thermal test cycles (updating 15/7/2010) anastasia xydou university of patras 1

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THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

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Page 1: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

THERMAL TEST CYCLES(Updating 15/7/2010)

Anastasia Xydou University of Patras1

Page 2: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Contents :

Manufacturing flow for test disk stracture Naming of disks Classification of RF disks Bonding and Thermal profiles Cleaning procedure Packaging and shipping

2

Page 3: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Machining QC (Ra and flatness measurement )

Cleaning

Heat treatment

QC (Ra and flatness measurement )

Microscopic observations

Bonding (VDL disks)

BakingPackaging andshipping

Main steps of manufacturing flow for samples:

3

Page 4: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Total disks =345(including the reference pieces)

i. 186 RF disks (d=12mm). a) 48 disks

b) 138 disks main steps for the 128 disks:

ii. 99 RF disks (d=80/85 mm).

main steps for the 96 disks :

Machining

Ra and flatness

measurement

Cleaning Heat treatment

Ra and flatness

measurement

Microscopic

observations

bonding (VDL disks) Baking

The rest 3 are the (References)

4

main steps: machining cleaning Heat treatment SEM

machining cleaning Heat treatment

DC sparks

XPS

H2 content baking

The rest 10 are the (References)

Page 5: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

iii. 60 RF elliptical disks

main steps for the 50 disks: Machining Cleaning Heat

treatment ESD

5

The rest 6 are the (References) and the 4 are spare disks

Page 6: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Every single disk has his own name the right sequence for understand its name is:

One example is:

Naming of disks :

Number cleaning method Firm/University Heat treatment Temperature Size

43 _ W C V 082 B

The number of the RF disk.

Cleaning procedure (w/o etching, only solvent)

Firm/University (CERN)

Heat treatment ( V Vacuum)

Temperature (820 °C)

Disks at d=80/85 mm

6

Page 7: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

P S T H 104 W C V B / C P B A 082 S h L Argon at few mbar

SLAC etching

W/O etching (only solvent)

Passivation

PVA TSINGHUA

CERN

BODYCOTESLAC

LISTEMANN

H2 at 1bar

H2 at few mbar

1040 °C

820 °C

Elliptical samples

Disks (d=80/85mm)

All the possible combinations are:

R REFERENCE PIECES (all stay at CERN)

vacuum

7

Page 8: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Production - surface after heat treatment 820 C 820 C 820 C 820 C 1040 C 1040 C 1040 C 1040 C

REFERENCE Vacuum Argon (mbar) HYDROGEN (mbar) H2 (1 bar) Vacuum Argon (mbar) HYDROGEN(mbar) H2 (1 bar)

w/o etch

Passivation

SLAC etch w/o etch

Passivation SLAC etch w/o etch

Passivation SLAC etch w/o etch Passivation SLAC etch

w/o etch

Passivation SLAC etch

w/o etch

Passivation SLAC etch w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

CERN 1 1 1 2 2 2 2 2 2 2 2 2 21Bodycote 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 36

PVA 2 2 2 2 2 2 12

SLAC 2 2 2 2 2 2 12

Tsinghua 2 2 2 2 2 2 12

Listemann 2 2 2 6

d=85/80 mm 1 1 1 4 4 4 4 4 4 2 2 2 4 4 4 4 4 4 4 4 4 4 4 4 6 6 6 99

Launched 30 pcs 85 mm (kugler) - 08.03.2010

SEM 70 pcs 80 mm launched

REFERENCE Vacuum Argon (mbar) HYDROGEN(mbar) H2 (1 bar) Vacuum Argon (mbar) Hydrogen (mbar) H2(1 bar)

w/o etch

Passivation SLAC etch w/o etch

Passivation SLAC etch w/o etch

Passivation SLAC etch w/o etch Passivation SLAC etch

w/o etch

Passivation SLAC etch

w/o etch

Passivation SLAC etch w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

CERN 1 1 1 1 1 1 1 1 1 9

Bodycote 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 18

PVA 1 1 1 1 1 1 6

SLAC 1 1 1 1 1 1 6

Tsinghua 1 1 1 1 1 1 6

Listemann 1 1 1 3

d= 12 mm 2 2 2 2 2 2 1 1 1 2 2 2 2 2 2 2 2 2 2 2 2 3 3 3 48

DC sparks - XPS - H2 content

REFERENCE Vacuum Argon (mbar) HYDROGEN (mbar) H2 (1 bar) Vacuum Argon (mbar) HYDROGEN(mbar) H2(1 bar)

w/o etch

Passivation

SLAC etch w/o etch

Passivation SLAC etch w/o etch

Passivation SLAC etch w/o etch Passivation SLAC etch

w/o etch

Passivation SLAC etch

w/o etch

Passivation SLAC etch w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

CERN 10 4 4 4 4 4 4 4 4 4 46

Bodycote 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 68

SLAC 4 4 4 4 4 4 24

10 8 8 8 4 4 4 4 4 4 4 4 4 8 8 8 8 8 8 4 4 4 4 4 138

d= 12 mm

Vacuum dynamics 200 pcs 12.65 mm launched

REFERENCE Vacuum Argon (mbar) HYDROGEN (mbar) H2 (1 bar) Vacuum Argon (mbar) Hydrogen (mbar) H2 (1 bar)

w/o etch

Passivation

SLAC etch w/o etch

Passivation SLAC etch w/o etch

Passivation SLAC etch w/o etch Passivation SLAC etch

w/o etch

Passivation SLAC etch

w/o etch

Passivation SLAC etch w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

w/o etch

Passivation

SLAC etch

CERN 2 2 2 2 2 2 2 2 2 2 2 2 24

Bodycote 2 2 2 2 2 2 2 2 2 18

SLAC 2 2 2 2 2 4 14

2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 4 56

elliptical samples

Concentrated tables :

8

Page 9: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

CERNVACUUM

820VACUUM

1040ARGON

1040 TOTAL

d=80mm 6 6 6 18

d=12mm 15 15 15 45Elliptical samples 6 6 6 18

TOTAL 27 27 27 81

BODYCOTEVACUUM

820ARGON

820Hydrogen

820 VACUUM

1040ARGON 1040

Hydrogen 1040 TOTAL

140 d=80mm 6 6 6 6 6 6 36

d=12mm 15 15 15 15 15 11 86Elliptical samples 6 6 6 18

TOTAL 21 27 27 21 21 23 140

SLAC H2 1040 H2 820 TOTAL

d=80mm 6 6 12

d=12mm 15 15 30

Elliptical samples 8 6 14TOTAL 29 27 56

TSINGHUA H2 1040 H2 820 TOTAL

d=80mm 6 6 12

d=12mm 3 3 6

TOTAL 9 9 18

PVAARGON

820(20 mbar)Hydrogen

1040 TOTAL

d=80mm 6 6 12

d=12mm 3 3 6

TOTAL 9 9 18

Separated information about each Firm or University :

LISTEMANN H2 1040

d=80mm 6

d=12mm 3

TOTAL 99

HYDROGEN means H2

at a few mbar

Page 10: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

10

FIRM/UNIVERSITY

D=12 mm

D= 80 mm Elliptical disks

TOTAL AMOUNTS OF DISKS (FOR EACH FIRM)

CERN 45 18 18 81

SLAC 30 12 14 56

BODYCOTE 86 36 18 140

TSINGHUA 6 12 ---- 18

PVA 6 12 ---- 18

LISTEMANN 3 6 ---- 9

TOTAL AMOUNTS OF DISKS( FOR EACH SHAPE)

176 96 50322

322+23 RP =345

TOTAL AMOUNT

A table to control the amount of disks:

Page 11: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

9 at CERN

1_WCV082

2_WCV104

3_WCA104

66_PCV082

67_PCV104

68_PCA104

131_SCV082

132_SCV104

133_SCA104

18 at BODYCOTE

16_WBV08217_WBA08218_WBh08219_WBV10420_WBA10421_WBh10481_PBV08282_PBA08283_PBh08284_PBV10485_PBA10486_PBh104

146_SBV082147_SBA082148_SBh082149_SBV104150_SBA104151_SBh104

6 at PVA

46_WPA082

47_WPh104

111_PPA082

112_PPh104

176_SPA082

177_SPh104

6 at SLAC

48_WSH082

49_WSH104

113_PSH082

114_PSH104

178_SSH082

179_SSH104

6 at TSINGHUA

58_WTH082

59_WTH104

123_PTH082

124_PTH104

188_STH082

189_STH104

3 at LISTEMANN

60_WLH104

125_PLH104

190_SLH104

48 RF disks (d=12mm) :

61_WCR

62_WCR

63_WCR

64_WCR

65_WCR

References(taken by Sergio)

11

Page 12: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

128 RF disks (d=12mm) plus 10 references:

36 at CERN

4_WCV0825_WCV0826_WCV0827_WCV0828_WCV1049_WCV104

10_WCV10411_WCV10412_WCA10413_WCA10414_WCA10415_WCA10469_PCV08270_PCV08271_PCV08272_PCV08273_PCV10474_PCV10475_PCV10476_PCV10477_PCA10478_PCA10479_PCA10480_PCA104134_SCV082135_SCV082136_SCV082137_SCV082138_SCV104139_SCV104140_SCV104141_SCV104142_SCA104143_SCA104144_SCA104145_SCA104

24 at SLAC

50_WSH08251_WSH08252_WSH08253_WSH08254_WSH10455_WSH10456_WSH10457_WSH104115_PSH082116_PSH082117_PSH082118_PSH082119_PSH104120_PSH104121_PSH104122_PSH104180_SSH082181_SSH082182_SSH082183_SSH082184_SSH104185_SSH104186_SSH104187_SSH104

68 at BODYCOTE

22_WBV08223_WBV08224_WBV08225_WBV08226_WBA08227_WBA08228_WBA08229_WBA08230_WBh08231_WBh08232_WBh08233_WBh08234_WBV10435_WBV10436_WBV10437_WBV10438_WBA10439_WBA10440_WBA10441_WBA10442_WBh10443_WBh10444_WBh10445_WBh10487_PBV08288_PBV08289_PBV08290_PBV08291_PBA08292_PBA08293_PBA08294_PBA08295_PBh08296_PBh08297_PBh08298_PBh082

99_PBV104100_PBV104101_PBV104102_PBV104103_PBA104104_PBA104105_PBA104106_PBA104152_SBV082153_SBV082154_SBV082155_SBV082156_SBA082157_SBA082158_SBA082159_SBA082160_SBh082161_SBh082162_SBh082163_SBh082164_SBV104165_SBV104166_SBV104167_SBV104168_SBA104169_SBA104170_SBA104171_SBA104172_SBh104173_SBh104174_SBh104175_SBh104

126_PCR

127_PCR

128_PCR

129_PCR

130_PCR

191_PCR

192_PCR

193_PCR

194_PCR

195_PCR

References

12

Page 13: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

18 at CERN

1_WCV082B

2_WCV082B

3_WCV104B

4_WCV104B

5_WCA104B

6_WCA104B

34_PCV082B

35_PCV082B

36_PCV104B

37_PCV104B

38_PCA104B

39_PCA104B

67_SCV082B

68_SCV082B

69_SCV104B

70_SCV104B

71_SCA104B

72_SCA104B

36 at BODYCOTE

7_WBV082B8_WBV082B9_WBA082B

10_WBA082B11_WBh082B12_WBh082B13_WBV104B14_WBV104B15_WBA104B16_WBA104B17_WBh104B18_WBh104B40_PBV082B41_PBV082B42_PBA082B43_PBA082B44_PBh082B45_PBh082B46_PBV104B47_PBV104B48_PBA104B49_PBA104B50_PBh104B51_PBh104B73_SBV082B74_SBV082B75_SBA082B76_SBA082B77_SBh082B78_SBh082B79_SBV104B80_SBV104B81_SBA104B82_SBA104B83_SBh104B84_SBh104B

12 at PVA

19_WPA082B

20_WPA082B

21_WPh104B

22_WPh104B

52_PPA082B

53_PPA082B

54_PPh104B

55_PPh104B

85_SPA082B

86_SPA082B

87_SPh104B

88_SPh104B

12 at SLAC

23_WSH082B

24_WSH082B

25_WSH104B

26_WSH104B

56_PSH082B

57_PSH082B

58_PSH104B

59_PSH104B

89_SSH082B

90_SSH082B

91_SSH104B

92_SSH104B

12 at Tsinghua

27_WTH082B

28_WTH082B

29_WTH104B

30_WTH104B

60_PTH082B

61_PTH082B

62_PTH104B

63_PTH104B

93_STH082B

94_STH082B

95_STH104B

96_STH104B

6 at Listemann

31_WLH104B

32_WLH104B

64_PLH104B

65_PLH104B

97_SLH104B

98_SLH104B

33_WCRB

66_PCRB

99_SCRB

References

96 RF disks (80/85 mm) plus 3 references:

13

Page 14: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

50 RF elliptical samples plus 6 references, plus 4 extra pieces:

18 at CERN

1_WCV082C

2_WCV082C

3_WCV104C

4_WCV104C

5_WCA104C

6_WCA104C

19_PCV082C

20_PCV082C

21_PCV104C

22_PCV104C

23_PCA104C

24_PCA104C

37_SCV082C

38_SCV082C

39_SCV104C

40_SCV104C

41_SCA104C

42_SCA104C

18 at BODYCOTE

7_WBA082C

8_WBA082C

9_WBh082C

10_WBh082C

11_WBh104C

12_WBh104C

25_PBA082C

26_PBA082C

27_PBh082C

28_PBh082C

29_PBh104C

30_PBh104C

43_SBA082C

44_SBA082C

45_SBh082C

46_SBh082C

47_SBh104C

48_SBh104C

14 at SLAC

13_WSH082C

14_WSH082C

15_WSH104C

16_WSH104C

31_PSH082C

32_PSH082C

33_PSH104C

34_PSH104C

49_SSH082C

50_SSH082C

51_SSH104C

52_SSH104C

53_SSH104C

54_SSH104C

17_WCRC

18_WCRC

35_PCRC

36_PCRC

55_SCRC

56_SCRC

References

14

Page 15: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Some difficulties in classification:

Disks 12 mm• W/O etching (Solvents) disks 1-65

1. Disk missing: 12 WCA1042. Two same disks: 3_WCA104 (one of two took the missing’s

name)3. Reference disks taken by Sergio

61_WCR62_WCR63_WCR64_WCR65_WCR

• Passivation disks 66-130– Four disks don’t have classification codes: 107, 108, 109 & 110 (From now on spare disks)

• SLAC etching disks 131-195– Reference disks instead of passivation cleaning had SLAC etching: 191, 192, 193, 194 & 195

• PCR SCR (change of code)

Disks 80/85 mm

• W/O etching (Solvents) disks 1-33– OK!

• Passivation disks 34-66– Disk missing: 63_PTH104B– Replacement disk: 72_SCV104B

• SLAC etching disks 67-99– Disks missing: 70_SCV104B & 72_SCA104B

– Replacement disks: 100 & 10115

Page 16: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Thermal trends for each thermal cycle :

0 100 200 300 400 500 600 7000

300

600

900

1200

2020 20

790 790820

600

820_VACUUM

Time (minutes)

T (°

C)

820 Vacuum

VACUUM BRAZING

FURNACE V1 - BRAZING PALCUSIL5 OR SCP1

Vacuum

.Pumping 90 min - vacuum <9.10-5 mbar

Level of homogenization

Increase 5 °C/min

T°C :790°C +/- 10°C pcs TP : 2H pièce +1H/-0min

Level of Brazing

Increase 2 °C/min

T°C : 820°C MINI pièce TP : 0 min +1/-0 setting

Observation

825°C SET POINT IN FURNACE

Cooling

Up to 600°C pcs +/-50°C

Cooling turbine -5 PSI under argon

Process Time(min)(1)→(2) .Pumping 90 min - vacuum <9.10-5 mbar, 20C 90(2)→(3) Increase 5 °C/min Up to 790 C 160 (3)→(4) 2H piece +1H/-0min, 790 C 120(4)→(5) Increase 2 °C/min up to 820°C 15(5)→(6) Cooling up to 600°C 60(6)→(7) Cooling turbine -5 PSI under argon (20C) 215

5°C/min 300°C/60 min600°C/120min 790°C/160min

2°C/min 20°C/10min 30°C/15min

4°C/min240°C/60min

16

Page 17: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

820_PPArgon

0 100 200 300 400 500 600 7000

300

600

900

1200

2020 20

790 790820

600

820_PPArgon

Time (minutes)

T (°

C)

VACUUM BRAZINGFURNACE V1 - BRAZING PALCUSIL5 OR SCP1

Vacuum

.Pumping 90 min - vacuum <9.10-5 mbar

Put in PPArgon - 2400l/h - 10mbar

Level of homogenization

Increase 5 °C/min

T°C :790°C +/- 10°C pcs TP : 2H pièce +1H/-0min

Level of Brazing

Increase 2 °C/min

T°C : 820°C MINI pièce TP : 0 min +1/-0 setting

Observation

825°C SET POINT IN FURNACE

Cooling

Up to 600°C pcs +/-50°C

Cooling turbine -5 PSI

Process Time(min)(1)→(2) .Pumping 90 min - vacuum <9.10-5 mbar (20C),Put in PPArgon-2400l/h-10mbar 90(2)→(3) Increase 5 °C/min Up to 790 C 160(3)→(4) 2H pièce +1H/-0min,790 C 120(4)→(5) Increase 2 °C/min up to 820°C 15(5)→(6) Cooling up to 600°C 60(6)→(7) Cooling turbine -5 PSI (20C) 215

5°C/min 300°C/60 min600°C/120min 790°C/160min

2°C/min 20°C/10min 30°C/15min

4°C/min240°C/60min

17

Page 18: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

1040_H2(both for 10mbar and 1bar )

0 100 200 300 400 500 600 7000

300

600

900

1200

2020 20

1040 1040

800

1040_H2

Time (minutes)

T (°

C)

VACUUM BRAZINGFURNACE V1

Vacuum

.Pumping 90 min - vacuum <9.10-5 mbar

Under PPH2 – 10mbar – 2400 L/H

Increase 5 °C/min

T°C :1040°C +/- 10°C TP: 1H30 pièce +/-10min

SET POINT IN FURNACE 1043°C

Reduction 4 °C/min up to 800°C FURNACE

T°C : 850°C +0/-20°C FURNACE at 800°C

Transition in high Vacuum

Cooling

Cooling turbine -5 PSI

Process Time(min)(1)→(2) .Pumping 90 min - vacuum <9.10-5 mbar 90(2)→(3) Increase 5 °C/min Up to 1040 C 210(3)→(4) 1H30 pièce +/-10min,to 1040 C 90(4)→(5) Reduction 4 °C/min up to 800°C 60(5)→(6) Cooling turbine -5 PSI 210

5°C/min 300°C/60 min900°C/180min 1040°C/210min

4°C/min240°C/60min

18

Page 19: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Compulsory changes according to the firms-universities offers :

After contacting with SLAC and Tsinghua, it was compulsory for the main schedule to be changed to the beside heat treatment processes. Both of them, couldn’t run at 10 mbar Hydrogen pressure. ONLY at 1bar.

Because of the past bad experiences at PVA with Argon partial pressure processes at about 5 mbar (due to plasma formation and burning of the heating insert), proposed to run at the 20 mbar pressure for the Argon process AVAILABLE OFFER.

AVAILABLE OFFER

AWAITING OFFERFOR FREE (in the framework of the collaboration)

19

LISTEMANN H2 1040

d=80mm 6

d=12mm 3

TOTAL 9

PVAARGON

820(20 mbar)Hydrogen

1040 TOTAL

d=80mm 6 6 12

d=12mm 3 3 6

TOTAL 9 9 18

SLAC H2 1040 H2 820 TOTAL

d=80mm 6 6 12

d=12mm 15 15 30

Elliptical samples 8 6 14TOTAL 29 27 56

TSINGHUA H2 1040 H2 820 TOTAL

d=80mm 6 6 12

d=12mm 3 3 6

TOTAL 9 9 18

Page 20: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

CERNVACUUM

820VACUUM

1040ARGON

1040 TOTAL

d=80mm 6 6 6 18

d=12mm 15 15 15 45

Elliptical samples 6 6 6 18

TOTAL 27 27 27 81

20

BODYCOTEVACUUM

820ARGON

820Hydrogen

820 VACUUM

1040ARGON 1040

Hydrogen 1040 TOTAL

d=80mm 6 6 6 6 6 6 36d=12mm 15 15 15 15 15 11 86Elliptical samples 6 6 6 18

TOTAL 21 27 27 21 21 23 140

AVAILABLE OFFER : 500 (vacuum) or1000 (Argon) CHF per cycle.At total = 2000 CHF

AVAILABLE OFFER : All the samples must be transferred together, in order to be used together and only for once to the heat treatment cycle of the cleaning of furnace-tool and before each series. Due to the difficulties in the stabilization at 10 mbar, it must be mentioned that the Argon pressure, will be at 5 mbar. The TOTAL OFFER rises to 8.500 € .

Page 21: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

Drilling (20-22/4) d=80/85mm

Preparation before the drilling.

The drilling of the RF-disks (opening hole at least d=3mm). Compulsory procedure before the cleaning due to the special clips which are used to handle the disks during the cleaning process

21

Page 22: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

The two views of the two different RF-disks (d=12mm and d=80mm). As it is visible, each disk has a special number on the one side (the other is for the thermal tests.)

A try for the RF-disks, to be categorized to three teams according to the three cleaning procedures. Each disk is installed to a special small bag, according to the cleaning method.

Classification-Packaging before cleaning

22

Page 23: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

CLEANING

W/O etching Passivation SLAC etching TOTAL

d=80mm 33 33 33 99

d=12mm 60 66 60 186

Elliptical samples 18 18 20 56

TOTAL 111 117 113 341

Cleaning procedure :

All the RF disks after the installation to the clean room (after received from Kugler) Classified to special plastics bags (each bag has a special label with a special number) Collected in short teams according to the below schedule and transferred to the

Surface treatments workshop, for the cleaning step.

After the cleaning procedure and the agreement with the firms/universities, all the RF disks would be transferred for the heat treatment procedure, in order to get simulated to each thermal cycle.

23

341

Page 24: THERMAL TEST CYCLES (Updating 15/7/2010) Anastasia Xydou University of Patras 1

DEVIS N/réf. VS100309-01

Villaz, le 09/03/10     A l’attention de : Monsieur LEBET Serge  V/ réf. DP/ Sté : CERN    Tél : 00 41 22 767 69 56  Affaire suivie par : Raymond SAEZ   Fax :        

Madame, Monsieur,

Nous vous remercions de votre demande de prix ci-dessus référencée et vous indiquons nos conditions pour le traitementde vos pièces :

DESIGNATION : ESSAI BONDING/BRASAGE TEST SURFACE Poids Unit.= de dim. :

MATIERE : CUIVRE CARACTERISTIQUES A OBTENIR :

TRAITEMENT PROPOSE QTEPoids (en

Kg ) *Unité Prix en Euros HT Mini de TTH HT

                 REALISATION DE DIVERS CYCLE THERMIQUE AVEC ECHANTILLON POUR TEST DE SURFACE SUR FOUR V1 COMPRENANT :           - HEAT TREATEMENT OF CLEANING FOR FURNACE AND TOOL BEFORE EACH SERIES 1   FORFAIT 1,000.00 €   - 1 CYCLE 820°C - VACUUM   1   FORFAIT 1,500.00 €   - 1 CYCLE 820°C - PP ARGON   1   FORFAIT 1,500.00 €   - 1 CYCLE 1040°C - VACUUM       1   FORFAIT 1,500.00 €   - 1 CYCLE 1040°C - PP ARGON       1   FORFAIT 1,500.00 €   - 1 CYCLE 1040°C - PP H2   1   FORFAIT 1,500.00 €   - EMBALLAGE SOUS AZOTE                                 P= Pièce - F= Forfait - K= Kilo - C=Cent - M=Mille - Fe=Fournée * poids calculé à vérifier  Le devis a été réalisé selon vos exigences mentionnées sur notre devis, toute exigence complémentaire fera l'objet d'une analyse et d'un éventuel avenant.

Offre basée sur une Quantité totale de pièces.Observations:

Impératif : joindre une copie de ce devis à votre commande ou en rappeler la référence. MerciToute commande reçue sans numéro de devis sera chiffrée au tarif approprié.

Traitement réalisé en notre usine de Villaz :Votre contact :Monsieur SIBUE Vincent 04 50 60 23 60

VALIDITE : 3 MOIS P.V. ou CERTIFICAT DE CONFORMITE : 25,00 € HT DIAGRAMME : 38,00 € HTTRANSPORT A / R : EN SUS CONDITIONS DE REGLEMENT : 30 jours nets

CONTRIBUTION A LA LUTTE POUR LA DEFENSE DE L'ENVIRONNEMENT DURABLE : 0,85% CONDITIONNEMENT : 2% TAXE CETIM : 0,1 %

FACTURATION HEBDOMADAIRE Prix remis sous réserve d'essais, sur présérie significative, pour validation. La garantie de certaines caractéristiques peut nécessiter un contrôle destructif. Le redressage et la protection sont facturés en sus au temps passé, sauf cotation précisée. CONDITIONS GENERALES DE VENTES : Ce devis est accompagné de nos Conditions Générales de Vente en page 2 Restant à votre disposition, nous vous prions d'agréer, Madame, Monsieur, nos salutations distinguées.

Raymond SAEZTél : 04 42 32 76 51 - Portable : 06 74 44 79 67 - e-mail : [email protected]

Ingénieur d'affaires en Brasage et Soudage FE CO XX 03.XX IM 01 Ind 8

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AKNOWLEDGEMENTS to :

Serge LebetThodoros KatopodisMargarita Saifoulina Maria FilippovaAlexandre SamoshkinGermana RiddoneNick Gazis

Thank you for your attention!

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