32 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Arsenic 3.8

1.5 0.18 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Barium 160

0.30 0.073 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Cadmium 0.47

1.5 0.25 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Chromium 21

1.5 0.40 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Copper 26

0.74 0.25 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Lead 57

1.5 0.42 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Selenium 1.0 J

0.74 0.089 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Silver <0.74

3.0 1.0 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Zinc 72


Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Barium 0.43 J

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:54 1Cadmium 0.0022 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:54 1Lead 0.022

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:54 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:10 1



Mercury 0.046 H 0.025 0.0076 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:05 1



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pH 7.68 0.200 0.200 SU 06/11/12 14:26 1



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Arsenic 0.10 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Barium 0.59

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:07 1Cadmium 0.0029 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:07 1Lead 34

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:07 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:15 1






(0.58 factor)

4.1


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Acenaphthene 0.031 J H 0.054 0.016 mg/Kg ☼ 06/07/12 07:07 06/08/12 13:27 1



0.054 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Anthracene 0.055 H

0.054 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[a]anthracene 0.33 H

0.054 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[a]pyrene 0.46 H

0.054 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[b]fluoranthene 0.63 H

0.054 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[g,h,i]perylene 0.32 H

0.054 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[k]fluoranthene 0.22 H

0.054 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Chrysene 0.49 H

0.054 0.015 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Dibenz(a,h)anthracene 0.072 H

0.054 0.022 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Fluoranthene 0.75 H

0.054 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Fluorene 0.038 J H

0.054 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Indeno[1,2,3-cd]pyrene 0.27 H


0.054 0.023 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Phenanthrene 0.11 H

0.054 0.020 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Pyrene 0.57 H

2-Fluorobiphenyl 53 30 - 119 06/07/12 07:07 06/08/12 13:27 1


Nitrobenzene-d5 42 06/07/12 07:07 06/08/12 13:27 130 - 115

Terphenyl-d14 58 06/07/12 07:07 06/08/12 13:27 136 - 134


Antimony 480 2.9 0.39 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:05 1


1.5 0.32 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Arsenic 310

1.5 0.17 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Barium 59

0.29 0.072 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Cadmium 0.42

1.5 0.24 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Chromium 14

1.5 0.40 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Copper 29

73 25 mg/Kg 06/06/12 10:14 06/07/12 13:17 100☼Lead 120000

1.5 0.42 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Selenium 0.68 J

0.73 0.088 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Silver 1.7

2.9 1.0 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Zinc 66


Arsenic 0.067 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Barium 0.81

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:11 1Cadmium 0.0058

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Chromium <0.025

0.75 0.50 mg/L 06/13/12 12:00 06/14/12 10:23 100Lead 120

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:11 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:17 1



Mercury 0.026 J H 0.028 0.0085 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:07 1



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pH 7.08 0.200 0.200 SU 06/11/12 14:29 1



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Arsenic 0.012 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Barium 0.57

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:15 1Cadmium 0.0024 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:15 1Lead 8.4

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:15 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:19 1






(0.58 factor)

2.8


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Acenaphthene 0.031 J H 0.053 0.016 mg/Kg ☼ 06/07/12 07:07 06/08/12 13:44 1



0.053 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Anthracene 0.027 J H

0.053 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[a]anthracene 0.39 H

0.053 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[a]pyrene 0.62 H

0.053 0.010 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[b]fluoranthene 0.72 H

0.053 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[g,h,i]perylene 0.46 H

0.053 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[k]fluoranthene 0.35 H

0.053 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Chrysene 0.48 H

0.053 0.015 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Dibenz(a,h)anthracene 0.11 H

0.053 0.022 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Fluoranthene 0.50 H

0.053 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Fluorene 0.020 J H

0.053 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Indeno[1,2,3-cd]pyrene 0.40 H


0.053 0.023 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Phenanthrene 0.13 H

0.053 0.019 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Pyrene 0.48 H

2-Fluorobiphenyl 60 30 - 119 06/07/12 07:07 06/08/12 13:44 1


Nitrobenzene-d5 50 06/07/12 07:07 06/08/12 13:44 130 - 115

Terphenyl-d14 71 06/07/12 07:07 06/08/12 13:44 136 - 134


Antimony 9.1 3.0 0.40 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:11 1


1.5 0.33 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Arsenic 14

1.5 0.18 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Barium 76

0.30 0.075 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Cadmium 0.32

1.5 0.25 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Chromium 15

1.5 0.41 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Copper 27

0.76 0.26 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Lead 2900

1.5 0.44 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Selenium 0.48 J

0.76 0.092 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Silver <0.76

3.0 1.0 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Zinc 64


Arsenic 0.023 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Barium 0.94

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:19 1Cadmium 0.0061

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:19 1Lead 23

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:19 1Silver <0.025


Mercury 0.000020 J H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:28 1



Mercury 0.034 H 0.024 0.0073 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:08 1



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pH 7.31 0.200 0.200 SU 06/11/12 14:32 1



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Arsenic 0.021 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Barium 0.72

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:23 1Cadmium 0.0039 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:23 1Lead 2.7

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:23 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:30 1






(0.58 factor)

2.7


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0.041 0.0075 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[a]pyrene 0.0095 J H

0.041 0.0080 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[b]fluoranthene 0.014 J H



0.041 0.0093 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Chrysene <0.041 H


0.041 0.017 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Fluoranthene <0.041 H

0.041 0.0094 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Fluorene <0.041 H




0.041 0.015 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Pyrene <0.041 H

2-Fluorobiphenyl 72 30 - 119 06/07/12 07:07 06/08/12 14:02 1


Nitrobenzene-d5 70 06/07/12 07:07 06/08/12 14:02 130 - 115

Terphenyl-d14 90 06/07/12 07:07 06/08/12 14:02 136 - 134


Antimony 0.87 J 2.3 0.30 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:17 1


1.1 0.25 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Arsenic 2.5

1.1 0.14 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Barium 63

0.23 0.056 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Cadmium 0.35

1.1 0.19 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Chromium 13

1.1 0.31 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Copper 20

0.57 0.20 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Lead 25

1.1 0.33 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Selenium <1.1

0.57 0.068 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Silver <0.57

2.3 0.78 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Zinc 44


Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1


0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Barium 0.65

0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:27 1Cadmium 0.0038 J

0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Chromium <0.025

0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:27 1Lead 0.026

0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Selenium <0.050

0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:27 1Silver <0.025


Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:31 1



Mercury 0.014 J H 0.020 0.0060 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:11 1



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pH 7.64 0.200 0.200 SU 06/11/12 14:36 1



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Qualifiers

GC/MS Semi VOA


H Sample was prepped or analyzed beyond the specified holding time

Qualifier


Metals


H Sample was prepped or analyzed beyond the specified holding time

Qualifier



Glossary



Abbreviation

%R Percent Recovery









QC Quality Control

RL Reporting Limit





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GC/MS Semi VOA

Prep Batch: 151984


Solid 3541500-46374-6 G19 (6-12") Total/NA

Solid 3541500-46374-8 I9 (6-12") Total/NA

Solid 3541500-46374-14 J13 (6-12") Total/NA

Solid 3541500-46374-16 J15 (6-12") Total/NA

Solid 3541500-46374-20 K7 (6-12") Total/NA





Solid 8270C 151984500-46374-6 G19 (6-12") Total/NA

Solid 8270C 151984500-46374-8 I9 (6-12") Total/NA

Solid 8270C 151984500-46374-14 J13 (6-12") Total/NA

Solid 8270C 151984500-46374-16 J15 (6-12") Total/NA

Solid 8270C 151984500-46374-20 K7 (6-12") Total/NA



Metals

Prep Batch: 151902


Solid 3050B500-46374-6 G19 (6-12") Total/NA

Solid 3050B500-46374-8 I9 (6-12") Total/NA

Solid 3050B500-46374-14 J13 (6-12") Total/NA

Solid 3050B500-46374-16 J15 (6-12") Total/NA

Solid 3050B500-46374-20 K7 (6-12") Total/NA





Solid 6010B 151902500-46374-6 G19 (6-12") Total/NA

Solid 6010B 151902500-46374-8 I9 (6-12") Total/NA

Solid 6010B 151902500-46374-14 J13 (6-12") Total/NA

Solid 6010B 151902500-46374-16 J15 (6-12") Total/NA

Solid 6010B 151902500-46374-20 K7 (6-12") Total/NA





Solid 6010B 151902500-46374-14 J13 (6-12") Total/NA

Prep Batch: 152273


Solid 7471A500-46374-6 G19 (6-12") Total/NA

Solid 7471A500-46374-8 I9 (6-12") Total/NA

Solid 7471A500-46374-14 J13 (6-12") Total/NA

Solid 7471A500-46374-16 J15 (6-12") Total/NA

Solid 7471A500-46374-20 K7 (6-12") Total/NA



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Metals (Continued)




Leach Batch: 152292


Solid 1311500-46374-5 G19 (0-6") TCLP

Solid 1311500-46374-6 G19 (6-12") TCLP

Solid 1311500-46374-7 I9 (0-6") TCLP

Solid 1311500-46374-8 I9 (6-12") TCLP

Solid 1311500-46374-8 DU I9 (6-12") TCLP

Solid 1311500-46374-8 MS I9 (6-12") TCLP

Solid 1311500-46374-13 J13 (0-6") TCLP

Solid 1311500-46374-14 J13 (6-12") TCLP

Solid 1311500-46374-15 J15 (0-6") TCLP

Solid 1311500-46374-16 J15 (6-12") TCLP

Solid 1311500-46374-19 K7 (0-6") TCLP

Solid 1311500-46374-20 K7 (6-12") TCLP

Solid 1311LB 500-152292/1-B LB Method Blank TCLP

Solid 1311LB 500-152292/1-C LB Method Blank TCLP



Solid 7471A 152273500-46374-6 G19 (6-12") Total/NA

Solid 7471A 152273500-46374-8 I9 (6-12") Total/NA

Solid 7471A 152273500-46374-14 J13 (6-12") Total/NA

Solid 7471A 152273500-46374-16 J15 (6-12") Total/NA

Solid 7471A 152273500-46374-20 K7 (6-12") Total/NA



Prep Batch: 152443


Solid 7470A 152292500-46374-5 G19 (0-6") TCLP

Solid 7470A 152292500-46374-6 G19 (6-12") TCLP

Solid 7470A 152292500-46374-7 I9 (0-6") TCLP

Solid 7470A 152292500-46374-8 I9 (6-12") TCLP

Solid 7470A 152292500-46374-8 DU I9 (6-12") TCLP

Solid 7470A 152292500-46374-8 MS I9 (6-12") TCLP

Solid 7470A 152292500-46374-13 J13 (0-6") TCLP

Solid 7470A 152292500-46374-14 J13 (6-12") TCLP

Solid 7470A 152292500-46374-15 J15 (0-6") TCLP

Solid 7470A 152292500-46374-16 J15 (6-12") TCLP

Solid 7470A 152292500-46374-19 K7 (0-6") TCLP

Solid 7470A 152292500-46374-20 K7 (6-12") TCLP

Solid 7470A 152292LB 500-152292/1-B LB Method Blank TCLP





Solid 7470A 152443500-46374-5 G19 (0-6") TCLP

Solid 7470A 152443500-46374-6 G19 (6-12") TCLP

Solid 7470A 152443500-46374-7 I9 (0-6") TCLP


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Metals (Continued)



Solid 7470A 152443500-46374-8 I9 (6-12") TCLP

Solid 7470A 152443500-46374-8 DU I9 (6-12") TCLP

Solid 7470A 152443500-46374-8 MS I9 (6-12") TCLP

Solid 7470A 152443500-46374-13 J13 (0-6") TCLP

Solid 7470A 152443500-46374-14 J13 (6-12") TCLP

Solid 7470A 152443500-46374-15 J15 (0-6") TCLP

Solid 7470A 152443500-46374-16 J15 (6-12") TCLP

Solid 7470A 152443500-46374-19 K7 (0-6") TCLP

Solid 7470A 152443500-46374-20 K7 (6-12") TCLP




Prep Batch: 152725


Solid 3010A 152292500-46374-5 G19 (0-6") TCLP

Solid 3010A 152292500-46374-6 G19 (6-12") TCLP

Solid 3010A 152292500-46374-7 I9 (0-6") TCLP

Solid 3010A 152292500-46374-8 I9 (6-12") TCLP

Solid 3010A 152292500-46374-13 J13 (0-6") TCLP

Solid 3010A 152292500-46374-14 J13 (6-12") TCLP

Solid 3010A 152292500-46374-15 J15 (0-6") TCLP

Solid 3010A 152292500-46374-16 J15 (6-12") TCLP

Solid 3010A 152292500-46374-19 K7 (0-6") TCLP

Solid 3010A 152292500-46374-20 K7 (6-12") TCLP

Solid 3010A 152292LB 500-152292/1-C LB Method Blank TCLP




Solid 6010B 152725500-46374-5 G19 (0-6") TCLP

Solid 6010B 152725500-46374-6 G19 (6-12") TCLP

Solid 6010B 152725500-46374-7 I9 (0-6") TCLP

Solid 6010B 152725500-46374-8 I9 (6-12") TCLP

Solid 6010B 152725500-46374-13 J13 (0-6") TCLP

Solid 6010B 152725500-46374-14 J13 (6-12") TCLP

Solid 6010B 152725500-46374-14 J13 (6-12") TCLP

Solid 6010B 152725500-46374-15 J15 (0-6") TCLP

Solid 6010B 152725500-46374-16 J15 (6-12") TCLP

Solid 6010B 152725500-46374-19 K7 (0-6") TCLP

Solid 6010B 152725500-46374-20 K7 (6-12") TCLP

Solid 6010B 152725LB 500-152292/1-C LB Method Blank TCLP


General Chemistry








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General Chemistry (Continued)











Solid D2974-87500-46374-5 G19 (0-6") Total/NA

Solid D2974-87500-46374-7 I9 (0-6") Total/NA

Solid D2974-87500-46374-13 J13 (0-6") Total/NA

Solid D2974-87500-46374-15 J15 (0-6") Total/NA

Solid D2974-87500-46374-19 K7 (0-6") Total/NA



Solid 9045C500-46374-6 G19 (6-12") Total/NA

Solid 9045C500-46374-8 I9 (6-12") Total/NA

Solid 9045C500-46374-14 J13 (6-12") Total/NA

Solid 9045C500-46374-16 J15 (6-12") Total/NA

Solid 9045C500-46374-20 K7 (6-12") Total/NA


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FBP NBZ TPH

53 47 71500-46374-6


G19 (6-12")

47 45 57500-46374-8 I9 (6-12")

53 42 58500-46374-14 J13 (6-12")

60 50 71500-46374-16 J15 (6-12")

72 70 90500-46374-20 K7 (6-12")


89 89 89MB 500-151984/1-A Method Blank

Surrogate Legend



TPH = Terphenyl-d14


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RL MDL


MB MB



<0.033 0.00780.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Anthracene






<0.033 0.00750.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Chrysene



<0.033 0.00760.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Fluorene




<0.033 0.0120.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Pyrene

2-Fluorobiphenyl 89 30 - 119 06/08/12 11:26 1

MB MB

Surrogate

06/07/12 07:07


89 06/07/12 07:07 06/08/12 11:26 1Nitrobenzene-d5 30 - 115

89 06/07/12 07:07 06/08/12 11:26 1Terphenyl-d14 36 - 134





Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Anthracene 1.67 1.37 mg/Kg 82 67 - 112






Chrysene 1.67 1.57 mg/Kg 94 66 - 118



Fluorene 1.67 1.51 mg/Kg 91 66 - 112




Pyrene 1.67 1.38 mg/Kg 83 66 - 119


Surrogate

89

LCS LCS





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RL MDL

Antimony <2.0 2.0 0.27 mg/Kg 06/06/12 10:14 06/06/12 20:48 1

MB MB


<1.0 0.221.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Arsenic

<1.0 0.121.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Barium

<0.20 0.0500.20 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Cadmium

<1.0 0.171.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Chromium

<1.0 0.271.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Copper

<0.50 0.170.50 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Lead

<1.0 0.291.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Selenium

<0.50 0.0600.50 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Silver

<2.0 0.692.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Zinc




Antimony 50.0 45.4 mg/Kg 91 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 10.0 8.74 mg/Kg 87 80 - 120

Barium 200 186 mg/Kg 93 80 - 120

Cadmium 5.00 4.65 mg/Kg 93 80 - 120

Chromium 20.0 19.5 mg/Kg 98 80 - 120

Copper 25.0 24.2 mg/Kg 97 80 - 120

Lead 10.0 9.60 mg/Kg 96 80 - 120

Selenium 10.0 8.22 mg/Kg 82 80 - 120

Silver 5.00 4.52 mg/Kg 90 80 - 120

Zinc 50.0 47.5 mg/Kg 95 80 - 120




Arsenic 0.100 0.0930 mg/L 93 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 2.00 1.94 mg/L 97 80 - 120

Cadmium 0.0500 0.0492 mg/L 98 80 - 120

Chromium 0.200 0.197 mg/L 99 80 - 120

Lead 0.100 0.0976 mg/L 98 80 - 120

Selenium 0.100 0.0886 mg/L 89 80 - 120

Silver 0.0500 0.0504 mg/L 101 80 - 120

Client Sample ID: Method BlankLab Sample ID: LB 500-152292/1-C LB

Matrix: Solid Prep Type: TCLP


RL MDL

Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:18 1

LB LB


<0.50 0.0100.50 mg/L 06/13/12 12:00 06/14/12 08:18 1Barium

<0.0050 0.00200.0050 mg/L 06/13/12 12:00 06/14/12 08:18 1Cadmium

<0.025 0.0100.025 mg/L 06/13/12 12:00 06/14/12 08:18 1Chromium

<0.0075 0.00500.0075 mg/L 06/13/12 12:00 06/14/12 08:18 1Lead


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Method: 6010B - Metals (ICP) (Continued)




RL MDL

Selenium <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:18 1

LB LB


<0.025 0.00500.025 mg/L 06/13/12 12:00 06/14/12 08:18 1Silver





RL MDL

Mercury <0.00020 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 11:49 1

MB MB





Mercury 0.00200 0.00199 mg/L 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 500-152292/1-B LB



RL MDL

Mercury 0.0000201 J 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:03 1

LB LB


Client Sample ID: I9 (6-12")Lab Sample ID: 500-46374-8 MS



Mercury <0.00020 H 0.00200 0.000968 H F mg/L 48 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: I9 (6-12")Lab Sample ID: 500-46374-8 DU



Mercury <0.00020 H <0.00020 H mg/L NC 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD





RL MDL

Mercury <0.017 0.017 0.0051 mg/Kg 06/09/12 10:05 06/09/12 14:00 1

MB MB



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Mercury 0.167 0.181 mg/Kg 108 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


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Leach 1311 06/09/12 13:30 PFK152292 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP

Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP

Analysis 7470A 1 152665 06/12/12 12:05 MBG TAL CHITCLP

Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP

Analysis 6010B 1 152812 06/14/12 08:26 TDS TAL CHITCLP


Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA



Prep 3541 06/07/12 07:07 STW151984 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8270C 1 152169 06/08/12 12:52 GES TAL CHITotal/NA




Analysis 7471A 1 152300 06/09/12 14:03 MBG TAL CHITotal/NA

Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP






Analysis 9045C 1 152439 CLM TAL CHITotal/NA

06/11/12 14:22

06/11/12 14:26

(Start)

(End)



Leach 1311 06/09/12 13:30 PFK152292 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP








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Prep 3541 06/07/12 07:07 STW151984 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













06/11/12 14:26

06/11/12 14:29

(Start)

(End)



Leach 1311 06/09/12 13:30 PFK152292 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP









Prep 3541 06/07/12 07:07 STW151984 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA












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Analysis 6010B 06/14/12 09:11 TDS1 152812 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP




06/11/12 14:29

06/11/12 14:32

(Start)

(End)



Leach 1311 06/09/12 13:30 PFK152292 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP









Prep 3541 06/07/12 07:07 STW151984 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













06/11/12 14:32

06/11/12 14:36

(Start)

(End)


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Leach 1311 06/09/12 13:30 PFK152292 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP









Prep 3541 06/07/12 07:07 STW151984 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













06/11/12 14:36

06/11/12 14:39

(Start)

(End)




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Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago 40461State ProgramAlabama 4

TestAmerica Chicago 01132CANELACCalifornia 9

TestAmerica Chicago E871072NELACFlorida 4

TestAmerica Chicago 939State ProgramGeorgia 4

TestAmerica Chicago N/AState ProgramGeorgia 4

TestAmerica Chicago N/AState ProgramHawaii 9

TestAmerica Chicago 100201NELACIllinois 5

TestAmerica Chicago C-IL-02State ProgramIndiana 5

TestAmerica Chicago 82State ProgramIowa 7

TestAmerica Chicago E-10161NELACKansas 7

TestAmerica Chicago 90023State ProgramKentucky 4

TestAmerica Chicago 66State ProgramKentucky (UST) 4

TestAmerica Chicago L2304DoD ELAPL-A-B

TestAmerica Chicago L2304ISO/IEC 17025L-A-B

TestAmerica Chicago 30720NELACLouisiana 6

TestAmerica Chicago M-IL035State ProgramMassachusetts 1

TestAmerica Chicago N/AState ProgramMississippi 4

TestAmerica Chicago 291State ProgramNorth Carolina DENR 4

TestAmerica Chicago R-194State ProgramNorth Dakota 8

TestAmerica Chicago 8908State ProgramOklahoma 6

TestAmerica Chicago 77001State ProgramSouth Carolina 4

TestAmerica Chicago T104704252-09-TXNELACTexas 6

TestAmerica Chicago P330-12-00038FederalUSDA

TestAmerica Chicago 460142NELACVirginia 3

TestAmerica Chicago 999580010State ProgramWisconsin 5

TestAmerica Chicago 8TMS-QState ProgramWyoming 8

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's

current list of certified methods and analytes.


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of 43 6/14/2012

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SDG Number: 500-46374-1

Login Number: 46374




List Number: 1

TrueRadioactivity either was not measured or, if measured, is at or below background

N/AThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.




TrueCOC is present.




TrueThere are no discrepancies between the sample IDs on the containers and the COC.








TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.





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Jeffrey.Cademartori

Text Box

SUPPLEMENTAL SEDIMENT SAMPLES


TestAmerica Job ID: 500-52298-1Client Project/Site: Naperville Sportsman Club



Authorized for release by:11/26/2012 12:00:57 PM





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Table of Contents


TestAmerica Job ID: 500-52298-1

Page 2 of 104TestAmerica Chicago

11/26/2012

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1


Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3


Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16


Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66



Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88


Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101


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Project/Site: Naperville Sportsman Club

Job ID: 500-52298-1


Narrative

Job Narrative

500-52298-1

Comments


Receipt

The samples were received on 11/13/2012 1:30 PM; the samples arrived in good condition, properly preserved and, where required, on

ice. The temperature of the cooler at receipt was 3.2º C.

GC/MS Semi VOA

Method(s) 8270C: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample -10 were outside control limits for two and

nine analytes, respectively. The associated laboratory control sample (LCS) recovery met the marginal exceedence acceptance

criteria.H10 (N30') (0-6") (500-52298-10)

Method(s) 8270C: The following samples were diluted due to the abundance of non-target analytes (hydrocarbon background): H10 (N30')

(0-6") (500-52298-10), J17 (N30;W20') (0-6") (500-52298-19), K12 (W25') (12-18') (500-52298-24). Elevated reporting limits (RLs) are

provided.


Metals

Method(s) 6010B: The extraction blank (LB) for preparation batch 170228 contained Pb above the reporting limit (RL). The associated

samples, 500-52298-21-24, contained detects for this analyte at concentrations greater than 10X the value found in the method blank;

therefore, re-extraction and/or re-analysis of samples was not performed.

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-52298-1 were outside control limits for

Sb. The MS was also out for Cu, and the MSD was also out for Se. The associated laboratory control sample (LCS) recovery met

acceptance criteria.

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) precision for sample 500-52298-1 was outside control limits for Cu.

The associated laboratory control sample (LCS) met acceptance criteria.

Method(s) 7470A: The continuing calibration verification (CCV) at line 45 in AD batch 170438 recoverd above the upper control limit for Hg.

The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

Method(s) 7470A: The laboratory control sample (LCS) for batch 170438 exceeded control limits for Hg. These analytes were biased high

in the LCS and were not detected in the associated samples; therefore, the data have been reported.

Method(s) 7470A: The matrix spike (MS) recovery for sample 52298-1 was outside control limits for Hg. The associated laboratory control

sample (LCS) recovery met acceptance criteria.


General Chemistry


Organic Prep



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Client Sample ID: F20 (0-6") Lab Sample ID: 500-52298-1


RL

0.053 mg/Kg

MDL

0.011





☼Benzo[g,h,i]perylene 0.053 mg/Kg0.018 Total/NA8270C10.046 J











☼Chromium 1.6 mg/Kg0.27 Total/NA6010B19.4





Barium 0.50 mg/L0.010 TCLP6010B10.45 J

Lead 0.0075 mg/L0.0050 TCLP6010B10.014


pH 0.200 SU0.200 Total/NA9045C17.82


☼Chrysene

RL

0.041 mg/Kg

MDL

0.0092











Barium 0.50 mg/L0.010 TCLP6010B10.64


Lead 0.0075 mg/L0.0050 TCLP6010B10.0077


pH 0.200 SU0.200 Total/NA9045C17.95


☼Antimony

RL

2.4 mg/Kg

MDL

0.32









TestAmerica Chicago

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Client Sample ID: F20 (12-18") (Continued) Lab Sample ID: 500-52298-3

☼Selenium

RL

1.2 mg/Kg

MDL

0.35




Barium 0.50 mg/L0.010 TCLP6010B10.73


Mercury 0.00020 mg/L0.000020 TCLP7470A10.000022 J *


pH 0.200 SU0.200 Total/NA9045C17.84

Client Sample ID: H20 (E20') (0-6") Lab Sample ID: 500-52298-4


RL

0.096 mg/Kg

MDL

0.020


















Lead 0.0075 mg/L0.0050 TCLP6010B10.051



pH 0.200 SU0.200 Total/NA9045C17.71


☼Antimony

RL

2.2 mg/Kg

MDL

0.29










Barium 0.50 mg/L0.010 TCLP6010B10.82



pH 0.200 SU0.200 Total/NA9045C17.95


☼Antimony

RL

2.4 mg/Kg

MDL

0.32



TestAmerica Chicago

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Client Sample ID: H20 (E20') (12-18") (Continued) Lab Sample ID: 500-52298-6

☼Arsenic

RL

1.2 mg/Kg

MDL

0.26


6010B Total/NA117







Barium 0.50 mg/L0.010 TCLP6010B10.71



pH 0.200 SU0.200 Total/NA9045C17.96

Client Sample ID: K10 (W25') (0-6") Lab Sample ID: 500-52298-7


RL

0.095 mg/Kg

MDL

0.020








☼Dibenz(a,h)anthracene 0.095 mg/Kg0.027 Total/NA8270C10.050 J





☼Antimony 270 mg/Kg36 Total/NA6010B506900








☼Silver 1.4 mg/Kg0.16 Total/NA6010B112



Barium 0.50 mg/L0.010 TCLP6010B10.54


Lead 0.0075 mg/L0.0050 TCLP6010B19.3



pH 0.200 SU0.200 Total/NA9045C17.31



RL

0.069 mg/Kg

MDL

0.014







TestAmerica Chicago

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Client Sample ID: K10 (W25') (6-12") (Continued) Lab Sample ID: 500-52298-8

☼Chrysene

RL

0.069 mg/Kg

MDL

0.016


8270C Total/NA10.10
















Lead 0.0075 mg/L0.0050 TCLP6010B143



pH 0.200 SU0.200 Total/NA9045C17.34


☼Antimony

RL

2.4 mg/Kg

MDL

0.32













Lead 0.0075 mg/L0.0050 TCLP6010B10.74



pH 0.200 SU0.200 Total/NA9045C17.53

Client Sample ID: H10 (N30') (0-6") Lab Sample ID: 500-52298-10


RL

0.21 mg/Kg

MDL

0.045











TestAmerica Chicago

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Client Sample ID: H10 (N30') (0-6") (Continued) Lab Sample ID: 500-52298-10

☼Antimony

RL

2.4 mg/Kg

MDL

0.32


6010B Total/NA1J1.5









Barium 0.50 mg/L0.010 TCLP6010B10.57


Lead 0.0075 mg/L0.0050 TCLP6010B10.47



pH 0.200 SU0.200 Total/NA9045C17.34


☼Arsenic

RL

1.2 mg/Kg

MDL

0.27


6010B Total/NA16.0







Barium 0.50 mg/L0.010 TCLP6010B10.72


Lead 0.0075 mg/L0.0050 TCLP6010B10.010


pH 0.200 SU0.200 Total/NA9045C17.45


☼Antimony

RL

2.1 mg/Kg

MDL

0.28










Barium 0.50 mg/L0.010 TCLP6010B10.77

Lead 0.0075 mg/L0.0050 TCLP6010B10.013



pH 0.200 SU0.200 Total/NA9045C17.54


TestAmerica Chicago

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RL

0.044 mg/Kg

MDL

0.0093





☼Naphthalene 0.044 mg/Kg0.0085 Total/NA8270C10.0087 J









Barium 0.50 mg/L0.010 TCLP6010B10.71

Lead 0.0075 mg/L0.0050 TCLP6010B10.0060 J



pH 0.200 SU0.200 Total/NA9045C17.53


☼Arsenic

RL

1.3 mg/Kg

MDL

0.29


6010B Total/NA15.4










Lead 0.0075 mg/L0.0050 TCLP6010B10.012



pH 0.200 SU0.200 Total/NA9045C17.68


☼Arsenic

RL

1.2 mg/Kg

MDL

0.26


6010B Total/NA15.5










Lead 0.0075 mg/L0.0050 TCLP6010B10.0073 J



TestAmerica Chicago

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pH

RL

0.200 SU

MDL

0.200


9045C Total/NA17.43

Client Sample ID: L6 (W20') (0-6") Lab Sample ID: 500-52298-16

☼Antimony

RL

2.5 mg/Kg

MDL

0.34













Lead 0.0075 mg/L0.0050 TCLP6010B10.0093



pH 0.200 SU0.200 Total/NA9045C17.14


☼Antimony

RL

2.3 mg/Kg

MDL

0.31












Barium 0.50 mg/L0.010 TCLP6010B10.88


Lead 0.0075 mg/L0.0050 TCLP6010B10.0076



pH 0.200 SU0.200 Total/NA9045C18.09


☼Antimony

RL

2.2 mg/Kg

MDL

0.29










TestAmerica Chicago

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Client Sample ID: L6 (W20') (12-18") (Continued) Lab Sample ID: 500-52298-18

Barium

RL

0.50 mg/L

MDL

0.010


6010B TCLP11.1


Lead 0.0075 mg/L0.0050 TCLP6010B10.0066 J



pH 0.200 SU0.200 Total/NA9045C18.11

Client Sample ID: J17 (N30;W20') (0-6") Lab Sample ID: 500-52298-19


RL

0.37 mg/Kg

MDL

0.078


8270C Total/NA50.46




















Lead 0.0075 mg/L0.0050 TCLP6010B10.12



pH 0.200 SU0.200 Total/NA9045C17.70


☼Anthracene

RL

0.093 mg/Kg

MDL

0.022















☼Antimony 260 mg/Kg35 Total/NA6010B505900

TestAmerica Chicago

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Client Sample ID: J17 (N30;W20') (6-12") (Continued) Lab Sample ID: 500-52298-20

☼Arsenic

RL

2.6 mg/Kg

MDL

0.57


6010B Total/NA11900







☼Silver 1.3 mg/Kg0.16 Total/NA6010B14.2



Barium 0.50 mg/L0.010 TCLP6010B10.54


Lead 0.0075 mg/L0.0050 TCLP6010B13.0



pH 0.200 SU0.200 Total/NA9045C17.30



RL

0.044 mg/Kg

MDL

0.0092


8270C Total/NA10.16




















Barium 0.50 mg/L0.010 TCLP6010B10.66

Lead 0.0075 mg/L0.0050 TCLP6010B10.66 B

Mercury 0.00020 mg/L0.000020 TCLP7470A10.000026 J B


pH 0.200 SU0.200 Total/NA9045C17.41

Client Sample ID: K12 (W25') (0-6') Lab Sample ID: 500-52298-22


RL

0.060 mg/Kg

MDL

0.013





TestAmerica Chicago

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Client Sample ID: K12 (W25') (0-6') (Continued) Lab Sample ID: 500-52298-22

☼Benzo[g,h,i]perylene

RL

0.060 mg/Kg

MDL

0.020





☼Dibenz(a,h)anthracene 0.060 mg/Kg0.017 Total/NA8270C10.020 J















Lead 0.0075 mg/L0.0050 TCLP6010B10.85 B


pH 0.200 SU0.200 Total/NA9045C17.33



RL

0.060 mg/Kg

MDL

0.013




















Barium 0.50 mg/L0.010 TCLP6010B10.60


Lead 0.075 mg/L0.050 TCLP6010B1073 B

Mercury 0.00020 mg/L0.000020 TCLP7470A10.000034 J B


pH 0.200 SU0.200 Total/NA9045C17.44


TestAmerica Chicago

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Client Sample ID: K12 (W25') (12-18') (Continued) Lab Sample ID: 500-52298-24


RL

0.24 mg/Kg

MDL

0.048
















Barium 0.50 mg/L0.010 TCLP6010B10.84


Lead 0.0075 mg/L0.0050 TCLP6010B18.6 B


pH 0.200 SU0.200 Total/NA9045C17.45

TestAmerica Chicago

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TestAmerica Chicago

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500-52298-1 F20 (0-6") Solid 11/09/12 13:15 11/13/12 13:30

500-52298-2 F20 (6-12") Solid 11/09/12 13:16 11/13/12 13:30

500-52298-3 F20 (12-18") Solid 11/09/12 13:17 11/13/12 13:30

500-52298-4 H20 (E20') (0-6") Solid 11/09/12 12:25 11/13/12 13:30

500-52298-5 H20 (E20') (6-12") Solid 11/09/12 12:26 11/13/12 13:30

500-52298-6 H20 (E20') (12-18") Solid 11/09/12 12:27 11/13/12 13:30

500-52298-7 K10 (W25') (0-6") Solid 11/09/12 11:50 11/13/12 13:30

500-52298-8 K10 (W25') (6-12") Solid 11/09/12 11:51 11/13/12 13:30

500-52298-9 K10 (W25') (12-18") Solid 11/09/12 11:52 11/13/12 13:30

500-52298-10 H10 (N30') (0-6") Solid 11/08/12 11:45 11/13/12 13:30

500-52298-11 H10 (N30') (6-12") Solid 11/08/12 11:46 11/13/12 13:30

500-52298-12 H10 (N30') (12-18") Solid 11/08/12 11:47 11/13/12 13:30

500-52298-13 J8 (0-6") Solid 11/08/12 12:00 11/13/12 13:30

500-52298-14 J8 (6-12") Solid 11/08/12 12:01 11/13/12 13:30

500-52298-15 J8 (12-18") Solid 11/08/12 12:02 11/13/12 13:30

500-52298-16 L6 (W20') (0-6") Solid 11/08/12 13:20 11/13/12 13:30

500-52298-17 L6 (W20') (6-12") Solid 11/08/12 13:21 11/13/12 13:30

500-52298-18 L6 (W20') (12-18") Solid 11/08/12 13:22 11/13/12 13:30

500-52298-19 J17 (N30;W20') (0-6") Solid 11/08/12 14:40 11/13/12 13:30

500-52298-20 J17 (N30;W20') (6-12") Solid 11/08/12 14:41 11/13/12 13:30

500-52298-21 J17 (N30;W20') (12-18") Solid 11/08/12 14:42 11/13/12 13:30

500-52298-22 K12 (W25') (0-6') Solid 11/08/12 13:55 11/13/12 13:30

500-52298-23 K12 (W25') (6-12') Solid 11/08/12 13:56 11/13/12 13:30

500-52298-24 K12 (W25') (12-18') Solid 11/08/12 13:57 11/13/12 13:30

TestAmerica Chicago

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Lab Sample ID: 500-52298-1Client Sample ID: F20 (0-6")Matrix: SolidDate Collected: 11/09/12 13:15






0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Anthracene <0.053




0.053 0.018 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[g,h,i]perylene 0.046 J


0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Chrysene 0.082



0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Fluorene <0.053




0.053 0.019 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Pyrene 0.12

2-Fluorobiphenyl 59 30 - 119 11/20/12 16:54 11/24/12 17:55 1


Nitrobenzene-d5 47 11/20/12 16:54 11/24/12 17:55 130 - 115

Terphenyl-d14 72 11/20/12 16:54 11/24/12 17:55 136 - 134


Antimony 0.75 J 3.3 0.43 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:26 1


1.6 0.36 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Arsenic 5.1

1.6 0.19 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Barium 55

0.33 0.081 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Cadmium 0.44

1.6 0.27 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Chromium 9.4

1.6 0.44 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Copper 18

0.82 0.28 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Lead 34

1.6 0.47 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Selenium 0.79 J

0.82 0.098 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Silver <0.82

3.3 1.1 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Zinc 59


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Barium 0.45 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 21:49 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 21:49 1Lead 0.014

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 21:49 1Silver <0.025


Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:37 1


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Mercury 0.031 0.025 0.0096 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:10 1



pH 7.82 0.200 0.200 SU 11/15/12 09:24 1


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0.041 0.0096 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Anthracene <0.041






0.041 0.0092 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Chrysene 0.012 J



0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Fluorene <0.041




0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Pyrene <0.041

2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/24/12 18:15 1


Nitrobenzene-d5 48 11/20/12 16:54 11/24/12 18:15 130 - 115

Terphenyl-d14 54 11/20/12 16:54 11/24/12 18:15 136 - 134


Antimony 0.75 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:48 1


1.1 0.24 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Arsenic 4.7

1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Barium 32

0.22 0.055 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Cadmium 0.27

1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Chromium 7.5

1.1 0.30 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Copper 13

0.55 0.19 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Lead 15

1.1 0.32 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Selenium <1.1

0.55 0.067 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Silver <0.55

2.2 0.76 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Zinc 37


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Barium 0.64

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 21:55 1Cadmium 0.0024 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 21:55 1Lead 0.0077

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 21:55 1Silver <0.025


Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:46 1


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Mercury 0.030 0.020 0.0076 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:12 1



pH 7.95 0.200 0.200 SU 11/15/12 09:27 1


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0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Anthracene <0.040






0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Chrysene <0.040



0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Fluorene <0.040




0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Pyrene <0.040

2-Fluorobiphenyl 65 30 - 119 11/20/12 16:54 11/24/12 18:34 1


Nitrobenzene-d5 60 11/20/12 16:54 11/24/12 18:34 130 - 115

Terphenyl-d14 60 11/20/12 16:54 11/24/12 18:34 136 - 134


Antimony 0.79 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:53 1


1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Arsenic 12

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Barium 44

0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Cadmium 0.29

1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Chromium 12

1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Copper 29

0.60 0.21 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Lead 18

1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Selenium 0.48 J

0.60 0.072 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Silver <0.60

2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Zinc 51


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Barium 0.73

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:02 1Cadmium 0.0021 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:02 1Lead <0.0075

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:02 1Silver <0.025


Mercury 0.000022 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:48 1


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Mercury 0.029 0.019 0.0073 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:18 1



pH 7.84 0.200 0.200 SU 11/15/12 09:30 1


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Lab Sample ID: 500-52298-4Client Sample ID: H20 (E20') (0-6")Matrix: SolidDate Collected: 11/09/12 12:25






0.096 0.023 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Anthracene <0.096






0.096 0.022 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Chrysene 0.052 J



0.096 0.022 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Fluorene <0.096




0.096 0.035 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Pyrene 0.048 J

2-Fluorobiphenyl 38 30 - 119 11/20/12 16:54 11/24/12 18:54 1


Nitrobenzene-d5 30 11/20/12 16:54 11/24/12 18:54 130 - 115

Terphenyl-d14 38 11/20/12 16:54 11/24/12 18:54 136 - 134


Antimony 2.8 J 5.9 0.78 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:58 1


2.9 0.64 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Arsenic 7.1

2.9 0.35 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Barium 81

0.59 0.15 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Cadmium 0.62

2.9 0.49 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Chromium 12

2.9 0.80 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Copper 22

1.5 0.51 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Lead 110

2.9 0.85 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Selenium <2.9

1.5 0.18 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Silver <1.5

5.9 2.0 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Zinc 64


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Barium 0.49 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:08 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:08 1Lead 0.051

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:08 1Silver <0.025


Mercury 0.000025 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:50 1


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Mercury 0.034 J 0.046 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:26 1



pH 7.71 0.200 0.200 SU 11/15/12 09:32 1


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0.040 0.0096 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Anthracene <0.040






0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Chrysene <0.040



0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Fluorene <0.040




0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Pyrene <0.040

2-Fluorobiphenyl 61 30 - 119 11/20/12 16:54 11/24/12 19:14 1


Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 19:14 130 - 115

Terphenyl-d14 58 11/20/12 16:54 11/24/12 19:14 136 - 134


Antimony 0.68 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:12 1


1.1 0.24 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Arsenic 8.6

1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Barium 55

0.22 0.054 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Cadmium 0.23

1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Chromium 15

1.1 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Copper 25

0.54 0.19 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Lead 16

1.1 0.31 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Selenium <1.1

0.54 0.065 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Silver <0.54

2.2 0.74 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Zinc 59


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Barium 0.82

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:39 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:39 1Lead <0.0075

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:39 1Silver <0.025


Mercury 0.000041 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:51 1


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Mercury 0.020 0.019 0.0074 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:28 1



pH 7.95 0.200 0.200 SU 11/15/12 09:35 1


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0.041 0.0096 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Anthracene <0.041






0.041 0.0092 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Chrysene <0.041



0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Fluorene <0.041




0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Pyrene <0.041

2-Fluorobiphenyl 65 30 - 119 11/20/12 16:54 11/24/12 19:33 1


Nitrobenzene-d5 58 11/20/12 16:54 11/24/12 19:33 130 - 115

Terphenyl-d14 67 11/20/12 16:54 11/24/12 19:33 136 - 134


Antimony 0.57 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:17 1


1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Arsenic 17

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Barium 60

0.24 0.059 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Cadmium 0.19 J

1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Chromium 15

1.2 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Copper 24

0.60 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Lead 15

1.2 0.34 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Selenium <1.2

0.60 0.072 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Silver <0.60

2.4 0.82 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Zinc 52


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Barium 0.71

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:45 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:45 1Lead <0.0075

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:45 1Silver <0.025


Mercury 0.000022 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:53 1


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Mercury 0.037 0.020 0.0076 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:30 1



pH 7.96 0.200 0.200 SU 11/15/12 09:37 1


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Lab Sample ID: 500-52298-7Client Sample ID: K10 (W25') (0-6")Matrix: SolidDate Collected: 11/09/12 11:50






0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Anthracene <0.095






0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Chrysene 0.13

0.095 0.027 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Dibenz(a,h)anthracene 0.050 J


0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Fluorene <0.095




0.095 0.035 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Pyrene 0.12

2-Fluorobiphenyl 60 30 - 119 11/20/12 16:54 11/24/12 19:53 1


Nitrobenzene-d5 48 11/20/12 16:54 11/24/12 19:53 130 - 115

Terphenyl-d14 62 11/20/12 16:54 11/24/12 19:53 136 - 134


Antimony 6900 270 36 mg/Kg ☼ 11/13/12 16:30 11/20/12 11:17 50


2.7 0.59 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Arsenic 2200

2.7 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Barium 87

0.54 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Cadmium 2.6

2.7 0.45 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Chromium 8.9

2.7 0.74 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Copper 23

68 23 mg/Kg 11/13/12 16:30 11/20/12 11:17 50☼Lead 150000

2.7 0.78 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Selenium 2.0 J

1.4 0.16 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Silver 12

5.4 1.9 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Zinc 60


Arsenic 0.11 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Barium 0.54

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:06 1Cadmium 0.0041 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:06 1Lead 9.3

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:06 1Silver <0.025


Mercury 0.000020 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:55 1


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Mercury 0.044 J 0.045 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:32 1



pH 7.31 0.200 0.200 SU 11/15/12 09:40 1


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0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Anthracene <0.069






0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Chrysene 0.10



0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Fluorene <0.069




0.069 0.025 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Pyrene 0.14

2-Fluorobiphenyl 58 30 - 119 11/20/12 16:54 11/24/12 20:12 1


Nitrobenzene-d5 45 11/20/12 16:54 11/24/12 20:12 130 - 115

Terphenyl-d14 67 11/20/12 16:54 11/24/12 20:12 136 - 134


Antimony 4.8 4.1 0.54 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:26 1


2.0 0.44 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Arsenic 7.1

2.0 0.24 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Barium 110

0.41 0.10 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Cadmium 0.52

2.0 0.34 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Chromium 13

2.0 0.55 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Copper 22

1.0 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Lead 950

2.0 0.58 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Selenium <2.0

1.0 0.12 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Silver <1.0

4.1 1.4 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Zinc 82


Arsenic 0.42 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Barium 1.1

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:12 1Cadmium 0.0048 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:12 1Lead 43

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:12 1Silver <0.025


Mercury 0.000023 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:56 1


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Mercury 0.067 0.033 0.013 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:34 1



pH 7.34 0.200 0.200 SU 11/15/12 09:43 1


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0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Anthracene <0.040






0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Chrysene <0.040



0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Fluorene <0.040




0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Pyrene <0.040

2-Fluorobiphenyl 51 30 - 119 11/20/12 16:54 11/24/12 20:32 1


Nitrobenzene-d5 50 11/20/12 16:54 11/24/12 20:32 130 - 115

Terphenyl-d14 53 11/20/12 16:54 11/24/12 20:32 136 - 134


Antimony 0.99 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:30 1


1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Arsenic 5.3

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Barium 77

0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Cadmium 0.27

1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Chromium 10

1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Copper 16

0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Lead 15

1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Selenium 0.58 J

0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Silver <0.61

2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Zinc 46


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Barium 1.2

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:18 1Cadmium 0.0045 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:18 1Lead 0.74

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:18 1Silver <0.025


Mercury 0.000026 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:58 1


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Mercury 0.010 J 0.021 0.0078 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:35 1



pH 7.53 0.200 0.200 SU 11/15/12 09:48 1


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Lab Sample ID: 500-52298-10Client Sample ID: H10 (N30') (0-6")Matrix: SolidDate Collected: 11/08/12 11:45






0.21 0.051 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Anthracene <0.21






0.21 0.049 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Chrysene 0.24



0.21 0.049 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Fluorene <0.21




0.21 0.078 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Pyrene 0.15 J

2-Fluorobiphenyl 73 30 - 119 11/20/12 16:54 11/24/12 20:52 5


Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 20:52 530 - 115

Terphenyl-d14 83 11/20/12 16:54 11/24/12 20:52 536 - 134


Antimony 1.5 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:34 1


1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Arsenic 7.1

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Barium 81

0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Cadmium 0.41

1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Chromium 14

1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Copper 20

0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Lead 72

1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Selenium <1.2

0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Silver <0.61

2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Zinc 87


Arsenic 0.015 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Barium 0.57

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:24 1Cadmium 0.0027 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:24 1Lead 0.47

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:24 1Silver <0.025


Mercury 0.000025 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:00 1


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Mercury 0.038 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:41 1



pH 7.34 0.200 0.200 SU 11/15/12 09:50 1


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0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Anthracene <0.040






0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Chrysene <0.040



0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Fluorene <0.040




0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Pyrene <0.040

2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/24/12 21:11 1


Nitrobenzene-d5 53 11/20/12 16:54 11/24/12 21:11 130 - 115

Terphenyl-d14 62 11/20/12 16:54 11/24/12 21:11 136 - 134


Antimony <2.4 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:38 1


1.2 0.27 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Arsenic 6.0

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Barium 130

0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Cadmium 0.20 J

1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Chromium 18

1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Copper 22

0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Lead 19

1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Selenium <1.2

0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Silver <0.61

2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Zinc 62


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Barium 0.72

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:31 1Cadmium 0.0020 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:31 1Lead 0.010

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:31 1Silver <0.025


Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:08 1


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Mercury 0.034 0.021 0.0079 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:43 1



pH 7.45 0.200 0.200 SU 11/15/12 09:53 1


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0.040 0.0094 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Anthracene <0.040






0.040 0.0090 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Chrysene <0.040



0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Fluorene <0.040




0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Pyrene <0.040

2-Fluorobiphenyl 54 30 - 119 11/20/12 16:54 11/24/12 21:31 1


Nitrobenzene-d5 55 11/20/12 16:54 11/24/12 21:31 130 - 115

Terphenyl-d14 61 11/20/12 16:54 11/24/12 21:31 136 - 134


Antimony 0.64 J 2.1 0.28 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:43 1


1.1 0.23 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Arsenic 7.6

1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Barium 110

0.21 0.052 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Cadmium 0.21

1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Chromium 13

1.1 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Copper 22

0.53 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Lead 15

1.1 0.30 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Selenium <1.1

0.53 0.064 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Silver <0.53

2.1 0.72 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Zinc 59


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Barium 0.77

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:37 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:37 1Lead 0.013

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:37 1Silver <0.025


Mercury 0.000028 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:10 1


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Mercury 0.030 0.019 0.0071 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:44 1



pH 7.54 0.200 0.200 SU 11/15/12 09:55 1


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0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Anthracene <0.044






0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Chrysene 0.017 J



0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Fluorene <0.044


0.044 0.0085 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Naphthalene 0.0087 J


0.044 0.016 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Pyrene <0.044

2-Fluorobiphenyl 54 30 - 119 11/20/12 16:54 11/24/12 21:51 1


Nitrobenzene-d5 47 11/20/12 16:54 11/24/12 21:51 130 - 115

Terphenyl-d14 59 11/20/12 16:54 11/24/12 21:51 136 - 134


Antimony <2.3 2.3 0.31 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:48 1


1.2 0.25 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Arsenic 7.8

1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Barium 100

0.23 0.058 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Cadmium 0.37

1.2 0.19 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Chromium 15

1.2 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Copper 24

0.58 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Lead 25

1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Selenium 0.67 J

0.58 0.070 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Silver <0.58

2.3 0.80 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Zinc 77


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Barium 0.71

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:43 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:43 1Lead 0.0060 J

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:43 1Silver <0.025


Mercury 0.000020 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:12 1


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Mercury 0.042 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:46 1



pH 7.53 0.200 0.200 SU 11/15/12 09:58 1


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0.046 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Anthracene <0.046






0.046 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Chrysene <0.046



0.046 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Fluorene <0.046




0.046 0.017 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Pyrene <0.046

2-Fluorobiphenyl 48 30 - 119 11/20/12 16:54 11/24/12 22:11 1


Nitrobenzene-d5 43 11/20/12 16:54 11/24/12 22:11 130 - 115

Terphenyl-d14 49 11/20/12 16:54 11/24/12 22:11 136 - 134


Antimony <2.6 2.6 0.35 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:52 1


1.3 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Arsenic 5.4

1.3 0.16 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Barium 120

0.26 0.065 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Cadmium 0.44

1.3 0.22 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Chromium 18

1.3 0.36 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Copper 19

0.66 0.23 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Lead 27

1.3 0.38 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Selenium 0.50 J

0.66 0.079 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Silver <0.66

2.6 0.90 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Zinc 98


Arsenic 0.012 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Barium 0.40 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:49 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:49 1Lead 0.012

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:49 1Silver <0.025


Mercury 0.000043 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:13 1


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Mercury 0.051 0.022 0.0084 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:48 1



pH 7.68 0.200 0.200 SU 11/15/12 10:01 1


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0.045 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Anthracene <0.045






0.045 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Chrysene <0.045



0.045 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Fluorene <0.045




0.045 0.016 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Pyrene <0.045

2-Fluorobiphenyl 47 30 - 119 11/20/12 16:54 11/24/12 22:31 1


Nitrobenzene-d5 44 11/20/12 16:54 11/24/12 22:31 130 - 115

Terphenyl-d14 52 11/20/12 16:54 11/24/12 22:31 136 - 134


Antimony <2.4 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:06 1


1.2 0.26 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Arsenic 5.5

1.2 0.14 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Barium 110

0.24 0.060 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Cadmium 0.22 J

1.2 0.20 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Chromium 18

1.2 0.33 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Copper 23

0.60 0.21 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Lead 23

1.2 0.35 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Selenium 0.47 J

0.60 0.072 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Silver <0.60

2.4 0.83 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Zinc 66


Arsenic 0.011 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Barium 0.43 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:55 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:55 1Lead 0.0073 J

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:55 1Silver <0.025


Mercury 0.000026 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:15 1


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Mercury 0.040 0.020 0.0077 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:50 1



pH 7.43 0.200 0.200 SU 11/15/12 10:03 1


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Lab Sample ID: 500-52298-16Client Sample ID: L6 (W20') (0-6")Matrix: SolidDate Collected: 11/08/12 13:20






0.041 0.0098 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Anthracene <0.041






0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Chrysene <0.041



0.041 0.0095 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Fluorene <0.041




0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Pyrene <0.041

2-Fluorobiphenyl 59 30 - 119 11/20/12 16:54 11/24/12 22:50 1


Nitrobenzene-d5 54 11/20/12 16:54 11/24/12 22:50 130 - 115

Terphenyl-d14 59 11/20/12 16:54 11/24/12 22:50 136 - 134


Antimony 0.45 J 2.5 0.34 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:11 1


1.3 0.28 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Arsenic 2.6

1.3 0.15 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Barium 76

0.25 0.063 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Cadmium 0.30

1.3 0.21 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Chromium 13

1.3 0.35 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Copper 16

0.64 0.22 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Lead 12

1.3 0.37 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Selenium 0.41 J

0.64 0.077 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Silver <0.64

2.5 0.87 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Zinc 52


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1


0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Barium 1.3

0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:02 1Cadmium 0.0021 J

0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:02 1Lead 0.0093

0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:02 1Silver <0.025


Mercury 0.000032 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:17 1


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Mercury 0.028 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:52 1



pH 7.14 0.200 0.200 SU 11/15/12 10:06 1


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0.041 0.0097 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Anthracene <0.041






0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Chrysene <0.041



0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Fluorene <0.041




0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Pyrene <0.041

2-Fluorobiphenyl 68 30 - 119 11/20/12 16:54 11/24/12 23:10 1


Nitrobenzene-d5 66 11/20/12 16:54 11/24/12 23:10 130 - 115

Terphenyl-d14 60 11/20/12 16:54 11/24/12 23:10 136 - 134


Antimony 0.54 J 2.3 0.31 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:16 1


1.2 0.25 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Arsenic 4.2

1.2 0.14 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Barium 37

0.23 0.057 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Cadmium 0.37

1.2 0.19 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Chromium 8.0

1.2 0.31 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Copper 28

0.58 0.20 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Lead 15

1.2 0.33 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Selenium 0.82 J

0.58 0.070 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Silver 0.082 J

2.3 0.79 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Zinc 58


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1


0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Barium 0.88

0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:23 1Cadmium 0.0044 J

0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:23 1Lead 0.0076

0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:23 1Silver <0.025


Mercury 0.000027 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:18 1


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Mercury 0.023 0.018 0.0069 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:54 1



pH 8.09 0.200 0.200 SU 11/15/12 10:08 1


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0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Anthracene <0.040






0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Chrysene <0.040



0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Fluorene <0.040




0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Pyrene <0.040

2-Fluorobiphenyl 58 30 - 119 11/20/12 16:54 11/24/12 23:30 1


Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 23:30 130 - 115

Terphenyl-d14 59 11/20/12 16:54 11/24/12 23:30 136 - 134


Antimony 0.79 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:21 1


1.1 0.24 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Arsenic 1.8

1.1 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Barium 78

0.22 0.055 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Cadmium 0.26

1.1 0.18 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Chromium 14

1.1 0.30 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Copper 19

0.55 0.19 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Lead 15

1.1 0.32 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Selenium <1.1

0.55 0.066 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Silver <0.55

2.2 0.76 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Zinc 54


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1


0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Barium 1.1

0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:29 1Cadmium 0.0022 J

0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:29 1Lead 0.0066 J

0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:29 1Silver <0.025


Mercury 0.000024 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:20 1


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Mercury 0.016 J 0.019 0.0074 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:56 1



pH 8.11 0.200 0.200 SU 11/15/12 10:11 1


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Lab Sample ID: 500-52298-19Client Sample ID: J17 (N30;W20') (0-6")Matrix: SolidDate Collected: 11/08/12 14:40






0.37 0.088 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Anthracene <0.37






0.37 0.084 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Chrysene 0.63



0.37 0.085 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Fluorene <0.37




0.37 0.14 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Pyrene 0.62

2-Fluorobiphenyl 56 30 - 119 11/20/12 16:54 11/24/12 23:50 5


Nitrobenzene-d5 46 11/20/12 16:54 11/24/12 23:50 530 - 115

Terphenyl-d14 74 11/20/12 16:54 11/24/12 23:50 536 - 134


Antimony 11 4.3 0.57 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:26 1


2.2 0.47 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Arsenic 15

2.2 0.26 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Barium 54

0.43 0.11 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Cadmium 0.47

2.2 0.36 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Chromium 11

2.2 0.59 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Copper 25

1.1 0.37 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Lead 2600

2.2 0.62 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Selenium <2.2

1.1 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Silver <1.1

4.3 1.5 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Zinc 71


Arsenic 0.026 J 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1


0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Barium 0.46 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:35 1Cadmium 0.0048 J

0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:35 1Lead 0.12

0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:35 1Silver <0.025


Mercury 0.000023 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:22 1


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Mercury 0.058 0.037 0.014 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:58 1



pH 7.70 0.200 0.200 SU 11/15/12 10:13 1


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0.093 0.021 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Chrysene 0.90



0.093 0.021 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Fluorene 0.031 J




0.093 0.034 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Pyrene 0.85

2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/25/12 00:09 1


Nitrobenzene-d5 47 11/20/12 16:54 11/25/12 00:09 130 - 115

Terphenyl-d14 58 11/20/12 16:54 11/25/12 00:09 136 - 134


Antimony 5900 260 35 mg/Kg ☼ 11/13/12 16:30 11/20/12 11:21 50


2.6 0.57 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Arsenic 1900

2.6 0.31 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Barium 75

0.52 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Cadmium 3.0

2.6 0.44 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Chromium 10

2.6 0.71 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Copper 27

66 23 mg/Kg 11/13/12 16:30 11/20/12 11:21 50☼Lead 110000

2.6 0.75 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Selenium 1.2 J

1.3 0.16 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Silver 4.2

5.2 1.8 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Zinc 99


Arsenic 0.047 J 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1


0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Barium 0.54

0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:41 1Cadmium 0.0043 J

0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:41 1Lead 3.0

0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:41 1Silver <0.025


Mercury 0.000038 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:24 1


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Mercury 0.047 0.045 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:03 1



pH 7.30 0.200 0.200 SU 11/15/12 10:16 1


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0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Anthracene <0.044






0.044 0.0099 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Chrysene 0.17



0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Fluorene <0.044




0.044 0.016 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Pyrene 0.15

2-Fluorobiphenyl 72 30 - 119 11/20/12 17:12 11/25/12 00:29 1


Nitrobenzene-d5 63 11/20/12 17:12 11/25/12 00:29 130 - 115

Terphenyl-d14 68 11/20/12 17:12 11/25/12 00:29 136 - 134


Antimony 4.9 2.5 0.34 mg/Kg ☼ 11/14/12 08:30 11/15/12 17:53 1


1.3 0.28 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Arsenic 9.1

1.3 0.15 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Barium 50

0.25 0.063 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Cadmium 0.34

1.3 0.21 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Chromium 12

1.3 0.34 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Copper 20

0.64 0.22 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Lead 890

1.3 0.37 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Selenium 0.56 J

0.64 0.076 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Silver <0.64

2.5 0.87 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Zinc 58


Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Barium 0.66

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:42 1Cadmium <0.0050

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 19:42 1Lead 0.66 B

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:42 1Silver <0.025


Mercury 0.000026 J B 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:07 1


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Mercury 0.027 0.020 0.0078 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:39 1



pH 7.41 0.200 0.200 SU 11/15/12 10:19 1


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Lab Sample ID: 500-52298-22Client Sample ID: K12 (W25') (0-6')Matrix: SolidDate Collected: 11/08/12 13:55






0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Anthracene <0.060






0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Chrysene 0.053 J

0.060 0.017 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Dibenz(a,h)anthracene 0.020 J


0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Fluorene <0.060




0.060 0.022 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Pyrene 0.058 J

2-Fluorobiphenyl 62 30 - 119 11/20/12 17:12 11/25/12 00:49 1


Nitrobenzene-d5 51 11/20/12 17:12 11/25/12 00:49 130 - 115

Terphenyl-d14 61 11/20/12 17:12 11/25/12 00:49 136 - 134


Antimony 27 3.7 0.49 mg/Kg ☼ 11/14/12 08:30 11/15/12 17:57 1


1.9 0.40 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Arsenic 22

1.9 0.22 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Barium 62

0.37 0.092 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Cadmium 0.37

1.9 0.31 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Chromium 12

1.9 0.50 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Copper 22

0.93 0.32 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Lead 4200

1.9 0.53 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Selenium <1.9

0.93 0.11 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Silver <0.93

3.7 1.3 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Zinc 62


Arsenic 0.017 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Barium 0.40 J

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:48 1Cadmium 0.0045 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 19:48 1Lead 0.85 B

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:48 1Silver <0.025


Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:12 1


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Mercury 0.046 0.031 0.012 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:41 1



pH 7.33 0.200 0.200 SU 11/15/12 10:21 1


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0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Anthracene <0.060






0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Chrysene 0.040 J



0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Fluorene <0.060




0.060 0.022 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Pyrene 0.039 J

2-Fluorobiphenyl 44 30 - 119 11/20/12 17:12 11/25/12 01:08 1


Nitrobenzene-d5 35 11/20/12 17:12 11/25/12 01:08 130 - 115

Terphenyl-d14 44 11/20/12 17:12 11/25/12 01:08 136 - 134


Antimony 43 3.2 0.42 mg/Kg ☼ 11/14/12 08:30 11/15/12 18:01 1


1.6 0.34 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Arsenic 32

1.6 0.19 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Barium 87

0.32 0.078 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Cadmium 0.59

1.6 0.26 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Chromium 13

1.6 0.43 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Copper 25

0.79 0.27 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Lead 4600

1.6 0.45 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Selenium 1.1 J

0.79 0.095 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Silver <0.79

3.2 1.1 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Zinc 82


Arsenic 0.32 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Barium 0.60

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:55 1Cadmium 0.0055

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Chromium <0.025

0.075 0.050 mg/L 11/19/12 08:00 11/20/12 11:25 10Lead 73 B

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:55 1Silver <0.025


Mercury 0.000034 J B 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:14 1


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Mercury 0.042 0.028 0.011 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:42 1



pH 7.44 0.200 0.200 SU 11/15/12 10:24 1


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0.24 0.058 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Anthracene <0.24






0.24 0.055 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Chrysene 0.11 J



0.24 0.056 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Fluorene <0.24




0.24 0.089 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Pyrene 0.16 J

2-Fluorobiphenyl 62 30 - 119 11/20/12 17:12 11/25/12 01:28 5


Nitrobenzene-d5 50 11/20/12 17:12 11/25/12 01:28 530 - 115

Terphenyl-d14 69 11/20/12 17:12 11/25/12 01:28 536 - 134


Antimony 2.4 J 2.6 0.35 mg/Kg ☼ 11/14/12 08:30 11/15/12 18:05 1


1.3 0.29 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Arsenic 8.0

1.3 0.16 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Barium 82

0.26 0.065 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Cadmium 0.35

1.3 0.22 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Chromium 15

1.3 0.36 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Copper 21

0.66 0.23 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Lead 530

1.3 0.38 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Selenium 0.57 J

0.66 0.079 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Silver <0.66

2.6 0.91 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Zinc 66


Arsenic 0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1


0.50 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Barium 0.84

0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 20:40 1Cadmium 0.0042 J

0.025 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Chromium <0.025

0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 20:40 1Lead 8.6 B

0.050 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Selenium <0.050

0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 20:40 1Silver <0.025


Mercury <0.00020 ^ 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:19 1


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Mercury 0.037 0.022 0.0086 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:48 1



pH 7.45 0.200 0.200 SU 11/15/12 10:26 1


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Qualifiers

GC/MS Semi VOA



Qualifier


Metals



Qualifier

* LCS or LCSD exceeds the control limits


F RPD of the MS and MSD exceeds the control limits

B Compound was found in the blank and sample.

4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not

applicable.

^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC exceeds the control limits.

Glossary



Abbreviation

%R Percent Recovery


DER Duplicate error ratio (normalized absolute difference)


DLC Decision level concentration



MDA Minimum detectable activity

MDC Minimum detectable concentration





QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)




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GC/MS Semi VOA

Prep Batch: 170477


Solid 3541500-52298-1 F20 (0-6") Total/NA

Solid 3541500-52298-2 F20 (6-12") Total/NA

Solid 3541500-52298-3 F20 (12-18") Total/NA

Solid 3541500-52298-4 H20 (E20') (0-6") Total/NA

Solid 3541500-52298-5 H20 (E20') (6-12") Total/NA

Solid 3541500-52298-6 H20 (E20') (12-18") Total/NA

Solid 3541500-52298-7 K10 (W25') (0-6") Total/NA

Solid 3541500-52298-8 K10 (W25') (6-12") Total/NA

Solid 3541500-52298-9 K10 (W25') (12-18") Total/NA

Solid 3541500-52298-10 H10 (N30') (0-6") Total/NA

Solid 3541500-52298-10 MS H10 (N30') (0-6") Total/NA

Solid 3541500-52298-10 MSD H10 (N30') (0-6") Total/NA

Solid 3541500-52298-11 H10 (N30') (6-12") Total/NA

Solid 3541500-52298-12 H10 (N30') (12-18") Total/NA

Solid 3541500-52298-13 J8 (0-6") Total/NA

Solid 3541500-52298-14 J8 (6-12") Total/NA

Solid 3541500-52298-15 J8 (12-18") Total/NA

Solid 3541500-52298-16 L6 (W20') (0-6") Total/NA

Solid 3541500-52298-17 L6 (W20') (6-12") Total/NA

Solid 3541500-52298-18 L6 (W20') (12-18") Total/NA

Solid 3541500-52298-19 J17 (N30;W20') (0-6") Total/NA




Prep Batch: 170478



Solid 3541500-52298-22 K12 (W25') (0-6') Total/NA

Solid 3541500-52298-23 K12 (W25') (6-12') Total/NA

Solid 3541500-52298-24 K12 (W25') (12-18') Total/NA















Solid 8270C 170477500-52298-1 F20 (0-6") Total/NA

Solid 8270C 170477500-52298-2 F20 (6-12") Total/NA

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GC/MS Semi VOA (Continued)



Solid 8270C 170477500-52298-3 F20 (12-18") Total/NA

Solid 8270C 170477500-52298-4 H20 (E20') (0-6") Total/NA



Solid 8270C 170477500-52298-7 K10 (W25') (0-6") Total/NA



Solid 8270C 170477500-52298-10 H10 (N30') (0-6") Total/NA

Solid 8270C 170477500-52298-10 MS H10 (N30') (0-6") Total/NA

Solid 8270C 170477500-52298-10 MSD H10 (N30') (0-6") Total/NA



Solid 8270C 170477500-52298-13 J8 (0-6") Total/NA

Solid 8270C 170477500-52298-14 J8 (6-12") Total/NA

Solid 8270C 170477500-52298-15 J8 (12-18") Total/NA

Solid 8270C 170477500-52298-16 L6 (W20') (0-6") Total/NA



Solid 8270C 170477500-52298-19 J17 (N30;W20') (0-6") Total/NA



Solid 8270C 170478500-52298-22 K12 (W25') (0-6') Total/NA



Metals

Prep Batch: 169568


Solid 3050B500-52298-1 F20 (0-6") Total/NA

Solid 3050B500-52298-1 DU F20 (0-6") Total/NA

Solid 3050B500-52298-1 MS F20 (0-6") Total/NA

Solid 3050B500-52298-1 MSD F20 (0-6") Total/NA

Solid 3050B500-52298-2 F20 (6-12") Total/NA

Solid 3050B500-52298-3 F20 (12-18") Total/NA

Solid 3050B500-52298-4 H20 (E20') (0-6") Total/NA



Solid 3050B500-52298-7 K10 (W25') (0-6") Total/NA



Solid 3050B500-52298-10 H10 (N30') (0-6") Total/NA



Solid 3050B500-52298-13 J8 (0-6") Total/NA

Solid 3050B500-52298-14 J8 (6-12") Total/NA

Solid 3050B500-52298-15 J8 (12-18") Total/NA

Solid 3050B500-52298-16 L6 (W20') (0-6") Total/NA



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Metals (Continued)



Solid 3050B500-52298-19 J17 (N30;W20') (0-6") Total/NA




Prep Batch: 169626



Solid 3050B500-52298-22 K12 (W25') (0-6') Total/NA







Solid 6010B 169626500-52298-21 J17 (N30;W20') (12-18") Total/NA

Solid 6010B 169626500-52298-22 K12 (W25') (0-6') Total/NA





Leach Batch: 170018


Solid 1311500-52298-1 F20 (0-6") TCLP

Solid 1311500-52298-1 DU F20 (0-6") TCLP

Solid 1311500-52298-1 MS F20 (0-6") TCLP

Solid 1311500-52298-2 F20 (6-12") TCLP

Solid 1311500-52298-3 F20 (12-18") TCLP

Solid 1311500-52298-4 H20 (E20') (0-6") TCLP

Solid 1311500-52298-4 DU H20 (E20') (0-6") TCLP

Solid 1311500-52298-4 MS H20 (E20') (0-6") TCLP

Solid 1311500-52298-5 H20 (E20') (6-12") TCLP

Solid 1311500-52298-6 H20 (E20') (12-18") TCLP

Solid 1311500-52298-7 K10 (W25') (0-6") TCLP

Solid 1311500-52298-8 K10 (W25') (6-12") TCLP

Solid 1311500-52298-9 K10 (W25') (12-18") TCLP

Solid 1311500-52298-10 H10 (N30') (0-6") TCLP

Solid 1311500-52298-11 H10 (N30') (6-12") TCLP

Solid 1311500-52298-12 H10 (N30') (12-18") TCLP

Solid 1311500-52298-13 J8 (0-6") TCLP

Solid 1311500-52298-14 J8 (6-12") TCLP

Solid 1311500-52298-15 J8 (12-18") TCLP

Solid 1311500-52298-16 L6 (W20') (0-6") TCLP

Solid 1311500-52298-17 L6 (W20') (6-12") TCLP

Solid 1311500-52298-18 L6 (W20') (12-18") TCLP

Solid 1311500-52298-19 J17 (N30;W20') (0-6") TCLP

Solid 1311500-52298-20 J17 (N30;W20') (6-12") TCLP


Solid 1311LB 500-170018/1-C LB Method Blank TCLP

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Metals (Continued)

Leach Batch: 170019


Solid 1311500-52298-21 J17 (N30;W20') (12-18") TCLP

Solid 1311500-52298-21 DU J17 (N30;W20') (12-18") TCLP

Solid 1311500-52298-21 MS J17 (N30;W20') (12-18") TCLP

Solid 1311500-52298-22 K12 (W25') (0-6') TCLP

Solid 1311500-52298-23 K12 (W25') (6-12') TCLP

Solid 1311500-52298-23 DU K12 (W25') (6-12') TCLP

Solid 1311500-52298-23 MS K12 (W25') (6-12') TCLP

Solid 1311500-52298-24 K12 (W25') (12-18') TCLP


Solid 1311LB 500-170019/1-E LB Method Blank TCLP

Prep Batch: 170225


Solid 3010A 170018500-52298-1 F20 (0-6") TCLP

Solid 3010A 170018500-52298-2 F20 (6-12") TCLP

Solid 3010A 170018500-52298-3 F20 (12-18") TCLP

Solid 3010A 170018500-52298-4 H20 (E20') (0-6") TCLP

Solid 3010A 170018500-52298-4 DU H20 (E20') (0-6") TCLP

Solid 3010A 170018500-52298-4 MS H20 (E20') (0-6") TCLP

Solid 3010A 170018500-52298-5 H20 (E20') (6-12") TCLP

Solid 3010A 170018500-52298-6 H20 (E20') (12-18") TCLP

Solid 3010A 170018500-52298-7 K10 (W25') (0-6") TCLP

Solid 3010A 170018500-52298-8 K10 (W25') (6-12") TCLP

Solid 3010A 170018500-52298-9 K10 (W25') (12-18") TCLP

Solid 3010A 170018500-52298-10 H10 (N30') (0-6") TCLP

Solid 3010A 170018500-52298-11 H10 (N30') (6-12") TCLP

Solid 3010A 170018500-52298-12 H10 (N30') (12-18") TCLP

Solid 3010A 170018500-52298-13 J8 (0-6") TCLP

Solid 3010A 170018500-52298-14 J8 (6-12") TCLP

Solid 3010A 170018500-52298-15 J8 (12-18") TCLP

Solid 3010A 170018500-52298-16 L6 (W20') (0-6") TCLP

Solid 3010A 170018500-52298-17 L6 (W20') (6-12") TCLP

Solid 3010A 170018500-52298-18 L6 (W20') (12-18") TCLP

Solid 3010A 170018500-52298-19 J17 (N30;W20') (0-6") TCLP

Solid 3010A 170018500-52298-20 J17 (N30;W20') (6-12") TCLP



Prep Batch: 170228


Solid 3010A 170019500-52298-21 J17 (N30;W20') (12-18") TCLP

Solid 3010A 170019500-52298-22 K12 (W25') (0-6') TCLP

Solid 3010A 170019500-52298-23 K12 (W25') (6-12') TCLP

Solid 3010A 170019500-52298-23 DU K12 (W25') (6-12') TCLP

Solid 3010A 170019500-52298-23 MS K12 (W25') (6-12') TCLP

Solid 3010A 170019500-52298-24 K12 (W25') (12-18') TCLP



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Metals (Continued)

Prep Batch: 170250


Solid 7471A500-52298-1 F20 (0-6") Total/NA

Solid 7471A500-52298-2 F20 (6-12") Total/NA

Solid 7471A500-52298-3 F20 (12-18") Total/NA

Solid 7471A500-52298-3 DU F20 (12-18") Total/NA

Solid 7471A500-52298-3 MS F20 (12-18") Total/NA

Solid 7471A500-52298-3 MSD F20 (12-18") Total/NA

Solid 7471A500-52298-4 H20 (E20') (0-6") Total/NA



Solid 7471A500-52298-7 K10 (W25') (0-6") Total/NA



Solid 7471A500-52298-10 H10 (N30') (0-6") Total/NA



Solid 7471A500-52298-13 J8 (0-6") Total/NA

Solid 7471A500-52298-14 J8 (6-12") Total/NA

Solid 7471A500-52298-15 J8 (12-18") Total/NA

Solid 7471A500-52298-16 L6 (W20') (0-6") Total/NA



Solid 7471A500-52298-19 J17 (N30;W20') (0-6") Total/NA




Prep Batch: 170259



Solid 7471A500-52298-22 K12 (W25') (0-6') Total/NA





Prep Batch: 170293


Solid 7470A 170019500-52298-21 J17 (N30;W20') (12-18") TCLP

Solid 7470A 170019500-52298-21 DU J17 (N30;W20') (12-18") TCLP

Solid 7470A 170019500-52298-21 MS J17 (N30;W20') (12-18") TCLP

Solid 7470A 170019500-52298-22 K12 (W25') (0-6') TCLP

Solid 7470A 170019500-52298-23 K12 (W25') (6-12') TCLP

Solid 7470A 170019500-52298-24 K12 (W25') (12-18') TCLP

Solid 7470A 170019LB 500-170019/1-E LB Method Blank TCLP



Prep Batch: 170296


Solid 7470A 170018500-52298-1 F20 (0-6") TCLP

Solid 7470A 170018500-52298-1 DU F20 (0-6") TCLP

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Metals (Continued)



Solid 7470A 170018500-52298-1 MS F20 (0-6") TCLP

Solid 7470A 170018500-52298-2 F20 (6-12") TCLP

Solid 7470A 170018500-52298-3 F20 (12-18") TCLP

Solid 7470A 170018500-52298-4 H20 (E20') (0-6") TCLP

Solid 7470A 170018500-52298-5 H20 (E20') (6-12") TCLP

Solid 7470A 170018500-52298-6 H20 (E20') (12-18") TCLP

Solid 7470A 170018500-52298-7 K10 (W25') (0-6") TCLP

Solid 7470A 170018500-52298-8 K10 (W25') (6-12") TCLP

Solid 7470A 170018500-52298-9 K10 (W25') (12-18") TCLP

Solid 7470A 170018500-52298-10 H10 (N30') (0-6") TCLP

Solid 7470A 170018500-52298-11 H10 (N30') (6-12") TCLP

Solid 7470A 170018500-52298-12 H10 (N30') (12-18") TCLP

Solid 7470A 170018500-52298-13 J8 (0-6") TCLP

Solid 7470A 170018500-52298-14 J8 (6-12") TCLP

Solid 7470A 170018500-52298-15 J8 (12-18") TCLP

Solid 7470A 170018500-52298-16 L6 (W20') (0-6") TCLP

Solid 7470A 170018500-52298-17 L6 (W20') (6-12") TCLP

Solid 7470A 170018500-52298-18 L6 (W20') (12-18") TCLP

Solid 7470A 170018500-52298-19 J17 (N30;W20') (0-6") TCLP

Solid 7470A 170018500-52298-20 J17 (N30;W20') (6-12") TCLP






Solid 6010B 170225500-52298-1 F20 (0-6") TCLP

Solid 6010B 170225500-52298-2 F20 (6-12") TCLP

Solid 6010B 170225500-52298-3 F20 (12-18") TCLP

Solid 6010B 170225500-52298-4 H20 (E20') (0-6") TCLP

Solid 6010B 170225500-52298-4 DU H20 (E20') (0-6") TCLP

Solid 6010B 170225500-52298-4 MS H20 (E20') (0-6") TCLP

Solid 6010B 170225500-52298-5 H20 (E20') (6-12") TCLP

Solid 6010B 170225500-52298-6 H20 (E20') (12-18") TCLP

Solid 6010B 170225500-52298-7 K10 (W25') (0-6") TCLP

Solid 6010B 170225500-52298-8 K10 (W25') (6-12") TCLP

Solid 6010B 170225500-52298-9 K10 (W25') (12-18") TCLP

Solid 6010B 170225500-52298-10 H10 (N30') (0-6") TCLP

Solid 6010B 170225500-52298-11 H10 (N30') (6-12") TCLP

Solid 6010B 170225500-52298-12 H10 (N30') (12-18") TCLP

Solid 6010B 170225500-52298-13 J8 (0-6") TCLP

Solid 6010B 170225500-52298-14 J8 (6-12") TCLP

Solid 6010B 170225500-52298-15 J8 (12-18") TCLP

Solid 6010B 170225500-52298-16 L6 (W20') (0-6") TCLP

Solid 6010B 170225500-52298-17 L6 (W20') (6-12") TCLP

Solid 6010B 170225500-52298-18 L6 (W20') (12-18") TCLP

Solid 6010B 170225500-52298-19 J17 (N30;W20') (0-6") TCLP

Solid 6010B 170225500-52298-20 J17 (N30;W20') (6-12") TCLP

Solid 6010B 170228500-52298-21 J17 (N30;W20') (12-18") TCLP

Solid 6010B 170228500-52298-22 K12 (W25') (0-6') TCLP

Solid 6010B 170228500-52298-23 K12 (W25') (6-12') TCLP

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Metals (Continued)



Solid 6010B 170228500-52298-23 DU K12 (W25') (6-12') TCLP

Solid 6010B 170228500-52298-23 MS K12 (W25') (6-12') TCLP

Solid 6010B 170228500-52298-24 K12 (W25') (12-18') TCLP

Solid 6010B 170225LB 500-170018/1-B LB Method Blank TCLP

Solid 6010B 170228LB 500-170019/1-B LB Method Blank TCLP





Solid 6010B 169568500-52298-1 F20 (0-6") Total/NA

Solid 6010B 169568500-52298-1 DU F20 (0-6") Total/NA

Solid 6010B 169568500-52298-1 MS F20 (0-6") Total/NA

Solid 6010B 169568500-52298-1 MSD F20 (0-6") Total/NA

Solid 6010B 169568500-52298-2 F20 (6-12") Total/NA

Solid 6010B 169568500-52298-3 F20 (12-18") Total/NA

Solid 6010B 169568500-52298-4 H20 (E20') (0-6") Total/NA



Solid 6010B 169568500-52298-7 K10 (W25') (0-6") Total/NA



Solid 6010B 169568500-52298-10 H10 (N30') (0-6") Total/NA



Solid 6010B 169568500-52298-13 J8 (0-6") Total/NA

Solid 6010B 169568500-52298-14 J8 (6-12") Total/NA

Solid 6010B 169568500-52298-15 J8 (12-18") Total/NA

Solid 6010B 169568500-52298-16 L6 (W20') (0-6") Total/NA











Solid 6010B 170228500-52298-23 K12 (W25') (6-12') TCLP

Solid 6010B 170228500-52298-23 DU K12 (W25') (6-12') TCLP

Solid 6010B 170228500-52298-23 MS K12 (W25') (6-12') TCLP



Solid 7470A 170296500-52298-1 F20 (0-6") TCLP

Solid 7470A 170296500-52298-1 DU F20 (0-6") TCLP

Solid 7470A 170296500-52298-1 MS F20 (0-6") TCLP

Solid 7470A 170296500-52298-2 F20 (6-12") TCLP

Solid 7470A 170296500-52298-3 F20 (12-18") TCLP

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Metals (Continued)



Solid 7470A 170296500-52298-4 H20 (E20') (0-6") TCLP

Solid 7470A 170296500-52298-5 H20 (E20') (6-12") TCLP

Solid 7470A 170296500-52298-6 H20 (E20') (12-18") TCLP

Solid 7470A 170296500-52298-7 K10 (W25') (0-6") TCLP

Solid 7470A 170296500-52298-8 K10 (W25') (6-12") TCLP

Solid 7470A 170296500-52298-9 K10 (W25') (12-18") TCLP

Solid 7470A 170296500-52298-10 H10 (N30') (0-6") TCLP

Solid 7470A 170296500-52298-11 H10 (N30') (6-12") TCLP

Solid 7470A 170296500-52298-12 H10 (N30') (12-18") TCLP

Solid 7470A 170296500-52298-13 J8 (0-6") TCLP

Solid 7470A 170296500-52298-14 J8 (6-12") TCLP

Solid 7470A 170296500-52298-15 J8 (12-18") TCLP

Solid 7470A 170296500-52298-16 L6 (W20') (0-6") TCLP

Solid 7470A 170296500-52298-17 L6 (W20') (6-12") TCLP

Solid 7470A 170296500-52298-18 L6 (W20') (12-18") TCLP

Solid 7470A 170296500-52298-19 J17 (N30;W20') (0-6") TCLP

Solid 7470A 170296500-52298-20 J17 (N30;W20') (6-12") TCLP

Solid 7470A 170293500-52298-21 J17 (N30;W20') (12-18") TCLP

Solid 7470A 170293500-52298-21 DU J17 (N30;W20') (12-18") TCLP

Solid 7470A 170293500-52298-21 MS J17 (N30;W20') (12-18") TCLP

Solid 7470A 170293500-52298-22 K12 (W25') (0-6') TCLP

Solid 7470A 170293500-52298-23 K12 (W25') (6-12') TCLP

Solid 7470A 170293500-52298-24 K12 (W25') (12-18') TCLP


Solid 7470A 170293LB 500-170019/1-E LB Method Blank TCLP







Solid 7471A 170250500-52298-1 F20 (0-6") Total/NA

Solid 7471A 170250500-52298-2 F20 (6-12") Total/NA

Solid 7471A 170250500-52298-3 F20 (12-18") Total/NA

Solid 7471A 170250500-52298-3 DU F20 (12-18") Total/NA

Solid 7471A 170250500-52298-3 MS F20 (12-18") Total/NA

Solid 7471A 170250500-52298-3 MSD F20 (12-18") Total/NA

Solid 7471A 170250500-52298-4 H20 (E20') (0-6") Total/NA



Solid 7471A 170250500-52298-7 K10 (W25') (0-6") Total/NA



Solid 7471A 170250500-52298-10 H10 (N30') (0-6") Total/NA



Solid 7471A 170250500-52298-13 J8 (0-6") Total/NA

Solid 7471A 170250500-52298-14 J8 (6-12") Total/NA

Solid 7471A 170250500-52298-15 J8 (12-18") Total/NA

Solid 7471A 170250500-52298-16 L6 (W20') (0-6") Total/NA

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Metals (Continued)





Solid 7471A 170250500-52298-19 J17 (N30;W20') (0-6") Total/NA



Solid 7471A 170259500-52298-22 K12 (W25') (0-6') Total/NA







General Chemistry



Solid Moisture500-52298-1 F20 (0-6") Total/NA

Solid Moisture500-52298-1 DU F20 (0-6") Total/NA



Solid Moisture500-52298-4 H20 (E20') (0-6") Total/NA



Solid Moisture500-52298-7 K10 (W25') (0-6") Total/NA



Solid Moisture500-52298-10 H10 (N30') (0-6") Total/NA






Solid Moisture500-52298-16 L6 (W20') (0-6") Total/NA



Solid Moisture500-52298-19 J17 (N30;W20') (0-6") Total/NA



Solid Moisture500-52298-22 K12 (W25') (0-6') Total/NA





Solid 9045C500-52298-1 F20 (0-6") Total/NA

Solid 9045C500-52298-2 F20 (6-12") Total/NA

Solid 9045C500-52298-3 F20 (12-18") Total/NA

Solid 9045C500-52298-4 H20 (E20') (0-6") Total/NA


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General Chemistry (Continued)




Solid 9045C500-52298-7 K10 (W25') (0-6") Total/NA


Solid 9045C500-52298-8 DU K10 (W25') (6-12") Total/NA


Solid 9045C500-52298-10 H10 (N30') (0-6") Total/NA



Solid 9045C500-52298-13 J8 (0-6") Total/NA

Solid 9045C500-52298-14 J8 (6-12") Total/NA

Solid 9045C500-52298-15 J8 (12-18") Total/NA

Solid 9045C500-52298-16 L6 (W20') (0-6") Total/NA



Solid 9045C500-52298-19 J17 (N30;W20') (0-6") Total/NA



Solid 9045C500-52298-22 K12 (W25') (0-6') Total/NA



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FBP NBZ TPH

59 47 72500-52298-1


F20 (0-6")

55 48 54500-52298-2 F20 (6-12")

65 60 60500-52298-3 F20 (12-18")

38 30 38500-52298-4 H20 (E20') (0-6")

61 56 58500-52298-5 H20 (E20') (6-12")

65 58 67500-52298-6 H20 (E20') (12-18")

60 48 62500-52298-7 K10 (W25') (0-6")

58 45 67500-52298-8 K10 (W25') (6-12")

51 50 53500-52298-9 K10 (W25') (12-18")

73 56 83500-52298-10 H10 (N30') (0-6")

66 57 66500-52298-10 MS H10 (N30') (0-6")

57 49 56500-52298-10 MSD H10 (N30') (0-6")

55 53 62500-52298-11 H10 (N30') (6-12")

54 55 61500-52298-12 H10 (N30') (12-18")

54 47 59500-52298-13 J8 (0-6")

48 43 49500-52298-14 J8 (6-12")

47 44 52500-52298-15 J8 (12-18")

59 54 59500-52298-16 L6 (W20') (0-6")

68 66 60500-52298-17 L6 (W20') (6-12")

58 56 59500-52298-18 L6 (W20') (12-18")

56 46 74500-52298-19 J17 (N30;W20') (0-6")

55 47 58500-52298-20 J17 (N30;W20') (6-12")

72 63 68500-52298-21 J17 (N30;W20') (12-18")

62 51 61500-52298-22 K12 (W25') (0-6')

44 35 44500-52298-23 K12 (W25') (6-12')

62 50 69500-52298-24 K12 (W25') (12-18')



78 72 85MB 500-170477/1-A Method Blank

89 79 119MB 500-170478/1-A Method Blank

Surrogate Legend



TPH = Terphenyl-d14

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RL MDL


MB MB



<0.033 0.00780.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Anthracene






<0.033 0.00750.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Chrysene



<0.033 0.00760.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Fluorene




<0.033 0.0120.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Pyrene

2-Fluorobiphenyl 78 30 - 119 11/24/12 12:22 1

MB MB

Surrogate

11/20/12 16:54


72 11/20/12 16:54 11/24/12 12:22 1Nitrobenzene-d5 30 - 115

85 11/20/12 16:54 11/24/12 12:22 1Terphenyl-d14 36 - 134





Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Anthracene 1.67 1.12 mg/Kg 67 52 - 110






Chrysene 1.67 1.27 mg/Kg 76 54 - 110



Fluorene 1.67 1.17 mg/Kg 70 52 - 112




Pyrene 1.67 1.30 mg/Kg 78 50 - 112


Surrogate

80

LCS LCS



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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)




Terphenyl-d14 36 - 134

Surrogate

85

LCS LCS


Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MS



Acenaphthene <0.21 2.20 1.46 mg/Kg 66 53 - 110☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Acenaphthylene <0.21 2.20 1.31 mg/Kg 59 51 - 110☼

Anthracene <0.21 2.20 1.50 mg/Kg 68 52 - 110☼

Benzo[a]anthracene 0.20 J 2.20 1.50 mg/Kg 59 57 - 110☼

Benzo[a]pyrene 0.34 2.20 1.39 F mg/Kg 47 56 - 110☼

Benzo[b]fluoranthene 0.38 2.20 1.32 F mg/Kg 43 50 - 110☼

Benzo[g,h,i]perylene 0.25 2.20 1.59 mg/Kg 61 54 - 117☼

Benzo[k]fluoranthene 0.26 2.20 2.09 mg/Kg 83 43 - 121☼

Chrysene 0.24 2.20 1.53 mg/Kg 59 54 - 110☼

Dibenz(a,h)anthracene <0.21 2.20 1.44 mg/Kg 65 52 - 118☼

Fluoranthene 0.14 J 2.20 1.75 mg/Kg 73 55 - 113☼

Fluorene <0.21 2.20 1.46 mg/Kg 66 52 - 112☼

Indeno[1,2,3-cd]pyrene 0.22 2.20 1.46 mg/Kg 56 53 - 116☼

Naphthalene <0.21 2.20 1.09 mg/Kg 50 48 - 110☼

Phenanthrene <0.21 2.20 1.69 mg/Kg 77 51 - 116☼

Pyrene 0.15 J 2.20 1.36 mg/Kg 55 50 - 112☼


Surrogate

66

MS MS




Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MSD



Acenaphthene <0.21 2.18 1.23 mg/Kg 56 53 - 110 17 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Acenaphthylene <0.21 2.18 1.07 F mg/Kg 49 51 - 110 20 30☼

Anthracene <0.21 2.18 1.29 mg/Kg 59 52 - 110 15 30☼

Benzo[a]anthracene 0.20 J 2.18 1.25 F mg/Kg 48 57 - 110 18 30☼

Benzo[a]pyrene 0.34 2.18 1.17 F mg/Kg 38 56 - 110 17 30☼

Benzo[b]fluoranthene 0.38 2.18 1.33 F mg/Kg 44 50 - 110 1 30☼

Benzo[g,h,i]perylene 0.25 2.18 1.25 F mg/Kg 46 54 - 117 24 30☼

Benzo[k]fluoranthene 0.26 2.18 1.66 mg/Kg 64 43 - 121 23 30☼

Chrysene 0.24 2.18 1.27 F mg/Kg 48 54 - 110 18 30☼

Dibenz(a,h)anthracene <0.21 2.18 1.13 mg/Kg 52 52 - 118 24 30☼

Fluoranthene 0.14 J 2.18 1.49 mg/Kg 62 55 - 113 16 30☼

Fluorene <0.21 2.18 1.20 mg/Kg 55 52 - 112 19 30☼

Indeno[1,2,3-cd]pyrene 0.22 2.18 1.19 F mg/Kg 44 53 - 116 21 30☼

Naphthalene <0.21 2.18 0.966 F mg/Kg 44 48 - 110 12 30☼

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Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MSD



Phenanthrene <0.21 2.18 1.28 mg/Kg 59 51 - 116 28 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Pyrene 0.15 J 2.18 1.17 F mg/Kg 47 50 - 112 16 30☼


Surrogate

57

MSD MSD







RL MDL


MB MB



<0.033 0.00780.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Anthracene






<0.033 0.00750.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Chrysene



<0.033 0.00760.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Fluorene




<0.033 0.0120.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Pyrene

2-Fluorobiphenyl 89 30 - 119 11/21/12 13:21 1

MB MB

Surrogate

11/20/12 17:12


79 11/20/12 17:12 11/21/12 13:21 1Nitrobenzene-d5 30 - 115

119 11/20/12 17:12 11/21/12 13:21 1Terphenyl-d14 36 - 134





Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Anthracene 1.67 1.18 mg/Kg 71 52 - 110






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Chrysene 1.67 1.26 mg/Kg 76 54 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits



Fluorene 1.67 1.23 mg/Kg 74 52 - 112




Pyrene 1.67 1.18 mg/Kg 71 50 - 112


Surrogate

78

LCS LCS








RL MDL

Antimony <2.0 2.0 0.27 mg/Kg 11/13/12 16:30 11/19/12 22:17 1

MB MB


<1.0 0.221.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Arsenic

<1.0 0.121.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Barium

<0.20 0.0500.20 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Cadmium

<1.0 0.171.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Chromium

<1.0 0.271.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Copper

<0.50 0.170.50 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Lead

<1.0 0.291.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Selenium

<0.50 0.0600.50 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Silver

<2.0 0.692.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Zinc




Antimony 50.0 46.8 mg/Kg 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 10.0 9.37 mg/Kg 94 80 - 120

Barium 200 191 mg/Kg 96 80 - 120

Cadmium 5.00 4.76 mg/Kg 95 80 - 120

Chromium 20.0 18.8 mg/Kg 94 80 - 120

Copper 25.0 24.1 mg/Kg 96 80 - 120

Lead 10.0 9.76 mg/Kg 98 80 - 120

Selenium 10.0 9.48 mg/Kg 95 80 - 120

Silver 5.00 4.26 mg/Kg 85 80 - 120

Zinc 50.0 47.7 mg/Kg 95 80 - 120

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Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 MS



Antimony 0.75 J 78.0 39.8 F mg/Kg 50 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Arsenic 5.1 15.6 19.6 mg/Kg 93 75 - 125☼

Barium 55 312 327 mg/Kg 87 75 - 125☼

Cadmium 0.44 7.80 7.33 mg/Kg 88 75 - 125☼

Chromium 9.4 31.2 37.8 mg/Kg 91 75 - 125☼

Copper 18 39.0 78.5 F mg/Kg 154 75 - 125☼

Lead 34 15.6 49.7 mg/Kg 102 75 - 125☼

Selenium 0.79 J 15.6 13.1 mg/Kg 79 75 - 125☼

Silver <0.82 7.80 6.31 mg/Kg 81 75 - 125☼

Zinc 59 78.0 132 mg/Kg 92 75 - 125☼

Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 MSD



Antimony 0.75 J 74.8 39.0 F mg/Kg 51 75 - 125 2 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Arsenic 5.1 15.0 17.9 mg/Kg 85 75 - 125 9 20☼

Barium 55 299 307 mg/Kg 84 75 - 125 6 20☼

Cadmium 0.44 7.48 6.86 mg/Kg 86 75 - 125 7 20☼

Chromium 9.4 29.9 34.9 mg/Kg 85 75 - 125 8 20☼

Copper 18 37.4 51.3 F mg/Kg 88 75 - 125 42 20☼

Lead 34 15.0 46.6 mg/Kg 86 75 - 125 7 20☼

Selenium 0.79 J 15.0 11.2 F mg/Kg 70 75 - 125 15 20☼

Silver <0.82 7.48 5.97 mg/Kg 80 75 - 125 6 20☼

Zinc 59 74.8 118 mg/Kg 79 75 - 125 11 20☼

Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 DU



Antimony 0.75 J 0.839 J mg/Kg 11 20☼

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Arsenic 5.1 5.08 mg/Kg 0.9 20☼

Barium 55 51.3 mg/Kg 7 20☼

Cadmium 0.44 0.410 mg/Kg 6 20☼

Chromium 9.4 9.25 mg/Kg 1 20☼

Copper 18 17.6 mg/Kg 5 20☼

Lead 34 30.0 mg/Kg 12 20☼

Selenium 0.79 J <1.6 mg/Kg NC 20☼

Silver <0.82 <0.79 mg/Kg NC 20☼

Zinc 59 56.0 mg/Kg 6 20☼




RL MDL

Antimony <2.0 2.0 0.27 mg/Kg 11/14/12 08:30 11/15/12 16:53 1

MB MB


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RL MDL

Arsenic <1.0 1.0 0.22 mg/Kg 11/14/12 08:30 11/15/12 16:53 1

MB MB


<1.0 0.121.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Barium

<0.20 0.0500.20 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Cadmium

<1.0 0.171.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Chromium

<1.0 0.271.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Copper

<0.50 0.170.50 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Lead

<1.0 0.291.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Selenium

<0.50 0.0600.50 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Silver

<2.0 0.692.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Zinc




Antimony 50.0 47.6 mg/Kg 95 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 10.0 9.75 mg/Kg 97 80 - 120

Barium 200 199 mg/Kg 99 80 - 120

Cadmium 5.00 4.81 mg/Kg 96 80 - 120

Chromium 20.0 19.3 mg/Kg 96 80 - 120

Copper 25.0 24.8 mg/Kg 99 80 - 120

Lead 10.0 10.0 mg/Kg 100 80 - 120

Selenium 10.0 9.52 mg/Kg 95 80 - 120

Silver 5.00 4.38 mg/Kg 88 80 - 120

Zinc 50.0 47.9 mg/Kg 96 80 - 120




Arsenic 0.100 0.0908 mg/L 91 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 0.500 0.490 J mg/L 98 80 - 120

Cadmium 0.0500 0.0476 mg/L 95 80 - 120

Chromium 0.200 0.195 mg/L 97 80 - 120

Lead 0.100 0.0969 mg/L 97 80 - 120

Selenium 0.100 0.0885 mg/L 89 80 - 120

Silver 0.0500 0.0472 mg/L 94 80 - 120




Arsenic 0.100 0.0937 mg/L 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 0.500 0.501 mg/L 100 80 - 120

Cadmium 0.0500 0.0486 mg/L 97 80 - 120

Chromium 0.200 0.198 mg/L 99 80 - 120

Lead 0.100 0.0986 mg/L 99 80 - 120

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Selenium 0.100 0.0899 mg/L 90 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Silver 0.0500 0.0483 mg/L 97 80 - 120




RL MDL

Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:22 1

LB LB


<0.50 0.0100.50 mg/L 11/19/12 08:00 11/19/12 21:22 1Barium

<0.0050 0.00200.0050 mg/L 11/19/12 08:00 11/19/12 21:22 1Cadmium

<0.025 0.0100.025 mg/L 11/19/12 08:00 11/19/12 21:22 1Chromium

<0.0075 0.00500.0075 mg/L 11/19/12 08:00 11/19/12 21:22 1Lead

<0.050 0.0100.050 mg/L 11/19/12 08:00 11/19/12 21:22 1Selenium

<0.025 0.00500.025 mg/L 11/19/12 08:00 11/19/12 21:22 1Silver

Client Sample ID: H20 (E20') (0-6")Lab Sample ID: 500-52298-4 MS



Arsenic <0.050 0.100 0.113 mg/L 113 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.49 J 0.500 1.01 mg/L 103 50 - 150

Cadmium <0.0050 0.0500 0.0503 mg/L 101 50 - 150

Chromium <0.025 0.200 0.202 mg/L 101 50 - 150

Lead 0.051 0.100 0.155 mg/L 104 50 - 150

Selenium <0.050 0.100 0.107 mg/L 107 50 - 150

Silver <0.025 0.0500 0.0530 mg/L 106 50 - 150

Client Sample ID: H20 (E20') (0-6")Lab Sample ID: 500-52298-4 DU



Arsenic <0.050 <0.050 mg/L NC 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Barium 0.49 J 0.502 mg/L 2 20

Cadmium <0.0050 <0.0050 mg/L NC 20

Chromium <0.025 <0.025 mg/L NC 20

Lead 0.051 0.0523 mg/L 2 20

Selenium <0.050 <0.050 mg/L NC 20

Silver <0.025 <0.025 mg/L NC 20




RL MDL

Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:24 1

LB LB


<0.50 0.0100.50 mg/L 11/19/12 08:00 11/19/12 19:24 1Barium

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RL MDL

Cadmium <0.0050 0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:24 1

LB LB


<0.025 0.0100.025 mg/L 11/19/12 08:00 11/19/12 19:24 1Chromium

0.0149 0.00500.0075 mg/L 11/19/12 08:00 11/19/12 19:24 1Lead

<0.050 0.0100.050 mg/L 11/19/12 08:00 11/19/12 19:24 1Selenium

<0.025 0.00500.025 mg/L 11/19/12 08:00 11/19/12 19:24 1Silver

Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 MS



Arsenic 0.32 0.100 0.421 mg/L 100 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.60 0.500 1.07 mg/L 94 50 - 150

Cadmium 0.0055 0.0500 0.0536 mg/L 96 50 - 150

Chromium <0.025 0.200 0.196 mg/L 98 50 - 150

Selenium <0.050 0.100 0.103 mg/L 103 50 - 150

Silver <0.025 0.0500 0.0504 mg/L 101 50 - 150

Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 MS



Arsenic 0.32 0.100 0.397 J mg/L 73 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.62 0.500 1.12 J mg/L 99 50 - 150

Cadmium <0.050 0.0500 0.0566 mg/L 113 50 - 150

Chromium <0.25 0.200 0.188 J mg/L 94 50 - 150

Lead 73 B 0.100 72.6 4 mg/L -438 50 - 150

Selenium <0.50 0.100 0.104 J mg/L 104 50 - 150

Silver <0.25 0.0500 0.0543 J mg/L 109 50 - 150

Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 DU



Arsenic 0.32 0.333 mg/L 4 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Barium 0.60 0.628 mg/L 4 20

Cadmium 0.0055 0.00550 mg/L 0.7 20

Chromium <0.025 <0.025 mg/L NC 20

Selenium <0.050 <0.050 mg/L NC 20

Silver <0.025 <0.025 mg/L NC 20




Arsenic 0.32 0.322 J mg/L 0.6 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

TestAmerica Chicago

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Barium 0.62 0.626 J mg/L 0.7 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Cadmium <0.050 <0.050 mg/L NC 20

Chromium <0.25 <0.25 mg/L NC 20

Lead 73 B 73.2 mg/L 0.3 20

Selenium <0.50 <0.50 mg/L NC 20

Silver <0.25 <0.25 mg/L NC 20





RL MDL

Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 09:39 1

MB MB





Mercury 0.00200 0.00200 mg/L 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




RL MDL

Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:31 1

MB MB





Mercury 0.00200 0.00268 * mg/L 134 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 500-170019/1-E LB



RL MDL

Mercury 0.0000279 J 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:03 1

LB LB


TestAmerica Chicago

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Client Sample ID: J17 (N30;W20') (12-18")Lab Sample ID: 500-52298-21 MS



Mercury 0.000026 J B 0.00100 0.000940 mg/L 91 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: J17 (N30;W20') (12-18")Lab Sample ID: 500-52298-21 DU



Mercury 0.000026 J B 0.0000273 J mg/L 5 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD




RL MDL

Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:35 1

LB LB





Mercury <0.00020 * 0.00100 0.000393 F mg/L 39 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits




Mercury <0.00020 * 0.0000237 J * mg/L NC 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD





RL MDL

Mercury <0.017 0.017 0.0064 mg/Kg 11/19/12 17:00 11/20/12 11:07 1

MB MB





Mercury 0.167 0.157 mg/Kg 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

TestAmerica Chicago

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Mercury 0.029 0.101 0.120 mg/Kg 90 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: F20 (12-18")Lab Sample ID: 500-52298-3 MSD



Mercury 0.029 0.102 0.121 mg/Kg 90 75 - 125 1 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD




Mercury 0.029 0.0226 mg/Kg 26 20☼

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD




RL MDL

Mercury <0.017 0.017 0.0064 mg/Kg 11/19/12 17:00 11/20/12 12:05 1

MB MB





Mercury 0.167 0.161 mg/Kg 96 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: 9045C - pH

Client Sample ID: K10 (W25') (6-12")Lab Sample ID: 500-52298-8 DU



pH 7.34 7.330 SU 0.1

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

TestAmerica Chicago

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Client Sample ID: F20 (0-6") Lab Sample ID: 500-52298-1Matrix: SolidDate Collected: 11/09/12 13:15


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP



Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA


Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP

Analysis 7470A 1 170438 11/20/12 11:37 BJB TAL CHITCLP

Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA

Analysis 7471A 1 170439 11/20/12 11:10 BJB TAL CHITotal/NA


Analysis 9045C 1 169904 EAT TAL CHITotal/NA

11/15/12 09:24

11/15/12 09:27

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:27

11/15/12 09:30

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

TestAmerica Chicago

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Analysis 8270C 11/24/12 18:34 DA1 170783 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA












11/15/12 09:30

11/15/12 09:32

(Start)

(End)

Client Sample ID: H20 (E20') (0-6") Lab Sample ID: 500-52298-4Matrix: SolidDate Collected: 11/09/12 12:25


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:32

11/15/12 09:35

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


TestAmerica Chicago

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Leach 1311 11/16/12 12:00 MP170018 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP











11/15/12 09:35

11/15/12 09:37

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:37

11/15/12 09:40

(Start)

(End)

Client Sample ID: K10 (W25') (0-6") Lab Sample ID: 500-52298-7Matrix: SolidDate Collected: 11/09/12 11:50


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




TestAmerica Chicago

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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP










11/15/12 09:40

11/15/12 09:43

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:43

11/15/12 09:45

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




TestAmerica Chicago

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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP









11/15/12 09:48

11/15/12 09:50

(Start)

(End)

Client Sample ID: H10 (N30') (0-6") Lab Sample ID: 500-52298-10Matrix: SolidDate Collected: 11/08/12 11:45


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:50

11/15/12 09:53

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA





TestAmerica Chicago

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Prep 3050B 11/13/12 16:30 RL169568 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








11/15/12 09:53

11/15/12 09:55

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 09:55

11/15/12 09:58

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA







TestAmerica Chicago

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Prep 7470A 11/19/12 16:00 BJB170296 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP






11/15/12 09:58

11/15/12 10:01

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 10:01

11/15/12 10:03

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









TestAmerica Chicago

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Prep 7471A 11/19/12 17:00 BJB170250 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




11/15/12 10:03

11/15/12 10:06

(Start)

(End)

Client Sample ID: L6 (W20') (0-6") Lab Sample ID: 500-52298-16Matrix: SolidDate Collected: 11/08/12 13:20


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 10:06

11/15/12 10:08

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











TestAmerica Chicago

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Analysis Moisture 11/13/12 14:51 CMV1 169544 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


11/15/12 10:08

11/15/12 10:11

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 10:11

11/15/12 10:13

(Start)

(End)

Client Sample ID: J17 (N30;W20') (0-6") Lab Sample ID: 500-52298-19Matrix: SolidDate Collected: 11/08/12 14:40


Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA












TestAmerica Chicago

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Analysis 9045C EAT1 169904 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

11/15/12 10:13

11/15/12 10:16

(Start)

(End)



Prep 3541 11/20/12 16:54 DEA170477 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA














11/15/12 10:16

11/15/12 10:19

(Start)

(End)



Prep 3541 11/20/12 17:12 DEA170478 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA












TestAmerica Chicago

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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

11/15/12 10:19

11/15/12 10:21

(Start)

(End)

Client Sample ID: K12 (W25') (0-6') Lab Sample ID: 500-52298-22Matrix: SolidDate Collected: 11/08/12 13:55


Prep 3541 11/20/12 17:12 DEA170478 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 10:21

11/15/12 10:24

(Start)

(End)



Prep 3541 11/20/12 17:12 DEA170478 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













TestAmerica Chicago

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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

11/15/12 10:24

11/15/12 10:26

(Start)

(End)



Prep 3541 11/20/12 17:12 DEA170478 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













11/15/12 10:26

11/15/12 10:29

(Start)

(End)



TestAmerica Chicago

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Laboratory: TestAmerica ChicagoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alabama 04-30-13404614State Program

California NELAC 9 01132CA 04-30-13

Georgia State Program 4 N/A 04-30-13

Georgia State Program 4 939 04-30-13

Hawaii State Program 9 N/A 04-30-13

Illinois NELAC 5 100201 04-30-13

Indiana State Program 5 C-IL-02 04-30-13

Iowa State Program 7 82 05-01-14

Kansas NELAC 7 E-10161 10-31-13

Kentucky State Program 4 90023 12-31-12

Kentucky (UST) State Program 4 66 04-11-13

L-A-B DoD ELAP L2304 01-06-13

L-A-B ISO/IEC 17025 L2304 01-06-13

Louisiana NELAC 6 30720 06-30-13

Massachusetts State Program 1 M-IL035 06-30-13

Mississippi State Program 4 N/A 04-30-13

North Carolina DENR State Program 4 291 12-31-12

North Dakota State Program 8 R-194 04-30-13

Oklahoma State Program 6 8908 08-31-13

South Carolina State Program 4 77001 04-30-13

Texas NELAC 6 T104704252-09-TX 02-28-13

USDA Federal P330-12-00038 02-06-15

Virginia NELAC 3 460142 06-14-13

Wisconsin State Program 5 999580010 08-31-13

Wyoming State Program 8 8TMS-Q 04-30-13

TestAmerica Chicago

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Login Number: 52298




List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.




TrueCOC is present.




TrueThere are no discrepancies between the containers received and the COC.








TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").





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1 2 3 4 5 analytical report 6 - naperville park district · 2017-12-07 · analytical report...

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