04/09/2018 rev.0 testamerica

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Denver4955 Yarrow StreetArvada, CO 80002Tel: (303)736-0100

TestAmerica Job ID: 280-107262-1TestAmerica Sample Delivery Group: DN0332Client Project/Site: S18-003/X18-005/W18-003/W18-002/S18-

002

For:CH2M Hill Plateau Remediation CompanyPO BOX 1600, MS H8-41Richland, Washington 99352

Attn: Mr. Scot Fitzgerald

Authorized for release by:4/9/2018 5:46:16 PM

Darlene Bandy, Project Manager I(303)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: CH2M Hill Plateau Remediation CompanyProject/Site: S18-003/X18-005/W18-003/W18-002/S18-002

TestAmerica Job ID: 280-107262-1SDG: DN0332

of 44TestAmerica Denver

4/9/2018

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

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Case NarrativeClient: CH2M Hill Plateau Remediation Company TestAmerica Job ID: 280-107262-1Project/Site: S18-003/X18-005/W18-003/W18-002/S18-002 SDG: DN0332

Job ID: 280-107262-1

Laboratory: TestAmerica Denver

Narrative

CASE NARRATIVE

Client: CH2M Hill Plateau Remediation Company

Project: S18-003/X18-005/W18-003/W18-002/S18-002

Report Number: 280-107262-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

The laboratory is not able to achieve project specified Highest Allowable Practical Quantitation Limits (HAPQL limits) for several analytes. These include: Boron 6010D, Phosphorus 6010D, Beryllium 6020B, Silver 6020B, Tin 6020B, Total Organic Halides 9020B. All analytes

met statistical limits, unless otherwise detailed in the individual sections below. As instructed by the client, the data is reported.

The Chain of Custody requests “6020_METALS_ICPMS: GW 01” analysis. Service List “6020_METALS_ICPMS: GW 01” includes Thorium, and while TestAmerica Denver holds Washington State (WDOE) accreditation for method 6020B, Thorium is not on the accreditation certificate at this time. Please note that Thorium is on TestAmerica Denver's primary ORELAP certification, and TestAmerica Denver is

pursuing full WDOE accreditation for this element. As instructed by the client, the laboratory proceeded with the requested Thorium analyses by method 6020B.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

RECEIPT

The samples were received on 3/9/2018 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 1.8º C.

VOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples B3HFP1 (280-107262-2) and B3H047 (280-107262-6) were analyzed for volatile organic compounds (GC-MS) in accordance

with EPA SW-846 Method 8260B. The samples were analyzed on 03/14/2018.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

SEMIVOLATILE ORGANIC COMPOUND (GC/MS SIM)

Sample B3HL11 (280-107262-1) was analyzed for Semivolatile Organic Compound (GC/MS SIM) in accordance with SW-846 8270D. The samples were prepared on 03/14/2018 and analyzed on 03/18/2018.

Benzo[a]anthracene, Chrysene and Fluoranthene were detected in method blank MB 280-407819/1-A at levels that were above the method

detection limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated

sample reported a result above the MDL and/or RL, the result has been flagged.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

TOTAL METALS (ICP)

Samples B3HFP1 (280-107262-2), B3HFP4 (280-107262-3), B3HFN4 (280-107262-4) and B3HFN7 (280-107262-5) were analyzed for

TestAmerica Denver of 44 4/9/2018

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Job ID: 280-107262-1 (Continued)

Laboratory: TestAmerica Denver (Continued)

Total Metals (ICP) in accordance with EPA SW846 6010D. The samples were prepared on 03/15/2018 and analyzed on 03/17/2018,

03/21/2018 and 03/22/2018.

Calcium, Magnesium and Potassium were detected in method blank MB 280-407758/1-A at levels that were above the method detection

limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated sample reported a result above the MDL and/or RL and the method blank concentration was greater than 5% of the sample concentration, the

result has been flagged.


TOTAL METALS (ICP/MS)

Samples B3HFP1 (280-107262-2), B3HFP4 (280-107262-3), B3HFN4 (280-107262-4), B3HFN7 (280-107262-5), B3H489

(280-107262-12), B3H4B0 (280-107262-13), B3H490 (280-107262-14) and B3H4B1 (280-107262-15) were analyzed for Total Metals (ICP/MS) in accordance with SW846 6020B. The samples were prepared on 03/15/2018 and analyzed on 03/16/2018 and 03/19/2018.

The Chain of Custody requests “6020_METALS_ICPMS: GW 01” analysis. Service List “6020_METALS_ICPMS: GW 01” includes Thorium, and while TestAmerica Denver holds Washington State (WDOE) accreditation for method 6020B, Thorium is not on the accreditation certificate at this time. Please note that Thorium is on TestAmerica Denver's primary ORELAP certification, and TestAmerica Denver is pursuing full WDOE accreditation for this element. As instructed by the client, the laboratory proceeded with the requested Thorium

analyses by method 6020B.

Strontium, Thallium and Manganese were detected in method blank MB 280-407757/1-A at levels that were above the method detection limit but below half the reporting limit. The values should be considered estimates, and have been flagged. If the associated sample reported a result above the MDL and/or RL and the method blank concentration was greater than 5% of the sample concentration, the

result has been flagged.

The accuracy and precision of Strontium in the MS/MSD performed on sample B3HFP1 (280-107262-2) in prep batch 280-407757 could not be reliably calculated due to the sample concentration reading greater than four times the spike amount. Control limits are not applicable and the MS/MSD results have been flagged “X”.


ALKALINITY

Samples B3HFP1 (280-107262-2) and B3H3R4 (280-107262-11) were analyzed for Alkalinity in accordance with SM20 2320B. The samples were analyzed on 03/15/2018 and 03/16/2018.


TOTAL ORGANIC HALIDES

Samples B3HJ95 (280-107262-7), B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10) were analyzed for

total organic halides in accordance with EPA SW846 Method 9020B. The samples were analyzed on 04/02/2018.

It can be noted that, due to analyst oversight, the MS/MSD for batch 280-409938 was re-analyzed on sample B3HJ95 (280-107262-7), , and all spike parameters were within control limits: MS = 107%; MSD = 110%; RPD = 3% (control limits: MS/MSD 75-125%; RPD 20).

The following samples in this SDG are associated with this MS/MSD: B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8

(280-107262-10). Please note that only the first analysis for sample B3HJ95 (280-107262-7) +MS/MSD in batch 280-409937 is reported.


TOTAL ORGANIC CARBON

Samples B3HJ95 (280-107262-7), B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10) were analyzed for total organic carbon in accordance with EPA SW-846 Method 9060A. The samples were analyzed on 03/28/2018 and 04/03/2018.

Due to analyst oversight, CHPRC project sample specific MS/MSD was not performed for analysis batch 280-409524. MS/MSD was

performed in the batch, but not on a CHPRC sample. All spike parameters were withing control limits: Sample 280-107418-3: MS =


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Job ID: 280-107262-1 (Continued)

Laboratory: TestAmerica Denver (Continued)

100%; MSD = 100%; RPD = 1%; Sample 280-107261-6: MS = 99%; MSD = 103%; RPD = 4% (control limits: MS/MSD 75-125%; RPD 20).

The following samples in this SDG are impacted: B3HJD6 (280-107262-8), B3HJD7 (280-107262-9) and B3HJD8 (280-107262-10).


We certify that this data package is in compliance with the SOW, both technically and for completeness, including a full description of,

explanation of, and corrective actions for, any and all deviations, from either the analyses requested or the case narrative requested. Release of the data contained in this hard copy data package has been authorized by the Laboratory Analytical Manager or designee and

the laboratory’s client services representative as verified by their signature on this report.

Reviewed and approved:

Darlene Bandy

Project Manager


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Login Sample Receipt Checklist

Client: CH2M Hill Plateau Remediation Company Job Number: 280-107262-1

SDG Number: DN0332

Login Number: 107262

Question Answer Comment

Creator: Pottruff, Reed W

List Source: TestAmerica Denver

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

60 CPM

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded. 1.8 C

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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CH2MHill Plateau C.O.C.#

Remediation Company CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST S18-003-437 l?age 1 of 1

Collector: Ed"- t)NO"';"'$-Z, ContacURequester: Karen Water s - Hu s t ed Telephone No.: 509-376 -4 650 JCtlPRC

$AF No.: S18 - 003 Sampling Origin: Hanford Site Purchase Order/Charge Code: 300071

Project Title: CERCLA, MARCH 2 018 Logbook No.: HNF -N-50 6 - Cf /-7 J Ice Chest No.: /2i u}S-- r llf 7 Shipped To (Lab) TestArne rica De nver I Method of Shipment Commercial Carrier Bill ofLadin"g/Air Bill No.: 1'7J'1 ~73'1 '-feids Protocol CERCLA Priority: 30 Days Offsite Property No.: C,f I ?S~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ** **Contains Radioact i ve Mater ial a t concentrat ions · t hat are N/ A not r e gula t ed f o r t r anspor tat i on p er 49 CFR / IATA Dangerous Goods Regula tions but are not releas abl e pe r DOE Order 4 58. l

-

Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative •- A -

,.

B3HL11 N WI Al\ U O LUI: 'il)'=t 4xl - L a G 8270 SVOA GCMS SIM : COMMON 7 / 40 Days Cool <=6C - - -

n 111 n rn 11111111 280-107262 Chain of Custody

D~J\'6 ~6 , \ i2..? ~-°1-l~

Relinquished~ 2":,,__/ ~ \'65? Received By: MAR O 8 2018 13~ Matrix .. ICHPRC - MAR O 8 20fR - - - - ---- = ~~~1.A.1'4--,..1=-ou.-._.,___::..._:_ ---=- S = Soil DS;;; Drum Solids

Print First and Last Name Signature '/Jate/Time Datemme SE = Sediment DL ;;; Drum Liquid

Relinquished By· ,~_,,_.,.,_....r,.n , , ~ / \~ Received By: ... ____ ______ ____ SO= Solid T ;;; Tissue

1~· -~-------- SL = Sludge WI = Wipe _ _ ate/Time Print First and Last Name Signature Datemme W =·Water L = Liquid

Recei~e~ B¼ f.,1 ,__ ~ N,.. ~ I 1W- -~-, ~ C°':5"5 o = O_il V = Vegetation - --- 1 K,.Q.~~ ~ 'h ~ V~ 1? i . A = Air X = Other

Date/Time Print First and Last Name Signature Date/Time

Relinquished By: Fe.cl £x,, Signature Print First and Last Name

Relinquished By: Received By:

Print First and Last Name Signature Datemme Print First and Last Name Signature Datemme

FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): Disposed By: Date/Time:

DISPOSITION Printed On 2/26/2018 FSR ID = FSR58268 A-6004-842 (REV 3)

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CB2MBi11 Plateau C.O.C.#

Remediation Company CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST S18-003-194 Pagel of l

Collector: L11lr)1~ 1CHMc W-0""3~-z.. Contact/Requester: Karen Waters-Husted Telephone No.: 509-376-4650 .

SAFNo.: S18 - 003 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71

Project Title: CERCLA, MARCH 2018 Logbook No.: HNF-N-506 CJ8 /s-:} ! lceChestNo.: (-jjj)- 74' / Shipped To (Lab) TestArnerica Denver II Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: ry,7 i t-]~{]~9 ~o~R Protocol CERCLA Priority: 30 Days Offsite Property No.: 01?-.f~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1

Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative

B3HFP1 N w 3-S ... ,o JO.;to lxSOO -mL G/P 6020_METALS_ICPMS: GW 01; 6 Months HN03 to pH <2

6010 METALS ICP: GW 06

B3HFP1 N w r 1X250-mL G/P 2320 ALKALINITY : COMMON 14 Days Cool <=6C

B3HFP1 N w Sx40-mL aGs* 8260 VOA GCMS: COMMON 14 Days HCl or H2S04

,l/ ~---to pH <2 / Cool <=6C

B3HFP4 y w s-0-,0 Jd~ lXS O 0-mL G/P 6020_METALS_ ICPMS: GW 01; 6 Months HN03 to pH <2 6010 METALS ICP: GW 06

Relinquish~ 3, ~--~.,, MAR n~ Received By: Troy Sa=-r- l,,.. /!;u,c,-/i tOS~ Matrix"

,. ' .• , rl,J'l./1 CHPRC '_/,,d"'f.._ • MAR. D B j1§/T1me s =Soil DS = Drum Solids

Print First and Last Name l Signature Date/Time Print First and Last Nam~ Signature

Relinquished By: Troy Ba~~~ SE = Sediment DL = Drum Liquid

MAR n B ?f118 ? 11 (lt Received By: !=EDEX SO= Solid T = Tissue CHPRC , ,

SL= Sludge WI =Wipe Print First and Last Name Signature Date/Time Print First and Last Name §ignature Datemme

~fbZ w =Water L = Liquid

Refinquished By: F~ctE~ Rec~d B~ pc{f.y- a= - 3-~-tt aq~ 0 =Oil V = Vegetation l Q. C W:::i, A =Air X = Other

Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time

Relinquished By: Received-By:


FINAL SAMPLE I Disposal Method (e.Q., Return to customer, per lab procedure, used in process): DISPOSITION

I Disposed By: I Datemme:

Printed On 1/15/2018 FSR ID= FSR57113 A-60D4-842 (REV 3)

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.0CH2MHill Plateau C.O.C.#

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST S18-003-193 Remediation Company

Page 1 of l

Collector: 1-anyRosane ~RC !) No"?:, "'Z-- Contact/Requester: Kar en Waters-Husted Telephone No.: 509 - 3 76- 4 65 0

SAF No.: S18-00 3 Sampling Origin: Ha n for d S i t e Purchase Order/Charge Code: 300 0 72

Project Title: CERCLA, MARCH 2 018 Logbook No.: HNF-N-5 06 qfJ l~s Ice Chest No.: GLu~-1({ J Shipped To (Lab) TestAmer ica Denver I Method of Shipment Commercial Carr i er Bill of Lading/Air Bill No.: '7 '7f '7 5'7?l1 L/(X?t> Protocol CERCLA Priority: 30 Days Offsite Property No.: q1?,S POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concent r ations t hat a r e N/A not regul a ted for tran sportation per 49 CFR / I ATA Dangerous Goods Regulat ions but are not relea sable p er DOE Order 45 8 .1

Sample No. Filter * Date Time NofType Cont.11iner . Sample Analysis Holding Time Preservative

B3HFN4 N w '5 ,'j-Jfd Ot:tJv; lxS OO -mL G/ P 6 020_METALS_ICPMS, GW 01; 6 Months HN03 to pH <2 6 010 METALS ICP: GW 0 6

B3HFN7 y w 3--g - i<cl oq~ lxSOO-mL G/ P 6020_ METALS_ICPMS : GW 01 ; 6 Months HN03 to p H <2 6 01 0 METALS ICP: GW 06

Relinquish~~ '-{ r:_ - A u 'R O 8 , ,n1g loss Received By: Troy Ba~_n,f L-· ~ Uft.D !'I 8 zn1a/0$5 . Matrix.. . :th'"?fl.e ....J~ ' PH-i -~ 1 · CHPI>~ l'l fl _/J~_'.i~- S = Soil OS= Drum Solids

Print First andLast Name Signature Date/Time Print First and LastName Signature Datemme SE S d. t DL D L" .d :;;; e 1men = rum 1qw

Relinquished By: Troye~onv. L· ~ 71118 . ·t.JO Received By: FEDEY. SO= Solid T = Tissue ------ -ce-11P-R"H-6 - 'P"'/\ MAR n 8 --- !1-j - - ------ - -------- - ---- SL = Sludge WJ = Wipe

Print First and Last Name Signature Date/Time Print First and Last Name Signal/Ke Date/Time W W t L L" "d , , ; a er = 1qu1

Relinquished By: 6?,cl tx Re~~f ott--l,\,r..P-- ~ ~~°' -1.f a1SS- o : O_il v = Vegetation

Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time A - Atr X - 0th er

Relinquished By: ____________ _ _ _ R_e_ce_iv_e_d_B_y_: ___________ _ _____ ___ _


FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process}: I Disposed By: I Date/Time:

DISPOSITION

Printed On 2/26/2018 FSR ID = FSR58267 A-6004-842 (REV 3)

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CB2MBi11 P1ateau C.O.C.#

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST XlS-005-143 Remediation Company

Pagel of 1

COiiector. l:anyRosane

J)ru0~7v Contact/Requester: WATERS-HUSTED, K Telephone No.: 376 - 4650 1':HPRC

SAF No.: X18 - 005 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71 . Project Title: Groundwater Background Study, Logbook No.: HNF - N- 506 91 /S3 Ice Chest No.: f,-)LiJ)-7lf7 Shipped To {Lab} TestAmerica Denver I Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: '701 fJ S()Y, 400B Protocol SURV Priority: 30 Days Offsite Property No.: q(?)$ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS *Contains Radioactive Material at concentrations that are not be Batch with A, I, S, and W SAFs. regulated for transportation per 49 CFR/IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1.

Sample No. Filter " Date Time No/Type Contatiner Sample Analysis Holding Time Preservative B3H047 N w 3-ff ... /~ IOJ3

5x40-rnL aGs* 8260_VOA_GCMS: COMMON 14 Days HCl or H2SO4 to pH <2 /

Cool <=6C

Relinquis-~ Ji f<~ MAR D 8 2019 ,o,s Received By: "f; s rr;. • t?-~ rp5J Matrix* · IC.ti!'BI; GlNl-:4 rcite:~on ~ £,' ~ 1 MAR D 8 Z018 Ji S = Soil DS = Drum Solids Print First and Last Name Signature Date/Time Print First and Last Name- Signature Date/Time

SE = Sediment DL = Drum Liquid Relinquished By: 'rg(.~Rn L,., ~ MAR n 8 ')fl1R I ~l) 0 Received By: FEDEX - SO= Solid T =Tissue

Print First and Last Name 4 Signature Datemme Print First and Last Name Signature Date/Time SL= Sludge WI =Wipe W =Water .. L = Liquid

Relinquished By: ~e..clG:. Rec:;':l~{d Ve H-V\v{f- ~k ··1-ei -I$ 69.,-:, 0 =Oil V = Vegetation A =Air X = Other Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time



FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): DISPOSITION

I Disposed By: I Date/Time:

Printed On 11/21/2017 FSR ID= FSR54035 A-6004-842 (REV 3)

---------~----:----c-;---....,-;-; --:-:-:: ---,-,-;: ----,-,:• f----

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CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST WlS-003-067 Realediation Company

Pagel of 2

Collector: ~ Clan Dru 01,;-z._ Contact/Requester: Karen Waters-Husted Telephone No.: 509-376-4650

SAFNo.: WlS - 003 Sampling Origin: Hanford Site Purchase Order/Charge Co~e: 3 o o o 11

Project Title: RCRA, MARCH 2018 Logbook No.: HNF-N-506 - C/'1-70 Ice Chest No.: {~W~- '74- / Shipped To (Lab) TestArnerica Denver I Method of Shipment Commercial carrier Bill of Lading/Air Bill No.: 'lf/ I J{ '51709 40l,'3 Protocol RCRA Priority: 30 Days Offsite Property No.: 0,f ?n POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1


B3HJ95 N w lx250-mL aG 9060 TOC: COMMON 28 Days HCl or H2S04

M ,RO 7 2018 l'i07 to pH <2 / Cool <=6C

B3HJD6 N w lxl-L aGs* 9020 TOX: COMMON 28 Days H2S04 to p H <2 / cool <=6C

B3HJD6 N w lx250-mL aG 9060_TOC: COMMON 28 Days HCl or H2S04 to pH <2 / cool <=6C

B3HJD7 N w lxl-L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2 / Cool <=6C

B3HJD7 N w l x250-mL aG 9060 TOC: COMMON 28 Days HCl or H2SO4 to pH <2 /

Cool <=6C B3HJD8 N w \ / ~,. lxl-L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2

/ Cool <=6C

RelinqyishedBy: (A~~ ~AR .· [[;oo Received By: SSU-f- MARO 7 1fl18t.S-o . Matrix* _ ~ 0 2 ,mt=--- - -----~~~ ______ __::....:.:....c:..:....=.. ·- S = Soll DS = Drum Solids

Print Pliiiiiz,~ Signature Date/Time Print First and Last Namf},. Date/Time SE = Sediment DL = Drum Liquid

Relinquished By: SSU-1 MAR O 8 2018 ro':;> MAR O 8 2018 1035 so= Solid T = Ti~sue . =-..:..=-----<=c.__ SL = Sludge WI = Wipe

re Date/Time Print First and Last Signature Date/Time W W t L L" .d = a er = 1qu1 Relinquished By: .....s1RCc;:,,e MAR O 8 2018 \~ Received By: FEDEX O = O!I V = Vegetation

. ---- A = Air X = Other Datemme Print First and Last Name ~1gnature Date/Time

Relinquished By: J:ed~ Ren~&JYc~1= ~ 'j BLt-,g 09'P Print First and Last Name Signature Date/Time Print First and Last Name Signature Date/Time

FINAL SAMPLE I Disposal Method (e.g., Return to customer, per tab procedure, used in process): Disposed By: Date/Time: DISPOSITION

Printed On 1/15/2018 FSR ID = FSR57207 A-6004--842 (R~ 3)

---------~----------;---:--------,-----,-,------,--.------;-, •

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CB2MHi11 P1ateau C.O.C.#

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST W18-003-067 Remediation Company

Page 2 of 2

Collector: ~cri... Dv\fc,~-z_, Contact/Requester: Karen Waters-Husted Telephone No.: 509-376-4650

SAF No.: W18-003 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71

Project Title: RCRA, MARCH 2018 Logbook No.: HNF-N-506. t!f'1- 7 0 Ice Chest No.: (A(fh- 7ll J Shipped To (Lab) TestAmerica Denver I Method of Shipment Commercial Carrier Bill of Lading/Air Bill No.: rJ0 f '7 ~-;7?{:f lf rf 11~

Protocol RCRA Priority: 30 Days Offsite Property No.: q[~5 POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that a re N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1


B3HJD8 N w ~ARO 7 20'

lx250-mL aG 9060 TOC: COMMON 28 Days HCl or H2SO4

9)~ to pH <2 / i l Cool <=6C

B3HJ95 N w J, ..J, lxl - L aGs* 9020 TOX: COMMON 28 Days H2SO4 to pH <2 / Cool <=6C

Relinquished By: fl/l-t-Cl£ MAR D-7 7ft"1 [50C Received By: 1~00 Matrix*

§fflfn;1 MAR O 7 7019 Prin~ast Name Signature Date/Time

S = Soil DS = Drum Solids Print First and L --;;------;;;- Signature Date/Time

SE = Sediment DL = Drum Liquid Relinquished By: SSU-1 MARO 8 2018 I~ Received By: ~~ G \-i CQ MAR O 8 2018 ro3S SO = Solid T = Tissue

Print First and Last Name /\ Sig,qatlJl'e Date/Time Print First anrf L~e · Signature Date/Time SL = Sludge WI = Wipe

Relinquished By: ~ 1~ifb.V y MAR O 8 20JB j ~ D() W == Water L = Liquid

Received By: FEOEX 0 == Oil V = Vegetation

Print First and Last NameV -- Signature Datemme Print First and Last Name J,ignature Date/Time A =Air X = Other

Relinquished By: f;d(x Re~e~,z f-tn/\~ {2.suR)l}~ 1-Cf-l& O~:U


FINAL SAMPLE I Disposal Method (e.g., Return to custome:r, per lab procedure, used in process): DISPOSITION

I Disposed By: I Dateffime:

Printed On 1/15/2018 FSR ID = FSR57207 A-6004-842 (REV 3}

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.0CH2MRi11 P1ateau

Remediation Company

Collector: .hatAgullar ICHPRC J;)Nc,"1TZ

- ------------ ---- ··- . - -

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST

Contact/Requester: Karen Waters - Husted Telephone No.: 509-376-4650

C.O.C.# WlS-002-016

Pagel of l

SAF No.: W18-002 Sampling Origin: Hanford Site Purchase Order/Charge Code: 300 071

Project Title: RCRA, February 2 018 Logbook No.: HNF- N- 506 - Ci 'i/q

Shipped To (Lab)I TestAmer ica Denve r Method of Shipment Commercial Carrier 8 Protocol RCRA Priority: 30 Days O!fsite Property No.:

POSSIBLE SAMPLE HAZARDS/REMARK ****Contains Radioactive Mater ial at c oncentr at i ons tha t are not regulat~d for transportation per 4 9 CFR / IATA Dangerou s Goods Regulations but are not releasable per DOE Order 458. 1

Sample No. I Filter 1 * Date Time I No/Type Container Sample Analysis

B3H3R4 N .w 1-3-i· L ~ IQ · 1x125-rnL r.; j p I 2320 ALKALINITY: GW 01 ,

-Relinqu~-"' Ru·

--..--.. ' .) M4R O 8 2818 Received By: Trg~g~~ l:~ MAR O 8 2018 l:?47f'. 'I. Jt.-wPRC I 1:26 ':I ,

Print First and Last No Signature Date/Time Print First and Last Name ___/ Signature Date/Time

Relinquished BYi-roy Bac~Jlbj__ l.• ~ MAR n B 1018 b "160 Received By: FEDEX CHPli'C

Print First and Last Name Signature Datemme Print First and Last Name " Signature Date/Time

Relinquished By: Fe.cl Ex R~aB~H-rvZf ,Lil,~) ;-v.- 2-'i-ar (trs:s Print First and Last Name Signature Date/Time Print Fil'st and Last Name Signature Date/Time




I Disposed By:

Printed On 1/4/2018 FSR ID= FSR55848

Holding Time Preservative

14 - Da ys Cool <=6C

Matrix" s =Soil DS = Drum Solids SE = Sediment DL = Drum Liquid SO= Solid T =Tissue SL= Sludge WI =Wipe W =Water L = Liquid 0 =Oil V = Vegetation A =Air X = Other

I Datemme:

A-6004-842 (REV 3)

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C.O.C.#

Remediation Company CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST SlS-002-020 Page 1 of 1

Collector: ~Aguilar 1),v o "3-; -z. Contact/Requester: Karen Waters-Husted Telephone No.: 509-376-4650

SAF No.: S18-002 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71.

Project Title: Sitewide Surv, February 2018 Logbook No.: HNF-N-'-506-',tj /11 Ice Chest No.: H t"S--'7 ll (-/ Shipped To (Lab) TestAmerica Denver I Method of Shipment commercial carrier Bill of L.adingfAir Bill No.: r](] f '7 '373 q £.IO[p i Protocol SURV Priority: 30 Days Offsite Property No.: 9{~5 POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS ****Contains Radioactive Material at concentrations that are N/A not regulated for transportation per 49 CFR / IATA Dangerous Goods Regulations but are not releasable per DOE Order 458.1

Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative B3H489 N - W ~-%-J!? uori lx500 -mL G/P 6020_METALS_ICPMS: Chr-omium (1) 6 Months HNO3 to pH <=2

B3H4B0 y w 3-8--J ?" I \0Cj lxS00 - mL G/P 6020_METALS_ICPMS: Chromium {1) 6 Months HNO3 to pH <2

- ---~ - -Relinquisliea u:,. (:~"'- / J MAR O 8 1018 t ""2.-0~ Received By: Tt~~~ 6 ~ MAR U 8 2018 l ?It( Matrix*

PrintFirstandLastNJme/ Signature Dateflime Print First and Last Na---j(ff Signature Date/Time s =Soil DS = Drum Solids

~ SE = Sediment DL = Drum Liquid

Relinquished By: Troy Ba~ /::'j {_ ~ MAR O 8 ?01R llfoO Received BfEOE)C SO= Solid T =Tissue CHPRC ' , • SL= Sludge WI =Wipe

Print First and Last Name Signature Datemme Print First and Last Name - Signature Date/Time W =Water L = Liquid

Relinquished By: \:tel Ex: Rit~Bt& f-k'"'QC1 l~Jfv- 5-Ci-lf a?~ 0 =Oil V = Vegetation

Print First and Last Name Signature Date/Time Print First and Last Name ~

Signature Dateflime A =Air X = Other


Print First and Last Name Signature Dateflime Print First and Last Name Signature Date/Time




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CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST SlS-002-021 Remediation Caapany Page 1 o f 1

Collector: JIB!Agullar DAJ c '3 7 --Z. Contact/Requester: Karen Waters-Husted Telephone No.: 509-376-465 0 /CHPRC

SAF No.: S18 - 0 02 Sampling Origin: Hanford Site Purchase Order/Charge Code: 3 o o o 71

Project Tit.le: Sitewi de s u rv, Feb ruary 2 018 Logbook No.: HNF- N- 5 06 - "f'7 / l) Ice Chest No.: GLO~~rJlf } Shipped To (Lab} Test Arnerica Denver I Method of Shipment commercial Carrier Bill of Lading/Air Bill No.: 'l '7 f '{ 511'1 t.l tfo5 Protocol SURV Priority: 30 Days Offsite Property No.: 0113~ POSSIBLE SAMPLE HAZARDS/REMARK SPECIAL INSTRUCTIONS **** Cont a i n s Radioactive Mat erial at concen trations that are N/ A not r egul ated for transportation per 49 CFR / IATA Dange rous Goods Regul ations but are not r e l easabl e per DOE Order 458.1

Sample No. Filter * Date Time No/Type Container Sample Analysis Holding Time Preservative B3H4 90 N . w 3-!?1 i i /oq· lx5 00 -mL G/P 6~2 0_METALS_ICPMS: Chromium (1 ) 6-Months HNO3 to pH <2 B3H4Bl y w ~-8-l i° 1104 l x S O O -mL G/P 602 0_METALS_ I CPMS: Chromium (1) 6 Months HN03 to p H <2

,.,--

Relinquished By. ~-e~---;---MAR J! 2018 J.;ur<f Received Bl/ir~~~~~ b~ MAR o 81018 l:Mf.{ - --- - - ----+--=.__-=e'--- S- ig_n_a_tu_re____ Date/Time Print First and Last Na:I Signature Dateffime SE S d. t DL D L" "d = e ,men = rum 1qU1 Relinquished By: r~:~~~ L· ~ MAR O B ?01R 111 p() Received BYfEDEX SO: Solid T : Tissue

Print First and Last Name Signature Date/Time Print First-and Last Name Signature Date/Time WSL - WSludt ge WL 1 - Wil_ IP~d _ = a er = 1qw Re~iv.Q,~ &tt--r,$ ~l 1¥--- s-'1-t.g c,q-s5 0 = O_il V = Vegetation .! · --- ~ ---~ - ~ ~ - ~~ A =Air X =Other Print First and Last Name Signature Date/Time

S =Soil

Relinquished By: FedEx Print First and Last Name Signature Date/Time

Matrix* DS = Drum Solids

Relinquished By: Recefved By:

Print First and Last Name Signature Date/Time I Print First and Last Name Signature Date/Time

FINAL SAMPLE I Disposal Method (e.g., Return to customer, per lab procedure, used in process): DJS POSITION



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I : Richland, WA US Delivered [ Signed for by: A GOMEZ.

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Weight

771757394068

85 lbs / 38 56 kg•

Dollvered To Sh Ipp1ng/Reoo1v1ng

Total shl1>ment weight 85 lbs I 38 56 kg•

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Special handling section

pl1# 9135/cooler# gws-7 47

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ARVADA, CO US

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DENVER.CO

MEMF'Hl9, TN

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https://www.fedex.com/apps/fedextrack/?action=track&tracknumbers=7717 57394068&loc... 3/12/2018

Definitions/GlossaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company

SDG: DN0332Project/Site: S18-003/X18-005/W18-003/W18-002/S18-002

Qualifiers

GC/MS VOA

Qualifier Description

U Analyzed for but not detected.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

GC/MS VOA TICs


J Indicates an Estimated Value for TICs

Qualifier

N Presumptive evidence of material.

GC/MS Semi VOA



Qualifier

B Analyte was found in the associated method blank as well as in the sample.

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Metals



Qualifier

B Estimated result. Result is less than the RL, but greater than MDL

C The analyte was detected in both the sample and the associated QC blank, and the sample concentration was </= 5X the blank

concentration.X See case narrative notes for explanation of the 'X' flag

General Chemistry


B Estimated result. Result is less than the RL, but greater than MDL

Qualifier


Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

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Definitions/GlossaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Glossary (Continued)

These commonly used abbreviations may or may not be present in this report.

TEF Toxicity Equivalent Factor (Dioxin)

Abbreviation

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method SummaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL DEN

SW8468270D SIM Semivolatile Organic Compounds (GC/MS SIM) TAL DEN

SW8466010D Metals (ICP) TAL DEN

SW8466020B Metals (ICP/MS) TAL DEN

SW8469020B Organic Halides, Total (TOX) TAL DEN

SW8469060A Organic Carbon, Total (TOC) TAL DEN

SMSM 2320B Alkalinity TAL DEN

Protocol References:

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100

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Sample SummaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

280-107262-1 B3HL11 Water 03/08/18 11:19 03/09/18 09:55

280-107262-2 B3HFP1 Water 03/08/18 10:28 03/09/18 09:55

280-107262-3 B3HFP4 Water 03/08/18 10:28 03/09/18 09:55

280-107262-4 B3HFN4 Water 03/08/18 09:26 03/09/18 09:55

280-107262-5 B3HFN7 Water 03/08/18 09:26 03/09/18 09:55

280-107262-6 B3H047 Water 03/08/18 10:28 03/09/18 09:55

280-107262-7 B3HJ95 Water 03/07/18 14:07 03/09/18 09:55

280-107262-8 B3HJD6 Water 03/07/18 14:07 03/09/18 09:55

280-107262-9 B3HJD7 Water 03/07/18 14:07 03/09/18 09:55

280-107262-10 B3HJD8 Water 03/07/18 14:07 03/09/18 09:55

280-107262-11 B3H3R4 Water 03/08/18 09:31 03/09/18 09:55

280-107262-12 B3H489 Water 03/08/18 11:09 03/09/18 09:55

280-107262-13 B3H4B0 Water 03/08/18 11:09 03/09/18 09:55

280-107262-14 B3H490 Water 03/08/18 11:09 03/09/18 09:55

280-107262-15 B3H4B1 Water 03/08/18 11:09 03/09/18 09:55

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Client Sample ResultsTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: 280-107262-2Client Sample ID: B3HFP1Matrix: WaterDate Collected: 03/08/18 10:28

Date Received: 03/09/18 09:55RL MDL

1,1,1-Trichloroethane 0.16 U 1.0 0.16 ug/L 03/14/18 12:43 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 0.27 ug/L 03/14/18 12:43 11,1,2-Trichloroethane 0.27 U

1.0 0.22 ug/L 03/14/18 12:43 11,1-Dichloroethane 0.22 U

1.0 0.23 ug/L 03/14/18 12:43 11,1-Dichloroethene 0.23 U


6.0 2.0 ug/L 03/14/18 12:43 12-Butanone (MEK) 2.0 U

5.0 0.98 ug/L 03/14/18 12:43 14-Methyl-2-pentanone (MIBK) 0.98 U

10 1.9 ug/L 03/14/18 12:43 1Acetone 1.9 U

1.0 0.16 ug/L 03/14/18 12:43 1Benzene 0.16 U

2.0 0.45 ug/L 03/14/18 12:43 1Carbon disulfide 0.45 U

1.0 0.19 ug/L 03/14/18 12:43 1Carbon tetrachloride 0.19 U

1.0 0.17 ug/L 03/14/18 12:43 1Chlorobenzene 0.17 U

1.0 0.16 ug/L 03/14/18 12:43 1Chloroform 2.3

1.0 0.16 ug/L 03/14/18 12:43 1Ethylbenzene 0.16 U

2.0 0.32 ug/L 03/14/18 12:43 1Methylene Chloride 0.32 U

1.0 0.20 ug/L 03/14/18 12:43 1Tetrachloroethene 0.20 U

1.0 0.17 ug/L 03/14/18 12:43 1Toluene 0.17 U

1.0 0.16 ug/L 03/14/18 12:43 1Trichloroethene 0.16 U

1.0 0.10 ug/L 03/14/18 12:43 1Vinyl chloride 0.10 U

2.0 0.19 ug/L 03/14/18 12:43 1Xylenes, Total 0.19 U

Isopropyl alcohol 73 ug/L 5.37 67-63-0 03/14/18 12:43 1

Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT

103/14/18 12:43N JHydrazine, methyl- 60-34-41.4 ug/L 6.62

1,2-Dichloroethane-d4 (Surr) 96 70 - 130 03/14/18 12:43 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 99 03/14/18 12:43 170 - 130

Dibromofluoromethane (Surr) 104 03/14/18 12:43 170 - 130

Toluene-d8 (Surr) 106 03/14/18 12:43 170 - 130

Lab Sample ID: 280-107262-6Client Sample ID: B3H047Matrix: WaterDate Collected: 03/08/18 10:28




1.0 0.27 ug/L 03/14/18 12:04 11,1,2-Trichloroethane 0.27 U


1.0 0.23 ug/L 03/14/18 12:04 11,1-Dichloroethene 0.23 U


6.0 2.0 ug/L 03/14/18 12:04 12-Butanone (MEK) 2.0 U

5.0 0.98 ug/L 03/14/18 12:04 14-Methyl-2-pentanone (MIBK) 0.98 U

10 1.9 ug/L 03/14/18 12:04 1Acetone 1.9 U

1.0 0.16 ug/L 03/14/18 12:04 1Benzene 0.16 U

2.0 0.45 ug/L 03/14/18 12:04 1Carbon disulfide 0.45 U

1.0 0.19 ug/L 03/14/18 12:04 1Carbon tetrachloride 0.19 U

1.0 0.17 ug/L 03/14/18 12:04 1Chlorobenzene 0.17 U

1.0 0.16 ug/L 03/14/18 12:04 1Chloroform 0.16 U

1.0 0.16 ug/L 03/14/18 12:04 1Ethylbenzene 0.16 U

2.0 0.32 ug/L 03/14/18 12:04 1Methylene Chloride 0.33 J

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)



Tetrachloroethene 0.20 U 1.0 0.20 ug/L 03/14/18 12:04 1


1.0 0.17 ug/L 03/14/18 12:04 1Toluene 0.17 U

1.0 0.16 ug/L 03/14/18 12:04 1Trichloroethene 0.16 U

1.0 0.10 ug/L 03/14/18 12:04 1Vinyl chloride 0.10 U

2.0 0.19 ug/L 03/14/18 12:04 1Xylenes, Total 0.19 U

Isopropyl alcohol 100 ug/L 5.37 67-63-0 03/14/18 12:04 1

Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT

103/14/18 12:04Tentatively Identified Compound None ug/L



4-Bromofluorobenzene (Surr) 106 03/14/18 12:04 170 - 130

Dibromofluoromethane (Surr) 101 03/14/18 12:04 170 - 130

Toluene-d8 (Surr) 112 03/14/18 12:04 170 - 130

Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)

Lab Sample ID: 280-107262-1Client Sample ID: B3HL11Matrix: WaterDate Collected: 03/08/18 11:19


Acenaphthene 10 U 95 10 ng/L 03/14/18 13:59 03/18/18 14:40 1


95 9.5 ng/L 03/14/18 13:59 03/18/18 14:40 1Acenaphthylene 9.5 U

95 13 ng/L 03/14/18 13:59 03/18/18 14:40 1Anthracene 13 U

95 3.1 ng/L 03/14/18 13:59 03/18/18 14:40 1Benzo[a]anthracene 3.5 J B

95 4.9 ng/L 03/14/18 13:59 03/18/18 14:40 1Benzo[a]pyrene 4.9 U

95 3.3 ng/L 03/14/18 13:59 03/18/18 14:40 1Benzo[b]fluoranthene 3.3 U

95 3.4 ng/L 03/14/18 13:59 03/18/18 14:40 1Benzo[g,h,i]perylene 3.4 U

95 4.8 ng/L 03/14/18 13:59 03/18/18 14:40 1Benzo[k]fluoranthene 4.8 U

95 3.0 ng/L 03/14/18 13:59 03/18/18 14:40 1Chrysene 3.8 J B

95 4.6 ng/L 03/14/18 13:59 03/18/18 14:40 1Dibenz(a,h)anthracene 4.6 U

95 4.3 ng/L 03/14/18 13:59 03/18/18 14:40 1Fluoranthene 4.7 J B

95 18 ng/L 03/14/18 13:59 03/18/18 14:40 1Fluorene 18 U

95 14 ng/L 03/14/18 13:59 03/18/18 14:40 1Indeno[1,2,3-cd]pyrene 14 U

95 5.1 ng/L 03/14/18 13:59 03/18/18 14:40 1Naphthalene 7.3 J

95 9.3 ng/L 03/14/18 13:59 03/18/18 14:40 1Phenanthrene 9.3 U

95 7.7 ng/L 03/14/18 13:59 03/18/18 14:40 1Pyrene 7.7 U

2-Fluorobiphenyl 72 42 - 120 03/14/18 13:59 03/18/18 14:40 1


Nitrobenzene-d5 73 03/14/18 13:59 03/18/18 14:40 143 - 120

Terphenyl-d14 82 03/14/18 13:59 03/18/18 14:40 147 - 120

Method: 6010D - Metals (ICP)



Boron 75.4 B 100 4.4 ug/L 03/15/18 08:26 03/22/18 21:27 1


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Method: 6010D - Metals (ICP) (Continued)



Calcium 29800 200 34.5 ug/L 03/15/18 08:26 03/17/18 04:49 1


100 22.0 ug/L 03/15/18 08:26 03/17/18 04:49 1Iron 37.0 B

200 10.7 ug/L 03/15/18 08:26 03/17/18 04:49 1Magnesium 6410

3000 13.5 ug/L 03/15/18 08:26 03/17/18 04:49 1Phosphorus 75.4 B

3000 237 ug/L 03/15/18 08:26 03/21/18 02:27 1Potassium 5430 C

1000 117 ug/L 03/15/18 08:26 03/17/18 04:49 1Sodium 97300

10.0 1.1 ug/L 03/15/18 08:26 03/17/18 04:49 1Vanadium 17.5



Boron 76.6 B 100 4.4 ug/L 03/15/18 08:26 03/22/18 21:47 1


200 34.5 ug/L 03/15/18 08:26 03/17/18 05:10 1Calcium 28300

100 22.0 ug/L 03/15/18 08:26 03/17/18 05:10 1Iron 22.0 U

200 10.7 ug/L 03/15/18 08:26 03/17/18 05:10 1Magnesium 6110

3000 13.5 ug/L 03/15/18 08:26 03/17/18 05:10 1Phosphorus 71.6 B

3000 237 ug/L 03/15/18 08:26 03/21/18 02:39 1Potassium 5150 C

1000 117 ug/L 03/15/18 08:26 03/17/18 05:10 1Sodium 93900

10.0 1.1 ug/L 03/15/18 08:26 03/17/18 05:10 1Vanadium 16.4

Lab Sample ID: 280-107262-4Client Sample ID: B3HFN4Matrix: WaterDate Collected: 03/08/18 09:26


Boron 16.3 B 100 4.4 ug/L 03/15/18 08:26 03/22/18 21:50 1


200 34.5 ug/L 03/15/18 08:26 03/17/18 05:13 1Calcium 27600

100 22.0 ug/L 03/15/18 08:26 03/17/18 05:13 1Iron 65.9 B

200 10.7 ug/L 03/15/18 08:26 03/17/18 05:13 1Magnesium 6070

3000 13.5 ug/L 03/15/18 08:26 03/17/18 05:13 1Phosphorus 72.0 B

3000 237 ug/L 03/15/18 08:26 03/21/18 02:42 1Potassium 5010 C

1000 117 ug/L 03/15/18 08:26 03/17/18 05:13 1Sodium 93700

10.0 1.1 ug/L 03/15/18 08:26 03/17/18 05:13 1Vanadium 13.4



Boron 15.8 B 100 4.4 ug/L 03/15/18 08:26 03/22/18 21:53 1


200 34.5 ug/L 03/15/18 08:26 03/17/18 05:16 1Calcium 28600

100 22.0 ug/L 03/15/18 08:26 03/17/18 05:16 1Iron 22.0 U

200 10.7 ug/L 03/15/18 08:26 03/17/18 05:16 1Magnesium 6240

3000 13.5 ug/L 03/15/18 08:26 03/17/18 05:16 1Phosphorus 79.9 B

3000 237 ug/L 03/15/18 08:26 03/21/18 02:45 1Potassium 4940 C

1000 117 ug/L 03/15/18 08:26 03/17/18 05:16 1Sodium 98300

10.0 1.1 ug/L 03/15/18 08:26 03/17/18 05:16 1Vanadium 14.0

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Method: 6020B - Metals (ICP/MS)



Aluminum 23.8 B 50.0 9.2 ug/L 03/15/18 08:26 03/19/18 16:41 1


2.0 0.40 ug/L 03/15/18 08:26 03/16/18 01:37 1Antimony 0.40 U

5.0 0.33 ug/L 03/15/18 08:26 03/19/18 16:41 1Arsenic 6.9

1.0 0.29 ug/L 03/15/18 08:26 03/19/18 16:41 1Barium 50.2

1.0 0.080 ug/L 03/15/18 08:26 03/16/18 01:37 1Beryllium 0.080 U

1.0 0.27 ug/L 03/15/18 08:26 03/16/18 01:37 1Cadmium 0.27 U

2.0 0.50 ug/L 03/15/18 08:26 03/16/18 01:37 1Chromium 8.2

1.0 0.054 ug/L 03/15/18 08:26 03/16/18 01:37 1Cobalt 0.054 U

2.0 0.56 ug/L 03/15/18 08:26 03/16/18 01:37 1Copper 0.56 U

1.0 0.18 ug/L 03/15/18 08:26 03/16/18 01:37 1Lead 0.18 U

1.0 0.31 ug/L 03/15/18 08:26 03/19/18 16:41 1Manganese 1.0 C

2.0 0.14 ug/L 03/15/18 08:26 03/16/18 01:37 1Molybdenum 5.8

2.0 0.30 ug/L 03/15/18 08:26 03/16/18 01:37 1Nickel 1.3 B

5.0 0.70 ug/L 03/15/18 08:26 03/16/18 01:37 1Selenium 1.3 B

5.0 0.033 ug/L 03/15/18 08:26 03/16/18 01:37 1Silver 0.033 U

10.0 0.30 ug/L 03/15/18 08:26 03/16/18 01:37 1Strontium 208

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 01:37 1Thallium 0.050 U

5.0 1.2 ug/L 03/15/18 08:26 03/16/18 01:37 1Thorium 1.2 U

10.0 0.77 ug/L 03/15/18 08:26 03/16/18 01:37 1Tin 0.77 U

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 01:37 1Uranium 2.7

10.0 2.0 ug/L 03/15/18 08:26 03/19/18 16:41 1Zinc 2.0 U



Aluminum 9.2 U 50.0 9.2 ug/L 03/15/18 08:26 03/19/18 16:53 1


2.0 0.40 ug/L 03/15/18 08:26 03/16/18 01:56 1Antimony 0.40 U

5.0 0.33 ug/L 03/15/18 08:26 03/19/18 16:53 1Arsenic 6.7

1.0 0.29 ug/L 03/15/18 08:26 03/19/18 16:53 1Barium 42.2

1.0 0.080 ug/L 03/15/18 08:26 03/16/18 01:56 1Beryllium 0.080 U

1.0 0.27 ug/L 03/15/18 08:26 03/16/18 01:56 1Cadmium 0.27 U

2.0 0.50 ug/L 03/15/18 08:26 03/16/18 01:56 1Chromium 5.0

1.0 0.054 ug/L 03/15/18 08:26 03/16/18 01:56 1Cobalt 0.070 B

2.0 0.56 ug/L 03/15/18 08:26 03/16/18 01:56 1Copper 0.56 U

1.0 0.18 ug/L 03/15/18 08:26 03/16/18 01:56 1Lead 0.18 U

1.0 0.31 ug/L 03/15/18 08:26 03/19/18 16:53 1Manganese 0.31 U

2.0 0.14 ug/L 03/15/18 08:26 03/16/18 01:56 1Molybdenum 5.3

2.0 0.30 ug/L 03/15/18 08:26 03/16/18 01:56 1Nickel 0.46 B

5.0 0.70 ug/L 03/15/18 08:26 03/16/18 01:56 1Selenium 1.2 B

5.0 0.033 ug/L 03/15/18 08:26 03/16/18 01:56 1Silver 0.033 U

10.0 0.30 ug/L 03/15/18 08:26 03/16/18 01:56 1Strontium 200

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 01:56 1Thallium 0.050 U

5.0 1.2 ug/L 03/15/18 08:26 03/16/18 01:56 1Thorium 1.2 U

10.0 0.77 ug/L 03/15/18 08:26 03/16/18 01:56 1Tin 0.77 U

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 01:56 1Uranium 2.6

10.0 2.0 ug/L 03/15/18 08:26 03/19/18 16:53 1Zinc 2.0 U

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Aluminum 20.2 B 50.0 9.2 ug/L 03/15/18 08:26 03/19/18 16:57 1


2.0 0.40 ug/L 03/15/18 08:26 03/16/18 02:00 1Antimony 0.40 U

5.0 0.33 ug/L 03/15/18 08:26 03/19/18 16:57 1Arsenic 4.9 B

1.0 0.29 ug/L 03/15/18 08:26 03/19/18 16:57 1Barium 43.0

1.0 0.080 ug/L 03/15/18 08:26 03/16/18 02:00 1Beryllium 0.080 U

1.0 0.27 ug/L 03/15/18 08:26 03/16/18 02:00 1Cadmium 0.27 U

2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:00 1Chromium 6.0

1.0 0.054 ug/L 03/15/18 08:26 03/16/18 02:00 1Cobalt 0.084 B

2.0 0.56 ug/L 03/15/18 08:26 03/16/18 02:00 1Copper 0.83 B

1.0 0.18 ug/L 03/15/18 08:26 03/16/18 02:00 1Lead 0.18 U

1.0 0.31 ug/L 03/15/18 08:26 03/19/18 16:57 1Manganese 1.4 C

2.0 0.14 ug/L 03/15/18 08:26 03/16/18 02:00 1Molybdenum 4.9

2.0 0.30 ug/L 03/15/18 08:26 03/16/18 02:00 1Nickel 0.78 B

5.0 0.70 ug/L 03/15/18 08:26 03/16/18 02:00 1Selenium 1.3 B

5.0 0.033 ug/L 03/15/18 08:26 03/16/18 02:00 1Silver 0.033 U

10.0 0.30 ug/L 03/15/18 08:26 03/16/18 02:00 1Strontium 175

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 02:00 1Thallium 0.050 U

5.0 1.2 ug/L 03/15/18 08:26 03/16/18 02:00 1Thorium 1.2 U

10.0 0.77 ug/L 03/15/18 08:26 03/16/18 02:00 1Tin 0.77 U

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 02:00 1Uranium 2.1

10.0 2.0 ug/L 03/15/18 08:26 03/19/18 16:57 1Zinc 2.0 U



Aluminum 9.2 U 50.0 9.2 ug/L 03/15/18 08:26 03/19/18 17:01 1


2.0 0.40 ug/L 03/15/18 08:26 03/16/18 02:03 1Antimony 0.40 U

5.0 0.33 ug/L 03/15/18 08:26 03/19/18 17:01 1Arsenic 5.0

1.0 0.29 ug/L 03/15/18 08:26 03/19/18 17:01 1Barium 40.3

1.0 0.080 ug/L 03/15/18 08:26 03/16/18 02:03 1Beryllium 0.080 U

1.0 0.27 ug/L 03/15/18 08:26 03/16/18 02:03 1Cadmium 0.27 U

2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:03 1Chromium 4.6

1.0 0.054 ug/L 03/15/18 08:26 03/16/18 02:03 1Cobalt 0.054 U

2.0 0.56 ug/L 03/15/18 08:26 03/16/18 02:03 1Copper 0.56 U

1.0 0.18 ug/L 03/15/18 08:26 03/16/18 02:03 1Lead 0.18 U

1.0 0.31 ug/L 03/15/18 08:26 03/19/18 17:01 1Manganese 0.41 B C

2.0 0.14 ug/L 03/15/18 08:26 03/16/18 02:03 1Molybdenum 4.9

2.0 0.30 ug/L 03/15/18 08:26 03/16/18 02:03 1Nickel 0.38 B

5.0 0.70 ug/L 03/15/18 08:26 03/16/18 02:03 1Selenium 1.0 B

5.0 0.033 ug/L 03/15/18 08:26 03/16/18 02:03 1Silver 0.033 U

10.0 0.30 ug/L 03/15/18 08:26 03/16/18 02:03 1Strontium 177

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 02:03 1Thallium 0.050 U

5.0 1.2 ug/L 03/15/18 08:26 03/16/18 02:03 1Thorium 1.2 U

10.0 0.77 ug/L 03/15/18 08:26 03/16/18 02:03 1Tin 0.77 U

1.0 0.050 ug/L 03/15/18 08:26 03/16/18 02:03 1Uranium 1.9

10.0 2.0 ug/L 03/15/18 08:26 03/19/18 17:01 1Zinc 2.0 U

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Chromium 104 2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:07 1


Lab Sample ID: 280-107262-13Client Sample ID: B3H4B0Matrix: WaterDate Collected: 03/08/18 11:09


Chromium 22.8 2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:11 1




Chromium 154 2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:15 1


Lab Sample ID: 280-107262-15Client Sample ID: B3H4B1Matrix: WaterDate Collected: 03/08/18 11:09


Chromium 24.8 2.0 0.50 ug/L 03/15/18 08:26 03/16/18 02:19 1


General Chemistry



Alkalinity as CaCO3 157000 5000 1070 ug/L 03/15/18 23:49 1


Lab Sample ID: 280-107262-7Client Sample ID: B3HJ95Matrix: WaterDate Collected: 03/07/18 14:07


Total Organic Halogens - Dup 7.7 U 30.0 7.7 ug/L 04/02/18 10:29 1


1000 155 ug/L 04/03/18 11:40 1Total Organic Carbon - Average 561 B

Lab Sample ID: 280-107262-8Client Sample ID: B3HJD6Matrix: WaterDate Collected: 03/07/18 14:07










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General Chemistry






Lab Sample ID: 280-107262-11Client Sample ID: B3H3R4Matrix: WaterDate Collected: 03/08/18 09:31


Alkalinity as CaCO3 118000 5000 1070 ug/L 03/16/18 00:11 1


5000 1070 ug/L 03/16/18 00:11 1Bicarbonate Alkalinity as CaCO3 118000

5000 1070 ug/L 03/16/18 00:11 1Carbonate Alkalinity as CaCO3 1070 U

5000 1070 ug/L 03/16/18 00:11 1Hydroxide Alkalinity as CaCO3 1070 U

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QC Sample ResultsTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 280-407821/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 407821

RL MDL


MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.27 U 0.271.0 ug/L 03/14/18 11:12 11,1,2-Trichloroethane

0.22 U 0.221.0 ug/L 03/14/18 11:12 11,1-Dichloroethane

0.23 U 0.231.0 ug/L 03/14/18 11:12 11,1-Dichloroethene

0.13 U 0.131.0 ug/L 03/14/18 11:12 11,2-Dichloroethane

2.0 U 2.06.0 ug/L 03/14/18 11:12 12-Butanone (MEK)

0.98 U 0.985.0 ug/L 03/14/18 11:12 14-Methyl-2-pentanone (MIBK)

1.9 U 1.910 ug/L 03/14/18 11:12 1Acetone

0.16 U 0.161.0 ug/L 03/14/18 11:12 1Benzene

0.45 U 0.452.0 ug/L 03/14/18 11:12 1Carbon disulfide

0.19 U 0.191.0 ug/L 03/14/18 11:12 1Carbon tetrachloride

0.17 U 0.171.0 ug/L 03/14/18 11:12 1Chlorobenzene

0.16 U 0.161.0 ug/L 03/14/18 11:12 1Chloroform

0.16 U 0.161.0 ug/L 03/14/18 11:12 1Ethylbenzene

0.32 U 0.322.0 ug/L 03/14/18 11:12 1Methylene Chloride

0.20 U 0.201.0 ug/L 03/14/18 11:12 1Tetrachloroethene

0.17 U 0.171.0 ug/L 03/14/18 11:12 1Toluene

0.16 U 0.161.0 ug/L 03/14/18 11:12 1Trichloroethene

0.10 U 0.101.0 ug/L 03/14/18 11:12 1Vinyl chloride

0.19 U 0.192.0 ug/L 03/14/18 11:12 1Xylenes, Total

Hydrazine, methyl- 1.32 N J ug/L 6.62 60-34-4 03/14/18 11:12 1

MB MB

Tentatively Identified Compound Dil FacPrepared AnalyzedDUnitQualifierEst. Result RT CAS No.


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

105 03/14/18 11:12 14-Bromofluorobenzene (Surr) 70 - 130

108 03/14/18 11:12 1Dibromofluoromethane (Surr) 70 - 130

117 03/14/18 11:12 1Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-407821/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 407821

1,1,1-Trichloroethane 5.00 4.92 ug/L 98 70 - 130

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,2-Trichloroethane 5.00 5.29 ug/L 106 70 - 130

1,1-Dichloroethane 5.00 4.98 ug/L 100 70 - 130

1,1-Dichloroethene 5.00 4.97 ug/L 99 70 - 130

1,2-Dichloroethane 5.00 4.97 ug/L 99 70 - 130

2-Butanone (MEK) 20.0 18.2 ug/L 91 70 - 130

4-Methyl-2-pentanone (MIBK) 20.0 18.1 ug/L 90 70 - 130

Acetone 20.0 18.3 ug/L 91 70 - 130

Benzene 5.00 5.27 ug/L 105 70 - 130

Carbon disulfide 5.00 5.11 ug/L 102 70 - 130

Carbon tetrachloride 5.00 5.16 ug/L 103 70 - 130

Chlorobenzene 5.00 5.24 ug/L 105 70 - 130

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Chloroform 5.00 4.99 ug/L 100 70 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Ethylbenzene 5.00 5.24 ug/L 105 70 - 130

Methylene Chloride 5.00 4.92 ug/L 98 70 - 130

Tetrachloroethene 5.00 5.34 ug/L 107 70 - 130

Toluene 5.00 5.40 ug/L 108 70 - 130

Trichloroethene 5.00 4.99 ug/L 100 70 - 130

Vinyl chloride 5.00 5.13 ug/L 103 70 - 130

Xylenes, Total 10.0 10.2 ug/L 102 70 - 130

1,2-Dichloroethane-d4 (Surr) 70 - 130

Surrogate

85

LCS LCS

Qualifier Limits%Recovery

1134-Bromofluorobenzene (Surr) 70 - 130

93Dibromofluoromethane (Surr) 70 - 130

105Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-407821/5Matrix: Water Prep Type: Total/NAAnalysis Batch: 407821

1,1,1-Trichloroethane 5.00 4.78 ug/L 96 70 - 130 3 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

1,1,2-Trichloroethane 5.00 5.23 ug/L 105 70 - 130 1 20

1,1-Dichloroethane 5.00 5.03 ug/L 101 70 - 130 1 20

1,1-Dichloroethene 5.00 4.75 ug/L 95 70 - 130 5 20

1,2-Dichloroethane 5.00 5.00 ug/L 100 70 - 130 0 20

2-Butanone (MEK) 20.0 18.2 ug/L 91 70 - 130 0 20

4-Methyl-2-pentanone (MIBK) 20.0 18.1 ug/L 91 70 - 130 0 20

Acetone 20.0 16.4 ug/L 82 70 - 130 11 20

Benzene 5.00 5.34 ug/L 107 70 - 130 1 20

Carbon disulfide 5.00 4.97 ug/L 99 70 - 130 3 20

Carbon tetrachloride 5.00 4.96 ug/L 99 70 - 130 4 20

Chlorobenzene 5.00 5.29 ug/L 106 70 - 130 1 20

Chloroform 5.00 4.92 ug/L 98 70 - 130 1 20

Ethylbenzene 5.00 5.32 ug/L 106 70 - 130 1 20

Methylene Chloride 5.00 4.93 ug/L 99 70 - 130 0 20

Tetrachloroethene 5.00 5.38 ug/L 108 70 - 130 1 20

Toluene 5.00 5.47 ug/L 109 70 - 130 1 20

Trichloroethene 5.00 5.06 ug/L 101 70 - 130 1 20

Vinyl chloride 5.00 4.92 ug/L 98 70 - 130 4 20

Xylenes, Total 10.0 10.3 ug/L 103 70 - 130 2 20


Surrogate

98

LCSD LCSD





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Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 407821

1,1,1-Trichloroethane 0.16 U 5.00 4.66 ug/L 93 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,1,2-Trichloroethane 0.27 U 5.00 5.11 ug/L 102 70 - 130

1,1-Dichloroethane 0.22 U 5.00 4.79 ug/L 96 70 - 130

1,1-Dichloroethene 0.23 U 5.00 4.58 ug/L 92 70 - 130

1,2-Dichloroethane 0.13 U 5.00 4.68 ug/L 94 70 - 130

2-Butanone (MEK) 2.0 U 20.0 17.7 ug/L 89 70 - 130

4-Methyl-2-pentanone (MIBK) 0.98 U 20.0 17.5 ug/L 87 70 - 130

Acetone 1.9 U 20.0 18.4 ug/L 92 70 - 130

Benzene 0.16 U 5.00 5.07 ug/L 101 70 - 130

Carbon disulfide 0.45 U 5.00 4.95 ug/L 99 70 - 130

Carbon tetrachloride 0.19 U 5.00 4.82 ug/L 96 70 - 130

Chlorobenzene 0.17 U 5.00 4.80 ug/L 96 70 - 130

Chloroform 2.3 5.00 7.14 ug/L 97 70 - 130

Ethylbenzene 0.16 U 5.00 4.73 ug/L 95 70 - 130

Methylene Chloride 0.32 U 5.00 4.62 ug/L 92 70 - 130

Tetrachloroethene 0.20 U 5.00 4.89 ug/L 98 70 - 130

Toluene 0.17 U 5.00 5.22 ug/L 104 70 - 130

Trichloroethene 0.16 U 5.00 4.69 ug/L 94 70 - 130

Vinyl chloride 0.10 U 5.00 4.50 ug/L 90 70 - 130

Xylenes, Total 0.19 U 10.0 9.38 ug/L 94 70 - 130


Surrogate

96

MS MS





Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 407821

1,1,1-Trichloroethane 0.16 U 5.00 4.72 ug/L 94 70 - 130 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,1,2-Trichloroethane 0.27 U 5.00 5.07 ug/L 101 70 - 130 1 20

1,1-Dichloroethane 0.22 U 5.00 4.90 ug/L 98 70 - 130 2 20

1,1-Dichloroethene 0.23 U 5.00 4.78 ug/L 96 70 - 130 4 20

1,2-Dichloroethane 0.13 U 5.00 4.87 ug/L 97 70 - 130 4 20

2-Butanone (MEK) 2.0 U 20.0 19.3 ug/L 97 70 - 130 9 20

4-Methyl-2-pentanone (MIBK) 0.98 U 20.0 18.2 ug/L 91 70 - 130 4 20

Acetone 1.9 U 20.0 19.1 ug/L 96 70 - 130 4 20

Benzene 0.16 U 5.00 5.14 ug/L 103 70 - 130 1 20

Carbon disulfide 0.45 U 5.00 4.94 ug/L 99 70 - 130 0 20

Carbon tetrachloride 0.19 U 5.00 4.87 ug/L 97 70 - 130 1 20

Chlorobenzene 0.17 U 5.00 5.02 ug/L 100 70 - 130 5 20

Chloroform 2.3 5.00 7.16 ug/L 97 70 - 130 0 20

Ethylbenzene 0.16 U 5.00 4.93 ug/L 99 70 - 130 4 20

Methylene Chloride 0.32 U 5.00 4.79 ug/L 96 70 - 130 3 20

Tetrachloroethene 0.20 U 5.00 5.00 ug/L 100 70 - 130 2 20

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Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 407821

Toluene 0.17 U 5.00 5.37 ug/L 107 70 - 130 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Trichloroethene 0.16 U 5.00 4.83 ug/L 97 70 - 130 3 20

Vinyl chloride 0.10 U 5.00 4.96 ug/L 99 70 - 130 10 20

Xylenes, Total 0.19 U 10.0 9.53 ug/L 95 70 - 130 2 20


Surrogate

96

MSD MSD





Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)

Client Sample ID: Method BlankLab Sample ID: MB 280-407819/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 408262 Prep Batch: 407819

RL MDL

Acenaphthene 11 U 100 11 ng/L 03/14/18 13:59 03/18/18 13:41 1

MB MB


10 U 10100 ng/L 03/14/18 13:59 03/18/18 13:41 1Acenaphthylene

14 U 14100 ng/L 03/14/18 13:59 03/18/18 13:41 1Anthracene

3.69 J 3.2100 ng/L 03/14/18 13:59 03/18/18 13:41 1Benzo[a]anthracene

5.1 U 5.1100 ng/L 03/14/18 13:59 03/18/18 13:41 1Benzo[a]pyrene

3.4 U 3.4100 ng/L 03/14/18 13:59 03/18/18 13:41 1Benzo[b]fluoranthene

3.6 U 3.6100 ng/L 03/14/18 13:59 03/18/18 13:41 1Benzo[g,h,i]perylene

5.1 U 5.1100 ng/L 03/14/18 13:59 03/18/18 13:41 1Benzo[k]fluoranthene

3.41 J 3.2100 ng/L 03/14/18 13:59 03/18/18 13:41 1Chrysene

4.8 U 4.8100 ng/L 03/14/18 13:59 03/18/18 13:41 1Dibenz(a,h)anthracene

4.65 J 4.5100 ng/L 03/14/18 13:59 03/18/18 13:41 1Fluoranthene

19 U 19100 ng/L 03/14/18 13:59 03/18/18 13:41 1Fluorene

15 U 15100 ng/L 03/14/18 13:59 03/18/18 13:41 1Indeno[1,2,3-cd]pyrene

5.3 U 5.3100 ng/L 03/14/18 13:59 03/18/18 13:41 1Naphthalene

9.8 U 9.8100 ng/L 03/14/18 13:59 03/18/18 13:41 1Phenanthrene

8.1 U 8.1100 ng/L 03/14/18 13:59 03/18/18 13:41 1Pyrene

2-Fluorobiphenyl 89 42 - 120 03/18/18 13:41 1

MB MB

Surrogate

03/14/18 13:59

Dil FacPrepared AnalyzedQualifier Limits%Recovery

92 03/14/18 13:59 03/18/18 13:41 1Nitrobenzene-d5 43 - 120

86 03/14/18 13:59 03/18/18 13:41 1Terphenyl-d14 47 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-407819/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 408262 Prep Batch: 407819

Acenaphthene 900 767 ng/L 85 70 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthylene 900 714 ng/L 79 70 - 130

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Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)


Anthracene 900 779 ng/L 87 70 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzo[a]anthracene 900 770 ng/L 86 70 - 130

Benzo[a]pyrene 900 736 ng/L 82 70 - 130

Benzo[b]fluoranthene 900 745 ng/L 83 70 - 130

Benzo[g,h,i]perylene 900 737 ng/L 82 70 - 130

Benzo[k]fluoranthene 900 778 ng/L 86 70 - 130

Chrysene 900 814 ng/L 90 70 - 130

Dibenz(a,h)anthracene 900 737 ng/L 82 70 - 130

Fluoranthene 900 763 ng/L 85 70 - 130

Fluorene 900 788 ng/L 88 70 - 130

Indeno[1,2,3-cd]pyrene 900 708 ng/L 79 70 - 130

Naphthalene 900 708 ng/L 79 70 - 130

Phenanthrene 900 763 ng/L 85 70 - 130

Pyrene 900 796 ng/L 88 70 - 130

2-Fluorobiphenyl 42 - 120

Surrogate

84

LCS LCS


89Nitrobenzene-d5 43 - 120

95Terphenyl-d14 47 - 120

Client Sample ID: B3HL11Lab Sample ID: 280-107262-1 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 408262 Prep Batch: 407819

Acenaphthene 10 U 868 766 ng/L 88 47 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Acenaphthylene 9.5 U 868 697 ng/L 80 39 - 120

Anthracene 13 U 868 753 ng/L 87 28 - 120

Benzo[a]anthracene 3.5 J B 868 765 ng/L 88 42 - 120

Benzo[a]pyrene 4.9 U 868 768 ng/L 88 38 - 120

Benzo[b]fluoranthene 3.3 U 868 776 ng/L 89 44 - 120

Benzo[g,h,i]perylene 3.4 U 868 766 ng/L 88 39 - 120

Benzo[k]fluoranthene 4.8 U 868 796 ng/L 92 43 - 120

Chrysene 3.8 J B 868 788 ng/L 90 35 - 120

Dibenz(a,h)anthracene 4.6 U 868 759 ng/L 87 27 - 126

Fluoranthene 4.7 J B 868 810 ng/L 93 46 - 120

Fluorene 18 U 868 796 ng/L 92 49 - 120

Indeno[1,2,3-cd]pyrene 14 U 868 734 ng/L 85 38 - 120

Naphthalene 7.3 J 868 714 ng/L 81 37 - 120

Phenanthrene 9.3 U 868 763 ng/L 88 46 - 120

Pyrene 7.7 U 868 863 ng/L 99 49 - 120


Surrogate

92

MS MS




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Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)

Client Sample ID: B3HL11Lab Sample ID: 280-107262-1 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 408262 Prep Batch: 407819

Acenaphthene 10 U 850 714 ng/L 84 47 - 120 7 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Acenaphthylene 9.5 U 850 675 ng/L 79 39 - 120 3 20

Anthracene 13 U 850 715 ng/L 84 28 - 120 5 20

Benzo[a]anthracene 3.5 J B 850 724 ng/L 85 42 - 120 6 20

Benzo[a]pyrene 4.9 U 850 670 ng/L 79 38 - 120 14 20

Benzo[b]fluoranthene 3.3 U 850 692 ng/L 81 44 - 120 11 20

Benzo[g,h,i]perylene 3.4 U 850 669 ng/L 79 39 - 120 14 20

Benzo[k]fluoranthene 4.8 U 850 695 ng/L 82 43 - 120 14 20

Chrysene 3.8 J B 850 755 ng/L 88 35 - 120 4 20

Dibenz(a,h)anthracene 4.6 U 850 654 ng/L 77 27 - 126 15 20

Fluoranthene 4.7 J B 850 693 ng/L 81 46 - 120 16 20

Fluorene 18 U 850 738 ng/L 87 49 - 120 8 20

Indeno[1,2,3-cd]pyrene 14 U 850 690 ng/L 81 38 - 120 6 20

Naphthalene 7.3 J 850 659 ng/L 77 37 - 120 8 20

Phenanthrene 9.3 U 850 720 ng/L 85 46 - 120 6 20

Pyrene 7.7 U 850 744 ng/L 88 49 - 120 15 20


Surrogate

87

MSD MSD




Method: 6010D - Metals (ICP)


RL MDL

Calcium 73.13 B 200 34.5 ug/L 03/15/18 08:26 03/17/18 04:01 1

MB MB


22.0 U 22.0100 ug/L 03/15/18 08:26 03/17/18 04:01 1Iron

18.99 B 10.7200 ug/L 03/15/18 08:26 03/17/18 04:01 1Magnesium

13.5 U 13.53000 ug/L 03/15/18 08:26 03/17/18 04:01 1Phosphorus

117 U 1171000 ug/L 03/15/18 08:26 03/17/18 04:01 1Sodium

1.1 U 1.110.0 ug/L 03/15/18 08:26 03/17/18 04:01 1Vanadium


RL MDL

Boron 4.4 U 100 4.4 ug/L 03/15/18 08:26 03/21/18 01:39 1

MB MB


560.8 B 2373000 ug/L 03/15/18 08:26 03/21/18 01:39 1Potassium

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Calcium 50000 48860 ug/L 98 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Iron 1000 977.7 ug/L 98 80 - 120

Magnesium 50000 49180 ug/L 98 80 - 120

Phosphorus 10000 9870 ug/L 99 80 - 120

Sodium 50000 52510 ug/L 105 80 - 120

Vanadium 500 497.8 ug/L 100 80 - 120


Boron 1000 1029 ug/L 103 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Potassium 50000 49460 ug/L 99 80 - 120

Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 408303 Prep Batch: 407758

Calcium 29800 50000 80550 ug/L 101 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Iron 37.0 B 1000 1064 ug/L 103 75 - 125

Magnesium 6410 50000 56800 ug/L 101 75 - 125

Phosphorus 75.4 B 10000 10230 ug/L 102 75 - 125

Sodium 97300 50000 154600 ug/L 115 75 - 125

Vanadium 17.5 500 527.0 ug/L 102 75 - 125


Potassium 5430 C 50000 55650 ug/L 100 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Boron 75.4 B 1000 1202 ug/L 113 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 408303 Prep Batch: 407758

Calcium 29800 50000 76240 ug/L 93 75 - 125 5 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Iron 37.0 B 1000 1025 ug/L 99 75 - 125 4 20

Magnesium 6410 50000 56150 ug/L 99 75 - 125 1 20

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Phosphorus 75.4 B 10000 10150 ug/L 101 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Sodium 97300 50000 144900 ug/L 95 75 - 125 6 20

Vanadium 17.5 500 522.8 ug/L 101 75 - 125 1 20


Potassium 5430 C 50000 54920 ug/L 99 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Boron 75.4 B 1000 1232 ug/L 116 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Antimony 0.40 U 2.0 0.40 ug/L 03/15/18 08:26 03/16/18 00:42 1

MB MB


0.33 U 0.335.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Arsenic

0.080 U 0.0801.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Beryllium

0.27 U 0.271.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Cadmium

0.50 U 0.502.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Chromium

0.054 U 0.0541.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Cobalt

0.56 U 0.562.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Copper

0.18 U 0.181.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Lead

0.14 U 0.142.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Molybdenum

0.30 U 0.302.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Nickel

0.70 U 0.705.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Selenium

0.033 U 0.0335.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Silver

0.310 B 0.3010.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Strontium

0.0890 B 0.0501.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Thallium

1.2 U 1.25.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Thorium

0.77 U 0.7710.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Tin

0.050 U 0.0501.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Uranium

2.0 U 2.010.0 ug/L 03/15/18 08:26 03/16/18 00:42 1Zinc

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Method: 6020B - Metals (ICP/MS) (Continued)


RL MDL

Aluminum 9.2 U 50.0 9.2 ug/L 03/15/18 08:26 03/19/18 15:36 1

MB MB


0.29 U 0.291.0 ug/L 03/15/18 08:26 03/19/18 15:36 1Barium

0.417 B 0.311.0 ug/L 03/15/18 08:26 03/19/18 15:36 1Manganese


Antimony 40.0 40.35 ug/L 101 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 40.0 38.76 ug/L 97 80 - 120

Beryllium 40.0 43.70 ug/L 109 80 - 120

Cadmium 40.0 42.50 ug/L 106 80 - 120

Chromium 40.0 38.26 ug/L 96 80 - 120

Cobalt 40.0 38.94 ug/L 97 80 - 120

Copper 40.0 40.47 ug/L 101 80 - 120

Lead 40.0 41.37 ug/L 103 80 - 120

Molybdenum 40.0 40.84 ug/L 102 80 - 120

Nickel 40.0 42.47 ug/L 106 80 - 120

Selenium 40.0 39.12 ug/L 98 80 - 120

Silver 40.0 40.13 ug/L 100 80 - 120

Strontium 40.0 43.98 ug/L 110 80 - 120

Thallium 40.0 40.87 ug/L 102 80 - 120

Thorium 40.0 41.10 ug/L 103 80 - 120

Tin 40.0 42.69 ug/L 107 80 - 120

Uranium 40.0 40.87 ug/L 102 80 - 120

Zinc 40.0 42.24 ug/L 106 80 - 120


Aluminum 400 426.0 ug/L 107 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 40.0 41.13 ug/L 103 80 - 120

Manganese 40.0 40.05 ug/L 100 80 - 120


Antimony 0.40 U 40.0 38.90 ug/L 97 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Beryllium 0.080 U 40.0 44.29 ug/L 111 75 - 125

Cadmium 0.27 U 40.0 42.33 ug/L 106 75 - 125

Chromium 8.2 40.0 46.80 ug/L 97 75 - 125

Cobalt 0.054 U 40.0 39.09 ug/L 98 75 - 125

Copper 0.56 U 40.0 39.99 ug/L 100 75 - 125

Lead 0.18 U 40.0 40.47 ug/L 101 75 - 125

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Molybdenum 5.8 40.0 46.22 ug/L 101 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Nickel 1.3 B 40.0 40.06 ug/L 97 75 - 125

Selenium 1.3 B 40.0 39.96 ug/L 97 75 - 125

Silver 0.033 U 40.0 40.23 ug/L 101 75 - 125

Strontium 208 40.0 239.0 X ug/L 78 75 - 125

Thallium 0.050 U 40.0 40.66 ug/L 102 75 - 125

Thorium 1.2 U 40.0 40.81 ug/L 102 75 - 125

Tin 0.77 U 40.0 40.76 ug/L 102 75 - 125

Uranium 2.7 40.0 43.49 ug/L 102 75 - 125


Aluminum 23.8 B 400 410.9 ug/L 97 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Arsenic 6.9 40.0 45.27 ug/L 96 75 - 125

Barium 50.2 40.0 85.78 ug/L 89 75 - 125

Manganese 1.0 C 40.0 41.64 ug/L 102 75 - 125

Zinc 2.0 U 40.0 41.48 ug/L 104 75 - 125


Antimony 0.40 U 40.0 41.61 ug/L 104 75 - 125 7 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Beryllium 0.080 U 40.0 45.30 ug/L 113 75 - 125 2 20

Cadmium 0.27 U 40.0 41.69 ug/L 104 75 - 125 2 20

Chromium 8.2 40.0 46.93 ug/L 97 75 - 125 0 20

Cobalt 0.054 U 40.0 39.70 ug/L 99 75 - 125 2 20

Copper 0.56 U 40.0 40.31 ug/L 101 75 - 125 1 20

Lead 0.18 U 40.0 41.10 ug/L 103 75 - 125 2 20

Molybdenum 5.8 40.0 47.93 ug/L 105 75 - 125 4 20

Nickel 1.3 B 40.0 39.87 ug/L 96 75 - 125 0 20

Selenium 1.3 B 40.0 40.33 ug/L 98 75 - 125 1 20

Silver 0.033 U 40.0 40.41 ug/L 101 75 - 125 0 20

Strontium 208 40.0 249.4 X ug/L 104 75 - 125 4 20

Thallium 0.050 U 40.0 41.12 ug/L 103 75 - 125 1 20

Thorium 1.2 U 40.0 41.66 ug/L 104 75 - 125 2 20

Tin 0.77 U 40.0 42.68 ug/L 107 75 - 125 5 20

Uranium 2.7 40.0 44.49 ug/L 105 75 - 125 2 20


Aluminum 23.8 B 400 450.9 ug/L 107 75 - 125 9 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

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Arsenic 6.9 40.0 46.46 ug/L 99 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 50.2 40.0 84.08 ug/L 85 75 - 125 2 20

Manganese 1.0 C 40.0 43.20 ug/L 105 75 - 125 4 20

Zinc 2.0 U 40.0 40.09 ug/L 100 75 - 125 3 20

Method: 9020B - Organic Halides, Total (TOX)


RL MDL


MB MB



Total Organic Halogens - Dup 100 110.2 ug/L 110 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: B3HJ95Lab Sample ID: 280-107262-7 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 409937

Total Organic Halogens - Dup 7.7 U 100 106.6 ug/L 107 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: B3HJ95Lab Sample ID: 280-107262-7 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 409937

Total Organic Halogens - Dup 7.7 U 100 109.5 ug/L 110 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


RL MDL


MB MB



Total Organic Halogens - Dup 100 110.2 ug/L 110 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 9060A - Organic Carbon, Total (TOC)


RL MDL

Total Organic Carbon - Average 155 U 1000 155 ug/L 03/28/18 14:50 1

MB MB



Total Organic Carbon - Average 25000 24970 ug/L 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


RL MDL

Total Organic Carbon - Average 155 U 1000 155 ug/L 04/03/18 11:07 1

MB MB



Total Organic Carbon - Average 25000 24810 ug/L 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: B3HJ95Lab Sample ID: 280-107262-7 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 410130

Total Organic Carbon - Average 561 B 25000 25450 ug/L 100 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: B3HJ95Lab Sample ID: 280-107262-7 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 410130

Total Organic Carbon - Average 561 B 25000 26680 ug/L 104 75 - 125 5 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: SM 2320B - Alkalinity


RL MDL

Alkalinity as CaCO3 1070 U 5000 1070 ug/L 03/15/18 22:57 1

MB MB


1070 U 10705000 ug/L 03/15/18 22:57 1Hydroxide Alkalinity as CaCO3

1070 U 10705000 ug/L 03/15/18 22:57 1Carbonate Alkalinity as CaCO3

1070 U 10705000 ug/L 03/15/18 22:57 1Bicarbonate Alkalinity as CaCO3

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Method: SM 2320B - Alkalinity (Continued)


Alkalinity as CaCO3 200000 218000 ug/L 109 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-408183/5Matrix: Water Prep Type: Total/NAAnalysis Batch: 408183

Alkalinity as CaCO3 200000 217400 ug/L 109 80 - 120 0 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: B3HFP1Lab Sample ID: 280-107262-2 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 408183

Alkalinity as CaCO3 157000 155000 ug/L 1 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

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QC Association SummaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


GC/MS VOA

Analysis Batch: 407821

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B280-107262-2 B3HFP1 Total/NA

Water 8260B280-107262-6 B3H047 Total/NA

Water 8260BMB 280-407821/6 Method Blank Total/NA

Water 8260BLCS 280-407821/4 Lab Control Sample Total/NA

Water 8260BLCSD 280-407821/5 Lab Control Sample Dup Total/NA

Water 8260B280-107262-2 MS B3HFP1 Total/NA

Water 8260B280-107262-2 MSD B3HFP1 Total/NA

GC/MS Semi VOA

Prep Batch: 407819


Water 3510C280-107262-1 B3HL11 Total/NA

Water 3510CMB 280-407819/1-A Method Blank Total/NA

Water 3510CLCS 280-407819/2-A Lab Control Sample Total/NA

Water 3510C280-107262-1 MS B3HL11 Total/NA

Water 3510C280-107262-1 MSD B3HL11 Total/NA



Water 8270D SIM 407819280-107262-1 B3HL11 Total/NA

Water 8270D SIM 407819MB 280-407819/1-A Method Blank Total/NA

Water 8270D SIM 407819LCS 280-407819/2-A Lab Control Sample Total/NA

Water 8270D SIM 407819280-107262-1 MS B3HL11 Total/NA

Water 8270D SIM 407819280-107262-1 MSD B3HL11 Total/NA

Metals

Prep Batch: 407757


Water 3020A280-107262-2 B3HFP1 Total/NA


Water 3020A280-107262-4 B3HFN4 Total/NA


Water 3020A280-107262-12 B3H489 Total/NA

Water 3020A280-107262-13 B3H4B0 Total/NA

Water 3020A280-107262-14 B3H490 Total/NA

Water 3020A280-107262-15 B3H4B1 Total/NA

Water 3020AMB 280-407757/1-A Method Blank Total/NA

Water 3020ALCS 280-407757/2-A Lab Control Sample Total/NA

Water 3020A280-107262-2 MS B3HFP1 Total/NA

Water 3020A280-107262-2 MSD B3HFP1 Total/NA

Prep Batch: 407758






Water 3010AMB 280-407758/1-A Method Blank Total/NA

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Metals (Continued)

Prep Batch: 407758 (Continued)


Water 3010ALCS 280-407758/2-A Lab Control Sample Total/NA

Water 3010A280-107262-2 MS B3HFP1 Total/NA

Water 3010A280-107262-2 MSD B3HFP1 Total/NA



Water 6020B 407757280-107262-2 B3HFP1 Total/NA


Water 6020B 407757280-107262-4 B3HFN4 Total/NA


Water 6020B 407757280-107262-12 B3H489 Total/NA

Water 6020B 407757280-107262-13 B3H4B0 Total/NA

Water 6020B 407757280-107262-14 B3H490 Total/NA

Water 6020B 407757280-107262-15 B3H4B1 Total/NA

Water 6020B 407757MB 280-407757/1-A Method Blank Total/NA

Water 6020B 407757LCS 280-407757/2-A Lab Control Sample Total/NA

Water 6020B 407757280-107262-2 MS B3HFP1 Total/NA

Water 6020B 407757280-107262-2 MSD B3HFP1 Total/NA



Water 6010D 407758280-107262-2 B3HFP1 Total/NA


Water 6010D 407758280-107262-4 B3HFN4 Total/NA


Water 6010D 407758MB 280-407758/1-A Method Blank Total/NA

Water 6010D 407758LCS 280-407758/2-A Lab Control Sample Total/NA

Water 6010D 407758280-107262-2 MS B3HFP1 Total/NA

Water 6010D 407758280-107262-2 MSD B3HFP1 Total/NA







Water 6020B 407757MB 280-407757/1-A Method Blank Total/NA

Water 6020B 407757LCS 280-407757/2-A Lab Control Sample Total/NA

Water 6020B 407757280-107262-2 MS B3HFP1 Total/NA

Water 6020B 407757280-107262-2 MSD B3HFP1 Total/NA







Water 6010D 407758MB 280-407758/1-A Method Blank Total/NA

Water 6010D 407758LCS 280-407758/2-A Lab Control Sample Total/NA



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General Chemistry



Water SM 2320B280-107262-2 B3HFP1 Total/NA

Water SM 2320B280-107262-11 B3H3R4 Total/NA

Water SM 2320BMB 280-408183/6 Method Blank Total/NA

Water SM 2320BLCS 280-408183/4 Lab Control Sample Total/NA

Water SM 2320BLCSD 280-408183/5 Lab Control Sample Dup Total/NA

Water SM 2320B280-107262-2 DU B3HFP1 Total/NA



Water 9060A280-107262-8 B3HJD6 Total/NA



Water 9060AMB 280-409524/4 Method Blank Total/NA

Water 9060ALCS 280-409524/3 Lab Control Sample Total/NA



Water 9020B280-107262-7 B3HJ95 Total/NA



Water 9020B280-107262-7 MS B3HJ95 Total/NA

Water 9020B280-107262-7 MSD B3HJ95 Total/NA



Water 9020B280-107262-8 B3HJD6 Total/NA







Water 9060A280-107262-7 B3HJ95 Total/NA

Water 9060AMB 280-410130/4 Method Blank Total/NA

Water 9060ALCS 280-410130/3 Lab Control Sample Total/NA

Water 9060A280-107262-7 MS B3HJ95 Total/NA

Water 9060A280-107262-7 MSD B3HJ95 Total/NA

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Surrogate SummaryTestAmerica Job ID: 280-107262-1Client: CH2M Hill Plateau Remediation Company


Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (70-130) (70-130) (70-130) (70-130)

DCA BFB DBFM TOL

96 99 104 106280-107262-2

Percent Surrogate Recovery (Acceptance Limits)

B3HFP1

96 94 100 100280-107262-2 MS B3HFP1

96 98 102 107280-107262-2 MSD B3HFP1

92 106 101 112280-107262-6 B3H047

85 113 93 105LCS 280-407821/4 Lab Control Sample

98 99 102 111LCSD 280-407821/5 Lab Control Sample Dup

103 105 108 117MB 280-407821/6 Method Blank

Surrogate Legend

DCA = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (42-120) (43-120) (47-120)

FBP NBZ TPHL

72 73 82280-107262-1

Percent Surrogate Recovery (Acceptance Limits)

B3HL11

92 95 108280-107262-1 MS B3HL11

87 89 90280-107262-1 MSD B3HL11

84 89 95LCS 280-407819/2-A Lab Control Sample

89 92 86MB 280-407819/1-A Method Blank

Surrogate Legend

FBP = 2-Fluorobiphenyl

NBZ = Nitrobenzene-d5

TPHL = Terphenyl-d14

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WMU Code WELL NAME SITE TYPE PARENT WMU DESCRIPTION

DN0332

SAMP NUM

1301-N 199-N-105A TSD 1301-N 1301-N Liquid Waste Disposal FacilityB3HJ95

1301-N 199-N-105A TSD 1301-N 1301-N Liquid Waste Disposal FacilityB3HJD6



241TX 299-W14-15 WMU SST 200 West Area Underground Waste Storage Tank FarmB3H3R4

241TY 299-W14-15 WMU SST 200 West Area Underground Waste Storage Tank FarmB3H3R4

04/09/2018 rev.0 testamerica

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