umatac industrial processes the alberta taciuk process (atp

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The Alberta Taciuk Proc ATP Technology Pilot Progr Modified Fischer Assay (MFA) First stage of testing. 100 g of feed per test. Small scale, quick, and inexpensive. Provides pyrolysis yield characterization and preliminary ore grade assessment. Industry standard assay. UMATAC Oil Shale Testing Equipment and Project Development Stages UMATAC Batch Retort Unit Second stage of testing. 2500 g of feed per test. Small scale, quick, and inexpensive. Provides pyrolysis yield sensitivity information and aids in combustion and drying studies. Larger product samples. UMATAC’s ATP60 Pilot System Third stage of testing. Up to 5 t/h feed (60 bbl/d oil sands equivalent feed rate). Designed to gather the final data necessary for design o a commercial plant. Produces representative oil, water, off gas, flue gas, and solids products for analysis. UMATAC Industrial Processes A company of Polysius Industry standard assay. An ATP Technology Pilot Program for Jordan Energy and Mining Ltd. Bulk sample site selection (JEML). Sample collection & crushing (JEML). Sample analysis & scoping studies. ATP60 scoping test. ATP60 performance runs & bulk sample collection. Mass & energy balances & reporting. 3 rd party testing (eg. hydrotreating). Larger product samples. solids products for analysis. Bulk Sample Excavation, Al Lajjun, Jordan Photograph Courtesy of Marston Canada Ltd. Scoping Study - Ore Sample Variability Bulk Sample Collection and Scoping Studies Excavation Depth (m) Free Moisture Content or MFA Yield Sample Variation vs. Depth of Excavation Free H2O Retort H2O C4+ Yield CO/CO2 C3- Yield Coke Yield cess (ATP) Technology ram for Jordan Oil Shales ATP60 Performance Tests and Bulk Oil Sample Collection Oil Recovery System m . of , . Distillations and FBP Monitoring of Two performance tests with bulk oil collection and comprehensive flue gas testing were done. The bulk oil sample met hydrotreating licensor specifications. In-House Oil Analysis Laboratory True Boiling Point - °C Hydrocarbon Products Distillation Stripped Off Gas Gas Naphtha Overhead Oil Fractionator Oil Bottom Oil 400 410 420 430 440 450 460 470 480 490 500 510 520 03:00 06:00 09:00 12:00 15:00 18:00 21:00 00:00 03:00 06:00 09:00 12:00 15:00 True Boiling Point , °C Time Heavy Oil Product 95%End-Point Monitoring Barrel Collection Times Steady State Window B.Oil L.Oil H.Oil Bulk Oil Sample . Testing Results 500 tonne bulk ore sample. No operational problems. Hydrocarbon yield verified & consistent with previous testing. Product oils characterized. All sub-streams measured and analyzed. Flue gas emissions identified and quantified, CO 2 emission reduction opportunity identified. Distillations and FBP Monitoring of Oil Product Third Party Pilot Testing and Analysis Boiling Point Fractions Prior to Hydrotreating Boiling Point Fractions After Pilot Hydrotreating - Naphtha, Jet/Kero, Diesel, Gas Oil, Light Oil - Hydrotreating tests confirmed high sulphur Jordan shale oil can be hydrotreated using conventional, but severe, hydrotreating technologies. Environmental and geotechnical analysis of spent shale. Engineering Studies Feasibility study completed in 2009. ATP60 test results available for front end engineering (FEED) and detailed engineering work in 2010/2011. % Distilled

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Page 1: UMATAC Industrial Processes The Alberta Taciuk Process (ATP

The Alberta Taciuk Process (ATP) TechnologyATP Technology Pilot Program for Jordan Oil Shales

Modified Fischer Assay (MFA)• First stage of testing.• 100 g of feed per test.• Small scale, quick, and

inexpensive.• Provides pyrolysis yield

characterization andpreliminary ore gradeassessment.

• Industry standard assay.

UMATAC Oil Shale Testing Equipment and Project Development Stages

UMATAC Batch Retort Unit• Second stage of testing.• 2500 g of feed per test.• Small scale, quick, and

inexpensive.• Provides pyrolysis yield

sensitivity information andaids in combustion anddrying studies.

• Larger product samples.

UMATAC’s ATP60 Pilot System• Third stage of testing.• Up to 5 t/h feed (60 bbl/d oil

sands equivalent feed rate).• Designed to gather the final

data necessary for design ofa commercial plant.

• Produces representative oil,water, off gas, flue gas, andsolids products for analysis.

UMATAC Industrial ProcessesA company of Polysius

• Industry standard assay.An ATP Technology Pilot Program for Jordan Energy and Mining Ltd.

• Bulk sample site selection (JEML).• Sample collection & crushing (JEML).• Sample analysis & scoping studies.• ATP60 scoping test.

• ATP60 performance runs & bulk samplecollection.

• Mass & energy balances & reporting.• 3rd party testing (eg. hydrotreating).

• Larger product samples. solids products for analysis.

Bulk Sample Excavation, Al Lajjun, Jordan

Phot

ogra

phC

ourt

esy

ofM

arst

onC

anad

aLt

d.

Scoping Study - Ore Sample Variability

Bulk Sample Collection and Scoping Studies

Exc

avat

ion

Dep

th (m

)

Free Moisture Content or MFA Yield

Sample Variation vs. Depth of ExcavationFree H2ORetort H2OC4+ YieldCO/CO2C3- YieldCoke Yield

The Alberta Taciuk Process (ATP) TechnologyATP Technology Pilot Program for Jordan Oil Shales

ATP60 Performance Tests and Bulk Oil Sample Collection

Oil Recovery SystemUMATAC’s ATP60 Pilot System

Up to 5 t/h feed (60 bbl/d oilsands equivalent feed rate).Designed to gather the finaldata necessary for design of

Produces representative oil,water, off gas, flue gas, andsolids products for analysis. Distillations and FBP Monitoring of

Two performance testswith bulk oil collection andcomprehensive flue gastesting were done. The

bulk oil sample methydrotreating licensor

specifications.

In-House Oil Analysis Laboratory

True

Boi

ling

Poin

t-°C

Hydrocarbon Products Distillation

Stripped Off GasGas NaphthaOverhead OilFractionator OilBottom Oil

400

410

420

430

440

450

460

470

480

490

500

510

520

03:00 06:00 09:00 12:00 15:00 18:00 21:00 00:00 03:00 06:00 09:00 12:00 15:00

True

Boi

ling

Poin

t ,°C

Time

Heavy Oil Product 95%End-Point Monitoring

Barrel Collection TimesSteady State Window

B.Oil

L.OilH.Oil

Bulk Oil Samplesolids products for analysis.Testing Results

• 500 tonne bulk ore sample.• No operational problems.• Hydrocarbon yield verified &

consistent with previous testing.• Product oils characterized.

• All sub-streams measured andanalyzed.

• Flue gas emissions identified andquantified, CO2 emission reductionopportunity identified.

Distillations and FBP Monitoring ofOil Product

Third Party Pilot Testing and Analysis

Boiling Point Fractions Prior to Hydrotreating

Boiling Point Fractions After Pilot Hydrotreating- Naphtha, Jet/Kero, Diesel, Gas Oil, Light Oil -

• Hydrotreating tests confirmed high sulphurJordan shale oil can be hydrotreated usingconventional, but severe, hydrotreatingtechnologies.

• Environmental and geotechnical analysis ofspent shale.

Engineering Studies• Feasibility study completed in 2009.• ATP60 test results available for front end

engineering (FEED) and detailedengineering work in 2010/2011.

% Distilled