test results units mql by analytical df date / time …...lab no : delta water non-ozonated sampled:...
TRANSCRIPT
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REPORT OF ANALYSISReport Number :
Project Information :
TN 38104
17-257-0252
21146
Delta Water PBC dba/Delta Water
1400 Union Ave
Mr. Jereme Cavallo
Memphis
Analytical Testing
Report Date :
Received :
09/21/2017
9/14/2017
Sample ID :
Lab No :
Sampled:Delta Water Non-Ozonated
92613 Matrix:
9/14/2017 11:15
Aqueous
Test Results Units MQL By AnalyticalMethod
Date / TimeAnalyzed
DF
<1 MPN/100mL 1Total Coliform 1 09/14/17 14:10 9223B-2004SBA
491 µS/cm 0.010Conductivity 1 09/15/17 09:05 2510B-2011SBA
<1 MPN/100mL 1E-coli 1 09/14/17 14:10 9223B-2004SBA
2.89 mg/L 0.100Nitrate (NO3-N) 1 09/14/17 13:45 EPA-300.0BKN
7.8 s.u.pH 1 09/14/17 15:35 4500H+B-2011TSP
314 mg/L 7.00Total Dissolved Solids 1 09/15/17 09:05 2510B-2011SBA
55.3 mg/L 0.100Total Calcium 1 09/20/17 23:39 EPA-200.7CCR
<0.005 mg/L 0.005Total Copper 1 09/20/17 23:39 EPA-200.7CCR
202 mg/L 0.100Hardness as CaCO3(SM-2340B) 1 09/20/17 23:39 EPA-200.7
<0.100 mg/L 0.100Total Iron 1 09/20/17 23:39 EPA-200.7CCR
<0.006 mg/L 0.006Total Lead 1 09/20/17 23:39 EPA-200.7CCR
15.6 mg/L 0.100Total Magnesium 1 09/20/17 23:39 EPA-200.7CCR
Qualifiers/
DefinitionsMethod Quantitation LimitMQLDilution FactorDF
Page 2 of 5
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Test Results Units MQL By AnalyticalMethod
Date / TimeAnalyzed
DF
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Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. !"#$#%#� &'()*(������+,-./.#0#� ����&('(1*� � 2!�34+!5� &'6(171� � 89:#/� ��������&81(')('17(�11�6� !;<#0/#/� &77�(6*(�=.//.//.>>.�� ?#".@,;0.#� ����&AB('� � 3?� &'1*�������������������������� C<"#D,%#� ��������&BE11���������������������������� 2.;F.0.#� &((1(6�G90H-I<J� &B((')� 89009//99�����&83(A(A)� 45!������������ &83(((1A���������������� G90H-I<J�KL8���&'1�� ������������������ � �
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12/20/2016 Delta Water PBC dba/Delta Water Mr. Jereme Cavallo 1400 Union Ave Memphis, TN, 38104 Ref: Analytical Testing
Lab Report Number: 16-333-0328 Client Project Description: Analysis Required for Source Approval
Dear Mr. Jereme Cavallo: Waypoint Analytical, Inc. received sample(s) on 11/28/2016 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Andy Parrish Project Manager
Page 1 of 39
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Page 3 of 39
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Test Results Units MQL By AnalyticalMethod
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Page 4 of 39
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Page 5 of 39
#=CL#
December 20, 2016
LIMS USE: FR - PROJECT MANAGER
LIMS OBJECT ID: 35279584
35279584Project:Pace Project No.:
RE:
Project ManagerWaypoint2790 Whitten RoadMemphis, TN 38133
16-333-0328: EXP 3133
Dear Project Manager:Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sakina [email protected] Manager
Enclosures
cc: Accounts Payable, Waypoint
Mr. Nathan A. Pera, Waypoint
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
Page 1 of 32
Page 6 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601L-A-B DOD-ELAP Accreditation #: L2417Alabama Certification #: 41590Arizona Certification #: AZ0734Arkansas CertificationCalifornia Certification #: 04222CAColorado CertificationConnecticut Certification #: PH-0694Delaware CertificationFlorida/TNI Certification #: E87683Georgia Certification #: C040Guam CertificationHawaii CertificationIdaho CertificationIllinois CertificationIndiana CertificationIowa Certification #: 391Kansas/TNI Certification #: E-10358Kentucky Certification #: 90133Louisiana DHH/TNI Certification #: LA140008Louisiana DEQ/TNI Certification #: 4086Maine Certification #: PA00091Maryland Certification #: 308Massachusetts Certification #: M-PA1457Michigan/PADEP CertificationMissouri Certification #: 235
Montana Certification #: Cert 0082Nebraska Certification #: NE-05-29-14Nevada Certification #: PA014572015-1New Hampshire/TNI Certification #: 2976New Jersey/TNI Certification #: PA 051New Mexico Certification #: PA01457New York/TNI Certification #: 10888North Carolina Certification #: 42706North Dakota Certification #: R-190Oregon/TNI Certification #: PA200002Pennsylvania/TNI Certification #: 65-00282Puerto Rico Certification #: PA01457Rhode Island Certification #: 65-00282South Dakota CertificationTennessee Certification #: TN2867Texas/TNI Certification #: T104704188-14-8Utah/TNI Certification #: PA014572015-5USDA Soil Permit #: P330-14-00213Vermont Dept. of Health: ID# VT-0282Virgin Island/PADEP CertificationVirginia/VELAP Certification #: 460198Washington Certification #: C868West Virginia DEP Certification #: 143West Virginia DHHR Certification #: 9964CWisconsin CertificationWyoming Certification #: 8TMS-L
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174Alabama Certification #: 41320Connecticut Certification #: PH-0216Delaware Certification: FL NELAC ReciprocityFlorida Certification #: E83079Georgia Certification #: 955Guam Certification: FL NELAC ReciprocityHawaii Certification: FL NELAC ReciprocityIllinois Certification #: 200068Indiana Certification: FL NELAC ReciprocityKansas Certification #: E-10383Louisiana Certification #: FL NELAC ReciprocityLouisiana Environmental Certificate #: 05007Maryland Certification: #346Michigan Certification #: 9911Mississippi Certification: FL NELAC ReciprocityMissouri Certification #: 236Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14Nevada Certification: FL NELAC ReciprocityNew York Certification #: 11608North Carolina Environmental Certificate #: 667North Carolina Certification #: 12710Oklahoma Certification #: D9947Pennsylvania Certification #: 68-00547Puerto Rico Certification #: FL01264South Carolina Certification: #96042001Tennessee Certification #: TN02974Texas Certification: FL NELAC ReciprocityUS Virgin Islands Certification: FL NELAC ReciprocityVirginia Environmental Certification #: 460165Wyoming Certification: FL NELAC ReciprocityWest Virginia Certification #: 9962CWisconsin Certification #: 399079670Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 32
Page 7 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Lab ID Sample ID Matrix Date Collected Date Received
35279584001 16-333-0328 Water 11/28/16 10:40 11/29/16 10:20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 32
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
35279584001 16-333-0328 EPA 504.1 2 PASI-OSMH
EPA 508.1 21 PASI-OJTJ
EPA 552.2 7 PASI-OSMH
EPA 524.2 49 PASI-OJLR
SM7500RnB-07 1 PASI-PANJV
EPA 900.0 1 PASI-PANEG
EPA 903.1 1 PASI-PAACM
EPA 904.0 1 PASI-PAJLW
ASTM D5811-95 1 PASI-PALAL
EPA 906.0 1 PASI-PAWRR
ASTM D5174-97 1 PASI-PARMK
EPA 420.4 1 PASI-OTK1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 32
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
35279584001 16-333-0328
Radon 282.5 ±73.6 (71.9)
C:NA T:NA
pCi/L 12/02/16 21:55 1pSM7500RnB-07
Gross Alpha 1.64U ±0.905
(1.64) C:NAT:NA
pCi/L 12/06/16 21:16EPA 900.0
Radium-226 0.584U ±0.350
(0.584)C:NA T:92%
pCi/L 12/15/16 10:27EPA 903.1
Radium-228 1.04U ±0.545(1.04)
C:68%T:84%
pCi/L 12/16/16 11:35EPA 904.0
Strontium-90 0.465U ±0.238
(0.465)C:97% T:NA
pCi/L 12/08/16 20:17 N2ASTM D5811-95
Tritium -49.9 ± 138(251) C:NA
T:NA
pCi/L 12/09/16 17:32EPA 906.0
Total Uranium 0.193U ±0.005
(0.193)C:NA T:NA
ug/L 12/19/16 16:04ASTM D5174-97
Phenolics, Total Recoverable 0.018 mg/L 12/15/16 14:490.010EPA 420.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 5 of 32
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Sample: 16-333-0328 Lab ID: 35279584001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Comments: • Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504.1 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane 0.0047U ug/L 12/06/16 04:38 96-12-812/05/16 17:040.019 0.0047 1
1,2-Dibromoethane (EDB) 0.0071U ug/L 12/06/16 04:38 106-93-412/05/16 17:040.0095 0.0071 1
Analytical Method: EPA 508.1 Preparation Method: EPA 508.1508.1 GCS Pesticides
Alachlor 0.034U ug/L 12/05/16 17:08 15972-60-811/30/16 10:150.19 0.034 1
Atrazine 0.061U ug/L 12/05/16 17:08 1912-24-911/30/16 10:150.096 0.061 1
gamma-BHC (Lindane) 0.0029U ug/L 12/05/16 17:08 58-89-911/30/16 10:150.019 0.0029 1
Chlordane (Technical) 0.045U ug/L 12/05/16 17:08 57-74-911/30/16 10:150.19 0.045 1
Endrin 0.0067U ug/L 12/05/16 17:08 72-20-811/30/16 10:150.0096 0.0067 1
Heptachlor 0.012U ug/L 12/05/16 17:08 76-44-811/30/16 10:150.038 0.012 1
Heptachlor epoxide 0.0029U ug/L 12/05/16 17:08 1024-57-311/30/16 10:150.019 0.0029 1
Hexachlorobenzene 0.018U ug/L 12/05/16 17:08 118-74-1 L311/30/16 10:150.096 0.018 1
Hexachlorocyclopentadiene 0.031U ug/L 12/01/16 17:28 77-47-4 L311/30/16 10:150.096 0.031 1
Methoxychlor 0.049U ug/L 12/05/16 17:08 72-43-511/30/16 10:150.096 0.049 1
PCB-1016 (Aroclor 1016) 0.077U ug/L 12/05/16 17:08 12674-11-211/30/16 10:150.096 0.077 1
PCB-1221 (Aroclor 1221) 0.028U ug/L 12/05/16 17:08 11104-28-211/30/16 10:150.096 0.028 1
PCB-1232 (Aroclor 1232) 0.028U ug/L 12/05/16 17:08 11141-16-511/30/16 10:150.096 0.028 1
PCB-1242 (Aroclor 1242) 0.049U ug/L 12/05/16 17:08 53469-21-911/30/16 10:150.096 0.049 1
PCB-1248 (Aroclor 1248) 0.060U ug/L 12/05/16 17:08 12672-29-611/30/16 10:150.096 0.060 1
PCB-1254 (Aroclor 1254) 0.022U ug/L 12/05/16 17:08 11097-69-111/30/16 10:150.096 0.022 1
PCB-1260 (Aroclor 1260) 0.063U ug/L 12/05/16 17:08 11096-82-511/30/16 10:150.096 0.063 1
PCB, Total 0.077U ug/L 12/05/16 17:08 1336-36-311/30/16 10:150.096 0.077 1
Simazine 0.066U ug/L 12/05/16 17:08 122-34-911/30/16 10:150.067 0.066 1
Toxaphene 0.58U ug/L 12/05/16 17:08 8001-35-211/30/16 10:150.96 0.58 1SurrogatesDecachlorobiphenyl (S) 56 % 12/05/16 17:08 2051-24-3 S511/30/16 10:1570-130 1
Analytical Method: EPA 552.2 Preparation Method: EPA 552.2552.2 Haloacetic Acids
Dibromoacetic Acid 0.00037U mg/L 12/02/16 14:49 631-64-111/30/16 11:250.0010 0.00037 1
Dichloroacetic Acid 0.00037U mg/L 12/02/16 14:49 79-43-611/30/16 11:250.0010 0.00037 1
Haloacetic Acids (Total) 0.00037U mg/L 12/02/16 14:4911/30/16 11:250.0010 0.00037 1
Monobromoacetic Acid 0.00037U mg/L 12/02/16 14:49 79-08-311/30/16 11:250.0010 0.00037 1
Monochloroacetic Acid 0.00037U mg/L 12/02/16 14:49 79-11-811/30/16 11:250.0010 0.00037 1
Trichloroacetic Acid 0.00037U mg/L 12/02/16 14:49 76-03-911/30/16 11:250.0010 0.00037 1Surrogates2,3-Dibromopropanoic Acid (S) 102 % 12/02/16 14:49 600-05-511/30/16 11:2570-130 1
Analytical Method: EPA 524.2524.2 MSV
Benzene 0.25U ug/L 12/09/16 17:00 71-43-20.50 0.25 1
Bromobenzene 0.25U ug/L 12/09/16 17:00 108-86-10.50 0.25 1
Bromodichloromethane 0.25U ug/L 12/09/16 17:00 75-27-41.0 0.25 1
Bromoform 0.25U ug/L 12/09/16 17:00 75-25-21.0 0.25 1
Bromomethane 0.25U ug/L 12/09/16 17:00 74-83-90.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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8 East Tower Circle
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(386)672-5668
Page 6 of 32
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Sample: 16-333-0328 Lab ID: 35279584001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Comments: • Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.
Analytical Method: EPA 524.2524.2 MSV
Carbon tetrachloride 0.25U ug/L 12/09/16 17:00 56-23-50.50 0.25 1
Chlorobenzene 0.25U ug/L 12/09/16 17:00 108-90-70.50 0.25 1
Chloroethane 0.28U ug/L 12/09/16 17:00 75-00-3 L30.50 0.28 1
Chloroform 0.25U ug/L 12/09/16 17:00 67-66-31.0 0.25 1
Chloromethane 0.46U ug/L 12/09/16 17:00 74-87-30.50 0.46 1
2-Chlorotoluene 0.25U ug/L 12/09/16 17:00 95-49-80.50 0.25 1
4-Chlorotoluene 0.25U ug/L 12/09/16 17:00 106-43-40.50 0.25 1
Dibromochloromethane 0.25U ug/L 12/09/16 17:00 124-48-11.0 0.25 1
Dibromomethane 0.25U ug/L 12/09/16 17:00 74-95-30.50 0.25 1
1,2-Dichlorobenzene 0.25U ug/L 12/09/16 17:00 95-50-10.50 0.25 1
1,3-Dichlorobenzene 0.25U ug/L 12/09/16 17:00 541-73-10.50 0.25 1
1,4-Dichlorobenzene 0.25U ug/L 12/09/16 17:00 106-46-70.50 0.25 1
Dichlorodifluoromethane 0.49U ug/L 12/09/16 17:00 75-71-8 L30.50 0.49 1
1,1-Dichloroethane 0.25U ug/L 12/09/16 17:00 75-34-30.50 0.25 1
1,2-Dichloroethane 0.25U ug/L 12/09/16 17:00 107-06-20.50 0.25 1
1,1-Dichloroethene 0.25U ug/L 12/09/16 17:00 75-35-40.50 0.25 1
cis-1,2-Dichloroethene 0.25U ug/L 12/09/16 17:00 156-59-20.50 0.25 1
trans-1,2-Dichloroethene 0.25U ug/L 12/09/16 17:00 156-60-50.50 0.25 1
1,2-Dichloropropane 0.25U ug/L 12/09/16 17:00 78-87-50.50 0.25 1
1,3-Dichloropropane 0.25U ug/L 12/09/16 17:00 142-28-90.50 0.25 1
2,2-Dichloropropane 0.25U ug/L 12/09/16 17:00 594-20-70.50 0.25 1
1,1-Dichloropropene 0.25U ug/L 12/09/16 17:00 563-58-60.50 0.25 1
1,3-Dichloropropene 0.25U ug/L 12/09/16 17:00 10061-02-6 N20.50 0.25 1
Ethylbenzene 0.25U ug/L 12/09/16 17:00 100-41-40.50 0.25 1
Methylene Chloride 0.44U ug/L 12/09/16 17:00 75-09-20.50 0.44 1
Methyl-tert-butyl ether 0.25U ug/L 12/09/16 17:00 1634-04-4 L30.50 0.25 1
Styrene 0.25U ug/L 12/09/16 17:00 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane 0.25U ug/L 12/09/16 17:00 630-20-60.50 0.25 1
Tetrachloroethene 0.25U ug/L 12/09/16 17:00 127-18-40.50 0.25 1
Toluene 0.25U ug/L 12/09/16 17:00 108-88-30.50 0.25 1
Total Trihalomethanes (Calc.) 0.25U ug/L 12/09/16 17:001.0 0.25 1
1,2,4-Trichlorobenzene 0.41U ug/L 12/09/16 17:00 120-82-10.50 0.41 1
1,1,1-Trichloroethane 0.25U ug/L 12/09/16 17:00 71-55-60.50 0.25 1
1,1,2-Trichloroethane 0.25U ug/L 12/09/16 17:00 79-00-50.50 0.25 1
Trichloroethene 0.25U ug/L 12/09/16 17:00 79-01-60.50 0.25 1
Trichlorofluoromethane 0.25U ug/L 12/09/16 17:00 75-69-4 L30.50 0.25 1
1,2,3-Trichloropropane 0.43U ug/L 12/09/16 17:00 96-18-40.50 0.43 1
Vinyl chloride 0.39U ug/L 12/09/16 17:00 75-01-40.50 0.39 1
Xylene (Total) 0.25U ug/L 12/09/16 17:00 1330-20-70.50 0.25 1
m&p-Xylene 0.25U ug/L 12/09/16 17:00 179601-23-10.50 0.25 1
o-Xylene 0.25U ug/L 12/09/16 17:00 95-47-60.50 0.25 1Surrogates4-Bromofluorobenzene (S) 86 % 12/09/16 17:00 460-00-470-130 1
Toluene-d8 (S) 96 % 12/09/16 17:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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(386)672-5668
Page 7 of 32
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Sample: 16-333-0328 Lab ID: 35279584001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Comments: • Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.
Analytical Method: EPA 524.2524.2 MSV
Surrogates1,2-Dichloroethane-d4 (S) 111 % 12/09/16 17:00 17060-07-070-130 1
Analytical Method: EPA 420.4420.4 Phenolics, Total
Phenolics, Total Recoverable 0.018 mg/L 12/15/16 14:490.010 0.0050 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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Page 8 of 32
Page 13 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
337540
EPA 524.2
EPA 524.2
524.2 MSV
Associated Lab Samples: 35279584001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1808332
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.25U 0.50 12/09/16 15:320.25
1,1,1-Trichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25
1,1,2-Trichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25
1,1-Dichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25
1,1-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25
1,1-Dichloropropene ug/L 0.25U 0.50 12/09/16 15:320.25
1,2,3-Trichloropropane ug/L 0.43U 0.50 12/09/16 15:320.43
1,2,4-Trichlorobenzene ug/L 0.41U 0.50 12/09/16 15:320.41
1,2-Dichlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25
1,2-Dichloroethane ug/L 0.25U 0.50 12/09/16 15:320.25
1,2-Dichloropropane ug/L 0.25U 0.50 12/09/16 15:320.25
1,3-Dichlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25
1,3-Dichloropropane ug/L 0.25U 0.50 12/09/16 15:320.25
1,3-Dichloropropene ug/L 0.25U 0.50 N212/09/16 15:320.25
1,4-Dichlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25
2,2-Dichloropropane ug/L 0.25U 0.50 12/09/16 15:320.25
2-Chlorotoluene ug/L 0.25U 0.50 12/09/16 15:320.25
4-Chlorotoluene ug/L 0.25U 0.50 12/09/16 15:320.25
Benzene ug/L 0.25U 0.50 12/09/16 15:320.25
Bromobenzene ug/L 0.25U 0.50 12/09/16 15:320.25
Bromodichloromethane ug/L 0.25U 1.0 12/09/16 15:320.25
Bromoform ug/L 0.25U 1.0 12/09/16 15:320.25
Bromomethane ug/L 0.25U 0.50 12/09/16 15:320.25
Carbon tetrachloride ug/L 0.25U 0.50 12/09/16 15:320.25
Chlorobenzene ug/L 0.25U 0.50 12/09/16 15:320.25
Chloroethane ug/L 0.28U 0.50 12/09/16 15:320.28
Chloroform ug/L 0.25U 1.0 12/09/16 15:320.25
Chloromethane ug/L 0.46U 0.50 12/09/16 15:320.46
cis-1,2-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25
Dibromochloromethane ug/L 0.25U 1.0 12/09/16 15:320.25
Dibromomethane ug/L 0.25U 0.50 12/09/16 15:320.25
Dichlorodifluoromethane ug/L 0.49U 0.50 12/09/16 15:320.49
Ethylbenzene ug/L 0.25U 0.50 12/09/16 15:320.25
m&p-Xylene ug/L 0.25U 0.50 12/09/16 15:320.25
Methyl-tert-butyl ether ug/L 0.25U 0.50 12/09/16 15:320.25
Methylene Chloride ug/L 0.44U 0.50 12/09/16 15:320.44
o-Xylene ug/L 0.25U 0.50 12/09/16 15:320.25
Styrene ug/L 0.25U 0.50 12/09/16 15:320.25
Tetrachloroethene ug/L 0.25U 0.50 12/09/16 15:320.25
Toluene ug/L 0.25U 0.50 12/09/16 15:320.25
Total Trihalomethanes (Calc.) ug/L 0.25U 1.0 12/09/16 15:320.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
Page 9 of 32
Page 14 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1808332
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
trans-1,2-Dichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25
Trichloroethene ug/L 0.25U 0.50 12/09/16 15:320.25
Trichlorofluoromethane ug/L 0.25U 0.50 12/09/16 15:320.25
Vinyl chloride ug/L 0.39U 0.50 12/09/16 15:320.39
Xylene (Total) ug/L 0.25U 0.50 12/09/16 15:320.25
1,2-Dichloroethane-d4 (S) % 108 70-130 12/09/16 15:32
4-Bromofluorobenzene (S) % 92 70-130 12/09/16 15:32
Toluene-d8 (S) % 101 70-130 12/09/16 15:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1808333LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1808334
1,1,1,2-Tetrachloroethane ug/L 4.55 89 70-1301015.1 13 40
1,1,1-Trichloroethane ug/L 5.05 101 70-1301035.1 2 40
1,1,2-Trichloroethane ug/L 5.15 102 70-1301125.6 8 40
1,1-Dichloroethane ug/L 4.95 99 70-1301045.2 5 40
1,1-Dichloroethene ug/L 5.85 115 70-1301175.9 2 40
1,1-Dichloropropene ug/L 5.55 109 70-1301115.5 1 40
1,2,3-Trichloropropane ug/L 3.75 75 70-130944.7 23 40
1,2,4-Trichlorobenzene ug/L 5.75 115 70-1301105.5 4 40
1,2-Dichlorobenzene ug/L 4.25 84 70-130874.3 3 40
1,2-Dichloroethane ug/L 5.95 118 70-1301145.7 3 40
1,2-Dichloropropane ug/L 3.95 78 70-130914.5 14 40
1,3-Dichlorobenzene ug/L 4.55 90 70-130984.9 9 40
1,3-Dichloropropane ug/L 4.15 82 70-130994.9 18 40
1,3-Dichloropropene ug/L 8.1 N210 81 70-130818.1 0 40
1,4-Dichlorobenzene ug/L 4.45 87 70-130934.6 6 40
2,2-Dichloropropane ug/L 5.05 100 70-1301105.5 9 40
2-Chlorotoluene ug/L 4.25 83 70-130804.0 5 40
4-Chlorotoluene ug/L 4.15 81 70-130884.4 9 40
Benzene ug/L 5.35 105 70-1301115.6 6 40
Bromobenzene ug/L 4.35 86 70-130834.2 3 40
Bromodichloromethane ug/L 4.65 92 70-130924.6 1 40
Bromoform ug/L 4.05 79 70-130834.2 5 40
Bromomethane ug/L 4.75 93 70-130864.3 8 40
Carbon tetrachloride ug/L 5.65 112 70-1301195.9 6 40
Chlorobenzene ug/L 4.75 95 70-1301055.2 10 40
Chloroethane ug/L 7.4 L05 149 70-1301517.6 2 40
Chloroform ug/L 5.45 108 70-1301055.3 3 40
Chloromethane ug/L 5.15 103 70-130763.8 30 40
cis-1,2-Dichloroethene ug/L 5.55 111 70-1301095.4 2 40
Dibromochloromethane ug/L 4.55 91 70-130824.1 10 40
Dibromomethane ug/L 5.05 100 70-1301085.4 8 40
Dichlorodifluoromethane ug/L 6.6 L05 132 70-1301256.2 5 40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1808333LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1808334
Ethylbenzene ug/L 4.85 96 70-1301015.0 4 40
m&p-Xylene ug/L 9.610 96 70-130969.6 0 40
Methyl-tert-butyl ether ug/L 7.8 L05 157 70-1301698.4 7 40
Methylene Chloride ug/L 5.35 106 70-130934.7 13 40
o-Xylene ug/L 4.65 93 70-130954.8 2 40
Styrene ug/L 4.35 85 70-130814.0 5 40
Tetrachloroethene ug/L 4.45 88 70-130964.8 8 40
Toluene ug/L 5.05 100 70-1301035.1 3 40
Total Trihalomethanes (Calc.) ug/L 18.520 92 70-1309118.2 2 40
trans-1,2-Dichloroethene ug/L 5.55 110 70-1301135.6 3 40
Trichloroethene ug/L 5.25 104 70-1301185.9 12 40
Trichlorofluoromethane ug/L 7.0 L05 139 70-1301487.4 6 40
Vinyl chloride ug/L 5.75 113 70-1301175.9 3 40
Xylene (Total) ug/L 14.215 95 70-1309614.4 1 40
1,2-Dichloroethane-d4 (S) % 109 70-130103
4-Bromofluorobenzene (S) % 102 70-130102
Toluene-d8 (S) % 100 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
336353
EPA 504.1
EPA 504.1
504 EDB DBCP
Associated Lab Samples: 35279584001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1801659
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
1,2-Dibromo-3-chloropropane ug/L 0.0049U 0.020 12/06/16 03:520.0049
1,2-Dibromoethane (EDB) ug/L 0.0075U 0.010 12/06/16 03:520.0075
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1801660LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1801781
1,2-Dibromo-3-chloropropane ug/L 0.20.25 80 70-1301130.28 34 40
1,2-Dibromoethane (EDB) ug/L 0.21.25 84 70-1301130.28 30 40
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1801877MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35279833001
1801878
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromo-3-chloropropane
ug/L .44 121 65-135114 6 40.440.0047U 0.53 0.50
1,2-Dibromoethane (EDB) ug/L .44 135 65-135120 12 40.440.0072U 0.59 0.52
REPORT OF LABORATORY ANALYSIS
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Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
335264
EPA 508.1
EPA 508.1
508 GCS Pesticide
Associated Lab Samples: 35279584001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1795133
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
Alachlor ug/L 0.035U 0.20 12/01/16 06:280.035
Atrazine ug/L 0.063U 0.10 12/01/16 06:280.063
Chlordane (Technical) ug/L 0.047U 0.20 12/01/16 06:280.047
Endrin ug/L 0.0070U 0.010 12/01/16 06:280.0070
gamma-BHC (Lindane) ug/L 0.0030U 0.020 12/01/16 06:280.0030
Heptachlor ug/L 0.012U 0.040 12/01/16 06:280.012
Heptachlor epoxide ug/L 0.0030U 0.020 12/01/16 06:280.0030
Hexachlorobenzene ug/L 0.019U 0.10 12/01/16 06:280.019
Hexachlorocyclopentadiene ug/L 0.032U 0.10 12/01/16 06:280.032
Methoxychlor ug/L 0.051U 0.10 12/01/16 06:280.051
PCB-1016 (Aroclor 1016) ug/L 0.080U 0.10 12/01/16 06:280.080
PCB-1221 (Aroclor 1221) ug/L 0.029U 0.10 12/01/16 06:280.029
PCB-1232 (Aroclor 1232) ug/L 0.029U 0.10 12/01/16 06:280.029
PCB-1242 (Aroclor 1242) ug/L 0.051U 0.10 12/01/16 06:280.051
PCB-1248 (Aroclor 1248) ug/L 0.062U 0.10 12/01/16 06:280.062
PCB-1254 (Aroclor 1254) ug/L 0.023U 0.10 12/01/16 06:280.023
PCB-1260 (Aroclor 1260) ug/L 0.066U 0.10 12/01/16 06:280.066
Simazine ug/L 0.069U 0.070 12/01/16 06:280.069
Toxaphene ug/L 0.61U 1.0 12/01/16 06:280.61
Decachlorobiphenyl (S) % 93 70-130 12/01/16 06:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1795134LABORATORY CONTROL SAMPLE:
LCSSpike
Alachlor ug/L 1.11 112 70-130
Atrazine ug/L 1.51.2 117 70-130
Chlordane (Technical) ug/L 0.047U
Endrin ug/L 0.060.05 119 70-130
gamma-BHC (Lindane) ug/L 0.11.1 113 70-130
Heptachlor ug/L 0.26.2 128 70-130
Heptachlor epoxide ug/L 0.12.1 125 70-130
Hexachlorobenzene ug/L 0.75 L0.5 149 70-130
Hexachlorocyclopentadiene ug/L 0.78 L0.5 156 70-130
Methoxychlor ug/L 0.60.5 121 70-130
PCB-1016 (Aroclor 1016) ug/L 0.080U
PCB-1221 (Aroclor 1221) ug/L 0.029U
PCB-1232 (Aroclor 1232) ug/L 0.029U
PCB-1242 (Aroclor 1242) ug/L 0.051U
PCB-1248 (Aroclor 1248) ug/L 0.062U
PCB-1254 (Aroclor 1254) ug/L 0.023U
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
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Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1795134LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1260 (Aroclor 1260) ug/L 0.066U
Simazine ug/L 1.0.88 114 70-130
Toxaphene ug/L 0.61U
Decachlorobiphenyl (S) % 114 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1795366MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
7555964002
1795367
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alachlor ug/L 2.2 108 65-135109 1 402.2ND 2.4 2.4
Atrazine ug/L 2.8 92 65-13575 20 402.8ND 2.5 2.1
Chlordane (Technical) ug/L 40ND 0.10U 0.10U
Endrin ug/L .11 116 65-135130 12 40.11ND 0.13 0.14
gamma-BHC (Lindane) ug/L .22 104 65-135103 1 40.22ND 0.23 0.23
Heptachlor ug/L .44 114 65-135115 0 40.44ND 0.51 0.51
Heptachlor epoxide ug/L .22 121 65-135122 1 40.22ND 0.27 0.27
Hexachlorobenzene ug/L 1.1 135 65-135131 4 401.1ND 1.5 1.5
Hexachlorocyclopentadiene ug/L 1.1 124 65-135132 7 401.1ND 1.4 1.5
Methoxychlor ug/L 1.1 126 65-135121 4 401.1ND 1.4 1.3
PCB-1016 (Aroclor 1016) ug/L 40ND 0.18U 0.18U
PCB-1221 (Aroclor 1221) ug/L 40ND 0.064U 0.064U
PCB-1232 (Aroclor 1232) ug/L 40ND 0.064U 0.064U
PCB-1242 (Aroclor 1242) ug/L 40ND 0.11U 0.11U
PCB-1248 (Aroclor 1248) ug/L 40ND 0.14U 0.14U
PCB-1254 (Aroclor 1254) ug/L 40ND 0.051U 0.051U
PCB-1260 (Aroclor 1260) ug/L 40ND 0.15U 0.15U
Simazine ug/L 1.9 94 65-13590 4 401.9ND 1.8 1.8
Toxaphene ug/L 40ND 1.4U 1.4U
Decachlorobiphenyl (S) % 101 70-130102 40
REPORT OF LABORATORY ANALYSIS
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Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
335276
EPA 552.2
EPA 552.2
5522 Haloacetic Acids
Associated Lab Samples: 35279584001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1795166
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
Dibromoacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037
Dichloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037
Haloacetic Acids (Total) mg/L 0.00037U 0.0010 12/02/16 09:520.00037
Monobromoacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037
Monochloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037
Trichloroacetic Acid mg/L 0.00037U 0.0010 12/02/16 09:520.00037
2,3-Dibromopropanoic Acid (S) % 95 70-130 12/02/16 09:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1795167LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromoacetic Acid mg/L 0.011.01 107 70-130
Dichloroacetic Acid mg/L 0.010.01 100 70-130
Haloacetic Acids (Total) mg/L 0.050.05 99
Monobromoacetic Acid mg/L 0.0095.01 95 70-130
Monochloroacetic Acid mg/L 0.0092.01 92 70-130
Trichloroacetic Acid mg/L 0.010.01 103 70-130
2,3-Dibromopropanoic Acid (S) % 109 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1795376MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35279528001
1795377
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dibromoacetic Acid mg/L .01 74 70-13074 0 30.015.1 ug/L 0.012 0.013
Dichloroacetic Acid mg/L M1.01 58 70-13056 2 30.012.5 ug/L 0.0083 0.0081
Haloacetic Acids (Total) mg/L .05 73 78 6.058.7 ug/L 0.045 0.048
Monobromoacetic Acid mg/L .01 93 70-13093 0 30.010.37Uug/L
0.0093 0.0093
Monochloroacetic Acid mg/L M1,R1.01 59 70-13088 39 30.010.37Uug/L
0.0059 0.0088
Trichloroacetic Acid mg/L .01 79 70-13080 0 30.011.2 ug/L 0.0091 0.00912,3-Dibromopropanoic Acid(S)
% 75 70-13078
REPORT OF LABORATORY ANALYSIS
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Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1795378MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35279706001
1795379
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dibromoacetic Acid mg/L .01 84 70-13082 2 30.010.37Uug/L
0.0084 0.0082
Dichloroacetic Acid mg/L M1.01 61 70-13060 2 30.013.1 ug/L 0.0092 0.0090
Haloacetic Acids (Total) mg/L .05 77 79 2.0510 ug/L 0.048 0.050
Monobromoacetic Acid mg/L .01 94 70-13096 3 30.010.37Uug/L
0.0094 0.0096
Monochloroacetic Acid mg/L M1.01 68 70-13085 22 30.010.37Uug/L
0.0068 0.0085
Trichloroacetic Acid mg/L .01 78 70-13073 4 30.016.9 ug/L 0.015 0.0142,3-Dibromopropanoic Acid(S)
% 95 70-13094
REPORT OF LABORATORY ANALYSIS
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Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
337822
EPA 420.4
EPA 420.4
420.4 Phenolics
Associated Lab Samples: 35279584001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1810523
Associated Lab Samples: 35279584001
Matrix: Water
AnalyzedMDL
Phenolics, Total Recoverable mg/L 0.0050U 0.010 12/15/16 14:440.0050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1810524LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1816951
Phenolics, Total Recoverable mg/L 0.41.4 102 90-1101000.40 3 20
REPORT OF LABORATORY ANALYSIS
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Page 22 of 39
#=ARR#
ANALYTICAL RESULTS - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Sample: 16-333-0328 Lab ID: 35279584001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water
Parameters Act ± Unc (MDC) Carr Trac Units Analyzed CAS No. Qual
• Split off 500 ml amber un-preserved bottle for Tritium analysis.• Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the samplepreservation requirement of pH <2 for radiochemistry analysis.
Comments:
Method
PWS: Site ID: Sample Type:
Radon 282.5 ± 73.6 (71.9)C:NA T:NA
pCi/L 12/02/16 21:55 10043-92-2 1pSM7500RnB-07
Gross Alpha 1.64U ± 0.905 (1.64)C:NA T:NA
pCi/L 12/06/16 21:16 12587-46-1EPA 900.0
Radium-226 0.584U ± 0.350 (0.584)C:NA T:92%
pCi/L 12/15/16 10:27 13982-63-3EPA 903.1
Radium-228 1.04U ± 0.545 (1.04)C:68% T:84%
pCi/L 12/16/16 11:35 15262-20-1EPA 904.0
Strontium-90 0.465U ± 0.238 (0.465)C:97% T:NA
pCi/L 12/08/16 20:17 10098-97-2 N2ASTM D5811-95
Tritium -49.9 ± 138 (251)C:NA T:NA
pCi/L 12/09/16 17:32 10028-17-8EPA 906.0
Total Uranium 0.193U ± 0.005 (0.193)C:NA T:NA
ug/L 12/19/16 16:04 7440-61-1ASTM D5174-97
REPORT OF LABORATORY ANALYSIS
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Page 23 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242497
EPA 904.0
EPA 904.0
904.0 Radium 228
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1191948
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Radium-228 pCi/L 12/16/16 11:350.0511 ± 0.373 (0.857) C:66% T:81%
REPORT OF LABORATORY ANALYSIS
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Page 24 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242090
SM7500RnB-07
SM7500RnB-07
7500Rn B Radon
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1189744
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Radon pCi/L 12/02/16 21:2223.8 ± 19.9 (32.0) C:NA T:NA
REPORT OF LABORATORY ANALYSIS
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Page 25 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242496
EPA 903.1
EPA 903.1
903.1 Radium-226
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1191947
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Radium-226 pCi/L 12/15/16 10:090.000 ± 0.313 (0.701) C:NA T:95%
REPORT OF LABORATORY ANALYSIS
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Page 21 of 32
Page 26 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242576
ASTM D5811-95
ASTM D5811-95
ASTM D5811 Sr 89/90 Eichrom
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1192327
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Strontium-90 pCi/L N212/08/16 13:290.407 ± 0.612 (1.30) C:96% T:NA
REPORT OF LABORATORY ANALYSIS
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Page 27 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242582
EPA 906.0
EPA 906.0
906.0 Tritium
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1192337
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Tritium pCi/L 12/09/16 16:3082.6 ± 148 (252) C:NA T:NA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
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#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242328
EPA 900.0
EPA 900.0
900.0 Gross Alpha/Beta
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1191351
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Gross Alpha pCi/L 12/07/16 09:29-0.104 ± 0.561 (1.63) C:NA T:NA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
Page 24 of 32
Page 29 of 39
#=QCR#
QUALITY CONTROL - RADIOCHEMISTRY
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
242704
ASTM D5174-97
ASTM D5174-97
D5174.97 Total Uranium KPA
Associated Lab Samples: 35279584001
Parameter UnitsAct ± Unc (MDC) Carr Trac Qualifiers
METHOD BLANK: 1192940
Associated Lab Samples: 35279584001
Matrix: Water
Analyzed
Total Uranium ug/L 12/19/16 15:55-0.011 ± -0.001 (0.193) C:NA T:NA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Act - Activity
Unc - Uncertainty: SDWA = 1.96 sigma count uncertainty, all other matrices = Expanded Uncertainty (95% confidence interval).Gamma Spec = Expanded Uncertainty (95.4% Confidence Interval)
(MDC) - Minimum Detectable Concentration
Trac - Tracer Recovery (%)
Carr - Carrier Recovery (%)
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - Ormond BeachPASI-O
Pace Analytical Services - GreensburgPASI-PA
ANALYTE QUALIFIERS
Sample 35279584001 from this analytical project was analyzed outside of the recommended Radon-222 hold time of fourdays. Results reported are decay corrected to the sample collection date and time supplied by the client.
1p
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples.
L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
35279584
16-333-0328: EXP 3133
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
35279584001 336353 33645616-333-0328 EPA 504.1 EPA 504.1
35279584001 335264 33546916-333-0328 EPA 508.1 EPA 508.1
35279584001 335276 33574616-333-0328 EPA 552.2 EPA 552.2
35279584001 33754016-333-0328 EPA 524.2
35279584001 24209016-333-0328 SM7500RnB-07
35279584001 24232816-333-0328 EPA 900.0
35279584001 24249616-333-0328 EPA 903.1
35279584001 24249716-333-0328 EPA 904.0
35279584001 24257616-333-0328 ASTM D5811-95
35279584001 24258216-333-0328 EPA 906.0
35279584001 24270416-333-0328 ASTM D5174-97
35279584001 33782216-333-0328 EPA 420.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/20/2016 11:20 AM
Pace Analytical Services, LLC
8 East Tower Circle
Ormond Beach, FL 32174
(386)672-5668
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