tensile and coefficient of friction testing of textured ... · dr. quinlan's post-doctoral...

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Tensile and Coefficient of Friction Testing of Textured Socket Specimens Julia Quinlan 1 , Vasanth Subramanian 1 , Jessica Yohay 1 , Gila Baer 1 , Brad Poziembo 2 and Stefania Fatone 1 1 Northwestern University Prosthetics-Orthotics Center and 2 Prosthetic Design Inc. Department of Physical Medicine and Rehabilitation, Northwestern University Prosthetics-Orthotics Center Funding Support This work was supported by the Office of the Assistant Secretary for Health Affairs, through the Neuromusculoskeletal Injuries Research Award under Award No. W81XWH-16-1-0485. Dr. Quinlan's post-doctoral fellowship was supported by the National Institute on Disability, Independent Living and Rehabilitation Research of the U.S. Department of Health and Human Services, Administration for Community Living (grants 90AR5010 and 90AR5031). UTS Results Aim To evaluate the effect of texture on the tensile strength of 3D printed socket samples and friction between socket sample/liner/sock using standardized tests. Specimen Fabrication To obtain samples necessary for standardized testing of UTS and COF, we printed rectangular sockets with flat sides. The flat sides were then cut to obtain flat samples of different textures: A) dumbbells for tensile testing and B) rectangular samples for COF testing. Dumbbell preparation utilized a cutting die (Universal Grip LLC.) attached to a uniaxial hydraulic material testing system (Instron, Norwood, MA) to stamp out specimens with ASTM D638 Type I dimensions. Testing Protocol Tensile testing Five dumbbell specimens per texture were measured using caliper, mounted to the Instron, preloaded to remove unwanted compression, and tested to failure. Rate of tensile loading was set at 5 mm/min per the ASTM D638 standard [2] and load was measured using a tension/compression load cell (1000 lb, MTS, Eden Prairie, MN). COF testing Five COF specimens per texture were secured to the COF table and a calibrated sled wrapped in a piece of liner and nylon sock was dragged across the textured surface. Friction forces were collected with a tension/compression load cell (LRF400, Futek, 2.2 lb, Irvine, CA). The drive speed of the apparatus was set to 180 mm/min per the ASTM D1894 standard [3]. Introduction 3D printing with fused deposition modelling (FDM) [1] results in objects with some texturing due to the deposition of materials layer-by-layer. However, the effect of socket texturing on socket suspension, rotation, fit, and comfort remains unknown. Textured prosthetic sockets may improve suspension by increasing the coefficient of sliding friction (COF) between the socket and liner-clad residual limb when compared to a smooth socket of the same material. However, printing different textures into the socket wall may influence bonding strength between layers, reducing ultimate tensile strength (UTS). Sockets A selection of different texture patterns were programmed and 3D printed using the SQUIRT-Shape System [1]. A smooth thermoformed socket and a SQUIRT-Shape socket with original texturing consisting of horizontal striations approximately 1.2 mm in depth were used as controls. Apparatus Testing utilized a uniaxial hydraulic material testing system (Instron, Norwood, MA). For tensile testing, dumbbells were secured to the Instron using action wedge grips. For COF testing, specimens were secured to a custom COF testing frame. References [1] Rovick J. Automated Fabrication of Sockets for Artificial Limbs. PhD Dissertation, Northwestern University, 1993. [2] ASTM D63814: Standard Test Method for Tensile Properties of Plastics. [3] ASTM D189414: Standard Test Method for Static and Kinetic Coefficients of Friction of Plastic Film and Sheeting. Hypothesis We hypothesized that texture of polypropylene copolymer socket specimens would vary the UTS of the material. We also hypothesized that texture of polypropylene copolymer socket specimens would vary the COF of the material. Significance set at p=0.05 for both hypotheses. Results There was a significant difference in UTS (p<0.0005) based on material texture with all textured samples being significantly weaker than the smooth reference samples (p<0.05). There was a significant difference in COF (p<0.0005) based on material texture, with both static (p<0.000) and kinetic COF (p<0.0005) being significantly different. While some textured samples had a larger static COF than the smooth reference sample, all but one textured sample had a lower kinetic COF. Original SQUIRT-Shape socket fabrication Methods and Results Textured Samples Horizontal line Vertical line Hemisphere Half-hemisphere Horizontal rectangle Vertical rectangle Checkerboard Densely distributed More aggressive (HD) Lightly distributed More subtle (LS) Reference Samples Test Description Tensile COF Smooth Raw Sheet (6mm thick) of Polypropylene Copolymer Tensile only Smooth Thermoformed rectangular socket made from 12 mm thick sheet of Polypropylene Copolymer Tensile COF Original SQUIRT-Shape Socket Textured socket Rectangular shape Width Horizontal Spacing Vertical Spacing Height Horizontal Spacing Depth Cross-sectional view of socket Socket Texture Textured socket Transtibial shape Bottom of the sled Top of the sled Nylon sock Liner Sled Textured COF specimen Dumbbells Stamping out dumbbells with cutting die Mounting holes COF (left) and tensile testing (right) set up Socket Sample Ultimate Tensile Strength [MPa] Static COF [N/N] Kinetic COF [N/N] Smooth Raw Sheet 24.48 0.352 0.341 Smooth Thermoformed 24.38 - - Original SQUIRT-Shape 15.46 0.363 0.304 14 Textured Samples 3.97 - 14.32 0.271 - 0.422 0.208 – 0.332 Original SQUIRT -Shape Smooth raw sheet Smooth thermoformed Data analysis UTS and static and kinetic COF were compared to reference samples that included a smooth sheet of the same polypropylene copolymer. UTS was assessed using a one-way ANOVA, while COF was assessed using a one-way MANOVA. Discussion Tensile testing revealed a wide range of material strengths that depended on the distribution density of texturing as well as on the type of texture pattern. COF testing demonstrated that different textures influence friction properties between the socket, liner and nylon sock, and can be increased compared to the original SQUIRT-Shape socket. Conclusions These results provide an initial understanding of the effect of texturing on material properties, but further cyclic and static failure testing and test set-ups that mimic real-world socket conditions are needed. COF Results COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] Smooth raw sheet COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] COF [N/N] Time [s] Original SQUIRT -Shape

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Page 1: Tensile and Coefficient of Friction Testing of Textured ... · Dr. Quinlan's post-doctoral fellowship was supported by the National Institute on Disability, Independent Living and

Tensile and Coefficient of Friction Testing of Textured Socket Specimens Julia Quinlan1, Vasanth Subramanian1, Jessica Yohay1, Gila Baer1, Brad Poziembo2 and Stefania Fatone1

1Northwestern University Prosthetics-Orthotics Center and 2Prosthetic Design Inc.

Department of Physical Medicine and Rehabilitation, Northwestern University Prosthetics-Orthotics Center

Funding Support This work was supported by the Office of theAssistant Secretary for Health Affairs, through the NeuromusculoskeletalInjuries Research Award under Award No. W81XWH-16-1-0485. Dr.Quinlan's post-doctoral fellowship was supported by the National Instituteon Disability, Independent Living and Rehabilitation Research of the U.S.Department of Health and Human Services, Administration for CommunityLiving (grants 90AR5010 and 90AR5031).

UTS Results

Aim To evaluate the effect of texture on the tensile strength of3D printed socket samples and friction between socketsample/liner/sock using standardized tests.

Specimen Fabrication To obtain samples necessary for standardized testing of UTS and COF,we printed rectangular sockets with flat sides. The flat sides were then cut to obtain flat samples ofdifferent textures: A) dumbbells for tensile testing and B) rectangular samples for COF testing.Dumbbell preparation utilized a cutting die (Universal Grip LLC.) attached to a uniaxial hydraulicmaterial testing system (Instron, Norwood, MA) to stamp out specimens with ASTM D638 Type Idimensions.

Testing ProtocolTensile testing Five dumbbell specimens per texture were measuredusing caliper, mounted to the Instron, preloaded to remove unwantedcompression, and tested to failure. Rate of tensile loading was set at 5mm/min per the ASTM D638 standard [2] and load was measured using atension/compression load cell (1000 lb, MTS, Eden Prairie, MN).COF testing Five COF specimens per texture were secured to the COFtable and a calibrated sled wrapped in a piece of liner and nylon sock wasdragged across the textured surface. Friction forces were collected with atension/compression load cell (LRF400, Futek, 2.2 lb, Irvine, CA). The drivespeed of the apparatus was set to 180 mm/min per the ASTM D1894standard [3].

Introduction 3D printing with fused deposition modelling (FDM) [1]results in objects with some texturing due to the deposition of materialslayer-by-layer. However, the effect of socket texturing on socket suspension,rotation, fit, and comfort remains unknown. Textured prosthetic socketsmay improve suspension by increasing the coefficient of sliding friction(COF) between the socket and liner-clad residual limb when compared to asmooth socket of the same material. However, printing different texturesinto the socket wall may influence bonding strength between layers,reducing ultimate tensile strength (UTS).

Sockets A selection of different texture patterns were programmed and3D printed using the SQUIRT-Shape System [1]. A smooth thermoformedsocket and a SQUIRT-Shape socket with original texturing consisting ofhorizontal striations approximately 1.2 mm in depth were used ascontrols.

Apparatus Testing utilized a uniaxial hydraulicmaterial testing system (Instron, Norwood, MA). Fortensile testing, dumbbells were secured to theInstron using action wedge grips. For COF testing,specimens were secured to a custom COF testingframe.

References[1] Rovick J. Automated Fabrication of Sockets for Artificial Limbs. PhD

Dissertation, Northwestern University, 1993.[2] ASTM D638−14: Standard Test Method for Tensile Properties of Plastics.[3] ASTM D1894−14: Standard Test Method for Static and Kinetic Coefficients

of Friction of Plastic Film and Sheeting.

Hypothesis We hypothesized that texture of polypropylene copolymersocket specimens would vary the UTS of the material. We also hypothesizedthat texture of polypropylene copolymer socket specimens would vary the COFof the material. Significance set at p=0.05 for both hypotheses.

Results There was a significant difference in UTS (p<0.0005) based on material texture with alltextured samples being significantly weaker than the smooth reference samples (p<0.05). There wasa significant difference in COF (p<0.0005) based on material texture, with both static (p<0.000) andkinetic COF (p<0.0005) being significantly different. While some textured samples had a larger staticCOF than the smooth reference sample, all but one textured sample had a lower kinetic COF.

Original SQUIRT-Shape socket fabrication

Methods and Results

Textured Samples

Horizontal line

Vertical line

Hemisphere

Half-hemisphere

Horizontal rectangle

Vertical rectangle

Checkerboard

Densely distributedMore aggressive (HD)

Lightly distributedMore subtle (LS)

Reference Samples

Test Description

Tensile COF

Smooth Raw Sheet (6mm thick)of Polypropylene Copolymer

Tensile only

Smooth Thermoformed rectangular socket made from 12 mm thick sheet of Polypropylene

Copolymer

Tensile COF

Original SQUIRT-Shape Socket

Textured socketRectangular shape

WidthHorizontal

Spacing

Vertical Spacing

Height

Horizontal Spacing

Depth

Cross-sectional view of socket

Socket Texture

Textured socketTranstibial shape

Bottom of the sledTop of the sled

Nylon sockLiner

Sled

Textured COF specimen

DumbbellsStamping out dumbbells with cutting die

Mounting holes COF (left) and tensile testing (right) set up

Socket Sample Ultimate TensileStrength [MPa]

Static COF [N/N]

Kinetic COF [N/N]

Smooth Raw Sheet 24.48 0.352 0.341Smooth Thermoformed 24.38 - -Original SQUIRT-Shape 15.46 0.363 0.30414 Textured Samples 3.97 - 14.32 0.271 - 0.422 0.208 – 0.332

Original SQUIRT -ShapeSmooth raw sheet Smooth thermoformed

Data analysis UTS and static and kinetic COF were compared toreference samples that included a smooth sheet of the samepolypropylene copolymer. UTS was assessed using a one-way ANOVA,while COF was assessed using a one-way MANOVA.

Discussion Tensile testing revealed a wide range of material strengthsthat depended on the distribution density of texturing as well as on thetype of texture pattern. COF testing demonstrated that different texturesinfluence friction properties between the socket, liner and nylon sock, andcan be increased compared to the original SQUIRT-Shape socket.

Conclusions These results provide an initial understanding of the effectof texturing on material properties, but further cyclic and static failuretesting and test set-ups that mimic real-world socket conditions are needed.

COF Results

COF

[N/N

]Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

Smooth raw sheet

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

COF

[N/N

]

Time [s]

Original SQUIRT -Shape