technical memorandum no. 3 for remedial …

57

PELA

TECHNICAL MEMORANDUM NO. 3

FOR REMEDIAL INVESTIGATION/FEASIBILITY STUDY

CITY DISPOSAL CORPORATION LANDFILL

(DUNN LANDFILL)

(PELA Reference No. 495201)

Appendix B.

Results of Analyses of Soil Samples and

Ground-Water Samples - Technical Report A

Volume III of III

CA1365-CA1378

CA1382, CA2013

February, 1990

P. E. LaMoreaux & Associates, Inc. —

Technical Report

for

CITY DISPOSAL CORPORATION LANDFILL

VOLUME III OF III

C/rim of Custody D»t» Required for ETC D*t» M»n*gement Summary Report*

CA1365-CA1378, WASTE MMKGEMENT, INC 405CAI382.CA2013

E/»p«*o*ETC Samp/f No. Company Facility Simple Point Dtte Time Hours

Swap T. Davis

President

This Tecrmieal Report is an INSITE Mrvic« generated Oy LOOESTffi D«tj n«i«g«i**nt Softuar*.

ETC

PESTICIDE/PCB DATA

838

ETC

QC SUMMARY

839

Lab Name: ETCNJ

Lab Code:

WATER PESTICIDE SURROGATE RECOUEPY

Con tract:

Case No.: SAS No.: SDG No

0102030405060703091011121514151617IS1920212227242526o~?4. -'

282930

-EP TC jgiSAMPLE NO.

QC70021GCA1859GSCA1359GRCA1859GCA1371G

'

W slC DBC ) #«».».»

7983768036

OTHER TOTIOUT

00000

SI <08C) - D l b u t y l c h l o r e n d a t e

ADUISORYQC LIMITS(24-154,1

page 1 of

# Column to be used to flag recovery values* 'v'a 1 ues outside QC 1 imi t sD Surrogates d i l u t e d out

FORM II PEST-1

8901/37 Re>

Lab Name: ETCNJ

Lab Code:

2EWATER PESTICIDE SURROGATE RECOVERY

Cont rac t:

Case No.: SAS No.: SDG No

I -&*r&rc1 SAMPLE NO.

01IQC70044GQ2ICA1858G03 ICA1858GS04ICA1858GRQ5IQC70Q44GS06ICA1372GQ7ICA1373G08ICA1374G09ICA1375G10ICA1376G11ICA1377G12ICA1378G13114115116117118119120121122123124125126127!281291301

SIC DBC ) #

841551461557670882578897375

OTHER TOTOUT

000000000000

SI (DBC) • Dlbutylchlorendate

ADVISORYQC LIMITS(24-154)

# Column to be used to flag* Ualues outside QC limitsD Surrogates diluted out

recovery values

page 1 of

FORM II PEST-1

891

1/87 Rev

SOIL PESTICIDE SURROGATE RECOVERY

Lab Name : ETCNJ Cont ract:

Lab Code: Case No.: SAS No.:

Level : CLOU/MED ) LOW

SDG No

010203040506070309101112131415161718192021222324252627282930

EPASAMPLE NO.

QC70076GCA1368GCA1368GSCA1368GRCA1369GCA1370GCA1365GCA1366GCA1367GCA2013G

SI(DBC)#

221 *93162 *186 *157 *422 *179 *148321 *146

OTHER TOTOUT

1011111010

SI iDBC) - D i b u t v l c h l o r e n d a t eADUISQRYOC LIMITS(20-150)

# Column to be used to flag recovery values* Ualues outside QC l i m i t sD Surrogates d i l u t e d out 892

page 1 of

FORM II PEST-2 1/87 Re-

3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY-

LabName:ETCNJ Contract:

Lab Code: Case No.: SAS No.: SDG 'No.:

M a t r i x Spike - ERA Sample No.: CA1368GS Leve 1 : (LOW/MED) LOUI

COMPOUND

qamma-BHC (L i ndane )Hep t ach 1 orA 1 dr inD i e Idr inEndr in4.4'-DDT

SPIKEADDEDC ug/Kg ).........62.01562. 01562.015155.039155.039155.039

SAMPLECONCENTRATION

(ug/Kg ).............

0. 0000. 0000.0000. 0000. 0000. 000

MSCONCENTRATION

t ug/Kq J........I....

40.57636 . 05550.384107.315102.021134.679

MSH

REC *......6553816966

QC 1LIMITSI

- REC. 1...... |46-127175-130 174-172 131-134142-139 123-1341

1

COMPOUND

qamma-EHC ( L i ndane )Hept ach lorH 1 dr inD i e 1 dr i nEnd r i n4. 4 '-DOT

SPIKEADDED(ug/Kg).........61.99161.99161.991154.979154.979154.979

MSDCONCENTRATION

(ug/Kg ).............

50.58545 . 10357. 160170.458134. 066165. 5o8

MSD

REC #

8273928487107

1% i QC L

RPD #1 RPD

22 1 5022 1 3113 1 4320 1 3827 1 4521 1 50

1

MITSREC.......46-12735-13034-13231-17442-17927-134

ft Co 1umn to be used to flag recovery and RPD values w i t h an a s t e r i s k

*Ualues outside of l i m i t s

RPD: 0 o u t o f 6 o u t s i d e l i m i t sSpike Recovery: 0 out of 12 outside limits

Comments: _________________________________________________________

FORM III PEST-2 1/87 Rev.

893

3EUIATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETCNJ Contract:

Lab Code: Case No.: SAS No.: SDG No.:

M a t r i x Spike - EP^ Sample No.: CA1858Gjix

COMPOUND

qamma-BHC( L i ndane )Hep tach 1 orA Idr inDieldr inEndr in4.4'-DDT

SPIKEADDED(ug^'L)

.200

.200

.200

.500

.500,500

SRMPLECONCENTRATION

(ug/L)

0. OQOO.OQO0. 0000.0000.000O.OQO

MSCONCENTRATION

Cug-'D

.254

.220

.221

.636

.272

.712'

MS*

REC ft

127 *110110127 *54 *142 *

QC 1LIMITS IREC. 1

56-123140-131 140-120 152-126156-121 138-1271

1

COMPOUND

gamma-BHC C Li ndane )Hep t ach lorAldr inD i e 1 d r i nEndr in4.4--DDT

1 SPIKE1 ADDED1 (ug/L)

1 .2001 .2001 .2001 .5001 .500t .5001

1 MSDICONCENTRATION1 (ug/L)

1 .2371 .2091 .214I .6341 .2691 .6911

MSD 1

REC #1

118 t105 1107 i127 I54 * 1

138 - 1

1H 1

RPD *l

7 t5 13 I0 11 13 1

1

QCRPD

152022182127

LIMITS1 REC.

156-123140-171140-120152-126156-121138-1271

# Column to be used to f l a g recovery and RPD values w i t h an a s t e r i s k

* Ualues outside of l i m i t s

RPD: 0 out of 6 o u t s i d e l i m i t sSpike Recovery: 6 out of 12 o u t s i d e l i m i t s

Cornmtfn t 5 :

FORM III PEST-1 1/-87 Rev.

894

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY

Lab Name: ETCNJ Contract:


Matrix Spike - jEPflr Sample No.: CA1859QS-

COMPOUND

gamma-BHCCLindane )Heptach lorAldrinDie Idr inEndr in4.4'-DDT

SPIKEADDEDCug/L)

.200

.200

.200

.500

.500

.500

SAMPLECONCENTRATION

Cug/L)

0.0000.0000.0000.0000. 0000.000

MSCONCENTRATION

Cug/L)

.160

.152

. 147

.403

.450

.289

MS 1 QC% 1 LIMITS

REC #1 REC....... )......

80 156-12376 140-13173 140-12081 152-12690 156-12158 138-127

1

COMPOUND

gamma-BHCCLindane )Hep t ach lorAldrinDie Idr inEndrin ,.4. 4 ' -DOT

SPIKEADDEDCug/L)

.200

.200

.200

.500

.500

.500

MSDCONCENTRATION

Cug/L)

.159

.146

.142

.428

.431

.292

MSD%REC #

807371868658

SRPD *

143641

QC LIMITS 'RPD 1 REC.

15 156-12320 140-13122 140-12018 152-12621 156-12127 138-127

I

^ Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside of l i m i t s

?PD: 0 out of 6 outside l i m i t s"like Recovery: 0 out of 12 outside limits

Comments:

FORM III PEST-1 1/87 Rev.

895

4LPESTICIDE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.

Lab Sample ID: QC70076G

Matr ix : (soi1/water) SOIL

Date Ext racted: 10/04/89

Date Analysed tl): 11/14/89

Time Analyzed Cl): 0834

Inst rument ID (' 1) : HA

GC Column ID C 1 .': 2250/2401

Cont rac t :

SAS Ho.: SDG No.:

Lab F i l e ID: >HA503

Leve1:Clow/med) LOW

Extraction:ISepF/Cont/Sono) SONC

Date Analyzed t 2'' : 11/28'89

Time Ana Lyzed C2): 0013

Instrument ID '2 >: KB

GC Column ID 12): 3S5P-210Q

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

0102030405Oc070809101112131415161718192021-~i

232-*2526

EPASAMPLE NO.

LABSAMPLE ID

CA1368GCA1368GSCA1368GP,CA13&9GCA1370GCA1365GCA1366GCA1367GCA2013G

DATEANALYZED 1

11/14/8911/14/8911/14/8911/14/8911/14/39ll/l*t/8911 /I 4/8 911/14/8911/14/39

DATEANALYZED 2

11/28/8911/28/89

11/28/89

896Lommen t s:

page 1 ofFORM IV PEST 1---87 Pe

4CPESTICIDE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No


Matrix: Csoi1/water) WATER

Date Extracted:

Date Analyzed CD: 10/25/89

Time Analyzed CD: 0310

Instrument ID CD: QB

GC Column ID CD: 2250/2401

Cont rac t :

SAS No . : SDG No. :

Lab File ID: >QB836

Level:Clow/mod) LOU

Extract ion: CSepF/Cont/Sonc ) OCIT-.

Date Analyzed C2>: IO/B//P^

Time Analyzed C2): 0141

Instrument ID (2): JB

GC Column ID C2): 3KSP-2100

THIS METHOD BLANK APPLIES TO THE FOLLQLJING SAMPLES, MS AND MSD:

1 EPA1 SAMPLE NO.•|............

Oil02103104105106107108109110111112113114115116 t17118119 t201211221231241251261

LABSAMPLE ID

CA1859GSCA1859GRCA1859GCA1371G

DATEANALYZED 1

10/25/8910/25/8910/25/8910/25/89

DATEANALYZED 2

t 0 /3 / Iff*'

897,omments:

jge 1 of /FORM IY PEST 1/87 Rev.

4CPESTICIDE METHOD BLANK SUMMARY

Lab Name: ETCN3

Lab Code: Case No

Lab Sample ID: QC7Q0446

Matrix: (soiI/water) WATER

Date Extracted: 09/29/89

Date Analyzed (1): 10/27/89

Time Analyzed CD: 0653

Instrument ID (1): HA

GC Column ID CD: 2250/2401

Cont ract:

SAS No.: SDG No.:

Lab File ID: >HA232

Level:Clow/med) LOW

Extract ion:CSepF/Cont/Sonc) CONT

Date Analyzed C2):

Time Analyzed C2):

Instrument ID (2):

GC Column ID (2): '

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

t EPA1 SAMPLE NO.

Oil02103104105 t06107108109110111112113114115116117118119120121122)231241251261

LABSAMPLE ID

CA1858GCA185BGSCA1858GRCA1372GCA1373GCA1374GCA1375GCA1376GCA1377GCA1378GCA1382G

DATEANALYZED 1

10/27/9910/27/8910/27/8910/27/8910/27/8910/27/8910/27/9910/27/8910/27/8910/27/8910/27/89

DATEANALYZED 2

898Common t s:

page 1 ofFORM IU PEST 1/87 Rev.

ETC

SAMPLE DATA

899

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matr ix : ( so i I /'wa te r ) SOIL

Sample w t / v o l : 2 5 . 0 ^°t^r Cg/mL) G«t**p4

Level: ( l o w / m e d ) LOLJ

SMoisture: not dec. 17 dec.

Extraction: (SepF/Cont/Sonc) SONC

GPC Cleanup: lY/N) Y pH: 6

Con t rac t:

SAS No.: SDG No.:

Lab Sample ID: CA1365G


Date Received: 09^23/89

Date Extracted: lCl/04/'89

Date Analyzed: ll-'14/89

Dilution Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug-''Kgj UG-"KG

3-19-64-6 —— ———— alpha-BHC_________319-65-7———————beta-BHC__________319-86-8 ——— ——— delta-BHC________5e-89-9---------gamma-BHC(Lindane).76-44-8---------Heptachlor________309-00-2 ——————— Aldrin____________1024-57-3-------Heptachlor epoxide.959-96-8 ——————— Endosul fan I______60-57-1-———____Dieldrin_________72-55-9 ———————— 4,4'-DDE__________72-20-8---------Endrin___________33213-65-9 ————— Endoaulfan II_____72-54-8 ———————— 4,4'-ODD__________1031-07-8----——Endosulfan sulfate50-29-3 ———————— 4,4'-DOT__________72-43-5-------—Methoxychlor______53494-70-5-—---Endrin ketone_____5103-71-9---——-alpha-Chlordane___5103-74-2-------gamma-Chlordane___8001-35-2----—-Toxaphene_________12674-11-2----—Aroclor-1016______.11104-28-2 ————— Aroc lor-1221______11141-16-5-- ——— ArocI or-1232______53469-21-9------Aroclor-1242______12672-29-6 ————— Aroc lor-1248_____11097-69-1 —— —— Aroclor-1254______11096-82-5 ————— Aroc lor-1260_____

991i111119'9619o9380

600600600600600600600600

0000

569S?0

Q

IUI.UIUIUIUIUIUIUIUIUIUIUIUIUuuuuuuuuuuuuu

FORM I PEST 1/87 Rev

900

CHROMRTOGRflM'File >Hfl5l8 1.8 aau.

400 800

520000-

480009;

440000-

40000&

3200B&

260000

20000&

5,0670076,5

2000

IS

Data File: >HA51Q::U4 Quant Output File:Name: InstrumentID: HAMisc: CA1365G,QG70076,5:53,24.96,40

Id File: IQ76IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95XSP2401 2UL INJLast Calibration: 891114 08:52

Operator ID: YY6148Quant Time: 891114 14:45Injected at: 891114 14:02

901

QUANT REPORT

Operator ID: YY6148 QuantOutput File: ^H*510::AQData F i l e : >Hrt510::U4Name:Misc: CA1365G,QG7QQ76,S:G3,24.96,40

7 Quant Time:Injected at:

D i l u t i o n Factor:

Page 1

391114 14:45891114 14:02

1.00000I n s t r u m e n t I D : H A

ID Fi le: IQ76IP: : USTit le: IFB/PST/PCB 1 . 5SSP225 0/1 . 95SSP240 1 2UL INJLast Calibration: 891114 08:52

Compound R. T . Scan# Height Cone Units

19) ttDibutylchlorendate

# Compound uses ESTD

29.13 1746 727234 .179 UG/ML 100

902

IDPESTfcIDE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

M a t r i x : (soil/water ) SOIL

Sample wt/vol: 24. 0-* g! -r- Cg/mL) G

Level: Clow/med) LOW

J i M o i s t u r e : not dec. 20 dec.

Extract ion: (SepF/Cont/Sonc) SONC

GPC Cleanup: (Y/N) Y pH: 6

Con tract:

SAS No.: SDG No. : •


Lab File ID: >HAS 11

Date Received: 09/23/39

Date Extracted: 10/04x89

Date Analyzed: 11/14/39

D i lu t ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug-''L or ug/Kg.1 UG/KG

3-19-64-6--------alpha- BHC________3 19-65-7-- —— —— beta-BHC_________319-36-8 —— ——— -delta-BHC________5B-8*-9---------gamma-BHCCLindane).76-44-8---------Heptachlor________3Q9-OCi-2--------Aldr in___________1024-57-3-------Heptachlor epoxide.959-98-8--------EndosuIf an I_____60-57-l---------Dieldr in__________72-55-9- ——— ——— 4, 4'-DDE__________72-20-3---------Endnn____________33213-65-9--———Endosulfan II____72-54-8-- —— ———4,4'-ODD__________1031-07-8-—----Endosulfan sulfate50-29-3———-----4,4'-DOT__________72-43-5------—-Methoxychlor______53494-70-5------Endrin ketone_____51Q3-71-9-------aIpha-Chlordane___5103-74-2-------gamma-Chlordanc___3001-35-2----——Toxaphene________12674-ll-2------Aroclor-1016 ______11104-28-2------Aroclor-1221_____11141-16-5 ————— Aroc lor-1232______57469-21-9------Aroclor-1242______12672-29-6———--Aroclor-1248______11097-69-1————-Aroclor-1254______11096-82-5 ————— Aroc lor-1260_____

0000000000

21020

, 02iHli4001( 0II 0n; oK o100200

J/

u-oJ.OD

20UOt)

0

Q

IUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIU

FORM I PEST903

1/87 Re-

CHBOMftTOGRflMFile >HflSll 1.0

480000-

408800;

36000&

288080-

240008-

£00000-

160083-

409 ' 808 1S00. r ... i ... I . . ...I. ... . . I . 1680

12

erye/b ,s is2000. I .

Data F i l e : >HA511::U4 Quant Output F i l e :Name: I n s t r u m e n t l D : HAMisc: CA1366G,QG70076,S:G3,24.04,40

Id F i l e : I076IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL IN3Last Calibration: 891114 08:52


904

QUANT REPORT Page 1 .

Operator ID: YY6148 ' Quant Re^: 7 Quant Time: 891114 15:31O u t p u t F i l e : ~HA511::AQ Injected at: 391114 14:47Data F i l e : >HA511::U4 D i l u t i o n Factor: 1.00000Name: I n s t r u m e n t I D : HAMisc: CA1366G,QG70Q76,S:G3,24.Q4,4Q

ID F i l e : I076IP::UST i t l e : IFB-'PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast C a l i b r a t i o n : 891114 OB:52

Compound R.T. Scan* Height Cone U n i t s q

19) # D i b u t y l c h l o r e n d a t e 29.15 1747 271298 .148 UG/ML 100


905

IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil'water) SOIL

Sample wt/vol: ^ 1'""9" * (g/mL) G" Ti'?

Leve1: (law/med) LOW

^Moisture: not dec. 27 dec.

Extract ion: CSepF/Cont ••'Sonc ) SONG


Con t rac t:

SAS No.: SDG No.: '


Lab Fil e ID: >HA512

Date Received: 09/23/8'?



Di lut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(uq/L or ug/Kg) UG/KG

>19-64-6--------alpha-BHC_________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC_________58-89-9 — ---- — -gamma-BHC(Lindane).76-44-8-—------Heptachlor________309-00-2------—Aldrin____________1024-57-3-------Heptachlor epoxide.959-98-8----——Endosulfan I______60-57-1--- — ----Dieldrin_________72-55-9---------4,4'-DDE__________72-20-8------——Endrin____________33213-65-9 ————— Endosulfan I I_____72-54-8 ———————— 4,4'-DDO__________1031-07-8-—-—-Endosulfan sulfate50-29-3--- ———— -4,4'-DDT__________72-43-5---------Methoxyen lor______53494-70-5-———Endrin ketone_____5103-71-9-------alpha-ChIordane___5103-74-2-------gamma-Chlordane.__8001-35-2-----—Toxaphene________1-2674-11-2- —— --Ar odor-10 16______111 04-28-2------Aroclor-1221_____11141-16-5 ————— Aroc lor-1232______53469-21-9------Aroclor-1242______12672-29-6——---Aroclor-1248______11097-69-1 ————— Aroc lor-1254______11096-82-5 ————— Aroc lor-1260______

10.0

11440

1 00

2: Q: o

rf*

J/

Q

IUiuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


906

CHRQnBTOGRBttFile >Hfl512 1.6

850000-

800000-

750000-

700000-

659800-

600006-

550000-

500000-

450000-

400000-

390000-

300000-

250090-

200000-

150009-

49C 800 1600 2000

Data File: >HA512::U4 Quant Output File:Name: Ins t rument ID: HAMisc: CA1367G,QG70076,S:G?,21.92,40

Id FiIe: I076IP::USTitle: IFB/PSTxPCB 1.5XSP2250/1.95SSP24Q1Last Calibration: 891114 08:52


2UL INJ

907

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^HA512::AQData File: >HA512::U4Name:Misc: CA1367G,QG70076,S:G3,21.92,40

ID File: I076IP::USTitle: IFB/PST/PCB 1. 5SSP2250/1. 95*SP24Q1Last Calibration: 891114 08:52

Quant TimeInjected at

Di lut ion Fac torInst rumen t ID

2UL INJ

Page 1

891114 16:16891114 15:33

1.00000HA

Compound R.T. Scanft Height Cone Units

19) t fD ibu ty lch lo renda te


29.15 1747 587076 .321 UG/ML 100

If 1+1 Iff

908

IDPESTicIDE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r ix : (soil --'water ) SOIL

Sample wt/vol: 25 .9" 3ti (g/mL) Gl v*-

J_evel: (low/med) LOLJ *''** ^

HMoisture: not dec. 14 dec.

Extract ion: (SepF/Cont/Sonc) SONC

GPC Cleanup: CY/N) Y pH: 5

Lon t rac t:

SAS No.: SDG No . :


Lab File ID: >HA5Q4


Date Extracted: 10/Q<4/89


Di1u t ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/KgJ UG-'KG

>19-64-6--------alpha-BHC________319-65-7-----——beta-BHC__________719-86-8- —————— del ta-BHC________58-89-9---------gamma-BHC(Lindane J.76-44-8——------Heptachlor________309-00-2- —— - —— Aldr in___________1024-57-3-------Heptachlor epoxide.959-98-8----——-Endosulfan I_____60-57-l---------Dieldrin_________72-5^-9 ———————— 4,4 '-DDE__________72-20-3---------Endrin____________J3213-6?-9 —— —— Endosulfan I I_____72-54-8 ———— ———4,4'-DDD_________1031-07-8-------Endosulfan sulfate.50-29-3 ———————— 4,4' -DDT_________72-4?-5---------Methoxychlor______"73494-70-5--- —— Endrin ketone_____5107-71-9—— ——— alpha-Chlordane___510?-74-2-------gamma-Chlordane___8GQl-35-2-------Toxaphene_________12674-11-2------Aroclor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5————-Aroclor-1232______53469-21-9------Aroclor-1242______12672-29-6------Aroclor-1248______11097-69-1------Aroclor-1254______11096-82-5------Aroclor-1260______

300.300300.300300.300300300

300.13000

5

u

FORM 1 PEST 1/87 Re-

909

CHROMfiTOSRBMF i l e >Hfl594 1.0 amu.

400 see is00Cfll3b86 ,057

1600

0076, Si t

SG00

D a t a F i l e : > H A 5 0 4 : : L I 4 Quant O u t p u t F i l e : " 1 H A 5 Q 4 : : A QName: Ins trument ID: HAM i s c : CA1363G , Q E 7 0 0 7 6 , S : S 3 , 2 5 . 8 7 , 4 0

I d F i l a : I 0 7 6 I P : : U ST i t l e : IFB/PST/PCB 1. 5?iSP22? 0/1. 95*SP240 1Last C a l i b r a t i o n : 891114 08:52


2UL INJ

910

Operator ID: YY6148Output File: 'SHA504::AQData File: >HA5Q4::U4Name:Misc: CA1368G ,QG7QQ76 ,S : G3 ,25 . 87 , 40

QUANT REPORT

Quant Rev: 7 Quant Time:Injected at:

D i l u t i o n Factor:Instrument ID:

ID File: I076IP: : USTitle: IFB/PST/PCB 1 . 5!*SP225 0/1 . 959SSP2401 2UL INJLast Calibration: 891114 08:52

Page 1

891114 10:11391114 09:28

l.OOQOOHA

Compound R.T. Scan* Height Cone Units

19) #Dibutylchlorendate


29. 17 1748 173818 . 0976 UG/ML 100

911

PESTICIDE ORGANIC;ID

, ANALY! s DATA SHEETERA SRMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r ix : Iso i 1 '-'water ) SOIL

Con tract:

Sample wt/vol: 27 . 2 to , ( g'mL> G

«/»^Level: flow/madJ LQU ''

SiMoisture: not dec. 2? dec.

Ex t r ac t ion: (. SepF/Con t /Sonc ) SONC

GPC Cleanup: (Y.-'N,i Y pH: 7

COMPOUND

No . : SDG Ho. :


Lab F i l e ID: >HA5Q7


Date Extracted: 10--Q4-89

Date Analyzed: ll-"l4/S9

D i lut ion Fac t o r : 1

CONCENTRATION UNITS:<-ug -'L or ug -t'.g l UG 'KG Q

I 3-19-6*4-6--------a Ipha-BHC_________I 319-65-7--------beta-BHC__________I 7 19-36-S — ------del ta-BHC_________I =8-89-9---------gamma-BHC( L i n d a n a >.I 76-44-3 ---------Heptachlor________I 3i)9-QO-2--------Aldr in____________I 1024-57-3-------Heptachlor epoxide.I 959-9S-8--------Endosulfan I_____I 60-57-1---- —---Dieldrin__________I 72-5"r-9---------4,4'-DDE__________I ^2-20-8---------Endrin____________I ??21?-6c-°------Endosu1fan II_____I 72-'?4-8---------4,4l-DDD__________I 10M-07-8-------Endosulfan sulfateI 50-29-3- ——— ——— 4,4'-DDT__________I 72-47-5---------Hethoxychlor______I t?34Q4-70-':>------Endrin ket one_____I 51Q3-71-9-------alpha-Chlordane___t 5107-74-2-------gamma-Ch1ordane___I 8001-35-2-------Toxaphenc_________I 12674-11-2---—-Aroclor-1016______I l l lOa-23-2------Aroclor-1221______I 11141-16-5 ————— Aroc lor-1232______1 53469-21-?--- - - -Aroclor-1242______I 12672-29-6------Aroclor-1243______I 11097-69-1------Aroclor-1254______I 11096-82-5--~-- -Aroclor-1260______I ___ ______________

FORH I PEST

000C00

:01°

21

*121I4101( 0li 0II 011 0li 02: o210

-J-O

, /

iuIUIUIUIUt uIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUu

1/87 Rev

912

CHROMATOQRPhFile >Hfi597 1.0 amu.

__ 400

560080-

440000-

360000-

32008^

£40006-

160000

808 1200*

CHi36?y ,Cie7e076 ,Si':1600 2000

16 20 24 28

Data File: >HA5Q7::U4. Quant Output File: /SHA507::AQName: Instrument ID: HAMisc: CA1369G ,QG70Q76,S:G3,23.16,40

Id File: I076IP::UST i t l e : IFB/PST./PCB 1. 554SP225Q/1. 95&SP2401 2UL INJLast Calibration: 891114 08:52


913

QUANT REPORT

Quan t Rev: 7Operator ID: YY614SOutput FiIB: ^HA5Q7:: AQData F i l e : >HA5Q7:: U4Name:Misc: CA1369G ,QG7Q076,S:G3,23.16,40

ID F i l e : I076IP::USTit le: IFB/PST/PCB 1. 5SSP225Q/1. 95*SP24Q 1Last C a l i b r a t i o n : 891114 08:52

Quan t Time :Injected at:

D i 1 u t ion Fac tor:Ins t rumen t ID:

2UL INJ

Page 1

391114 12:29891114 11:45

1. O Q O O OHA

Compound R.T. Scan* Height Cone U n i t s

e f e a DIIC19) tOibutylch lorendate

tt Compound uses ESTD

6 . 8 5 409 104192 .0336 UG/ML 10029.15 1747 2SS130 .157 UG/ML 100

914

CHROMBTOGRBMFile >KB18? 1.0 amu. . . Cfil.<o?S ,ai37@67*fsu

1300000:

120060^

100000&

90000*

300QQ0-

70000fr

600000;

400000-

seoaee-

466 800 1260 1*06 20<?9. . . 1 . . . 1 . . 1 . . . 1 . . . . . . l . . . 1 . . . 1 . . . 1 . . . r

| I A4 ' 8 12 ' 16 ' 29 ' 24 28 ' 32 '

Data F i l e : ^KB189::U2 Quant Output File: 'XKB189::AQName: Ins t rument ID : teftMisc: CA1769G .QG70076,S:G7,23.16,40

Id File: I076IC::UST i t l e : IFB/PST/PCB 6' X 2 MM ID 3SSP-2100 2 UL IN3Last C a l i b r a t i o n : 891128 00:29

Operator ID: KTS582Quant T tme: 891128 01:27Injected at: 891128 00:52

914

QUANT REPORT

Operator ID: KT8582Output FiIe: ^KB189::AQData Fila: >KB189::U2Name :Misc: CA1369G , QG70076,S:G?,23.16,40

Quant Rev: 7 Quan t Time:Injected at

D i 1 ut ion Fac tor1 ns t rumen t ID1

ID Fila: I076IC::USTitle: IFB/PST/PCB 6' X 2 MM ID 3*SP-21QQ 2Last Calibration: 891128 00:29

UL INJ

Compound R.T, Scan* Height

Page 1

891128 01:2^891123 00:52

1. 0 0 i] 0 0

Cone Un i ta

915

PESTICIDEID

ORGAN ICS ANALY*ERA SAMPLE NO

IS DATA SHEET

Lab Name: ETCMJ

Lab Code: Case No.:

Matr ix: (so iI/water ) SOIL

Samp le wt/vo 1 : 2*. Q 3° -*- <g/mD G

Level: Clow/med) LOW " >

h Moisture: not dec. 20 dec.

Extraction: ( SepF/Con t -'Sonc ) SONC

C-PC Cleanup: CY/N) Y pH: 7

Con t ract:

SAS No.: SDG No.: •




Date Extracted: 10-'04/89

Date Analyzed: H---14/39

Di lution Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ugXL or ug/Kg,' UG/KG

FORM I PEST

Q

3-19-64-6------- -a loha-BHC319-65-7 ——————— beta-BHC319-36-8 ——————— aelta-BHC58-89-9------- — oamma-BHCCLindane )76-44-8 — - — ----Heptach lor309-00-2 ——————— A l d r i n1024-57-3-------Heptachlor epoxide959-96-8-------- Endosul fan I60-57-1 ---------Die Idr in72-55-9---------4.41- DDE72-20-8---------Endnn37213-65-9 ————— Endosulf an I I72-54-8 ———————— 4. 4 '-ODD1031-07-8-------Endosulfan su 1 fate50-^9-3 ——— ———— 4 ,4 '-DOT72-43-5---------Methoxvchlor53494-70-5 — — — Endrin ketone5103-71-9 ——— —— alpha-Chlordane5103-74-2---- — -gamma- Chlardane8 001-35-2------- To xaphene12674- 11-2--- ---Aroc lor- 10 1611104-23-2 ————— Aroc lor- 122111141-16-5 ————— Aroc lor- 123253 46 9- 2 1-9------ Aroc lor- 12 4212672-2-5-6 ———— --Aroclor-1243 ,11097-69-1 ————— Aroc lor- 125411Q96-32-5- — ---Aroc lor- 1260

\

'11111

?

?I?11411111??

0 J0000Q000 H

33)

I)0 >I u

I cP

I p00ao ^000

( 0C 0 WCO U*v

1p iu

IUIUIUIUIUIU

I IUto iu

IUIUIUIUIU

' IUe* IU0 IUro iu

IUoc IU

IUIUIU

* IUoo iu•00 IU

1

1/87 Rev

916

CHROnflTQBROMFile >HflS09 1.6 aau.

1080009;

900000J

398000

600000

S0000&

300000

400 •. 1 . . . 1 880 1200. i . . j_ i . . . i .

CR1379(

1600 2888i ... . _ i ..._

12 24 28

Data File: >HA509::U4 Quant Output File: AHA509::AQName: Inat rument ID: HAMiac: CA1370G,QG70076,S:G3,24.Q5,40

Id File: I076IP::USTi t le : IFB/PST/PCB 1.5HSP2250/1.95HSP2401 2UL INJLast C a l i b r a t i o n : 891114 08:52

Operator ID: YY6148Q u a n t T i m e : 891114 14:00I n j e c t e d at: 891114 13:16

917

QUANT REPORT

Operator ID: YY6148 Quant Re^:Output File: "VHA509::AQData File: >HA509::U4Name :Mis-c: CA1370G,QG?Q076,3:53,24.05,40

ID File: I076IP::USTitle: IFB/PST/PC8 1.5SSP225Q/1.95S(SP24Q1Last Calibration: 891114 08:52

Compound

7 Quan t T ime:Injected at:

Di lut ion Fac tor:I n s t r u m e n t ID:

2UL INJ

Page 1

891114 14:008°1114 13:16

1.00000HA

R.T. Scan* Height Cone Un i ts

3) »Duia DHC19) ttDibutytchlorendate


6.87 410 113472 .0365 UG^-'ML 10029.13 1746 773381 .422 DC/ML 100

918

CHROtlftTQGRflnFile ;-KBl?0 1.0 amu. . CHlji70G fa67007& ,'* it

1600000-

1400000-

1200000-

1000000-

900990-

600000-

403000-

•

400 800 1299 1609 2000

^UJuwVJV

n\V. - A

• 1 ' ' ! ••-TT •'•T Tir*rTl ' I ' 1 ' 1 ' 1 ' ! ' i ' ! ' 1 ' I •4 8 12 16 20 24 28 32

Data F i l e : >KB1«0::U2 Quant Output File: AKB19Q::AQName: I n s t r u m e n t I D : •kfi'Misc: CM1370G ,QG7Q076 ,S : G3 , 2*>. 05,40 fe,#

Id Fi le: I076IC: :US "T i t l e : IFB/PST/PCB 61 X 2 MM ID 3*SP-21QO 2 UL INJ "Last C a l i b r a t i o n : 891128 00:29

Operator ID: KT8?82Quant Time: 391128 02:06Injected at: S91128 01:31

919

OUANT REPORT . Page 1

Operator ID: KT35B2 Quant Rev: 7 Quant Time: 391128 02:436Output F i l e : 'XKB190: :AO Injected at: 891128 01 = 31Data File: >KB19Q::U2 D i l u t i o n Factor: 1.00000Name: I n s t r u m e n t I D : K*5Misc: CA1370G .QG70076,S:G3,24.05,40

ID File: I076IC:TUST i t l e : IFB/PST/PCB 6' X 2 KM ID 3V3P-21QQ 2 UL INJLast C a l i b r a t i o n : 891128 0 0 : 2 9

Compound R . T . Scan* H e i g h t Cone U n i t s

920

PESTICIDEID

ORGANICS ANALYiERA SAMPLE NO

IS DATA SHEET

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil/water) UATER

Sample ut/vo1 : 990.0 Cg/mL) ML

Leve1: tlow/med > LOW

J. Mo i s t u r e : not dec. dec.

Extraction: (SepF/Cont/Sonc) SEPF

GPC Cleanup: (Y/N) N pH:

Cont rac t:

SAS No.: SDG No. :


Lab File ID: >QB840

Date Received: o<?/i<?

Date Extracted:


Di lut ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(uq/L or uq/Kq) UG/L 0

319-64-6----319-65-7 —— -319-86-8 —— -C Q QQ Q

76-44-8-----

1024-57-3---959-98-8----60-57-1-----~>'~ _ R P _ Q _ _ _ _ .

72-20-8 ——— -33213-65-9--72-54-8-----1071-07-8---50-29-3---—72-43-5 ——— -53^94-70-?--5103-71-9---5103-74-2---8Q01-35-2---12674-11-2--111Q4-28-2--11141-16-5--53469-21-9--12672-29-6--11097-69-1--11096-82-5--

- — — aloha-BHC-----beta-BHC-- —— delta-BHC-----qamma-BHC C L i ndane ).____Hep t ach 1 o r-----Aldr in-----Heptachlor epoxide-____£ n closu 1 i an I-----D ic Idr in.----**. 4'-DDE-----Endr i n-----Endosulfan I I- ——— 4.4'-DDD_ _ _ _ _ Endosulfan s u 1 f a t e-----4.4'-DDT-----Me t hoxych lor-----Encirin ketone.____ a lpha-Ch lordane-____gamma-Ch lordane.--.-Toxaphene- ——— Aroc lor-1016.----Aroc lor-1221- — --Aroc lor-1232-----Aroc lor-1242._ — -Aroc lor-1248.____Aroc lor-1254.----Aroclor-1260

.051 U

. 051 U

.051 U

.051 U

.051 U

.051 U

.051 U

.051 U

. 100 U

. 100 U

. 100 U

. 100 U

. 100 U

. 100 U

.100 U

.510 U

. 100 U

.510 U

.510 U2 U.510 U.510 U.510 U.510 U.510 U1 U1 U

FORM I PEST 1/87 Re-.

921

CHROMBTOGROMfile >QB840 1.8 arou.

489 800 1200

CR1371S ,0678821,L 1C

1680 2088850008-

800000-

758808-

788888-

658988-

600888-

S50900-

500000-

450000-

400008-

350808-

300000-

250000-

200008-

' ' ' ' 12 ' "iV ' "2'0 '

Data File: >QB84Q::U6 Quant Output File: QB840::AQName: Instrument ID: QfrMisc: CA1371G ;QG70Q21,L:G2, 990,10

Id File: I 021 IP::USTitle: IFB/PST/PCB 1.5KSP225 0/1.95SSP2401 2UL INJLast Calibration: 891025 09:04


922

QUANT REPORT Page- 1

Quant Rev: 7Operator ID: YY6148Output File: ~QB840::AQData File: >QB840::U6Name:Misc: CA1371G .QG70021,L:G2, 990,10

ID File: I021IP::USTit le: IFB/PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: 891025 09:04

Quant Time:Injected at

Dilution FactorInstrument ID

2UL IN3

891025 09:18891Q25 06:18

1.00000Off"

Compound R.T. Scantt Height Cone Units

„4~

_,

0

ni nHrW-t?-. .1*1 r. '

•l JLC" _ _._ AJ — Tbamma

i «Delta•} — #fl la> i-> — flHepta

) »alpha

•* IE^DE. * , ,> ID' 'id» tCndri• — *4 .4'

% *, ,?C

^pur•eh 1-or-BHCneh lor

Chieulfan

DDF

no-B&BuUan

r.rs-p

— epox ide* O*Pie•iH ane-I. I

-44— U-

t?-) — ft£nd r t a — a ,4- "**-

19

#

) #Dibut

Compound

ylchlorendate ii/^/^f

uaes ESTD

68991314151516171820202222222325

r 27

' 32

.72

.23

.23

.82

.53

.70

.85

.85

.37

.58

.62

.22

.75

.05

.80

.87

.50

.50

.72

.13

40149255258781088094994998010531115121112431321136613701408152816611926

2611213952103042227289610883205123968192

16003845123648320561121653774353

153728

.00328

.00213

.00205

.00372.000184.000254. 0000895.000123.000956.0000427.000425.000184.000245.00107.000134.000234.00556.00329.00234.0858

UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100100100100100100100100100100100100100100100100100100100

923

ru« >JBI

429AAAJ

-480000-

3-19SQO-

"•" ";

2BWWMW-

• J

55 1.0 URU. CP1371R ,n67BB?l ,L«fir

490 . see . i20e . is.ee . ae.ee

0

3

1

1 i1 Ul i 1iw n A i

VvO ' v-K 'k- /V J

V

DM

1

\

I

\

4 ' e ' ia ' is s;e ' a!4 ' e!e ' a'e ' s's

Data t-ile: >JU11?^::U4Name:

Id f- i IB: lUi^lL: : Ubl i t l e : 1 1- UxPb I /HUHLast Calibration:

Uperator 1U: YY614UUuant Time: HV1U31Injected at:

U8:12

Uuant Output h i l eInatrumentlL)

924

KtPUKI Page 1

LJperator 1U: YY6148 Quant Kev: / Quant l i m e : aviUM Ub:>0Uutpu t F i le : AJUJ,^& : : AU Injected at: ByiU^lO'^i'^bData h i l e : >JU1-?'?::U4 Dilution ractor: l.UUUUUName: Ins t rument 1Hisc '•

IU Ftle:t i t l e : IPb/PbTXPCB 3SSP-21UOLast Calibration: BVlU^l Ua:l*

Compound K.f. bean* Height Cone Units q

lVJ*Uibutylchlorcndate 2b.U> 16b^ I'jU/b^ .UVU4 Ub/HC 1UU

ft Compound uses hb I L)

925


ERA SAMPLE NO

Lab Name: ETCNJ Cont rac t:


Matrix: (soil/water) WATER Lab Sample ID: CA1372G

Sample wt/vol: 990.0 (g/mL) ML Lab File ID: >HA238

Level: (low/med) LOW Date Received: 09/2 /89

\ Moisture: not dec. dec. Date Extracted: 09/29/89

Extraction: CSepF/Cont/Sonc) CONT

GPC Cleanup: CY/N) N pH:


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9-————-gamma-BHC(Lindane).76-44-8- —————— -Heptachlor_______309-00-2 ——————— Aldrin____________1024-57-3---—--Heptachlor epoxide.959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8 —————— Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5-- — ———— Methoxychlor______53494-70-5 ————— Endrin ketone____5103-71-9 —————— alpha-Chlordane___5103-74-2 —————— gamma-Chlordane___8001-35-2 —————— Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232_____53469-21-9—————Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5 ————— Aroc lor-1260_____

,051.051,051,051051,051,051,051100100100,100100100100510100510510

»510510510510510

Q

IIDIDIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtu

FORM I PEST9261/87 Rev,

CHROMflTOGROnF i l e >HR239 1.0 amu,

408 see iseeCfil37£G,QG70044,L16

1600280006

aseeeej£39300-

sieeeaj£00000

13000*

170000^

£8 3£

Data File: >HA238::U4Name :

Quant Output File: AHA238::AQInstrument ID: HA

Mi sc: CA13 72G,QG70 044,L:G2,99 0,10

Id File: I044IP::UST i t l e : IFB/PST/PCB 1.5SSP225G/1.95SSP2401 2UL INJLast Calibration: 891030 12:07

Operator ID: KT8582Quant Time: 891030 12:22Injected at: B91027 16:43

C(

927

QUANT REPORT Page. 1

Operator ID: KT9592 Quant Rev: 7 Quant Time: 891030 12:22Output File: ^HA238::AQ Injected at: 891027 16:43Data File: >HA238::U4 D i l u t i o n Factor: 1.. 00000Name: Instrument ID: HAMisc: CA1372G,QG7QQ44,L:G2,990,10

ID File: I044IP::USTitle: IFB/PST/PCB 1.5KSP2250/1.95SSP2401 2UL INJLast Calibration: 891030 12:07

Compound R.T. Scan* Height Cone Units q

19) ttDibutylchlorendate 29.17 1748 93440 .0701 UG/ML 100

# Compound uses ESTD'/*<S*f

928


ERA SAMPLE NO

Lab Name: ETCNJ Cont ract:


Matrix: (soil/water) WATER Lab Sample ID: CA1373G

Sample wt/vol: 940.0 Cg/mL) ML Lab F i l e ID: >HA239

Level: Clow/med) LOW Date Received: 09/ 7/89

X Moisture: not dec. dec. Date Extracted: 09/29/89

Extraction: (SepF/Cont/Sonc) CQNT



Dilution Factor: 1


319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8———————delta-BHC________58-89-9- ——————— gamma-BHCCLindane ).76-44-8 ———————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3—-——-Heptachlor epoxide.959-98-8 ——————— Endosulfan I______60-57-1————————Dieldr in_________72-55-9 ———————— 4,4'-DDE_________72-20-8————————Endr in___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8 — - ——— Endosulfan sul fate50-29-3 ———————— 4,4'-DOT_________72-43-5 ——— — —— Methoxychlor______53494-70-5—————Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2————-gamma-Chlordane___8001-35-2—-----Toxaphene________12674-11-2—————Aroclor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroclor-1248_____11097-69-1 ————— Aroc lor-1254_____

1 11096-82-5 ————— Aroc lor-1260_____I_________________________________

.053

.053

.053

.053

.053

.053

.053

.053

.110

. 110

.110

.110

.110

.110

.110

.530

.110

.530

.5302.100.530.530.530.530.5301.1001.100

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIU

FORM I PEST9291/87 Rev

CHRQMfiTOGRflMFile >Hfl239 1.0 aim. CHI373&,OG70M4 ,L iG£

830 1208 1668

12- i j , ] | . | j , |=8 24 28 32

Data File: >HA239::U4Name:

Quant Output File: "-HA239::AQInstrument ID: HA

Misc: CA1373G,QG70044,L:G2,940,10

Id File: I044IP: : USTitle: IFB/PST/PCB 1 .5SSP2250/1 . 95HSP2401 2UL INJLast Calibration: 891030 12:07

Operator ID: KTB5B2Quant Time: 891030 12:23Injected at: 891027 17:30

930

QUANT REPORT

Quant Rev: 7Operator ID: KT8582Output File: ^HA239:: AQData File: >HA239::U4Name:Misc: CA1373G,QG7Q044 ,l_: G2 ,940 ,10

ID File: I044IP::USTit le: IFB/PST/PCB 1.5XSP2250/1.95SSP24Q1Last Calibration: 891030 12:07

Quant TimeIn jected 'at

Di lut ion FactorIns t rument ID

2UL INJ

Page 1

891030 12:23891027 17:30

1.00000HA

Compound R.T. Scan* Height Cone Uni ts


* Compound uses ESTD

29.15 1747 117248 .0879 UG/ML 100

931


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: C so i1/wa t e r) WATER

Sample wt/vol: 980.0 (g/mL> ML

Level: (low/med) LOW

% Moisture: not dec. dec.

Extraction: (SepF/Cont/Sonc) CONT


Con t rac t :

SAS No.: SDG No.:


Lab File ID: >HA24Q

Date Received: 09/ 7/89

Date Extracted: 09x29/89

Date Analyzed: 10/27x89

Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) U6/L Q

319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 ------76-44-8 —— ——309-00-2 —— «1024-57-3 ———959-98-8 ————60-57-1 ------72-55-9 - — ---72-20-8 ------33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 — - ——72-43-5 —— ——53494-70-5 ——5103-71-9 ———5103-74-2 ———9001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC---qamma-BHCCLindane )---Heptach lor—— Aldr in---Heptachlor epoxide---Endosu 1 fan I---Die Idr in—— 4.4'-DDE---Endr in---Endoau 1 f an I I—— 4.4'-OOD---Endoaulfan aulfate—— 4r4'-DDT---Methoxychlor---Endr in katona,.---a Ipha-Chlordane---qamma-Ch lordane ,---Toxaphene— -APQC lor-1016—— Aroclor-1221---Aroc lor-1232—— Aroclor-1242---Aroc lnr-1248—— Aroclor-1254---Aroc lor-1260

FORM I PEST

.051

.051

.051

.051

.051

.051

.051

.051

. 100

.100

.100

.100

.100

.100

.100

.510

.100

.510

.5102.510.510.510.510.51011

Ilu-ll)IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIU1 19321/87 Re^

CHROMRTOQRflMFile >Hfl240 1.9 «nu. Cfll3746,0570044,LiSi

340080;

320000;

30000*

280080;

260000;

240900;

220000;

200000;

180000-

400 800 1200 16002000

I I I 1 I I12 16 20 28

Data F i l e : >HA240::U4 Quant Output File: ^HA240::AQName: Instrument ID: HAMi»c: CA1374G,QG70044,L:G2,980,1Q

Id Fila: I044IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891030 12:07

Operator ID: KT8582Quant Time: 891030 12:25Injected at: 891027 18:18

QUANT REPORT

Quant Rev: 7Operator ID: KT8582Output File: ^HA240::AQData File: >HA240::U4Name:Misc: CA1374G,QG70Q44,L:G2,980,1Q

ID File: I044IP::USTitle: IFS/PST/PCB 1.5SSP2250/1.95XSP2401Last Calibration: 891030 12:07

Quant Time;Injected at

Di lut ion FactoriInst rumen t ID'

2UL INJ

Page 1

891030 12:25891027 18:18

1.00000HA




29.13 1746 33920 .0254 UG/ML 100

934


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code:

Cont rac t:

Case No.:


Sample wt/vol: 940.0 Cg/mL) ML


H Moisture: not dec. dec.

Extract ion: (SepF/Cont/Sonc> CONT


SAS No.: SDG No.:


Lab File ID: >HA241

Date Received: Q9/J7/89



Dilution Factor: 1


319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delt«-BHC________58-89-9—-—--—gamma-BHCCLindane).76-44-8———----Heptsenior_______309-00-2 ——————— Aldrin___________1024-57-3 —————— Heptachlor epoxide.959-98-8 ——————— Endosulfan I_____60-57-1--- — ——— Dieldr in_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8-———Endosulfan sulfate.50-29-3 ———————— 4,4'-DOT_________72-43-5————————Methoxychlor______53494-70-5 ————— Endrin ketone____5103-71-9 —————— alpha-Chlordane___5103-74-2----—-gamma-Cnlordane___8001-35-2-———Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5 ————— Aroc lor-1260______

.053

.053

.053

.053

.053

.053

.053

.053,110.110.110.110.110.110.110.530.110.530.5302!lOO.530.530.530.530,5301.1001.100

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUI

FORM I PEST9351/87 Rev

CHROMBTOSRflM>Hfl241 1.0 amu. Cfll3756,Q670044,L

240000-

£20009-

aieeee-

ee see 1200

28 32

Data FiName :

>HA241: : U4 Quant Output File: ^HA241::AQInstrument ID: HA

: CA1375G,QG70044,L:G2,940,10

Id Fi le: IQ44IP: :UST i t l e : IFB/PST/PCB 1 . 5HSP22SO/1 .95XSP2401 2UL INJLast Ca l ib ra t ion : 891030 12:07

Operator ID: KT8582Quant Time: 991030 12:27In jec ted at: 891027 19:05

936

QUANT REPORT

Quant Rev: 7Operator ID: KT9582Output File: ~HA241::AQData File: >HA241:iU4Name:Misc: CA1375G,QG70044,L:92,940,10

ID File: I044IP::USTitle: IFB/PST/PCB 1.5HSP2250/1.95SSP2401Last Calibration: 891030 12:07


Di lut ion Factor:Inst rument ID

2UL INJ

Page. 1

891030 12:27891027 19:05

1.00000HA

Compound R.T. Scantf Height Cone Units



29.15 1747 103873 .0779 UG/ML 100

937


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.


Sample wt/vol: 980.0 (g/mL) ML


Moisture: not dec. dec.

Extraction: CSepF/Cont/Sonc) CQNT


: SDG No.:


Lab File ID: >HA242

Date Received: 09/ /89





319-64-6———————alpha-BHC________.319-65-7———————bet«-BHC_________319-86-8 ——————— delta-BHC________58-89-9-—————gamma-BHCCLindane),76-44-8 ———————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3 —————— Heptachlor epoxide.959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8——————Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5-—---——Methoxychlor______53494-70-5—————Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Chlordane___8001-35-2 —————— Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5—————Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254______11096-82-5 ————— Aroc lor-1260_____

.051

.051

.051

.051

.051

.051

.051

.051

.100

.100

.100

.100

.100

.100

.100

.510

.100

.510

.5102.510.510.510.510.51011

IIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST938

1/87 Rev

CHROriRTOSRflnFile >Hfl242 1

300008-

290000-

280000-

270000-

260000-

250880-

240000-

230000-

220000-

210000-

200000-

190000-

188880-

1 70000- •4

.0 «mu. CR1376G,Q070044,Liee

400 ( 800 , 1200 | 1600 | 2000

10

a1

v ^ - — - - J4 8 ' 12 ' 16 ' 20 ' 24 ' 28 ' 32 '

Data File: >HA242::U4Name :

Quant Output File: ^HA242::AQInstrument ID: HA

Misc: CA1376G,QG70044,L:G2,980,10

Id File: I044IP::USTitle: IFBxPST/PCB 1.5SSP2250/1.95XSP24Q1 2UL INJLast Calibration: 891030 12:07


939

QUANT REPORT Pag*. 1

Operator ID: KT8582 Quant Rev: 7 Quant Time: 891030 12:29Output File: 'SHA242::AQ Injected at: 991027 19:53Data File: >HA242::U4 Dilution Factor: 1,00000Name: Instrument ID: HAMisc: CA1376G,QG7Q044,L:G2,980,1Q

ID File: I044IP:: USTit le: IFB/PST/PC8 1.5SSP2250/1.95SSP24Q1 2UL INJLast Calibration: 891030 12:07

Compound R.T. Scan* Height Cone Uni t» q

19) #Dibutylchlorendate 29.15 1747 118465 .0888 UG/ML 100



EPA SAMPLE NO.

Lab Name: ETCNJ Cont ract:


Matrix: (soi1/water) WATER Lab Sample ID: CA1377G

Sample wt/vol: 990.0 Cg/mL) ML Lab File ID: >HA244

Level: (low/med) LOW Date Received:

Moisture: not dec dec.


GPC Cleanup: CY/N) N PH:



Dilution Factor: 1


319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9- — ————— gamma-BHCCLindane).76-44-8 — —————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3 —————— Heptachlor epoxide959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9-- —————— 4,4'-DDE_________72-20-8 ———————— Endr in___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8--—-—Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5 ———————— Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9 —————— alpha-Cnlordane___5103-74-2----——gamma-Chlordane___8001-35-2— ———— Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroclor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69 1 ————— Aroclor-1254_____11096-82-5 ————— Aroc lor-1260_____

.051,051.051.051.051.051.051.051.100.100.100.100.100.100.100.510.100.510.5102.510.510.510.510.51011

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST941

1/87 Rev

CHRCmpTQQRfltlFilm >Hfig44 1.0 *nu.

400

340000-

220000-

200009-

isaeee-

16000*4

Cfll377Q ,Q678e44

600 i20e 1600 a gee

Data File: >HA244::U4 Quant Output File:Name: Instrument ID: HArtisc: CA1377G,QG70044,L:G2,990,10

Id File: I0441P::USTi t l e : IFB/PST/PCB 1.5XSP225Q/1.95HSP24Q1 2UL 1NJLast Ca l ib ra t ion : 991030 12:07

Operator ID: KT8582Quant Time: 891030 12:31Injected at; 891027 21:28

942

QUANT REPORT P«9V 1

Operator ID: KT8582 Quant Rev: 7 Quant Time: 891030 12:31Output File: AHA244::AQ Injected at: 891027 21:28Data File: >HA244::U4 Dilution Factor: 1,00000Name: InstrumentID: HAMisc: CA1377G,QG70Q44,I_:G2,990,10

ID File: I044IP::UST i t l e : IFB/PST/PCB 1.5KSP2250/1.95SSP2401 2UL INJLast Calibration: 891030 12:07

Compound R.T. Scant Height Cone Units q


t Compound uses ESTD

943


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: CsoiI/water) WATER

Sample wt/vol: 940.0 Cg/mL) ML

Level: (low/med) LOtJ

% tlo is ture : not dec. dec.


GPC Cleanup: (Y/N) N PH:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA245

Date Received: 09/ /89



Dilution Factor: 1


319-64-6 ——— -319-65-7 —— -319-86-8 ——— -58-89-9 ———— -76-44-8 ———— -309-00-2 ——— •1024-57-3 —— -959-98-8 ——— •60-57-1 ———— -72-55-9 ———— •72-20-8 ———— -33213-65-9 ——72-54-8 ———— -1031-07-8 —— -50-29-3 ———— -72-43-5 ———— -53494-70-5---5103-71-9 —— -5103-74-2 —— -8001-35-2 —— -12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1--11096-82-5 ——

. —— alpha-BHC- —— beta-BHC- —— delta-BHC----oamma-BHCCLindane )----Heptachlor——— Aldr in----Heptachlor epox ide----Endosul fan I----Die Idr in. —— 4r4'-DDE----Endr in— --Endosulfan II. —— 4r4'-DDD----Endosu 1 f an sulfate. —— 4r4'-OOT----Methoxychlor----Endr in katone----alpha-Chlordane•_--qamm»-Ch lordane----Toxaphene .----AraeIar-1016. —— Aroclor-1221. ——— Aroclnr-1232——— Aroclor-1242._ — Aroelor-1248- — Aroc lor-1254. — -Aroc lor-1260

FORM I PEST

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

.110

.110

.110

.110

.530

.110

.530

.5302.100.530.530.530.530.5301.1001.100

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI9

1/8744Rev

O.t.

Quant Output FInstrument

ft"', Cft137SG,QG70044,L:G2,940,10

: :AQ

-

945

QUANT REPORT

Operator ID: KT8582 QuantOutput File: ^HA245::AQData File: >HA245::U4Name:Misc: CA1379G,QG70044,L:G2,940,10

ID File: I044IP::USTitle: IFB/PST/PC8 1.5SSP225Q/1.95SSP24Q1Last Calibration: 891030 12:07

7 Quant Time:Injected at:

Di lut ion Factor:Instrument ID:

2UL INJ

Page. 1

891030 12:32891027 22:15

1.00000HA


19) tDibutylchlorendate


29.15 1747 100609 .0754 UG/ML 100

946


ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code:

Contract:

Case No.:

Matrix: (soil/water) UIATER

Sample wtx^ol: 980.0 Cg/mL) ML

Level: ClowXmed) LOW

\ Moisture: not dec. dec.

Extract ion: (SepF/Cont/Sonc) CONT

GPC Cleanup: (YxN) N pH:

CAS NO. COMPOUND

SAS No.: SDG No.:


Lab File ID: >HA246

Date Received: Q9x-3 >89


Date Analyzed: 10x27x89

Dilut ion Factor: 1

CONCENTRATION UNITS:(ugXL or ugXKg) UGxL Q

319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-39-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

- — alpha-BHC—— beta-BHC—— delta-BHC---aamma-BHCCLindane )—— Heptaehlor——— Aldr in---Heptach lor epox ide—— Endosulfan I---Die Idr in—— 4.4'-DDE---Endr in , , ,—— Endosulfan I I—— 4. 4 '-ODD- — Endosulfan sul fate—— 4.4--DDT---Methoxychlor— -Endr in ketona niiii-in- — a Ipha-Ch lordana---gamma-Ch lordana ..,„....,.,—— Toxaphana—— Aroclor-1016—— Aroelor-1221—— Aroclor-1232—— Aroelnr-1242—— Aroelor-1248—— Ar iclnr-1254——— Aroclor-1260

FORM I PEST

.051

.051

.051

.051

.051

.051

.051

.051

.100

.100

.100

.100

.100

.100

.100

.510

.100

.510

.5102.510.510.510.510.51011

1tuIUIUIUIUIUtuIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

9471X87 Rev

CHROtlflTOGRflhFlit >Hfl246 1.0 AMU.

eee 1206

Cfll382GtQG7Q044,L

1600 3000

IS 16

Data File: >HA246::U4Name:


riisc: CA1382G,QG70044,L:G2,980,10

Id File: I044IP::USTitle: IFBxPSTxPCB 1.5SSP2250xl.95HSP2401 2UL INJLast Calibration: 891030 12:07


948

QUANT REPORT

Quant Rev: 7Operator ID: KT8582Output File: ^HA246::AQData File: >HA246::U4Name:Misc: CA1382G,QG7QQ44,L:G2,980,10

ID File: I044IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95XSP24Q1Last Calibration: 891030 12:07


Di lut ion FactorInstrument ID:

2UL INJ

891030 12:34891027 23:03

1.00000HA

Compound R.T. Scanfl Height Cone Units

19) *Dibutylchlorendate


29.15 1747 104961 .0787 UG/ML 100

949

IDPESTfcIDE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont rac t

SAS No.

M a t r i x : (soil/water) SOIL

Sample wt/vo 1 :

Level: (low/med) LOW

9i Moisture: not dec. 17 dec.

Extraction: (SepF/Con t/Sonc) SONC


SDG No.:


Lab File ID: >HA513

Date Rece ived: 09/23'-'89

Date E x t r a c t e d : 10/04/89


D i l u t i o n Fac t o r : 1

GAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug-'Kg> UG/KG

3-19-64-6-—————— alpha-BHC________719-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-6'5-9---------gamma-BHC<Lindane).76-44-8--- ————— Heptachlor________309-00-2- —————— Aldr in____________1024-57-3-------Heptachlor epox ide.959-98-8--------Endosulfan I______60-57-1----- — — Die Idr in_________72-55-9 ——— ——— -4, 4'-DDE__________72-20-8---------Endrin____________33213-65-9 ————— Endosulfan I I____72-54-8 ————— ——4 ,4'-ODD__________1031-07-8- —----Endosulfan sulfate,50-29-3 ———————— 4,4'-DDT__________72-43-5-----—--Methoxychlor______53494-70-5------Endrin ketone_____5103-71-9---—--alpha-Chlordane___51G3-74-2-------gamma-Chlordane___8001-35-2-------Toxaphene________12674-11-2 — —— -ArocI or-1016______11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— Aroc lor-1232______57469-21-9------Aroclor-1242______12672-29-6———--Aroclor-1248______11 097-69-1------Aroclor-1254______11096-82-5——---hroclor-1260______

VrfO

<f

Q

I111IUIK!UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST950

1/87 Rev.

CHROMflTOGROMFile >Hfl583 1.0 amu.

40Q - 800

0.0700766,0.873976,31';

2000

48000

36000

160009

IS 16 20 24 28

Data File: >HA503::U4 Quant Output File:Name: Instrument ID: HAMisc: QC70076G,QG70076,S:G7,30.0Q,,40

Id F.i le: I076IP: : UST i t l e : IFB/PST/PCB 1. 5*SP225Q/1. 95*SP24Q1 2UL INJLast Calibration: 891114 08:52

Operator ID: YY6148Quant Time: 391114 09:17I n j e c t e d at: 891114 08:34

951

QUANT REPORT Page 1 .

Operator ID: YY6148 ' Quant Rev: 7 Quant Time: 891114 09:17O u t p u t F i l e : AHA5Q3::AQ I n j e c t e d at: 891114 08*34Data File: >HA5Q3::U4 D i l u t i o n Factor: 1.00000Name : Ins t rumen t I D: HAMisc: QC70Q76G,QG70076,S:G3,30.QO,40

ID F i l e : IQ76IP: : UST i t l e : IFB/PST/PCB 1 . 5KSP2250/1 . 9SSSP2401 2UL INJLast C a l i b r a t i o n : 891114 08:52

Compound R.T. Scanft Height Cone U n i t s q

3) ttDeta BMC —————— 'A>t 6.87 410 85440 .0275 UG/ML 10019) #Dibutylchlorendate 29.12 1745 405315 .221 UG/ML 100


952

CHRQflflTOGRPnFile >KB189 l.e amu.

480 £000

26 32

Data F i l e ; >KB138: :U2 Quant Output Fi le: *K8188::AQh4a me : I n s t r u me n t ID:Miac: O C 7 0 0 7 6 G , O G 7 0 0 7 6 , S : G 3 , 3 0 , 4 0

Id F i le : I O ? 6 l C : : U ST i t l e : 1FB---PSTXPCB 6' X 2 MM ID 3*SP-21QO 2 UL INJLast C a l i b r a t i o n : 891128 00 :29

Opera to r ID: KT8582Quant T ime: 8Q1128 00:48I n j e c t e d at : 891123 00:13

953

QUANT REPORT

Operator ID: KT8532Output File: AKB188::AQData File: >KB138::U2Name:Misc: QC70076G,QG70076,S:G3,30,40

Quan t Rev: 7 Quant TimeInjected at

Dilution Fac torI ns t rumen t ID

Page 1

891128 00:438*1128 00:13

1.00000

ID File: I076IC:: USTitle: IFB/PST/PCB 6' X 2 MM IDLast Calibration: 391128 00:29

Compound

3*SP-21QO 2 UL INJ

R.T. Scan# Height Cone Un i ts

954

ETC

STANDARDS DATA

955

0102030405060708091011121314

8DPESTICIDE EVALUATION STANDARDS SUMMARY

Lab Name:ETCNJ Contract:


Instrument ID: HA GC Column ID: 225Q/.' 401

Dates of Analyses: 10/26/89 to 10/30/89

Evaluation Check for Linear i t 1 -

PESTICIDE

ALDRINENDRIN4.4'-DDTDBG

CALIBRATIONFACTOR

EUAL MIX A

1523200.2243200. 1396800.1595250. 1

1 CALIBRATIONi FACTOR1 EUAL MIX B

i 1584320.21 249600.01 293120.01 622730.01

CALIBRATIONFACTOR

EUAL MIX C

148*800.0228160.0271680. 0552325.0

«/-10. i'lS)

T.34.6

20.9**6.0

Cl

If > 10.0*4 RSD , plot a standard curve and determine the ngfor each sample in that set from the curve.

Eva luation Check for 4,4' -DDT/Endr in Breakdown(percent breakdown expressed as total degradat ion

INITIALEUAL MIX BEUAL MIX BEUAL MIX BE 'AL MIX BEUAL MIX BEUHL MIX BEUAL MIX BEUAL 'MIX BEUAL MIX BEUrtL MIX BEUAL MIX BEi'*L MIX BEUAL MIX BEU^L MIX B

DATEANALYZED

10/26/8910/27/8910/27/8910/28/89

TIMEANALYZED

1519061020400612

ENDRIN

17.10.0

13.828.9»»

4,4'-DDT

8.46.48.521. 0*»

COMB I NED(2) 1

1

I

u^K 1

1-

1

1

1

t

i

See form i n s t r u c t i o n s .

FORM UII1 PEST-1 1/87 Rev.

956

8EPESTICIDE EUALUATION FOR STANDARDS SUMMARY

E v a l u a t i o n of Retention Time Shift for Dibuty1chlor-mdat

Lab Name:ETCNJ

Lab Code:

I n s t r u m e n t ID: HA

Case No.J

Cont rac t:

SAS No.: SDG No.:

GC Column 10:2250/2-31


01020304

06070809101112131415161718

202122232425262728293031323334

363?38

EPA 1 LAB SAMPLESAMPLE NO. i ID.......... [............

1 EUALA1 EUALB1 EUALC1 IMDA1 I NOBIDDII D D I I1 DD I I I1 TOXAPHIAR10161 AR1221IAR1232IAR12421 AR1248IAR1254IAR12&QIQC70Q25GICA1360GICA1860GSICA136GGRIQC70025GS1 EUALBIQC70Q44GICA185BGICA1858GSICA185SGRIDC70Q44GS1 I NDAICA1372GICA1373GICA1374GICA1375GiC«1376G1 EUALBICA1377GICA1378GICA1382G

,I UCTOOA^'E

DATEANALYZED

10/26/8910/26/3910/26/8910/26/3910/26/8910/26/3910/26/8910/26/8910/26/8910/26/8910/26/8910/26/8910/26/8910/27/3910/27/8910/27/8910/27/8910/27/8910/27/8910/27/3910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/-27/8910/27/8910/27/8910/27/8910/27/8910/27/8910/27/89

TIMEANALYZED

14371519160217241807185019322015205721402222230523470030011201550237032004020445052306100653073508X809Q10943i0261643173018181*05195320402128221523032351

%D

0.0. 1

0. 0- 1. 1. 1.1- 1.1. 1.1. 1.11.1. 1.1. 1. 1.2.2.2.2.2.2-2.1.1.1.2.22.2. 1.2.2.2.2

»

<JA

Ualues o u t s i d e of QC l i m i t s (2.OS for packed columns,0.3S for capillary columns)

page 1 of 2957

FORM U I I I PEST-2 1/87


Evaluation of Retention Time Shift for Dibuty1chlorendate

Lab Name:ETCNJ

Lab Code:

Instrument ID: HA

Case No.:

Cont ract:

SAS No.:

GC Column ID:2250/2401


1 ERA1 SAMPLE NO.

01 10210 3 10410 5 10610710 8 10* 1101111121131141151161171181lv |20 121122123124125126 12712812913 0 131 132133 13413 5 13613 7 1381

LAB SAMPLEID

Z5tK37^UJ v* U U -^ U 3

INDBICA13Q1GCA/IO/4C ft 1 3 0 1 G GO1/V V-cm3eicRc/w *<«Cftl37-9S CAM vt>L«r W 1. *f U \J IJt*"7 * *

EUALBCA177^GC4/f^I NDA <S**,a jINDB ,o/5" AH

DATEANALYZED

lU'^C)'' O"

10/28/6910/28/89

tf 10/28/89* 10/28/89"* lU'iO'HTi L\jS £#s t$y

10/28/89^ 10/28/89

1 10/30/8910/30/89

TIMEANALYZED

0038012602130301034904360524'3612065909291017

SD

0 . 0. 1

0 . 00. 00 . 0

. u0 . 0. 1

0 . 0.1

0 . 0

»

Ua lues outside of QC l i m i t s (2.OS for packed columns,0.3S for capillary columns) 958

page 2 ofFORM "JI I I PEST-2 1/87 Rev.

C*lib F i l * i C044IPtiUS Comp #C * l i b 0*t»i 891030 11:16

4.4--EDE.24-

.20-

Conc ..1*-

.15-

.16-

.ee-

.04-

.0

400090

C'jmpound * 1 C a l i b File: CC44IP::US

Compound: 4,4'-DDEIs. d:

File: >HA215 >HM216 ''HA217C;.<nc: . 0100 . 0^00 .200

Rf: .29E+7

Average of 3 Rfa:1st Degree E q u a t i o n :

lit. Decree Corr Coef:2nd Degree Equat ion:

2nd Decree Corr Coef:

.33E+7 (10.91 K Rsd)y * -.002077 + .OOOQQ03<x).9993346y - .0028279 * .0000002Cx)

.0000000 Ry: .0000000

00000001.000000

In the above equat ions'.

Cone Sld Area Std9 ~ --------- x - ————————

Cone Istd Area Istd

Istd Cone for all c a l i b r a t i o n points is: 1.

959

Cilib Film'. C944IPi:US Comp # gCalib D»l«: 891030 11:16

: 4,4'-COD

Cone .US/ML

200393 406(300

R«>pons« Ratio

Compound C a l i b File: CO*i4IF::US

HA217.200

.24E+7 (10.99 S Rsd) Rx: . 0 0 0 0 0 0 0 Ry:y - - .001330 + . 0 0 0 0 0 0 4 ( x ).9995250

Compound: 4 ,4 ' -ODDIs; d:

Fi le: >HA215 >HA216Cone: . 0100 . 0 5 0 0

Rf: .21E+7 .26E+7 .

Average of 3 Rfa:1st Degree Equation:

1st Deuree Corn Coef:2nd Degree Equation: y - .0027633 + .0000003(x) + .OOOOOOQ(

2nd Degree Corr Coef: 1.000000

In the above equations:

Cone Std Area Stdy " ————— * • —------

Cone Istd Area Istd

Istd Cone for all calibration points is: 1.00

.0000000

960

C*lib Fil«t Cd44IP:tUS Comp * 3Calib D*t«) 891830 11:16Comp: 4,4'-DDT

.34-

Conc .US'IIL

e.eo-

Response Ratio

C> mprjund # 3 Calib File: C044IP::US

Compound: 4 ,4 ' -DOT

File: >H*215 >HA216 >HA217Cone: .0100 .0^00 .200

Rf: .13E*7 .23E+7 .23E+T

Average of 3 Pfs: .21E*7 (14.68 S Rsd) Rx: .0000000 Ry=1st Degree Equation: y - .0011237 * ,OOOOOG4fx)

1st Degree Corr Cuef: .99989992nd Degree Equation: y • .0029836 + .0000004(x> + .0000000(xA2 ;

2nd Decree Corr Coef: 1.000000


Cone St-d Area Stdy • ————— * " —------

Cone Istd Area Istd

Istd Cone for all calibration points is: 1. (H-

.0000000

961

3DPESTICIDE EUALUATION STANDARDS SUMMARY

Lab NameiETCNJ Contract:


Instrument ID: HA GC Column ID: 2250/2401


Evaluation Check for Linearity

11 PEST 1C IDE11 .............IALDRIN1 ENDR I Nl*+.4'-DDT1 DBCt

CALIBRATIONFACTOR

EUAL MIX A

13496GO. 5512000. 1772800. 1752000. 1

CALIBRATIONFRCTOP

EUAL MIX B.............

1-937920.5526720.0734720. 0754560. 0

CALIBRATIONFACTOR

EUAL MIX C«.»....--».

1871770. 0486720. 0725760. 0694080. 0

% RSD'. < .-•'«10.0%)

2.44. 01.44.7

'1) If > 10.Q9ti RSD, p l o t a standard curve and determine the ngfor each sample in that set from the .curve.

Evaluation Check for 4,4'-DDT/Endr in Breakdown(percent breakdown expressed as t o t a l degradation)

0102070405060708091011121314

INITIALEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BE'JAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX B

DATEANALYZED

11/13/8911/14/8911/14/89

TIMEANALYZED

180312312018

ENDR IN

--------

15.214.312.8

4,4'-DDT

........

7 . 14.65.5

COMBINEDC2)

( 2 ) See form instructions.

FORM 01 I I PEST-1 1/37 Rev.

(1 )

962


Evaluation of Retention Time Shift for Dibutylchlorendate

Lab Name:ETCNJ Con t rac t

Lab Code: Case No.: SAS No.: SDG No

Instrument ID: HA GC Column 10:2250/2401


010203040506070809101112131415161"?181920212223242526•~>~>2329303132333435363"738

EPA 1 LAB SAMPLESAMPLE NO. 1 ID

IEUALA1 EUALB1 EUALC1 INDAt I NDB1 TOXAPH1 AR1016IAR1221IAR12321 AR1242IAR12481 AR1254IAR1260IQC70076GICA1368GICA1368GSICA1368GRICA1369G1 EUALBICA1370GICA1365GICA1366GICA1367GICA2013G1 INDA1 GPCBLANKIOC70Q76GS1 EUALB! INDA1 I NDB11I11111

DATEANALYZED

11/13/8911/13/8911/13/8911/13/8911/13/8911/13/8911/13/8911/13/8911/13/8911/14/8911/14/8911/14/8911/14/8911/14/8911/14/8911/14/89ll'14/8911/14/8911/14/8911/14/8911/14/8911/14X8911/14/8911/14/8911/14/8911/14/8911/14/8911/14/8911/14/8911/14/89

TIMEANALYZED

171718031848193420202105215122372323000800540140022508340928101310591145123113161402144715331618175818431929201821122158

D

0. 0. 1

0.0.1. 1. 1

0.0. 1

0.0. 1. 1.1. 1.3. 1.2.2.2

0. 0.2.2.2.2. 1.1.3.3

1.51.92.5

*

*

Ualues outside of QC l i m i t s (2.0% for packed columns,0,3% for c a p i l l a r y columns)

963

page 1 ofFORM UII I PEST-2 1/87 Rev

8DPesticide Evaluation Standards Summary

Lab Name:ETC Co rp. Contract:

Lab Code: Case No.: SAS Mo.: SDG No.:

Instrument ID: JB GC Column ID: : VSP-2100

Dates of Analyses: velSc/^f to ».o(

Evaluation Check for L i n e a r i t y

PESTICIDE

ALDRINENDR I N4,4'-DDT ____OBC

CALIBRATIONFACTOR

EUAL MIX A

17099102. 01456000.2526600. 17^7600. 1

CALIBRATIONFACTOR

EUAL HIX B

2547220.51662730. 0509440. 0617230. l

CALIBRATIONFACTOR

EUAL MIX C

2489610. 01696650. 043 3 5 2 S . 08U6QS? . 0

% RSDI </•1 0 . LI «; )

101.1**S. 14. ?2.6

1) If > 10.0'« RSD, plo t a standard curve and determine the; ngfor each sample in that set from the curve.

Evaluation Check for 4,4 -DDT/Endrin Breakdown(percent breakdown expressed as t o t a l degradation'

• 111 =«,*.» = „...

1 I N I T I A L01 1 EUHL nix B02 I E' AL MIX B0 1 \ EUAL M I X B041 EUAL MIX BO1;. I EUAL MIX B06 1 EUAL MIX B0 M E'JAL MIX BLI 8 1 EUAL MIX BCIV 1 E'JAL MIX B10 1 EUAL MIX B11 ! EUAL MIX E12 ! EUAL MIX B15 1 E'-'AL MIX B141 E'JAL MIX B

1

DATEANALYZED

10/50/8910/31/39

TIMEANALYZED

17370011

ENDR 1 N 4,4 -LJUT COME into12 1

6.41C. 7

(2) See form i n s t r u c t i o n s .

FORM UI I 1 PEST-1 1 '87 Rev

(1

964

8EE'.'a l u a t i o n of Re tent ion Time Shift for D i b u t y l c h l o r e n d a t e

Lab Name:ETC Corp. Contract:

Lab Code: Case No.: SAS No.: SOG No.:

Instrument ID: JB

Dates of Analyses:

GC Co 1umn ID:? V3P-2100

\O/3<

1 EPA1 SAMPLE

01 !02!03 I04 |05 !06 !07!03 109 110 111112 117 114115 116117118 119 I20 121 122 127 124125126 127|2312P I30 131 t32 133 t34135 176 1T- |

781

1 LAB SAMPLENO. 1 ID

IE UAL A1 EUALB1 EUALCt INDA! INDBIQC70025&ICA1974GIQC70U26GICA1976GICA19~'7G1 EUALBICA1973GIOC70021GICA1371G1 I MO A1 I NOB1t11111111I!i11t111|1!

DATEANALYZED

10/30/8910/30/8910/30/39 •10/30/8910/30/8910/30/8910/70/8910/30/8910/30/3910/30/8910/31/8910/31/8910/31/8910/31/3910/31/3910/31/89

TIME 1ANALYZED 1

« = = » = = = *.. | =1652 I1737 11313 !1358 !1943 12023 12112 12157 1•-. 0 ' o |

" 1 •-] —t \*..•*.' \0 0 1 1 i0056 !0141 :0225 !0310 10355 1

!1!!t1|1111111!111111!

% \D 1 *

0.01. 1 1. 1 1. 1 1.2 1

C . 0 t0.01. 1 1. 1 1. 1 1. 1 1. 1 1. 1 !. 1 1. 1 i.2 1

I1Ii!

1i

111;1!111!1tI11

''a lues outside o t" QC l i m i t s (2. OH for packed column 5,0.7% for c a p i l l a r y columns'

p a 9 e 1 o f 1965

FORM UII[ PEST-2 1/87

3DPESTICIDE EUALUHTIQN STANDARDS SUMMARY

Lab Name:ETCNu Contract:


Instrument ID: KB GC Column ID: 5SSP-2100

Dates of Analyses: ll/27.'89 to Ilx28'89


1(PESTICIDE

ALDRINENDRIN4. A '-DOTDBC

CALIBRATIONFACTOR

EUAL MIX A

913600.2483200. 1211200. 0294400 . 1

CALIBRATIONFACTOR

EUAL MIX B

930560.35?D32Q.O196480 . 0317440 . 0

CALIBRATIONFACTOR

EUAL MIX C

976000. 0532800.0276160.0299200. 0

% RSD

10 . OH J.«=,...

3.25 . 79 . 34. 0

'.I.1 If > 10.OS RSD, p l o t a standard curve and determine the ngfar each sample in that set from the curve.

Evaluation Check for 4,4'-ODT-'Endrin Breakdown(percent breakdown expressed as t o t a l degradation)

0102030405Do0706Oq

1011

INITIALEUAL MIX BEUAL MIX BEUAL MIX 6EUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX B

DATEANALYZED

11x27. -'8911 '26 '8*11 '28 '89

TIMEANALYZED

201703291219

ENDRIN ^,4' -DDT COMBINEDC2:<

6 .99.25.9

' 2 .' See form instructions.

FORM UI I I PEST-1

(1)

Rev.

966

8EPESTICIDE EUALUATIQN FOR STANDARDS SUMMARY

Evaluation of Retention Time S h i f t for Dibutylchlorendate

Lab NamesETCNO

Lab Code: Case No.:

Instrument ID: KB

Con t rac t :

SAS No.: SDG No.:

GC Column 1C': 3KSP-21QO


01020704

0506

OS091011121314

2021.-i.-,

24 I25 I2o I

28

30 i

73 !341

36 i

79

EPASAMPLE NO.

LAB SAMPLEID

EUALAEUALBEUALCINDAI MDBAR1254AP1260QC"*Q076GCA1369GCA1770Grnn10TG CA 3M :~t r* "? r * n R rz — **• *wL* ' y u v ij liiA tf"!EUALBCA2346GCA234~T'GCA2343GCA2344GCA2342GI NDAQC70050GCA1930GOC70055GCA2150GEUALBINDAINDB

DATEAI-4ALYZED

11/27/8911/27 --39ll--'27-''8g1 1 1 •' O ~? / O QJ. X ' 4m f • O '

11/2 7 --'8 9ll/27.-'8911/27/8911/23/3911/28/89ll''28/39

6 11/28/8911/23/8911/28/8911/28 ""3911/28/8911 '28/8911/28/8911/28/8911/28/8911/28/8911/28/8*11/28/8911/28/8911/28/8911/28/8911/28/89

T I HEANALYZED

197820172056217622152254277300130052013102100250032*040804 +80527Do 0603240Q030942102211011140121912591338

D

0. 00.0. 1

0.0. 1

. 0. 0. 1

0.0. 1.2.2. s.

. 1

.3

. 31.9

T

.3

.3

.4

.3

. 3

*

****

* Us I Lies outside of QC l i m i t s (2.0?S for packed columns,0.7S for c a p i l l a r y columns)

967

page 1 oFHPM IM I 1 PF=.T-?

8DPESTICIDE EVALUATION STANDARDS SUMMARY

LabName:ETCNJ Contract:


Instrument ID: QB GC Column ID: 2250/2401

Dates of Analyses: (0/A^XPf to (*/?S~/jrf


11 PEST 1C IDE1!.«.».. -..«».1 ALDRINIENDRIN14. 4 '-DOTIDBC1

CALIBRATIONFACTOREUAL MIX A

...»»«.»..2528000.5992000.2S 763 00. 1659200. 1

CALIBRATIONFACTOREUAL MIX B

2635440.51041280. 01226240. 0686030. 0

CALIBRATIONFACTOR

E'JAL MIX C

2631690.0993405 . 01236485.0667200. 0

X RSD( <./=10. 0!i)

3. 12.718.4**2. 1

(.I.- If > 10. Ot RSD, pl o t a standard curve and determine the ngfor -each sample in that set from the curve.

Evaluation Check for 4,4'-DDT/£ndrin Breakdown(percent breakdown expressed as t o t a l degradation)

0102030405060708091011121314

INITIALEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX BEUAL MIX B

DATEANALYZED

10/24/3910/25/89

TIMEANALYZED

13250704

ENDRIN

9.710.2

4,4 ' -DOT

3. 010.8

COMBINED(2)

f 2 ) See form instructions.

FORM UI I 1 PEST-1 1/87 Rev

968


Evaluation of Retention Time Shift for D\buty1chIorendate

Lab Name:ETCNJ

Lab Code: Case No.:

Con t r a c t

SAS No.: SOG No

Instrument ID: QB

Dates of Analyses: (0/-? /£<? t o

GC Column 10:2250/2401

01020304051360703091011121314151617IS192021•->•?2324252627.-i,j293031T-'

35363738

ERA 1 LAB SAMPLESAMPLE NO. 1 ID

IEUALAIEMAL81 EUALC1 INDA1 I NOBIDDIIDDI II DD I I I1 TOXAPHIAR10161 AR12211 AR12321 AR1242t API 2 431 AR12541 AR12601QC70021GICA18S9GSICA1359GR1 CA1859G1CA1371GI EUALB1 QC^O 020G /owPWrrVQtinClCi^^065GICA2&**€LCfV""V~'C "1 INDA p| Yt INDB M|"" '11t111111

DATEANALYZED

10/24x8910/24/3910/24/8910/24/3910/24/8910/24/3910/24/8910/24/3910/24/8910/24/3910/24/3910/24/8910/25/8910/25/3910/25/8910/25/3910/25/8910/25/3910/25/8910/25/3910/25/8910/25/8910/25/8910/25/3910/25/8910/25/3910/25/8910/25/8910/25/89 •

TIMEANALYZED

08221725141214591545163217191806185319402027231500020049013602230310035704440531061807040819090609531040112713531531

D

0. 0i J.

.3

. 3

.3

.3

.27.3

< i..2.2.2.2•72

. 4

. 6

. 2

1.71.21.21.42. 1O T

1.83.94.6

Ualues outside of QC l i m i t s (2,0% for packed columns,0.3S for c a p i l l a r y columns)

page 1 of969

FORM MI I I PEST-' 1/87 Rev.

C»lib Fil«i CBSlIPnUS Comp # 1C-lib D*t«i 891325 06i57Compi 4 , 4 ' - [ D E

Cone .

e.ee-1

eeeeeeR«»pon»« R*tio

Compound * 1 Cal ib File: C021IP::US

Compound: 4,4'-DDEUtd:

File: >0&825 >CB826 vQB827Cone: .0100 .0500 .200

Rf: .41E+7 .46E+7 .48E*7

Average of 3 Rfs: .45E+7 ( 7.31 S Rsd) Rx: .0000000 Ry:1st Degree Equation: y - .0019513 + .0000002Cx)

1st Degree Corr Coef: .99998192nd Degree Equation: y - .0010875 + .0000002Cx) + -.000000Cx^2 -



Cone Std Area Stdy • _ _ _ _ _ _ _ _ _ X • ---———----

Cone Istd Area Istd

Istd Cone for all calibration points is: l.OC

.OOOOOOC

970

C-llb Fil-i CaSlIPnUS Conp #Ctlib 0-t.i 891QE5 68:57Compt 4 , 4 ' - [ D O

Cone

e.ee-1433000

R*spon*« Ratio800090

Compound * 2 Calib File: C021IP::US

Compound: 4,4'-ODD13 t d :

File: >QB825 >OB826 >QB827Cone: .0100 .0500 .200

Rf: .31E+7 .36E+7 .35E*7

H^erage of 3 Rf*: .34E*7 C 7.76 S Rsd) Rx: .00000001st Degree Equation: y « .0006146 + .0000003(x)

1st Degree Corr Coef: .99997012nd Degree Equation: y - .0017008 + .0000003Cx) + .0000000(x


In the aboue equat ions:

Cone Std Area Stdy * _ _ _ _ _ _ _ _ _ x - ---------

Cone Istd Area Istd

Istd Cone for all calibration points is: 1.00

0000000

971

ZL6

O O O O C O O * 0 0 0 0 0 0 0 '

0 0 • I : * i

p 5 *• x

3003

:euoi)cnba

O O O O O O ' I

6608666*C * ) £ Q O O Q O O * + 69^1500' - *

D O S '

JJ03 eajBaQuoi

bO 1 0 0 1 0 ' !9S89D<

S n : : d I I 2 0 D = £ * punoduirQ

iijxsn• 3UOO

I O ] - . * * > idu tooC20T68 t » > V Q q t [ » o

sri"dIT500 » » I ? J q ? I » 0

PESTICIDE''PCS STANDARDS SUMMARY

Lab Namt: ETCNJ

Lab Code:

I n s t r u m e n t ID: HA

Case No.:

Con t rac h i

SA3 No,: SDG No.:

GC Column ID: 2250x2*01

11 COMPOUND11 .............l a l p h a - B H C[beta-BHCI d e l t a - B H C1 .-jamma-BHC1 Hep t ach lor1 rt I d r i n1 Hept . epox i de1 Endosu 1 f an I_1 D i e 1 d r i nl«. 4 '-DDE1 Endr i nlEpdo&u 1 fan I I14.4'-DDD1 E'-ido . su 1 f a t eI4.4'-DDT1 Me t ho *ych I o r _ _1 End r i n U.e tone1 a . C h ! o r d a n eI g . Chlordane_1 TO •". api >ene1 Aroc lor-10161 A r o c I O r - 1 '2 2 11 Aroclor-12321 nr oc lor-12421 Aroclor-12481 Aroc lur-12541 A r oclor-126Q_1

DATEtS) OF FROM: 10X26X89ANALYSIS TO: 10X27-'89T I M E l S ) OF FROM: 1724ANALYSIS TO: 0155

RT

4.486.937.985.887.258.67

12.3814.6016.7016.2513.7720.8820.7226.1722.7030.3530.3314.2813.3821. 037.274. 107.277.27

12.6817.1327.55

fW i t

FWOM4 . 56.907.955.837. 198.61

12.3514.5216.6416.2018.7220.8120.6726.0922.6230.2530.2614.2513.3520.377. j.94. 067.197. 19

12.5616.9627.27

?T I-JDOU (CALIBRATION

TO I FACTOR...... !.»......*..

4.511 28163606.961 8217608.011 14553605.941 22937607.311 19456008.721 17510-40

12.411 147456014.681 126208016.761 116992016.301 112446018.321 24832020.961 75520020.771 83712026.241 65536022.731 66830030.451 26649630.411 35712014.311 106624013.411 133120021.291 25^927.341 2873604.141 795307.341 7,83367.341 1219Q4

12.81 1 3516417.301 6668827.831 107649

1

DATE OF ANALYSIS 10x27x8"TIME OF ANALYSIS 1026EPA SAMPLE NO.(STANDARD) I^DA

RT

5.887.258,67

12.3314.5816.70

20.87

22.o830.33

1 iC A L I B F A T I O N I Q N T I so

FACTOR l Y x N t........... | ... .....

11i

2426881 1 Y 5.82104720 l Y 8.21853440 1 Y 5.81460500 i Y 1.01374740 1 Y 8.9124~i7Q ! Y 6.3

1i

825610 1 Y 1 9,3i i1 1

766^30 ! Y :l-*.626*802 1 Y I 6.0

1 !

1 1,

1 1! [

1 1

! 1< i1 1

Under QNT Y-'N:SiO mu-r t be lessor equa1 to 20.

enter Y if q u a n t i t a t i o nthan or equal to 15.OS

OS for c o n f i r m a t i o n .

was performed, N ifor quant i tat ion,

f not per f- orm-and less than

Nu t e: Dfcf. e r m i n i n g that no compounds were found abo^e the CRQL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.0% cr i • -sr i*

F'.i r- m i j i t i c o m p o n e n t a n a l y t e s , the s i n g l e largest peak that is c h a r a c t e r i a t i cof the component a h o u l d be used to e s t a b l i s h r e t e n t i o n t i m e and ;»D.I d e n t i f i c a t i o n of such a n a l y t e s is based p r i m a r i l y on p a t t e r n r e c o g n i t i o n .

page 1 of FORM IX PEST 1x8 Re'

973

PESTICIDE'-PCB STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code:

Instrument ID: HA

Case No.:

Cont rac t :

SAS No.: SDb No.:

GC Column ID: 2250/24.31

11 COMPOUND!|.......»«.M..1 a Lpha-BHCIbeta-BHC1 d* 1 1. a-BHC1 uamma-BHC1 Hep t ach lor-1 A 1 dr in1 Hep t , ep.o * i de1 Endosu 1 fan I1 Die 1 d r i n14.4'-DDE1 Eridr- i n1 Endosu 1 fan II1 « .4 ' -0001 Endo . su 1 f a teI4,4'-OOT1 Me t hoxych 1 or1 Endr in ke t one1 a . Ch lor dar.i*_1 g . Ch 1 ordane_1 Toxao^ene1 Aroc lor-1016lAroclor-1221IAroclor-12321 "-ti'OC I rj r' ~ 12** 21 Aroc lor-12481 Mroc 1 or- 1254__1 Arac lor-12601

DATECS) OF FROM: 10/26/89ANALYSIS TO: 1Q/27---89TIME'S) OF FROM: 1724ANALYSIS TO: 0155

RT

4.486.937.93£.837.258.67

I.-. T Cii . >0

14.6016 . 7016.2518.7720.8320.7226. 1722.7030.3530.3314.2313.3821. 087.274. 107.277.27

12.6817. 1327.55

fUllr

FROM

4.4$6. '507.955.837.198.6112.3514.5216.6416.2018.7220.3120.6726.0922.6230.2530.26la. 2513.3520.877. )94. 067.197.19

12.5616.9627.27

?T 1>iOOU 1

TO 1...... |

4.51 !'6.9618.0115.9417.3113.72 112.41114.68116.76116.30118.82120.96120.77126.24122.7813 0 . 45 130.41 114.31 113.41121.29 17.3414. 1417.3417.341

12.31117.30127.331

1

CALIBRATIONFACTOR

23163608217601455360229376019456001751040147456012620801169920112^430248320755200837120655360663800266496357120106624013312002579228736079530783361219848516466688107649

DATE OF ANALYSIS 10/28/89TIME OF MHALVilS 0126EPA SAMPLE NO.(STANDARD) INDB

RT

4.486. "527.98

1i CALIBRATION1 FACTOR

I 30374401 3665601 1547520i

1 1JNT 1 ;D

1 Y/NI

1 Y 1 7.3i Y i 5.51 Y 1 6.3

t 1 11 I1 1 1

16.2318.75

20.7026. 13

111 119~4401 33408011 8908801 7232101

i :1 1i Y I 6,51 Y 134.5*i 11 Y 1 6.4i Y IL0.41 1

1 . >30.3214.2813.37

1 389130I 11136001 1421^001i1

1 Y 1 9.01 Y 1 4.4i Y 1 6.71 1i i1 1

1 i i1 1 11 1 !1 1 11 i 11 1 1

under ONT Y--'N:Jifj rim1* t D* 1 e*-or equal to 20

enter Y if quantitation• than or- equal to 15.0%OS for confirmation.

was performed, N if not per-rorrn*for q u a n t i t a t i o n , and less than

Note! Determining that no compounds w«r« found above the CRCL is aq u a n t i t a t i o n , and therefore at least one column must fiiee t the 15. 0\

f o rnt ofc r- ; • «r i a

For muiticomponent anatytes, the single largest peak that is characteristicof the compci nent should be used to establish retention time and ^sD.I d e n t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognition.

page 2 of FORM IX PEST 974 1/S' Rev

PESTICIDE/PCS STANDARDS SUMMARY

Lab Naitus; ETCNJ Contract:


Instrument ID: HA GC Column ID-1 22^0/2401

COMPOUND

alpha-BHCb*ta-5HCde 1 ta-8HCcamma -8HCHep t ach 1 orM i d r i nêp t . ep.ox i deEndos'j 1 fan I_Die Idr in ,..„_.„ _4.4' -DDEEnd r i nEndosu I fan IIir4'-DODEM do . su I fa t e4.4--DDTlift t ho :• VCh lo»'_

End r i n ke l one-i . Ch o rdaneg . Ch lordaneTovaDêneAroc lor-1016A r- o C 1 0 r - 1 2 2 1Aroclor-1232Aroc lor-1242Aroc lor-1248_Aroc lor-1254Aroc lor-1260

OATECS) OF FROM: 10/26/89ANALYSIS TO: 10/27/89TIMEfS) OF FROM: 1724ANALYSIS TO: 0155

RT

4.436.937.*35.3d7.258. 67

12.3814. 6016.7016.2518.7720.8820.7226. 1722.7030.3530.3314.2313.382 1 . 037.274.107.277.2712.6817.1327.55

FWU

FROM

4. 456.907.955.337. 198.61

12.3514.5216.6416.2018.7220.8120.6726 . 0922.6230.2530.2614.2513.3520.877.194. 067.197. 1912.5616.9627.27

?T 1ÔOUi (CALIBRATION

TO 1 FACTOR

4.511 281o3606.961 8217608. Gil 14553605.941 22937607.311 19456008.721 1751040

12.411 147456014.681 126208016.761 116992016.30 1 112448018.821 24832020.961 75520020.771 83712026.241 65536022.781 66330030.451 26*49630.411 35712014.311 10o624Q13.411 133320021.291 257927.341 2873604.141 795807.341 733367.341 121984

12.811 8516417.301 6668827.831 107649

1

DATE OF ANALYSIS 10/30/89TIME OF ANALYSIS *929EPA SAMPLE NO.C STANDARD) IfnJA

R"!

5.857.228.63

12 . 3714.5516.67

20.83

22 . 6530-28

1CAuIBRfTlONIQNTI SO

FACTOR iY/Ni........... |-..|.....

11 1

i2961920 1 Y 129.1*2563961 l Y i 2.0-2195201 1 Y 125.4*164*920 1 Y i L.91598720 1 Y 126.7"1442560 1 Y I'. 3.3*

1 1i 1

928640 1 Y 123.0*l t1 1

99*050 1 Y f-9.4*395268 1 Y 148.3-

1 1i 1

1 1 11 : .. 1i 1 11 < 1

t 1i 11 11 11 1

Under QNT Y/N: enter Y if q u a n t i t a t ion9iO rout 1 be less than or equal to 15.OSor equal to 20.OS for c o n f i r m a t i o n .

performed, N if not performerfor q u a n t i t a t i o n , and less than

Note:q jan t i t a

Determining that no compounds were found above theand therefore at least one column must meeti on ,

CPQL isthe 15. i"

form ofcr i a r i a

For mu,ticomponen t analytes, the s i n g l e largest peak that is c h a r a c t e r i s t i cof the component should be used to e s t a b l i s h r e t e n t i o n time and ' D.I d e n t i f i c a t i o n of such analytes is based p r i m a r i l y on p a t t e r n r e c o g n i t i o n .

page 3 of FORM IX PEST 975 1/8 Rev

PE5TICIDE/PCS STANDARDS SUMMARY

Lab Na'«e: ETCNJ

Lab Code:

Inst rument ID: HA

Case Ho.:

Con t rac t:

SAS NO .: SDL; NO . =GC Column ID: 2250/2401

t1 COMPOUND11 ...... ..„----lalpha-BHCIbeta-BHCIdelta-BHCI qamma-3HCIHeptachlor1 A l d r i n1 Hep t . epox ide1 Endosu 1 fan II D i e l d r in14, 4 '-DDE ____1 Endr in1 Endosu 1 fan I II4.4--DDD1 Endo . su 1 f a t e_14. 4 '-DOT1 Me thoxych 1 or_1 Endr i n ke tonela. Ch lordane_1 ci . Ch lordane_1 Toxaphene1 Aroc 1 or- 10 16IAroclor-12211 Aroclor-12321 Aroc lor-1242_lAroc lor-1248iAroc lor-12541 Aroc lor-12601

DATECS) OF FROM: 10/26/89ANALYSIS TO: 10/27/89TIMECS) OF FROM:1724ANALYSIS TO: 0155

RT

4.486.937.935.387.258.6712.3814.6016.7016.2518.7720.3820.7226. 1722.7030.3530.3314.2813.3821.087.274.107.277.2712.6817.1327.55

FUI

FROM

4.456.907.955.837.193.6112.3514.5216.6416.2018.7220.8120.6726.0922.6230.2530.2614.2513.3520.877.194.067. 197.1912.5616.9627.27

*T 1-ioou i CALIBRATION

TO 1 FACTOR

4.511 28163606.961 3217608.011 14*53605.941 22957607.311 19456008.721 175104012.411 147456014.631 126208016.761 116992016.301 112^43018.321 24832020.961 75520020.771 83712026.241 65536022.781 66880030.451 26649630.411 35712014.311 106624013.41 t 133120021.291 257927.341 2873604.141 795807.341 783367.341 12198412.811 8516417.301 6608827.831 107649

1

DATE OF ANALYSIS 10/30/89 1TME OF ANALYSIS 1017EPA SAMPLE NO. 1f STANDARD) P-.'B

1

RT

4.476, ''27.97

16.2218.73

20.6826. 12

30.2814.2713.37

Cr-LlBFATIONFACTOR

354562110Ci'.':2401820160

1370880440320

1012480840330

42945013 12 QUO1629440

1

fQNTI. SD 1Y/Ni... |-.... iY 125. 9»lY I.2.0*Y 125.1-1

>\ \11 1;1 I

Y U1.9-Y 177. 3»l

1Y 120.9-1Y 13.2*

1 1[

Y 120. 3*1Y I :. 1. 0«Y 122.4*1

11 1!1 11

___ 1 _____ 11t 1t

Under QNT Y/N: enter Y if quantitationSD must be less than or equal to 15.0%or equ41 to 20.OS for confirmation.

was performed, N if not performed,for quan t i ta-. i on , «nd !«ss i- sn

Note: Determining that no compounds wtere found above the C-'QL i ft a *> rm o -q u a n t i t a t i o n , and therefore at least one column must meat the 15.OS criteria

For mu 11 icomponen t analyLes, the single largest peak that is charaui.eri.vicor the component should be used to establish retention time and SD.I d e n t i f i c a t i o n of such analytes is based primarily on pattern recogn.tion

page 4 of FORM IX PEST 976 1/87


Lab Name: ETCNJ

Lab Code:

Inst rument ID: HA

Case No.'

Con t rac t

SAS No. SDG No

GC Column ID: 2250x2401

11 COMPOUND1|..........«».lalpha-BHCtbeta-BHC1 de 1 ta-BHC1 oamma-SHC1 Hep t ach lor1 A 1 d r i n1 Hep t . epox i de1 Endosu 1 f an I_1 Die Idr in14. 4 '-DDE1 End r in1 Endosu 1 f an II1 *4.4 ' -ODD1 Endo . su 1 f a t e!4.4'-DDT1 he thoxych 1 o r _1 End r i n I* e t oneia. Chlordanei q . Ch 1 ordane1 Toxaphene1 Aroc lor-10161 Aroc lor-12211 Aroc lor-12321 Aroc 1 o r- 12421 Aroc lor- 12481 Aroc lor-12541 Aroc lor-12601

DATE'.S) OF FROM: 11/13/89ANALYSIS TO: 11/14/89TIME'.S'J OF FROM: 1934ANALYSIS TO: 0225

1 RTRT t WINDOW

1 FROM 1 TO

4.486.937. 985.87~? oq8.6?12.3814.5816.7016.2518.7720.3720 .7226. 1322.7030.373 0 . 3 314.3013.3821. 087.274.107.277.2812.68.7. 152^.58

3.991 4.986.26 1 7.617.241 8.735.421 6.316.771 7.738. 13 1 9.2011.73! 13.0313.SSI 15.2915.991 17.4115. 191 17.3117.641 19.9020.071 21.6619.591 21.3524.831 27.4421.921 23.4829.251 31.4828.641 32.0313.311 15.2912.391 14.3720.871 21.297.19! 7.344.061 4.147.191 7.347.211 7.3612.561 12.8116.981 17.3227.311 27.86

1

CALIBRATIONFACTOR

418050115526402201600366082033382602590720222080019712011743370156096062144015732401185280102400010867204743701061770135472019212812694438489811622411187216205011909289344165953

DATE OF ANALYSIS 11x14/89TIME OF ANALYSIS 1758ERA SAMPLE NO.t STANDARD) INDA

PT

5.857.238 .6512.37"14.5716.68

20.85

22.7030.35

CALIBRATIONFACTOR

79091417613*612748160234752020761611858570

1679370

1210240526850

1

QNTY/N

YYYYYY

Y

YY

%D

6.38.26.15.75.36.6

6.4

11.411. 1

Under QNT Y/N: enter Y if quant i t a t ion was performed, N if not performed.*iD must be less than or equal to 15.09* for quan t i t at i on, and less thanor equal to 2 0 . 0'« for confirmation.

Note: Determining that no compounds were found above the CRQL is a form ofquant i t a t ion, and therefore at least one column must meet the 1^.0% criter i a

For mu 11 iccrnponer, t analyses, the single largest peak that is characteristicof the component snould be used to establish retention time and ?tD.I d e n t i f i c a t i o n of such analytea is based p r i n a r i l y on pattern recognition.

page 1 o V FORM l',< PEST 977 1 -87 Rev

PESTICIDE/RGB STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code:

Instrument ID: HA

Case No.:

Con t rac t:

SAS No.: SDG No.i

GC Column ID: 2250x2401

t1 COMPOUNDi

1 aloha-SHC1 beta-BHC _____I d e l ta-BHC1 aamrro-BHC1 Hep tach 1 or1 A Idr in1 Hep t . epox i de1 Endosu 1 f an I_1 D i c 1 d r i nI4.4'-DDE1 End r in1 Endosu 1 f an II14,4' -DDD1 Endo . su 1 f a t e14.4 '-DOT1 Me t hoxych lor_lEndrin ke t onela. Ch lordane1 q . Ch 1 o rdane1 Toxaphene1 Rroc lor-10161 A r o c 1 o r - 1 2 2 11 Aroc lor- 12321 Aroc 1 or- 1242I Aroc lor-1246lAroc 1 o r - 1 2 5 4_1 Hroc lor-1260I

DATEtS) OF FROM: 11x17/89ANALYSIS TO: 11/14x89TIME(S) OF FROM: 1934ANALYSIS TO: 0225

RT

4. 486.9?7.985.877.258.6712.7814.5816.7016.2518.7720.3720.7226.1322.7030.3730.3?14.7013.7821.087.274. 107.277.28

12.6817. 1527.58

fwit

FROM

3 . 996 .267.245.426 . 778. 1311.7713.8815.9915. 1917.6420.07lg .5924.8321.9229.2528.6413.3112.3920.877. 194. 067. 197.21

12.5616.9327.31

*TJDOW

TO

4. 987.618.736.317 . 7"^9.2013. 0315.2917.4117.3119.9021.6621.8527.4423 .483 1 . 4832.0315.2914.3721.297.344. 147.347.36

12.8117.3227.86

CALIBRATION'FACTOR

418050115526402201600366032073382602590720222080019712011743370156096062144015782401185280102400010867204743701061770185472019212812694438489811622411187216205011909289344165953

DATE OF ANALYSIS 11x14x89TIME OF ANALYSIS 2112ERA SAMPLE NO.C STANDARD) INDA

RT

6.127.528.9712.7514.9817. 10

21.32

23 . 1531. OG

CALIBRATIONFACTOR

415934138232012922440250198022162601994980

1807790

1287680544124

QNTY/N«»«

Y

YYYYY

SD

.....

————

13.614.512.812.712.414.4

1Y

YY

! •

14.5

18.5*14.7

—————

—————

Under ONT YxN: enter*iD must be less thanor equa1 to 20.OS for

Y if quant i tat ion wasor e q u a l to 15.OS forcon f i rrna t i on .

performed, N if not per formed.q u a n t i t a t i o n , and less than

Note: Determining that no compounds were found above the CRQL is a form ofquant s t a t i o n , and therefore at least one column must meet the 15.0fi c r i t e r i a

For multicomponent analytea, the single largest peak that ia characteristicof the component should be used to establish retention time and '«D.I d e n t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognition.

page of FORM IX PEST 1X87 Re-.-


Lab Name: ETCNJ

Lab Code:

Instrument ID: HA

Case No.:

Con t rac t:

SA£ No.: SDG No.:

GC Column ID: 2250/2401

I DATE<:SJ OF FROM: 11/13/391 ANALYSIS TQ:ll./l4/891 TIMECS) OF FROM: 19341 ANALYSIS TO: 022511

COMPOU1ID 1 RT1

alpha-BHC 1 **.^8beta-8HC t 6.^3delta-BHC 1 7.98qamma-BHC 1 5.37Heptachlor I 7.25A 1 d r i n 1 8.67Hep t . epox i de 1 12 . 3SEndosulfan I 1 14.58Die Idr in 1 Ifc. 704. 4 '-ODE 1 16.25Endrin 18.77Endosu 1 fan III 20.874. 4 '-ODD 20.72Endo . su 1 f ate_l 26 . 13-.4'-DDT 22.70llethoxvchlor 1 30.37Endrin k e t o n e l 30.3?a . Ch lordane_l 14. 30q. Ch lordane_l 1? . 38Toxaphene I 21.08Aroclor-1016 1 7.27Aroc lor-1221 1 4. 10Aroclor-1232 1 7.27Aroc lor- 1242 t 7.28Aroc lor- 1248 1 12.68Aroclor-1254 1 17.15Aroclor-1260 1 27, *8

t

FUllh

FROM

3 . 996.267.245.426.778. 13

11.7313.3815.9915. 1917.6420. 0719.5924.8321 .9229 . 2528 .6413.3112.3920.877. 194. 067. 197.2112.5616.9827.31

?T 1^JDQW 1 CALIBRAT I OH

TO 1 FACTOR

4.98! 41305017.611 15526408.731 22016006.311 36608207.731 33382609.201 259072013.031 222080015.29 1 197120117.411 174337017.31 1 156096019.901 62144021.66 1 15782*4021.85 1 118528027.441 102400023.481 108672031.481 47437032. 03 1 106177015.291 185472014.371 192128121.291 269447.341 3848984.141 1162247.341 1118727.361 16205012.811 11909217.321 8934427.861 165953

1

DATE OF ANALYSIS 11/14/89TIME OF ANALYSIS 2158ERA SAMPLE NO.f STANDARD) I NOB

RT

4.727. 258.33

lb.7519.30

21.2526.75

31. 1314.7713.85

CALIBRATIONFACTOR

425346116183002268160

1664010666240

12576101076420

109500019619802004081

QNTY/N

Y'('Y

YY

YY

YYY

SD

1.74.23.0

6 . 6• ~? o

6. 15. 1

____3. 15.84.3

Under- QHT Y- 'N: enter Y if q u a n t i t a t i o n was performed, N if not performed.*SQ must be less than or equal to 15.OS for q u a n t i t a t i o n , and less thanor equal to 20.OH for confirmation.

Note: D e t e r m i n i n g that no compounds were found above the CRQL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.OS c r i t e r i a

For m u l t i c o r n p o n e n t analytes, the single largest peak that is characteristicof the component should be used to establish retention time and SD.I d e n t i f i c a t i o n of such analytes is based primarily on pattern recognition.

page 3 of FORM IX PEST 979 1/87 Re.

Pes ticide/PCB Standards Surnma r y

LabName:ETCCorp. Contract:

Lab Code: Case Mo.: SAS No.: SDG No.:

Instrument ID: JB GC Column ! D: 3VBP-2 1 3 0

1 COMPOUND11

'alpha-BHC

ids 1 ta-BHC1 a aroma -BHC1 Hep t ach lor' 'M d r i n1 Hep t . epox i de! tndosu 1 fan Il Die Idr in14,4' -DDE1 End r i nl Endosu 1 f an II.4,4' -DDDI tndo . su 1 f a t e14 ,4'-DDTi He t ho *ych 1 or! End r i n ke t one! a . Ch 1 or dane3 . Ch 1 o r dane_

l TO,- apheneA Aroc lor-1016! Aroc lor-12211 Aroc lor-12321 Aroc lor-12421 Aroc lor-1248:Aroclor-12541 Aroc lor-1260

DATE(S) OF FROM: (Olô/PlANALYSIS TO: to/30 /FfTIME(S) OF FROM: (SSSANALYSIS . TO: J<?î

RT

3.003.25

3.636.337.379.6011 .5713. 1213.3314. 1514.4515.6817. 10

23 . 2519.78

Fw i r

FROM

2.973.213.713.606.307.799 .5011.5313.0813.2514. 1114.4115.6517. 0613.5323 .211 ° . 75

?T4DOU

TO

3 . 031, «"» Q

3.793.676.377.959. 7011.6013. 1513.5214. 1914.4915.7217. 1418.6023 .2919.32

CALIBRATIONFACTOR

3360020151746020Q7U603074580293390026726602228500941450193089022169701677450121921088001012768101235350S33028784650

DATE OF ANALYSIS 10/3 1/89 ITIME OF ANALYSIS 0310 1EPA SAMPLE NO. INDA 1(STANDARD? •

\RT

3.636 * '"*7.879 . 6011.5513. 10

14.43

18.': 5

CAL1BRAT10N1UMTI "iD :FACTOR 1 V-'NI ' 1

1 1 !

! 1 I1 1 !! 1 !

3249940 ! *J 1 5 . 7 I7046420 ! 1 3.7 ;2603660 1 1 2.4 12291220 l__l 2.8 i963970 1 1 2 . 9 11^87210 l_j' 1 2.9 !

I 1 • 11 ! !

1247370 1 fJ \ 2.3 l1 : l1 t 1

1219350 1 V \ 1.3 i830468 i ±J \ .3 !

1 ! i1 ! 1i i :1 ! 1i i ;1 1 1I t !1 I !1 1 11 t 11 ! I

Under QNT Y-'N: enter Y if q u a n t i t a t i o n was performed, N if not performed.*;D must be less than or equal to 15.0% for q u a n t i t a t i c n , and less thanor equal to 20.0*« for confirmation.

Not*: Determining that no compounds were found aboê '.he C*QL is a form ofq.jan t i t a t ion f and therefore at least one column mu i t meet the 15 . O'i c r i t e r i a

For mu 1 t i componen t analytes, the single largest peak that i=. c h a r a c t e r i s t i co *•" the componen t shou Id be used to establish retention t i me and !«D." J e n t i f i c a t i o n of such analytes is based prima r i l y on p a t t e r n r e c o g n i t i o n .

p * g e 1 o f FORM IX PEST 9:0 1/37

F'es t ic i de-'PCB Standards Summary

Lab Name:ETC Corp. Contract:

Lab Code: Case No.: SAS No.: SDG No

Inst rument ID: JB GC Column I D: ?'.SP-2100

1 COMPOUND!1

'alpha-BHC•1 beta-BHCIde 1 ta-BHC1 qamma-BHCI Hep t ach lor1 A l d r ini Hep t . epox i de! Endosu 1 fan I1 Die Idr in14,4' -DDE1 En d r i n! Endosu If an II, 4,4'-DDD! Endo . su 1 f a t e_! 4,4' -DDT! He tho.. ych lor1 t_ndr i n ke t onela. Ch 1 o r daneg . Ch lordane_

I Toxaphene1 rtroc lor-10161 Aroc lor-1221i rtroclor-1232_1 Aroc lor-1242' Aroc lor-1248i Aroc lor-12541 Aroc lor-1260

DATECS) OF FROM: lOjse./*^ANALYSIS TO: iO\sclS^TIMECS) OF FROM: \}5~fANALYSIS TO: Ht/3

RT

3. 003.253 . 753.636.337.879. 6011.5713. 1213.3814. 1514.4515 .6817. 1018. 5?23.2519 . 78

FLJU

FROM

2.973.213.713.606. 307. 799.50

11.5313. 0813.2514. 1114.4115 .6517. 0618.5323.2119.75

?TJDOW

TO

3. 033.293.793.676.377. 95«.7Q11.6013. 1513.5214. 1914.4915 . 7217.1418.60

19 . 82

CALIBRATIONFACTOR

3360020151746020070603074580293890026726602228500941450193089022169701677450121921083001012768101235850833028784650

11

DATE OF ANALYSIS 10-x31-'a9TIME OF ANALYSIS 0355ERA SAMPLE NO. INDB(STANDARD)

RT

3. 003 . 2 T3.73

13.3814. 13

15.6717. US

19.77

CALIBPATION1QNTI fiC-FACTOR 1 Y, 'Ml

! t

3471381 ! AJ ! 3.3Ir-55l40 1 ] 1 2.52IJ96661 ! ^ 1 4.5

1 11 11 ;

1 1I 11 1

2225291 1 XJ 1 .41715850 1 fJ \ 2.3

! 189153U 1 *J 1 1.31315850 1 Lt \ 3.1

1 1! 1

804480 1 X> 1 2.51 11 1! 11 11 !1 11 11 1! i1 1

Under CINT Y-'N: enter Y if q u a n t t t a t i o n uas pe r formed, N if not pe r f orr-ied.VJ must be less than or equal to 15.OS for q u a n t i t a t i o n , and leas thanor equal to 20.OH for confirmation.

Note: Determi-.ing that no compounds were found above the CRUL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.J% c r i t e r i

For rnulticomponent analytes, the single largest peak that is c h a r a c t e r i s t i cof the component should be used to establish r e t e n t i o n *ime and "iD.'dentificaMon of such analytes is based p r i m a r i l y on pattern recognition.

page of FORM IX PEST 931 1/87 Pev.

PESTICIDE---PCB STANDARD; NUMMARY

Lab Name: ETCNJ

Lab Code:

Inst rument ID: KB

Case No.:

Cont rac t:

SnS No.: SDG No.:

GC Column ID: 3SSP-2100

11 COMPOUND11 .............1 a Ipha-BHCIbeta-EHCI d e l ta-BHC1 oamma-BHC1 Hep t ach.1 or1 Aldnn1 Hep t . epox i de1 Endosu 1 f an I_1 Die Idrin14. i '-DDE1 Endr i n1 Endosu I f an II1 4.4'-DDO1 Endo . su 1 f a t e1 4.4'-DDT1 Me t ho x yen lor_1 Endr in ke t onela. Ch 1 o rdane1 g . Ch 1 ordane_1 Toxaphene1 Aroc lor-10161 Aroc lor-12211 Aroclor-1232_1 Aroc lor-1242_1 Aroc lor-12481 A roc IOP- 1254_I APOC lor-1260_1

DATECS) OF FROM: 11/27/89ANALYSIS TO: ll-'27/39TIMECS) OF FROM: 2 136ANALYSIS TO: 22 15

RT

2.552 . 753.173. OS5.376.776.3310. 1511.5811. S312.5712.9014. 0715.7716 .8321. 1717.9010.379.45

unFROM

2.512.723. 133.035.296 . 668.25

10.0511.4811.8112. 4b12.6713.9615.2616.7321. 0517.7910.309.38

?TIDOW

TO

2.592.783.203. 135.446.878.42

10.2511.6911.9512.6712.9314. 1715.4716.9421.2318.0110.449.52

CALIBRATIONFACTOR

1335040122720085702012966401387520976220888320675340669440 .7353605548805427204320004864004ob5604307224518409459201008640

DATE OF ANALYSIS 11/28/89TIME OF ANALYSIS 0903EPA SAMPLE NO.( STANDARD ) INDA

PT

3 . 075 . 336.728.28

10.1011.53

12.73

16.7821.10

CALIBRATIONFACTOR

1^400001354240997380878080669440666880

542080

465280420366

ONTY/N

NNNNNN

N

nN

%D

11. 12.42.21.2.9. 4

. 1

_ 32 , 3

Under QNT Y.-'N:SD must be lessor equal to 20.

e n t e r Y i f q u a n t i t a t i o nthan or e q u a l to 15.OS

OH for c o n f i r m a t i o n .

was performed, N if not performed.for q u a n t i t a t i o n , and less than

Note: Determining that no compounds were found above the CRQL is a form ofquant i t a t i o n , and therefore at least one column must meet the 15.OS c r i t e r i a

For mu1ticomponent analytes, the single largest peak that is c h a r a c t e r i s t i cof the component should be used to establish r e t e n t i o n t i m e and SC.I d e n t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognition.

page 1 of FORM IX PEST o I/; Rev

PEST 1C IDE/PCS STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code;

Instrument ID: KB

Case No . :

Con tract:

SAS No.: SDG No.:

GC Column ID: 3SSP-2100

COMPOUND

alpha-BHCbeta-BHCdel ta-BHCaamma-BHCHep t ac HI o rH 1 dr inHep t . epox i deEndosu 1 f an I_D i e I d r i n4 ,4 '-DDEEndr i nEndosu 1 f an II4.4'-DODEn do . su 1 f a t e^.4'-DDTMe t ho> ych lor_End r i n ke t onea . Ch 1 o rdaneq . Ch 1 or daneToxapheneAroc lor-1016Aroclor-1221_Aroc lor-1232Aroc lor-1242nroclor-1248Aroclor-1254Hroc 1 or- 12oO

DATECS) OF FROM: 11/27/89ANALYSIS TO: 11/27/89TIME'.S) OF FROM: 2136ANALYSIS TO =2215

RT

2.5?2. 753. 173 . 035.376 . 778 . 37

10. 1511.5811.8512.5712.8014. 0715.3716.8321.1717.9010.779.45

wirFROM

2.512.723. 133. 035.296 .66S.25

10.051 1 . 4811.8112.4612.6713.9615.26U.7321.0517.7910.309.38

*TsIDOUl

TO

2 . 5°2.783.203. 135 . 446.378. 42

10.2511.6911.9512.6712.9314. 1715.4716.9421.28le.oi10.449.52

CALIBRATIONFACTOR13350401227200857020129664013875209762208883206753406694407353605548805427204320004864004oo5604307224518409459201008640

DATE OF ANALYSIS 11/28/89TIME OF ANALYSIS 1259ERA SAMPLE NO.I STANDARD) INDA

RT

3.055.326.708.2810. 0811.52

12 . 72

16 . 7"?21.10

CALIBRATIONFACTOR

1441230141184010132209152006796806S4160

556160

481920438653

ONTY/N

NNNNNN

N

NN

\D

11.21.83.83. 0.6

2.2

2.5

3.31.8

Unde r ONT Y/N: enter Y if q u a n t i t a t i o n was performed, N if not per formed.SD must be less than or equal to 15.OS for qua n t i t a t i o n , and less thanor equal to 20 . Q?i for confirmation.

Note: Determining that no compounds we re found above the CPQL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.0'• c r i t e r i a

For multicomponent ana 1yt es, the single largest peak * ha t is c h a r a c t e r i s t i cof the component should be used to establish retention time and %D.I d e n t i f i c a t i o n of such analytes

page 2 of

is based p r i m a r i l y on pattern recognition.93$FORM IX PEST 1/87 Re'.-

PESTICIDE/PCB STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code:

Inst rumen t ID: KB

Case No.:

Con t rac t:

SAS No.: SDG No.:

GC Column ID: 3S5P-2100

!1 COMPOUND1

1 alpha-BHC ___Ibsta-BHC _____1 dm 1 ta-BHC1 qamma-BHCIHeptacKlor1 A 1 d r i n1 Hep t . epox ide1 Endosu I f an I1 Die Idr.in14 .4 '-DDE1 End r i n1 Endosu 1 1' an II14, 4 '-ODD ____1 Endb . su 1 f a t e_1 4.4'-DDT1 Me t hoxych 1 o r1 End r i n ke t onela. Ch 1 o rdane_1 g . Ch 1 o r dane_1 Toxaphene1 Aroclor-10161 Aroc lor-12211 Aroc lor-1232_1 Aroc 1 or- 12421 Aroc lor-1248iAroc 1 o r - 1 2 5 4_1 Aroc lor-12601

DATE(S) OF FROM: 11/27/89ANALYSIS TO: 11/27/89TIME '.S3 OF FROM: 2 136ANALYSIS TO 122 15

RT

2 . 552.75J. 173.085.376.77S.3310. 1511.5811.8312.5712.8014. 0715,3716.8721.1717.9010.379.45

umFROM

2.512.723. 133. 035 . 296 .668.2510. 0511.4811.8112.4612.6713-9615.2616.7321.0517.7910.309.38

ii

?T^IDQU

TO

2.592.783.203. 135.446.378.42

10.2511.6911.9512.6712.9314. 1715 . 4716.9421.2918.0110.449 . 52

CALIBRATIONFACTOR

13750401227200857020129664013875209762208883206758406o94407353605548805427204320004864004665604307224518409459201008640

DATE OF ANALYSIS 11/28/89TIME OF ANALYSIS 1338ERA SAMPLE NO.(STANDARD) 1NDB

RT

......2.532.753. 17

11.3512.52

14. 0215.32

17.8510.339.42

CALIBRATIONFACTOR

15052801336380946440

761600604300

435200508800

46o5609574401027840

ONTY/N

NNN

NN

NN

SD

12.83.910 . 4

—————

—————

7.*9.0

4 . r-j

N ? . ?N i i . :N ! 1 .

i11

1

11

Under ONT Y'N: enter Y if q u a n t i t a t i o n was performed, N if not performed.*tD must be less than or equal to 15. OS for quantitation, and less thanor equal to 20. OS for confirmation.

Not*: Determining that no compounds were found above the CRQL is a form otq u a n t i t a t i o n , and therefore at least one column must meet the 15.0'n c r i t e r i a

For multicomponent analytes, the single largest peak that is c h a r a c t e r i s t i cof the component should be used to establish retention t i me and SO.I d e n t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognition.

page 3 of 3 FORM IX PEST 934

PESTICI-DE/PCB STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code: Case No. :

Instrument ID: QB

Cont rac t :

SAS No . :

GC Column

SDG No . :

ID: 2250/2401

11 COMPOUND1|...... .......lalpha-BHCIbeta-BHC(del ta-BHC1 gamma-BHC ____1 Heptach lar1 Aldrin1 Hept . epox idelEndosulfan" I_1 Die Idr in ____14. 4 '-DDE1 Endr in1 Endosu I fan I I14. 4 '-ODD1 Endo . su 1 f ate14. 4 '-DOT1 Me thoxych lor_t Endr in ketonela. Chlordane_Ig. Chlordane1 Toxaphene1 Aroclor-1016IAroclor-1221_IAroclor-12321 Aroclor-1242IAroclor-1248_IAroclor-1254_1 Aroclor-1260t

DATE(S) OF FROM: 10/24/89ANALYSIS TO: 10/25/89TIMECS) OF FROM: 1459ANALYSIS TO: 0223

1 RT 1RT 1 LJ I NDQUJ 1 CAL I BRAT I ON

1 FROM 1 TO t FACTOR....... j...... |...... |...........

5.171 4.351 5.981 49158217.951 6.891 9.011 13730409.131 7.971 10.301 25152016.771 5.951 7.581 39859418.321 7.401 9.241 32793819.901 8.911 10.891 2991360

13.801 12.631 14.971 243969016.131 14.861 17.411 207488118.331 16.951 19.711 188289017.931 16.341 19.521 176961020.481 18.751 22.221 104497022.671 21.181 24.151 119680022.501 20,771 24.231 128000027.921 25.581 30.251 93056024.571 21.581 27.551 99904033.251 30.601 35.901 37133032.931 29.681 36.191 53440015.871 14.351 17.391 178688014.921 13.431 16.401 213888122.831 22.601 23.061 523858.381 B.30I 8.471 4723224.081 4.041 4.121 2800648.381 8.301 8.471 1502748.381 8.301 8.471 22195214.571 14.421 14.711 21094620.351 20.151 20.551 12147224.381 24.141 24.631 144768

1 1 1

DATE OF ANALYSIS 10/25/89TIME OF ANALYSIS 1358EPA SAMPLE NO.(STANDARD) INDA

RT

7.158.75

10.3714.3516.7318.98

23.37

25.2834.50

CALIBRATIONFACTOR

505560140347413655701288512124486402214500

1413170

1094800399508

QNTY/N

YYYYYY

Y

YY

SD

————

26. 8»23. Q«22. 2»18. 3«18.0-17. 6«

18. 1»

9.67.6

Under QNT Y/N:SD must be lessor equal to 20.

enter Y if quantitationthan or equal to 15.OS

OS for confirmation.

was performed, N if not performed,for quantitation, and less than

Note: Determining that no compounds were found above the CRQL is a form ofquantitation, and therefore at least one column must Tteet the 15.OS criteria

For mu1ticomponent analytes, the single largest peak that is characteristicof the component should be used to establish retention time and SD.Identification of such analytes is based primarily on pattern recognition.

page 1 of FORM IX PEST 00 1/87 Rev

PEST 1C IDE/PCS STANDARDS SUMMARY

Lab Name: ETCNJ

Lab Code: Case No. :

Instrument ID: QB

Cont ract :

SAS No . :

GC Column

SDG No . :

ID: 2250/2401

11 COMPOUND1)....»..-..»..talpha-BHC ___Ibeta-BHC ____Idelta-BHC ___1 gamma-BHCt Hep t ach lorl A l d r int Hep t . epox i det Endosu 1 f an" I1 Die Idr in14, 4 '-DDE _____1 Endr in ,1 Endosu 1 fan I II4,4'-DDD ____1 Endo . su 1 fate14, 4 '-DOT ____1 Methoxych lor1 Endr in ket onela. Chlordane_Ig. Chlordane—1 Toxaphenet Aroclor-1016IAroclor-1221IAroclor-1232_IAroclor-1242IAroclor-1248IAroclor-1254IAroclor-12601

DATECS) OF FROM: 10/24/89ANALYSIS TO: 10/25/89TIMECS) OF FROM: 1459ANALYSIS TO: 0223

RT

5.177.959. 136.778.329.9013.8016.1318.3317.9320.4822.6722.5027.9224.5733.2532.9315.8714.9222.838.384.088.388.3814.5720.3524.38

RTUIINDOLJ

FROM 1 TO...... | ------

4.351 5.986.891 9.017.971 10.305.951 7.587.401 9.248.911 10.8912.63 1 14.9714.861 17.4116.951 19.7116.341 19.5218.751 22.2221.181 24.1520.771 24.2325.581 30.2521.581 27.5530.601 35.9029.681 36.1914.351 17.3913.431 16.4022.601 23.068.301 8.474.041 4.128.301 8.478.301 8.4714.421 14.7120.151 20.5524.141 24.63

I

CALIBRATIONFACTOR

49158211373040251520139859413279381299136024396802074881188289017696101044970119680012800009305609990403713305344001786880213888152385472322280064150274221952210946121472144768

DATE OF ANALYSIS 10/25/89TIME OF ANALYSIS 1531EPA SAMPLE NO.(STANDARD) INDB

RT

5.558.459.68

18.6821.30

23.3229.0223.32

34.4716.5815.62

CALIBRATIONFACTOR

630124116930603097100

21072101229190

153814010867201548160

61896021919612615640

QNTY/N

YYY

YY

YYY

YYY

SD'

28.2*23.3*23. 1»

19. 1»17. 6»

20.2*16.8*55.0*

15. 8*22.7*22.3*

Under QNT Y/N:SD must tae lessor equa 1 to 20.

enter Y if quantitationthan or equal to 15.OS

OS for confirmation.

was performed, N if not performed,for quantitat ion, and less than

Note: Determining that no compounds were found above the CRQL is a form ofquantitat ion, and therefore at least one column must meet the 15,OS criteria

For multicomponent analytes, the single largest peak that is characteristicof the component should be used to establish retention time and HD.Identification of such analytes is based primarily on pattern recognition.

page 2 of FORM IX PEST 936 1/87 Rev,

CHROMBTOSRfiM";ie > H A £ I B 1.9 arou. EVR^fl

f • 1 • t • 1 • 14 8 is a* 1 • 1 • 1 • 124 ae 1 • 132

D-s ta Fi le:Name :M i s c : EUALW

: : U4 Quant Output Fi le: '"HfcIns t rument ID: HA

Id F i l e : I DMA: :UST i t l e : IFB/PST/PCB 1. "7%SP2250/1Last C a l i b r a t i o n : 891003 00:29

Operator ID'. YY6148Quant Time: 891026 16:06I n j e c t e d at: 891026 14:37

2UL IN.!;

937

QUANT REPORT

Operator ID: YY6148Output File: *HA21Q

Quant Rev; 7

Data F i l e :Name :Misc: EUALA

>HA210ACU4

10 F i l e : IDHA::UST i t l e : IFB''PST/"PCB 1.5SSP225Q/1Last C a l i b r a t i o n : 891003 00:29

Compound

Ouant TimeInjected at

Di lut ion FactorInst rument ID

UL IN*

R.T. Scan* Height

Page 1

8°1Q26 16:.0r.891026 14:37

1.0000 CHA

Cone Units

6 '11)13)16)13 )

20)

* fi 1 d P in#«i, 4 '-DDE*Endr in*4,4'-DOT*C i b u t y 1 c h 1 o r e n d a t e#Endr in ke tone

81618222930

.67

.42

.75

.63

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518933

1123135617501318

1523257648647*36

119051152

. 00659. 000404.00516. 00941. 0174

. 00303

UG/'MLUG--MLUG/MLUG-'MLUG/'MLUG ML

100io=:100lOf10010 i

Compound use* ESTD

938

CHRQMQTOGRQM

20131?

28 32

Data FUe:Name :M i a c : EUHLB

: : U4 Quant Output Fi le:Inst rument ID: HA

Id File: IDHA::UST i t l e : IFB--PST.--PCB 1. 5SSP2250^1 - 95SSP240 1 2UL I NOLast Calibration: 891003 00:29

Operator ID: YY6148Quant Time: 891026 16:07In jected at: 891026 15:19

989

QUANT REPORT

Operator ID: YY6148Output Fi le: AH*211: :

Quan t Rev: 7

D a t a Ft le: >Hfl211: : U4

Misc: EUALB

10 File: IDHA: : USTitle: IFB''PST/PCB 1 . 5SSP2250/1 . 95SSP24Q1Last C a l i b r a t i o n : 891003 00:29

Quan t T imeInjected at

D i 1 ution Fac tor:Inst rumen t ID

2UL IN,'

Page 1

891026 16:0"8Q1Q26 15:19

1.3000.HA

Compound R.T. Scan* H e i g h t Cone Un i ts

6 '11)13>14)16)17)1-3)

20)

ttAidr*.4 , 4 '*E'-dr*4 , 4 '#^-4(#Endr

in-DDEi n-ODD-DDTin a 1 dehyde

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8161820222?2930

.67

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. 77

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513977

112412491360142317491810

79216396

249601792

293124223M62273

9 0 5 M

.0343.OOOc.29

.0265.00175.0347

. 006^4.0913

. 00278

UG/MLUGxUG,-'UG-'UG/L'ij''

UG/UG/

nuMLMLMLMLMLML

1001EK10 010.1001010010

Compound uses ES~D

990

CHROMOT06PQMl .B EVflLC

49* 1200

Data F i l e : >H*212::U4Name:Misc: EUALC

Id F i l e : IDH^:: UST i t l e : IFE/PST -PCB 1. t5%SP221?Q.-'lLast C a l i b r a t i o n : 891003 00=29


Quant Output F i le: ^HA212::ACInst r-ument ID: HA

1 2UL INJ

991

Operator ID: YY6148Output File: *HA212: : AQData File: >HA212::U4Name :Misc: EUALC

QUANT REPORT

Quant. Rev: 77 Quan t TimeInjected at

D i1u t ion Fac torIns t rument ID

Page 1-

891026 16:4:"891026 16:02

1. 0 0 0 0 :HA

ID F i l e : IDHA::USTitle: IFB---PST/PCB 1.5SSP2250/1.95SSP2401 2UL IN-"Last C a l i b r a t i o n : 891003 00:29

Compound R.T. Scantf H e i g h t Cone Units

6 311)17)14)ID)17)1*>20)

#A 1 d P#4,4'#EndPit4 , 4 '#•4,4'#EndP#Cubu*Endp

in-ODEi n-DOD-ODTin a 1 dehydet y 1 c hin ke

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UG-UG/UG-UG-

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UG/'MLUG/'UG/UG/'

ML'ML'ML

10010-10010;.10010 ;10010

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992

266

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O p e r a t o r ID: YY6148Cut pu t File:Data F i l e :Name :Misc: DD I

QUANT REPORT

Quant Rev; 7

:U4

ID F i l e : I044IP::UST i t l e : IFB-'PSTxPCB 1.5&SP225Q/1.Last C a l i b r a t i o n : 891003 00:29

Compound

9 ) »a-i-pliB-Ch lur dane1J ) #4, 4'-DDE14) 4t4,4'-DDD15) fr£ desul Pan II16) *4,4'-DDT13) tg"d?iv 1 ci" «•• i i.t-19) t t D i b u t y l c h l o r e n d a t e

32) itAB3 - a ) *MB 1.5 a j-740 J *ni'iSL- lor—1294

42 ) ')-Mp 1 ? ^r tl 3


uuan t TimeInjected at

D i l u t i o n FactorIns t rumen t ID

2UL IN;

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Page 1

891026 ,9:?'891026 18:50

1. J 0 0 G 'HA

Cone Units

7.1214. 1716.2320 . 7Q20.7022.6825.732*. 1722.685. 0214.1716.2319.6220.7Q

425343972

124012401359154217481359

8*3

1175

3648576

292482105621056176641344

7705617664

576292487809

21

00137

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. '-1 i j. .*00852.367. 0792

UG/'PILUbXMLUGxMLUG-T1LUG''MLUGXML

UG/MLUGxMLUG .-'MLUG/ML

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Id File: I044IP::UST> t Is: IFB''PST -PCS l.'"VLast C a l i b r a t i o n : 891003 00:29

O p e r a t o r ID: YY6l<i8Quant T ime: 891026 20:17I n j e c t e d a t : 9 ° L 0 2 c 19:72

Quant Output F i l e : 'xHrtInst rumen* ID: HA

AO 1 2UL INJ

995

QUANT REPORT Page

Operator ID: YY6148 Quant Rev:Output File: *HA216::AQData File: >hA216::U4Name :Misc: DO II

ID File: I 04-4 IP: : USTitle: IFB/PST/PCB 1.5SSP2250/1.95KSP2401Last Calibration: 891003 00:29

7 Ouant T i m e iInjected at

D i 1 u t ion ^"ac tor:Ins t rument ID

JL INC

891026 19:321 . J 0 0 0 '

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UG/MLUG/MLUG/MLUG.'MLUG/MLUG/MLUG/MLUG ''MLUG/MLUG/MLUG/MLUG/MLUG/MLUG /MLUG/MLUG 'MLUG-'MLU — 'M*

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Operator ID: YY*148Quant Time: 891026 20:5r'I" ject ed at : 8*1026 20: 15

Quant Output F i le : ^HAInst rument ID: HA

. 95SSP24Q1 2UL ING

997

QUANT REPORT Page 1

OpeOutDat

rPa

* to r ID: YY6148ur F i le : ^HA217: ;AQFi le : >HA217::U4

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#•* ,4' -ODEj t * ,4 ' -DODttE-nJu.-.j 1 f dii I I*4,4 ' -DDT#£• i bu I: y I ch 1 or en da t e

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C !*ta F i l e : >H«231: : U4Name !M i s c : E'JALB

Quant Output File:Inst rument ID: HA

Id File: I 0441P: :UST'.tle: IFB/PST-'PCB 1. r'*SP225 0/1. 95HSP240 1 2UL INJLast C a l i b r a t i o n : 891007 00:29

Operator ID: YYc. 146Ouant Time: 891027 06:51Injected at: 89J.Q27 06=10

999

Ope ra t or ID:Chj tpu f F i l e :Data F i l e :Name :Misc: EUrtLB

YY6148

QUnNT REPORT

: AC:U4

7 Quan t T i me:Injected at:

D i l u t i o n Fac t o r:I nst rument ID:

Page

8-?l 027891027

iHM

•16:?06: 10•i 0 0 0 i

ir* F l i p : IOA4IP: :UST i t l e : IFB---PST/PCB 1.5SSP2250/1.95HSP2^01Last Calibration: 891007 00:29

2UL IN

* C

Cumpound R.T. Scan* Height Cone Un i ts

6 '11)13114)io>19)

#rt I d r*4,4'tEndr114,4 '#4,4'Jt=D i b u

i-i--t

nDDEnODDDOTylch lorendate

81618202229

.65

. 15

.75

.85

.63

. 15

517967

11231249139917-7

83840r-12

313612048376336 : 61

.0363.Q00"9

.0333. 002 GO. 04«6. 0^29

UG''US/UG/UG/UG/i_L i J , '

MLML.MLML'MLML

10010"1001010010-

ound uses ESiD

CHRCflflTOGEQM' i 1 e J>.iS.*t3 1 .S amu.. EVfiLS

i i3£

Oaf a File: >H*243: :U4Name :

Quant Output F i l e : ^H^Inst rumen t ID: HA

Id Fi lc: I04-.IP: : U9T - . t l e : IF&'PST/PCB 1. 5NSP2250/1. 95%SP240 1 2UL INJLast C a l i b r a t i o n : 891003 00:29

Operator ID: KT8582Ouant Time: 3Q1Q2"? 21:2oInjected at: 891027 20:40

: : AQ

1001

QUwNT REPORT

Operator ID: KT8582Output File: AHM243

Ouant

Data File:Name :disc: EUALB

>HA243::U4

ID File: IO-4IP::USTitle: IFB.-'PST/PCB 1, 5HSP2250/1. 9£?jSP2401Last C a l i b r a t i o n : 891003 00:29

7 Quan t T i meInjected at

Di 1 ut ion Fac ».or:Inst rument ID

JL IN;

Pag* 1

8-1027 ••1:2-891027 20:40

1.0000

Compound R.T. Scan* Height Cone Dm ts

6>11)13)14)1-,)17)1* )20)

#r-#4ftE*4***

•=dr,4'r.dr,4',4'

tEndr#0#Ei

bundr

in-DDE1 n-ODD-DDTin a 1 detv.'det. v 1 e h ! o r e n d a t ei n k e t o n e

81618202227293C

.65

. 17

.75

.82

.68

.70

.17

.22

517968

112312471359142017A8IS 11

84928^04

279042 0 48295043 2 r 2 M6^8411 2 2 8 M

.0367.000494

.0296. 00200.0350

.00*34. 0994

.Ob 72 3

UG-'UG.'UG-'Iji- 'UG..SJC--UG.''UG-'

•MLML'MLMLMLML ,'MLML

10010.100101001010010

Co if i pound uses ESTO

CHROMBTOGRflMIT Me >Mfl49B" 1.8 a»u.

400

216008-

212000-

208000-

204000-

£00000-

196080-

192080-

186800-

184000-

180080-

176808-

172009-• <

168080-

12.00

EVflLfl

1600

is 20 24

Data Fi le: >HA490: :U4Name :Misc: EOALA

Ouant Output File: ~HA490::AQIns t rument ID: HA

Id File: I076IP::UST i t l e : IFB/PST/PCB 1.5HSP2250/1.95SSP2401 2UL INJLast Calibration: 391031 13:04

Operator ID: YY6148Quant Time: 891113 18:01Injected at: 89111? 17:17

Operator ID: YY6143Output File:Data File:Name :Misc: EUALA

QUANT REPORT

Quant Rev: 7

>HA490AQU4

ID File: I076IP::USTitle: IFB/PST/PCB 1. 554SP225Q/1. 95SSP240 1Last Calibration: 891031 13:04

7 Quan t T ime :In jec ted at :

D i l u t i o n Fac tor:Instrument ID:

2UL INJ

Page I

391113 ISiOl891113 17:17

1. 00000HA

Compound R.T. Scan# Height Cone U n i t s

6)13)16)19)

#A 1 d r#Endr*4,4'#Dibu

ini n-DOTt y Ich lorenda te

8182229

.67

.77

.72

.20

518112413611750

1849610240665615040

.00487. 0143.00427.0101

UG/MLUG/MLUG/MLUG/ML

100100100100

Compound uses ESTD

t\ ••*v U

CHROnf lTOGRQMFile >HfM91 1.8 EVRLB

400 800 1200 1600. r . . . . i . . . i . . . i . . . i . 2000

32

Data Fi le: >HA491::U4Name:Misc: EUALB

Quant O u t p u t F i l e : ~HA491: :AQI n s t r u m e n t ID: HA

Id File: I076IP::UST i t l e : IFB/PST/PCB 1.5HSP2250/1.95SSP2401 2UL INOLast Calibration: 891031 13:04


003

\

Operator ID: YY6148Output F i l e : AHA491::AQData File: >HA491:: U4Name :Misc: EUALB

ID F i l e : I076IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/Last C a l i b r a t i o n : 891031 13:04

Compound

QUANT REPORT

Quant Rev: 77 Quan t T ime:Injected at:

D i 1 u t ion Fac tor:

Page 1

39111? 18:47391113 16.:Q3

1. 00000Inst rument ID: HA

1.95*iSP24fll 2UL INJ

R.T. Scan* Height Cone Uni ts

6)13)14)16)17)19)20)

#Aldr in#Endr in#4 ,4 ' -ODD#4, 4 '-DOT#Endr in a 1 dehyde#D i bu t y 1 oh lorendate#Endr in ke t one

8.18.20.22.23.29.30.

67757872831830

518112312451361142817491816

96896526722560334725248754564225

.0255

.0736. 00144.0215.00432.0509

. 00545

UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100100100100100100


Uu6

CHROflflTOGRflMFile >KfM92 1.8 amu.

, 4 0 0

380000-

2000

Data File: >HA492:: U4Name:Misc: EUALC

Quant Output File: >SHA492::AQInstrument ID: HA

Id File: I076IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/1.95*SP2401 2UL INJLast Calibration: 891031 13:04


1UG7

Operat or ID:O u t p u t File:Data File:Name :Misc: EUALC

YY6143AHA492>HA492

QUANT REPORT

Quant Rev: 7AQU4


Di 1 u t ion Fac torInstrument ID

Page 1

391113 19:32691113 13:48

1.00000HA

ID File: IQ76IP::UST i t l e : IF8/PST/PCB 1. 5*SP225Q/1Last Calibration: 891031 13:04

Compound

95%SP24Q1 2UL INJ

R.T. Scan* H e i g h t Cone Units

6)13)14)16)17)19)20)

ttAldttEnd#4,4#4,4*End

rriir

#DibuttEnd r

i nin-DDD-DOTin a Idehydetylch lorendatei n ke t one

8182022232930

.67

.77

.80

.72

.87

.20

.30

518112412461361143017501816

187137973444160

651529408

1388168321

.0493. 136

.00233.0418

. 00774.0937.0107


100100100100100100100

Compound uses E3TD

CHRQMRTOBRflMFi le >Hfl595 1.0 amu.

400 eee

260000:

2S8000;

21000^

1S0000J

17000^ ^V——'

8 12

2089

Data Fi le:Name :Misc: EUALB

>HA5Q8: : U4 Quant Output File: AHA508::AQInstrument ID: HA

Id Fi le: I076IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP24Q1 2UL INJLast Calibration: 891114 08:52

Operator ID: YY6148Quant Time: 891114 13:14I n j e c t e d at: 891114 12:31

Ope ra t o r ID:O u t p u t F i l e :Data F i l e :Name :disc: EUALB

YY6148AHA508>HA508

QUANT REPORT

Quant Rev: 7: AQU4

7 Quant TimeI n j e c t e d a t

D i l u t i o n FactorIns t rument ID

Page 1

891114 13:14891114 12:71

1. 00000HA

ID File: IQ76IP::USTit le: IFB/PST/PCB 1.5%SP225Q/1Last C a l i b r a t i o n : 891114 08:52

Compound

95!iSP2401 2UL INJ

R.T. Scan* Hei g h t Cone Un i ts

6)13)14)16)17)19)20)

#A 1 d r#Endr#4,4'#4,4'#Endr#Dibu#Endr

ini n-ODD-DOTin aldehydet y l c h l o r e n d a t ein ke t one

8.18.20.22.23.29.30.

67777372802028

518112412421361142617501815

94976555531728

355855376

748173904

.0183

. 0447. 000729

. 0164.00338.0408

.00184

UG/MLUG/MLUG/MLUG.-'MLUG/MLUG/riLUG/ML

100100100100100100100

# Compound uses ESTD \tt2tP]

1010

CHRQnOTOSRQMFile >HP520 l.B amu.

408 800 1208 16.01? 200@1 .

32

Data F i l e : >HA520::U4Name :Misc: EUALB

Quant Output File:I n s t r u m e n t ID: HA

: :AQ

Id F i le : I O ? 6 1 P : : U ST i t l e : IFB/PST/PCB 1, 5*SP2250/1. 959SSP2401 2UL INJLast Cal ibrat ion: 891114 08:52

O p e r a t o r ID: YY6148Quant T ime : 391114 21:02I n j e c t e d at : 391114 20:18

1011

Operator ID:Ou t put F i l e :Data File:Name :Misc: EYALB

YY6148"HA520>HA52Q

QUANT REPORT

Quant Re^: 7AQU4

7 Quan t T imeInjected at

D i lut ion Fac torIns t rument ID

Page 1

891114 21:02S91114 20;18

1.00000HA

ID F i l e : I076IP::USTit le: IF6/PST/PC8 1. 5*SP22<?0/1Last Ca l i b r a t i o n : 891114 08:52

Compound

95%SP24Q1 2UL 1NJ

R.T. Scan* Height Cone U n i t s

6)13)14)16)17)19)20)

#A 1 d r#End#4 ,4#4,4#£nd

r1

ir

#DibuttEnd r

inin-DDD-DOTin a Idehydet y Ich lorenda tein ketone

8.19.21.23.24.29.30.

90081205186375

532114312651331144917761843

97738M568962176371344288764804032

.0189

.0458.000918

.0171.00270.0418

. 00190


100100100100100100

Compound uses ESTD

U i I

CHROMfiTOGRflHFile >JB140 l.e aau. EVRLfi

38000*-

360000-

340000-

320000-

380306-

2ft660fr

260000-

24000*.'- ""

400 806 1260 166>3 30 0t'. . . 1 ^^ , | r . . i . . . i . . . i . . . t . . . i . . . i . . . i . . T i . . . i . .

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"JBJ40

I d F i l e : I C 2 5 1 C : : U ST i t l e : IFB-'PST/PCB 3?iSP-2100Last C a l i b r a t i o n : 8^1031 08:1

Operator ID: YY6148Quant Time: 8^1031 08:13Injected at: 891030 16:52

Operator ID: YY6148Output F i l e : 'VJ8140: : ACData F i l e : >JB14Q::U4Name :Misc: EYALA

ID F i l e : I 025 1C::UST i t l e : IFB/PST.'PCB 3^SP-2100Last C a l i b r a t i o n : 691031 08:12

Compound

QUANT REPORT

Quan t K&v: 77 Quan t Time:Injected at:

D i l u t i o n Factor:1 ns t rumen t ID:

Page 1

891=J31 US:17891030 16:52

1 . 0 0 0 0 0

to.

R.T . Scan* Height Cone Un i ts

f

*-

6

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111314

1-fr

1617

192 '<•

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)

)-)))

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)i1-,

ftijuiiiin#A 1 d ri -F -

34 t 4 '#Endr3-i , 4 '4-* , 4

3£ndr

3D i b u3EndrA [ .p * I-,

r r r r -

10 DIICi n

a Ch io rd * n *_-DDEl n-ODD-DPT-DDTin a ldehyde* U 1 * a n S u l f a t et y l c h l o r e n d a t ein k e t o n e... , . . f. fo i a -J-err — 4-~> 6, Q , .- ->-

3.7.9.

10.13.14.

1 D .

18.15.17.23.19.23.

O i.

6365P 7

4215732053731 O

0578-r g

n^;

217458

6 5 0805849944

10921112944

103116831187141J3

o . oi? os> 9 in

1344. ._| -t

51229120 -

3520

105323520

57615552

1344

.000146. 01' 45

. 0 C 0 3 0 2

.000115. 00863. OU200

. CU426

. 0 0 1 5 7. U b U i. i.O

.00932. 0 0 0 8 5 6

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UGUGUGUGUGUG

UGUGUbUGUGUGMn

'ML.'ML•'ML

•'ML.TIL.'ML•'MLXML-'ML.'ML'ML

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10010 1'10010U10010U1UO1 0 01UO•t 1 . . .

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1 0 1 4

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420000

400300

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4 8 12 16 20 24 28

Data Fi lc: > JB1-41: : U4Name :Mist: E

Id Fi le: 10'JSIC: : UST i t l e : IFB.'PST.'PCB 3%SP-2100Last C a l i b r a t i o n : 891031 QB:

Operator ID: YY6148Ouant Time: S910J1 08:14Injected at: 8*1030 17:77

Quar, t Ou t pu t F i l e1 ns t rumen t ID

loir,

Qpe ra t or ID:Out put F i l e :Data F i l e :Name :Misc: EUALB

YY6148~JBl4l:> JB141:

QUANT REPORT

Quant Pev: 7

U4

7 Quan t Time:Injected at

D l 1 u t ion Fac tor:Instrument ID

Page 1

8*1031 OS:148*1030 17:37

1 . 0 U U 0 C

-rtID F i l e : I025IC::UST i t l e : IFB/PST/PCB 3*iSP-210t!Last C a l i b r a t i o n : 891031 08:12

Compound


R.T. Scan* Height Cone Units

6 i11)1?)16?17)19)20)

#ft 1 dr in#4,4' -DDE#End r i n#4,4' -DDT#Endr i n aldehyde#D i bu t y 1 ch lorendate#Endr 10 ke t one

7 ,13.14.IS.15.28.19.

87421555720373

472£05349

1 1 i 394316821184

127761"68

1662^3509448640

S 1 7'J S5504

. 0. 0 u 0

. 0

. Li. 00

* i_H

. oc

— -"!_'

1 73

4962LI63S5490TC •)

UGUGUGUGUGUGUG

-'ML.'ML•'ML""IL^ML• '"L.•'ML

'1ii111j.

00Uv

ocOv

uo00:JC

1 ' • •' /•I U I • 1

CHROMBTOCRQHFile >JB14i- 1.0 »mu. ETVOLC

640030-1

i

520000-

4800ee;44000^

-400000-

J.j

. , . j

Hi•••

460 800 1230 1600 2000

3

;

i 3 3L I

J3 3i _?

o«N

1

i"* Ji-• i

y t£3l-s e

o» ui- 10

1 1 | • 1 • ! ' 1 ' ! ' 1 ' 1 • 1 • I • 1 ' 1 '1 '1 ' 1 ' 1 • 1 ' 1 ' 1 '4 6 12 I* 20 24 28 32 3*

D.3ra F i l e : >Jfcl42: : U-iUame :Misc: EUHLC

Quant Ou^ut File: "JS142::A1.I ns t rumen t 10: jX

Id F i l e : I 02?1C: :UST i t l e : IFB.'PST/PCB 3?iSP-21QO

C a l i b r a t i o n : - 891031 08:12

Operator ID: YV614SQuant Time: 891031 03: 15In jec ted at : 8V 1030 13: 13

1 ' ' 7I U i /

QUflNT REPORT Page

Operator ID: YY6148Output F i l e : ~JB142::ACData F i l e : >JB142::U4Name :riisc: EUALC

ID Fi le: I 025 1C::UST i t l e : IFB/PST/PC8 3^SP-210QLast Calibration: 891031 06:12

Compound

Quant Rev:

2 J4) JM'su i. aih lur6 i 4fildr in7 1 •te p I. j L fi 1 o T epox i de

11) #4,4'-DDE13i #Endr i n1-) #4,4'-DUD16) #4,4'-DOT173 #Endrin aldehyde18 ) rtCjiUuAU 1 tan su fTa * el'J ) #Dibutylch lorendate'JO) itEndrm ketone ^fy^~-' ( ''•'• lo" ^^ (J/3///7

# C o mp o u n d uses ES T D

7 Quant Time:Injected at

D i l u t i o n Factor:Ins t rumen t ID

891031 OS:15S'n07U IS: 13

1. 0 0 :J 0 C

R.T. Scan* Height Cone Un i t s

3.586.'J8886338

91314. 1515 .58lS.r->515.5817.3023.0319. "1525.88

°3511139'.! 5

103816821135

3*61216

24396112801536

3 3 9 ' 3 08334

83347 id 4

161217

OUIJ146 UG-'MLU O U 2 0 7 UG-'ML iUO

. 0-66 ULi-'ML i : tOOUUl'87 UG-T1L iO^JQ U 0 3 4 6 UG-'ML mO

.101 UG.TIL 101;.00476 UU 'ML 1UC

i> t «u -1 i HT" 'M( '* n I"1

. U-• 7 j. i-'ls- 'Tl_ * U I-

. CU374 UG'TIL 1'JOOOLH50 UG-T1L 10U

. 0967 UG-'ML i1!:.!. 00579 UG..T1L : f.:i:3 8 4 . D C NC CAL iB iyO

1018

C H R O M f l T O G R O MFi l e > J B 1 S 0 1 .8 *mu.

403

440000-

3603C&-

340000;

3200Q0J

300000^

230800-

EVhi-B

806 1266 16 63

12

D a t a F i l e : > J B 1 ? 0 : : U 4f-lame :r t isc : EUttLB

Id F i l e : 1025 1C: :UST i t l e : IFB-'PST-PCB ?%SP-2100Last C a l i b r a t i o n : 8*1031 03:12

O p e r a t o r ID: YY6148Quant Time: 8g1031 08:16I n j e c t e d at: 391031 00:11

Quant Ou t pu t F i l eInstrument ID

1019

Operator ID: YY6148Output F i l e : ~Jbl5Q: : ftQData F i l e : > 36150: : U4Name :Misc:

QUANT

Quan t

Page

ID File: I 025 1C: : UST i t l e : IFB-'PST.-'PCB 3SSP-2100Last Calibration: 891031 08:1';

Compound

7 Ouan t T i ri:e :Injected at:

D i l u t i o n Factor-:Ins t rumen t 1C:

U31 UW:16C?! OC:ll

1 . U L: 0 0 L:

P.T. Scan* Height Cone Un i t s

6 J #W1d r i n17 ) irEndr i n1.4) ^-,4'-16) ^4,4'l"i #Endrin a IdehydsI1*) t f D i b u t y l c h l o r e n d a t e2 'J i #£nd r i o V. e t one


7.3814. 1315.72 94518.53 131215.72 9^328.02 16*119.70 1182

.0-21 UG-T1L

. u^:u UG-TIL. CU5A2 UG-'ML

. 'J2U6 UG'"1L. 01J425 UG-T1L

. 'J4V9 !JG 'ML. OU473 UG-'ML

101-l o O10C

1 0 2 0

CMROMBTOeRftMFile >KB181 1.0 amu. . EVRLfl

53£e00-

231000-

£30000-

229000-

226000-

227000-

226900-

225000-

224000-

££3600-

£££000-

££1006-

££0000-' j

400 80? 1200 161J0 2000I c-*r>rJ

m"

f

VA^U

D

us«

4 1

J ^_ —— ,„ „

4 8 IS 16 £0 £4 £S 32

Data Fi le: >KB181: : U2Name :Misc: EUALtt

Quant Output File: "KB181::AQInstrument ID:

1C*Id Fi le: I076IC: : UST i t l e : IFB---PST/-PCB 6' X 2 Mr) ID ?*SP-2100 2 UL INJLast C a l i b r a t i o n : 891128 00:29

Operator ID: KT8"?82Quant Time: 89H28 00:31In jected at : 8Q1127 19:38

•J r: ...' I- ..

Ope ra t or IDOutput F i l eData File:Name:Mi set EUALA

KT8532

QUANT REPORT

Quant Rev: 7

>KB181AQU2

7 Quant TimeInjected at

Dilution Fac torInst rumen t ID

Page 1

891123 00:J1891127 19:38

l.QOQOO

ID File: I076IC::USTitle: IFB--PST/PCB 6( X 2 MM IDLast Calibration: 891128 00:29

Compound

3%SP-2100 2 UL INJ

R.T. Scantf Height Cone Units

6)13)16)19)20)

ttA 1 d r i#Endr i#4,4'-ttDibut

nnDOTV 1 ch

ttEndr in keIto renda t eone

612162918

.75

.57

.35

.20

.00

405754101115121030

9186966442245883768

. 00470

.00371

. 00453

.00958. 000850

UG/MLUG/MLUGXMLUG/MLUG/ML

100100100100100

Compound uses ESTD

1CJ22

CHROttOTOGRBMFile >KB182 1.8 amu. . EVflLB

-£80000-

275000-

270009-

265009-

260000-

255000-

£45000-

24000fr

235000-

330000-•

225000-

400 900 1206 1600 2000. . . i . . . i . . . i , , . i . . . i . . . i . , . t . . . i . . . i . . . i

N

i

fs.«"

uv'l — J^ _si

8tri

i

coof

iM

(A 1 \ a)— 1 —

1

V .' 1 • 1 • 1 • 1 • 1 - 1 • 1 • 1 • \ • 1 | ' 1 • ! ' 1 ' 1 ' | ' I

4 8 12 16 20 24 28 32

Data F i l e : >KB162::U2Name:Misc: EUALB

Quant Output File: ^KB182::AQI n s t r u m e n t ID: "KPi

Id F i l e : I076IC::UST i t l e : IFB---PST/PCB 6' X 2 MM ID ?*SP-21GO 2 UL INJLast Calibration: 891128 00:29

Operator ID: KT8582Quant Time: 891123 00:32In jected at: 891127 20: 17

1U23

QUANT REPORT

Ope ra tor ID:Output F i l e :Data File:Name :flisc: EUALB

KT3532 Quant Rev: 7

>KB182ftQU2


D i lut ion Fac torIns t rument ID

Page 1

391128 00:32-691127 20:17

1.00000JiA-

ID F i l e : I076IC::UST i t l e : IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891128 00:29

Compound

5SSP-2100 2 UL INJ

R.T. Scan* Height Cone Uni ta

6)13)14)16)19)20)

#A 1 d PtEndp#4,4'#4,4'*DibuttEndr

i nin-DDD-ODTt y 1 ch lorendatein ke t one

6.12.14.16.25.17.

775707822093

406754844100915121076

4652853632262419648317442316

.0238

.0483.00304.0211.0517

.00312

UGXMLUG/T1LUG/MLUG/MLUG/MLUG/ML

100100100100100100


1024

CHROMflTOGRflMfilm >KB183 1.0 amu.

400

340009-

330000-

320000-

310008-

380000-

£30000-

£70000-

260000-

£50000-

240000-

22P900-

EVflLC

800 1200 1690 2090i ... i ... i ..... i ... i . . . . i ... i .. ^. j-

1 - I - I • 1 • [

12 16 20 £4 28

Data Fi le: >KB183: :U2Name :Miac: EU^LC

Quant Output F i le : ^KB183::AQInstrument ID: WT

I d F i l e : I Q 7 6 I C : : U ST i t l e : IFB/PST/PCB 6' X 2 MM ID 3*SP-21QQ 2 UL INJLast C a l i b r a t i o n : 891128 0 0 : 2 9

O p e r a t o r ID: KT6?82Ouant Time: 891128 O Q : ? 3In j e c t e d at : 891127 20 :56

1 f'iI u

Operator IDOutput F i l eData File:Name:Mi so: EUALC

KT85S2"KB183>KB183

QUANT REPORT

Quan t Rev: 7

U2

7 Quan t TimeInjected at

D i lut ion Fac torIns t rumen t ID

Page 1

391123 00:.?3.SQ1127 20:56

1.00000

ID File: I0761C::UST i t l e : IFB.-'PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891128 00:29

Compound

39SSP-210Q 2 UL INJ

R.T. Scan* Heigh* Cone U n i t s

6)13)14)16)19)20)

#A 1 d rttEndr#4,4'#4,4'#Dibu*Endr

i nin-DDD-DOTtylch lorendatein k e t o n e

61214162517

.77

.57

.02

.90

.22

.90

406754841101415131074

97600106560672047232598409934

.0500

.0960. 00773. 0506. 0974.0110

UG/TILUG''MLUG/MLUG/MLUG/MLUG/ML

100100100100100100

Compound uses ESTD

CHROMflTOGRflnFi le >KS193 1.0 amu. . EVflLB

280000-

275000-

270000-

265000-

260000-

25S000-

£50000-

£45000-

£40000-

235000-

£30000:£25000-

££0800-

400 805 120^ 1600 2000. . . r . . . i . . . I . . . I . . . I . . . 1 . . . i . . . I . . , I . . . I

£<M

mr--«i

^ -J <^ __

ID

in«

CD^ A*1^ a^ I *

I A / X 1^~ — — ^ W^ —— ..... ._/ v_- —— —1 • 1 • 1 • 1 • 1 • 1 • 1 ' 1 • 1 • 1 • 1 • 1 I ' 1 1 • 1 • 1

4 8 IS 16 20 24 28 32

Data F i l e : >KB193 : :U2 Quant Output F i le :Name : Ins t rumen t ID:Misc : EUALB

Id File: I076IC::UST i t l e : IFB/PST'PCB 6' X 2 MM ID ?!»SSP-210Q 2 UL IN3Last Cal ibra.t ion: 891128 00:29


1027

QUANT REPORT

Operator ID: KT8582O u t p u t F i l e : "KB193::AQData F i l e : >KB193::U2Name:Misc: EUALB

ID F i l e : I0761C::UST i t l e : IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891128 00:29

Compound

Quan t Re^: 7 Quant TimeInjected at

D i lut ion Fac torI ns trumen t ID

Page 1

891128 04:jOA891128 07:29

1. O O G O O

3!SSP-2100 2 UL INJ

R.T , Scan* Height Cone Uni ts

6)13)14)16)19)20)

#Aldr in#£ndr in#4,4'-DDD#4, 4 '-DOT#Dibutylch lorendatettEndr in ketone

61213162?17

.75

.55

.98

.78

.18

.90

405753839

100715111074

45952513283840

18176300163200

.0235

.0463. 00444.0195. 0489

.00354

UG/MLUG/-MLUG-'MLUG/MLUG/MLUG/ML

100100100100100100

Compound uses ESTD

1U28

CHRQMOTOGRfln>KB204

290000-

283000-

2S0000-

£75000-

278000-

263080-

268088"

253808-

250080-

£45388-

£38608-

£35008-

£20300-

400 800 1200

EVRLB

1600 £000

1£

Data F i l e : >KB2Q4::U2Name :M i s c : EUALB

Quant O u t p u t File:I n s t r u m e n t ID:

KB204::AQ

Id F i l e : I076IC::UST i t l e : IFBxPST/PCB 6' X 2 MM ID 3SSP-2100 2 UL INOLast. C a l i b r a t i o n : 891128 00:29

Operator ID: KT8582Quant Time: 891128 12:54Injected at: 891128 12: 19

1U29

QUANT REPORT

Operator IDOutput F i l eData File:Name :Misc: EUALB

KTS532"-KB204>KB204

Quant PC'AQU2



Page 1

891128 12:,54.891128 12:19

1 . 0 0 0 0 0JriA-

ID F i l e : I076IC::UST i t l e : IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891128 00:29

Compound

3XSP-21QQ 2 UL INJ

R.T. Scant Height Cone U n i t s

6)13)14)16)19)20)

#Aldr inftEndr i n#4,4'-DDD#4,4'-D.DTttDibutylchlorendate#Endr in ke t one

6.12.14.16.25.17.

725000731037

403750840

100415061072

45632538S82304

19136294402240

.0234

. 0436.00267.0205. 0479

. 00248

UG/MLUG.'MLUG-'MLUG/MLUG/MLUG/ML

100100100100100100

Compound uses ESTD

1U30

CHROMflTOSRflnFile >QB829 1.0 *»u.

400

EVflLB

8 IS 16 30 84 £6 32 36

Data File: >QB820::U6Name :Misc: EUALA

Quant Output File: ^QB820::AQInstrument ID: flR

Id File: I021IP::USTit le: IFBXPST/PCB 1.5KSP225Q/1.95SSP2401 2UL INJLast Calibration: 891019 23:51


1031

QUANT REPORT

Operator ID: YY6148Output File:Data File:Name:Misc: EUALA

>QB820AQU6

Quant Rev'- 7

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95HSP2401Last Calibration: 891019 23:51

Quant Time:In jected at

Di lut ion Factor:Instrument ID

2UL INJ

Page- 1

891024 10:41891024 08:22

1.00000

Compound R,T. Scan* Height Cone Units

6)11)13)14)16)17)19)20)

#Aldr in#4, 4 '-DDEtEndr in#4, 4 '-ODD#4, 4 '-DOT#Endr in aldehydetOibutylchlorendate#Endr in ketone

9.13.20.22.24.25.31.32.

8500424750475887

5891078122313461468152618931970

252803072198403648175361664

13184512

.00417

.00163.0108

.000713.0178.00109.0101

.000544

UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100100100100100100100

Compound uses ESTD

103?I w *J '.

CHROMQTOGRfirtF i l e >Q6821 1.0 MU.

490

320000-

300000-

380000-

260000-

240000-

220000-

200000-

190000-

600 1200

IAJ16 20 24

2000

$

36

Data Fi le : >QBB21::U6Name:M i s c : EUALB

Quant Outpu t Fi le : "QB821::AQI n s t r u m e n t I D :

Id File: IQ21IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891019 23:51


1033

QUANT REPORT

Operator ID:Output File:Data File:Name:Misc: EUALB

YY6148 Quant Rev: 7

>QB821:AQU6

10 File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95KSP2401Last Calibration: 891019 23:51



2UL INJ

Page- 1

891024 14:10891024 13:25

1.00000


6)11)13)14)16)17)19)20)

#Aldrin#4, 4 '-DDE#Endrin#4, 4 '-ODD*4,4'-DDT#Endr in aldehyde#D ibutylchlorendate#Endr in ketone

9.17.20.22.24.25.31.32.

8793455253556588

5901074122513491470153118971971

1342723712

1041286954

1226246208686084992

.0221.00182.0569

.00196.0735.00406.0527

.00531


100100100100100100100100

# Compound uses E5TD

1034

CHROMQTOGRBHFile >OB

440000-

488000-

360000-

320000-

200000-

240000-

20eoee-

922 1.0 AflU. EVflLC

400 f 600 t 1200 ( 1600 r 2000

S ^- S

l> ____ _«^_

r-

S

8K

»dLM•«.f>

* AH _ /v

uss

8l

' ' ; ' 8" ' 'iV ' '16 ' '2'0' ' 2'4 ' 2'6 ' 3'2 ' ' &' ' '

Data Fi le:Name :Misc: EOALC

>QB822: : U6 Quant Output F i l e : ^QB822::AQInstrument ID:

Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP225Q/1.95NSP2401 2UL INJLast Calibration: 891019 23:51


1035

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^08822::AQData File: >QB822::U6Name:Misc: EUALC

ID File: 1021 IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP24Q1Last Calibration: 891019 23:51

Quant Time:In jected at:

Oi lut ion Fac tor:Inst rument ID:

2UL 1N3

Page- 1

891024 14:57891024 14:12

1.00000

Compound R.T. Scan* Height Cone Unit*

6)11)13)14)16)17)19)20)

#Aldr in#4, 4 '-DDE#Endrin#4,4 '-ODD*4,4'-DDT#Endrin aldehyde$0ibutylchlorendateftEndr in ket one

9.17.20.22.24.25.31.32.

8895475255576788

5911075122613491471153218981971

2631696208

199681124802472971286413344011072

.0434.00252

.109.00404

.140.00841

.102.0118


100100100100100100100100


1036

CHROflfiTOGRflUOD IFile >QB823 1.8 amu.

28 ' 32 36

Data File: >QB825::U6Na me:Misc: DD I

Quant Output File: AQB825::AQInstrument ID: QR

Id File: I021IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891024 16:76

Operator ID: YY614BQuant Time: 891024 17:17Injected at: 891024 16:32

f 1uo

Operator ID: YY6148Output File: ^QB825::AQData File: >QB825::U6

QUANT REPORT

Quant Rev: 7

Data File:Name:Misc: DD I

ID File: IQ21IP::USTitle: IFB/PST/PCB 1.5SSP225Q/1.95KSP2401Last Calibration: 891024 16:36


Di lut ion Factor:Inst rumen t ID

2UL INJ

Page- 1

891024 17:17891024 16:32

1.00000Off


11)14)16)19)

#4,4'-DDE#4,4'-ODD#4,4'-DDT#Dibutylchlorendate

17.93 1074 4140822.50 1348 3106624.57 1472 2060831.67 1898 93568

,0117 UG/ML 100.0121 UG/ML 100.0103 UG/HL 100.0523 UG/nt 100


038

CHROMPTOGRPMF i l e >Q68£6 1.8

498 eee 1280

00 II

i$ee . eoee

Data F i l e : >QB826::U6Name:Miac: DD II

Quant Output File: ^QB826::AQInstrument ID:

Id File: I021IP::USTit la: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891024 16:36


1039

Operator ID:Output File:Data File:Name:Misc: DO II

YY6148

QUANT REPORT

Quant

>QB926AQU6

ID File: I021IP::USTitle: IFB/PST/PCB 1.5HSP2250/1.95XSP2401Last Calibration: B91024 16:36

7 Quant Time;In jected at:

Di lut ion Factor:Inst rumen t ID:

2UL INJ

Page- 1

891024 18:04891024 17:19

1.00000


11) #4,4'-DDE14) #4,4'-DDD16) *4,4'-DDT19) #Dibutylchlorendate


17.92 1073 22686522.48 1347 17900924.55 1471 13408031.65 1897 87808

0647 UG/tlU0699 KG/ML0671 UG/ML0490 UG/ML

100100100100

1040

CHROMfiTOGRftHFile >QB

1300088:

1388080:

110080$

1880084

900008;

70000$

680000J

500000:

400009;

300000;

200008J

927 1.0 Amu. DD III

400 800 1200 1600 2000

m

V

a.

uT

f

~

t

P

.A /\' 'I' ' ' k - ' 'iV ' '.I*' ' '<*'' 'I* ' 'a1.' ' '& ' '3'* ' '

Data File: >QB827::U6Name:f l isc : D D I I I

Quant Output File:Instrument ID:

-QB827::AQ

Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891024 16:36


1 C 4 1

Operator ID: YY6148Output File: "Q8827:Data Fi1«: >QB827:Name:Misc: DD III

QUANT REPORT

Quant Rev: 7AQU6

ID File: I021IP::USTit le: IFB/PST/PCB 1.5SSP2250/1.95KSP2401Last Calibration: 891024 16:36


Di lut ion Factor:Ins t rument ID:

2UL INJ

Page- 1

891024 18:51891024 18:06

1.00000

Compound R.T. Scant Height Cone Units

11)14)16)19)

#4, 4 '-DDE#4, 4 '-ODD#4, 4 '-DOT#Dibuty loh lorendate

15202229

.98

.20

.15

.12

957121013271745

957141M709790M613391M92396M

.270

.277

.307.0516


100100100

Compound uses ESTD

1042

CHROMftTOGRfinFile >QB841 1.0 anu.

400 1200

EVHLB

1600 £000

16 29 a4 ee 3S 36

Data File: >QB841::U6Name:tlisc: EUALB


Id File: I021IP::USTitle: IFBxPST/PCB 1.5SSP2250/1.95KSP2401 2UL INJLast Calibration: 891024 16:36


1043

N

Operator ID:Output File:Data File:Name:Misc: EUALB

YY6148

QUANT REPORT

Quant Rev: 7

>QB841AQU6


Dilut ion FactorIns t rument ID

Page- 1

891025 07:49891025 07:04

1:00000

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1Last Calibration: 891024 16:36

Compound

95KSP2401 2UL INJ


6)11)13)14)16)17)19)20)

#Aldr in#4, 4 '-DDE#Endr in#4, 4 ( -ODD*4,4'-DDT#Endrin aldehyde#Dibutylchlorendate#Endrin ketone

10.18.20.22.24.25.31.33.

0210636873789523

5991084123613591482154519151992

1536643520

11340811008120576

6144778246720

.0257.000995.0543.00430.0603

.00376.0435.00629

UE/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100100100100100100100

Compound uses ESTD

1044

CHRQMflTOSRflM. H*cl3 l.e urn. INDfl

320000-1i

240.3C.0-j

,1 ii

TJU

1 . .. 1 1200 200*

"T"" ! ' T ' T "' I1 ' T ' I'"' I""—r •Itf It 80 24 2* 32

Data File: >H^1I113 : : U4Name :M:ac: IND«

Quant Output File:Instrument ID: HA

I d F U e : I DMA : : UST! t le: IFB-'PST/PCe 1 . «>KSP22?Qxl . 95KSP240 1 2UL INJLast C a l i b r a t i o n : 891003 0 0 : 2 9

or ID: YYrl48Quant Time: 891026 18:0?In je'.t-id at : 8*1026 17:24

1045 ^

QUANT REPORT

Quant Rev*. 7Operator ID: YY6148Output File: ^H*213::AOData F i l a : >HA213::U4Name :Misc: INDA

ID File: IDH«;:USTit le: IFB'PSTVPCB 1.5NSP2250/1.95SSP2401Last C a l i b r a t i o n : 891003 00:29

Quant TimeI n j e c t e d at

D i l u t i o n Fac torInstrument ID

2UL IN;

891026 18:Or8^1026 17:24

1. i J 0 0 0 -'

Compound R.T. Scan* H e i g h t Cone Un its

2 )4)6 i7)10)12)15 i16)1 ">19)2 . i

#G*mma-BHC*Heptach lor#A I d r i nitHep tachlor epox i de*E'idoaulfan I#D i e 1 d r i n*E"dosulf an I I4^,4' -DOT#E"d r i n a 1 dehyde#Dibutylchlorendate#Mi- (: hoy yen lor

5.7 .8.

12.14.16.20.22.23.29.30.

832567386070ae7Q971835

351•43351S741874

100012511360143617491819

1146889723087552737236310411699275520663805587266688133248

.0365

. 0"66

.0379

. 0387

.0392

. OS .18

.0343

.07*3

. 0917

.0977.441

UGxMLUS 'MLUG/MLUG-'MLUG/MLUG-'MLUG-'MLUG MLUG/MLUG.-'PILUG/ML

10010'10010:100101001010010'100

Compound uses E3TD

1U46

CHROMOTOGROMFile .•fthi£14 INDE

Name il-lisc: I NOB

>HA2i4: : U4

Id File: IDHA: : UST i t l e : IFB'PST/PCB 1 . Last C a l i b r a t i o n : 891003 00:29

Quant Output Fi le: AHAInstrument ID: HA

. 95»iSP24Q 1 2UL INJ

or ID: YYol48Quant T ime: 8^1026 18:48I n j e c t e d a t : 8*1026 18:07

1U47

QUANT REPORT

Operator ID: YY6148Output File: ^HA214: :

Quant

Data Fi la:Name :Mi<5c: I NOB

>HA214: : U4

I 0 F i 1 « : IDHA: :UST i t l e : IFB/PST/PC8 1.5SSP225 0/1.*'Last Calibration: 891003 00:29

Compound

7 Ouan t Time'Injected at

Di 1 u t ion pac tor:Instrument ID

2UL IN,'

R.T, Scan* Height

Page 1-

8'; 02o 8:4-891026 18:'07

1. 0 0 0 0 i"

Cone Units

1)3)5)8)9 .'11)17 '14)18 '19)2 :J 1

#^lpha-BHCABeta-BHC#C»3lte-BHCftgamma-Ch lordane#a i oha-Ch lordanefc4 ,4'-::DE#E-dr in*4,4'-DDD#Endosulfari su 1 * a t ettDibutylchlorendatettE^'dr m ke t one

4.6 .7.13.14.16.IS.20.26.29.30.

4893983828257772171833

2674144778018?^9731124124115fr81"491813

140818410387276866560533121124432433237712655365203235712

.0355

.0761

.0344

. or 32

.037?

.0739

.0264

.0819

.0849

.0763

.0939

UG/MLUG/MLUG/'MLUG-'MLUG/MLUb.'MLUG/MLUb.'MLUG/MLUG 'MLUG/ML

1001010010100101001010010;.100

Compound uses ESTD

1043

i l s 1.6 arnu. INC-H

IS It at' 29

C i taName :

le: Quant Output File: ^HAInat rum«n t ID: HA

Id File: I044IP::USTitle: !FS-'PST,"PC& 1. VSSP2250/1! . 95SSP240 1 2UL INOLast C a l i b r a t i o n : 891003 00:29

O p e r a t o r I D : YV6148Quant Time: 891027 11:0"*I n j e c t e d at. : 8^1027 10:26

U 4 9

REPORT

Quant Rev.-Operator ID: YY6i«8Output File: 'VH*237: : AOData File: >HA237::U4Name •'Misc: INDA

ID F i le : I 044 IP: :UST i t l e : IFB/'PST/PCB 1. 5»iSP2250/l. 959(SP-:401Last C a l i b r a t i o n : 8 9 ? L Q 0 3 0 0 : 2 9


Di lu t ion Fac torInst rumen t ID

:UL IN;

Page 1

8'= 1027 11:0"891027 10:26

1.0000HA

Compound R.T, Scan* Height Cone Un i ts

2 )4)6 >7)

10)12)1" i

16)I'-)19)2 - )

#G.JfnmJtHept*^ 1 d r

•a-BHCach 1 ori n

^Heptachlor#Endos'j 1 f arii^Diel#E-.do^4 ,4 '

#E'.dr*Dibu#n-th

d r i ns u i a n-DOTm a idet y 1 ch 1 oOx ych 1 0

epox i deI

I I

hyd*r e n d a t er

5.7 f

8.12.14.16.20.22.23 .29.30,

8825673858708768931733

3SL4335 US741877

1 0 0 012^01 7> T- 914741"1481818

12134410^2169267273T.2568737

1244178256176673547216 0 801

142401

.0386

. 07- -6

. 0401

.0383

. 0427

. 0359

.0921

. 0*09

.0898, 1 1 a * i

.472

UGU^UGUGUGUGUGUGUGU&UG

/'ML/'ML-ML-•ML/'ML'MLML

-ML-•-ML'ML

/•ML

10010.10010:10010'1001010010 .100

Compound :STD

10CO

o<E

O-xjCM3. <LI X

10o

0 O

lL -c

4J •>

3 ECL D

O OC

a

•iZ)

LID

-' E

Z

J

-tC-lQ-

If-O-

O QvIT- C-lIN •-C-l <=>CL <=>LO

U' O

Ul CO

» Q. Ca o*-* f- '**

^T Q. *O v i.—• m ja

ll. -4) m

— •• uu. — -

t-4 *Or-( C J

(N <-*O O

C^ CD COTO (N C<Lfi O d1

H a- '.'^ co co

•—• o <JE

t. - -OO I- 1>

t- C 4"I) ifj "*

O O --

Operator ID: KT8P;82Output File: AHA249::AQData F i l e : >HA249::U4

QUANT REPORT

Quan t Rev: 7

Page 1-

Miac: INOB

ID Fi!*: IQ44IP::USTitle: IFB/PST/PCB 1.5SSP22SO/1L<»t C a l i b r a t i o n : 891003 00:29

Compound

;%SP2401

Quan t TimeInjected at

Di lut ion FactorI n s t r u m e n t ID

IN:.

026 '.12: 1-01:'26

1 . J 0 0 0

Compound uses ESTD

R.T. Scan* Height Cone U n i t s

1)3)

8)9 .11)13.'1 4 )IS J19)2-j •'

Off* 1 pha-BHC•i-Beta-BHC

#gamma-Ch lordane# a 1 p h a - Ch lordaneJl-4,4 ' -4t"dr i4>« , 4 ' -# E " d o •?*Dibul#E-id r i

r OE-pL-DD•j 1 anylch 1n ket

s u 1 f a t eo renda t eone-

467

1314161820262030

.48

.92

.98

.37

.28

.23

.75

.70

.13

. 15

.32

413477800

*7211231240156617*718 i^

1T18724372377376710405^680119^44334083*038723219"?47338913

.0383

.0366

.0408

.0389

. 0:-'41

. 0355

. i"!c(71

.0937

. U--42. 102

UG--

UGxU& 'UG--UG-'UG/UG,-UG'UG •'UG/

MLMLMLMLMLMLMLMLMLMLML

1001010010ICO101031010010100

1052

CHROnaTOGRan^'ile . 'hHr5/ 1.6 Amu.

338800-

30000P-

7000(3*-1

600000-

330000-

50000&-

itee gey*

Data Fi le: >H^257: : 114Name :

Quant O u t p u t F i l e :I n s t r u m e n t ID: HA

Id File: I 044 IP: : UST i t l e : IF5''PS~'PCB 1 .Last Calibration: 891003 00:29

2UL INJ

Operator ID:Quant Time: S'1030 10:15In jected at. : 8^ LQ70 09:29

1053

nfv/ff

QUANT REPORT Page

Operator ID: KT3532Output File: 'SHA25^:Data Fi le: >hA257:N-sme :Misc: INDft

ID File: IQ44IF: : USTit le: IFB/PSTVPCBLast Ca 1 ibrat ion i 89

: AQ:U4

1.5%SP2250/11003 00:29

Compound

2 ' *G,>roma-3HC4) *Heptach lor6 i *A i d r i P7 ) wHep tachlor epo

1 1 ) itEfdosu 1 fan I12) #Dieldrin151 *E^dosu 1 tan II16) #4, 4 '-DOT

x : i de

1 "^ ) *Efidrin aldehyd*

Quant R

. 95 MSP 2

R

5~?8

121416202223

19) ^Oibutylchlorendate 292 ; ) 4 >"-: t h o * ' ,i c h 1 o r 30

ev:

-01

.T.

.85

.22

.63

.37

. 55

.67

.83

.65

.88, 12.28

7I

Di lutIns

2UL

Scan*

749431516740871*og12481357143117451815

Cuan t T i me :njected at:i on Fac tor:trument ID:

IN;

He ight

!*;=• 09612S44810*760SC-967993614-256923649 * v u 567 693"r-851«7634

S9a*HA

A 0301030

1

Cone

. 0

. 04-

.04

. ij«

71*37573

. 0496

. i J,

.

V1,11

'5604181223

.655

1009

J 1::'29

. n o 0 o '

Un

UG/UG--'UG---UG.--UG/UG.'UG.'UG 'UG/UGUG/

i ts

MLMLMLMLMLMLMLMLMLMLML

q1001010010100101001010010100


1054

-::e /Hftifat i.S smu

D-'.a F i l e :Name :h ^c: INDS

Quant O u t p u t F i l e : AHA258Instrument. ID: HA

Id F i le: 104-IP::USTi He: IFE PST.-PC8 1. 5!iSP2250/l. 95*SP2401 2UL IN.3Last C a l i b r a t i o n : 891003 00:29

Oysra ta r ID: KTb t?82Quant T ime: 891030 10:08I n j e c t e d at : 8^030 10:17

1055

REPORT

Operator ID: KTS532 Quant Rev:Output File: ~H«258:: AQData File: >HA258::U4Name ;Misc: INDB

ID F i l e : 1044 IP: :UST i t l e : IFB/PST/FCB 1.5SSP225Q/1.95SSP2401Last Calibration: 891003 00=29

7 Ouan t T ; me :Injected at

D i l u t i o n Factor:I ns t rumerit ID

:JL IN;.

Page

£-1030 1089i030 10

1

Compound R.T. Scan* Height Cone Un i ts

11

1 -'3)5 !8)9 i1)'*• )

#*ipha-BHC*8eta-BHC#D« I ta-BWC4gamma-Ch lordaneHt« i oha-Ch lordsr.e414 ,4 '-DDE*Er-dr in

14) it- ,4' -ODD112

.-: )9 )•; 1

#£- dosM I f an sulfatc#D i b u t y 1 c h lorenddte#Fr d r i n ke t one

4.6 .7.

13.14.16.18.20.26.29 .30.

4792973727227363121328

244*>8w

11•• '1Jt «L

15j. ••13

or.1376005471oo39

46.15

1772815011291008814726560013703844 0 3 2

10 i 243840336^06542945

. 0447

. Ci-40

.0430

. U«o8

.0458

. 0'J*2

.0467

.0990. 109

. Q93«.113

UGUG

,-MLML

UG/'MLUGUGUGUGUGUGUG-UG

,-ML/ML•ML-'ML.-•ML-'ML•'ML••'ML

100101001010010'1001010010100

Compound uses ESTD

CMRQMPTOSRflMF i l e >Mfl493 1.9 amu. TUDfl

900000-

700900-

£00 00

400 • t 800 t _ iy?. , 3-50g . . . . . gg,gg

Data File: >HA493::U4Name :Misc: INDA


Id File: I076IP:: UST i t l e : IFB/PST/PCB 1,5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891031 13:04


1U57

QUANT REPORT

Operator ID: YY6148 QuantOutput File: ^HA493::AQData File: >HA493::U4Name :Misc: INDA

ID File: I 076 IP::USTit le: IFB/PST/PCB 1.5*SP2250/1.95KSP24Q1Last Calibration: 891031 13:04

7 Quant Time 1

Injected atD i lut ion Fac tor:

Inst rumen t ID:

2UL INJ

Page 1

891113 20:18891H3 19:34

1.00000HA

Compound R.T. Scan* Height Cone Unit*

2)4)6)7)

10)12)15)16)17)19)21)

#Gamma-BHCftHeptach lor#Aldrin#Hep tachlor epoxideftEndosu 1 fan I#D i e Idr in#Endosu 1 fan II*4,4'-DDT#End r in aldehydeftDibutylchlorendate#Me thoxych lor

5.7.8.12.14.16.20.22.23.29.30.

8725673858708770901837

350433518741873

100012501360143217491820

1830411669131295361110409856017433715782410867279552103040237185

.0365

.0335

. 0341

.0349

.0356

. 0697

.0961

. 0698

.0655

.0695.363

UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100100100100100100100100100100


CHROMOTOGftflM[file >Hfl494 "1.0 wi.

400

40Q000:I

1200

IHDB

1600 2000

28 32

Data File: >HA494::U4Name :Misc: INDB


Id Fi le: I076IP: : USTit le: IFB/PST/PCB 1 . 5SSP2250/1 . 95SSP2401Last Calibration: 891031 13:04

Operator ID: YY6148Quant Time: 891113 21:03Injected at : 891113 20:20

2UL INJ

1U59

Operator ID: YY6148O u t p u t F i l e :Data File:Name :Misc: INDB

QUANT REPORT

Quant Rev: 7

>HA494AQU4


D i lut ion Fac torIns t rumen t . ID

Page 1

891113 21:0389111? 20:20

1.00000HA

ID F i l e : 1076IP::UST i t l e : IFB/PST/PCB 1.5*SP225 0/1Last C a l i b r a t i o n : 891031 13:04

Compound

95SSP2401 2UL I NO

R.T. Scan* Hei g h t Cone Un i ts

1)3)5)8)9 )11)13)14)18)19)20)

ftAlpha-BHC*Bet«-BHC#Delta-BHCttgamma-Ch lordane#a 1 pha-Ch lordane#4, 4 '-DDEftEnd r in#4, 4 '-ODDttEndosu 1 f an sulfatettDibutylch lorendate#End r in ketone

4.6.7.13.14.16.18.20.26.29.30.

4893983830257772131833

26741447780185697311241241156617491818

2090257763211008096064927361560966214411852810240091584106177

.0339,0433.0344.0333.0400. 0654. 0869.0665.0679.0618.137


100100100100100100100100100100100

Compound uses ESTD

1UCO

CHRQMBTOGROHFile >HR514 1.0 amu. INDR

110000*

90000*

80000*

70000*

60000*

500000:

40000*

30000*

20000*

400 ' 800 1200 1606 2000. . . i . ^ _ ^ j . . . i . . . T . . . i . . . i . . . i . . . i . . . . . i .

.1.

s

^ § s R ^ - is

JlLiA IL JULjvL^4 8 12 16 20 24 28 35

Data File: >HA514::U4Name :Misc: INDA


Id Ftle: I076IP::USTit le: IFB/PST/PCB 1.5SSP225Q/1.95SSP2401 2UL INJLast Calibration: 891114 08:52

O p e r a t o r ID: YY6148Quant Time: 891114 18:41Injected at: 891114 17:58

1061

\

Operator IDOutput F i l eData File:Name :Misc: INDA

YY6148

QUANT REPORT

Quant Rev; 7

>HA514::U4

ID File: IQ76IP::UST i t l e : IFB/PST/PCB 1.5*SP2250/1.95SSP2401Last Calibration: 891114 08:52


D i l u t ion Fac torIns t rumen t I D

2UL INJ

Page 1

391114 13:41891114 17^58

1.00000HA

Compound R.T. Scantt Height Cone Un its

2)4)6)7)10)12)15)16)17)19)21)

#Gamma-BHC#Heptach lor#A 1 d P i nftHeptach lor epoxide#Endosul fan I#0 i e 1 d r i nftEndosu 1 fan I I#4, 4 '-DOTftEndr in a 1 dehyde#D ibu ty Ich lorendatettMe thoxych lor

5.7.8.12.14.16.20.22.23.29.30.

8523653757688570881735

34943251774Q87299912491360143117481819

19545718067313740811737610380813585716793712102465504110336263425

.0267

.0271

.0265

.0264

.0263

.0533

.0532

.0557

.0537

.0602.278


100100100100100100100100100100100


U62

CHRQMQTOQRQMFile >HflS

1300000-

1200000-

1100000-

1000000-

900000:

300000:

700000^

600000;

500000-

400008:

30000^

£00900:•

DataName :M isc :

as 1.0 amu. iNDfl460 • 800 1280 1600 2969. . . i . . . i . .. .1 . . . r. . . . i . . . i . . .1 . . . i. . . . i . . . i...

-*-_

Ss« . ^ s. ;P*- r * *O ** * i * ' i * w l r1 qi ^ 5 * ^ ^ p % _ Ji/l

III ii I ft K A^ JUul juLJl n lul/L. 7 V \ ^i . i . i • , . , - , . i . , . i - , . , . -j > | ' i i i ' i > r°*°"4 6 12 16 20 24 28 32

File: >HA525 ::U4 . Quant Output Fi le:Instrument ID: HA

INDA

Id Fi le: I076IP::USTit le: IFB/PSTxPCB 1.5HSP225Oxl.95SSP2401 2UL 1NJLast Calibration: 891114 08:52


QUANT REPORT

Quant Rev: 7

Page

Operator ID: YY614SOutput File: ^HA525::AQData File: >HA525::U4Name:Misc: INDA

ID File: I076IP::UST i t l e : IFB'PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: 891114 08:52


D i l u t i o n Fac torIns t rumen t ID

!UL INJ

891114891114

1HA

21:5621:12ooooo

Compound R.T. Scan* Height Cone Un i ts

2467

10121516171921

)))).i))))))

#Gamma-BHC#Heptach lor#Aldr in*Hep tachlor epoxide#Endosu 1 fan I*Die Idr inttEndosu 1 fan I I4t4,4'-DDTttEndrin aldehyde#D ibutylch lorendate#Me t hoxych 1 or

6.7.3.12.14.17.21.23.24.29.31.

1252977598103215377700

365449536763897

102412771387146017841858

207967M191160M146122M125099M110813M199498M180779M12876891520116544272062M

.0284

.0236

.0282

.0232

.0281

.0572

.0573

.0592

.0575

.0636.287


100100100100


1064

CHROMOTQGRflnF i l e >Hfl526 1.9 amu.

408

40008$;3S000&

3400e.fr

28000*

26980

220000-

£03000^

18000^

see 1200

INCfB1600 £000

16 24 28 32

Data F i l e : >HA526::U4Name:Miac: INDB


Id File: I076IP::UST i t l e : IFB/PST/PCB 1.5KSP2250/1.95HSP2401Last C a l i b r a t i o n : 891114 08:52


2UL INJ

1U65

QUANT REPORT

O p e r a t o r IDOut pu t F i l eData FiIe:Name :Misc: INDB

YY6148AHA526>HA526

Quant ReiAQU4

ID F i l a : I076IP::USTit le: IFB/PST/PCB 1.5SSP2250/1.95HSP2401Last Calibration: 891114 08:52


D i l u t i o n Fac tor:Ins t rument ID:

2UL INJ

Page 1

891114 22:418^1114 21:58

1. 00000HA

Compound R.T. Scan* H e i g h t Cone Un i ts

1)3)5)8)9)

11)13)14)18)19)20)

ftAlpha-BHC#Beta-BHC#Delta-BHC#gamma-Ch lordane#alpha-Ch l o r d a n e#4, 4 '-DDEttEnd r in#4, 4 '-ODDtfEndosulfan s u l f a t e#D i bu t y Ich lorendatettEnd rin k e t o n e

478

1314161921262931

,72.25.33.35.77.75.30.25.75.92.13

281433498829884

100311561273160317931866

212673M80915M113408M100204M98099M

166401M66624M

125761M107642M95659M109500M

. 0254

.0261

.0258

.0261

.0264

.0533

.0536

.0571

.0526

.0522

.0516


100

100


1 U66

CHROMOTOGROMFil» >JB143 1.0 »mu .

480 ( see

900000-

85*00 &-

8080fl0-

750000-

700080-

6GCQQO-

500000-•

450000-.

4 e>w we y-•

350900-

30y«0e-wj

1 _i

INDA

i2@0 1690 20ee. i . . . . . . i . . . i . . . i . . . i . .

KS

"Ki

ii'

.

^ T

«' |5 g> ^1 *; irt

1 * -

hI 1 A 1 14 8 12

? ._ t1-S "^

* 1,-J BIT iIk16

(__ ____ ^

Q09

A29 24 28 32 36

Data F i l e : >JB143::U4hJame :M i s c : iHDtt

Id F i le : I 0 2 5 I C : : U ST i t l e : IFB/PSTXPCB 3'/.SP-2100Last Calibration: SSO^O? 12:02


Quant Output F i l eInstrument ID

J&14?

1U67

Operator ID: YY6148Output File: /VJB143::AQData Fi le: > JE143: : U4Name :Misc: INDA

ID Fi le: I025IC: : USTi t l e : IFB/PST/PCB 3?iSP-2100Last

o j4)6 I•7 j

113)12)15 i16)17)19 '21 T

C a l i b r a t i o n : 8S0707 12:02

Compound

ftGamma-BHCftHep t ach I orfttt 1 d r i nftHeptachlor epoxidettEndosu 1 fan 1ftD i e 1 d r i nftEndosu 1 fan II#4, 4 '-DOTftEndr i n a 1 dehydeftD i b u t y 1 c h lore n dateftHe t ho> ych lor

QUANT REPORT

Quan t Rev : 7 Quan t T i me : 891Injected at: 8'J1

Di l u t i o n Factor:I n 3 t r u me n t ID: -i**"

R.

3.6.7 .9.11.13.14.13.15.28.23.

T

6373876057j. t.45575303«. .-

Scan ft

218? S 04725^66' 4~"37867

11149 -7 -"I

,• t

16821395

He ight

15372°146°4513363311142594145

1930891219211235851121-538379 2416514

Cone

0

3"

. 16

. 1173633

. 1

S.6

Page

31 08

1 . 0 Li

G

o

•305

.159

. ", ~2

•i. 1

333*2 .416514

^i-980.

7323•->u0

Un

UG/UG 'NOUG/UG-'UG/UG.'UG • 'UG/MONO

1

:03

its

ML1LCfiLl"1LML1LMLHLMLC«L 1CALI

q100i U «j

eiuoi 0 ',:1UO10 C1UO1001UO

tlbt:81 'JO

ft Compound uses ESTD

1U68

c co oC TDa n3 TM- QI

na.

00

3(I —.•• O

CO -<

M <>O O l-^l>) VjJ ft-O H> CO

O03

r H —Ql *-* Q

T ^- T)n -

n - —o» a>

o- co "-> \ oa T) i-j

o \ n3 TJ •••• n ••cc cCO If)CO 'jJ

O TDM t

oo

oM

^ Ci>Iff 3o «

CO

O0)

03

OCOiD

0- o

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O

5 ro

c:.o\

Operator ID: YY6148Output File: AJB144: : ACData Fi lc= >JB144: : U4Name :Misc: INDB

ID Fi le: I025IC: : UST i t l e : IFB/PST/PCB 3«SP^Last C a l i b r a t i o n : 880707

QUANT REPORT

Quant Rev: 77 Quart t T i me :Injected at:

Di 1 ut ion Fac tor:Instrument ID:

Page 1

89:031 03:048*1070 1'5:42

1.CD 000

12: 02

Compound R.T. Scan* Height Un i ts

1 J3)p )

3)9 I

11 )17)143IS)19)2U)

#Alpha-BHC#Beta-BHC#De1ta-BHC#gamma-Ch1o rdanettalpha-Chlordane#4,4'-DDE#Endrio#4,4'-DDD#Endo3uIfan sul fa tet t D i b u t y l c h l o r e n d a t e#Endr in ke t one

3 . 0 0 130 168001 .120 UG-'ML3 . 2 5 195 ^s->3, . f81 UG-T1L3.75 225 100753 .115 UG-'ML

10 .80 648 99535 9 9 5 8 5 . 0 0 MO CAL11.80 708 76608 7 6 6 0 8 . 0 0 NO CAL13.38 803 221697 .926 UG-'ML14.15 849 167745 16^745.0 MO CAL15.68 941 88001 .968 UG-'ML17.10 1026 127681 127681.0 NO CAL2 8 . 0 0 1680 744*6 74496.00 NO CAL19.78 1187 78465 .417 UG/ML

100100100

I 31 DC16100

10 CI 61 CO

100IB1UO1B10U

1JO

Compound ua-es ESTD

1U70

CHROMQTOGRQMFilf >JB

950000-

900000-

850000-

800800-

750000-

650000-

600800-

550000-

508388-

459*0*-

400000-

350800-

3e0*e^250800-,

152

1

1 .0

-t

3 ;u]u

4

amu .

00 8

<f

»i

r«v *•; ipi,yju3 12

t"? 1200

cHC

2

ri

r-l

ill illLl.1 • 1 • 1 • I ' ! •

16 2k;

INIlM

163$ 28@6

3•i•<

o«C-4LJ __

I • ! • I • I • : • I • I • I •24 28 32 36

Data File: >JB152: : U4Uame :

Quan t Out pu t FileIns t rumen t ID

Id F i l e : 102? 1C: : UST i t l e : IPS.'PST.'PCB 3%SP-2lOCLast Cal i brat ion: 891031 OS: 12

Operator ID: YV61ASQuant Tirne: 391031 08:17Injected at : 8*1031 03: 10

1U71

Operator ID: YY6148Output F i l e : AJB152Data File: >JB152Ma me :Misc: INDA

QUftNT REPORT

Quant Rev: 7

Page 1

U4

7 Quan t T ime :I n j e c t e d a t :

Di 1 u t ion Fac t o r :I ns t rumen t ID:

SV1071 07:101 . U 0 a 0 C

C70

ID Fi le: I025 IC: :UST i t l e : IFB-'PST/PCB 3!fiSP-2100Last Calibration: 891071 08:1!

Compound R.T. Scan# Height Cone Un 11 s

l-f

467

10121516171921

#

) ttGamma-BHC) #Hep t ach 1 orJ #A 1 d r i n) ttHep tachlor epoxide) ftEndosu 1 fan I) #D i e 1 d P i n) #Endosu 1 fan I I) #4, 4 '-DOT) *Endrin aldehyde) #Dibutylchlopendate) ^Me t hoxych 1 OP

Compound uses ESTD

2.6.7" .9.11.13.14.18.15.28.23.

63323760551043555002*. .•

2133794725 66937g6366

1113930

16811/94

1624971523211304331145619689719872112473712198511500984864

. 415234

. 0264

. U25^

.0244

. U'J57

. 0257

. 0515

.0512

. 0494

.0513

.0509.249

UG/'MLUG-'MLUG-'MLUG-'1LUG/MLUG "MLUG-'MLUG-'MLUG^'MLUG.'MLUG-'ML

1^* a«/* ///

100i 0 C100: o c-1001SC100IOL;1UO;o;:I'JO

1U72

cr.

«DC3 C TJ

— ft (1

O B fll

« H Oa ~ •»

3Hi (1 ->~ .. o

CO CO -C~O •Ji -C|_J ,_! O

C3 o t-1

*-j| ViJ 4>I-* t-> CO

o o•-•4 CO" "Ml CO

^^^

r H ~ u z oft «- u. ^ LJI Hitn ^ t« 2 ~j-» •— ~n o n* o1

n r. .. ..n •• — -nm n- — -1 — «— •• ,_ •—•- 1 | !_, IV

CT CD — CD1 \ Q

«• (/i '.Tl Cj- -i — TOO \ f' i--3 ~0 " '-Jl• • f •• 'jj

CD CCC' U">•0 '"J C»-• i* i*0 (f>

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O I-*CC 0

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rf:' — •

Cr~ "~I)______ « ———— —— ,— —— ••'! Ifl.ttv

"^ZHT-::; =*—— — 1 1 7SC —————— _. — ___________ _ _ _ _ _ 135E

^ ^===- —— 15.67

</

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w

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00

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uo

QUANT REPORT Page 1

Operator ID: YY6143Output F i l e : ~JB153::AQData F i l e : )JB153::U4Name !M;sc: INDB

I LI File: 1025 1C: : UST i t l e : IFBXPST-''RCB 3*SP-21QQLast Calibration: 8*1031 08:12

Compound

Quant Rev:7 Quan t T i me'Injected at

D i l u t i o n F a c t o fI ns t rumen t ID

1 0 S : 18

1. 0 C L: 0 U

Compound u 3-es ESTO

R . T . 3can# Height Cone Un 11

1 )7' )P :

3 )9 J

il -'1 .' 1

14^

13 )19 )21' i

ttfllph#Be t a#Ue 1 t

a-BHC-8HCa-BHC

t tgamma-Ch 1 o*a Ipf'^ 4 ^ 4 '#Endr*4 , 4 '^Endo#Dibu#tndr

a-Ch lo-DDEi n-ODD3 u 1 f a r.ty Ich 1in k e t

rdaner d a r. e

iu 1 f at*o r e n d a t eone

3.3 .3 .

10.11.13.14.

1? .17 .27.19 .

0023-i-i

807333136708*877

:

i'fc67!;!

O

g1!J

1611

30U42448' IJ-7'J348

40

2f-70

86

1735697~1-ir-. 7

10483?lOl^L:^

-no o • J• • c- O o/-• • ..-,p . .g

1 7 1 c 3 <;

89 lr: 3

1.' 158?"'66 USSO 448

. 0253 UG

. "21.- 6 US-

. 0261 UG-

. ::2EI; UG

. 02V;4 UG-

. :.:'; L'2 UG

. C511 UG-

. Llf:U7 UG-

.0515 UG

. ! _ ! — * w UG •

.0513 UG •

"ML'ML'Ml

- —11

"ML'ML'ML'ML'ML'ML'ML

1UOi 0 ::1 U 0: o L;1 !J C

1 '.' i.'I :.! '•'•1 ;.: I-1 :J ijI :j :;1 'J C-

fvltf

CHROnflTOGRflMF i l e >KB164 1.8 amu, , INDfl

900000-

650080-

75000*-

700006-

650000-

600000-

550800-

500000-

450000-

400000-

390000-

300000-

850000-

406 t 860 , 1200 ( 1600 ( 2000

*

fcEJ

.s S3S i-§l 1 §4 3 12 16 20 24 26 3S

Data Fi le:Name :Misc: INDA

>K8184: : U2 Quant O u t p u t F i l e : "KB184::AQIns t rumen t ID:

Id Fi le: I076IC: : UST i t l e : IFBxPST/PCB 61 X 2 MM ID 7SSP-2100 2 UL INJLast Calibration: 391122 15:26

Operator ID: KTS582Quant Time: 891128 QQ:20I n j e c t e d at: 391127 21:36

1075

QUftNT REPORT

Operator ID: KT8582Output File: 'SKB184: :

Quant RevOut putData F i l e :Name:Misc:

>KB194::U2


Di1u t ion Fac torIns t rumen t ID

Page 1

891128 00:20891127 21:36

1.00000

ID F i l e : I076IC::USTitle: IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891122 15:26

Compound

3S4SP-21QQ 2 UL INJ


2)4 )6)7 )10)12)15)16)17)19)21)

#Gamma-BHC#H«ptach lor#AldrinttHep t ach 1 orttEndosu 1 fan#Dic Idr inttEndosu 1 fan#4,4'-DDT

epox i deI

I

ttEndr in a 1 deh#Dibutylch lottMe t h-oxych 1 o

rr

I

ydeenda t e

356810111216132521

. 08

.37

.77

.33

. 15

. 8

.80

.83

.82

.20

. 17

185322406500609695763

1010829

15121270

64832693764881144416337926694454272466564238030720215361

.0250,0235.0225.0236. 0237.0458.0463. 0447. 0444.0493.235


100100100100100100100100100100100

Compound uses ESTD

CHROMOTOGRflMF i l e >KB185 l.P amu.

400

INDB

300000-

220000-

800 1200

32

Data File: >KB1S5::U2Name :Misc: INDB

Quant Output FileInstrument ID

Id File: I 076 1C:: UST i t l e : IFB."PST/PCB 6' X 2 MM ID 3SSP-21QO 2 UL INJLast C a l i b r a t i o n : 891122 15:26


1 t\r~> nU / /

Operator ID: KT3582Output File: ^KB1B5Data F i l a : >KB185Name :M i a c : INDB

Quant Re-ACU2


D i l u t i o n FactorIns t rumen t ID

Page 1

391128 00:.21-891127 22:15

1.00000

.atie: IFB/PST/st

PCB 6 1 X 2 MM ID 3SSP-2100 2 UL INJCalibration: 891122 15:26

Compound

111

1 )335 )8)9)1'.'3 j4 )18)19)o Q J

#Alpha-BHCttBe ta-SHC#De Ita-BHC#gamma-Ch Io rdane#a Ipha-Ch lordane#4 ,4 '-DDE#Endr i n#4, 4 '-ODD#Endosu 1 fan au 1tDibutylch#Endr- i n ke

fate1 o rends t et one

R.

2.2.7 .

9.10.11.12.14.15 .25 .17.

T.

55751745T "?

33G, 7

0777

1890

Scan*

153165190567622713754844922

15111074

He ight

6675261360428515043247296735365548843200486403257645184

Cone

.0260

.0253

.0256

.0229

. 0232

.0451

. 0625

.0418

. 0492

.0523

. 0468

Un it*

UG/ML •UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG-'MLUG/MLUG/ML

q100100100100100100100100100100100


1u78

c

nQ.

o

CO CO

00

r H "oi ~ a(A r+

(i -n •• —Oi (P

cr CD —-i \ oft "D '-1~ Ul O-^^ _I J__,

o \ n3 "0 "•• Cl ••

CD CCO (/I

10 xCO

IO

to•o ->

o

LftDIIO

oo

Cr

~ a>ui 3n »

zn

Oa

CD-o

C1-3

Oca3

3o> O~j fC XI=1 C

o »

•O-o

ru w(A OG> ®

w 01 a- ff*

3.07

21.10

ox

3>O

Operator IDOut put F i l eData File:Name :Misc: INDA

KT3582AKB199>K8199

QUANT REPORT

Quan t Rev: 7AOU2

7 Quan t Time:Injected at

Di lut ion Fac torIns t rumen t ID

ID File: I076IC::USTitle: IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 391128 00:29

Compound

3?iSP-2100 2 UL INJ

R.T. Scantf Height

Page 1

891128 09:.39.3*1128 09:03

1.00000

Cone Un i ts

2)4)6 )~? )10)12 )15J16)17)19.'21)

#Gamma-BHCttHep t ach la r#A 1 d r i n#Heptachlor epoxideftEndosu 1 fan I#Die Idr in#Endosu 1 fan IIIN, 4 '-DOT#Endr i n aldehyde#D i but y 1 ch lorendate#Methoxych lor

356310111216132521

.07

.33

.72

.23

. 10

. 53

.73

.73

.75

. 12

. 10

184320403497606692764

100732515071266

720006771249869439Q4334726668354208465284115223416210433

.0273

.0244

.0255

.0247

.0248

. 0498

. 0499

.0499

. 0480

.0463.244

LJG-'MLLJG/'MLUG--MLUG.-'MLUG/MLUG/MLUG/MLUG/MLUG---MLUG/MLUG/'ML

100100100100100100100100100100100

Compound uses ESTD

1 • *i\ U

CHRGMflTOGRflMF i l e > K B

900000-

350000-

800000-

750000-

700000-

650000-

600000-

550000-

500000-

450000-

400000-

300000-

2^0000-

295 1.8 amu. . I N O f t400 806 1200 1600 2000

U

5

T1**"' ^ ^* t-l O ^ ^^ ^ vS I 1 "^

L J A . A U f \ A A H *i • , • i i • : • i • i • i i i r • i • i • i • : : • i

4 8 12 16 SO £4 £8 32

Data F i l e : >KB205::U2Name :Misc: I MDft

Quant O u t p u t F i l e : AKB205::AQInstrument ID:

Id F i l e : 1076 1C: :UST i t l e : IFB-'PST/PCB 6' X 2 MM ID 3%SP-2100 2 UL INJLast Calibration: 891123 00:29

Operator ID: KTS582Quant Time: 891128 13:7?Injected at: 891128 12:59

1 (•. •"*1 UO

Ope ra t or ID:Output File:Data File:Name :Misc: INDA

KT8582

QUANT REPORT

Quant Rev: 7

>KB2Q5::U2


Oi lu t ion Fac torInstrument ID

Page 1

891128 13:33891128 12=59

1. 00000

ID FiIB: I076IC::UST i t l e : IFB--'PST/PCB 6' X 2 MM IDLast Calibration: 891128 00:29

Compound

3%SP-2100 2 UL INJ

R.T. Scanft Height Cone Units

2)4 )6)7)10)12 )15J16)17)19)21 )

#Gamma-BHC#Heptach lor#Aldr in^Heptachlor epoxidettEndosu 1 fan I#Die Idr inttEndosu 1 fan II#4,4' -DDT#Endr i n a Idehyde#D i b u t y 1 c h 1 o r e n d a t ettMe th-oxych lor

356B10111216132521

.05

.32

.70

.28

.08

.52

.72

.77

.75

.12

. 10

183319402497605691763

100682515071266

72064705925066145760339846841655616431924102430203219329

.0278

.0254

. 0259

.0258

.0251

.0511

.0512

.0516

.0478

. 0492.255

UG/MLUGUGUGUGUGUGUGUGUGUG

/ML/ML/ML/ML/ML/ML/ML/ML/ML/ML

100100100100100100100100100100100

Compound uses ESTD

1U32

CHROHftTOGRflMFile >KB206 1.0 *mu. INDB

310000;

300000J

290000^

£78930

see

: ' l ' l ' l ' lIS 16 20

l ' i24 £9 32

Data Fi1*: >KB2Q6::U2Name :Misc: INDB

Quant Output File: "KB2Q6::AQInstrument ID:

Id Fi la: I076 IC : :UST i t l e : IFB/PST/PCB 6' X 2 MM ID 39SSP-2100 2 UL INJLast C a l i b r a t i o n : 891123 00 :29

O p e r a t o r ID: KT3582Quant T ime : 891128 14:13I n j e c t e d at: 891128 13:38

033

Ope ra t o r ID:Out put F i l e :Data File:Name :Misc: INDB

KT8582

QUANT REPORT

Quant Re^i 7

>KB206::U2


D i 1 ut ion Fac torIns t rument ID

Page 1

391123 14:.13-891128 13=33

1. 00000

ID File: I076IC::UST i t l e : IFB/PST/PCB 6' X 2 MM IDLast C a l i b r a t i o n : 891128 00:29

Compound

3*iSP-21QQ 2 UL INJ

R.T. Scant Height Cone Uni ts

1)3)3)3)9 i11)1?)14)IS'19)20 )

#Alpha-BHC#Bata-BHC#Delta-BHC#gamma-Ch lordanetfalpha-Chlo#4, 4 '-DOE#End r in#4 ,4 '-ODD#Endoau 1 fan#Dibuty IchlttEndn in k e t

rdane

su 1 f ateo renda te v

one

2 .2.3.9.10.11.12.14.15.25.17.

5375174233355202321285

152165190565620711751841919

15071071

7526466819473225139247872761606043047520508803238446656

.0282

. 0272

. 0276

.0255

.0253

.0518

. 0545

. 0504

.0523

.0527

.0516

UG/MLUG/MLUG/MLUG/MLUG/MLUG-'MLUG-'Mt_UG/riLUG/MLUG/MLUG'-ML

100100100100100100100100100100100

Compound uses ESTD

1U34

CHROnBTOQRCinFlit >QB823 1.0 uu.

B0000&

60000*

40000*

30000*

20000*

12.00iNOfi

1680 2086

4 8 12 16 29 24 28 32 36

Data File: >QB823::U6Name:Misc: INDA,,,,,,.09x.1/.5NG

Quant Output File:Instrument ID:

Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1,95SSP2401 2UL INJLast Calibration: 891019 23:51


Uo5

QUANT REPORT

Operator ID: YY6148Output File: 06823:: AQData File: >QB823::U6Name:Misc: INDA,,, , , , . 05/.I/.5NG

ID File: I021IP::USTitle: IFB/PST/PCB 1.5KSP2250/1Last Calibration: 991019 23:51

Compound

Quant Rev: 7 Quant Time:In jected at

Di lut ion FactoriInstrument ID:

Page- 1

891024 15:43B91024 14:59

1.00000•QA--

95SSP24Q1 2UL INJ

R.T. Scan* He ight Cone Uni ts

2)4)6)7)10)12)15)16)17)19)21)

#Gamma-BHC#Heptach lor#Aldr in#Heptach lor epoxide#Endosulfan ItDieldr in#Endosu 1 fan I I#4,4'-DDT#Endr in aldehydettDibutylch lorendate#Methoxych lor

6891316182224253133

.77

.32

.90

.90,13.33.67.57.65.69.25

404497592826966109813581472153718991993

199297163969149568121984103744188289119680999048179289536185665

.0242

.0255

.0247

.0348

.0244

.0523

.0512

.0615

.0535

.0687.320


100100100100100100100100100100100

Compound uses E5TD

U 0 O

CHROMQT06RQMFile >aeea4 i.e «nu. INDB,,,....ev.iNs

400 , see , *g,M. ... 16.°.e. . .aa.ee.

18 24 38

Data File: >QB824::U6Name:Misc: INDB,,,,,,.05/.ING

Quant Output File: ~QB624::AQInstrument ID: Qft

Id File: I 021 IP::USTitle: IFB/PST/PCB 1.5SSP225 0/1.95SSP2401Last Calibration: 891019 23:51


2UL INJ

* i '. •> *7I Uo /

QUANT REPORT

Operator ID: YY6148Output File: AQB824::AQData File: >QB824::U6Name:Misc: INOB,,,,,,.05/.1NG

ID Fila: I021IP::USTitle: IFB/PST/PCB 1.5SSP225Q/1Last Calibration: 891019 23:51

Compound

Quant Rev: 7 Quant Time:In jec ted at


Page- 1

891024 16:30891024 15:45

1.00000

95SSP2401 2UL INJ


1)3)5)8)9)11)13)14)18)19)20)

#Alpha-BHC*8eta-BHC#Delta-BHC#gamma-Ch lordanettalpha-Ch lordane#4, 4 '-DDE#Endr in#4,4'-DDD#Endosu Ifan sulfate#Dibu ty Ich lorendate#Endr in ke t one

5.7.9.14.15.17.20.22.27.31.32.

1795139287934850926793

30B475546893950

107412271348167318981974

2457916865212576010694489344176961104497128000930567161653440

.0243

.0250

.0252

.0265

.0260

.0509

.0571

.0476

.0530

.0550

.0568


100100100100100100100100100100100


1038

CHROttflTOSRflnFile >QB817 1.0 amu.

496

1200000

60009*

60000

S0000&;

40000

aeeeee

1200INDH, , , , , , .05'.!'.3

1606 2006

ill T i i i r i i i p i n ^ j i i r T^4 8 12 16 20 24 26 32 36

Data F i l e : >QB847::U6Name:nisc: INDA,,,,,,.05/.I/.5 NG

Quant Output File: ^QB847::AQInstrument ID: JQft

67*3



10 89

QUANT REPORT

Operator ID: YY6148Output File: ^QB847::AQData File: >QB847::U6Name:Misc: INDA,,,,,,.Q5/.1/.5 NG

ID File: I021IP:: USTitle: IFB/PST/PCB 1.5KSP2250/1Laat Calibration: 891025 09:04

Compound

Quant 7 Quan t T ime:In jected at

Di lut ion FactoriInat rument ID

Page- 1

891025 16:24891025 13:58

1.00000QA-

95SSP24Q1 2UL INJ


2)4)6)7)10)12)15)16)17)19)21)

#Gamma-BHCfHeptach lor#Aldr in#Heptach lor a pox ide#Endosulfan 1#Die Idr in#Endosu 1 fan I I#4,4'-DDT#Endr in a Idehyde#Dibuty Ich lorendate#Methoxych lor

7.8.10.14.16.13.23.25.26.32.34.

1575373573983728428050

427523620859

1002113714001515158319662068

252780M201737M182785M144256M122432M221450M141317M109480M96428M106062M19975 4M

.0317

.0308

.0306

.0296

.0295

.0588

.0590

.0400

.0589

.0592.269


100100100

100

Compound uses ESTD

1090

CHROnftTOGRBHTile >QB858 1.8 *mu.

408

520080-

INDB

1200 1688 2808I . . ._!_.. ± . . I . . . I . . . I . . . I . .

480008-

440000-

36000*

280000-

200008

160880-

,16 £0 84 28 32 36

Data File: >QB858::U6Name:Misc: INDB

Quant Output File: ^QB858::AQInstrument ID: Q*

Id F i l e : I 021 I P : : U STitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891025 09:04


QUANT REPORT

Operator ID:Output File:Data File:Name:Misc: INDB

YY6148 Quant

> 0665 8AQU6

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: 891025.09:04

7 Quant TimeIn jec t ed at

Dilu t ion Fac torInst rumen t ID

2UL INJ

Page- 1

891025 16:16891025 15:31

1.00000

Compound



1)3)5)8)9)11)13)14)16)17)18)19)20)

#Alpha-BHC#Beta-BHC#Delta-SHC#gamma-Ch lordane#a Ipha-Ch lordane#4, 4 '-DDE#Endr in#4, 4 '-ODD#4, 4-' -DOT#Endrin aldehyde#Endosu Han sulfate*Dibutylchlorendate#Endr in ketone

58915161821232325293334

.55

.45

.68

.62

.58

.68

.30

.32,32.30.02.03.47

331505579935993

11191276139713971516173919802066

315062MB4653M154855M130782M1Q9598M210721M122919M153814M1548163264

10S672M84856M61996M

.0320

.0308

.0308

.0306

.0307

.0468

.0588

.0451

.0545.00200.0584.0474.0579

UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML

100100

100100100100

100100

1U92

o

00

1 -II T

1) O

U. -•

0. D*-> L

O ftC

DO

r-o

or-

O

a

O 00If, -I

Q.in

Ui COD LD

« Q- CQ. \ O^- \- -~

J IP ^•J Q. «o \ t-— Iti JD

v n— -- u

U. —

z r — H

1) Oe *

r r\<N ^

CO

-C .-• --<> O •>>- 00 CD

o -— i?

E

3 C

OU^NT REPOR

Opera tor ID:O'j t put F i 1 * :Data F i l e :N.Tiine :M i s c : TOXAPH

Y Y 6 - 4 8"Hfi218 : : C> H A 2 1 8 : = U 4

Quant 7 Do an t T i me '.Injected at:

D i 1 u t ion Fac t o r:Instrument ID:

10 Fi U: I0^4IP: : USTit le: IFB-'PSTVPCB 1. 5XSP225 0/1Last C a l i b r a t i o n : 8 '51030 11:18

2**oi 2UL IN;

R.T. Scant Height

Page 1-

8*? 030 U:2'691026 2Q:'I?7

1 -1000

Coric Un i ts

1'-)22)2 ""• ">24)

*C'>#To#Tu#To

& u t y 1 c h lorendatexaphenex a [j t"> e n e - '2xaphene~3

29212016

. 13

. 08

.30

. 70

17*9126312161000

6*472 .0491n33

:. 3417441630

111

.22

.39

. 23

UG^'MLU& 'MLUG/T1LUG 'rlL

1001010010'

O ij n d u S e

1U94

CHROMOTOGROMf i l e >H?M95 1.3 amu.

280000

270000^

26000&J

250900:

2200001

20000*

170000-^

TOKPPH

480 ' 800 1200 1600 2000. I . . . L . . . I ... I ... I ... I ... 1 . . . . . I . . . L .

12 20 24 28i r

32

Data Fi le: > H A 4 9 5 : : U 4Name :Misc: TOXAPH

Quant Output F i le : / S HA495: :AQInstrument ID: HA

Id File: I076IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/1.95*SP24Q1Last C a l i b r a t i o n : 891031 13:Q4

Operator ID: YY6148Quant Time: 891113 21:49I n j e c t e d at: 891113 21: 05

:UL INJ

1 U 9 5

Operator ID: YY6148Output File: ^HA495Data File: >HA495Name:Misc: TOXAPH

QUANT REPORT

Quant Rev: 7: AQ:U4

ID File: I076IP::UST i t l e : IFB/PST/PCB 1.5SSP2250/1.95HSP2401Last Calibration: 891031 13:04



2UL INJ

Page 1

391113 21:4989111? 21:05

1. 00000HA


19)22)23)24)

f t D i b u t y l c h l o r e n d a t eftToxaphene#Toxaphene-2#Toxaphene-3

29212016

. 18

.08

.32

.68

174912631217999

83136538882444834112

.0561.665.469.718

UG/M1LUG/MLUG/MLUG/ML

100100100100

Compound uses ESTD

1U96

CHROnRTOCRBflFilt >QB828 1.9 «nu.

489 888 1200

TOXHPH,,,,,,2 NG

1600 2000

860008;820808

440000J400088

32088*

680000

8 12 16 28 24 28 32

Data File: >QB82B::U6Name:Misc: TOXAPH,,,,,,2 NG


Id File: I021IP::USTi t le : IFB/PST/PCB 1.5HSP2250/1.95SSP2401 2UL INJLast Ca l ib ra t ion : 891024 16:36

Operator ID: YY6148Quant Time: 891024 19:38In jected at: 891024 18=5?

1u97

QUANT REPORT

Operator ID: YY6148Output File: AQBB28::AQData File: >QB928::U6Name:Misc: TOXAPH,,,,,,2 NG

ID File: I021IP::USTitle: IFB/PST/PCB 1•5XSP225 0/1Last Calibration: 891024 16:36

Quant Rev: 7 Quant TimeIn jected at

Di lut ion FactorInstrument ID

Page- 1

891024 19:38891024 18:53

1.00000OR"

Compound

95KSP24Q1 2LJL INJ

R.T. Scan* Height Cone Uni ts

19)22)23)24)

#Dibutylchlorendate#Toxaphene#Toxaphene-2#Toxaphene-3

31.65 1897 102465 .0572 DC/ML 10022.83 1368 1Q4769 1.23 UG/ML 10018.28 1095 64576 1.36 UG/ML 10022 .02 1319 84097 1.31 UG/fIL 100


1U98

sro<E

|T-v_o

/I'62

El 0

tXL

<I <II X

V O

3 ta D3 «O «

C

c•0-to

C-J<!X

— ct

oZ

o-I0.to

\O CD

CM ••

CL <-!ai

00

.. a c£L \ O

•J U> *^•st a «o '•- t.—• l Ci Jl

U. -u n

— - U- w

O U L_ — *->£ »l +* rtH» -* "U *"* *0

Z r « H _J

•> 0

CD

T-t

O

>

o - *••

0 t-

Operator ID: YY6148Output- File: AHA219::AQData File: >HA219:: U-4Name :Misc: AR1016

QUANT REPORT

Quan t Rev: 77 Quant T i .e :Injected at:

D i lu t ion Fac tor':Instrument ID:

Page 1

3'5 ! 030 '1:2-691026 21:40

1 . L) Q 0 0HA

ID File: IQ^IP: : UST i t l e : I FB--'PST/PCB 1. 5%SP2250/1. 95KSP24Q 1 2JL IN-Last C a l i b r a t i o n : 891030 11:18


1 5 ) #D i bu t-v'l ch 1 o rend a t e25) #Aroclor 10162n) #ft(? 1016-227) JtAR 1016-3

^ Con.pound uses ESTD

29.17 17487.27 4345.48 3279.13 ~46

79041 .0593 UG^ML 1001*3630 .~OQ U .-'ML 10"

84352 .297 UG^ML 10057728 .725 UG-T1L 10"

1100

(o/V

CHPOttQTQGPOH1.0 amu.

2000

Data Fi le: >Name :Misc: AP1221

Quant Output File: ^HA220::AOInstrument ID: HA

Id Fi-le: I04-IP: : USTt t le: IF&.-PST/PCB 1. 5KSF2250/1. 95SSP24Q1 2UL INJLast Calibration: 891030 11:18

Cue rat or ID: YY6148Quant Time: 891030 11:31Injected at: 891026 22:22

1 •, r-I I u

Operator ID: YY6148Output Fi le: AHFi220Data File: >HA220Name:Misc: AR1221

QUANT REPORT

Quant Rev: 7: AQU4

ID F i l e : IQ44IP::UST i t l e : IFB 'PST/PCB 1.5SSP2250/1.95SSF2401Last C a l i b r a t i o n : 8*1.030 11:18

t T i m e :I n j e c t e d a t :

D i 1 u t ion Fac t o r :In» t rumen t ID:

IN.

Page 1

S9 1030 11:3.691026 22=22

1. i3 0 0 0 -'HA


19;,28)2 « i30)

#D i b u t •-.> Ich l o r e n d a t e#Aroc 1 or4«P*AR

12'M1221

1221-2-3

29.18•4. 10

2.135.45

1749244126325

6534539790220604,724

.0490~.3

.OS

7 I10t?o

UG/UC---'UG^LIC-

t1LML'MLML

10010'"100ID1

Compound uses E£TD

CHKQMOT06RQM

i i i i '. \ i ' i i ] i r12 16 2* 24 2* 3£

Data Fila: >HA221::U4Na me:Misc: AP1232

Quant Output File:I n s t r u m e n t ID: HA

Id Fi le: I 04*IP::UST i t l e : IFE.'PST/PCB 1. 5*SP2250/1. 95?iSP240 1 2UL INJLast Calibration: 891070 11:18

Operator ID: YY6148Quant Time: 891030 11:37Injected at: 891026 23:Q5

1103

Operator ID: YY6148Output F i l e : AHA221Data F i l e : >HA221

QUANT REPORT

Quant Rev: 7AQU4

Misc: AR1232

ID Ft le: IIK4I P: : UST i t l e : IFBxPST/PCB 1.5%SP225 0/1,95SSP2«01List Ca l i b ra t i on : 891030 11:18

Ouant T ime :I n j e c t e d a t :

Di1u t ion ^ac t o r ;I ns t rurnen t ID'-

2UL

Page 1

8'- i030 11:?:891026 23:'05

1 . 0 0 0 0 '

Compound R . T . Scan# Height Cone Uni ts

1*131)3-M33)

#0 i bu t y I ch lore n date*Aroclor 1232#fr3 12T2-24tAR 1232-3

2975T

.18

.27

.43

.95

1749-34327475

67457391682329613248

.0506.333.213. 179

UG/UC--'UG-u&--j

"MLML'ML'ML

10010 =10010

Compound uses ESTO

i u

CMROnPTOGRfln1.0 HR1242

see isee seee

Data Fila: >HA222::U4Name:Misc: AR1242


Id File: 1044IP::USTitle: IFB-'PST/PCB 1.5SSP2250/1.95SSP2401 2UL INOLast Calibration: 891030 11:13


1 . -I I-I IO

QUANT REPORT Page

Operator ID: YY6148 QuantOutput File: ^HA222::AQData File: >HA222::U4Name:hisc: AR1242

ID File: I044IP::USTitle: IFB^PST/PCB 1.5SSP2250/1.95SSF24Q1Last Calibration: 89i030 11:18

7 Quant T ime:In jected at :

Di1u t ion Fac tor:Inst rumen t ID:

JL IN:

891030891026

1HA

ll23

3r47

Compound R.T. Scan* Height Cone Un i t ft

19)34)35)36)

#0 ibut y Ich lorenda te#Aroclor 1242#AP 1242-2#AR 1242-3

2971214

.17

.27

.68

.27

1748434759354

60417609922185614720

.0453.331.255.218

UG/'tlLUS/MLUG/MLUGxML

10010 V

100IQi

Compound uses ESTD

11 06

CHRCtlflTOGSflM

183000!

1.0 AfflU.

eee 1260

D*ta File: >HA223::U4Name:t-'.sc: AR1248

Quant Output FileInst rumen t ID

Id File: I044IP::USTitle: IFBXPST-'PCB 1. 5HSP2250/1. 95SSP24Q 1 2UL IN..Last Calibration: 891030 11:18

Operator ID: YY6148Quant Time: 891030 11:3^Injected at: 891027 00:30

::AQ

i07

\

QUANT REPORT

Operator ID: YY6148Output File: ^HA223::AQData File: >HA223::U4Name:Misc: AR1248

10 File: IQ44IP::USTitle: IFB/PST/PCB 1.5KSP2250/1Last Calibration: 891030 11:18

Quant Rev: 7 Quant Time:In jec ted at

Di lut ion Factor!Inst rument ID

2UL IN

Page -1

891030 11:3"891027 00:30

l.flOOO'HA

Compound

19) SDibutylcnlorendate37) #Aroclor 124833) #AR 12*8-239) #AR 1248-3

R.T. Scan*

29.18 174912.68 7S99.13 54610.53 630

Height

5964942*323488028224

Cone Units

. 0447 UG/ML.529 U&.'ML.320 UG/ML.708 UG/ML

q100101001Q>

Compound uses ESTD

1108

CHROnfiTOGRflttile >HA

ssaeae-r

700300-I

630000-

soeoee-

330003H

'30000-j

1.3 a»u.

400RR1234

2000

' 4 VK of

is se S4 a* 3*

Data FiName :Misc:

U4 Quant Output File:Instrument ID: HA

Id File: I044IP::USTitle: IFB'PST-'PCB 1.5SSP2250/1.95KSP2401 2UL INJLast Calibration: 891030 11:18

Operator ID: YY6148Quant Time: 891030 11:3*Injected at: 891027 01:12

1 109

Operator ID: YY6148Output File: *HA224'Data File: >HA224:Name:Misc: AR1254

QUANT REPORT

Quant Rev: 7AQU4

ID File: IQ*4IP::USTitle: IFB/PST/PCB 1.5SSP2250/1Last Calibration: 891030 11:18

Compound

Ouan t T i me :Injected at:

D i l u t i o n Fac tor:Ins t rument ID:

IN;

R.T. Scan* Height

Page 1

691050 11:3-891027 01:'l2

1.0000HA

Cone Units

19)40)41 )42)

#0 ibu ty 1 ch lorendate#Aroclor 1254#AP 1254-2#AR 1254-3

29.17.14.18.

17130553

174810268*i

1110

5*322066688573447*4 6

.445

. 876

.532

.636

UG/'hLUGUGUL-

/•MLx-ML-'ML

10010='10010'

Compound uses ESTD

11 10

\

File >Hfl233 1.8 4»u.

190000-

HR1E60

88U , 1288 , 1 882890

88 3S

Data File: >HA225::U4Name:Misc: AR1260

Quant Output FiletInstrument ID: HA

:: AQ

Id File: I044IP::USTitle: IFB/PST/PC6 1.5*SP2250xl.95XSP2401Last Calibration: 891030 11:18


2UL INJ

1 1 1 1

QUANT REPORT

Operator ID: YY6148Output File: ~HA225::AQData File: >HA225::U4Name •ttisc: AR1260

10 File: IQ44IP::USTitle: IF8/PST/PCB 1.5SSP225Q/1Last Calibration: 891030 11:18

Compound

Quant Rev: • 7 Quant T ime iIn jected at:

Di lut ion Fact or:Inst rument ID:

Page 1

891030 11:4:891027 01:55

l.OOOOC-HA

95KSP24Q1 2UL


19) $DibutyIchlorendate43) *Aroclor 126044) *AR 1260-245) *AR 1260-3


29.18 1749 571716 .429 UG/MU 10027.55 1651 107649 .''30 US/ML 10C22.48 1347 77632 .834 UG/ML 10019.83 1183 66561 .609 US/ML 10i

1 1 1 2

CHROMflTOQRfiflFile >Hfl496 1.0 MU.

490

300000.

36000ft

34900ft

32099ft

399909;

290000;

26000ft

24999ft

22999ft

29000ft

18000ft

2000

12 16 24 32

Data File; >HA496;:U4Name:Misc: ARID 16

Quant Output File: *HA496::AQInstrument ID: HA

Id File: I 076 IP::USTitle: IFB/PST/PCB 1.5NSP225 0/1.95SSP2401Last Calibration: 891031 13:04


2UL INJ

V113

QUANT REPORT

Operator ID: YY6148Output File: ^HA496Data File: >HA496Name:tlisc: AR1016

Quant Rev: 7AQU4

ID File: I076IP::USTitle: IFB/PST/PCB 1.5XSP2250/1.95XSP24G1Last Calibration: 891031 13:04



2UL INJ

Page 1

891113 22:35891113 21J51

1.00000HA


19) #Dibutylchlorendete25) tAroclor 101626) *AR 1016-227) #AR 1016-3


29.20 1750 106049 .0715 UG/ML 1007.27 434 192449 .289 UG/ML 1005.48 327 112576 .288 UG/ML 1009.15 547 76992 .286 UG/ML 100

1 I i 4

CHROMBTOQRflllFile >H«497 1.0 amu. flRl£21

440000-

360000-

320000-

200000-

240000-

200000-

160000-

2000

0 12 16 20 84 20 ' 32 '



Id File: I 076 IP::UST i t le : IFB/PST/PCB 1.5XSP225Q/1.95XSP2401 2UL INJLast Ca l ib ra t ion : 891031 13:04

Operator ID: YY6148Quant Time: 891113 23:21In jec ted at: 891113 22:37

1H5

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^HA497::AQData File: >HA497::U4Name:disc: AR1221

ID File: I076IP::USTitle: IFB/PST/PCB 1.5SSP225Q/1.95SSP2401Last Calibration: 891031 13:04

Quant Time:Injected at:

Di lut ion Factor:Ins t rument ID:

2UL INJ

Page 1

891113 23:21891113 22.:37

1.00000HA


19) ftDibutylchlorendate28) #Aroclor 122129) #AR 1221-230) *AR 1221-3

$ Compound uses ESTD

29.18 1749 944014.10 244 581122.13 126 353925.42 323 9792

.0637 UG/ML 100.289 UG/ML 100.282 UG/ML 100.311 UG/ML 100

1 '11 6

CHROnflTOSRBflFile >Hfll?e 1.0 amu.

480900-

44080fr

49000&

328888;

280000J

24000^

288888^

12

1680 3889. . . i . . .1 . . . i . ... i. .

28 32



I d F i l e : I 0 7 6 I P : : U STit le: IFB/PST/PCB 1.5SSP2250/1. 95SSSP2401Last Calibration: 891031 13:04


2UL I NO

11 i 7

QUANT REPORT

Operator ID: YY6148Output Fi le: ~HA498Data Fi le: >HA498Name:Misc: AR1232

QuantAQU4

ID File: I076IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95KSP24Q1Last Calibration: 891031 13:04


Di lut ion Factor:Inst rument.ID

2UL INJ

Page 1

891114 00:06891113 23;23

1.00000HA


19) fcDibutylchlorendate31) *Aroclor 123232) #AR 1232-233) #AR 1232-3


Compound uses ESTD

1 i i s

\

CHROMOTOORPMFile >HR499 1.0 a»u.

409 900 1200 1608 2680

IS 24 32

Data File: >HA499:: U4Name:Misc: AR1242


Id Fi le: I076IP::USTit le: IFB/PST/PCB 1.5SSP2250/1.95SfiSP2401 2UL INJLast Calibration: 891031 13:04


1 1 1 9

Operator ID: YY6148Output File: ^HA499Data File: >HA499Name:Misc: AR1242

QUANT REPORT

Quant Rev: 7:AQU4


Di lut ion Fac torInst rument ID

Page 1

891114 00:52891114 QQ.:08

1.00000HA

ID File: I076IP::USTit le: IFB/PST/PCB 1.5SSP225Q/1Last Calibration: 891031 13:04

Compound

95SSP2401 2UL INJ


19) #Dibutylchlorendate34) #Aroclor 124235) #AR 1242-236) *AR 1242-3

4 Compound uses ESTD

29.23 1752 830737.28 435 3102512.98 777 10329714.25 853 42561

0560 UG/ML.280 UG/ML.331 UGXML.195 UG/ML

100100100100

1 I 20

CHROnflTOQROMFile >Hfl580 l.e amu.

408RR1£4S

see 1200 2000

Data File: >HA500: : 1)4Name:M i s c : AR1248

Quant Output File:Inatrument ID: HA

: :AQ

Id F i l e : I 0 7 6 I P : : U ST i t l e : IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL INJLast C a l i b r a t i o n : 891031 13:04

O p e r a t o r ID: YY6148Quant T i m e : 891114 01:38I n j e c t e d at: 891114 00:54

1 121

QUANT REPORT

Operator ID: YY6148 ' Quan tOutput File: ^HA50Q:: AQData File: >HA5QO::U4Name:Misc: AR1248


7 Quant Time:Injected at

Di lut ion Fact or:Instrument ID

2UL INJ

Page 1

891114 01:38891114 00;54

1.00000HA


19) tOibutylchlorendate37) #Aroclor 124838) #AR 1248-239) #AR 1248-3


29.18 1749 81665 .0551 UGxhL 10012.68 759 59546 .267 UG/ML 1009.13 546 47680 .272 UG/ML 10010.53 630 39488 .283 UG/ML 100

1122

CHROMflTOSROMFi le >HR301 1.8 arau. flR1254

i™100000*

99000*

79009*

600000;

50000*

40008*;

300000;

£0000*

400 • 800 1200 1600 2000

BO

s1

m tg

- */V^^M^/AA^AA^SWV4 8 ' 12 ' 16 ' 20 ' 24 ' 28 ' 32 ' .

Data File: >HA301::Name:Misc: AR1254


Id File: I076IP::USTitle: IFB/PSTVPC8 1.5SSP2250/1.95SSP2401 2UL INJLast Calibration: 891031 13:04


VI 23

QUANT REPORT

Operator ID: YY6148Output File: AHA501Data File: >HA5Q1Name:ttisc: AR1254

Quant Rev: 7AQU4

Quant TimeIn jected at

Di lut ion Factor:Inat rument ID

Page 1

891114 02:23891114 01;40

1.00000HA

ID File: IQ76IP:: USTitle: IFB/PST/PCB 1.5SSP225D/1Last Calibration: 891031 13:04

Compound

95XSP24Q1 2UL INJ

R.T. Scanft Height Cone Units

19) ftDibutylchlorendate40) #Aroclor 125441) #AR 1254-242) #AR 1254-3


29.18 1749 79885317.15 1027 8934414.05 841 6969618.55 1111 101120

q ..539 UG/fIL 100.549 UG/ML 100.448 UGxML 100.622 UG/ML 100

112*

CHROHPTOGRflMFi le >Hfl38Z 1.8 Ainu.

490

1200000

1008800:

90000&J

706000;

609000;

900008;

400090

200000:

800 1200 1600 2000

12 16 20

Data File: >HA502::U4Name '•Misc: AR1260


Id File: I076IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95\SP2401 2UL INJLast Calibration: 891031 13:04


1125

QUANT REPORT

Operator ID: YY6148Output File: ^HA5Q2Data Fila: >HA502Name:Misc: AR1260

Quant Rev: 7:AQU4

ID Fila: I076IP::USTit la: IFB/PST/PCB 1.5*SP2250xl.95SSP2401Laat Calibration: 891031 13:04

Quant TimeIn jectad at

Dilut ion FactorInstrument ID

2UL IN3

Page 1

891114 03:09891114 02J25

1.00000HA


19)43)44)45)

#Dibutylchlorendate#Aroclor 1260#AR 1260-2#AR 1260-3

29.18 1749 89664527.58 1653 16595322.50 1348 12339219.85 1189 121601

.605 UG/ML

.609 UG/ML

.614 UG/ML

.697 UG/tIL

100100100100

Compound uses ESTD

1126

CHROMBTOGRRttFile >QB829 1.0 anu.

460000-440000-420000-

400000-90000*

360000-

340000-

seoooo-300000-

280000-

260000-

£40000-

&S0000-200000-

180000-

0f 0 , 12,00

RR1016,,,,,,.5 NG

1600 . 20.00

12 16 24 20 36

Data File: >QB829::U6Name:Misc: AR1016,,,,,,.5 NG


Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95HSP2401 2UL INJLast Calibration: 891024 16:36


\

QUANT REPORT Page-

Operator ID:Output File:Data File:Name:Misc: AR1016

YY6148

>QB829::U6

....... 5 NG

Quant Rev: 7

ID File: I021IP::USTitle: IFB/PST/PCB 1.5HSP225Q/1.95SSP24Q1Last Calibration: 891024 16:36

Quant TimeIn jected at


2UL INJ

891024 20:25891024 19:40

1.00000


19) tDibutylchlorendate29) #Aroclor 101626) #AR 1016-227) *AR 1016-3


31.65 1897 1198098.38 501 2361616.38 3S1 14425611.95 715 90944

.0669 UG/ML 100.275 UG/ML 100.275 UG/ML 100.284 UG/ML 100

CHROflPTOSRflnFlit >QB830 1.0 MU.

1200

RR1S21,,,,,,.5 MS

1600 2000

20 24 20 328 ' 12 36

Data F i l e = >QB830::U6Name:Misc: AR1221,,,,,,.5 NG

Quant Output File: *QB830::AQInstrument ID:

Id File: I021IP::U5Title: IFB/PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: 891024 16:76


2UL INJ

VI 29

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^QB83Q::AQData File: >QB83Q::U6Name:Misc: AR1221,,,,,,.5 NG

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: 891024 16:36

Quant Time:Injected at'


2UL INJ

Page. 1

891025 08:41891024 20:27

1.00000


19) *Dibutylchlorendate28) tAroclor 122129) #AR 1221-230) #AR 1221-3


31.65 1897 95168 .0531 UG/ML 1004.08 243 140032 .575 UG/hL 1002.43 144 41792 .287 UG/ML 1004.77 284 70272 .756 UG/ML 100

VI 30

CHROHflTOGRftMFi l t >OB831 1.0 *»u.

t 400 , 000 ..... ia,ae. . 1500 2000, ...

4 8 12 16 80 £4 Z9 32 36


Quant Output File: AQB8M::AQInatrument ID:

Id File: I021IP::USTitle: iFB/PST/PCB 1. 5HSP2290/'l .99*SP2401 2UL INJLast Calibration: 891024 16:36


1 I 31

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ~QB83l::AQData File: >Q883l: :U6Name:Misc: AR1232,,,,,,.5 NG


Quant Time:Injected at:


2UL INJ

Page. 1

891029 00:00891024 23:15

1.00000-Off


19)31)32)33)

#Dibutylchlorendate#Aroclor 1232#AR 1232-2#AR 1232-3



1 I 32

CHROnflTOGRQnFlla >QB832 1.0 auu.

400

RRlS^e,,,,,,.5 NG

1$00 .

000000-

750000-

700000-

6S0000-

688888-

550000-

500000-

450000-

400000-

350000-

300000-

350000-

aeoooo-158888-


Quant Output File: AQB832::AQInstrument ID:

Id File: I021IP: : USTi t le : IFB/PST/PCB 1 . 5SSP2250/1. 95SSP2401Last Cal ibra t ion: 891024 16:36

Operator ID: YY6148Quant Time: 891025 00:47In jec ted at: 89102? 00:02

2UL INJ

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: "QB832::AQData File: >QB832::U6Name:Misc: AR1242,,,,,,.5 NG



Di lut.ion Factor:Instrument ID:

2LJL INJ

Page- 1

891025 00:4789102? 00:02

1.00000


19)34)35)36)

tDibutyIchlorendatetAroclor 1242*AR 1242-2#AR 1242-3

31.63 18968.38 50112.00 71814.08 843

87040 .0486 UG/ML 100110976 .299 UG/ML 10046208 .291 UG/ML 10056577 .422 UG/tlL 100

Compound uses ESTD

VI 34

CHROMflTOQRflnFilt >OB833 l.O «»u. BR1248, ,.....5 N6

440000-

400000-

360000-

320000-

288880-

240008-

200000-

160000-

1280 | 16,00 , 2888

24 88 32 36

Data File: >QB833::U6Name:Miac: AR1248,,,,,,.5 NG

Quant Output File: "Q8833::AQInstrument ID: -Oft*

Id File: I021IP::USTitle: IFB/PST/PCB 1. 5*SP225Q/1. 95KSP2401 2UL INJLast Calibration: 891024 16:36

Operator ID: YY6148Quant Time: 89102? 08:42Injected at: 891025 00:49

VI 35

QUANT REPORT

Operator ID:Output File:Data File:Name :Misc: AR1248

YY614S*QB833::AQ>QB833: : U6

.5 NG

Quant Rev: 7

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95KSP2401Last Calibration: 891024 16:36


Di lut ion Factor:In»trument ID:

2UL INJ

Page- 1

891025 08:42891025 00:49

1.00000


19)37)38)39)

*0ibuty Ichlorenda te#Aroclor 1248*AR 1248-2#AR 1248-3

31141115

.57

.93

.98

189787271.4957

890251054735132874688

.0497.415.285.430


100100100100


U36

CHROhflTOQRflMFile >QB834 1.9 fiRl£54 , , , , , , 1 N6

32 36

Data Fila: >QB834::U6Name:Misc: AR1254,,,,,, 1 NG


Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95KSP2401 2UL INJLast Calibration: 891024 16:36


1 l 37

QUANT REPORT

Operator ID: YY6148Output File: "QB834::AQData File: >QB834::U6Klmm* ;

Quant Rev: 7

DataName:Misc: AR1254,,,,,, 1 NG

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP225 0/1.95SSP2401Last Calibration: 891024 16:36


Di lut ion Factor:Inst rument ID:

2UL INJ

Page- 1

891025 02:21891025 01:36

1.00000


19) fDibutylchlorendate40) tAroclor 125441) *AR 1254-242) #AR 1254-3

4 Compound uses ESTD

31.68 189920.35 121918.90 113223.02 1379

888708 .496 UG/ML 100121472 .566 UG/ML 100111232 .568 UG/ML 10095296 .598 UG/ML 100

VI 38

CHROHPTOSRPHFUt >QB63S 1.0 ABU.

408

HR18H, , ,

1208888;

1100000!

1000000;

900000;

880000;

700000

S00000J

40000fr

300088J

S0880&

***

8 ' 84 36

Data F i l e : >QB83?::U6Name:Misc: AR1260,,,,,, 1 NG

Quant Output File: AQB835::AQInstrument ID:

Id File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401 2UL 1NJLast Calibration: 891024 16:36


Vl 39

QUANT REPORT Page-

Operator ID:Output File:Da t a File:Name:disc: AR1260,,,,,,

YY6148AQB835::AQ>QB835::U6

1 NG

Quant Rev: 7

ID File: I021IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP2401Last Calibration: B91024 16:36

Quant Time:In jected at'


2UL INJ

891025 03:08991025 02:23

1.00000QA-


19)43)44)45)

tDibutylchlorendate#Ar.oclor 1260#AR 1260-2#AR 1260-3

31.65 1897 87283724.38 1461 14476.821.63 1296 12428929.97 1796 122048

.487 UG/MU 100

.637 UG/ML 100

.658 UG/ML 100

.530 UG/ML 100


VI 40

ETC

RAW QC DATA

Vi41


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Coda:

Cont ract:

Case No.:

Matrix: (soil/water) WATER

Sample ut/vol: 10QO. (g/mL) ML

Leve 1 : ( loui/med ) LOU

S Mo isture : not dec. dec.

Extraction: (SepF/Cont /Sonc ) SEPF


SAS No.: SDG No.:


Lab File ID: >QB836

Da te Rece wed :

Date Extracted:


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

319-64-6 ——————— alpha-SHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9-———--—gamma-BHCCLindane).76-44-8 ———————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3——-——Heptachlor epoxide959-98-8——————-Endosulfan I______6Q-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8————————Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-DDD__________1031-07-8 —————— Endosulfan sulfate.50-29-3 ———————— 4,4 '-DOT_________72-43-5---------Methoxychlor_____53494-70-5 ————— Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Chlordane___80Q1-35-2--—---Toxaphene________12674-11-2 ————— Aroc lor-10 16_____11104-28-2 —— —— Aroclor-1221_____11141-16-5 ————— Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242______12672-29-6 ————— Aroc lor-1248______11097-69-1 ————— Aroc lor-1254______11096-82-5 ————— Aroc lor-1260_____

,050,050,050,050,050,050050,050100

, 100,100,100100,100100500100500500

j500500500500500

1 I 42

Q

IIUIUIUtuIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUI

FORM I PEST 1/87

CHRoriflTOGRflM>QB836 1.0 uiu. ac700218,Q670021 ,L

440000-

40eeee-

360000-

330000-

280000-

240008-

200000-

i6 24 28 32 36

Data File: >QB836::U6 Quant Output File:Name: Instrument ID: -QAMisc: QC70021G,QG70021,L:G2,1000,10 d

Id File: I021IP: : USTitle: IFB/PST/PCB 1.5XSP2250X1.95SSP2401 2UL INJLast Calibration: 891025 09:04


1143

QUANT REPORT Page- 1

Operator 10: YY6148 Quant Rev: 7 Quant Time: 891029 09:08Output File: *QB836::AQ Injected at: 891025 03:10Data File: >QB836::U6 Dilution Factor: 1.00000Name: Instrument ID:Misc: QC70021G,QG7Q021,L:G2,1000,10

ID File: I021IP::USTit le: IFB/PST/PCB 1.5XSP2250/1.95SSP2401 2UL INJLast Calibration: 891025 09:04

Compound R.T. Scant Height Cone Units q

19) tDibutylchlorendate 31.63 1896 141184 .0788 UG/hL 100


Vi44

Filt >JB134

7200001

688060

400 eee 12.00OC.7dBgl8,nB7BBPl,l. if

i6.ee , seee .

4 ' e ' i2 16 ' z'e ' s!4 ' s!e ' s:e ' 36

Uata Hile: >JU1'?4::U4Name:

Uuant Uutput KileInstrument ID

.iti2jlUUU,lU

Id h i le: lU'^^lL: :USl i t l e : IKb/PSI/PLBLast Ualibration: BV1031 UB:12

Operator 1O: YY614UUuant Time: BV1U31 U8:29Injected at: UV1Q>1 Ul:41

1 ,45

\

UUftNl RtPORl Page

Uperator ID: YY614b Uuant kev: 7 Quant lime: 891UJ1 U8:2VUutput rile: "JBl$4::flLJ Injected at: UVlU^l Ul:41Uata File: >Jbl«?4::U4 Dilution ractor: l.UUUUUName: Instrument ID: Jfi"Hi so: UL7UU^1G,UG7UU21,L:U'JI!,10UO,1U .

ID r i la: 1U251C: :USTitle: IrB/PST/HUBLast Calibration:

Compound K. 1 . bcanf Height Cone Units q

1VJ #Uibutylchlorendate 2B . 0> 1682 136321 .Ubl7Utsi/nL 1UU

9 Compound uses tb I D

1146


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ha t r i x : (soil /wa ten) WATER

Sample wt/vol: 1000. Cg/mL) ML

'Level: Clow/med) LOW

H Moisture: not dec. dec.


GPC Cleanup: fYxN) N PH:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA232

Date Received: 09x x89

Date Extracted: 09/29/8?

Date Analyzed: 10/27x89



319-64-6———————alpha-BHC________319-65-7———————beta-BHC_________319-86-8 —————— delta-BHC_______58-89-9———————gamma-BHCCLindane ).76-44-8 ———————— Heptachlor_______309-00-2——————Aldrin__________1024-57-3——————Heptachlor epoxide959-98-8——————Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9—————Endosulfan II____72-54-8 ——————— 4,4'-ODD________1031-07-8—————Endosulfan sulfate.50-29-3————————4,4'-DOT_________72-43-5————————Methoxycnlor_____53494-70-5————Endrin ketone____5103-71-9 ————— alpha-Chlordane__5103-74-2 —————— gamma-Chlordane___8001-35-2 ————— Toxaphene_______12674-11-2————Aroclor-1016_____11104-28-2--———Aroclor-1221_____11141-16-5————Aroc lor-1232_____53469-21-9—————Aroc lor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1—————Aroc lor-1254_____11096-82-5—————Aroclor-1260_____

.050

.050

.050

.050

.050

.050

.050

.050

.100

.100

.100

.100

.100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

Q

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I PEST 1/87 Rev,

1147

CHROHAT09RQMFile >HA232 1.9 *»u. QC78B44G,Q8700447Ui C

geee

16 28 24 28 32

Data File: >HA232::U4 Quant Output File: ^Name! Instrument ID: HAMisc: QC70044G,QG70044,L: 62,1000,10

Id File: I044IP: : USTitle: IFB/PST/PCB 1 . 5SSP225 0/1 . 95SSP240 1Last Calibration: 891030 12:07


2UL I NJ

1148

\

QUANT REPORT Page 1

Operator ID: YY614B Quant Rev: 7 Quant Time: 891030 12:18Output File: AHA232::AQ Injected at: 891027 06:53Data File: >HA232::U4 Dilution Factor: 1.00000Name: Instrument ID: HAMiac: QC7Q044G,QG70Q44,L:G2,1000,10

ID File: I044IP::USTitle: IFB/PST/PC8 1.5SSP2250/1.95HSP2401 2UL INJLast Calibration: 891030 12:07

Compound R.T. Scan* Height Cone Units q


t Compound uses ESTD ~p

1 149

IDPESTICIDE QRGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code:

Gont ract:

Case No.:

Matr ix : ( so i l /wa te r ) SOIL

Sample wt /vo l : 3 0 . 0 <g/mL) G

Level: ( low/med) LOW

SAS No . : SDG No . :

Lab Sample ID: DC70076G

Lab Fi le ID: >HA503

Date Received: QCV27"'00

S M o i s t u r e : n o t dec. dec.

Extraction: ( SepF/Con t /Sonc ) SONC

GPC Cleanup: CY/N) Y pH:



Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/KG

319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-39-9—— — ——— gamma-BHCCLindane).76-44-8 — - — ——— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3-------Heptach lor epoxide,959-9S-8 ————— --Endosulfan I_____60-57-1 —— ————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8-————Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5- — ————— Methoxychlor_____53494-70-5—-——Endrin ketone____5103-71-9 —————— alpha-Chlordane___5103-74-2—--—-gamma-Chlordane___8001-35-2 ———— — Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232______53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5 ————— Aroc lor-1260_____

Q

IIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM 1 PEST 1 I 50 1/87 Rev,

CHROMBTOGRQHFile >Hfl313 1.0 anu.

4

,0679076 ,S IQ'

1600 SO.OO

48008*

44096*

360000;

320000-

160009-

12 16 £4

D a t a F i l e : > H A 5 1 3 : : U 4 . Quant O u t p u t F i l e : A

Name: I n s t r u m e n t ID: HAM i s c : CA2013G,Q,G70076,S:G3,24.92,40

Id File: IQ76IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95HSP2401 2UL INJLast Calibration; 391114 08:92

Operator ID: YY6148Ouant Time: 891114 17:02Injected at: 89.1114 16:18

1 l 51

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: AHA513::AQData File: >HAS 13::U4Name:Miac: CA2013G,QG70076,S:G3,24.92,40

ID File: I 076 IP::USTitle: IFB/PST/PCB 1.5SSP225Q/1.95SSP2401Last Calibration: 891114 08:92

Quant Time!Injected at

Di lut ion Factor:Inat rument ID:

2UL INJ

Page 1

891114 17:02891114 16;18

1.00000HA


3) *Beta-BHC19) tDibutylchlorendate


6.87 410 77248 .0249 UG/ML 10029.17 1748 267330 .146 UG/ML 100

Vi 52

CHROHPT09RPMFil. >KB

200000&

180080*

1600300-

1400000-

1208000;

100000*

60000*

60000*

400000-

L?l 1.0 **U. . Cfl£103B ,Cte70e76,Slt

400 | 808 r 12,00 , 1603 , 3000

k.Axow' A - , ,, , V . A.4 8 12 16 20 24 28 32

Data File: >KB191::U2 Quant Output File: *KB191::AQName: Inst rument ID:Misc : Cri210?9- .QG70076 ,S:G3 .24. 92 .40

Id File: 1 076 1C:: USTitle: IFB/PST/PCB 6' X 2 MM ID 3HSP-2100 2 UL INJLast Calibration: 891128 00:29


VI 53

QUANT REPORT

Operator ID:Output Fi lc:Data Fi le:Name :Misci

KT3582~KB191: : AQ>KB191: : U2

Quant Rev:

,QG70076,S:G3,24.92,4Q

7 Quan t Time:In jected at

Dilu t ion Factor:Instrument ID:

Page 1

891128 02:.45-891128 02:10

1.00000

ID File: I076IC::USTitle: IFB/PST/PCB 6' X 2 MM IDLast Calibration: 891128 00:29

Compound

7SSP-2100 2 UL INJ


1154

\

-STO-

PESTICIDE ORGAN ICS ANALYSIS DATA SHEET

Lab Name: ETCNJ

Lab Code: Case No.:

Matr ix: (so i1/water) SOIL

Sample wt/vol: SS-r6 3° Cg/mL) G*W>7

Lave 1 : ( low/med ) LOW

SMoisture: not dec. 14 dec.

Extraction: (SepF/Cont/Sonc) SONC

GPC Cleanup: CY/N) Y PH: 5

Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA1368GS

Lab File ID: >Htt5Q5




Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/KG

319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9--—-----gamma-BHCCLindane).76-44-8 ———————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3---—--Heptachlor epoxide.959-98-8 ——— ——— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE__________72-20-8----—---Endrin___________33213-65-9 ————— Endosulfan II____72-54-8——————--4,4'-ODD_________1031-07-8-—--—Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5— ————— -Methoxychlor_____53494-70-5—-——Endrin ketone_____5103-71-9 ————— alpha-Chlordene__5103-74-2——---gamma-Chlordane___8001-35-2 — ———— Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6-————Aroclor-1248_____11097-69-1 ————— Aroc lor-1254______11096-32-5 ————— Aroc lor-1260_____

9.3009V. 3009\3QQ

9\300

Q

IUI UIUtI1IUIUIIUIIUIUIUIIUIUIUIUIUIUtuIUIUtuIUIU

FORM I PEST 1/87 Rev.

55

CHROMBT06RPMFile >Hfi5B5 1.8 anu. CR136895 ,QS70076 ,S i£

3200808-

2608000-

240000*

1680000-

808808-

488888-

480 ' 800 1280 1688 2888

» R 8 ^ ft S R

« K «! 7 «S ^ ft\JUJL__ A , A JV / V yv

• i • i • F • i • i • i i • i • i • i • i • i • i • r • i ' 1 ' 1 '4 8 12 16 28 24 28 32

Data File: >HA505::U4 Quant Output File:Name: Instrument ID: HAMisc: CA1368GS,QG70076,S:G3,25.80,40

Id File: I076IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95*SP2401 2UL INJLast Calibration: 891114 08:52


Vl 56

QUANT REPORT

Quant Rev: ?Operator ID: YY6148Output File: ysHA505::AQData File: >HAS05: :U4Name :Misc: CA1368GS,QG70076,S:G3,25.8Q,4Q

ID File: I076IP::USTitle: IFB/PST/PCB 1.5SSP2250/1.95SSP24Q1Last Calibration: 891114 08=92


Di lu t ion Facto rInst rumen t . ID

2UL INJ

Page 1

391114 10:57891114 10;13

1. 00000HA


2)4)6)12).13)16)19)

#Gamma-BHC#Heptachlor#AldrinttD i e 1 d r i nttEndr in#4, 4 '-DOT#Dibutylch lorendate

5.7.8.16.18.22.29.

87236370777013

350432516

10001124 .13601746

19161715526516838524134681786188602297538

.0262

.0233

.0325

.0692

.0658

.0869.162


100100100100100100100

Compound uses ESTD

Vi57


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: (soil/wa tar) WATER


Level: Clow/med) LQU

\ Moisture: not dec. dec.

Extract ion: (SepF/Cont/Sonc) CQNT


Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA234

Date Received: Q9/ f/89



Dilut ion Factor: 1


319-64-6 —— —319-65-7 ————319-86-8 ————58-89-9 —— ——76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —— ——72-55-9 —————72-20-8 —— ——33213-65-9 ——72-54-8 ————1031-07-8- ——50-29-3 —————72-43-5 —— ——53494-70-5 ——5103-71-9 ———5103-74-2 - ——8001-35-2 —— -12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——

—— alpha-BHC—— beta-BHC—— delta-BHC— -gamma-BHC(Lindane)---Heptach lor- — Aldr in---Haptachlor epox ide---Endosu 1 f an I—— Dieldr in—— 4r4'-DDE- — Endr in---Endosul f an II—— 4r4'-DDD—— Endnaulfan aulfate—— 4,4'-DDT,---Methoxychlor_.ii. , „—— Endrin ketone—— alpha-Chlordan*---gamma-Ch lordane __,...„ ,---Toxaphene ,,,„,„„,_ — Arnelor-1016—— Aroc lor-1221__i,,__ , ,.,—— Aroclor-1232—— Aroclor-1242 _

12672-29-6 —————— Aroc Ior-124811097-69-1 ——11096-82-5 ——

—— Aroelnr-1254—— Aroclor-1260

.050

.050

.050

.050

.050

.100

.100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

1IUIUtu111IUIU1IU1IUIUtu1IUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST VI 58 1/87 Rev.

CHROMRT08RRHFile >Hfl234 1.8 wu.

4

CH1858GS,QS78044,L

16.00 2000

Data File: >HA234::U4 Quant Output File: AHA234::AQName: Ins trumen t ID: HAMisc: CAie58GS,QG70044,L:G2,1000,10

Id F i l e : I044IP::USTitle: IFB/PST/PCB 1.5KSP2250/1.95SSP2401 2UL INJLast Calibration: 891003 00:29


1159VI

QUANT REPORT

QuantOperator ID: YY6148Output File: AHA234::AQData File: >HA234::U4Name:Misc: CA1858GS,QG70044,L:G2,1000,10

ID File: I044IP::USTit le: IFB/PST/PCB 1.5SSP2250/1.95HSP24Q1Last Calibration: B91003 00:29



2UL INJ

Page 1

891027 09:05891027 08:18

1.00000HA


#Gamma-BHC#Heptach lor#A 1 d r i n#Die Idr in#Endr in*4,4'-DDT#Dibutylchlorendate

5.877.238.6516.6818.7522.6829.15

350432517999112313591747

79872584325107292116M2560160023M99457

.0254 UG/ML

.0220 UG/ML

.0221 UG/ML

.0636 UG/ML

.0272 UG/ML

.0712 UG/ML. 146 UG/ML

100100100100100100100

246

12!13:16:19:# Compound uses ESTD

Vi 60

IDPESTICIDE ORGANIC3 ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Caoi1/water) WATER


Level: (low/mod) LOUI

Cont rac t:

SAS No.:

S Mo isture : not dec. dec.

Extraction: (SepF/Cont/Sonc ) SEPF


SDG No.:


Lab File ID: >QB837

Date Received:

Date Extracted:


Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug^Kg) UG/L Q

11 319-64-6 ————319-65-7 ————T19-86-8 ————58*89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-6 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-SHC—— beta-BHC—— delta-SHC---oamma-BHCCLindane )---Heptach lor- — Aldr in---Heptachlor epoxide---Endoau 1 fan I---Die Idr in—— 4.4--DDE---Endr in---Endosu 1 f an I I—— 4.4'-DDD---Endosulfan aulfate—— 4T4l-DDT---Methoxychlor---Endrin katone---alpha- Chlordane---gamma-Ch lordana---Toxaphene_—— Aroclor-1016—— Aroclor-1221,,....,.——— Aroclor-1232—— Aroclor-1242---Aroclor-1248——— Aroclop-1254---Aroclnp-1260

.050

.050

.050

,050.050

.100

. 100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

1IUIUIU1I1IUIU1IU1IUIUIU1IUIUIUtuIUIUIUIUIUIUIUIU1


Vl 61

CHROnflTOSRftHFile >OB837 1.8 anu.

408

J l l *340000;

320000-

240000-

200000

100000-

CR1859GS ,0670021 ,TTit

8 12 16' ' '2*0 ' '24" ' 32 36

Data File: >QB877::U6 Quant Output Filet *QB837::AQName: Instrument ID:Miac: CA1859GS,QG70021,L:G2,1000,10

Id File: I021IP::USTitle: IFB/PST/PCB 1.5KSP2250/1.95SSP2401Last Calibration: 891025 09:04


2UL INJ

Vi 62

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^QB837::AQData File: >QB837::U6Name:Misc: CA1859GS,QG70021,L:G2,1000,1Q

ID File: I021IP::USTitle: IFB/PST/PGB 1.5SSP2250/1.95KSP24Q1Last Calibration: 891025 09:04


Di lut ion Factor'Inst rument ID:

2UL INJ

Page- 1

891025 09:11891025 03:57

1.00000


2)4)6)12)13)16)19)

#G«mm«-BHC#Heptachlor#Aldrin#Die Idr in#Endr in#4, 4 '-DOT#Dibuty Ich lorendate

6.8.9.18.20.24.31.

77328832475572

404497591

1097122614711901

12774499904879361516809401674409M148544

.0160

.0152

.0147

.0403

.0450

.0289

.0830


100100100100100

100


1 I 63


EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil/water) SOIL

Sample wt/vol: 25.0 30 ^^ Cg/mL) Gf,M&fLevel: C low/med) LOLJ

% Moisture: not dec. 14 dec.

Extraction: CSepF/Cont/Sonc) SONC

GPC Cleanup: <Y/N) Y pH: 5

Con t ract:

SAG No.: SDG No.: '

Lab Sample ID: CA1369GR

Lab File ID: >HA506




Dilut ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/KG

3-19-64-6——— ——— alpha-BHC_________319-65-7——— ——— beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9---—----gamma-BHCCLindane).76-44-8—----—-Heptachlor_______309-OQ-2-- ————— Aldrin___________1024-57-3----——Heptachlor epoxide.959-98-8- —————— Endosulfan I_____60-57-1 ———————— Dieldr in_________72-55-9---------4,4'-DDE__________72-20-8———— ——— Endr in____________33213-65-9 —— ——Endosulfan I I____72-54-8 ———————— 4,4'-DDD_________1031-07-8-------Endosulfan sulfate50-29-3--- ———— -4,4'-DOT__________72-4?-5---------Methoxychlor_____53494-70-5---—-Endrin ketone_____51Q3-71-9-------alpha-Chlordane___5I03-74-2-------gamma-Chlordane___8001-35-2 ————— -Toxaphene_________12674-11-2 — - —— Aroclor-1016______1110-4-28-2 ————— Aroc lor-1221_____11141-16-5———--Aroclor-1232______5?469-21-9------Hroclor-1242______12672-29-6———--Aroc1 or -1243______11097-69-1 —— —— Aroclor-1254______11096-32- = —————Aroc lor-1260______

».3009\3009A3QQ i

FORM I PEST

Q

IUIUIUIIIIUIUIIUItuIUIUIIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev

Vl64

CHROMflTOeRQHFile >HP

4806000;

4000000-

3600000;

3290990-

2909999-

£40000*

200000*

169009*

60090*

40000*]

586 1.9 amu. CR13686R .QS79076 ,S it

400 • 800 1200 1600 2000

lu 8 4)e r~-* R 3 * R 5 8Id ij- * «i (J

VJU A. A I A A A4 8 12 16 20 24 28 32 •

Data File: >HA506::U4 . Quant Output File:Name: Instrument ID: HAMisc: CA13696R,Q670076,S:03,25.81,40



VI 65

QUANT REPORT

ID YY6148^HA5Q6>HA506

AQU4

QuantOpera torOutput F i l eDa ta File: * nnv u o « • w**Name:Misc: CA1368GR,QG70076,S:G3,25.81,40



D i lut ion Facto r:Instrument ID:

2UL INJ

Page 1

891114 11:43891114 10;59

1.00000HA

Compound R.T. Scan# Height Cone Units

2)4)6)12)13)16)19)

ttGamma-BHC#Hept«ch lor#Aldrin#Die Idr in#Endr in#4, 4 '-DOTftDibutylchlorendate

5.7.8.16.18.22.29.

87236368757015

350432516999112313601747

238977194305191105293506107517232194341378

.0326

.0291

.0369

.0842

.0865.107.186


100100100100100100100

Compound uses ESTD

1'l66


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: C »o i1/wa t e r) WATER


Level: (low/med) LOU

% Moi&ture: not dec. dec.



Contract:

SAS No.: SDG No.:

Lab Sample ID: CA1B5BGR

Lab File ID: >HA235

Date Received: 09/.14/89



Dilut ion Factor: 1


319-64-6———————alpha-BHC________319-65-7———————beta-BHC_________319-86-8 —————— delta-BHC_______58-89-9———————gamma-BHC(Lindane).76-44-8———————Heptachlor_______309-00-2———————Aldrin___________1024-57-3—————Heptachlor epoxide959-98-B———————Endosulfan I_____60-57-1 — - ————— Die Idr in_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ——————— Endr in__________33213-65-9————Endosulfan II____72-54-8————————4,4'-ODD_________1031-07-8——————Endosulfan sulfate50-29-3————————4,4'-DOT_________72-43-5————————Methoxychlor_____53494-70-5—————Endrin k«ton«_____5103-71-9—————alpha-Chlordane__5103-74-2 —————— gamma-Ch lordane___8001-35-2 ————— Toxaphene_______12674-11-2—————Aroclor-1016_____11104-28-2—————Aroc lor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9 ————— Aroclor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroclor-1254_____11096-82-5 ————— Aroc lor-1260_____

050050050

.050

.050

.100

.100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

IUIUIUIIIIUIUIIUIIUIUIUIIUIUIUIUIUIUtuIUIUIUIUIU

FORM I PEST 67

CHROnOTOSRQM>HA235 1.8 AftU. ,(1678844,1. IC

1288 , 1688 . 2888

Data File: >HA235::U4 Quant Output File: ^Name: Instrument ID: HAMisc: CA1858GR,QG70044,L:92,1000,10

Id File: I044IP::USTitle: 1FB/PST/PCB 1.5XSP2250/1.95SSP2401 2UL INJLast Calibration: 891003 00:29


1 I 68

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: *HA235::AQData File: >HA235::U4Name:Misc: CA1858GR,QG70Q44,I_:G2,100 0,10

ID File: I044IP::USTit lei IFB/PST/PCB 1.5XSP2250/1.95SSP2401Last Calibration: 891003 00:29



2UL INJ

Page 1

891027 09:41891027 09:01

1.00000HA


2)4)6)12)13)16)19)

#Gamma-BHCtHeptachlor*Aldrin#Dieldr intEndr in#4, 4 '-DOT#Dibuty Ich lorendate

5.7.8.16.18.22.29.

87236970756815

3504325171000112313591747

743685568049536917132534558310M105409

.0237

.0209

.0214

.0634

.0269

.0691.155

UG/MtUG/MLUG/riLUG/MLUG/MLUG/MLUG/ML

100100100100100100100

Compound uses ESTD

Vi 69


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil/water) WATER

Sample uit/vol: 1000. Cg/mL) ML

Level: (iow/med) LQLJ

S Mo is ture: not dec. dec.

Extraction: (SepF/Cont/Sonc) SEPF


Cont rac t:

SAS No.: SDG No. :

Lab Sample ID: CA1859GR

Lab File ID: >QB838

Date Rece wed:

Date


Dilut ion Factor : 1


FORM I PEST

Q

319-64-6 -----319-65-7 — ——319-86-8 ————CO O Ci Q

76-44-8 —————309-00-2 -----1024-57-3 ----959-98-8 -----60-57-1 —————72-55-9- -----72-20-8 ----- -33213-65-9 — -72-54-8-- —— -1031-07-8 - ——50-29-3 ------72-43-5 ------53494-70-5 ——5103-71-9 — —5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ---11096-82-5 ——

—— aloha-BHC—— beta-BHC—— delta-BHC---aamma-BHCCLindane )---Heptach lor—— Aldr in---Heptachlor epoxide---Endoau 1 fan I---Die Idr in—— 4.4'-DDE---Endr in---Endosulfan II—— 4.4'-DDD---Endoaulfan sulfate—— 4.4--DDT---Methoxychlor---Endr in ketone---alpha-Ch lordane---qamma-Ch lordana---Toxaphene—— Aroc lor-1016—— Aroclor-1221—— Aroc lor-1232—— Aroclor-1242—— Aroc lor-1248— -Aroclor-1254—— Aroclor-1260

.050

.050

.050

.050

.050

. 100

.100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011 .

1IU111tu111IUIUtIU1IUIUIU1IUmIUtuIUIUIUIUIUIUIUtu1

1/87 Rev

VI 70

CHROnOTOfiftfltlFile >QB838 1.8 *>u.

400

Cfll8C9BR,0678021,1 iC

1200 1600 2000

' 4 ' 8 ' IS ' 16 ' 24 28

Data File: >QB838::U6 Quant Output File: AQB838::AQName: Instrument ID: -QAMiac: CA1899GR,QG70021,L:G2,10QQ,10 Qfi

id File: I021IP::USTit le: IFB/PST/PCB 1.5HSP2250/1.99SSP2401 2UL INJLast Calibration: 891029 09:04


1 i 71

QUANT REPORT

Quant Rev: 7Operator ID: YY6148Output File: ^QB838::AQData File: >QB838::U6Name:Misc: CA1859GR,QG7Q021,L:G2,1000,10

ID File: I021IP::USTitle: IFB PST/PCB 1.5SSP225Q/1.95SsSP2401Last Calibration: 891029 09:04



2UL INJ

Page- 1

891025 09:14891025 04:44

1.00000Off


2)4)6)12)13)16)19)

*Gamma-BHC#HeptachlortAldrin#Die Idr in#Endr in#4, 4 '-DOT*Dibu ty Ich lorendat e

68918202431

.82

.37

.95

.38

.55

.63

.77

407500595

1101123114761904

12697696000851201610899017675573M136768

.0159

.0146

.0142

.0428

.0431

.0292

.0764


100100100100100

100


Vl 72

ETC

CHAIN OF CUSTODY

n 73

\

ENVIRONMENTAL TESTING and CERTIFICATION ' Sftal No f) /,5 7 7 W ETC Job*CAl365

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date

Company PELA

F.ftilltyttit.. CITY DISPOSALC/0 HOLIDAY INN MADISON SMITH EAST

Artrtr««- I90X/EXIT 12 AND 18 EAST, MADISON,

RealnH 89/07/28 By l5 ^

Attn- DAN GREEN

Dh«rui.(414) 631 - 3150

U1I 53704

SAMPLE IDENTIFICATION

F^ility 1 4 Q ^ 1 1 I 1 1 1 1 CW^A*^FiciiMytftiM Codi

Sampl* Pnint- ftf-l^ lD Al 1 1 1 1 1 1 ISl^l^l°MZ.Soufc* Coot Voui Stmpi* Point ID Snrt Datt(Irorn D4IOH) |1*I1 tullily) <VV'MM(DO)

Source Codes-Wen • (W) Outtell . . . . . . (O) Bottom Sediment . . , (B) Surlece Impoundment ... (I)Soil (S) River/Stream ,(R) Oeneration Point (G) Treatment Facility . . . . , ,{T)

S»-|ft 1{Optional S«mBi» Poml Ovtcripnonti

iZI 1 / lo^tfi^l | i jSIStftrt Tint CIMteO Hour*

[1400 11. Clock) (COmpPXMI >

Leacnate Collection Sya. . . . . (C) Other . . . . . . . . . . . .IX)

SHUTTLE CONTENTSBOTTLE

No

2

1

1

1

1

Typ»

UOA

CON

MET

CON

TB

Size

4Q

J 1000

> 250

LJ 125

40

'

PrM»rv.

NONE

NONE

NONE

NONE

cc/ns

ANALYSIS

UOLATILES

PST/-PCB/BNA

METAL (SO ID

CY/T

TRIP BLANK

SAMPLERFIIL (VfN) Observations

Ss/y

/^tM» rf.*****'

^/•- X,,4l/i

LABObservations

l^~

l^ ——————

^^

l^^

CHAIN OF CUSTODY CHRONICLE

1.Shuttle Openec/py: (printSignature:

Date: Time:Intact:

2.

I have received these materials in good condition from the above person.Name: *,. — .. . . . ._ ._ . Signature:

Date: Time: /o; Remarks:

3.

I have received these materials in good condition from the above person.Name: -r- _ r-..-. . tN Signature:

Date: Time: Remarks:

Shuttle Sealed By: (print)Signature:

LAB USE ONLY

SHUTTLE *

ETC FIELD PARAMETER FORM (CC2)Form 0002

Simptt Min*g«m«nt

s,

V, -

Iftrtuftrt.atJpUtiDATE(Tf MM 00)

SAMPLING METHOD:

Sampler Material S

Tubing Material

Sample Composited Yflf

Well Elevation <ft/msl)Depth to Ground water (ftGroundwater Elevation (f

1st I I I I »T01

2nd I I I I WTO»

3rd I I I I«T«Ml

1th ' 1 1 1 <*TO)

t t"l 1 ro/ tMVtoTMV

Sample Appearance: _ &Weather Conditions: _ 5Othar

FTCJOB* LV' £>(#hA , » - * t il l^iTn^i i i i i i tSarnpi* Po|nt kJi i*-3 i-uui i i i i i i

Sourc* Coat tempM Point 1.0.

FIELD PROCEDURES

III 1,51* 1 1 1 1 1 1 | 1 1START PUKE ELAPSED HW WATCR VOL. IN CASINO VOLUME PUMEDI2«00 Hr CiocH) (Oiilonii (Qtltonti

A-Subrrwrclbl* Pump 0-OtpQ«r/Bottl» .- _ __B-ISCO E-Baltor X-Othf f " J (*f 7^ B^C-BI*dd«r Pump F-Scoop/Shov«( (SPtcifY OTHIRI

A-Ttflon C-PVCB-M.IH D-PlMtlc X-Othtr —————————— ,..,-, .^ —————————

•PKIFY OTHER)A-T«tlon C-Poly«thy(«n«B-Tygon D-Sllfcon X-Otlwi —————————— —g—-—- ————————— .

»•ProeMurMProportMm

FIELD MEASUREMENTS

1 1 1 1 1 1 uteiin.rthfft) II i 1 1\ 1 1 1 1 i „,„.,! $ampun«pth^nbn.weinm) 1 1 /l3"lDl

tmsh 1 1 1 1 1 1

15t i i i I krsr, i i i ill| | | I | wnfMi | | | I I I

Jnd I I I I I -«^ I I I I I !

arn I I I I I ra I M ill4 t h I I I I I « £ I I I 1 1 1

I I I I I ImTurtURy

FIELD COMMENTS

«M/M L'<^ Br**z* £6 F

FILTERING: Usa Chain of Custody (CC1) to Indicate which bottles wars filtered

Samplar: .TSffT" &M&£'^*/& Fmplnyar ^^Lfl

I certify that sampling procedures were in accordajjca-^/lth applicable EPA state and corporate protocols.

2^81 n^^-^^-^ 1 75.o«., i • *^k'*'£// y

Tlw Envbonmental Servlcec Company ORIGINAL


S«mpl« Mtnig«m«ntoe/w

lflfl^fl,Z,Zj

PTC JOB* \_VM \b-?^ yft^mpLDnint LT1 l^l^l*fl 1 1 1 1 1 "1

FIELD PROCEDURES

I i i5f i i i i i i 1 iPURU6 DATE START PURGI ELAPSED MRS WATER VOL. IN CASINO VOLUME PURGED(YV MM 00) {2400 Hi CI«Ch) (Qtlloni) (O«HDfW

SAMPLING METHOD:

... A-Submwslblt Pump D-Dlpp«r/Sotti« ._ , •*__ _ Sampler Type X *«co Mali* x-ottw ¥ Lf^rr TU Be

^ C-BI*dd«r Pump F-Scoop/Showl ' IWKIFY OTHERI

. . . . . . flj *-T«»lon C-PVCSampler Material *•? B-Mtt«i n.p>»*>- x.r»h«

Tubing Material | __ trJion

Sample Composited YOU

Well Elevation (ft/msl) 1 _Depth to Ground water (ft) | _Groundwater Elevation (ft msl) 1 _

i.tl 1 1 ! (§TO» iat 1 1Hi

2ndl III <"»> y«rt 1 1P*>

3rd! 1 1 «TD> 3rd I 1*

4th 1. 1 i »TW 4th 1 1

1 1 1 I re, |

(•PiCIPV OTHIR)

C-Polytthyl«n«0-Slllcon XOtfwi ————————— (iHtdpyoTMift ————————

PracMuwPraeeniwts

FIELD MEASUREMENTS1 | | 1 yy.nn.pth (ft) Mil

1 1 1 i fiampi. n^pth ( non.w«ll) (ftt 1 ! 11 51^M i l

1 ll 1 JSfi 1 1 M M II 1 1

1 1 1 ""*"" 1 1 ! 1 1 1 1 1' i < tiwc I I I I I I I - ,i

I I I UHAH" I M M M I I1 1 1 ittft'C '<« ' ' ' ' I ' 1 ii ItpOQ» exum ,_--,, peipiiii 1 1 i ipeam v^m

i i I rss i I I I I I I iI I M m .

••Mppv TVffip TufvWHy

FIELD COMMENTS

Waathur Conditions- 3{tAA* ( *<.»

OthflrI / / 1

FILTERING: Use Chain of Custody (CC1) to indicate which bottles were filtered

Sampler ^=^» £FAJ&*^A*2\ "N Pmnlnw.f nFlLA

I certify that sampling procedures were in acceptance with applicable ERA state and corporate protocols.

t.is*,SF( ^J^^^ 11 77<D.», f • 's-*/^,/,/'

v v r V7 * hteMv* •( EiKkmMMl T»««HM *M TuBniUiiii CmfThe InvlronnMntal S«rvtec* Company ORIGINAL

ENVIRONMENTAL TESTING anti CERTIFICATION Seal NO.

CHAIN OF CUSTODY FOflMfCCI) ORIGINAL>MjM89/07/29

ETCJob*CA1367

By:

Company: PELA Attn.: DAN GREEN

Facility/Site: £1TY DISPOSALC/QHQLTDAY INN MADISON SMITH EAST

Address: I90//EX1T 12 AND IB EAST, MADISON, Ul 53704


Phn^-C4l4) 631 - 3150

I 4_PFacility:

Sample Point: liMiiElIl

* .fiq-T>lOptitfnii S«mon Point DMcnoiionti

i J5ISoure* CM* Vouf S»moit Point ID SU'I 0*11 Start Tim*Itiom Miow) H*li iu*i»r) (VVfMM/00) (1400 *'. cloeM [cempo*il«i

Source Code*;Well (W) Oulfall (0) Bottom Sediment. .(8) Surface impoundment. ..(1} Lecchate Collection Sys.. .. .(C) Ottw .Son <S) ftiver/Slream (Rl Generation Pom i .. .(0) Treatment facility .. (T) LaKe /Oee tn . . . . . . . . . . . . . . ,|LJ Specify

.(Xt


NO

2

1

1

1

1

Type

UOfi

CONl

MET

CONl

TB

Size

60

J 1000

S 250

J 125

40

Present.

NONE

NONE

NONE

NONE

EC/MS

ANALYSIS

UOLATILES

PST/PCB/BNA

METAL(SOIL)

CY/T

TRIP BLflNK

SAMPLERFi>t rvmi Observations

sss<^/

LABObservations

^"

Si/

S^


2.

Shuttle Opened By; (priSignature: //^st

have received these materials in good condition from the above person.Name: ..,.._., .... . Signature:

Remarks:Date; g-6- Time:

3.

I have received these materials in good condition from the above personName: "T———__^ e-jix, - . .-is. Signature:



LAB USE ONLY Q

SHUTTLE*

ETC FIELD PARAMETER FORM (CC2) Form 0002Sample Managementoa/u

ETC JOB * C^VVM/")

AamnlA Pni«» IM 13 1^1 1 I 1 i l i i i • ISogrc* COM temp* Hunt 1.0.

FIELD PROCEDURES

|&^£fli2.i2] ill 1 i i5l l i i i ifYV If

SAMPLING ME

Sampler Type

Sampler Mater

Tubing Materia

Sample Compc

Well ElevationDepth to GrourGroundwater-E

1st

2ndIM

3rd•n

4th*»

I I IftMiite

Sample AppeaWeather CondiOther

, i , l1 DATE START PUPKtE ELAPSED MM WATER VOL. IN CASINO VOLUME MWMDMOD) U400 M. Ctoe*) |0«IIOA«> lOaiion*)

THOD:

X A-9ubm*rslblt Pump D-OlpMriBottl* -_ . ,_ _M8CO E-Bailw X-O1h*r ^^H TL/Sfc

p^

——— C-Biiddar Pump F-Scoop/Shown (weciFvoTMtmti A-Ttdon C-PVC

J A-Tallon C-Polyathyltnt

Sited YJB

OTMIft

OTMtm

»reeMiK«PTooon.oM

FIELD MEASUREMENTS

(fi/m«l) 1 1 1 | \ „„.! Wflll O^pth (ft) | 11 1 1 1 1 1 1dwat«r(ft) 1 I 1 1 1 _ _ | Sample Depth (non-wellHft) | ,_

lavation (ft msl) 1 1 1 1 1 I I

(STDt 1 1 mwofli 1 |— l o t L . ' •!«•«•- 1 1

*TO) 2M | | -ft | |

«"» 3 rd 1 1 M? III*™) 4th 1 1 i1? 1 1

r« | | | | | |,m,T«np TwWdtty

FIELD COMMENTS

tion«- >fuAf\u , L{5.WV "ft<*«t-e f uZi A"I

1 1 1/l lol

1 1 1eeve: IMPBI

i i iMM MtM

I 1 1

1 1 1••M WHM

FILTERING:

Sampler 7l

Use Chain of Custody (CC1) to Indicate which bottles were filtered

?#>& etx-£*sz> Em0.rtu.r P£Lf(I certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

(0*i*> f /A•*¥-* (J f j ' ^--^_TlM InvironmanUI S«rvtcM Company ORIGINAL

\

^ ^B. PNVIPnuUPNTAI TFSTIHG *na CERTIFICATION Coal Wn

CHAIN OF CUSTODY FORM (CC1)

Onmppny PEL.A

F.riiityKit.1. C ITY DISPOSAL

ORIGINAL Date Seal

PpTJi77 ETCJ0b»Cfll?68

Bd 89x07/28 By « ^i "" — "

Attn. DAN GREEN

Dhnn..<4!4) 631 - 3150C/0 HOLIDAY INN MADISON SMITH EAST

Aririmv I90//EXIT 12 AND 18 EAST, MADISON, Ull 53704


Exility 1 4 »M 1 1 1 I 1 1FlCility'SiM CMi

RamplAPninf l£|-blD|Zj 1 1 1 1 1

(0

lAlT Ot*? IZ. 1^-Soo'« CM* Tout Stmei* Pomi ID Slirl Otl*Itrom MIOVI (l«tl lutt.ly) IVYlMM/DOl

Sourc* Cod«i:Wall |W) Outfall . . . (O) Bottom Sadlmtnt . . . .(B) 3url«i Impoundment . (I) LtacSoil IS) Rivvr'Straam . .(R) Gen arat ion Point . . . (0) Traaimant Facility . . . . . .(T) Ltha

Blionti Mmpit Po-nt Dt»efiDi'on*l

1 Siart Tim* HMMd Hour*U400 nr cwcm icomooiiiM

Mt«Coltaeilon5yt.....(C) OttMr . . . . . . . . . . .. . w

SHUTTLE CONTENTS•OTTLE

No

2

1

1

1

Typ.

UOft

CON!

nET

CON

st»40

J 1000

> 250

J 125

-

PraMrv.

NONE

NONE

NONE

NONE

ANALYSIS

UOUftTILES

PST/PCB/BNft

METAL (SO ID

CYXT

SAMPLERFill. (Y/N) Ob«»rv«tions

./

/

/

s

LABObMrvatlqfu

I/J/-/y

^CHAIN OF CUSTODY CHRONICLE

2.

Shuttle Opene,Signature:

have received these materials in good condition from the above person.Name: /?/ j , _ . / .__, Signature:

Date: Time: Remarks: jitj

have received these materials in good condition from the above person.

3.Date: Time: Remarks: 30

Shuttle Sealed By: (print) -r-Signature:

LAB USE ONLY Quned By:'SHUTTLE* ^V

FIELD PARAMETER FORM (CC2)Form 0002

Sample ManagementOB/S8

lart^.itl(YYMMDO)

SAMPLING METHOD:

>/ jSampler Type £ l

Sampler Material O E

Tubing Material E

Sample Composited Y/4

Well Elevation (ft/msl)Depth to Ground water (ftGroundwater Elevation (ft

i i i J-_^.1.t I I ffTD)M

Snrt I «TD>M

3rd I »T<»

4th I »TO»

FIELD

|

FTCJOB* Csftl 3(/%

Sample Point IdJ LS'l'DlSeurc* Coo*

PROCEDURES

iSl I I I I ISTART PUAOE ILARSED MRS WATIR VOL. IN CASINO(2*00 HI CWck) (Gallon*)

2.1 i i t i i i 1tampu Roint i.O

( , , ! , !VOLUME ntNOEO

(O*IWfl«l

-Submertlble Pump D-Dipper/Bottie _ , _^ _^J-1SCO E.Ballaf » th« Pu< U- TO»^>Bladder Pump F-Scoopf\-Teflon C-PVC»-Metai D-Piattick-Teflon C-PotyetrHygon 0-Slllcon

I

Shovel

K.<"Hh „„ , „ „, „,

•>"•"•

marv OTHER)

ISPIOPY OTMiRI

0PICIFV OTHIW

^oew»WPropeftieM

FIELD M1 I I I1 1 1 1

mal) 1 I 1

i,, MM

M l4 t h I I I

I I I I CO | | ISametaTeme

Sample Appearance:

TwMdinr

EASUREMENTS

. _ I Well Depth (ft)I i

J — I Sample Depth (non-well) (ft)

M«»rpwtnuU4i

I 1tfWOfll 1 1•t »'C 1 ———— jj- ——————— I 1—

unweni

J*™

1 1 11 / 15-16 1

1 1 1 1

1 1 1 1

M I I I*•*• wMtt

1 1 I 1

FIELD COMMENTS

Wnath«r Conditions: <,.««- L£*U4- &**ei«- • ££* £

Other

FILTERING: Usa Chain of Custody (CC1) to indlcata which bottlaa wara

Sampler TePP fifX,&<W*A£&(Punt)

I certify that sampling procedures were in accordap

Employer TOn\

flltarad

AOvith applicable ERA state and corporate protocols.

1MIM • <SignBI««l// // jS'l ' ———n I f s J -f I

Th* Environmental f*nrieM Company ORIGINAL

1 ^^^^i e^^^Bt ENVIRONMENTAL TESTING »nd CERTIFICATION ' Seal

CHAIN OF CUSTODY FORM (CC1) OR.QINAL Date

Company:

Facility/Site:

Address:

PELA

CITY DISPOSAL

I90//EX1T 12 ANDMAD 1 SON DM1 Til CftOT

18 EAST, MADISON,

No. &!(?£.(?{£ ETC Job «CA1?69

« i . 8V/07/2B _ KCS«al«d By:

DAN GREENAttrv:

(414) 631 - 3150PhnnA-

UI 53704


Facility:

Sample Poin

Source CoderWen (W) CSod -.(Si F

iVit: &|-ljSou'» Cow\1iam ottowi

)utlaii, . . . . .liver/Si ream

5| 1 1 1 1 1FiciMy'Sit* Coat

Si-Dks i i iYOU' S*"iplt Poin

lit It lUilityl

.(Ot Bottom Sediment(R) Generation Point

1 I 1 LoafXT" "|i"(4ci\ Lcf->*rtQ ^} 1

i i i 1 \B\^\^\Zit ID Sll'l Q«lt

IVVfMMrDDl

. . . . (B) Surface impoundment ,,,.(!)

. . (0) Treatment Facility . . . . . (Tl

42[iOBtj7'lsy^7^$e'iBj'oni; l2>|

Stvl Timt El«MM Hour*II«00 h>. GIOCH) (compotittl

LeacnaieCollecilonSyr....(C) Other . . . . . . . . . . . . . . (X)L<k.jnrun fit *n«e!fv


No

2

1

1 .

1

1

1

TyptVOA

TB

CONL

METS

CYAC

CONL

Sizt

40

40

1000

250

125

125

Present.

NONE

GC/MS

NONE

NONE

NaQH

NONE

ANALYSIS

UOLATILES

TRIP BLANK

PSTXPCB/BNA

METAL (SOIL)

CY/T

CY/T

SAMPLER•lit (YfN) Observations

^

v/

^

•

»/

S

LASObservations

L"x'

^~-

^ ___

is~ •

s #*t!<L^ ^/xr/3/jf'fe^A?^

/

CHAIN OF CUSTODY CHRONICLEShuttle Opened By: (print)Signature:

Date:

Seal ft:Time:Intact:

2.

have received these materials in good condition from the above person.Name: -r" __ ^-.. - . -^ Signature:


3.

I have received these materials in good condition from the above person.Name: Signature:

1 I 32


Shuttle

Signature S«al#:

Time:

Intact:

LAB USE ONLY

SHUTTLE* _ TEMP. -C .SEAL* z i>flk/

FIELD PARAMETi

\&\i ICî^ iii2-lMMWCDATE(VYMMOW

SAMPLING METHOD:

Sampler Type X

Sampler Material O

Tubing Material

Sample Composited Y/

Well Elevation1ft/msl)Depth to Ground water (fGroundwater Elevation (

1st | (STW

5nri 1 «m

3rd ' | OTTDJPh

4th 1 CTOJ*

I I Itamp** T«mp

Sample Appearance: _ J

Othar

/I fllî/^GU TESTING tna CERTIFICATION ETP, JOB # ( rtl-'\&J

so cr\oui /ôoi Sample Point I^J 1^|Q£• n 1 \jniWl \\*1*£f SourctCOM

FIELD PROCEDURES

1 III 1 1 1^1 1 1 I I 1 1START njMQE ILAnED HRS WATER VOL. IN CASINO11400 Hr ClOCk) (Q«lk>ni|

A-Subm«r»lbl« Pump D-Olpp«r/Botit« rtj ., _B-ISCO E-Ballar X-Ot^t' rbU "" T

31 1 1 1 1 1 1S*mB)« Poini 1.0.

1 1 1 1 1VOLUMK IHJMCD

tx?»^-C-Bladdtf Pump P-Scoop/Shovil ISPICIFY OTHENI

A-T«flon C-PVCDMVIVI uriHiic (*l«iCIFr OTHW)

A-T«flon C-Poly*thy(«ntB-Tygon 0-SMicon X-Othtf —————————— ————————————————

*

•OFYOTHtn

KocMuwrrepoRiom

FIELD MEASUREMENTS

1 1 1 1 i , , „ „ ! w*nn«pth(ft)t) 1 1 1 1 1 .„.,_) Ramplfl Depth (non.w«ll) (ft)

tmah 1 1 1 1 1 |

i i 1 wntam I |I3t I I i .. M-r I

I I I ""*« I tJnrt I I I .tMT I I

. . II | iMiriem I I.- rri I I I ..«.« _ ...... L. — I

4 t h i l l r r , i i> I I I I I Inn

TufWdny

FIELD COMMENTS

itfj-r.-w.-.j- ^^bcrve* fjLjMTN '• fa¥ P' '

1 1 1 1 11 1 /IStOl

1 1 1 1 11 1 1 1 1MlM MM)

1 I N I1 1 1 1 I

FILTERING: Use Chain of Custody (CC1) to Indicate which bottles wort filtered

Sampler 3~f&F GWC-CA^Lb emn.0».r P«4

I certify that sampling procedures-were in accordance with applicable ERA state and cc

2zt*r*<r ^>^\}*^~-~**<--tom / **«yp / f^^^

»rporate protocols.

133ORIGINAL

ENVIRONMENTAL TESTING «nd CERTIFICATION Seal No. erc Job «C*1370

CHAIN OF CUSTODY FORM (CC

PELAr.ftmpany:

* >,u «•* CITY DISPOSALParlNty/fiite: _ ._.......-., n~rii_

W 0mG:NALDateSeale(:. 89x07/28 D KCBy

... DAN GREENAttn.-

1 I,-1* U nUL 1 UH T 1 IHN IIHU 1 SUM 3111 1 n E.M3 II90//EXIT 12 AND 18 EAST, MADISON, UI

Address- ' '

(414) 631 - 3150

53704


Parillt • 4| °l 5I 1 1 1 ! 1 1Ficii'IylSilt CM*

Sflmplp pninl- £]-l l!il 5 l I I I !Sourc* Cod* You' S*mpt* Poini 10Ittorn M'owi |I«M luili(y)

Sou'Ct Cod«s:WtH <W) OutUII (Ot Bottom Sediment .(6)

lOplonii SimQi* Poini Dt*tnptiO"»)

Slut Dit» Slin Tim* Ilapietf HourslYViMM/OOl 11400 ft. GIOGHI (compoiii*)

Surface impoundment . .(i) L«cfi»t» Collection Sy*. , . . .(C) Other . . . . . . . WTf»tm>nl FiellKy (T> LffO^tl" III SP»fl"V


No

4

2

2

2

•

Type

YOACONL

METS

CONL

Size

40

1000

250

125

Prssenr,

NONE

NONE

NONE

NONE

ANALYSIS

YOLATILES

PST/PC8/BNA

METAL (SO ID

CY/T

SAMPLERnit. (Ym) Observations

<S

sss

LABObservations

L/

^

^

^


2.

Shuttle Opened By: (print)Signature:

I have received these materials in gooaVcondition from the above person.Signature:

Remarks:Date: 2*2. Time:

3.

I have received these materials in good condition from the above person.Name: Signature: 1 'I 84Date: Time: Remarks:

4.Shuttle Seated By

X*Signature: X

Date:

Seal ff:Time:Intact:

SHUTTLE • EMP 'C SEAL *__Tlme:.COND. _

TESTING mnH CERTIFICATION

FIELD PARAMETER FORM (CC2)ETC JOB #Sample Point L£J 1 1

Souret Coo« 9«mpw »oint 1,0.

FIELD PROCEDURES

DATE(VY MM DO)

SAMPLING METHOD:

START PUN!12400 Hi CMcfc)

ELAPSED HM WATIft VOL. IN CASINO VOLUMI PUMOEDlO«llont)

Sampler Type yCA-Submtrslblt Pump D-Dtpp«r/Bottl«B-ISCOC-BI«dd«r Pump

E-B«lltrF-Seoop/Showi X-Oth»r

CIPV OTHER

Sampler Material

Tubing Material

Sample Composited

.6

ed '

A-T«flonB-M«til

A-T«(lonB-Tygon

«tt

C-PVC

C-?oty«thyt»nt(SMOPV OTHER)

™™.

Well Elevation (ft/msl)Depth to Ground water (ft)Groundwater Elevation (ft msl)

FIELD MEASUREMENTS

I—I I 1 i I I Well Depth (ft)I I I I i I i Sample Depth (non-well) (ft)I I I I 1 I I

1 1 1 1 1

1st I

2nd I

3rd I

4th I

<m> 1st

WTD' 2nd

(STDt 3rd

»TW 4th

|CC)

.

•wfnpM Twnp

•t»*C

•I M'C

•ta-c

JMTUTiifWdlfy

Sample Appearance:_^£f_WeathOther

FIELD COMMENTS

FILTERING: Ua* Chain of Custody (CC1) to Indicate which botttot w«r« flltorad

l nnl)

certify that sampling procedures were ip^Cc rdance with applicable EPA state and corporate protocols.

Vl 35ORIGINAL

ENVIRONMENTAL TESTING *n0 CERTIFICATION Seat NO. Q l<"7 7 73 ETC Job * CA1371

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed _J!l Ll __ By: ^- £

Company:

Facility/Site:

Address:

PELAAttn.: DAN GREEN

CITY DISPOSALC-'-O HOLlDftV SniTH E*3T—— Pnone:

1414) 631 - 3150

190/xEXIT 12 AND 18 EAST, MADISON. UI 53704


Facility: P ?. lOplionil S»<r>0it Point D«»C'iptiont)

Sourcf CM*'0*l

Your Scmpi* Point 10{ It't ju»Iilyl

Sli'l Oilt(YY/MM/DOl

Sim Tim*(3400 hr. CWCMI

EI10M4 Houri(eompotn*)

Sourct Coda*:Wall .. (W) Oultall....... (O) Bottom Sadlmam . , , , (B) Surtict impouodmani.... (I) Laaetiata Collaclion Sy»..... (C) Oin«rSoil - . (Si Rlwar/Straam. . (HI Qanaration Point . . . . (0) Tftitmam Facility . . . . . . (T) LaKafOcaan . . . . . , . , . . , . . . . |L)

(X)

SHUnLE CONTENTSBOTTLE

No

2

1

2

2

1

TVP«tJOf

T6

EXT

EXT

MET

Sin

40

-40

1000

10UO

1000

PtMfnr.

NONE

GCXPIS

none

none

HN03

ANALYSIS

WOLATILES

TRIP BLANK

EXTRB/nS.

PST/PC8

HETALS

SAMPLERFlit (V(N) Observations

*/

*/

*/

-/

s

LABObMrvatlonsx^*

\s^,•///^


1.

2.

3.

4.

LAB

SHU*

Shuttle OpenedAy: (prinrf *v . . CLoff±-\Signature: ^^_^Ca— I have received these Tnatertals in good conditionName:

Date: Time:

I have received these materials in good conditionName:

Date: Time:

Shuttle Sealed By: (print) fl LfiiffAld / JllTSignature: ( {fa fa /Sfa^dAti^

JRPONIYQp.n^tR^ K .** t '^4*- Al-f/h U r -^Liffm P * \ i / TPMP T, /•

Date: p ,f* g£ Time: /T : j <•Seal #: o \ S ~l TI 3 Intact: — '

from the above person.Signature:

Remarks:

from the above person.Signature: 1 i A 6

Remarks:

j/-ry Date: /99//¥/09 Time: /- . — -'/-, Seal #: folk ~lhl 4 '"tact: &-(^

nif.. ^//^/O T,m.- 'X<rSEAL* P/'Z? /^Vr.ONn st^L&S^S


Sample Management06/88

ETC JOB #

Sample PointSource COM tampM Pwnr i.O.

. ,I// ,•

FIELD PROCEDURES

WRGI DATf(YY MM 001

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

STAftT FUBGI<3*» Hf Clock)

ILAPSIO HHS WATCfl VOL. IN CASINO((Ullont)

VQUIUf PUMOCDlQ«IMoM

A-Submerslble Pump CXDIpper/BottieB-ISCOC-BI«dder Pump

A-TeflonB-MtUI

A-TetlonB-Tygon

E-Ball«rF-Scoop/ShovelC-PVC

C-PolyetfiyleneD-SHlcon

X-Oth«r

X-Other

X-Othet

ISMCIFY ormm

itMOPv OTMIRi

PtocMurwProponieni

FIELD MEASUREMENTS

Depth to Ground water (ft)Groundwater Elevation (ft msl)

I |3|gig|^| sample Depth (non-well) (ft)111/

1st I

2nd I

4th I

-™. 1st

I ! i i I I

I I I |_|

Ml5 Mm/on*•1»'C

4th •t M'C

LJMM

LJMIH

LJ1 ' l ' t ' 1 <•«• 1 1 1 1 .1 I-IH

tempto Temp

FIELD COMMENTSSample Appearance:.

FILTERING: Us* Chain of Custody (CC1) to Indlcatt which bottles w«r» flltorpd

Sampler^ £/JtV7Z>*J LJA/C&V________ Employer 7&A__________

I certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.1 j 37

Th» Environmental Swteexi Comoanv

ENVIRONMENTAL TESTING and CERTIFICATION Seal No.

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed

ETC Job # (LA IA1 1

By:

Company: Attn.: _>.

Facility/Site: ~Ji»/in

Address: ——————

Phone:


Facility:

Sample Point:

i\t\f\ (Jfl(OBOon» SlffiDi* Point M*C'iBI>onil

Sovrc* Cod* Tour S«mpl* Poml 10<Mlt jultilyl

Slirt 0«t* Surt Tim*12*00 nt. cm*)

Sourc* Cod*t:W«H..|W) OulUil . . ..10) Bottom Stdimtnt ..|8) Surtictlmpoundmtnt... (I) LMChittCollKtlonSy».... .|C) Oth«f ..Soil (S) Rivtr/Slrtam. (R) Generation Poinl , ,,. |G) Tfutment FtciMty ...... (T) Llkt/OcMn .. . . . . . . . . . . . . . |L| Specify

IX)


No Type Size Prsserv. ANALYSISSAMPLER

Fill (V«) ObservationsLAB

Observations


1.

2.

3.

4.

Shuttle OpenetfyBy: (pr)/t) *KSignature: i ^W«—

I have received these materialsName:

Date:

I have received these materialsName:

Date:

Shuttle Sealed By: (print) A ,

Signature. ^&4fZf> ~p&

*W GdtOTJ Date: J&-"\-8-\Seal #: oo^-s«v * *^

in good condition from the above person.Signature:

Time: Remarks:

in good condition from the above person.Signature:

Time: Remarks:

ApbiJ A/A/flSEV Dat* M]ltl&'Wt&h Seal#: ffl%5^

Time:^ Intact:

11

) Time:Intact:

0"l MS"~s

38

/7:30«*-•

LAB USE ONLY Opened By:SHUTTLE* ________

Date: 4-/9-P1-e .SEAL*

__Time:.COND. _

ETC FIELD PARAMETER FORM (CC2) form 0002.Sample Management

oe/M

ETC JOB # PMtitilSample Point 1 1 t

l«mtn« tani I.D.

PROCEDURES

FUME DATE(W MM ODt

STAHT PUROIIMOO Mr CloeW

ELAPSED H«S WATER VQl IN CASINO VOLUMI PUNQED. (Oillont) (Qilkon*)

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

A-Subrrwslbl« Pump D-Dfppcr/BottltB-ISCOC-Biaddar PumpA-TefionB-Matal

E-BailarF-Scoop/Shovel

C-PVCD-PUstic

OPOIyathyltna

I$«CJFY OTHIW

x-othar

X-Olhei

(1F1CIFY OTHER)

(W»ECIFY OTMEB)

FIELD MEASUREMENTS

Depth to Ground water (ft)Ground water Elevation (ft msl) / I

Sample Depth (non-well) (ft)

1st 1st J LJ

«h. ff .

' ' 't l r e ,

wiWmtMarc

HTUSwnpta Twnp TwMdMy

Sample Appearance;Weather Conditions:Other-

//£>FIELD COMMENTS

f i i^^Î f ^*f f t tW"âa jiafifif - ' - '•tîf^"- ^ * JRFf/tfa* t^T f^rfffft_f^L&f* ••

7g 72) Pl/£ &!&#£• f/AMeX.) 2''£M3jL

FILTERING: Us* Chain of Custody (CC1) to Indicate which bottlas war* flltarad

Sampler: Employer:

I certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

1139Fnvlrnnm*nt»l S*rvlcH Company

ENVIRONMENTAL TESTING *nd CERTIFICATION

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed

Seal NO. 0/ 771/7 ETC job* Cft1372

89/1)6/01 „... • /»

PELA Attn.: DAN GREEN

Facility/Site: DISPOSALC/0 MOLlCJH'l' INN IIHD1SON SMITH EH5T—— Pnone:——19Qx/EXIT 12 AND 18 EAST, MADISON, UI 53704

(414) 631 - 3150


Facility: I f P f I I I I I I 1 LFleHMy/f .!• COM <OOKon«l MmDW Point Micnpitomi

Source CMC(Horn Mlo«l

Tour i IDiu»tily>

Sl«ft Oitt(VVJMM/DOl

Sun Tim*(2400 if. clock)

U4Tf IBMM Hou**icompowMt

Sourct CoMs:Wtll .. (VW Outfall....... (0) Bottom SMimtnt.... (B) Surtact Impoundment.... (I) LMCMIt Collection Sy«,... C) OtnwSoil .(S) Htvtr/Slwtm ,|fl) OfncratlonPoint ....(O) TrMttnvnlFacility ......ft)

• IX)


No Type Sin Pmorv, ANALYSISSAMPLER

Observation*LAB

ObMfvatlora

UOf 4Q NONE UOLATILES

TB 4Q CC/MS TRIP BLANK

EXT 1000 none EXTRBXMS

EXT 1000 none PST/PCB

MET loorj HN03 METALS

/•W

IffN


1.Shuttle OpenetfT&y: (print)Signature:

Date:Seal«: Oi

Time;Intact:

2.

I have received these materials In good condttton from the above person.Name: >>^^^t . • , Signature:

Date: Time: «»» Remarks:

3.

I have received these materials in good condition from the above person.Name: Signature: VI 90Date: Time: Remarks:

Shuttle Sealed By: (print)

Signature:

LAB USE ONLY OpenedSHUTTLE* /"T"?

FIELD PARAMETER FORM (CC2)* * OS/S6

Sample Point l&COl (SSourc* Cod*

Rt 1

FIELD PROCEDURESI

PUKIB DATE(YYMMDO)

START PUKE[2400 Hi CUM)

ELAPBED H(tt WATER VOL IN CASINO VOLUME PUHOEO

SAMPLING METHOD:I . . I j A-Subir

Sampler Type MMi B*tsco7 ' fT*r r-.iii.rif

A-Submartlbl* Pump D-Olppcr/Bottl*B-tSCOC-Bltddtr Pump

E-BaltorF-Scoop/Showl (MtCtFY OTHER)

Sampler Material

Tubing Material

$ A-T«(lonB-M«til

A-Ttflon< - B-Tygon

C-PVCD-PlMtlc

C-PolytthylcrwD-SHlcon

Sample CompositedPnxmiim^PfiMiM »««•

Well Elevation (ft/mat)Depth to Ground water (ft)Groundwater 'Elevation (ft msl)

1st

FIELD MEASUREMENTS -I i I I Well Depth (ft) I I I i I I

Sample Depth (non-well) (tt) I I I i I I*4*15

I I I I 1 I J

l 1 1* V° 1 H •"'** II 1 1 1 1 1 .I9B'(> 1

2ndLL2l£l_U *"» 2nd L_L

3rd Ljll£LiJ «T01 3rd LL

4th LJj?l£LzJ »™ 4th 1 I111

«t»*C I 1

<-o NTUTiwfeMHy

FIELD COMMENTS

Weather Conditions:_J£UA^Other- HP Of-

*ilehv

¥ • SFILTERING: Us* Chain of Custody <CC1)1o Indicate which bottles were flltentd"

Sampler: Employer.

certify that sampling procedures we** in accordance with applicable EPA state and corporate protocols.

•*f£ rt£Z£ JZ^. 1 1 9 1

The invtronmenUl tervioM Company ORIGINAL

\

ENVIRONMENTAL TESTING «rtfl CERTIFICATION Seal NO.

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date

ETC Job It

.By:

Company: Attn.:

Facility/Site: —.

Address: _


Facility: I I I

Sample Point: JUj-l ( ikt/J.ftl|

\4\A\S\ L3>i Stmoi* Pomi D*ie>ipi>onii

Sou'C* COMllFOm D*10«1

tov' Stmoi* Pomi ID11*11 ju»tilyi

D*t*IVVIMMIOOl

Start rm*(1400 hi C10CN)

So urea CootsWtll -IWt OSon IS)

. (0) Bottom SMtmant . ,|B) Surface I mpoundmant.. ,|1) Laacnat* Collection Sya.... (C) Olhar - •raam .|R) Qanaration Pomi . (Q) Treat mint Facility . . . . . .(T) Laka/Ocein . . . . . . . . . . . . . . .(L) Specify

.(XI


No Type Sizt Prt««nr. ANALYSISSAMPLER

Flit (Y/HJ Observation*Ui

Observations

j_j£

CHAIN OP CUSTODY CHRONICLE

2.

have received these materials in good condition from the above person.Name: /• / ^^ ___ 1 , _ _ ^.^*> Signature:

Remarks:+8 Time:

3.

I have received these materials in good condition from the above person.Name: Signature: 1 I 9 2Date: Time: Remarks:

LAB USE ONLY Opened By:SHUTTLE* _______


Stmpljl ManigcmtntOB/88

Sample Point ll*>| I I i&iU-lRif i^iftgl iSourci Coo* Stmei* Point 1.0

|5tGE DATE

ITT MM DD)

FIELD PROCEDURES

I . /Lgf U(3«00 Mr Clock)

ELAPSED HUS WATER VQL IN CASING(Qailoni)

l/i5tVOLUME PUMQED

(0»iionn

SAMPLING METHOD:

Sampler Type X/t

Sampler Material

Tubing Material

Sample Composited

A-Sul>m«rilbl« Pump D-Oipptr/Bottl«B-ISCO E-Bail«rC-Blidd*r Pump F-Scoop/Shov«l

C-PVC0-Plt8!tc

C-Polytthyltn«D-Silicon

(SPtcirv OTHim

X-Oth«r

X-Othtt

fflPICIPr OTHint

FIELD MEASUREMENTS


i Well Depth (ft)2 |5"I3 ICp I Sample Depth (non-well) (ft)i i i i

3l31SL«ni i M

1.1 (»TO| 1st •tas-cMM. BOM.

,„„•n

13-15-1<lh 51^ (8TO) 4th

(*C)

•I38*C

LJ•pff§> Mnel,

NTUSMiipltTtmp TiHbMtty

Sample Appearance:Weather Conditions:,Other.

RELD COMMENTS

TS rtp PA&MG-

FILTERING: Use Chain of Custody (CC1) to Indicate which bottles were 'filtered

Sampler: Employer:

certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

1 1 3 3The Environmental S«rvic«* Company

ENVIRONMENTAL TESTING *ntf CERTIFICATION Seal No.

OF CUSTODYFORM(CC1) ORIGINAL DateSealed

ETC Job #

By:

Attn.: DAN GREEN

Facility/Site:-.*^

Address:ISON SMITH gftSTEAST, MADISON, UI 53704

(414) 631 - 3190


Facility: I t P f I I I I I

Sample Point: / ftl I I I I

(Option*! S«mpl* Poin

t* COM voui Sample P«mi 10(itM |o»tity)

n 0*l« Sl«rt Tim*11*00 i»

Souret CoOw:«•)( .. (W) Outfall....... (0) Bottom S«dlm*nt.... (8) Surftct impoundment.... (I) L««ehil« Collection 3y»..... <C) Otntr ..Soil... (SI Alvtr/8ir«cfn..(R) a«n«f«t<on Polni .. . .(Q) Trcitmtnl Facility . . . . . .{T| LMt/OCMn . ... . ... ,. ,.(U Spvclty

.(X)


No

2

Type

TB

EXT

EXT

ME!

Stee

NONE

4

1000

100

lootr*-*

GC/I1S

non*

non«

HN03

tZf

ANALYSIS

yOLATlLES

TRIP BLANK

EXTRBxnS

PSTxPCB

hETALS

SAMPLERriH. (Y/N)

U

A/

/

iZ.

U

rV

Obtervatlont

J

CHAIN OF CUSTODY CHRONICLEShuttle Opened*y {prfSignature:

Date: Time:: n-

2.

\ have received these materials in good condition from the above personName:


3.

I have received these materials in good condition from the above person.Name: /f . ^^ . , , .. t**^s Signature:


1 I94

/"' — ^T~Shuttle Sealed By: (print)

Signature:

LAB USE ONLY Opened By:SHUTTLE *

ETC FIELD PARAMETER FORM (CC2) Form 0002Sampi* Marwgwiwnt

OB/SB

ere JOB*Sample Point

FIELD PROCEDURES

(WMMDO)

SAMPLING METHOD:

START PUMI12*00 Mr doom

IL*niD HM WATM VOL IN CASINOlOWtoni)

VOLUMI njMIDIO«llon«

Sam pier Type

Sampler Material

Tubing Material

Sample Composited

A*Subnwrsibl* Pump D-Dlppw/Bottl*B-ISCO E-B«HtfC-BI«dd*r Pump F-Scoop/ShovtlA-TeflonB-M«ui

C-PVCD-PlMttcC-Poly«tfiyl«n«D-Slllcon

X-Oth*r

X-Othtr

Well Elevation (ft/msl)Depth to Ground water (ft)Ground water Elevation (ft msl)

FIELD MEASUREMENTSWell Depth (ft) LSample Depth (non-well) (ft) L I I i

2ndL_iiUJiJ

3rd2nd

3rd

4thLJ3L2l3|iwi 4th I I

FIELD COMMENTSSample AppearancesWeather Conditions^Other

FILTERING: U«« Chain of Custody (CC1) to Indicate which bottlts were flltamd

Sampler: Employer

certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

———— 1 1 9 5(Mm TTThe Invfronmental tendcM Company ORIGINAL

ENVIRONMENTAL TESTING ina CERTIFICATION Seal NO. 4M0*

CHAIN OF CUSTODY FORM (CCf) ORIGINAL Date SealedETC Job *

__ By:

Company:

eacHity/Site:

Address:

Attn.: -JJ/Ln


Facility:

Sample Point: iH-l /(Optional simple Point Description*)

lourc* COMllrom 0«lo«t

Your S«mpw Point ID|l«rl fusllfy)

Q\1\A1&\&\ \ri\<*tf\4Star) Oat* * Si"»n ilmt'

(TYMMfDOl (3400 nr. clock)

SourcaCMM:Wall . .<WJ Outfall...... .(O> iottom Sadlmant... .(B) Surfaca Impoundment.. .(I) Laacwa Collection Sys.... .(C) Othef ..Soil ...IS) Rlw/Straim. .(Rt Q«n«ritlon Point ... .(G) Trwtnwnt Facility ..... .(T) Ukt/OCMft . . . . . . . . . . . . . . .(LJ Spaclty

• ixt


No Type Size PreMrv. ANALYSISSAMPLER

Pill (YM) ObMnratloniLAB

Obeenatlont

V


1.Shuttle Opened Jft: (priSignature:

Timt: on*-s-a Intact:

2.

I have received these materials in good condttlon from the above personName: 4V * Signature:*

Remarks:Date: 0? /*/&*

3.

I have received these materials in good condition from the above person.Name: Signature: 1 'I 9 6



Signature:

LAB USE ONLY Opened By:SHUTTLE » _

ETC FIELD PARAMETER FORM (CC2) Form 0002Scmpta Mirwgwntnt

os/ss

ETC JOB # _______

Sample Point UiJ LScwretCoM

i i

I DATE(YY MM 00)

SAMPLING METHOD:

START njno4400 Nr Clock}

FIELD PROCEDURES

KLAKIO HW WATER VOL. IN CASINOMtellon«

VOUIMf PUMED

Sampler Type [xT-l

Sampler Material IAJQ &M«UI

Tubing Material fr/C

A-SubmmlbHi PumpB-I8COC-BMwMtr Pump

D-OlpO«"Bottl«E-BalltrP-8eoop/Shov«lC-PVCD-PlMtlC

pPiOFYOTHM)

Sample Composited

Well Elevation (ft/msl)FIELD MEASUREMENTS

I Ifl5lfrl«lftl we.l Depth (ft)

Ground water Elevation (ft msl)

i.tL_J

3rd

4th

l&IPJ •ta*c

4th U8I2J •ta-c J I I I I I I |__1

I I I I I IN™

FIELD COMMENTS

. $3 -M.ZI * f ?.FILTERING: Use Chain of Custody (CC1) to Indicate which bottles were filtered

Sampler (UJ9y7&/V £/44D5£Y_____ Employer

certify that sampling procedures wjue in accordance with applicable EPA state and corporate protocols.

11 97The EnvironiTMntal tanHoee Company ORIGINAL

ENVIRONMENTAL TESTING tna CERTIFICATION Seal No. ere job ff CA1374

AIN OF CUSTODY FORM (CC1) ORIGINAL Date sealed _£L^15L_ By:

Company:

facility/Site:

Address:

Attn.: DAN GREEN

Phone: (414) 631 - 3190

I90/ 18 EAST, MADISON, UI 53704


Facility:

Sample Point:P*c ill Win* Coo*

&3HYour 5*mp(* Point ID

(1*11 juiiity)Start Oil*

(WfMMJDO)

(OBlKHutScmdvPoinl OMCription*)

j l/i2»i3ifel UStart Tim* Eiaewa HOW

ICOmpOOlM12400 i". eioek)Source Code*Well . .(W) OutWI...... .(0) BottomStdim«nt... .(B) SurfMtImpoundment... .(|| L««eh«l*Collection5y». .. .|C) Oth«Soil ... IS) fllvtr/Strwm.. |R) Contrition Point , . . . (Q) Treatment Feclllty . . . . . . (T) Like/Ocean . . . . . . . . . . . . . . . (U Speci


No Type Sin(JQt

TB

EXT

EXT

MET

4(

4G

10QC

1000

1000

NONE

CC/MS

non«

non«

HN03

ANALYSIS

UOLATILES

TRIP BLANK

EXTRB/MS

PSTXPC8

METALS

SAMPLERFHt(Y/N)

AJ

A/A/

A/A/

ObMrvatlont

L/tX

CHAIN OF CUSTODY CHRONICLEShuttle OpeSignature: &

D***:Seal*:

Tim<:

Intact:

2.

I have received the» materials in good condition from the above person.Name: -**.__. ^-vt ^ , . »^ Signature:

Date Remarks:

3.




SHUTTLE*

ETC FIELD PARAMETER FORM (CC2) Font) 0002iMot

QO/tt

ETC JOB #

Sample t LO Q 1 ISource CM* tamow Peon i.O.

FIELD PROCEDURESi2,U

WHO! DATE(YVMMOOl

STANT PUMOI(3400 Mr CtoCKI

iCUtntO HM WATER VOL IN CASINO

(OMWiw)

I I . I Z f l lVOLUME PUMIO

lOtlionii

SAMPLING METHOD:

Sampler Type fl/C,

Sampler Material

Tubing Material

Sample Composited

A-Subm«rtlbi« Pump D-CHptwr/Bottlfl

C>Bladd«r Pump F-Scoop/Shov«iC-PVC

C-Poly«ttiyl«n«

x-otrw

X-Othtr

(8WCIFV OTHIft)


(•TO)

FIELD MEASUREMENTS

I I I I i I J Well Depth (ft)Sample Depth (non-well) (ft) i l l

LJ

M«4th

I I \7£&\sss. Li i \1\$\f •ta*c

INTUTMMtty

Sample AppearanceL. 1^Weather Conditions:

FIELD COMMENTS

FILTERINQ: Use Chain of Cuttody (CC1) to Indicate which bottlat wara flltarad

________ Employer _iPnnn

certify that sampling procedures were in accordance with applicable EPA state and corporate protocols

ORIGINAL

ENVIRONMENTAL TESTING »nd CERTIFICATION ' Seal No. 4^-*W> ETC Job It

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Oate Sealed _AiJ£___ By: _

Company: _

Cacility/Site: a.

/W/nr Attn.:


Facility: I I I I \4\6 L/l

Sample Point: fej-llF»cil'ty/8it» CM* (Oplionii " 0««er>plioni)

Souret Coot(Iron MIOW)

YOUI S«mpl* Point ID{(•It (UXilyi

gffl^rfl&lfel I / 12 15 Ifel 1 15TSlin Dili

IVVJMhUDD)Sun Tim*

(9400 Xf. eioek)E<«P*M Heun

Sourct CodM:W»II..(W) Outfall... . . . - IO) Bottom Sadlmtnt... .(B) Surlict Impoundment... ,{l) L»cr>«<« Colltction Syl., ...(CJ Oth»r ..Soil . . (S) RlvtrfStrtam .(R) Gtncraiion Point .. , .(O) Tr«tm«m F«cility . . . . . .(T) Laki'Ocwn . . . . . . . . . . . . . , .(U Specify

.(X)


No Typt Slz* PrM«rv ANALYSISSAMPLER

Flit (Vfffl ObservationsLA1

Observation*

Mff&fol

CHAIN OF CUSTODY CHRONICLEShuttle Opened/By: (prlSignature:

Dale: Time:4. <4O Intact:

I have received these materials in good condition from the above personName: *,..._ . , ... ^, Signature:


1 have received these materials in good condition from the above person,Name: Signature: 1 2 C QDate: Time: Remarks:


Signature:

SHUTTLE »

ETC FIELD PARAMETER FORM (CC2) Sampl* Management08/S8

ETC JOB «Sample Point

Sowre* COM tan>DW tani 1.0.

FIELD PROCEDURES

FUMIOATE(YVMMODI

START PUHQE12400 Ht CloeM)

i +5lEUPSED HAS WATER VOL. IN CASING

i iVOLUME PURGED

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

A-Submerslbl* Pump D-Dlpp«r/Bottl«B-ISCO E-8*ll«fC-Bi«ddw Pump F-Scoop/ShovtiA-T«(lon 'B-M«UI

A-T«flon8-Tygon

C-PVCD-Pi tat IcC-Polytthyltn*D-Sliicon

X-Oth«r

X-Oth«r

x-Othti

ProcMurw roeon rant


FIELD MEASUREMENTS

I i I I

I I I I i 1 I

VgalJ Depth (ft)le Depth (non-well) (ft) I i I I

3rd

4th

1st

2nd

3rd

4th

•two

inMom

LJ

I I I I I IHTU

FIELD COMMENTSSample Appearance:Weather Conditions:Other:

t.FILTERING: U&» Chain of Custody (CC"l)1o IndlcaU which bottlts w«r« flltartd

Sampler: Employer:

I certify that sampling procedures were in accordance with applicable EPA state and corporate protocols.

The Environ. A«ntat S«r\kt«« ComfMny ORIGINAL

ENVIRONMENTAL TESTING «nd CERTIFICATION Seal NO. 0/*SV />T / £TC Job #

CHA/N OF CUSTODY FORM fCCt) ORIGINAL Date Sealed _J**W*±_ By: _

Company:

Facility/Site:

Address:

Attn.: DAN GREEN

Phone:(414) 631 - 3150

EAST, MADISON, UI 93704


fJL?Facility:

Sample Point: l!i}-LDttcriptieow

i LIvour SWIIB<* Pdini 10

(ltd justify)3TV1 Tim*

<a«oo i». CKKIHWMO noun

(tram Mttoit (ltd justify) (VViMMfOD)

Source Code*:Well . ,(W) Outfett . . . . . .(O) Bottom Sediment.., .<B) Surface impoundment... .(I) L«*er>«i« Collection SyrSoil . (S) Rlve«Stre«m .(B) Oenerttion P«nt ... ,{Q) Treatment Fteillly . . . . . , [T ) Lahe^cean . . . . . . . . .(U Specify

SHUTTLE CONTENTS•onLE

UOLAT1LES

TRIP BLANK

ANALYSIS SAMPLERFlit (Y(N)

/UObservations

sy

1.

AIN OF CUSTODY CHRONICLEShuttle OpenedSignature:

Dat9:

Seal»:Tlma:

Intact:

2.

I nave received these materials in good condition from the above person.Name:

Date: "2, * 3a0£*i Remarks:

3.

I have received these materials In good condition from the above person.Name: Signature: 1202Date: Time: Remarks:

4.Shuttle Sealed By: (print)

Signature:

iABiISFniaiv

SHUTTLE*

ETC FIELD PARAMETER FORM (CC2)form 0009

TwntOB/SB

ETCJOB#Sample Point i i I

Sou ic» COM fttmpM Point 1,0.

FIELD PROCEDURES

PUMKOATI(YYHMOO)

SAMPLING METHOD:

9TAHT KtMU(2«M Hr Ctoem WATIH VOL IN CASINO VOLUMC MJMHO

Sampler Type w A-Subnwrilbl* Pump D-Oipp«r/Bottl«

Sampler Material

Tubing Material

Sample Composited I jpN I

B-I8COC-Btatttr PumpA-TtdonB-M«UI

E-BiitoP-Scoop/Shov«lC-PVC0-PlMtic

C-Poty«thyl«n«0-Slllcon

X-Otlwr

x-othtr

X-OtlW

(SPCCIFY OTMlHi

(MfCtFY OTHIHl

FIELD MEASUREMENTSWell Elevation (ft/mst) I I I I i I I Well Depth (tt) I_LJ!Depth to Ground water (ft) I 1 I 2.L5"J2.£. | sample Depth (non-well) (ft) 1 1 1 !Groundwater Elevation (ft msl) LJ__LJ__L_LJ

1st

2nd 4L2 2nd I 1 1 b'l fcl / 13rd I l^t^l II •"» 3rd I I M5l3lgl ffSR

m|| ••••L flMkM.

ft .31 mot 4th S1fel3l I Ll/IOiZJ*'c.

. MM.LJ

I I I I I INTU

FIELD COMMENTS

Weather nnnditioMfQth«r

FILTERING: UM Chain of Custody (CC1) to Indicate which bottlts wtra flltartd

Sampler(fmnt

Employer

certify that sampling procedures were fn accordance with applicable EPA state and corporate protocols

The Invlronmental Servlcee CompMiy ORIGINAL

\

ENVIRONMENTAL TESTING antf CERTIFICATION ' Seal NO. V^ - wO ETC Job # LJA/S^

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Date Sealed _£iiJ5___ By:.

Company:

Facility/Site:

Address:

itimr Attn.:^


Facility: I i i i i i i \4\a i^lFMlllly'SiU Cod* (Option* i S«moi« Point D*tcripltonn

Sample Point: MSouretCoo*Ifrom b«tow)

Your SwnpM *oini 10(Mfi tut i»yl

Start Oltf{VVMMrOOl

Slvt Tim*(2*00 iw, clock)

IMM4C Hour*[COfflpCWl*)

Sourct Codm:Wall . .(W) Outfall...... .(O) Bottom Sadlmant... .(8) Surtacalmpoundmani... .(I) Laacnatt Collection Syt.... .(C) Otnar ..Soil . ,(S| Rtvar/Straam. (H) OanarationPotnt ... .(Q) Traatmant Facltlty . . . . . .(T) Laka/Ocaan . . . . . . . . . . . . . . .(L) Spacify


No Typt Size Pratenr. ANALYSISSAMPLER

Flit (Yft<> ObservationsLAB

Observations

Affi

AST)


1.Shuttle OpenechBy: (priSignature:

Date: Time:Intact:

2.

l have received these materials in good condition from the above person.Name: yitv. _ , . . . _^_x Signature:


3.

I have received these materials in good condition from the above person.Name: Signature: 1204Date: Time: Remarks:

Shuttle Sealed By: (print)Signature: Seal*:

Time:Intact:

SHUTTLE «t .Time: I&**

TPMP «c 4* SEAL* _^ CONO. _t

ETC FIELD PARAMETER FORM (CC2) Form 0002Sample Mtn«gtm«m

08/W

PTC JOB* £&£'&'

Ramnle Point lU^ lllfrlW|5|£?iAiRi t i1 rSourc* COM Stmpu tani 1.0.

FIELD PROCEDURES

Iffif lAf 2-ifiJ l/r^3fll 1 i3l 1 i i/Lî/ l i iPltoGEOATE|YY MM DO)

SAMPLING METHOD:

Sampler Type fl£-

Sampler Material AfC.

Tubing Material Al£^

Sample Composited J

Well Elevation (ft/msl)Depth to Ground water iGroundwater Elevation

1st feL&!" *™

,„„ fcl<?4l <T,3rd J^, „„

ii siSTAHT njME ELAPSED MBS WATCH VOL. IN CASING VOLUME PURGED(3400 Mr dock) lOtllontj (Gallon*!

A-Subnwraibl« Pump 0-Olpptf/Bottt« . „._B-ISCO £.B«ll«r y.nth.r faf [\ Uti 1~fae,T*>C-BI«M«r Pump F-Scoop/Shov«t (SPfCtPY oTHlft)

A-Ttflon C-PVCBMW uriHiic '»FICIFV OTMEllliA-T«flon C-Poly«thyltneB-Tygon D-SIMcon XOIhw ——————————— gRoPvoi ————————————HIM)

P'OcMyWPfOpWtWW

FIELD MEASUREMENTS

1 , 111 .,.,..„ w^nn*pth(ft) | 1 31 V 1.51 31'*) [„.. 1 ^l^t -l«*l Q?mpl« n«pth (n^n.Âlh (ft) | ___ |_

ftmal) L__L.!,. , 1

» « . 1 1 / \<T\U\ 1 1 **om 1 1 1 1 12nd 1 1 / '^ |llffl i ' ••««•': ' I I I I

• .,* I 1 1*1515-161 -a 1 1 I I T«h kl>!3l<.To» 4th I I /I51&I..3I SR 1 III

1 lllOJ-m-•wfHpM TWnp

Sample App«aranc«- C

« 1 1 1 1 1 l««TwbMHy

FIELD COMMENTSie&^ AJO Abae

1 1 1 1

1 I I I

1 1 1 .1

1 M lM WHt

1 I I I

Waathar Conditions- fit ***.&-** 4k Art*fZ.* •*!*/- *"a*P

Oth»r £«<// -Qtfytfli • • »

t-—-/ -^ yMÂJj^^J

3V. 53" 2. - 4» .Z?" / J(gi9 LtblPT — !.$(£*' Y V •• .o^ £V£V«M«$ iFILTERING: Use Chain of Custody (CC1) to Indicate which bottlts wsrs ffltarsd

Samplnr {J-4+fl*t<. L^.*.*£$&4 Pmnlnw«r r^f^/T(Pfintl I /

I certify that sampling procedures' were in accordance with applicable EPA state and corporate protocols.

Tlw CnvfrofuiMntai S*rvlc** Company

ENVIRONMENTAL TESTING anO CERTIFICATION

CHAIN OF CUSTODY FORM (CC1) ORIGINALSeal No. Cft1376

.By: . (J

Company: PELA .„Ann : DflN GREEN

CITY DISPOSAL (414) 631 - 3150

Add re

- — L/u MULIUHT nsN iiHUisun— sni m K.HSI — • • -— • —— - —I9U//EXIT 12 AND 18 EAST. MADISON. Ul 53704««• ' *


Facility: f P ? 1 1 1 1 1 1 1FtciinyfSii* Cog* lOoiionti Sf"on Pomi Oncnpiionti

•II KSiMMiAiCt i i 1 Ififllîfllî^l IrfifliSl 1 l5i<TSou'ct Cod* You' 3*mpi* Po.ni'iD Sl'i'i Oil* ' Sun Tint* ' E<*nM Hou'tirromMIOwi <l*lt lullity) iTWMM/DD) I3400"r GlOChi (<compOt<ll>

Sourct CodtrW»il (Wl OutUM . .{0) Bottom Stdimcnt . .(B) Surtic* ImpourKjmant [It Ltachai* Collection Syi, . . [O Otntr ... . (XI


NO

2

1

2

2

1

|1

-*_i

)

1

1.

2.

3.

4.

Typ«

U0«

TB

EXT

EXT

flET

SIM

40

40

1C1UC

1000

10QC

3°o;ity

'/zr"»-2.r.,f

Prsstrv.

NONE

GCXMS

none

none

HN03

A&^

n*oeJ^S>/t*A«

*iio

ANALYSIS

UOLAT I LES

TRIP BLANK

EXTRB/nS

PST/PC9

METALS

dy/îctf-Pwi ^w^r/v^r-tvW.-t^

TDc-

SAMPLERFIH. (Y(N)

/o/Â>fjifljfjt1//X

Observations

y, 2,-nl

y

^xy—^-^

X-"

^

LABObservations

^X

^

C^

^

L/L/

L/

Lf/i-^

CHAIN OF CUSTODY CHRONICLEShuttle Openedyfiy: ipnSignature: JJ^^&.

^ 9/?*/ (S^ffW/ Date: 8-^-8H Time: \(p-.*SO+* __ Seal #: o v*r"l"i 4-"1 Intact: ^'

1 have received these materials in good condition from the above person. A /— ^— f !

Name: -j. ^ £*Mtffl Siflnature: AM )<^-^^

Date: 2*3- SCP 2^ Time: (2«C<Z^ emarks : //£îf

1 have received these materials in good condition from the above person.Name: Signature: 1 ' / 1 <

Date: Time: RemarKs:

Shuttle Sealed By: (print) -TfcTP e*i4j /U\NSignature: <^ / ;

LAB USE ONLY Qg«l

SHUTTLE » /-3y

r -*-w^>^

Date: t?-ie?e<7 Time: /yW~*:Qjl5m4fi Intact: «^_

x*f / Zft^/jisA*. .*&*/ n.to. y/2+jfc*, T!m«- //J ^T

^ TEMP -c /P*2 SEAL « O> C"_=) 3V/P cONn /^srtJ&ZS

\

ETC FIELD PARAMETER FORM (CC2) Form 0002Sampl* M*mg*m«nt

08/86

ETC JOB #

Sample Point lid I f ftSourc* COM S«mpW Point i.D

FIELD PROCEDURES

PlMCE DATE|VV MM DDI

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

(1400 Nf CIOMIELAPSED HAS WATER VOL. IK CASING

(QiHontlVOLUME PUftQCD

|Q«llon*l

A-Sut>nwr»lbl* Pump D-Dlpp«f/BottleB-ISCOC-Blidd«r PumpA-TtflonB-Mttal

A-T«llonB-Tygon

E-B«ll«rF-Scoop/Shov«l

C-PVC0-PlasticC-Poiy«thyl«naD-Slllcon

X-Oth«r

X-Oth«f

X-Olhai

LU€.I(SPtCIFV OTMlfll

ffKCIFYOTHEH)


FIELD MEASUREMENTSI I I i I I Well Depth (ft)7m

I 1 I Isample Depth (non-well) (ft) i i i i i

1st I

2nd I

4th!

&1&II unWeni•t»'C

^ 2nd

(STO) «i ,.4jra

(3TW 4th

•tM'C

urnteni•12S'C

NTUTMMp TmW«ly

FIELD COMMENTS>» y . . _^

Sample Appearance:Weather Conditions: __ __ __ __ _Qthar /// MBtntfru ~_. MP "TO ttP 2- *f /}/'4-

= 3. * '3.FILTERING: Use Chain of Custody (CC1) to indicate which bottles were filtered

Sampler: Employer:

certify that sampling procedures were in^cewdance with applicable EPA state and corporate protocols.

— 1^07 _A •ybattan' "• •iiKifofwafnaJ Ti aajHajn ana TaTtM Environmental Service* Compeny ORIGINAL

ENVIRONMENTAL TESTING »nd CERTIFICATION . Seal NO. 4lQ- 44$ ETC Job # d*Al-Wlt

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Datesealed.Ai^fi———By:.

Company:

Facility/Site.

Attn.:

Address:


Facility: I I H/l^uTl

Sample Point: fcJ-Liionai S*mpl* ^oif

Sourc* COM(trom Mlo«)

tour S*mDM tami ID(Mlt jutllfy)

Sun Tinw(1400 nr. doem

Sourc* CoOtrWtll .(W) OutfallSoil . .(Si

.(0) Bottom SMInwnl. ,..(B) Surface Impoundment.,..(!) LMcnttt Collection Syt.... .<Q OHw ..(Rl Qvncration Point ...(0) Tr«im«nt F«clllty . . . . . .(T) Lakt/OcMfl . . . . . . . . . . . . . . .(L) Specify

.(X)


No Type Size Present ANALYSISSAMPLER

Fill (TIM. ObservationsLAB

Observations

/TA.C


1.Shuttle Openecfly: (print),Signature: jt/M._

Date:Seal #:

Time:Intact:

I have received these materials in good condition from the above person.Name: -r- __ ,- ,, . „ Signature:


I have received these materials In good condition from the above person.Name: Signature:


Shuttle Sealed By: (prjnt)

Signature:

SHUTTLE #

ETC FIELD PARAMETER FORM (CC2) Form 0002Sample Minig«mtnt

08/88

ETC JOB »

Sample Poin

FIELD PROCEDURES

L i u iZi' d&&\!\ \ 5i,3l i

fcAtet/*t luj \l i6-iiuBi<?i*iRi i • I1

Soure* Coot Mmpl* Point |.D

AL .<t , , 1 /,(,!PURGE DATE START WJPWI ELAPSED HAS WAT! ft VOL. IN CASINO VOLUME PUMQEO(TV MM 001 '1400 Mr Clock) (Otllonu tQtlloni)

SAMPLING METHOD:

I y / | A-Submtnlbl« Pump D-Qlpptr/BottleSampler Type |ArJ B-ISCO E-B>n«r x-otrwr11 1 C-BI»ddtr Pump F-Scoop/8hov«)

« , »• . • i /L/x A'T«(lon C-PVCSampler Material /w^ B-M*tai 6-Piastic x-otherf tt t* * _i i A//* A-T«llon C-Poty«thyl«n«Tubing Material /^ a-Tvoon o-snicon x-otti«i

Sample Composited ^pNProcMurwPn

FIELD MEASUREMENTS

Wall FlAvatlon (ft/m*l) L.JL.,.. 1 i ... 1 W«» PftP»h

Dapth to Ground water (ft) | | 2 1 5"i J [0| ^mpl^ p«f

Qrounrt«/atareiavatinn{ftmsl) LJ... 1 1 |

i,t liisiJiTO 1at i /ivioiokrsr.2nd I dleJ 1 1 TO 9BH i f iv few I ra

aA ava*L aaiM. laMi

3rt i/.iaiai«w M i i /i v 1^ ioi -a.«h i/îcn-™ 4th i / i v i / i C o i rss

1 1 11 21 3 « | | | | | IHTUSMRpM Tf)ma> T ureWtty

FIELD COMMENTSSampla Appaaranca- <* | A^ NiCs ^SlNo!

Waathar Conditions! ûi^^H ft^Û ftf#*»^ (_iAr,' 2jLl

Othar iîO 1 I ^v A^Pfriov-?

I JI l^.-^BTs1SKCIFT OTHCRT

(SMCIFY OTHER

AFfCIPT OTH0V

>oonioni

m) I I Vl4 l2-l<ol)lh(non.u»«ll)(ft) I I I 1 I

1 1 1 1 1 1 1

M 1 1 1 1 1

1 1 1 1 1 1 1 1W»MMMMf| MhM MUM*

1 1 1 1 1 1 !

<^°F-

V£.2.£i- "2.C1 iCi =- 2/,/^.jV . JLSfi-J/W - 'S.VS' *v ~- (3.afli Vr*«/*»*iFILTERING: Use Chain of Custody (CC1) to indlcata which

Samplar T&t~F ^^^C^r^b Employer fifnnn

I certify that sampling procedures were in accordance with applicable

(0*l*i V (Signature)

bottlas wara flltarad

fey^

EPA state and corporate protocols.

The Environmental Sorviees Company ORIGINAL

\

ENVIRONMENTAL TESTING tna CERTIFICATION ' Seal No.

CHAIN OF CUSTODY FORM (CC1) ORIGIN DateSeaied

.ETC Job #89/08/U1 .,———————— By:.

Company:

Facility/Site:

Address:

PELfl Attn.: DAN SREEN

CITY DISPOSALC;'Q MOHPar INN HftpISOH SMITH CftST——I90//EXIT 12 AND 18 EAST, MADISON, UI

(414) 631 - 3150

53704


Facility:

Sample P

Source CodWen (WlSoil (S)

I f P ? I I I i I I I I I

3int: hSJ-Sou'Ct Co

t»Ouileii .River'Strei

'•Cil'ly'Sit* Coat (ODIion*! S*"tpii Pomi D«Knol>an«l

Kit Your S«moi«*o>m iD Sllrt Otit ' SWri T'rn* ElBMM H<*) |l*'l lUltilyl (VYIMMIDDl (2400 ftr. CIOCHI (COmpOW

(0) Bottom Sediment . . . (B) Surttee Impoundment . . (I) LMcnete Collection 5yt. . (C) Olhem <R) Generation Pomi ....(Q) Treatment Ftciltiy . . . . , (T) Lake/Ocean . . . . . . . . . . . . . . .(L) SDM

Wl

. . . . . . . . . . . . . . . . . ( X )

ry ——————————————


No

2

1

2

2

1

/i

I1

I

1

Type

uo*

TB

EXT

EXT

MET

Size

4C

40

1000

1000

1000

5bo

''rur!z<i^5•11?"

Prssera.

NONE

GC/MS

none

none

HN133

*>*^

!»•*<*

*£f*

A4»«

^.AtoD

ANALYSIS

UOLATILES

TRIP BLANK

EXTRB/MS

PST/PCB

METALS

CVîD^

^^ .I'^WÔi

dvL10?pi ™5^

SAMPLERFill (Y/H)

^

(0fj

ftJLA/V/Â/

Observations

yi/ 2Ml'syyS*/ysis

LAB. Observations

I/

r /

^/I

-/

[/

\S

(/ /

^/u/

L/CHAIN OF CUSTODY CHRONICLE

1.

2,

3.

4.

Shuttle Opened/By: (priSignature: jjy_ *•$

7*) >>^w &ucffU^< — -

Date: a ,f-. a«t Time: t /"-*.« A: o\^~n «+-\ Intact: ^x

I have received these materials in good condition from the above person. A/C~^^- S^~}Name: -r-_ cîx -r-i Signature: /&&r s\^*~**~*^**''^

P V ~Date: 2'=?^*^S^ Time: (p"?3^ Remarks: «v

I have received these materials in good condition from the above person.Name: Signature: 1 'v 1 fl


Shuttle Sealed By: (print) "Tjwe: /Â/^Â'/^T^Signature: /£*$£ C

LABUSEONLYOêni

SHUTTLE* /C*

Date: 7-?- s^s*i Time: n !<•^Z ——— -»c^ Seal#: ^/r^-V2' Intact: *tr

^^y /j^^ f^Jtf n.te 9%7^J(9 Tim- /d?^>-^f" TEMP, -c /// SSAH. /-J?/<^7cX3 r.own ,^-t^S


Sample M«n«g«nwrtoe/w

ETCJSamp

OB# {Lft&ll

IA Point kjJ II l6lU>lfcl i fciafci -i ISou'ct Cod* Simpw Point 1.0.

FIELD PROCEDUP

\8rt \ d\ i 2i9l l# ff i$ l^l ! L6lPUiQE DATE STAP.T PUP.QE ELAPSED HHS(VY MM ODl 12400 H< Clock)

SAMPLING METHOD:

*// A-Subm«r»ible Pump D-DlpptrfBottl*Sampler Type /\/C B-ISCO E-Btiir

f C-8l«dd«r Pump F-Scoop/Shovel

. t* * • , A/* A-Ttflon C-PVCSampler Material /T/C B-MIUI o-pi»stic_ . , .. t-. . . di* A-T«(lon C-Polytthylen*Tubing Material /fL a-Typon o-siiieon

Sample Composited JgN

ES

I 1/iViP.I i , i/,siWATER VOL. IN CASING VOLUME PURGED

1 Gallon ii (G« non il

^/u/,-2,/v<S>WCCIPY

K.ftth.r(SPCCIPV

K.ft»h«r

DTMfRl

OTMiR)

(SPf CIFY QTMf P.)

ProCMu WPtODOl loni

FIELD MEASUREMENTSWflll Fixation (ft/m..!) 1 1, 1 1 1 Wftll Oftpth (ft) | __ I

n«pth to Ground water (ft) | | | 2. 5 J, 51^1 <?flmnl» Hanth fnnn.«/«IIWft\ 1 !

Groundwater Elevation (ft msl) 1 , 1 | i 1

LL61&I1I«"» SflVl —1 / fi? I OJ (f TO) ! 1 1 £? 2 1 ft 1 "m'em

A j 1 /JQ i /_ 1 (STD) « ^ 1 1 IJ l ^,1 ^t um'«1113rd | (f5l™ 1 to| IS1B' ^rrt | | |^h?|OI iiM'fi

pti WM.OMM.

Ath 1 /i 1 1 & <8TD) 4th | | | S| 3 1^| "ft

1 /I/ lnkc> 1 1 1 t IN™SwiipM Tamp TwbMlty

1 1 1

1 1 1

1 1 1(MhwMniMMO <n

1 1 1(•WMrwrwiMMn *i

31^14.1311 1 1 1

1 1 1 1*hM <***

1 1 1

M i lMM MH*

1 1 1 1MM uMtt

FIELD COMMENTSSampla App«aranca: „, <P t'CÂ^ /W O CS Sr ^

Wsath«r Condition*- Su/1/li. ^-^*y*A tf/te&2^^**^

Other: l^>etl ^.ot^-W'-V .V\^ -Tl-V"* j>^^ - Ô^J^t 'J'0 P

'•

3i.*^- 25.rv--^^^/^3/i^//Fr = /.y^c'fl5r^*T.^ jc /c,«i-riFILTERING: Use Chain of Custody (CC1) to Indicate which bottles were filtered

Samnler: <2&T&£~ C/J£- ( A-/J PS EmployiPunti

I certify that sampling procedures were in accordances with app

ID..., ij I5ûr/>r \

• r P^7_4

licable EPA state and corporate protocols.

1211The Environmental Services Company

ENVIRONMENTAL TESTING intt CERTIFICATION Seal NO. • *&&

CHAIN OF CUSTODY FORM (CC1) ORIGINAL p.,«SM,«d

ETC Job it

By

Company: UJmr Attn.: *

Address:


Facility: I

Sample Point: ItU-l \I£HLOI Bl I i"2lgilgj i(Option* I Sim01* Point

Sou'C* Cod*(irom Miow)

irt 0*11IVY/MMfODl

Sun Tim*iWOOnr

Soufet Codti:Well . ,(Wl Outlal l . . . . . .(0) BottomSMlnwnt... .(B) SurticcImpoundment... .(I) LMChaMCollectionSys.... .(C)Soil .. (St RlwfStrtam.. (R) Qtntritton Point .... (Q) TrMimcnl Fjctlity . . . . . . m Ltk«/Oe«n . . . . . . . . . . . . . . . (L) Sptclty

• IX)


No Type PlVMTV. ANALYSISSAMPLER

Flit (YfN) ObservationsLAB

ObMrvallons

/•*\/


1.Shuttle Openedy: (prlSignature:

Date: Tlme:

Intact:

2.

I have received these materials In good condition from the above person.Name: ^- — . - . . -^ Signature:

Remarks:Time:

3.

I have received these materials in good condition from the above person.Name: Signature: V/12Date: Time: Remarks:


Signature: &&

LAB USE ONLYSHUTTLE*

\


Scmpto M*n*gtm«nt06/M

ETC JOB # (Lft 1 271

It f*-iU)iBi\SoutctCoM MfflOM Mm I.O.

FIELD PROCEDURESrt.fi-

E DATE(YV MM DO)

TART nJftOEMOO Hi Clock)

EUPSID MRS WATER VOL IN CASINOI I I 1/fcSf

VOLUME MJROCO

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Ik A>Subm0relbl* Pump D-Dlpp«r/BoMt«

&

e-iscoC-Bladdtr PumpA-T*flone-M*U!

E-B«ltorF>Scoop/8hovtlC-PVCD-Plullc

X-Ottwr

X-Othtr

X-Othti

ISKCIFY OTHOT

Sample Composited

FIELD MEASUREMENTSWell Elevation (ft/msl)Depth to Ground water (ft)Groundwater Elevation (ft msl)

2Well Depth (ft)

I .

I I I 1 I I

<.»i*t

1 1 I 8 I 3 I 8 I •i»x

3rd 3rd

4th

•I2S'C

PCI

M2f*C

IMTU

i i i i i

FIELD COMMENTSSample Appearance:.

FILTERING: Us« Chain of Custody (CC1) to indicate which botttes w«r* fllUrtd

Sampler Employer

certify that samplingj>rocedwes were in accordant with applicable EPA state and corporate protocols.

1213'///—"/^ sTascr*"<-^ TheEnvh

C*».EnvlronnMntal S*nH3*« Company ORIGINAL

ENVIRONMENTAL TESTING and CERTIFICATION ' Seal No. ETCJQb* CA1378

CHAIN OF CUSTODY FORM (CC1) ORIGINAL n«t-s«u.ri 89,-oa/oi By. ^ C-

Company: PELA

* .... «-. C ITY DISPOSAL Bu (414) 631 - 3150Facility/Site: —, .„ _ .—.,,.,., ..... ,,..»,,«^., .,.., ,,. „... ,— Phone:C'~0 riOLTttiwY INN MADISON SMITH EnSTI90/VEXIT 12 AND 18 EAST, MADISON, UII 53704Address: ___.——————————————————:———————'.__


Facility:

Sample P

Sou ret CocW«ll |W)Soi . IS)

1 f P P 1 1 1 1 1 1 1

Dint: lltJ-Sou ft* Ca

ts:Outf«n.River/Sift

FicHHy/Sil* COO*1

I Op t ion* i Samoi* Po>ni D*tctiption»i

1 lSi*Uî1IZi?t- U indi^l 1 i2L5ttfl* Your Simon Pomi ID St»rl Oa.it Stlft Tmt El* MM Hou'i*> lun ju»iilyi |YViMM/OD» i2WO nt eiocki (compoxm

(0) Bottom SMim*>ni .(B) Surf act Impoundment . . (I) Lt*ehattColl«ciionSy*.. . . .(Cl Other . . . . , <xim (Rl r,«n«r«tiOftPoifil (Gl TrMlmanl Facility (Tl 1 •t, Orf tn ([,) $pwMfy


No

2

1

2

2

1

11It1

1

I

Type

U0i=

TB

EXT

EXT

MET

Sin

40

40

1000

1000

1000

52*7

'/a?"

'/§•/tr/zj-

Prt»«rv.

NONE

GC/MS

none

none

HNQ3

**fo3

M>*€

^SoY

A/^C

^^T

ANALYSIS

UQLATILES

TRIP BLANK

EXTRB/MS

PST/PCB

METALS

r^-^rPto(!"** /^^T3 ' *-

£&\Qr^£L

T&CCHAIN

1.

2.

3-

4.

Shuttle Openedydy: <pri/ / j

Signature: d/+~-'\/3/Â^ <^

SAMPLERFlit (YIN)

1

r|)

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OF CUSTODY CHRONICLE

(LC®J Date: A - -d^ Time: |(at oC.*, Seal#: ois^-\i<\ Intact:

I have received these materials in good condition from the above person. f j

Date: 2 r- J S *) Time: //afaf Remarks: '^tfe-//ftJf^lK —————————— ——————— (^ ———————————————————————————

I have received these materials in good condition from the above person.Name: Signature: 1 ^ 1 4


Shuttle Sealed By: (print) "TJ-r— - *~j,'Ct^ 1 /, .T^Signature: {2$^

LABUSEONLYÎJWnJ

SHUTTLE » **'

Date: 2?*»«^ Time: Ifi5^5— R-u^4^^ ^ SeaU: d[<?&W(h lnt»ct: a^ '

rrt^v-V / /v>,5 I' 'jfj&tSJ•* -1 " «V(

TEMP -C ^ SEAL* <V-S?7*?^d< r-OND V^r?^^

ETC FIELD PARAMETER FORM (CC2) FomOOWHMflt0848

Sample Point lid 11 ifiJUllBiSoure* COM SwnpM Point I.D-

FIELD PROCEDURES

MJHQE DATE|YY MM 00)

START PUKE12400 Hf CtocK)

ELAPSED MRS WATER VOL. IN CASINO(tollonu

\2\VOUIME PUMQE

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

&1 A-Subnwralbl* PumpB-ISCOC-Bl*dd*r PumpA-Tfflon'B-Mittl

D-DlpD*r/Bottl«£-B«ll«rF-Scoop/Shovtl

C-PVCD-PlMtlc

ISMCIFV OTHER)

X-Othtf

x-ottwONOFV OTMfBt

(SPECIFY OTHIRI

Sample Composited ¥TN

Well Elevation (ft/msl)Depth to Ground water (ft)Groundwater Elevation (ft mal)

FIELD MEASUREMENTS

I i I I Well Depth (ft)Sample Depth (non-well) (ft)

I | | 1 1 1 1

! 1 i 1 1

(•*•€ pWW

•12S-C

3rd

4tht / I / I

m I

NTUTwtMHy

FIELD COMMENTSSample Appearance:.Weather Conditions:Otherî

ee: 4l./\wy fat4*k.L- i^fê/i18! î^yt^LJ jtotL.'^ $Pf4L*jf f J ' Z. ~ -TT. I __f

, * *^nt *^T£^f C /^ _72LCfit**l

*FILTERING: Use Chain of Custody (CC1) to Indloatt which bottles were filtered

Sampler: At*yl/TS Employer

I certify that sampling procedures were inâee^rdance with applicable EPA state and corporate protocols.

1*15A »uM0w •*The Environmental Servtew Company ORIGINAL

N

ENVIRONMENTAL TESTING tnd CERTIFICATION Seat NO,

CHAIN OF CUSTODY FORM (CC1) ORIGINAL Dateseaied.ETC Job*

——— By:_

Company: u)mr Attn.:

Facility/Site: _».

/~)


Facility: j£l(Opnen«i 5*mpl« Pemt

Sample Point: liJ-l I i£t^l Si I I I2.i«dlUWMHeuriSCHJ'C* Coot You' Simple M-nt ID SUrt Oat* Slari

Ifrom Miowl il*tl (uitilyi [VYrMMfDO) (3400 hi. clock)

Souret Cod«Well . (W) O u t ( « l l . . . . (0) Bottom S«dlm«nt. .. (B) SurfK* Impoundmtnt.... (t) LMCtiai* CollMlloh Syl..... (O 0»W ..Soil . .(5) RtvertStrum. |fl) 0«n«r»tion Point . .|0) Tr«iim«nt Facility . . . . . .(T) LjhtrfOcMn .............. .(L) Sptclfy

.(X)


No Typ« Sin Pnnenr ANALYSISSAMPLER

FltL (Y/N) ObttrvatlonsLAB

Observations

CHAIN OF CUSTODY CHRONICLEShuttle Opened^y: (priSignature:

Date:Seal #:

Time: o"7*/5"Intact: ==7

2.

have received these' materials in good condition from the above person.Name: Sionature:

Date: Remarks:A.

3.

1 have received these materials in good condition from the above person.Name: Signature:


1216


Signature: "

LAB USE ONLY Op

SHUTTLE # _ _

FIELD PARAMETER FORM (CC2)08/88

ETC JOB #,

Sourci Codt S*moi» Point i.O.

PUHOE DATE(YY MM DDI

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

1 IfaAalSTAftT PURQC(3400 Hr Clock)

FIELD PROCEDURES

ELAPSED HAS WATER VOL. IN CASINO(CUllonil

VOLUME W«OI((QlllentJ

Pump D-Otpp«r/Bottl«B-ISCO E-8all«rC-BI*dd«f Pump F-Scoop/Shov«l

A-T*flonB-M«ni

A-T«flonB-Tygon

C-PVC

OPoly«thyl«nt

X-Othflr

X-Ottwr

X-Othti

(WfCIFY OTHIH)

(MKIFV OTHCm

(MtCfFY DTHIft)


1st

FIELD MEASUREMENTS

I 1 I 1 Well Depth (ft)Sample Depth (non-well) (ft) 1 1 1 1

3rd umtofli•t»*C j i i i i i 11_i

4,h •IM'C

INTU•ellnpie) TMnp TwbMHy

FIELD COMMENTSSample App«aranr.«- J/.- UU^ /vi^tt^ U -Un -y^

londltlona: 3it**.*« tvfop Ar^*>^ u^f"

Other,

r -*

. 6, VFILTERING: Use Chain of Custody (CC1) to Indicate which bottles were filtered

Sampler:

I certify that sampling procedures>vrafe in accordance with applicable EPA state and corporate protocols.

1 1 i * *7Z i 7o* ******** TIMMHM wtri Tiem t»«i C«p.

The Environmental Services Comiyany OPiGlNAL

ENVIRONMENTAL TESTING »na CERTIFICATION Seal No. .

CHAIN OF CUSTODY FORM (CC1) ORlGtNAL DateSeaiod

__ FTCJahH CA1362

89/09x25 fly KG

Company: PEL ft

Facility/Site: CITY DISPOSAL___________________C/0 HOLIDAY INN MADISON SMITH EAST

Address- I9QX/EX1T 12 AND IB EAST. MADISON. Ull

Attn.: CLAYTDN LINDSEY

Phone: (414) 631 - 3190

53704


Facility:

Sample Point: LXl-LEiMI CMI

SlLiA-lAJlklSou re* CM*ilfom Miowi

vour S*mpi« Pom I IDIW'i ju»tilyl

jntl S*I*IDI« Po>nl

JJMSIl'i D»i«

IVYlMM'ODiStart Tih

H400 KI. clock)

i3|f IIPMd MOufl

Source Codts:W*H |W) Outfall . . . . .(0) BottomStdimtnt. <B) Sutfac*Impoundmini. .(I) Lt«ch«nCo(l»c1lonSy». .. .(C) OttwSoil .. (SI RivtrfStrMm (fil QtntratiortPoinl , .. .(0) Trwiment Facility ... (T) LaK*fOc««n . , , . , . , , . . . . . . .(U


No

2

3

1

1

1

1

1

1

1

1

Typ»

iJOA

EXT

MEll

MET

COS

FL

COh

COS

CONCON

Sl»

40

1000

900

500

LI 125

. 125

5 125

5 125

S 125

J 125

PrtMfv.

NONE

none

HN03

HN03

NONE

NONE

H2S04

H2SQ4

H2S04

NONE

ANALYSIS

, / T<*/ **-*V/cUOLAT1LES / Wf.LL*>m -(*L,

/EXT/MSXCC

METALS

CYANIDE

CHLOR

FLUOR IDE

TOC

N03/N02

PHENOL

PH/SCQND

SAMPLERFin. (Ymi

ffi>fSHX^tJ1*

Ob»«rvatlon*

•

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^

^

^

^x J

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•

•*

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LABObservation*

t^1^

L^^/, L -

^^

^

i^

(/CHAIN OF CUSTODY CHRONICLE

2.

Shuttle Opened By: (print)Signature:

I have received trtese materials in gootftondition from the above person.Name: -r-_ **.<*.. ^ Signature:


3.

I have received these materials in good condition from the above person.Name; Signature: 1218


4.Shuttle Sealed By:Signature:

SHUTTLE*


Scmpl* Management08/68

Ifl^iAfl^ 1 / i V i A w S lPUROE DATE(VV MM DO)

SAMPLING METHOD:

Sampler Type •

Sampler Material

Tubing Material

Sample Composited

START PURQElajaWWCloeW

"TCSubnwilbl* PumpB-ISCOC-Blidd«r Pump

"^Ttflon IB-M lal

A-Ttllon (B-Tygon

//N

ETC JOSample

FIELD PROCEDURE

1 i i3l

R* ^/afj?

Dnln, IVJ IFlUD|&,< - i f t i A / i VT -I ISou it t CM* S*mp<« Point i.D

Jili i i e?l i I , lELAPSED HH9 WATER VOL. IN CJ*INQ VOLUME PURGED

(6«Honii |O«ltonii

>Dlpp«r/Bottl0••Bailer x:-Scoop'Shovt>l

>PVC3-Piastic X>Poiy«thyl«n«^Silicon *

tn«»(SPtciPy o

Olh«r

THM)

(SPtcirr OTHER)

nth.,(SPECIFY OTHIN)

PrecMuWProportiant

Well Elevation (ft/msl)Depth to Ground waterGroundwatsr Elevation

1st I l*T

F

(ft) 1(ftmsl) 1

» ... 1 I 1

3nri I I (WDI ?nH I I Ipit •PM.OOM

3rd I I I <»TD' 3rd I I I

4th I I I *TW 4th I I I

I I I l <Bflfltple) TWflp

Sample Appearance:Weather Conditions: _ ,Other g»4-tf«S T

ELD MEASUREMENTS1 , j Welinepth(ft) |

i _ 1 Sample Deoth (non-welh (ftl 1 _i i i

unWem... MM'C __

iHiriemt

tifiWemL

j luntm•1M*C

I

I I

I I

I I

1 1i 1

1 1

1 1to* wntta

1 1UN ItMM

1 1

1 1 1 1 1 IHTUTinbWIty

j4-»O

jL/TX/-f*!-W7 A&

FIELD COMMENTS

fef qjrr ^ '/yum-%.If ^*^ ftr^ ', /

5 ^.4J feo* Pt

s «p»A-ft€-i^

FILTERING: Use Chain of Custody (CC1) to indicate which bottles were filtered

Sampler "SVp - ttW^sf/UD Pmn.nU.r. ffiZLA

\ certify that sampling procedures were in accordance with appli

,D.,t. Q CfrQftllyr*

:able ERA state and corporate protocols.

1^19TtM Envlronmwital S«rvlcM Company

ENVIRONMENTAL TESTING tno CERTIFICATION Seal No. 4&Q'• ^40 ETC Job*

CHAIN OF CUSTODY FORM (CC1) ORIGINAL DateSealed_&£j£____By:

Company; Attn.:

Facility/Site: ..

Address: _

- f!*


I I I l>TlFacility: 1 I Ir*ti"iv"auv \*uuv

Sample Point: i)fl-lFi^iDi &CiA-iA/iKi iSou'C* Coot foul Simoit Poml ID

t Simoi* Pom ( utiecptiofiti

Slirt 0«l*(YY/MM'DOl

Sli'i Tun* ClARtM Hour*

Sou'Ct CootsWfH (Wi Oullall (0) Bottom StOimtm (B) SurUe* Impound m to I . .(I) Lt«ch«HColl«llon Sy* .,, ,(C) Other .Soil lS> Rivtr'Slr«m <Ri Qcntrtlton Point . . (0| Trt»tm«ni Facility . . . . . .(T) Litit/Octtn . . . . . . . . . . . . . .(LI SlMCHv


No Typt Prvserv. ANALYSISSAMPLER

Flit (YIN) ObservationsUB

ObMrvatfons

CHAIN OP CUSTODY CHRONICLEShuttle Opened/pySignature:

Date:Seal #: 00-^34

Time:Intact:

. /r

2.

I have received these materials in good condition from the above person.Name: -r _ — . - . . . • > * Signature:



Date; Time: Remarks:

•;?n

: Shuttle Sealed

tvvianHUFHTAL TESTING *ntt CERTIFICATION

FIELD PARAMETER FORMETC JOB #. T^EE

i I.D.

WMI DAT!(YY MM 001

STAflT W12400 Hr OocM)

FIELD PROCEDURES

ILAPltD MM WATf M VOL IN CASINOr

i i i i t<VOLUME PUMIE

SAMPLING METHOD:

Sam pier Type

Sampler Material

Tubing Material

Sample Composited

A*Subm*ralbl« Pump D-Dtpp«r/Bottl«B-ISCO E-BallwC-BI«dd*r Pump F-Scoop/Showl

if

A-Ttflon C-PVC§-M«UI D-PlMtlc

C-Poly*thyl«n«

X-Othtr

X-Oth«i

Y/N


FIELD MEASUREMENTSI I I I 1 I I weMDepth(ft) I I I 1 II I I I 1 I I Sample Depth (non-well) (ft) I I I 1 II I I I 1 I I

1st «™» 1st

ttWC

3rd! I I I !•"• 3rd I I I I I

4th I I I I I *™> 4th I I I I Iph fpM.«wi«.

I l l |ro I I I I

•t»*c

MU*C

INTUTufbuny

Sample Appearance:Weather Conditions:Other

FIELD COMMENTS

FILTERING: Usa Chain of Custody (CC1) to Indleata which bottlas wara flltarad

Sampler

I certify that sampling procedures were in apeordance with applicable EPA state and corporate protocols.

ORIGINAL

ENVIRONMENTAL TESTING and CERTIFICATION

CHAIN OF CUSTODY FORM (CC1)

Seal No. ETCJ0b,cft2017

89/09/21 KC

Company: PELA L.INDSEY

^ ,.,. *,. CITY DISPOSALFacility/Site: Cr0 hOLlPA'l' INN MAPISON SMITH CflST Phone:(414) 631 - 3150

190/^EXIT 12 AND IB EAST, MADISON, UI 53704


I 1

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.(X)


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Flit (YIN) ObservationsLAB

Observations

UOA 40 NONE UOLATILES

iS- -4* JB1B BL

EXT 1000 none EXT/MSXCC

MET 900

CONU 125 NONE CYANIDE

— TjViPQ JU4IT" tJ(*>C ~rr HA*

&* A/>£

CHAIN OF CUSTODY CHRONICLEShuttle Opened By: (print)Signature:

Date:

Seal*: Intact:

2.

I have received thrfie materials in gooiMondltion from the above person.Name: _. _. . rs. Signature:

Remarks:Time:

3.

I have received these materials in good condition from the above person.Name: Signature: 1222


Shuttle Sealed By

Signature:

LAB USE ONLY

SHUTTLE*

ENVIRONMENTAL TESTING tnff CERTIFICATION

FIELD PARAMETER FORM (CC2)ETC JOB #Sample Point L£J

FIELD PROCEDURES

TE(YYMMOOI

tTAHT MJMI12400 Hr CMC*)

u5TELAPSID HRS WATER VOL IN CASINO

I I I I IVOLUMC PUTOID

SAMPLING METHOD:

Sampler Type

Sampler Material

Tubing Material

Sample Composited

A-Sufanwslbl* Pump 0-Oipp«r/Bottl*B-ISCOC-Bladdflr PumpA-TtflonB-MtUI

A-T«ftonB-Tygon

E-B«lltrF-Scoop/Showl

C-PVCD-Plaillc

C-Poly«trtyl«n«Q-Silicon

x-Otrnf

X-Othtr

X-Othti

(•TCCIFY OTHIB)

ISKCtFY OTHIW


FIELD MEASUREMENTS1 i _L

I I 1 I i I III I i i i I

Well Depth (ft)Sample Depth (non-well) (ft)

I I I

let I

2nd I

3rd I

1st

2nd

3rd

4th

re,

•12B'C

•ttf'C

•tas-c

•t»*c

IHTUTuAMHy

FIELD COMMENTS

Weather CondltlonarOther:

. *too*»nr > Lt*

FILTERING: Use Chain of Custody (CC1) to Indicate which bottle* were filtered

Sampler: Jfe^& ~&*SSpBp ^hJSOtncj Employer

I certify that sampling procedures were in acpaidance with applicable EPA state and corporate protocols.

ORIGINAL

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technical memorandum no. 3 for remedial …

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