wilson, tabatha

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Wilson, Tabatha

From: Reiber, LorettaSent: Tuesday, May 13, 2014 8:29 AMTo: Wilson, TabathaSubject: FW: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016Attachments: 0537_001.pdf; RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN

70-00016; 644597.pdf

Can you please put the attachments and this e‐mail on the web and Zylab? Thanks.

From: Tom Hammons [mailto:[email protected]] Sent: Friday, May 02, 2014 1:15 PM To: Reiber, Loretta; Suel, Kevin Cc: Chuck Hammock; Mitch Colvin Subject: FW: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Loretta, Attached are the dioxin results, I had previously sent them on 3/25. I spoke witht eh lab and the pesticide RL was a typo. Attached is the corrected report from the lab. Thanks, Tom Hammons

From: Tom Hammons Sent: Tuesday, March 25, 2014 5:47 PM To: Reiber, Loretta; Suel, Kevin Cc: Chuck Hammock; Mitch Colvin Subject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Loretta, Thank you for the congratulations. After receiving your email I reviewed what was submitted and realized that I inadvertently left out the dioxin results. These results were from the Summit lab and were in the attachments of the complete report. These results are included in the attachment that accompanies this email. If I need to resubmit the complete report, let me know. I attempted to contact you this afternoon concerning the MQL’s of some of the pesticides. After speaking with Mr. Suel, I reviewed some of our previous PPS data and I see that some of the MQL’s appear to be incorrect. I will contact the lab and attempt to clear this up. Thanks Tom Hammons Lion Oil Company

From: Reiber, Loretta [mailto:[email protected]] Sent: Monday, March 24, 2014 3:14 PM

2

To: Tom Hammons; Suel, Kevin Cc: Chuck Hammock; Mitch Colvin Subject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Tom, I have looked at the PPS information that you e‐mailed to me. I didn’t receive any information regarding dioxins. Also, several of the pesticides on page 2 of the lab report were listed as having an MQL of 1,000 µg/l. Since that is much higher than what is required, I’m questioning if the units are incorrect. Can you please look into the matter? Congratulations on your new baby! Thanks. Loretta

From: Tom Hammons [mailto:[email protected]] Sent: Friday, March 21, 2014 5:26 PM To: Suel, Kevin; Reiber, Loretta Cc: Chuck Hammock; Mitch Colvin Subject: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Pleased see the attached PPS for the Lion Oil Refinery 010 Outfall. A hard copy is also en route via Fed Ex. If you have any questions, feel free to give me a call at 870‐864‐1449. Thanks Tom Hammons Lion Oil Company

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Wilson, Tabatha

From: Reiber, LorettaSent: Monday, April 28, 2014 1:36 PMTo: Tom Hammons; Suel, KevinCc: Chuck Hammock; Mitch ColvinSubject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016

I have not received the dioxin results or the information regarding the pesticides. Was it submitted and I just haven’t seen it? If it has not been submitted, please let me know ASAP when I can expect to see it. Loretta Reiber, P.E. Engineer, NPDES Permits

From: Reiber, Loretta Sent: Wednesday, March 26, 2014 7:46 AM To: 'Tom Hammons'; Suel, Kevin Cc: Chuck Hammock; Mitch Colvin Subject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Just submit the dioxin results. We don’t need the whole report again. I just figured you were sleep deprived when they weren’t included After you contact the lab regarding the pesticides, please let me know what they have to say. Thanks.

From: Tom Hammons [mailto:[email protected]] Sent: Tuesday, March 25, 2014 5:47 PM To: Reiber, Loretta; Suel, Kevin Cc: Chuck Hammock; Mitch Colvin Subject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Loretta, Thank you for the congratulations. After receiving your email I reviewed what was submitted and realized that I inadvertently left out the dioxin results. These results were from the Summit lab and were in the attachments of the complete report. These results are included in the attachment that accompanies this email. If I need to resubmit the complete report, let me know. I attempted to contact you this afternoon concerning the MQL’s of some of the pesticides. After speaking with Mr. Suel, I reviewed some of our previous PPS data and I see that some of the MQL’s appear to be incorrect. I will contact the lab and attempt to clear this up. Thanks Tom Hammons Lion Oil Company

From: Reiber, Loretta [mailto:[email protected]] Sent: Monday, March 24, 2014 3:14 PM To: Tom Hammons; Suel, Kevin

2

Cc: Chuck Hammock; Mitch Colvin Subject: RE: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Tom, I have looked at the PPS information that you e‐mailed to me. I didn’t receive any information regarding dioxins. Also, several of the pesticides on page 2 of the lab report were listed as having an MQL of 1,000 µg/l. Since that is much higher than what is required, I’m questioning if the units are incorrect. Can you please look into the matter? Congratulations on your new baby! Thanks. Loretta

From: Tom Hammons [mailto:[email protected]] Sent: Friday, March 21, 2014 5:26 PM To: Suel, Kevin; Reiber, Loretta Cc: Chuck Hammock; Mitch Colvin Subject: Lion Oil Company, NPDES Permit Number AR0000647, AFIN 70-00016 Pleased see the attached PPS for the Lion Oil Refinery 010 Outfall. A hard copy is also en route via Fed Ex. If you have any questions, feel free to give me a call at 870‐864‐1449. Thanks Tom Hammons Lion Oil Company

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement

Results05/01/2014Printed: Page 1 of 7

Report To

Mitch Colvin Tom Hammons

Lion Oil

P. O. Box 7005

1000 McHenry

El Dorado, AR 71731-7005

644597LIN5-LAccount Project

Results

BottleCASFlagsRLUnitsResultsParameter

1280758 Priority Pollutant Scan

02/26/2014 09:00:00T HammonsCollected by:

02/26/2014Received:

Liquid Aqueous Affiliation: Lion Oil

Prepared: 03/07/2014 10:00:00

EPA 1613 -- Subcontr 03/07/2014 10:00:00SKL QCgroupAnalyzed

See Attached SEMO2378-tetrachlorodibenzo-p-dioxin

Prepared: 557089 02/27/2014 09:45:00

EPA 200.8 5.4 02/27/2014 15:19:00WOB QCgroup 557158Analyzed

0.000873 mg/L J0.001 7440-36-0Antimony 23N

0.00464 mg/L 0.0005 7440-38-2Arsenic 23N

<0.0005 mg/L 0.0005 7440-41-7Beryllium 23N

<0.0005 mg/L 0.0005 7440-43-9Cadmium 23N

0.00203 mg/L 0.0005 7440-47-3Chromium 23N

0.00515 mg/L 0.001 7440-50-8Copper 23N

0.00371 mg/L 0.0005 7439-92-1Lead 23N

0.00453 mg/L 0.001 7440-02-0Nickel 23N

0.00733 mg/L 0.001 7782-49-2Selenium 23N

<0.0005 mg/L 0.0005 7440-22-4Silver 23N

0.00032 mg/L J0.0005 7440-28-0Thallium 23N

EPA 200.8 5.4 02/28/2014 13:05:00WOB QCgroup 557309Analyzed

0.0527 mg/L 0.005 7440-66-6Zinc 23N

Prepared: 557069 02/27/2014 10:15:00

EPA 245.1 3 02/28/2014 10:15:00WOB QCgroup 557243Analyzed

0.240 ug/L 0.200 7439-97-6Mercury 20N

Prepared: 557067 02/27/2014 12:00:00

EPA 420.4 1 02/28/2014 11:12:43MDD QCgroup 557249Analyzed

0.0044 mg/L J0.005Phenolics, Total Recoverable 25N

Prepared: 557175 02/27/2014 09:00:00

EPA 608 02/28/2014 13:06:00KJS QCgroup 557283Analyzed

<0.200 ug/L 0.200 12674-11-2PCB-1016 26N

<0.200 ug/L 0.200 11104-28-2PCB-1221 26N

<0.200 ug/L 0.200 11141-16-5PCB-1232 26N

<0.200 ug/L 0.200 53469-21-9PCB-1242 26N

<0.200 ug/L 0.200 12672-29-6PCB-1248 26N

<0.200 ug/L 0.200 11097-69-1PCB-1254 26N

<0.200 ug/L 0.200 11096-82-5PCB-1260 26N

<0.010 ug/L 0.010 309-00-2Aldrin 26N

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.5.17.799 www.ana-lab.com

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

NELAP-accredited #T104704201

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Results




02/26/2014Received:



<0.0253 ug/L 0.0253 319-84-6Alpha-BHC(hexachlorocyclohexane) 26N

<0.0101 ug/L 0.0101 319-85-7Beta-BHC(hexachlorocyclohexane) 26N

<0.0101 ug/L 0.0101 319-86-8Delta-BHC(hexachlorocyclohexane) 26N

0.0640 ug/L 0.0101 58-89-9Gamma-BHC(Lindane) 26N

<0.0101 ug/L 0.0101 12789-0306Chlordane 26N

<0.0253 ug/L 0.0253 72-54-84,4-DDD 26N

<0.0253 ug/L 0.0253 72-55-94,4-DDE 26N

<0.0101 ug/L 0.0101 50-29-34,4-DDT 26N

<0.0101 ug/L 0.0101 60-57-1Dieldrin 26N

<0.010 ug/L 0.010 959-98-8Endosulfan I (alpha) 26N

<0.0101 ug/L 0.0101 33213-65-9Endosulfan II (beta) 26N

<0.0101 ug/L 0.0101 1031-07-8Endosulfan sulfate 26N

<0.0101 ug/L 0.0101 72-20-8Endrin 26N

<0.0253 ug/L 0.0253 7421-93-4Endrin aldehyde 26N

<0.010 ug/L 0.010 76-44-8Heptachlor 26

<0.010 ug/L 0.010 1024-57-3Heptachlor epoxide 26N

<0.0101 ug/L 0.0101 8001-35-2Toxaphene 26N

Prepared: 557195 02/27/2014 09:00:00


<0.0404 ug/L 0.0404 2921-88-2Chlorpyrifos 27N

Prepared: 557275 02/28/2014 12:50:00

EPA 624 02/28/2014 12:50:00AAC QCgroup 557275Analyzed

<1.00 ug/L 1.00 71-43-2Benzene 09N

<1.00 ug/L 1.00 75-27-4Bromodichloromethane 09N

<1.00 ug/L 1.00 75-25-2Bromoform 09N

<1.00 ug/L 1.00 74-83-9Bromomethane (Methyl Bromi 09N

<1.00 ug/L 1.00 56-23-5Carbon Tetrachloride 09N

<1.00 ug/L 1.00 108-90-7Chlorobenzene 09N

<1.00 ug/L 1.00 75-00-3Chloroethane 09N

0.790 ug/L J1.00 67-66-3Chloroform 09N

<1.00 ug/L 1.00 74-87-3Chloromethane 09N

<1.00 ug/L 1.00 124-48- 1Dibromochloromethane 09N

<1.00 ug/L 1.00 75-34-31,1-Dichloroethane 09N

<1.00 ug/L 1.00 107-06-21,2-Dichloroethane 09N

<1.00 ug/L 1.00 156-60-5trans-1,2-Dichloroethene 09N

<1.00 ug/L 1.00 75-35-41,1-Dichloroethylene 09N

<1.00 ug/L 1.00 78-87-51,2-Dichloropropane 09N

<1.00 ug/L 1.00 10061-01-5cis-1,3-Dichloropropene 09N

<1.00 ug/L 1.00 10061-02-6trans-1,3-Dichloropropene 09N

<1.00 ug/L 1.00 100-41-4Ethylbenzene 09N

<1.00 ug/L 1.00 75-09-2Methylene chloride 09N

<1.00 ug/L 1.00 79-34-51,1,2,2-Tetrachloroethane 09N

<1.00 ug/L 1.00 127-18-4Tetrachloroethylene 09N





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Results




02/26/2014Received:



<1.00 ug/L 1.00 108-88-3Toluene 09N

<1.00 ug/L 1.00 71-55-61,1,1-Trichloroethane 09N

<1.00 ug/L 1.00 79-00-51,1,2-Trichloroethane 09N

<1.00 ug/L 1.00 79-01-6Trichloroethylene 09N

<1.00 ug/L 1.00 75-01-4Vinyl chloride 09N

Prepared: 557311 02/28/2014 13:15:00


<1.00 ug/L P1.00 107-02-8Acrolein 13N

<1.00 ug/L 1.00 107-13-1Acrylonitrile 13N

Prepared: 557312 02/28/2014 13:15:00


<1.00 ug/L 1.00 110-75-82-Chloroethylvinyl ether 13N

Prepared: 557103 02/27/2014 07:50:00


<1.01 ug/L 1.01 83-32-9Acenaphthene 24N

<1.01 ug/L 1.01 208-96-8Acenaphthylene 24N

<1.01 ug/L 1.01 120-12-7Anthracene 24N

<1.52 ug/L 1.52 92-87-5Benzidine 24N

<1.01 ug/L 1.01 56-55-3Benzo(a)anthracene 24N

<1.01 ug/L 1.01 50-32-8Benzo(a)pyrene 24N

<1.01 ug/L 1.01 205-99-2Benzo(b)fluoranthene 24N

<1.01 ug/L 1.01 191-24-2Benzo(ghi)perylene 24N

<1.01 ug/L 1.01 207-08-9Benzo(k)fluoranthene 24N

<1.01 ug/L 1.01 85-68-7Benzyl Butyl phthalate 24N

<1.01 ug/L 1.01 101-55-34-Bromophenyl phenyl ether 24N

12.6 ug/L 1.01 84-74-2Di-n-butylphthalate 24N

<1.01 ug/L 1.01 193-39-5Indeno(1,2,3-cd)pyrene 24N

<1.01 ug/L 1.01 111-91-1Bis(2-chloroethoxy)methane 24N

<1.01 ug/L 1.01 111-44-4Bis(2-chloroethyl)ether 24N

<1.01 ug/L 1.01 39638-32-9Bis(2-chloroisopropyl)ether 24N

<1.01 ug/L 1.01 91-58-72-Chloronaphthalene 24N

<1.01 ug/L 1.01 95-57-82-Chlorophenol 24N

<1.01 ug/L 1.01 7005-72-34-Chlorophenyl phenyl ethe 24N

<1.01 ug/L 1.01 218-01-9Chrysene (Benzo(a)phenanthrene) 24N

<1.01 ug/L 1.01 53-70-3Dibenz(a,h)anthracene 24N

<5.07 ug/L 5.07 541-73-11,3-Dichlorobenzene 24N



<2.03 ug/L 2.03 91-94-13,3'-Dichlorobenzidine 24N

<1.01 ug/L 1.01 120-83-22,4-Dichlorophenol 24N

<1.01 ug/L 1.01 84-66-2Diethyl phthalate 24N

<1.01 ug/L 1.01 131-11-3Dimethyl phthalate 24N

<1.01 ug/L 1.01 105-67-92,4-Dimethylphenol 24N

<2.03 ug/L 2.03 51-28-52,4-Dinitrophenol 24N





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Results




02/26/2014Received:



<2.03 ug/L 2.03 121-14-22,4-Dinitrotoluene 24N

<2.03 ug/L 2.03 606-20-22,6-Dinitrotoluene 24N

<1.01 ug/L 1.01 122-66-71,2-DPH (as azobenzene) 24N

<1.14 ug/L 1.14 117-81-7Bis(2-ethylhexyl)phthalate 24N

<1.01 ug/L 1.01 206-44-0Fluoranthene(Benzo(j,k)fluorene) 24N

<1.01 ug/L 1.01 86-73-7Fluorene 24N

<1.01 ug/L 1.01 118-74-1Hexachlorobenzene 24N

<1.04 ug/L 1.04 87-68-3Hexachlorobutadiene 24N

<1.01 ug/L 1.01 77-47-4Hexachlorocyclopentadiene 24N

<2.03 ug/L 2.03 67-72-1Hexachloroethane 24N

<1.01 ug/L 1.01 78-59-1Isophorone 24N

<1.01 ug/L 1.01 59-50-7p-Chloro-m-Cresol (4-Chloro-3-me 24N

<2.03 ug/L 2.03 534-52-14,6-Dinitro-2-methylphenol 24N

<1.01 ug/L 1.01 91-20-3Naphthalene 24N

<1.01 ug/L 1.01 98-95-3Nitrobenzene 24N

<1.01 ug/L 1.01 88-75-52-Nitrophenol 24N

<1.01 ug/L 1.01 100-02-74-Nitrophenol 24N

<1.01 ug/L 1.01 62-75-9N-Nitrosodimethylamine 24N

<1.01 ug/L 1.01 86-30-6N-Nitrosodiphenylamine (as DPA 24N

<2.03 ug/L 2.03 117-84-0Di-n-octylphthalate 24N

<5.00 ug/L 5.00 87-86-5Pentachlorophenol 24N

<1.01 ug/L 1.01 85-01-8Phenanthrene 24N

<1.01 ug/L 1.01 108-95-2Phenol 24N

<1.01 ug/L 1.01 621-64-7N-Nitrosodi-n-propylamine 24N

<1.01 ug/L 1.01 129-00-0Pyrene 24N

<1.01 ug/L 1.01 120-82-11,2,4-Trichlorobenzene 24N

<2.03 ug/L 2.03 88-06-22,4,6-Trichlorophenol 24N

Prepared: 557137 02/27/2014 08:45:00

SM 3500-Cr B-2009 02/27/2014 08:45:00PJD QCgroup 557137Analyzed

<3.00 ug/L 3.00 7440-47-3Hexavalent Chromium 01N

Prepared: 557048 02/27/2014 10:50:00

SM 4500-CN¯ E-1999 02/27/2014 17:26:44RSV QCgroup 557212Analyzed

0.00202 mg/L J0.005Cyanide 19N

The above methods that we used are approved for NPDES reporting as listed in 40 CFR 136 Table 1B or Ana-Lab has specific approval from EPA to use

these methods for NPDES reporting.

Sample Preparation

1280758 Priority Pollutant Scan 02/26/2014Received:





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Sample Preparation


Prepared: 02/26/2014 00:00:00

02/26/2014 00:00:00AAJ QCgroupAnalyzed

7 SUBottle pH 01z

7 SUBottle pH 02z

7 SUBottle pH 03z

7 SUBottle pH 04z

7 SUBottle pH 05z

<2 SUBottle pH 06z

<2 SUBottle pH 07z

>12 SUBottle pH 08z

<1 degreesBottle Temperature on Receipt 01


















Prepared: 557089 02/27/2014 09:45:00

EPA 200.2 2.8 02/27/2014 09:45:00TES QCgroup 557089Analyzed

50/50 mlLiquid Metals Digestion 06N

Prepared: 557069 02/27/2014 10:15:00

EPA 245.1 3 02/27/2014 10:15:00PJD QCgroup 557069Analyzed

50/25 mlMercury Liquid Metals Digestion 06N

Prepared: 557067 02/27/2014 12:00:00

EPA 420.4 1 02/27/2014 12:00:00CDB QCgroup 557067Analyzed

50/50 mlPhenol Distillation 07N

Prepared: 557175 02/27/2014 09:00:00


Entered 1.00Polychlorinated Biphenyls 26N

Prepared: 557175 02/27/2014 09:00:00





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Sample Preparation


EPA 614/608/617/1657 02/27/2014 09:00:00DWL QCgroup 557175Analyzed

1/989 mlLiquid-Liquid Extr. W/Hex Ex 04

Prepared: 557195 02/27/2014 09:00:00

EPA 614/608/617/1657 02/27/2014 09:00:00DWL QCgroup 557195Analyzed

1/989 mlSolvent Extraction 04

Prepared: 557175 02/27/2014 09:00:00

EPA Method 608 02/28/2014 13:06:00KJS QCgroup 557285Analyzed

EnteredADEQ ArkansasPesticide Exp. 26z

Prepared: 557195 02/27/2014 09:00:00


EnteredChlorpyrifos Expansion 27z

Prepared: 557311 02/28/2014 13:15:00

EPA Method 624 02/28/2014 13:15:00AAC QCgroup 557311Analyzed

EnteredAcrolein/Acrylonitrile Exp. 13N

Prepared: 557312 02/28/2014 13:15:00

EPA Method 624 02/28/2014 13:15:00AAC QCgroup 557312Analyzed

EnteredADEQ Arkansas VOA 13z

Prepared: 557103 02/27/2014 07:50:00

EPA Method 625 02/27/2014 07:50:00TRP QCgroup 557103Analyzed

1/986 mlLiquid-Liquid Extraction, BNA 05N


EnteredADEQ ARKANSAS ABN 24z

Prepared: 557048 02/27/2014 10:50:00

SM 4500-CN¯ E-1999 02/27/2014 10:50:00CRG QCgroup 557048Analyzed

25/50 mlCyanide Distillation 08N





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Qualifiers:

J - Analyte detected below quantitation limit P - Spike recovery outside control limits due to possible matrix

We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's

corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US

Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate

TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking

Water Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of

Environmental Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana

Department of Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals

Drinking Water (NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment

Waste Water and Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not

covered under NELAC scope of accreditation.

These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of

Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.

RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical

Abstract Service number.

C. H. Whiteside, Ph.D., President





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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Quality Control Page 1 of 2805/01/2014Printed


LELAP-accredited #02008

Employee Owned Integrity Caring Continual Improvement

LIN5 -LAccount Project

Mitch Colvin Tom Hammons

Lion Oil

P. O. Box 7005

1000 McHenry

El Dorado, AR 71731-7005

Report ToWW

644597

SM 4500-CN¯ E-1999Liquid Aqueous 557212

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Cyanide 557048 ND 0.00665 0.020 mg/L 114223662

CCV

FileOutLimits%Recover%UnitsKnownReadingParameter

Cyanide 0.533 0.500 mg/L 107 90.0 - 110 114223661

Cyanide 0.525 0.500 mg/L 105 90.0 - 110 114223672

Cyanide 0.506 0.500 mg/L 101 90.0 - 110 114223683

Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Cyanide 1279990 Duplicate 0.00974 0.00954 mg/L 2.07 20.0

Cyanide 1280475 Duplicate 0.00582 ND mg/L 4.37 20.0

ICV


Cyanide 0.210 0.200 mg/L 105 90.0 - 110 114223660

LCS

OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter

Cyanide 557048 0.198 0.200 mg/L 98.8 90.0 - 110 114223663

LCS Dup

Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter

Cyanide 557048 0.198 0.199 0.200 90.0 - 110 98.8 99.4 mg/L 0.504 20.0

Mat. Spike

FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter

Cyanide 1279990 0.114 0.00954 0.100 mg/L 104 90.0 - 110 114223667

Cyanide 1280475 0.109 ND 0.100 mg/L 103 90.0 - 110 114223670

EPA 420.4 1Liquid Aqueous 557249

Blank


Phenolics, Total Recoverable 557067 ND 0.00377 0.005 mg/L 114224445

CCV


Phenolics, Total Recoverable 0.197 0.200 mg/L 98.5 90.0 - 110 114224444

Phenolics, Total Recoverable 0.192 0.200 mg/L 96.0 90.0 - 110 114224453

Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Phenolics, Total Recoverable 1280241 Duplicate 0.0095 0.0113 mg/L 17.3 20.0


Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.17.799 www.ana-lab.com



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ICV


Phenolics, Total Recoverable 0.200 0.200 mg/L 100 90.0 - 110 114224443

LCS


Phenolics, Total Recoverable 557067 0.204 0.200 mg/L 102 90.0 - 110 114224446

LCS Dup


Phenolics, Total Recoverable 557067 0.204 0.198 0.200 90.0 - 110 102 99.0 mg/L 2.99 20.0

Mat. Spike

FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter

Phenolics, Total Recoverable 1280241 0.216 0.0113 0.200 mg/L 102 90.0 - 110 114224450

SM 3500-Cr B-2009Liquid Aqueous 557137

Blank


Hexavalent Chromium 557137 ND 1.74 3.00 ug/L 114221752

Hexavalent Chromium 557137 ND 1.74 3.00 ug/L 114221760

CCV


Hexavalent Chromium 85.0 80.0 ug/L 106 90.0 - 110 114221753

Hexavalent Chromium 85.0 80.0 ug/L 106 90.0 - 110 114221759

LCS


Hexavalent Chromium 557137 84.8 80.0 ug/L 106 85.0 - 115 114221754

LCS Dup


Hexavalent Chromium 557137 84.8 84.0 80.0 85.0 - 115 106 105 ug/L 0.948 15.0

MS

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Hexavalent Chromium 1280758 83.2 0 ND 80.0 70.0 - 130 104 ug/L 20.0

MSD


Hexavalent Chromium 1280758 83.2 83.0 ND 80.0 70.0 - 130 104 104 ug/L 0 20.0

EPA 200.8 5.4Liquid Aqueous 557158

Blank


Antimony 557089 ND 0.000399 0.001 mg/L 114222236

Arsenic 557089 ND 0.000193 0.0005 mg/L 114222236

Beryllium 557089 ND 0.00006050.0005 mg/L 114222236

Cadmium 557089 ND 0.000209 0.0005 mg/L 114222236

Chromium 557089 ND 0.000282 0.0005 mg/L 114222236

Copper 557089 ND 0.000425 0.001 mg/L 114222236

Lead 557089 ND 0.000227 0.0005 mg/L 114222236

Nickel 557089 0.000343 0.000264 0.001 mg/L 114222236

Selenium 557089 ND 0.000728 0.001 mg/L 114222236





Report Page 9 of 46

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Silver 557089 ND 0.00006280.0005 mg/L 114222236

Thallium 557089 ND 0.000174 0.0005 mg/L 114222236

Zinc 557089 0.0126 0.00123 0.005 mg/L * 114222236

CCV


Antimony 0.0503 0.05 mg/L 101 90.0 - 110 114222213

Antimony 0.0511 0.05 mg/L 102 90.0 - 110 114222226

Antimony 0.0503 0.05 mg/L 101 90.0 - 110 114222234

Antimony 0.0496 0.05 mg/L 99.2 90.0 - 110 114222242

Antimony 0.0498 0.05 mg/L 99.6 90.0 - 110 114222253

Antimony 0.0504 0.05 mg/L 101 90.0 - 110 114222262

Arsenic 0.0497 0.05 mg/L 99.4 90.0 - 110 114222213

Arsenic 0.0505 0.05 mg/L 101 90.0 - 110 114222226

Arsenic 0.0494 0.05 mg/L 98.8 90.0 - 110 114222234

Arsenic 0.0487 0.05 mg/L 97.4 90.0 - 110 114222242

Arsenic 0.0487 0.05 mg/L 97.4 90.0 - 110 114222253

Arsenic 0.0508 0.05 mg/L 102 90.0 - 110 114222262

Beryllium 0.0491 0.05 mg/L 98.2 90.0 - 110 114222213

Beryllium 0.047 0.05 mg/L 94.0 90.0 - 110 114222226

Beryllium 0.048 0.05 mg/L 96.0 90.0 - 110 114222234

Beryllium 0.0466 0.05 mg/L 93.2 90.0 - 110 114222242

Beryllium 0.0476 0.05 mg/L 95.2 90.0 - 110 114222253

Beryllium 0.046 0.05 mg/L 92.0 90.0 - 110 114222262

Cadmium 0.0501 0.05 mg/L 100 90.0 - 110 114222213

Cadmium 0.0503 0.05 mg/L 101 90.0 - 110 114222226

Cadmium 0.050 0.05 mg/L 100 90.0 - 110 114222234

Cadmium 0.0496 0.05 mg/L 99.2 90.0 - 110 114222242

Cadmium 0.0497 0.05 mg/L 99.4 90.0 - 110 114222253

Cadmium 0.0494 0.05 mg/L 98.8 90.0 - 110 114222262

Chromium 0.0498 0.05 mg/L 99.6 90.0 - 110 114222213

Chromium 0.0494 0.05 mg/L 98.8 90.0 - 110 114222226

Chromium 0.0486 0.05 mg/L 97.2 90.0 - 110 114222234

Chromium 0.0491 0.05 mg/L 98.2 90.0 - 110 114222242

Chromium 0.0491 0.05 mg/L 98.2 90.0 - 110 114222253

Chromium 0.0506 0.05 mg/L 101 90.0 - 110 114222262

Copper 0.0501 0.05 mg/L 100 90.0 - 110 114222213

Copper 0.0486 0.05 mg/L 97.2 90.0 - 110 114222226

Copper 0.0476 0.05 mg/L 95.2 90.0 - 110 114222234

Copper 0.0481 0.05 mg/L 96.2 90.0 - 110 114222242

Copper 0.0481 0.05 mg/L 96.2 90.0 - 110 114222253

Copper 0.0493 0.05 mg/L 98.6 90.0 - 110 114222262

Lead 0.0507 0.05 mg/L 101 90.0 - 110 114222213

Lead 0.0506 0.05 mg/L 101 90.0 - 110 114222226

Lead 0.0523 0.05 mg/L 105 90.0 - 110 114222234

Lead 0.0514 0.05 mg/L 103 90.0 - 110 114222242

Lead 0.0521 0.05 mg/L 104 90.0 - 110 114222253

Lead 0.0504 0.05 mg/L 101 90.0 - 110 114222262

Nickel 0.0495 0.05 mg/L 99.0 90.0 - 110 114222213

Nickel 0.0489 0.05 mg/L 97.8 90.0 - 110 114222226

Nickel 0.0475 0.05 mg/L 95.0 90.0 - 110 114222234





Report Page 10 of 46

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4






CCV


Nickel 0.0482 0.05 mg/L 96.4 90.0 - 110 114222242

Nickel 0.0478 0.05 mg/L 95.6 90.0 - 110 114222253

Nickel 0.0496 0.05 mg/L 99.2 90.0 - 110 114222262

Selenium 0.0503 0.05 mg/L 101 90.0 - 110 114222213

Selenium 0.0511 0.05 mg/L 102 90.0 - 110 114222226

Selenium 0.0513 0.05 mg/L 103 90.0 - 110 114222234

Selenium 0.0499 0.05 mg/L 99.8 90.0 - 110 114222242

Selenium 0.0493 0.05 mg/L 98.6 90.0 - 110 114222253

Selenium 0.0519 0.05 mg/L 104 90.0 - 110 114222262

Silver 0.0496 0.05 mg/L 99.2 90.0 - 110 114222213

Silver 0.0498 0.05 mg/L 99.6 90.0 - 110 114222226

Silver 0.0494 0.05 mg/L 98.8 90.0 - 110 114222234

Silver 0.049 0.05 mg/L 98.0 90.0 - 110 114222242

Silver 0.0492 0.05 mg/L 98.4 90.0 - 110 114222253

Silver 0.0489 0.05 mg/L 97.8 90.0 - 110 114222262

Thallium 0.0504 0.05 mg/L 101 90.0 - 110 114222213

Thallium 0.0501 0.05 mg/L 100 90.0 - 110 114222226

Thallium 0.0518 0.05 mg/L 104 90.0 - 110 114222234

Thallium 0.0504 0.05 mg/L 101 90.0 - 110 114222242

Thallium 0.051 0.05 mg/L 102 90.0 - 110 114222253

Thallium 0.0495 0.05 mg/L 99.0 90.0 - 110 114222262

ICV


Antimony 0.0513 0.05 mg/L 103 90.0 - 110 114222212

Arsenic 0.0502 0.05 mg/L 100 90.0 - 110 114222212

Beryllium 0.0505 0.05 mg/L 101 90.0 - 110 114222212

Cadmium 0.0515 0.05 mg/L 103 90.0 - 110 114222212

Chromium 0.0508 0.05 mg/L 102 90.0 - 110 114222212

Copper 0.0513 0.05 mg/L 103 90.0 - 110 114222212

Lead 0.0517 0.05 mg/L 103 90.0 - 110 114222212

Nickel 0.0507 0.05 mg/L 101 90.0 - 110 114222212

Selenium 0.0505 0.05 mg/L 101 90.0 - 110 114222212

Silver 0.0492 0.05 mg/L 98.4 90.0 - 110 114222212

Thallium 0.0524 0.05 mg/L 105 90.0 - 110 114222212

LCS


Antimony 557089 0.511 0.500 mg/L 102 85.0 - 115 114222237

Arsenic 557089 0.518 0.500 mg/L 104 85.0 - 115 114222237

Beryllium 557089 0.199 0.200 mg/L 99.3 85.0 - 115 114222237

Cadmium 557089 0.260 0.250 mg/L 104 85.0 - 115 114222237

Chromium 557089 0.513 0.500 mg/L 103 85.0 - 115 114222237

Copper 557089 0.494 0.500 mg/L 98.9 85.0 - 115 114222237

Lead 557089 0.536 0.500 mg/L 107 85.0 - 115 114222237

Nickel 557089 0.487 0.500 mg/L 97.3 85.0 - 115 114222237

Selenium 557089 0.532 0.500 mg/L 106 85.0 - 115 114222237

Silver 557089 0.102 0.100 mg/L 102 85.0 - 115 114222237

Thallium 557089 0.515 0.500 mg/L 103 85.0 - 115 114222237

Zinc 557089 0.501 0.500 mg/L 100 85.0 - 115 114222237






1

2

3

4






LCS Dup


Antimony 557089 0.511 0.508 0.500 85.0 - 115 102 102 mg/L 0.589 20.0

Arsenic 557089 0.518 0.514 0.500 85.0 - 115 104 103 mg/L 0.775 20.0

Beryllium 557089 0.199 0.200 0.200 85.0 - 115 99.3 99.8 mg/L 0.501 20.0

Cadmium 557089 0.260 0.264 0.250 85.0 - 115 104 105 mg/L 1.53 20.0

Chromium 557089 0.513 0.504 0.500 85.0 - 115 103 101 mg/L 1.77 20.0

Copper 557089 0.494 0.497 0.500 85.0 - 115 98.9 99.3 mg/L 0.605 20.0

Lead 557089 0.536 0.546 0.500 85.0 - 115 107 109 mg/L 1.85 20.0

Nickel 557089 0.487 0.489 0.500 85.0 - 115 97.3 97.7 mg/L 0.410 20.0

Selenium 557089 0.532 0.531 0.500 85.0 - 115 106 106 mg/L 0.188 20.0

Silver 557089 0.102 0.103 0.100 85.0 - 115 102 103 mg/L 0.976 20.0

Thallium 557089 0.515 0.526 0.500 85.0 - 115 103 105 mg/L 2.11 20.0

Zinc 557089 0.501 0.506 0.500 85.0 - 115 100 101 mg/L 0.993 20.0

LDR


Antimony 0.198 0.2 mg/L 99.0 90.0 - 110 114222214

Arsenic 9.52 10 mg/L 95.2 90.0 - 110 114222217

Beryllium 9.90 10 mg/L 99.0 90.0 - 110 114222217

Cadmium 9.59 10 mg/L 95.9 90.0 - 110 114222217

Chromium 9.26 10 mg/L 92.6 90.0 - 110 114222217

Copper 4.59 5 mg/L 91.8 90.0 - 110 114222216

Lead 9.68 10 mg/L 96.8 90.0 - 110 114222217

Nickel 4.52 5 mg/L 90.4 90.0 - 110 114222216

Selenium 10.2 10 mg/L 102 90.0 - 110 114222217

Silver 9.49 10 mg/L 94.9 90.0 - 110 114222217

Thallium 9.63 10 mg/L 96.3 90.0 - 110 114222217

MS


Antimony 1280443 0.516 0 0.00286 0.500 70.0 - 130 103 mg/L 20.0

Arsenic 1280443 0.522 0 0.00366 0.500 70.0 - 130 104 mg/L 20.0

Beryllium 1280443 0.196 0 0.000111 0.200 70.0 - 130 97.9 mg/L 20.0

Cadmium 1280443 0.258 0 ND 0.250 70.0 - 130 103 mg/L 20.0

Chromium 1280443 0.508 0 0.000479 0.500 70.0 - 130 102 mg/L 20.0

Copper 1280443 0.490 0 0.00307 0.500 70.0 - 130 97.4 mg/L 20.0

Lead 1280443 0.522 0 0.000493 0.500 70.0 - 130 104 mg/L 20.0

Nickel 1280443 0.482 0 0.00191 0.500 70.0 - 130 96.0 mg/L 20.0

Selenium 1280443 0.528 0 0.00244 0.500 70.0 - 130 105 mg/L 20.0

Silver 1280443 0.101 0 0.0000979 0.100 70.0 - 130 101 mg/L 20.0

Thallium 1280443 0.505 0 0.000804 0.500 70.0 - 130 101 mg/L 20.0

Zinc 1280443 0.499 0 0.00914 0.500 70.0 - 130 98.0 mg/L 20.0

Antimony 1280492 0.514 0 0.00164 0.500 70.0 - 130 102 mg/L 20.0

Arsenic 1280492 0.522 0 0.0013 0.500 70.0 - 130 104 mg/L 20.0

Beryllium 1280492 0.192 0 ND 0.200 70.0 - 130 96.0 mg/L 20.0

Cadmium 1280492 0.256 0 ND 0.250 70.0 - 130 102 mg/L 20.0

Chromium 1280492 0.505 0 0.000339 0.500 70.0 - 130 101 mg/L 20.0

Copper 1280492 0.532 0 0.0482 0.500 70.0 - 130 96.8 mg/L 20.0

Lead 1280492 0.516 0 0.000707 0.500 70.0 - 130 103 mg/L 20.0

Nickel 1280492 0.481 0 0.00226 0.500 70.0 - 130 95.7 mg/L 20.0

Selenium 1280492 0.526 0 ND 0.500 70.0 - 130 105 mg/L 20.0

Silver 1280492 0.0988 0 0.000122 0.100 70.0 - 130 98.7 mg/L 20.0






1

2

3

4






MS


Thallium 1280492 0.487 0 ND 0.500 70.0 - 130 97.4 mg/L 20.0

Zinc 1280492 0.497 0 0.0117 0.500 70.0 - 130 97.1 mg/L 20.0

MSD


Antimony 1280443 0.516 0.521 0.00286 0.500 70.0 - 130 103 104 mg/L 0.966 20.0

Arsenic 1280443 0.522 0.518 0.00366 0.500 70.0 - 130 104 103 mg/L 0.966 20.0

Beryllium 1280443 0.196 0.197 0.000111 0.200 70.0 - 130 97.9 98.4 mg/L 0.509 20.0

Cadmium 1280443 0.258 0.256 ND 0.250 70.0 - 130 103 102 mg/L 0.976 20.0

Chromium 1280443 0.508 0.499 0.000479 0.500 70.0 - 130 102 99.7 mg/L 2.28 20.0

Copper 1280443 0.490 0.483 0.00307 0.500 70.0 - 130 97.4 96.0 mg/L 1.45 20.0

Lead 1280443 0.522 0.525 0.000493 0.500 70.0 - 130 104 105 mg/L 0.957 20.0

Nickel 1280443 0.482 0.475 0.00191 0.500 70.0 - 130 96.0 94.6 mg/L 1.47 20.0

Selenium 1280443 0.528 0.524 0.00244 0.500 70.0 - 130 105 104 mg/L 0.957 20.0

Silver 1280443 0.101 0.100 0.0000979 0.100 70.0 - 130 101 99.9 mg/L 1.10 20.0

Thallium 1280443 0.505 0.508 0.000804 0.500 70.0 - 130 101 101 mg/L 0 20.0

Zinc 1280443 0.499 0.492 0.00914 0.500 70.0 - 130 98.0 96.6 mg/L 1.44 20.0

Antimony 1280492 0.514 0.515 0.00164 0.500 70.0 - 130 102 103 mg/L 0.976 20.0

Arsenic 1280492 0.522 0.528 0.0013 0.500 70.0 - 130 104 105 mg/L 0.957 20.0

Beryllium 1280492 0.192 0.193 ND 0.200 70.0 - 130 96.0 96.5 mg/L 0.519 20.0

Cadmium 1280492 0.256 0.255 ND 0.250 70.0 - 130 102 102 mg/L 0 20.0

Chromium 1280492 0.505 0.511 0.000339 0.500 70.0 - 130 101 102 mg/L 0.985 20.0

Copper 1280492 0.532 0.533 0.0482 0.500 70.0 - 130 96.8 97.0 mg/L 0.206 20.0

Lead 1280492 0.516 0.519 0.000707 0.500 70.0 - 130 103 104 mg/L 0.966 20.0

Nickel 1280492 0.481 0.482 0.00226 0.500 70.0 - 130 95.7 95.9 mg/L 0.209 20.0

Selenium 1280492 0.526 0.532 ND 0.500 70.0 - 130 105 106 mg/L 0.948 20.0

Silver 1280492 0.0988 0.0988 0.000122 0.100 70.0 - 130 98.7 98.7 mg/L 0 20.0

Thallium 1280492 0.487 0.487 ND 0.500 70.0 - 130 97.4 97.4 mg/L 0 20.0

Zinc 1280492 0.497 0.497 0.0117 0.500 70.0 - 130 97.1 97.1 mg/L 0 20.0

EPA 245.1 3Liquid Aqueous 557243

Blank


Mercury 557069 ND 0.0684 0.100 ug/L 114224329

CCV


Mercury 5.12 5.000 ug/L 102 90.0 - 110 114224325

Mercury 5.10 5.000 ug/L 102 90.0 - 110 114224333

Mercury 5.12 5.000 ug/L 102 90.0 - 110 114224340

ICL


Mercury 19.4 20.00 ug/L 97.0 90.0 - 110 114224320

ICV


Mercury 5.10 5.000 ug/L 102 90.0 - 110 114224319

LCS


Mercury 557069 4.86 5.00 ug/L 97.2 85.0 - 115 114224330






1

2

3

4






LCS Dup


Mercury 557069 4.86 4.85 5.00 85.0 - 115 97.2 97.0 ug/L 0.206 20.0

MS


Mercury 1280758 9.90 0 0.240 10.0 70.0 - 130 96.6 ug/L 14.0

MSD


Mercury 1280758 9.90 9.76 0.240 10.0 70.0 - 130 96.6 95.2 ug/L 1.46 14.0

EPA 200.8 5.4Liquid Aqueous 557309

Blank


Zinc 557089 0.00166 0.00123 0.005 mg/L 114225505

CCV


Zinc 0.0498 0.05 mg/L 99.6 90.0 - 110 114225502

Zinc 0.0496 0.05 mg/L 99.2 90.0 - 110 114225513

ICV


Zinc 0.0506 0.05 mg/L 101 90.0 - 110 114225501

LCS


Zinc 557089 0.507 0.500 mg/L 101 85.0 - 115 114225506

LCS Dup


Zinc 557089 0.507 0.509 0.500 85.0 - 115 101 102 mg/L 0.394 20.0

LDR


Zinc 9.35 10 mg/L 93.5 90.0 - 110 114225504

MS


Zinc 1280492 0.501 0 0.0114 0.500 70.0 - 130 97.9 mg/L 20.0

MSD


Zinc 1280492 0.501 0.502 0.0114 0.500 70.0 - 130 97.9 98.1 mg/L 0.204 20.0

EPA Method 625Liquid Aqueous 557270

Blank


1,2,4-Trichlorobenzene 555103 ND 0.941 1.00 ug/L 114234323

1,2-Dichlorobenzene 555103 ND 1.04 5.00 ug/L 114234323

1,2-DPH (as azobenzene) 555103 ND 0.238 1.00 ug/L 114234323



2,4,6-Trichlorophenol 555103 ND 1.24 2.00 ug/L 114234323

2,4-Dichlorophenol 555103 ND 0.222 1.00 ug/L 114234323






1

2

3

4






Blank


2,4-Dimethylphenol 555103 ND 0.536 1.00 ug/L 114234323

2,4-Dinitrophenol 555103 ND 1.34 2.00 ug/L 114234323

2,4-Dinitrotoluene 555103 ND 1.53 2.00 ug/L 114234323

2,6-Dinitrotoluene 555103 ND 1.29 2.00 ug/L 114234323

2-Chloronaphthalene 555103 ND 0.150 1.00 ug/L 114234323

2-Chlorophenol 555103 ND 0.275 1.00 ug/L 114234323

2-Nitrophenol 555103 ND 0.554 1.00 ug/L 114234323

3,3'-Dichlorobenzidine 555103 ND 1.39 2.00 ug/L 114234323

4,6-Dinitro-2-methylphenol 555103 ND 1.15 2.00 ug/L 114234323

4-Bromophenyl phenyl ether 555103 ND 0.772 1.00 ug/L 114234323

4-Chlorophenyl phenyl ethe 555103 ND 0.202 1.00 ug/L 114234323

4-Nitrophenol 555103 ND 0.789 1.00 ug/L 114234323

Acenaphthene 555103 ND 0.177 1.00 ug/L 114234323

Acenaphthylene 555103 ND 0.240 1.00 ug/L 114234323

Anthracene 555103 ND 0.241 1.00 ug/L 114234323

Benzidine 555103 ND 1.40 1.50 ug/L 114234323

Benzo(a)anthracene 555103 ND 0.225 1.00 ug/L 114234323

Benzo(a)pyrene 555103 ND 0.900 1.00 ug/L 114234323

Benzo(b)fluoranthene 555103 ND 0.547 1.00 ug/L 114234323

Benzo(ghi)perylene 555103 ND 0.881 1.00 ug/L 114234323

Benzo(k)fluoranthene 555103 ND 0.252 1.00 ug/L 114234323

Benzyl Butyl phthalate 555103 ND 0.204 1.00 ug/L 114234323

Bis(2-chloroethoxy)methane 555103 ND 0.277 1.00 ug/L 114234323

Bis(2-chloroethyl)ether 555103 ND 0.348 1.00 ug/L 114234323

Bis(2-chloroisopropyl)ether 555103 ND 0.738 1.00 ug/L 114234323

Bis(2-ethylhexyl)phthalate 555103 ND 1.12 1.12 ug/L 114234323

Chrysene

(Benzo(a)phenanthrene)

555103 ND 0.289 1.00 ug/L 114234323

Dibenz(a,h)anthracene 555103 ND 0.689 1.00 ug/L 114234323

Diethyl phthalate 555103 ND 0.253 1.00 ug/L 114234323

Dimethyl phthalate 555103 ND 0.540 1.00 ug/L 114234323

Di-n-butylphthalate 555103 ND 0.978 1.00 ug/L 114234323

Di-n-octylphthalate 555103 ND 1.92 2.00 ug/L 114234323

Fluoranthene(Benzo(j,k)fluor

ene)

555103 ND 0.318 1.00 ug/L 114234323

Fluorene 555103 ND 0.275 1.00 ug/L 114234323

Hexachlorobenzene 555103 ND 0.871 1.00 ug/L 114234323

Hexachlorobutadiene 555103 ND 1.03 1.03 ug/L 114234323

Hexachlorocyclopentadiene 555103 ND 0.536 1.00 ug/L 114234323

Hexachloroethane 555103 ND 1.05 2.00 ug/L 114234323

Indeno(1,2,3-cd)pyrene 555103 ND 0.596 1.00 ug/L 114234323

Isophorone 555103 ND 0.429 1.00 ug/L 114234323

Naphthalene 555103 ND 0.225 1.00 ug/L 114234323

Nitrobenzene 555103 ND 0.271 1.00 ug/L 114234323

N-Nitrosodimethylamine 555103 ND 0.542 1.00 ug/L 114234323

N-Nitrosodi-n-propylamine 555103 ND 0.425 1.00 ug/L 114234323

N-Nitrosodiphenylamine (as

DPA

555103 ND 0.404 1.00 ug/L 114234323

p-Chloro-m-Cresol

(4-Chloro-3-me

555103 ND 0.588 1.00 ug/L 114234323

Pentachlorophenol 555103 ND 0.960 10.0 ug/L 114234323

Phenanthrene 555103 ND 0.269 1.00 ug/L 114234323






1

2

3

4






Blank


Phenol 555103 ND 0.332 1.00 ug/L 114234323

Pyrene 555103 ND 0.291 1.00 ug/L 114234323

CCV


1,2,4-Trichlorobenzene 51600 50000 ug/L 103 80.0 - 120 114224822

1,2-Dichlorobenzene 60200 50000 ug/L 120 80.0 - 120 114224822

1,2-DPH (as azobenzene) 49800 50000 ug/L 99.6 80.0 - 120 114224822

1,3-Dichlorobenzene 46100 50000 ug/L 92.2 80.0 - 120 114224822

1,4-Dichlorobenzene 48300 50000 ug/L 96.6 80.0 - 120 114224822

2,4,6-Trichlorophenol 50500 50000 ug/L 101 80.0 - 120 114224822

2,4-Dichlorophenol 48700 50000 ug/L 97.4 80.0 - 120 114224822

2,4-Dimethylphenol 43800 50000 ug/L 87.6 80.0 - 120 114224822

2,4-Dinitrophenol 53300 50000 ug/L 107 80.0 - 120 114224822

2,4-Dinitrotoluene 51600 50000 ug/L 103 80.0 - 120 114224822

2,6-Dinitrotoluene 44700 50000 ug/L 89.4 80.0 - 120 114224822

2-Chloronaphthalene 45200 50000 ug/L 90.4 80.0 - 120 114224822

2-Chlorophenol 46000 50000 ug/L 92.0 80.0 - 120 114224822

2-Nitrophenol 48700 50000 ug/L 97.4 80.0 - 120 114224822

3,3'-Dichlorobenzidine 53700 50000 ug/L 107 80.0 - 120 114224822

4,6-Dinitro-2-methylphenol 60200 50000 ug/L 120 80.0 - 120 114224822

4-Bromophenyl phenyl ether 51600 50000 ug/L 103 80.0 - 120 114224822

4-Chlorophenyl phenyl ethe 66000 50000 ug/L 132 80.0 - 120 * 114224822

4-Nitrophenol 62800 50000 ug/L 126 80.0 - 120 * 114224822

Acenaphthene 47100 50000 ug/L 94.2 80.0 - 120 114224822

Acenaphthylene 43800 50000 ug/L 87.6 80.0 - 120 114224822

Anthracene 56100 50000 ug/L 112 80.0 - 120 114224822

Benzidine 41300 50000 ug/L 82.6 80.0 - 120 114224822

Benzo(a)anthracene 48400 50000 ug/L 96.8 80.0 - 120 114224822

Benzo(a)pyrene 51300 50000 ug/L 103 80.0 - 120 114224822

Benzo(b)fluoranthene 56800 50000 ug/L 114 80.0 - 120 114224822

Benzo(ghi)perylene 48400 50000 ug/L 96.8 80.0 - 120 114224822

Benzo(k)fluoranthene 46300 50000 ug/L 92.6 80.0 - 120 114224822

Benzyl Butyl phthalate 45200 50000 ug/L 90.4 80.0 - 120 114224822

Bis(2-chloroethoxy)methane 46900 50000 ug/L 93.8 80.0 - 120 114224822

Bis(2-chloroethyl)ether 45300 50000 ug/L 90.6 80.0 - 120 114224822

Bis(2-chloroisopropyl)ether 48400 50000 ug/L 96.8 80.0 - 120 114224822

Bis(2-ethylhexyl)phthalate 44500 50000 ug/L 89.0 80.0 - 120 114224822

Chrysene


45100 50000 ug/L 90.2 80.0 - 120 114224822

Dibenz(a,h)anthracene 53100 50000 ug/L 106 80.0 - 120 114224822

Diethyl phthalate 50500 50000 ug/L 101 80.0 - 120 114224822

Dimethyl phthalate 47100 50000 ug/L 94.2 80.0 - 120 114224822

Di-n-butylphthalate 52700 50000 ug/L 105 80.0 - 120 114224822

Di-n-octylphthalate 43000 50000 ug/L 86.0 80.0 - 120 114224822


ene)

45500 50000 ug/L 91.0 80.0 - 120 114224822

Fluorene 60900 50000 ug/L 122 80.0 - 120 * 114224822

Hexachlorobenzene 52800 50000 ug/L 106 80.0 - 120 114224822

Hexachlorobutadiene 57600 50000 ug/L 115 80.0 - 120 114224822

Hexachlorocyclopentadiene 59600 50000 ug/L 119 80.0 - 120 114224822






1

2

3

4






CCV


Hexachloroethane 56500 50000 ug/L 113 80.0 - 120 114224822

Indeno(1,2,3-cd)pyrene 48500 50000 ug/L 97.0 80.0 - 120 114224822

Isophorone 48800 50000 ug/L 97.6 80.0 - 120 114224822

Naphthalene 55700 50000 ug/L 111 80.0 - 120 114224822

Nitrobenzene 48000 50000 ug/L 96.0 80.0 - 120 114224822

N-Nitrosodimethylamine 56900 50000 ug/L 114 80.0 - 120 114224822

N-Nitrosodi-n-propylamine 63600 50000 ug/L 127 80.0 - 120 * 114224822


DPA

57600 50000 ug/L 115 80.0 - 120 114224822

p-Chloro-m-Cresol

(4-Chloro-3-me

53500 50000 ug/L 107 80.0 - 120 114224822

Pentachlorophenol 59600 50000 ug/L 119 80.0 - 120 114224822

Phenanthrene 49800 50000 ug/L 99.6 80.0 - 120 114224822

Phenol 58800 50000 ug/L 118 80.0 - 120 114224822

Pyrene 49700 50000 ug/L 99.4 80.0 - 120 114224822

DFTPP

FileOutLimits%%ReadingRefMassParameter

DFTPP Mass 127 131163 198 21102 54.9 40.0 - 60.0 114224821

DFTPP Mass 197 131163 198 0 0.0 0 - 1.00 114224821

DFTPP Mass 198 131163 198 38444 100.0 100 - 100 114224821

DFTPP Mass 199 131163 198 2662 6.9 5.00 - 9.00 114224821

DFTPP Mass 275 131163 198 8485 22.1 10.0 - 30.0 114224821

DFTPP Mass 365 131163 198 1012 2.6 1.00 - 100 114224821

DFTPP Mass 441 131163 443 4456 80.9 0 - 100 114224821

DFTPP Mass 442 131163 198 28113 73.1 40.0 - 100 114224821

DFTPP Mass 443 131163 442 5511 19.6 17.0 - 23.0 114224821

DFTPP Mass 51 131163 198 12860 33.5 30.0 - 60.0 114224821

DFTPP Mass 68 131163 69.0 0 0.0 0 - 2.00 114224821

DFTPP Mass 69 131163 198 17434 45.3 0 - 100 114224821

DFTPP Mass 70 131163 69.0 0 0.0 0 - 2.00 114224821

LCS


1,2,4-Trichlorobenzene 555103 18.5 25.0 ug/L 74.1 22.0 - 147 114234324

1,2-Dichlorobenzene 555103 18.9 25.0 ug/L 75.7 32.0 - 129 114234324

1,2-DPH (as azobenzene) 555103 22.0 25.0 ug/L 88.1 0.100 - 130 114234324



2,4,6-Trichlorophenol 555103 20.5 25.0 ug/L 82.0 37.0 - 144 114234324

2,4-Dichlorophenol 555103 17.6 25.0 ug/L 70.2 39.0 - 135 114234324

2,4-Dimethylphenol 555103 7.61 25.0 ug/L 30.4 32.0 - 119 114234324 *

2,4-Dinitrophenol 555103 14.6 25.0 ug/L 58.3 0.100 - 191 114234324

2,4-Dinitrotoluene 555103 19.2 25.0 ug/L 76.6 39.0 - 139 114234324

2,6-Dinitrotoluene 555103 18.8 25.0 ug/L 75.4 50.0 - 158 114234324

2-Chloronaphthalene 555103 18.0 25.0 ug/L 72.0 60.0 - 118 114234324

2-Chlorophenol 555103 17.4 25.0 ug/L 69.6 23.0 - 134 114234324

2-Nitrophenol 555103 17.7 25.0 ug/L 70.9 29.0 - 182 114234324

3,3'-Dichlorobenzidine 555103 17.2 25.0 ug/L 68.8 0.100 - 262 114234324

4,6-Dinitro-2-methylphenol 555103 23.6 25.0 ug/L 94.6 0.100 - 191 114234324

4-Bromophenyl phenyl ether 555103 22.7 25.0 ug/L 90.8 53.0 - 127 114234324

4-Chlorophenyl phenyl ethe 555103 24.5 25.0 ug/L 98.1 25.0 - 158 114234324






1

2

3

4






LCS


4-Nitrophenol 555103 11.9 25.0 ug/L 47.8 0.100 - 132 114234324

Acenaphthene 555103 19.3 25.0 ug/L 77.3 47.0 - 145 114234324

Acenaphthylene 555103 16.5 25.0 ug/L 66.0 33.0 - 145 114234324

Anthracene 555103 21.6 25.0 ug/L 86.2 27.0 - 133 114234324

Benzidine 555103 4.71 25.0 ug/L 18.8 0.100 - 130 114234324

Benzo(a)anthracene 555103 20.7 25.0 ug/L 82.8 33.0 - 143 114234324

Benzo(a)pyrene 555103 21.3 25.0 ug/L 85.2 17.0 - 163 114234324

Benzo(b)fluoranthene 555103 20.6 25.0 ug/L 82.4 24.0 - 159 114234324

Benzo(ghi)perylene 555103 30.4 25.0 ug/L 122 0.100 - 219 114234324

Benzo(k)fluoranthene 555103 20.4 25.0 ug/L 81.8 11.0 - 162 114234324

Benzyl Butyl phthalate 555103 21.6 25.0 ug/L 86.3 0.100 - 152 114234324

Bis(2-chloroethoxy)methane 555103 21.0 25.0 ug/L 84.0 33.0 - 184 114234324

Bis(2-chloroethyl)ether 555103 23.5 25.0 ug/L 94.0 33.0 - 184 114234324

Bis(2-chloroisopropyl)ether 555103 16.8 25.0 ug/L 67.2 36.0 - 166 114234324

Bis(2-ethylhexyl)phthalate 555103 23.6 25.0 ug/L 94.2 8.00 - 158 114234324

Chrysene


555103 20.7 25.0 ug/L 82.6 17.0 - 168 114234324

Dibenz(a,h)anthracene 555103 27.6 25.0 ug/L 110 0.100 - 227 114234324

Diethyl phthalate 555103 20.1 25.0 ug/L 80.4 0.100 - 114 114234324

Dimethyl phthalate 555103 18.1 25.0 ug/L 72.4 0.100 - 112 114234324

Di-n-butylphthalate 555103 22.0 25.0 ug/L 88.2 1.00 - 118 114234324

Di-n-octylphthalate 555103 18.2 25.0 ug/L 72.8 4.00 - 146 114234324


ene)

555103 18.5 25.0 ug/L 74.1 26.0 - 137 114234324

Fluorene 555103 21.6 25.0 ug/L 86.5 59.0 - 121 114234324

Hexachlorobenzene 555103 23.5 25.0 ug/L 94.1 0.100 - 152 114234324

Hexachlorobutadiene 555103 19.3 25.0 ug/L 77.2 24.0 - 116 114234324

Hexachlorocyclopentadiene 555103 12.9 25.0 ug/L 51.5 0.100 - 130 114234324

Hexachloroethane 555103 18.2 25.0 ug/L 72.9 40.0 - 113 114234324

Indeno(1,2,3-cd)pyrene 555103 27.6 25.0 ug/L 110 0.100 - 171 114234324

Isophorone 555103 20.7 25.0 ug/L 82.7 21.0 - 196 114234324

Naphthalene 555103 21.2 25.0 ug/L 84.6 21.0 - 133 114234324

Nitrobenzene 555103 21.9 25.0 ug/L 87.6 35.0 - 180 114234324

N-Nitrosodimethylamine 555103 19.6 25.0 ug/L 78.4 0.100 - 130 114234324

N-Nitrosodi-n-propylamine 555103 21.4 25.0 ug/L 85.5 0.100 - 230 114234324


DPA

555103 23.4 25.0 ug/L 93.6 0.100 - 130 114234324

p-Chloro-m-Cresol

(4-Chloro-3-me

555103 19.3 25.0 ug/L 77.3 22.0 - 147 114234324

Pentachlorophenol 555103 22.6 25.0 ug/L 90.4 5.00 - 112 114234324

Phenanthrene 555103 21.0 25.0 ug/L 84.1 54.0 - 120 114234324

Phenol 555103 10.6 25.0 ug/L 42.2 5.00 - 112 114234324

Pyrene 555103 21.3 25.0 ug/L 85.3 52.0 - 115 114234324

Surrogate

FileLimits%Recover%UnitsKnownReadingTypeSampleParameter

2,4,6-Tribromophenol 132690 CCV 66300 100000 ug/L 66.3 10.0 - 150 114224822

2-Fluorobiphenyl-SURR 132690 CCV 54900 50000 ug/L 110 30.0 - 150 114224822

2-Fluorophenol-SURR 132690 CCV 44800 100000 ug/L 44.8 10.0 - 150 114224822

4-Terphenyl-d14-SURR 132690 CCV 51300 50000 ug/L 103 30.0 - 150 114224822

Nitrobenzene-d5-SURR 132690 CCV 44200 50000 ug/L 88.4 30.0 - 150 114224822

Phenol-d6-SURR 132690 CCV 62000 100000 ug/L 62.0 10.0 - 150 114224822






1

2

3

4






Surrogate


2,4,6-Tribromophenol 555103 Blank 50.8 100 ug/L 50.8 10.0 - 150 114234323

2,4,6-Tribromophenol 555103 LCS 76.2 100 ug/L 76.2 10.0 - 150 114234324

2,4,6-Tribromophenol 555103 LCS Dup 84.8 100 ug/L 84.8 10.0 - 150 114234325

2-Fluorobiphenyl-SURR 555103 Blank 22500 50000 ug/L 45.0 30.0 - 150 114234323

2-Fluorobiphenyl-SURR 555103 LCS 41300 50000 ug/L 82.6 30.0 - 150 114234324

2-Fluorobiphenyl-SURR 555103 LCS Dup 42300 50000 ug/L 84.6 30.0 - 150 114234325

2-Fluorophenol-SURR 555103 Blank 28300 100000 ug/L 28.3 10.0 - 150 114234323

2-Fluorophenol-SURR 555103 LCS 46900 100000 ug/L 46.9 10.0 - 150 114234324

2-Fluorophenol-SURR 555103 LCS Dup 42800 100000 ug/L 42.8 10.0 - 150 114234325

4-Terphenyl-d14-SURR 555103 Blank 24500 50000 ug/L 49.0 30.0 - 150 114234323

4-Terphenyl-d14-SURR 555103 LCS 40700 50000 ug/L 81.4 30.0 - 150 114234324

4-Terphenyl-d14-SURR 555103 LCS Dup 39400 50000 ug/L 78.8 30.0 - 150 114234325

Nitrobenzene-d5-SURR 555103 Blank 27200 50000 ug/L 54.4 30.0 - 150 114234323

Nitrobenzene-d5-SURR 555103 LCS 34900 50000 ug/L 69.8 30.0 - 150 114234324

Nitrobenzene-d5-SURR 555103 LCS Dup 33600 50000 ug/L 67.2 30.0 - 150 114234325

Phenol-d6-SURR 555103 Blank 21800 100000 ug/L 21.8 10.0 - 150 114234323

Phenol-d6-SURR 555103 LCS 41200 100000 ug/L 41.2 10.0 - 150 114234324

Phenol-d6-SURR 555103 LCS Dup 36800 100000 ug/L 36.8 10.0 - 150 114234325

2,4,6-Tribromophenol 1280758 UNKNOWN77.2 101 ug/L 76.4 10.0 - 150 114224823

2-Fluorobiphenyl-SURR 1280758 UNKNOWN37.3 50.7 ug/L 73.6 30.0 - 150 114224823

2-Fluorophenol-SURR 1280758 UNKNOWN33.5 101 ug/L 33.2 10.0 - 150 114224823

4-Terphenyl-d14-SURR 1280758 UNKNOWN44.9 50.7 ug/L 88.6 30.0 - 150 114224823

Nitrobenzene-d5-SURR 1280758 UNKNOWN31.5 50.7 ug/L 62.1 30.0 - 150 114224823

Phenol-d6-SURR 1280758 UNKNOWN29.3 101 ug/L 29.0 10.0 - 150 114224823


BFB

FileOutLimits%%ReadingRefMassSampleParameter

BFB Mass 173 557275 174 48 0.5 0 - 2.00 114224858

BFB Mass 174 557275 95.0 10326 90.8 50.0 - 100 114224858

BFB Mass 175 557275 174 726 7.0 5.00 - 9.00 114224858

BFB Mass 176 557275 174 10058 97.4 95.0 - 101 114224858

BFB Mass 177 557275 176 669 6.7 5.00 - 9.00 114224858

BFB Mass 50 557275 95.0 2047 18.0 15.0 - 40.0 114224858

BFB Mass 75 557275 95.0 5336 46.9 30.0 - 60.0 114224858

BFB Mass 95 557275 95.0 11367 100.0 100 - 100 114224858

BFB Mass 96 557275 95.0 807 7.1 5.00 - 9.00 114224858

Blank


1,1,1-Trichloroethane 557275 ND 0.265 1.00 ug/L 114224861

1,1,2,2-Tetrachloroethane 557275 ND 0.270 1.00 ug/L 114224861


1,1-Dichloroethane 557275 ND 0.496 1.00 ug/L 114224861

1,1-Dichloroethylene 557275 ND 0.404 1.00 ug/L 114224861


1,2-Dichloropropane 557275 ND 0.415 1.00 ug/L 114224861

2-Chloroethylvinyl ether 557275 ND 0.423 1.00 ug/L 114224861

Benzene 557275 ND 0.187 1.00 ug/L 114224861

Bromodichloromethane 557275 ND 0.307 1.00 ug/L 114224861

Bromoform 557275 ND 0.288 1.00 ug/L 114224861






1

2

3

4






Blank


Bromomethane (Methyl

Bromi

557275 ND 0.554 1.00 ug/L 114224861

Carbon Tetrachloride 557275 ND 0.459 1.00 ug/L 114224861

Chlorobenzene 557275 ND 0.226 1.00 ug/L 114224861

Chloroethane 557275 ND 0.396 1.00 ug/L 114224861

Chloroform 557275 ND 0.211 1.00 ug/L 114224861

Chloromethane 557275 ND 0.391 1.00 ug/L 114224861

cis-1,3-Dichloropropene 557275 ND 0.488 1.00 ug/L 114224861

Dibromochloromethane 557275 ND 0.185 1.00 ug/L 114224861

Ethylbenzene 557275 ND 0.180 1.00 ug/L 114224861

Methylene chloride 557275 ND 0.570 1.00 ug/L 114224861

Tetrachloroethylene 557275 ND 0.391 1.00 ug/L 114224861

Toluene 557275 ND 0.314 1.00 ug/L 114224861

trans-1,2-Dichloroethene 557275 ND 0.518 1.00 ug/L 114224861

trans-1,3-Dichloropropene 557275 ND 0.223 1.00 ug/L 114224861

Trichloroethylene 557275 ND 0.562 1.00 ug/L 114224861

Vinyl chloride 557275 ND 0.228 1.00 ug/L 114224861

CCV


1,1,1-Trichloroethane 19.4 20.0 ug/L 97.0 70.0 - 130 114224857

1,1,2,2-Tetrachloroethane 22.1 20.0 ug/L 110 70.0 - 130 114224857

1,1,2-Trichloroethane 20.3 20.0 ug/L 102 70.0 - 130 114224857

1,1-Dichloroethane 21.0 20.0 ug/L 105 70.0 - 130 114224857

1,1-Dichloroethylene 20.2 20.0 ug/L 101 70.0 - 130 114224857

1,2-Dichloroethane 18.7 20.0 ug/L 93.5 70.0 - 130 114224857

1,2-Dichloropropane 20.3 20.0 ug/L 102 70.0 - 130 114224857

Benzene 20.7 20.0 ug/L 104 70.0 - 130 114224857

Bromodichloromethane 18.3 20.0 ug/L 91.5 70.0 - 130 114224857

Bromoform 15.1 20.0 ug/L 75.5 70.0 - 130 114224857


Bromi

18.3 20.0 ug/L 91.5 70.0 - 130 114224857

Carbon Tetrachloride 18.3 20.0 ug/L 91.5 70.0 - 130 114224857

Chlorobenzene 18.8 20.0 ug/L 94.0 70.0 - 130 114224857

Chloroethane 21.0 20.0 ug/L 105 70.0 - 130 114224857

Chloroform 20.5 20.0 ug/L 102 70.0 - 130 114224857

Chloromethane 22.3 20.0 ug/L 112 70.0 - 130 114224857

cis-1,3-Dichloropropene 17.5 20.0 ug/L 87.5 70.0 - 130 114224857

Dibromochloromethane 15.6 20.0 ug/L 78.0 70.0 - 130 114224857

Ethylbenzene 19.2 20.0 ug/L 96.0 70.0 - 130 114224857

Methylene chloride 21.1 20.0 ug/L 106 70.0 - 130 114224857

Tetrachloroethylene 20.3 20.0 ug/L 102 70.0 - 130 114224857

Toluene 19.9 20.0 ug/L 99.5 70.0 - 130 114224857

trans-1,2-Dichloroethene 20.8 20.0 ug/L 104 70.0 - 130 114224857

trans-1,3-Dichloropropene 17.5 20.0 ug/L 87.5 70.0 - 130 114224857

Trichloroethylene 19.8 20.0 ug/L 99.0 70.0 - 130 114224857

Vinyl chloride 22.7 20.0 ug/L 114 70.0 - 130 114224857

IS Areas

PrepSetFileOutHighLowCCVISMReadingTypeSampleParameter

1,4-DichlorobenzeneD4

(ISTD)

557275 LCS 140400 142600 71300 213900 114224859 557275






1

2

3

4






IS Areas



(ISTD)

557275 LCS Dup 139900 142600 71300 213900 114224860 557275


(ISTD)

557275 Blank 129700 142600 71300 213900 114224861 557275

ChlorobenzeneD5 (ISTD) 557275 LCS 234200 244100 122100 366200 114224859 557275

ChlorobenzeneD5 (ISTD) 557275 LCS Dup 236700 244100 122100 366200 114224860 557275

ChlorobenzeneD5 (ISTD) 557275 Blank 235300 244100 122100 366200 114224861 557275


(ISTD)

1280758 UNKNOWN123100 142600 71300 213900 114224862 1280758

ChlorobenzeneD5 (ISTD) 1280758 UNKNOWN220800 244100 122100 366200 114224862 1280758

IS RetTime



(ISTD)

557275 LCS 12.01 12.01 11.95 12.07 114224859 557275


(ISTD)

557275 LCS Dup 12.01 12.01 11.95 12.07 114224860 557275


(ISTD)

557275 Blank 12.01 12.01 11.95 12.07 114224861 557275

ChlorobenzeneD5 (ISTD) 557275 LCS 9.623 9.623 9.563 9.683 114224859 557275

ChlorobenzeneD5 (ISTD) 557275 LCS Dup 9.623 9.623 9.563 9.683 114224860 557275

ChlorobenzeneD5 (ISTD) 557275 Blank 9.623 9.623 9.563 9.683 114224861 557275


(ISTD)

1280758 UNKNOWN12.01 12.01 11.95 12.07 114224862 1280758

ChlorobenzeneD5 (ISTD) 1280758 UNKNOWN9.623 9.623 9.563 9.683 114224862 1280758

LCS


1,1,1-Trichloroethane 557275 19.5 20.0 ug/L 97.4 75.0 - 125 114224859

1,1,2,2-Tetrachloroethane 557275 21.9 20.0 ug/L 110 60.0 - 140 114224859

1,1,2-Trichloroethane 557275 21.8 20.0 ug/L 109 71.0 - 129 114224859

1,1-Dichloroethane 557275 22.1 20.0 ug/L 110 72.0 - 128 114224859

1,1-Dichloroethylene 557275 19.2 20.0 ug/L 95.9 50.0 - 150 114224859

1,2-Dichloroethane 557275 19.8 20.0 ug/L 99.2 68.0 - 132 114224859

1,2-Dichloropropane 557275 20.5 20.0 ug/L 102 34.0 - 166 114224859

2-Chloroethylvinyl ether 557275 13.3 20.0 ug/L 66.3 10.0 - 224 114224859

Benzene 557275 21.4 20.0 ug/L 107 64.0 - 136 114224859

Bromodichloromethane 557275 19.1 20.0 ug/L 95.4 65.0 - 135 114224859

Bromoform 557275 15.5 20.0 ug/L 77.4 71.0 - 129 114224859


Bromi

557275 18.8 20.0 ug/L 94.0 14.0 - 186 114224859

Carbon Tetrachloride 557275 18.1 20.0 ug/L 90.3 73.0 - 127 114224859

Chlorobenzene 557275 21.0 20.0 ug/L 105 66.0 - 134 114224859

Chloroethane 557275 21.6 20.0 ug/L 108 38.0 - 162 114224859

Chloroform 557275 21.6 20.0 ug/L 108 67.0 - 133 114224859

Chloromethane 557275 19.1 20.0 ug/L 95.3 10.0 - 204 114224859

cis-1,3-Dichloropropene 557275 17.4 20.0 ug/L 87.0 24.0 - 176 114224859

Dibromochloromethane 557275 16.6 20.0 ug/L 82.8 67.0 - 133 114224859

Ethylbenzene 557275 19.2 20.0 ug/L 96.2 59.0 - 141 114224859

Methylene chloride 557275 21.1 20.0 ug/L 106 60.0 - 140 114224859

Tetrachloroethylene 557275 20.8 20.0 ug/L 104 73.0 - 126 114224859

Toluene 557275 20.7 20.0 ug/L 104 74.0 - 126 114224859

trans-1,2-Dichloroethene 557275 20.3 20.0 ug/L 101 69.0 - 131 114224859

trans-1,3-Dichloropropene 557275 17.7 20.0 ug/L 88.6 50.0 - 150 114224859






1

2

3

4






LCS


Trichloroethylene 557275 19.8 20.0 ug/L 99.0 66.0 - 133 114224859

Vinyl chloride 557275 17.9 20.0 ug/L 89.6 10.0 - 196 114224859

LCS Dup


1,1,1-Trichloroethane 557275 19.5 18.5 20.0 75.0 - 125 97.4 92.6 ug/L 5.05 30.0

1,1,2,2-Tetrachloroethane 557275 21.9 21.8 20.0 60.0 - 140 110 109 ug/L 0.913 30.0

1,1,2-Trichloroethane 557275 21.8 20.8 20.0 71.0 - 129 109 104 ug/L 4.69 30.0

1,1-Dichloroethane 557275 22.1 21.0 20.0 72.0 - 128 110 105 ug/L 4.65 30.0

1,1-Dichloroethylene 557275 19.2 17.2 20.0 50.0 - 150 95.9 86.1 ug/L 10.8 30.0

1,2-Dichloroethane 557275 19.8 19.4 20.0 68.0 - 132 99.2 97.2 ug/L 2.04 30.0

1,2-Dichloropropane 557275 20.5 19.9 20.0 34.0 - 166 102 99.7 ug/L 2.28 30.0

2-Chloroethylvinyl ether 557275 13.3 12.3 20.0 10.0 - 224 66.3 61.4 ug/L 7.67 30.0

Benzene 557275 21.4 20.6 20.0 64.0 - 136 107 103 ug/L 3.81 30.0

Bromodichloromethane 557275 19.1 18.6 20.0 65.0 - 135 95.4 92.8 ug/L 2.76 30.0

Bromoform 557275 15.5 15.3 20.0 71.0 - 129 77.4 76.6 ug/L 1.04 30.0


Bromi

557275 18.8 18.6 20.0 14.0 - 186 94.0 93.1 ug/L 0.962 30.0

Carbon Tetrachloride 557275 18.1 17.1 20.0 73.0 - 127 90.3 85.5 ug/L 5.46 30.0

Chlorobenzene 557275 21.0 20.1 20.0 66.0 - 134 105 100 ug/L 4.88 30.0

Chloroethane 557275 21.6 19.8 20.0 38.0 - 162 108 99.0 ug/L 8.70 30.0

Chloroform 557275 21.6 20.8 20.0 67.0 - 133 108 104 ug/L 3.77 30.0

Chloromethane 557275 19.1 18.4 20.0 10.0 - 204 95.3 91.8 ug/L 3.74 30.0

cis-1,3-Dichloropropene 557275 17.4 16.9 20.0 24.0 - 176 87.0 84.6 ug/L 2.80 30.0

Dibromochloromethane 557275 16.6 15.8 20.0 67.0 - 133 82.8 78.8 ug/L 4.95 30.0

Ethylbenzene 557275 19.2 18.8 20.0 59.0 - 141 96.2 93.8 ug/L 2.53 30.0

Methylene chloride 557275 21.1 20.6 20.0 60.0 - 140 106 103 ug/L 2.87 30.0

Tetrachloroethylene 557275 20.8 19.4 20.0 73.0 - 126 104 97.0 ug/L 6.97 30.0

Toluene 557275 20.7 19.6 20.0 74.0 - 126 104 98.0 ug/L 5.94 30.0

trans-1,2-Dichloroethene 557275 20.3 19.7 20.0 69.0 - 131 101 98.7 ug/L 2.30 30.0

trans-1,3-Dichloropropene 557275 17.7 17.3 20.0 50.0 - 150 88.6 86.4 ug/L 2.51 30.0

Trichloroethylene 557275 19.8 19.3 20.0 66.0 - 133 99.0 96.4 ug/L 2.66 30.0

Vinyl chloride 557275 17.9 16.1 20.0 10.0 - 196 89.6 80.4 ug/L 10.8 30.0

MS


1,1,1-Trichloroethane 1280758 19.6 0 ND 20.0 52.0 - 162 98.0 ug/L 30.0

1,1,2,2-Tetrachloroethane 1280758 22.4 0 ND 20.0 46.0 - 157 112 ug/L 30.0

1,1,2-Trichloroethane 1280758 20.6 0 ND 20.0 52.0 - 150 103 ug/L 30.0

1,1-Dichloroethane 1280758 20.8 0 ND 20.0 59.0 - 155 104 ug/L 30.0

1,1-Dichloroethylene 1280758 20.3 0 ND 20.0 0.100 - 234 102 ug/L 30.0

1,2-Dichloroethane 1280758 19.5 0 ND 20.0 49.0 - 155 97.5 ug/L 30.0

1,2-Dichloropropane 1280758 20.7 0 ND 20.0 0.100 - 210 104 ug/L 30.0

2-Chloroethylvinyl ether 1280758 16.2 0 ND 20.0 0.100 - 305 81.0 ug/L 30.0

Benzene 1280758 21.1 0 ND 20.0 37.0 - 151 106 ug/L 30.0

Bromodichloromethane 1280758 19.2 0 ND 20.0 35.0 - 155 96.0 ug/L 30.0

Bromoform 1280758 14.5 0 ND 20.0 45.0 - 169 72.5 ug/L 30.0


Bromi

1280758 19.4 0 ND 20.0 0.100 - 242 97.0 ug/L 30.0

Carbon Tetrachloride 1280758 18.6 0 ND 20.0 70.0 - 140 93.0 ug/L 30.0

Chlorobenzene 1280758 19.1 0 ND 20.0 37.0 - 160 95.5 ug/L 30.0

Chloroethane 1280758 21.4 0 ND 20.0 14.0 - 230 107 ug/L 30.0






1

2

3

4






MS


Chloroform 1280758 22.3 0 0.790 20.0 51.0 - 138 108 ug/L 30.0

Chloromethane 1280758 22.9 0 ND 20.0 0.100 - 273 114 ug/L 30.0

cis-1,3-Dichloropropene 1280758 17.2 0 ND 20.0 0.100 - 227 86.0 ug/L 30.0

Dibromochloromethane 1280758 16.4 0 ND 20.0 53.0 - 149 82.0 ug/L 30.0

Ethylbenzene 1280758 19.5 0 ND 20.0 37.0 - 162 97.5 ug/L 30.0

Methylene chloride 1280758 21.3 0 ND 20.0 0.100 - 221 106 ug/L 30.0

Tetrachloroethylene 1280758 20.6 0 ND 20.0 64.0 - 148 103 ug/L 30.0

Toluene 1280758 20.3 0 ND 20.0 47.0 - 150 102 ug/L 30.0

trans-1,2-Dichloroethene 1280758 21.3 0 ND 20.0 54.0 - 156 106 ug/L 30.0

trans-1,3-Dichloropropene 1280758 17.1 0 ND 20.0 17.0 - 183 85.5 ug/L 30.0

Trichloroethylene 1280758 20.7 0 ND 20.0 71.0 - 157 104 ug/L 30.0

Vinyl chloride 1280758 27.8 0 ND 20.0 0.100 - 251 139 ug/L 30.0

MSD


1,1,1-Trichloroethane 1280758 19.6 19.3 ND 20.0 52.0 - 162 98.0 96.5 ug/L 1.54 30.0

1,1,2,2-Tetrachloroethane 1280758 22.4 22.4 ND 20.0 46.0 - 157 112 112 ug/L 0 30.0

1,1,2-Trichloroethane 1280758 20.6 20.9 ND 20.0 52.0 - 150 103 104 ug/L 0.966 30.0

1,1-Dichloroethane 1280758 20.8 20.5 ND 20.0 59.0 - 155 104 103 ug/L 0.966 30.0

1,1-Dichloroethylene 1280758 20.3 20.7 ND 20.0 0.100 - 234 102 104 ug/L 1.94 30.0

1,2-Dichloroethane 1280758 19.5 19.0 ND 20.0 49.0 - 155 97.5 94.8 ug/L 2.81 30.0

1,2-Dichloropropane 1280758 20.7 20.6 ND 20.0 0.100 - 210 104 103 ug/L 0.966 30.0

2-Chloroethylvinyl ether 1280758 16.2 20.6 ND 20.0 0.100 - 305 81.0 103 ug/L 23.9 30.0

Benzene 1280758 21.1 20.7 ND 20.0 37.0 - 151 106 104 ug/L 1.90 30.0

Bromodichloromethane 1280758 19.2 18.2 ND 20.0 35.0 - 155 96.0 90.9 ug/L 5.46 30.0

Bromoform 1280758 14.5 14.4 ND 20.0 45.0 - 169 72.5 72.0 ug/L 0.692 30.0


Bromi

1280758 19.4 18.8 ND 20.0 0.100 - 242 97.0 94.1 ug/L 3.04 30.0

Carbon Tetrachloride 1280758 18.6 17.8 ND 20.0 70.0 - 140 93.0 89.1 ug/L 4.28 30.0

Chlorobenzene 1280758 19.1 19.0 ND 20.0 37.0 - 160 95.5 94.8 ug/L 0.736 30.0

Chloroethane 1280758 21.4 21.2 ND 20.0 14.0 - 230 107 106 ug/L 0.939 30.0

Chloroform 1280758 22.3 21.2 0.790 20.0 51.0 - 138 108 102 ug/L 5.71 30.0

Chloromethane 1280758 22.9 22.1 ND 20.0 0.100 - 273 114 110 ug/L 3.57 30.0

cis-1,3-Dichloropropene 1280758 17.2 17.0 ND 20.0 0.100 - 227 86.0 85.2 ug/L 0.935 30.0

Dibromochloromethane 1280758 16.4 15.4 ND 20.0 53.0 - 149 82.0 76.8 ug/L 6.55 30.0

Ethylbenzene 1280758 19.5 19.4 ND 20.0 37.0 - 162 97.5 97.0 ug/L 0.514 30.0

Methylene chloride 1280758 21.3 21.5 ND 20.0 0.100 - 221 106 108 ug/L 1.87 30.0

Tetrachloroethylene 1280758 20.6 20.3 ND 20.0 64.0 - 148 103 101 ug/L 1.96 30.0

Toluene 1280758 20.3 20.3 ND 20.0 47.0 - 150 102 101 ug/L 0.985 30.0

trans-1,2-Dichloroethene 1280758 21.3 20.8 ND 20.0 54.0 - 156 106 104 ug/L 1.90 30.0

trans-1,3-Dichloropropene 1280758 17.1 17.1 ND 20.0 17.0 - 183 85.5 85.4 ug/L 0.117 30.0

Trichloroethylene 1280758 20.7 20.4 ND 20.0 71.0 - 157 104 102 ug/L 1.94 30.0

Vinyl chloride 1280758 27.8 25.5 ND 20.0 0.100 - 251 139 127 ug/L 9.02 30.0

Surrogate


1,2-DCA-d4 (SURR) 557275 CCV 22.5 20.0 ug/L 112 70.0 - 130 114224857

1,2-DCA-d4 (SURR) 557275 LCS 22.0 20.0 ug/L 110 70.0 - 130 114224859

1,2-DCA-d4 (SURR) 557275 LCS Dup 21.9 20.0 ug/L 110 70.0 - 130 114224860

1,2-DCA-d4 (SURR) 557275 Blank 22.0 20.0 ug/L 110 70.0 - 130 114224861

Bromofluorobenzene

(SURR)

557275 CCV 19.8 20.0 ug/L 99.0 70.0 - 142 114224857






1

2

3

4






Surrogate


Bromofluorobenzene

(SURR)

557275 LCS 19.5 20.0 ug/L 97.5 70.0 - 142 114224859

Bromofluorobenzene

(SURR)

557275 LCS Dup 19.9 20.0 ug/L 99.5 70.0 - 142 114224860

Bromofluorobenzene

(SURR)

557275 Blank 20.6 20.0 ug/L 103 70.0 - 142 114224861

Dibromofluoromethane

(SURR)

557275 CCV 20.8 20.0 ug/L 104 70.0 - 140 114224857


(SURR)

557275 LCS 21.1 20.0 ug/L 106 70.0 - 140 114224859


(SURR)

557275 LCS Dup 20.8 20.0 ug/L 104 70.0 - 140 114224860


(SURR)

557275 Blank 20.2 20.0 ug/L 101 70.0 - 140 114224861

TolueneD8 (SURR) 557275 CCV 20.7 20.0 ug/L 104 70.0 - 140 114224857

TolueneD8 (SURR) 557275 LCS 20.9 20.0 ug/L 104 70.0 - 140 114224859

TolueneD8 (SURR) 557275 LCS Dup 21.2 20.0 ug/L 106 70.0 - 140 114224860

TolueneD8 (SURR) 557275 Blank 20.5 20.0 ug/L 102 70.0 - 140 114224861

1,2-DCA-d4 (SURR) 1280758 UNKNOWN22.3 20.0 ug/L 112 70.0 - 130 114224862

1,2-DCA-d4 (SURR) 1280758 MS 22.0 20.0 ug/L 110 70.0 - 130 114230125

1,2-DCA-d4 (SURR) 1280758 MSD 22.0 20.0 ug/L 110 70.0 - 130 114230126

Bromofluorobenzene

(SURR)

1280758 UNKNOWN20.2 20.0 ug/L 101 70.0 - 142 114224862

Bromofluorobenzene

(SURR)

1280758 MS 19.5 20.0 ug/L 97.5 70.0 - 142 114230125

Bromofluorobenzene

(SURR)

1280758 MSD 19.8 20.0 ug/L 99.0 70.0 - 142 114230126


(SURR)

1280758 UNKNOWN19.7 20.0 ug/L 98.5 70.0 - 140 114224862


(SURR)

1280758 MS 20.4 20.0 ug/L 102 70.0 - 140 114230125


(SURR)

1280758 MSD 20.0 20.0 ug/L 100 70.0 - 140 114230126

TolueneD8 (SURR) 1280758 UNKNOWN20.9 20.0 ug/L 104 70.0 - 140 114224862

TolueneD8 (SURR) 1280758 MS 20.9 20.0 ug/L 104 70.0 - 140 114230125

TolueneD8 (SURR) 1280758 MSD 20.8 20.0 ug/L 104 70.0 - 140 114230126

EPA 608Liquid Aqueous 557283

Blank


PCB-1016 557175 ND 0.155 0.500 ug/L 114232801

PCB-1221 557175 ND 0.143 0.500 ug/L 114232801

PCB-1232 557175 ND 0.143 0.500 ug/L 114232801

PCB-1242 557175 ND 0.143 0.500 ug/L 114232801

PCB-1248 557175 ND 0.143 0.500 ug/L 114232801

PCB-1254 557175 ND 0.143 0.500 ug/L 114232801

PCB-1260 557175 ND 0.143 0.500 ug/L 114232801

CCV


PCB-1016 1170 1000 ug/L 117 70.0 - 130 114224967

PCB-1016 1000 1000 ug/L 100 70.0 - 130 114232807

PCB-1260 980 1000 ug/L 98.0 70.0 - 130 114224967

PCB-1260 866 1000 ug/L 86.6 70.0 - 130 114232807






1

2

3

4






LCS


PCB-1016 557196 9.60 10.0 ug/L 96.0 24.3 - 151 114232803

PCB-1260 557196 7.13 10.0 ug/L 71.3 23.2 - 147 114232803

Surrogate


Decachlorobiphenyl 557175 Blank 104 100 ug/L 104 10.0 - 200 114232801

Tetrachloro-m-Xylene (Surr) 557175 Blank 73.1 100 ug/L 73.1 10.0 - 200 114232801

Decachlorobiphenyl 1280758 UNKNOWN0.0403 0.101 ug/L 39.9 10.0 - 200 114224969

Tetrachloro-m-Xylene (Surr) 1280758 UNKNOWN0.0632 0.101 ug/L 62.6 10.0 - 200 114224969


Blank


4,4-DDD 557175 ND 0.0194 0.025 ug/L 114231283

4,4-DDE 557175 ND 0.0161 0.025 ug/L 114231283

4,4-DDT 557175 ND 0.00591 0.010 ug/L 114231283

Aldrin 557175 ND 0.00253 0.010 ug/L 114231283

Alpha-BHC(hexachlorocyclo

hexane)

557175 ND 0.015 0.025 ug/L 114231283

Beta-BHC(hexachlorocycloh

exane)

557175 ND 0.00871 0.010 ug/L 114231283

Chlordane 557175 ND 0.00188 0.010 ug/L 114231283

Delta-BHC(hexachlorocycloh

exane)

557175 ND 0.00523 0.010 ug/L 114231283

Dieldrin 557175 ND 0.00653 0.010 ug/L 114231283

Endosulfan I (alpha) 557175 ND 0.00719 0.010 ug/L 114231283

Endosulfan II (beta) 557175 ND 0.00767 0.010 ug/L 114231283

Endosulfan sulfate 557175 ND 0.00333 0.010 ug/L 114231283

Endrin 557175 ND 0.00857 0.010 ug/L 114231283

Endrin aldehyde 557175 ND 0.0144 0.025 ug/L 114231283

Gamma-BHC(Lindane) 557175 ND 0.00897 0.010 ug/L 114231283

Heptachlor 557175 ND 0.00147 0.010 ug/L 114231283

Heptachlor epoxide 557175 ND 0.00128 0.010 ug/L 114231283

Toxaphene 557175 ND 0.00373 0.010 ug/L 114231283

CCV


4,4-DDD 98.9 100 ug/L 98.9 85.0 - 115 114224986

4,4-DDD 120 100 ug/L 120 85.0 - 115 * 114231289

4,4-DDE 103 100 ug/L 103 85.0 - 115 114224986

4,4-DDE 108 100 ug/L 108 85.0 - 115 114231289

4,4-DDT 94.0 100 ug/L 94.0 85.0 - 115 114224986

4,4-DDT 117 100 ug/L 117 85.0 - 115 * 114231289

Aldrin 105 100 ug/L 105 85.0 - 115 114224986

Aldrin 103 100 ug/L 103 85.0 - 115 114231289


hexane)

103 100 ug/L 103 85.0 - 115 114224986


hexane)

112 100 ug/L 112 85.0 - 115 114231289


exane)

97.3 100 ug/L 97.3 85.0 - 115 114224986


exane)

110 100 ug/L 110 85.0 - 115 114231289






1

2

3

4






CCV



exane)

94.5 100 ug/L 94.5 85.0 - 115 114224986


exane)

106 100 ug/L 106 85.0 - 115 114231289

Dieldrin 94.6 100 ug/L 94.6 85.0 - 115 114224986

Dieldrin 121 100 ug/L 121 85.0 - 115 * 114231289

Endosulfan I (alpha) 98.0 100 ug/L 98.0 85.0 - 115 114224986

Endosulfan I (alpha) 117 100 ug/L 117 85.0 - 115 * 114231289

Endosulfan II (beta) 94.8 100 ug/L 94.8 85.0 - 115 114224986

Endosulfan II (beta) 117 100 ug/L 117 85.0 - 115 * 114231289

Endosulfan sulfate 89.1 100 ug/L 89.1 85.0 - 115 114224986

Endosulfan sulfate 107 100 ug/L 107 85.0 - 115 114231289

Endrin 94.1 100 ug/L 94.1 85.0 - 115 114224986

Endrin 121 100 ug/L 121 85.0 - 115 * 114231289

Endrin aldehyde 93.5 100 ug/L 93.5 85.0 - 115 114224986

Endrin aldehyde 111 100 ug/L 111 85.0 - 115 114231289

Gamma-BHC(Lindane) 92.3 100 ug/L 92.3 85.0 - 115 114224986

Gamma-BHC(Lindane) 108 100 ug/L 108 85.0 - 115 114231289

Heptachlor 88.9 100 ug/L 88.9 85.0 - 115 114224986

Heptachlor 107 100 ug/L 107 85.0 - 115 114231289

Heptachlor epoxide 97.9 100 ug/L 97.9 85.0 - 115 114224986

Heptachlor epoxide 116 100 ug/L 116 85.0 - 115 * 114231289

LCS


4,4-DDD 557175 0.861 1.00 ug/L 86.1 34.3 - 136 114231284

4,4-DDE 557175 0.919 1.00 ug/L 91.9 44.1 - 130 114231284

4,4-DDT 557175 1.00 1.00 ug/L 100 24.4 - 154 114231284

Aldrin 557175 0.732 1.00 ug/L 73.2 25.5 - 119 114231284


hexane)

557175 0.813 1.00 ug/L 81.3 30.2 - 126 114231284


exane)

557175 0.916 1.00 ug/L 91.6 39.3 - 147 114231284


exane)

557175 0.873 1.00 ug/L 87.3 42.5 - 135 114231284

Dieldrin 557175 1.02 1.00 ug/L 102 41.6 - 140 114231284

Endosulfan I (alpha) 557175 0.927 1.00 ug/L 92.7 34.1 - 126 114231284

Endosulfan II (beta) 557175 0.925 1.00 ug/L 92.5 41.3 - 129 114231284

Endosulfan sulfate 557175 0.938 1.00 ug/L 93.8 43.6 - 142 114231284

Endrin 557175 1.01 1.00 ug/L 101 39.4 - 148 114231284

Endrin aldehyde 557175 0.928 1.00 ug/L 92.8 40.8 - 137 114231284

Gamma-BHC(Lindane) 557175 0.811 1.00 ug/L 81.1 29.9 - 130 114231284

Heptachlor 557175 0.779 1.00 ug/L 77.9 18.9 - 128 114231284

Heptachlor epoxide 557175 0.935 1.00 ug/L 93.5 42.1 - 132 114231284

LCS Dup


4,4-DDD 557175 0.861 0.832 1.00 34.3 - 136 86.1 83.2 ug/L 3.43 40.0

4,4-DDE 557175 0.919 0.873 1.00 44.1 - 130 91.9 87.3 ug/L 5.13 40.0

4,4-DDT 557175 1.00 0.984 1.00 24.4 - 154 100 98.4 ug/L 1.61 40.0

Aldrin 557175 0.732 0.752 1.00 25.5 - 119 73.2 75.2 ug/L 2.70 40.0


hexane)

557175 0.813 0.816 1.00 30.2 - 126 81.3 81.6 ug/L 0.368 40.0






1

2

3

4






LCS Dup



exane)

557175 0.916 0.869 1.00 39.3 - 147 91.6 86.9 ug/L 5.27 40.0


exane)

557175 0.873 0.828 1.00 42.5 - 135 87.3 82.8 ug/L 5.29 40.0

Dieldrin 557175 1.02 0.967 1.00 41.6 - 140 102 96.7 ug/L 5.33 40.0

Endosulfan I (alpha) 557175 0.927 0.885 1.00 34.1 - 126 92.7 88.5 ug/L 4.64 40.0

Endosulfan II (beta) 557175 0.925 0.883 1.00 41.3 - 129 92.5 88.3 ug/L 4.65 40.0

Endosulfan sulfate 557175 0.938 0.923 1.00 43.6 - 142 93.8 92.3 ug/L 1.61 40.0

Endrin 557175 1.01 0.951 1.00 39.4 - 148 101 95.1 ug/L 6.02 40.0

Endrin aldehyde 557175 0.928 0.895 1.00 40.8 - 137 92.8 89.5 ug/L 3.62 40.0

Gamma-BHC(Lindane) 557175 0.811 0.802 1.00 29.9 - 130 81.1 80.2 ug/L 1.12 40.0

Heptachlor 557175 0.779 0.812 1.00 18.9 - 128 77.9 81.2 ug/L 4.15 40.0

Heptachlor epoxide 557175 0.935 0.893 1.00 42.1 - 132 93.5 89.3 ug/L 4.60 40.0

Surrogate


Decachlorobiphenyl 132147 CCV 96.1 100 ug/L 96.1 0.100 - 180 114224986

Decachlorobiphenyl 132147 CCV 119 100 ug/L 119 0.100 - 180 114231289

Tetrachloro-m-Xylene (Surr) 132147 CCV 100 100 ug/L 100 9.90 - 130 114224986

Tetrachloro-m-Xylene (Surr) 132147 CCV 99.4 100 ug/L 99.4 9.90 - 130 114231289

Decachlorobiphenyl 557175 Blank 104 100 ug/L 104 0.100 - 180 114231283

Decachlorobiphenyl 557175 LCS 99.8 100 ug/L 99.8 0.100 - 180 114231284

Decachlorobiphenyl 557175 LCS Dup 104 100 ug/L 104 0.100 - 180 114231285

Tetrachloro-m-Xylene (Surr) 557175 Blank 73.1 100 ug/L 73.1 9.90 - 130 114231283

Tetrachloro-m-Xylene (Surr) 557175 LCS 61.6 100 ug/L 61.6 9.90 - 130 114231284

Tetrachloro-m-Xylene (Surr) 557175 LCS Dup 65.2 100 ug/L 65.2 9.90 - 130 114231285

Decachlorobiphenyl 1280758 UNKNOWN0.0403 0.101 ug/L 39.9 0.100 - 180 114224987

Tetrachloro-m-Xylene (Surr) 1280758 UNKNOWN0.0632 0.101 ug/L 62.6 9.90 - 130 114224987


Blank


Chlorpyrifos 557195 ND 0.0394 0.040 ug/L 114225107

CCV


Chlorpyrifos 958 1000 ug/L 95.8 80.0 - 120 114225106

Chlorpyrifos 1180 1000 ug/L 118 80.0 - 120 114226875

LCS


Chlorpyrifos 557195 0.727 1.00 ug/L 72.7 6.22 - 164 114225108

LCS Dup


Chlorpyrifos 557195 0.727 0.812 1.00 6.22 - 164 72.7 81.2 ug/L 11.0 30.0

Surrogate


Tributylphosphate 132891 CCV 1180 1000 ug/L 118 0.100 - 495 114225106

Tributylphosphate 132891 CCV 1940 1000 ug/L 194 0.100 - 495 114226875

Triphenylphosphate 132891 CCV 1010 1000 ug/L 101 0.100 - 1070 114225106

Triphenylphosphate 132891 CCV 1200 1000 ug/L 120 0.100 - 1070 114226875






1

2

3

4






Surrogate


Tributylphosphate 557195 Blank 1130 1000 ug/L 113 0.100 - 495 114225107

Tributylphosphate 557195 LCS 1250 1000 ug/L 125 0.100 - 495 114225108

Tributylphosphate 557195 LCS Dup 1380 1000 ug/L 138 0.100 - 495 114225109

Triphenylphosphate 557195 Blank 934 1000 ug/L 93.4 0.100 - 1070 114225107

Triphenylphosphate 557195 LCS 832 1000 ug/L 83.2 0.100 - 1070 114225108

Triphenylphosphate 557195 LCS Dup 889 1000 ug/L 88.9 0.100 - 1070 114225109

Tributylphosphate 1280758 UNKNOWN1.40 1.01 ug/L 139 0.100 - 495 114225110

Triphenylphosphate 1280758 UNKNOWN0.790 1.01 ug/L 78.2 0.100 - 1070 114225110


BFB


BFB Mass 173 557311 174 4 0.2 0 - 2.00 114225541

BFB Mass 174 557311 95.0 2066 83.5 50.0 - 100 114225541

BFB Mass 175 557311 174 142 6.9 5.00 - 9.00 114225541

BFB Mass 176 557311 174 2065 100.0 95.0 - 101 114225541

BFB Mass 177 557311 176 127 6.2 5.00 - 9.00 114225541

BFB Mass 50 557311 95.0 429 17.3 15.0 - 40.0 114225541

BFB Mass 75 557311 95.0 1068 43.2 30.0 - 60.0 114225541

BFB Mass 95 557311 95.0 2473 100.0 100 - 100 114225541

BFB Mass 96 557311 95.0 187 7.6 5.00 - 9.00 114225541

Blank


Acrolein 557311 ND 0.883 1.00 ug/L 114225545

Acrylonitrile 557311 ND 0.697 1.00 ug/L 114225545

CCV


Acrolein 42.1 40.0 ug/L 105 70.0 - 130 114225542

Acrylonitrile 42.3 40.0 ug/L 106 70.0 - 130 114225542

IS Areas



(ISTD)

557311 LCS 31610 32430 16220 48650 114225543 557311


(ISTD)

557311 LCS Dup 31750 32430 16220 48650 114225544 557311


(ISTD)

557311 Blank 29570 32430 16220 48650 114225545 557311





(ISTD)

1280758 UNKNOWN30730 32430 16220 48650 114225546 1280758


IS RetTime



(ISTD)

557311 LCS 14.66 14.66 14.60 14.72 114225543 557311


(ISTD)

557311 LCS Dup 14.67 14.66 14.60 14.72 114225544 557311






1

2

3

4






IS RetTime



(ISTD)

557311 Blank 14.67 14.66 14.60 14.72 114225545 557311





(ISTD)

1280758 UNKNOWN14.67 14.66 14.60 14.72 114225546 1280758


LCS


Acrolein 557311 56.6 40.0 ug/L 142 0.100 - 425 114225543

Acrylonitrile 557311 42.3 40.0 ug/L 106 71.0 - 117 114225543

LCS Dup


Acrolein 557311 56.6 58.4 40.0 0.100 - 425 142 146 ug/L 2.78 30.0

Acrylonitrile 557311 42.3 44.3 40.0 71.0 - 117 106 111 ug/L 4.61 30.0

MS


Acrolein 1280758 52.9 0 ND 40.0 70.0 - 130 132 * ug/L 30.0

Acrylonitrile 1280758 41.8 0 ND 40.0 70.0 - 130 104 ug/L 30.0

MSD


Acrolein 1280758 52.9 38.8 ND 40.0 70.0 - 130 132 * 97.0 ug/L 30.6 * 30.0

Acrylonitrile 1280758 41.8 41.5 ND 40.0 70.0 - 130 104 104 ug/L 0 30.0

Surrogate


1,2-DCA-d4 (SURR) 557311 CCV 19.6 20.0 ug/L 98.0 70.0 - 130 114225542

1,2-DCA-d4 (SURR) 557311 LCS 20.5 20.0 ug/L 102 70.0 - 130 114225543



Bromofluorobenzene

(SURR)

557311 CCV 18.2 20.0 ug/L 91.0 70.0 - 142 114225542

Bromofluorobenzene

(SURR)

557311 LCS 18.8 20.0 ug/L 94.0 70.0 - 142 114225543

Bromofluorobenzene

(SURR)

557311 LCS Dup 19.0 20.0 ug/L 95.0 70.0 - 142 114225544

Bromofluorobenzene

(SURR)

557311 Blank 19.7 20.0 ug/L 98.5 70.0 - 142 114225545


(SURR)

557311 CCV 20.6 20.0 ug/L 103 70.0 - 140 114225542


(SURR)

557311 LCS 20.2 20.0 ug/L 101 70.0 - 140 114225543


(SURR)

557311 LCS Dup 20.3 20.0 ug/L 102 70.0 - 140 114225544


(SURR)

557311 Blank 20.5 20.0 ug/L 102 70.0 - 140 114225545

TolueneD8 (SURR) 557311 CCV 18.8 20.0 ug/L 94.0 70.0 - 140 114225542

TolueneD8 (SURR) 557311 LCS 19.3 20.0 ug/L 96.5 70.0 - 140 114225543

TolueneD8 (SURR) 557311 LCS Dup 18.8 20.0 ug/L 94.0 70.0 - 140 114225544

TolueneD8 (SURR) 557311 Blank 18.9 20.0 ug/L 94.5 70.0 - 140 114225545







1

2

3

4






Surrogate


1,2-DCA-d4 (SURR) 1280758 MS 20.4 20.0 ug/L 102 70.0 - 130 114229683

1,2-DCA-d4 (SURR) 1280758 MSD 20.4 20.0 ug/L 102 70.0 - 130 114229684

Bromofluorobenzene

(SURR)

1280758 UNKNOWN18.8 20.0 ug/L 94.0 70.0 - 142 114225546

Bromofluorobenzene

(SURR)

1280758 MS 19.3 20.0 ug/L 96.5 70.0 - 142 114229683

Bromofluorobenzene

(SURR)

1280758 MSD 18.5 20.0 ug/L 92.5 70.0 - 142 114229684


(SURR)

1280758 UNKNOWN20.7 20.0 ug/L 104 70.0 - 140 114225546


(SURR)

1280758 MS 21.1 20.0 ug/L 106 70.0 - 140 114229683


(SURR)

1280758 MSD 21.1 20.0 ug/L 106 70.0 - 140 114229684

TolueneD8 (SURR) 1280758 UNKNOWN18.5 20.0 ug/L 92.5 70.0 - 140 114225546

TolueneD8 (SURR) 1280758 MS 19.2 20.0 ug/L 96.0 70.0 - 140 114229683

TolueneD8 (SURR) 1280758 MSD 18.9 20.0 ug/L 94.5 70.0 - 140 114229684


BFB


BFB Mass 173 557312 174 4 0.2 0 - 2.00 114225547

BFB Mass 174 557312 95.0 2066 83.5 50.0 - 100 114225547

BFB Mass 175 557312 174 142 6.9 5.00 - 9.00 114225547

BFB Mass 176 557312 174 2065 100.0 95.0 - 101 114225547

BFB Mass 177 557312 176 127 6.2 5.00 - 9.00 114225547

BFB Mass 50 557312 95.0 429 17.3 15.0 - 40.0 114225547

BFB Mass 75 557312 95.0 1068 43.2 30.0 - 60.0 114225547

BFB Mass 95 557312 95.0 2473 100.0 100 - 100 114225547

BFB Mass 96 557312 95.0 187 7.6 5.00 - 9.00 114225547

Blank



1,1,2,2-Tetrachloroethane 557312 ND 0.217 1.00 ug/L 114225551



1,1-Dichloroethylene 557312 ND 0.388 1.00 ug/L 114225551


1,2-Dichloropropane 557312 ND 0.267 1.00 ug/L 114225551

2-Chloroethylvinyl ether 557312 ND 0.107 1.00 ug/L 114225551

Benzene 557312 ND 0.186 1.00 ug/L 114225551

Bromodichloromethane 557312 ND 0.186 1.00 ug/L 114225551

Bromoform 557312 ND 0.549 1.00 ug/L 114225551


Bromi

557312 ND 0.338 1.00 ug/L 114225551

Carbon Tetrachloride 557312 ND 0.285 1.00 ug/L 114225551

Chlorobenzene 557312 ND 0.120 1.00 ug/L 114225551

Chloroethane 557312 ND 0.370 1.00 ug/L 114225551

Chloroform 557312 ND 0.294 1.00 ug/L 114225551

Chloromethane 557312 ND 0.304 1.00 ug/L 114225551

cis-1,3-Dichloropropene 557312 ND 0.0689 1.00 ug/L 114225551

Dibromochloromethane 557312 ND 0.119 1.00 ug/L 114225551






1

2

3

4






Blank


Ethylbenzene 557312 ND 0.243 1.00 ug/L 114225551

Methylene chloride 557312 ND 0.231 1.00 ug/L 114225551

Tetrachloroethylene 557312 ND 0.324 1.00 ug/L 114225551

Toluene 557312 ND 0.182 1.00 ug/L 114225551

trans-1,2-Dichloroethene 557312 ND 0.256 1.00 ug/L 114225551

trans-1,3-Dichloropropene 557312 ND 0.0877 1.00 ug/L 114225551

Trichloroethylene 557312 ND 0.241 1.00 ug/L 114225551

Vinyl chloride 557312 ND 0.926 1.00 ug/L 114225551

CCV



1,1,2,2-Tetrachloroethane 18.6 20.0 ug/L 93.0 70.0 - 130 114225548


1,1-Dichloroethane 21.1 20.0 ug/L 106 70.0 - 130 114225548

1,1-Dichloroethylene 21.1 20.0 ug/L 106 70.0 - 130 114225548

1,2-Dichloroethane 18.7 20.0 ug/L 93.5 70.0 - 130 114225548

1,2-Dichloropropane 18.8 20.0 ug/L 94.0 70.0 - 130 114225548

2-Chloroethylvinyl ether 17.9 20.0 ug/L 89.5 70.0 - 130 114225548

Benzene 18.7 20.0 ug/L 93.5 70.0 - 130 114225548

Bromodichloromethane 16.5 20.0 ug/L 82.5 70.0 - 130 114225548

Bromoform 13.9 20.0 ug/L 69.5 70.0 - 130 * 114225548


Bromi

21.0 20.0 ug/L 105 70.0 - 130 114225548

Carbon Tetrachloride 16.3 20.0 ug/L 81.5 70.0 - 130 114225548

Chlorobenzene 17.8 20.0 ug/L 89.0 70.0 - 130 114225548

Chloroethane 21.5 20.0 ug/L 108 70.0 - 130 114225548

Chloroform 20.6 20.0 ug/L 103 70.0 - 130 114225548

Chloromethane 23.0 20.0 ug/L 115 70.0 - 130 114225548

cis-1,3-Dichloropropene 17.0 20.0 ug/L 85.0 70.0 - 130 114225548

Dibromochloromethane 15.7 20.0 ug/L 78.5 70.0 - 130 114225548

Ethylbenzene 17.3 20.0 ug/L 86.5 70.0 - 130 114225548

Methylene chloride 22.8 20.0 ug/L 114 70.0 - 130 114225548

Tetrachloroethylene 18.2 20.0 ug/L 91.0 70.0 - 130 114225548

Toluene 18.0 20.0 ug/L 90.0 70.0 - 130 114225548

trans-1,2-Dichloroethene 22.1 20.0 ug/L 110 70.0 - 130 114225548

trans-1,3-Dichloropropene 16.5 20.0 ug/L 82.5 70.0 - 130 114225548

Trichloroethylene 17.6 20.0 ug/L 88.0 70.0 - 130 114225548

Vinyl chloride 22.4 20.0 ug/L 112 70.0 - 130 114225548

IS Areas



(ISTD)

557312 LCS 31610 32430 16220 48650 114225549 557312


(ISTD)

557312 LCS Dup 31750 32430 16220 48650 114225550 557312


(ISTD)

557312 Blank 29570 32430 16220 48650 114225551 557312





(ISTD)

1280758 UNKNOWN30730 32430 16220 48650 114225552 1280758






1

2

3

4






IS Areas



IS RetTime



(ISTD)

557312 LCS 14.66 14.66 14.60 14.72 114225549 557312


(ISTD)

557312 LCS Dup 14.67 14.66 14.60 14.72 114225550 557312


(ISTD)

557312 Blank 14.67 14.66 14.60 14.72 114225551 557312





(ISTD)

1280758 UNKNOWN14.67 14.66 14.60 14.72 114225552 1280758


LCS



1,1,2,2-Tetrachloroethane 557312 17.6 20.0 ug/L 88.0 60.0 - 140 114225549


1,1-Dichloroethane 557312 23.2 20.0 ug/L 116 72.0 - 128 114225549

1,1-Dichloroethylene 557312 19.4 20.0 ug/L 97.2 50.0 - 150 114225549

1,2-Dichloroethane 557312 18.8 20.0 ug/L 93.8 68.0 - 132 114225549

1,2-Dichloropropane 557312 19.4 20.0 ug/L 97.1 34.0 - 166 114225549

2-Chloroethylvinyl ether 557312 17.4 20.0 ug/L 87.2 10.0 - 224 114225549

Benzene 557312 19.0 20.0 ug/L 94.9 64.0 - 136 114225549

Bromodichloromethane 557312 17.7 20.0 ug/L 88.4 65.0 - 135 114225549

Bromoform 557312 13.2 20.0 ug/L 66.0 71.0 - 129 114225549 *


Bromi

557312 22.1 20.0 ug/L 111 14.0 - 186 114225549

Carbon Tetrachloride 557312 17.2 20.0 ug/L 85.8 73.0 - 127 114225549

Chlorobenzene 557312 18.7 20.0 ug/L 93.6 66.0 - 134 114225549

Chloroethane 557312 22.4 20.0 ug/L 112 38.0 - 162 114225549

Chloroform 557312 21.5 20.0 ug/L 107 67.0 - 133 114225549

Chloromethane 557312 20.8 20.0 ug/L 104 10.0 - 204 114225549

cis-1,3-Dichloropropene 557312 16.8 20.0 ug/L 83.8 24.0 - 176 114225549

Dibromochloromethane 557312 15.9 20.0 ug/L 79.4 67.0 - 133 114225549

Ethylbenzene 557312 17.6 20.0 ug/L 88.0 59.0 - 141 114225549

Methylene chloride 557312 22.7 20.0 ug/L 113 60.0 - 140 114225549

Tetrachloroethylene 557312 18.7 20.0 ug/L 93.4 73.0 - 126 114225549

Toluene 557312 18.2 20.0 ug/L 91.0 74.0 - 126 114225549

trans-1,2-Dichloroethene 557312 21.0 20.0 ug/L 105 69.0 - 131 114225549

trans-1,3-Dichloropropene 557312 15.6 20.0 ug/L 78.2 50.0 - 150 114225549

Trichloroethylene 557312 17.9 20.0 ug/L 89.3 66.0 - 133 114225549

Vinyl chloride 557312 17.7 20.0 ug/L 88.4 10.0 - 196 114225549

LCS Dup



1,1,2,2-Tetrachloroethane 557312 17.6 18.1 20.0 60.0 - 140 88.0 90.6 ug/L 2.91 30.0







1

2

3

4






LCS Dup


1,1-Dichloroethane 557312 23.2 22.2 20.0 72.0 - 128 116 111 ug/L 4.41 30.0

1,1-Dichloroethylene 557312 19.4 18.6 20.0 50.0 - 150 97.2 93.1 ug/L 4.31 30.0

1,2-Dichloroethane 557312 18.8 18.1 20.0 68.0 - 132 93.8 90.6 ug/L 3.47 30.0

1,2-Dichloropropane 557312 19.4 18.5 20.0 34.0 - 166 97.1 92.6 ug/L 4.74 30.0

2-Chloroethylvinyl ether 557312 17.4 17.1 20.0 10.0 - 224 87.2 85.7 ug/L 1.74 30.0

Benzene 557312 19.0 17.8 20.0 64.0 - 136 94.9 89.2 ug/L 6.19 30.0

Bromodichloromethane 557312 17.7 16.6 20.0 65.0 - 135 88.4 83.0 ug/L 6.30 30.0

Bromoform 557312 13.2 13.7 20.0 71.0 - 129 66.0 68.4 * ug/L 3.57 30.0


Bromi

557312 22.1 21.3 20.0 14.0 - 186 111 106 ug/L 4.61 30.0

Carbon Tetrachloride 557312 17.2 15.7 20.0 73.0 - 127 85.8 78.4 ug/L 9.01 30.0

Chlorobenzene 557312 18.7 18.3 20.0 66.0 - 134 93.6 91.3 ug/L 2.49 30.0

Chloroethane 557312 22.4 21.2 20.0 38.0 - 162 112 106 ug/L 5.50 30.0

Chloroform 557312 21.5 20.5 20.0 67.0 - 133 107 102 ug/L 4.78 30.0

Chloromethane 557312 20.8 19.2 20.0 10.0 - 204 104 96.0 ug/L 8.00 30.0

cis-1,3-Dichloropropene 557312 16.8 15.8 20.0 24.0 - 176 83.8 79.2 ug/L 5.64 30.0

Dibromochloromethane 557312 15.9 14.8 20.0 67.0 - 133 79.4 74.2 ug/L 6.77 30.0

Ethylbenzene 557312 17.6 16.9 20.0 59.0 - 141 88.0 84.6 ug/L 3.94 30.0

Methylene chloride 557312 22.7 22.4 20.0 60.0 - 140 113 112 ug/L 0.889 30.0

Tetrachloroethylene 557312 18.7 18.0 20.0 73.0 - 126 93.4 90.2 ug/L 3.49 30.0

Toluene 557312 18.2 17.4 20.0 74.0 - 126 91.0 87.0 ug/L 4.49 30.0

trans-1,2-Dichloroethene 557312 21.0 19.8 20.0 69.0 - 131 105 99.0 ug/L 5.88 30.0

trans-1,3-Dichloropropene 557312 15.6 15.3 20.0 50.0 - 150 78.2 76.3 ug/L 2.46 30.0

Trichloroethylene 557312 17.9 17.1 20.0 66.0 - 133 89.3 85.3 ug/L 4.58 30.0

Vinyl chloride 557312 17.7 16.3 20.0 10.0 - 196 88.4 81.6 ug/L 8.00 30.0

MS



1,1,2,2-Tetrachloroethane 1280758 19.0 0 ND 20.0 46.0 - 157 95.0 ug/L 30.0


1,1-Dichloroethane 1280758 24.1 0 ND 20.0 59.0 - 155 120 ug/L 30.0

1,1-Dichloroethylene 1280758 21.2 0 ND 20.0 0.100 - 234 106 ug/L 30.0

1,2-Dichloroethane 1280758 19.3 0 ND 20.0 49.0 - 155 96.5 ug/L 30.0

1,2-Dichloropropane 1280758 20.0 0 ND 20.0 0.100 - 210 100 ug/L 30.0

2-Chloroethylvinyl ether 1280758 17.4 0 ND 20.0 0.100 - 305 87.0 ug/L 30.0

Benzene 1280758 19.7 0 ND 20.0 37.0 - 151 98.5 ug/L 30.0

Bromodichloromethane 1280758 18.0 0 ND 20.0 35.0 - 155 90.0 ug/L 30.0

Bromoform 1280758 13.8 0 ND 20.0 45.0 - 169 69.0 ug/L 30.0


Bromi

1280758 23.2 0 ND 20.0 0.100 - 242 116 ug/L 30.0

Carbon Tetrachloride 1280758 17.2 0 ND 20.0 70.0 - 140 86.0 ug/L 30.0

Chlorobenzene 1280758 19.5 0 ND 20.0 37.0 - 160 97.5 ug/L 30.0

Chloroethane 1280758 23.5 0 ND 20.0 14.0 - 230 118 ug/L 30.0

Chloroform 1280758 23.1 0 0.810 20.0 51.0 - 138 111 ug/L 30.0

Chloromethane 1280758 21.2 0 ND 20.0 0.100 - 273 106 ug/L 30.0

cis-1,3-Dichloropropene 1280758 16.9 0 ND 20.0 0.100 - 227 84.5 ug/L 30.0

Dibromochloromethane 1280758 16.0 0 ND 20.0 53.0 - 149 80.0 ug/L 30.0

Ethylbenzene 1280758 18.2 0 ND 20.0 37.0 - 162 91.0 ug/L 30.0

Methylene chloride 1280758 24.0 0 0.660 20.0 0.100 - 221 117 ug/L 30.0

Tetrachloroethylene 1280758 19.8 0 ND 20.0 64.0 - 148 99.0 ug/L 30.0






1

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MS


Toluene 1280758 18.7 0 ND 20.0 47.0 - 150 93.5 ug/L 30.0

trans-1,2-Dichloroethene 1280758 22.3 0 ND 20.0 54.0 - 156 112 ug/L 30.0

trans-1,3-Dichloropropene 1280758 17.0 0 ND 20.0 17.0 - 183 85.0 ug/L 30.0

Trichloroethylene 1280758 18.4 0 ND 20.0 71.0 - 157 92.0 ug/L 30.0

Vinyl chloride 1280758 19.6 0 ND 20.0 0.100 - 251 98.0 ug/L 30.0

MSD



1,1,2,2-Tetrachloroethane 1280758 19.0 18.5 ND 20.0 46.0 - 157 95.0 92.3 ug/L 2.88 30.0


1,1-Dichloroethane 1280758 24.1 24.0 ND 20.0 59.0 - 155 120 120 ug/L 0 30.0

1,1-Dichloroethylene 1280758 21.2 20.0 ND 20.0 0.100 - 234 106 100 ug/L 5.83 30.0

1,2-Dichloroethane 1280758 19.3 19.7 ND 20.0 49.0 - 155 96.5 98.7 ug/L 2.25 30.0

1,2-Dichloropropane 1280758 20.0 19.8 ND 20.0 0.100 - 210 100 98.9 ug/L 1.11 30.0

2-Chloroethylvinyl ether 1280758 17.4 17.7 ND 20.0 0.100 - 305 87.0 88.6 ug/L 1.82 30.0

Benzene 1280758 19.7 19.2 ND 20.0 37.0 - 151 98.5 96.0 ug/L 2.57 30.0

Bromodichloromethane 1280758 18.0 17.6 ND 20.0 35.0 - 155 90.0 88.0 ug/L 2.25 30.0

Bromoform 1280758 13.8 13.1 ND 20.0 45.0 - 169 69.0 65.7 ug/L 4.90 30.0


Bromi

1280758 23.2 22.8 ND 20.0 0.100 - 242 116 114 ug/L 1.74 30.0

Carbon Tetrachloride 1280758 17.2 16.8 ND 20.0 70.0 - 140 86.0 84.0 ug/L 2.35 30.0

Chlorobenzene 1280758 19.5 19.3 ND 20.0 37.0 - 160 97.5 96.6 ug/L 0.927 30.0

Chloroethane 1280758 23.5 22.6 ND 20.0 14.0 - 230 118 113 ug/L 4.33 30.0

Chloroform 1280758 23.1 22.9 0.810 20.0 51.0 - 138 111 110 ug/L 0.905 30.0

Chloromethane 1280758 21.2 20.8 ND 20.0 0.100 - 273 106 104 ug/L 1.90 30.0

cis-1,3-Dichloropropene 1280758 16.9 16.1 ND 20.0 0.100 - 227 84.5 80.6 ug/L 4.72 30.0

Dibromochloromethane 1280758 16.0 15.3 ND 20.0 53.0 - 149 80.0 76.6 ug/L 4.34 30.0

Ethylbenzene 1280758 18.2 18.0 ND 20.0 37.0 - 162 91.0 90.2 ug/L 0.883 30.0

Methylene chloride 1280758 24.0 23.8 0.660 20.0 0.100 - 221 117 116 ug/L 0.858 30.0

Tetrachloroethylene 1280758 19.8 19.8 ND 20.0 64.0 - 148 99.0 99.2 ug/L 0.202 30.0

Toluene 1280758 18.7 18.9 ND 20.0 47.0 - 150 93.5 94.6 ug/L 1.17 30.0

trans-1,2-Dichloroethene 1280758 22.3 21.9 ND 20.0 54.0 - 156 112 109 ug/L 2.71 30.0

trans-1,3-Dichloropropene 1280758 17.0 16.1 ND 20.0 17.0 - 183 85.0 80.5 ug/L 5.44 30.0

Trichloroethylene 1280758 18.4 17.9 ND 20.0 71.0 - 157 92.0 89.6 ug/L 2.64 30.0

Vinyl chloride 1280758 19.6 17.7 ND 20.0 0.100 - 251 98.0 88.5 ug/L 10.2 30.0

Surrogate


1,2-DCA-d4 (SURR) 557312 CCV 19.6 20.0 ug/L 98.0 70.0 - 130 114225548

1,2-DCA-d4 (SURR) 557312 LCS 20.5 20.0 ug/L 102 70.0 - 130 114225549



Bromofluorobenzene

(SURR)

557312 CCV 18.2 20.0 ug/L 91.0 70.0 - 142 114225548

Bromofluorobenzene

(SURR)

557312 LCS 18.8 20.0 ug/L 94.0 70.0 - 142 114225549

Bromofluorobenzene

(SURR)

557312 LCS Dup 19.0 20.0 ug/L 95.0 70.0 - 142 114225550

Bromofluorobenzene

(SURR)

557312 Blank 19.7 20.0 ug/L 98.5 70.0 - 142 114225551


(SURR)

557312 CCV 20.6 20.0 ug/L 103 70.0 - 140 114225548






1

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Surrogate



(SURR)

557312 LCS 20.2 20.0 ug/L 101 70.0 - 140 114225549


(SURR)

557312 LCS Dup 20.3 20.0 ug/L 102 70.0 - 140 114225550


(SURR)

557312 Blank 20.5 20.0 ug/L 102 70.0 - 140 114225551

TolueneD8 (SURR) 557312 CCV 18.8 20.0 ug/L 94.0 70.0 - 140 114225548

TolueneD8 (SURR) 557312 LCS 19.3 20.0 ug/L 96.5 70.0 - 140 114225549

TolueneD8 (SURR) 557312 LCS Dup 18.8 20.0 ug/L 94.0 70.0 - 140 114225550

TolueneD8 (SURR) 557312 Blank 18.9 20.0 ug/L 94.5 70.0 - 140 114225551


1,2-DCA-d4 (SURR) 1280758 MS 20.4 20.0 ug/L 102 70.0 - 130 114230030

1,2-DCA-d4 (SURR) 1280758 MSD 20.4 20.0 ug/L 102 70.0 - 130 114230031

Bromofluorobenzene

(SURR)

1280758 UNKNOWN18.8 20.0 ug/L 94.0 70.0 - 142 114225552

Bromofluorobenzene

(SURR)

1280758 MS 19.3 20.0 ug/L 96.5 70.0 - 142 114230030

Bromofluorobenzene

(SURR)

1280758 MSD 18.5 20.0 ug/L 92.5 70.0 - 142 114230031


(SURR)

1280758 UNKNOWN20.7 20.0 ug/L 104 70.0 - 140 114225552


(SURR)

1280758 MS 21.1 20.0 ug/L 106 70.0 - 140 114230030


(SURR)

1280758 MSD 21.1 20.0 ug/L 106 70.0 - 140 114230031

TolueneD8 (SURR) 1280758 UNKNOWN18.5 20.0 ug/L 92.5 70.0 - 140 114225552

TolueneD8 (SURR) 1280758 MS 19.2 20.0 ug/L 96.0 70.0 - 140 114230030

TolueneD8 (SURR) 1280758 MSD 18.9 20.0 ug/L 94.5 70.0 - 140 114230031

RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%

Blank - Method Blank; LCS - Laboratory Control Sample; CCV - Continuing Calibration Verification; MS - Matrix Spike; ICV - Initial Calibration

Verification; LDR - Linear Dynamic Range Standard; DFTPP - GC/MS Tuning Compound; BFB - GC/MS Tuning Compound






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wilson, tabatha

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