task1 : indentify the major organic component in the contaminated tank using nmr

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The task was to identify the cause of an unusual purple colour in a waste holding tank on an industrial estate. The tank was the direct responsibility of the company “Facilities Management” and was used to collect aqueous waste from two different pharmaceutical companies: “RU Regular” and “RU Pain 3”. Both companies denied being responsible for causing the Purple Solution. The final was hosted by the Department of Chemistry at the University of Reading. 250 schools entered the competition (with 3 students per team) and 18 schools made it to the final. As the map shows the finalists came from all over the UK. Working as a team, each school had to complete 3 related analytical tasks; to solve the ‘Purple Solution’ problem team members then had to work together and combine their results. The activities were designed to test the pupils analytical skills as well as their problem solving skills. The students also had to follow certain deadlines and they all did this brilliantly. All of the pupils in the competition were in their first year of A- levels. Dr Joanne Elliott the local TASK1: Indentify the Major Organic Component in the contaminated tank using NMR. Task 2: Determine, by using a Spectrophotometer, the amount of iron in the drainage water from the Acid Storage Farm. TASK 3: Determine the amount of Aspirin in the input sample from “RU Pain3” by a series of titrations. In addition determine that the waste stream contains salt as well as Aspirin 1ST PLACE : SIR JOHN DEANE’S COLLEGE, Northwich. They were awarded a £750 cheque for their school and each team member received Amazon vouchers. "We can't quite believe it but are delighted to have won! The day was challenging but lots of fun and we learnt a lot. The competition has definitely made me think about studying chemistry at higher education, hopefully at somewhere like Reading." - Jack Hoffman, a team member of the winner team THE PURPLE SOLUTION 2011 National Final Schools Analyst Competition Heather White, Anne Thomas (teacher) , David Nicholson, Jack Hofmann. The winning team from Sir John Deane's College in Northwich 2 nd Place: Arnold School, Blackpool 3 rd Place: North Halifax Grammar School , Halifax “It was a little bit more challenging than what we have done before but this is good!” - Anna Haycock (Ysgol Brynrefail School) Poster produced by Year 10 work experience students Mariya Geneshka and Jose Dean-Lewis between June 20th to June 24 th 2011 Leighton Park School The Final Task The judges took into account the analytical skills of the team as well as the results gained. The teams had to produce a detailed analytical report including a breakdown of their results and a solution to the problem. Whilst the judges decided on the winners, the competitors were entertained with a lecture by Dr Matthew Almond on spectroscopy and the The Chemistry Department Natalie Smyth Friend's School Ben Nicholson, Lord Lawson of Beamish School Tiffany Shum, Chigwell School Johannes Kangur Stamford Endowed School From RU Regular From RU Pain3

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Page 1: TASK1 :  Indentify the Major Organic Component in the contaminated tank using NMR

The task was to identify the cause of an unusual purple colour in a waste holding tank on an industrial estate. The tank was the direct responsibility of the company “Facilities Management” and was used to collect aqueous waste from two different pharmaceutical companies: “RU Regular” and “RU Pain 3”. Both companies denied being responsible for causing the Purple Solution.

The final was hosted by the Department of Chemistry at the University of Reading. 250 schools entered the competition (with 3 students per team) and 18 schools made it to the final. As the map shows the finalists came from all over the UK.

Working as a team, each school had to complete 3 related analytical tasks; to solve the ‘Purple Solution’ problem team members then had to work together and combine their results.

The activities were designedto test the pupils analytical skills as well as their problem solving skills.The students also had to follow

certain deadlines and they all did this brilliantly.

All of the pupils in the competition were in their first year of A- levels.

Dr Joanne Elliott the local organiser said “I hope those competing were inspired by our state-of-the-art facilities and will consider a career in chemistry.”

TASK1: Indentify the Major Organic Component in the contaminated tank using NMR.

Task 2: Determine, by using a Spectrophotometer, the amount of iron in the drainage water from the Acid Storage Farm.

TASK 3: Determine the amount of Aspirin in the input sample from “RU Pain3” by a series of titrations. In addition determine that the waste stream contains salt as well as Aspirin

1ST PLACE: SIR JOHN DEANE’S COLLEGE, Northwich.They were awarded a £750 cheque for their school and each team member received Amazon vouchers.

"We can't quite believe it but are delighted to have won! The day was challenging but lots of fun and we learnt a lot. The competition has definitely made me think about studying chemistry at higher education, hopefully at somewhere like Reading."   - Jack Hoffman, a team member of the winner team

THE PURPLE SOLUTION2011 National Final

Schools Analyst Competition

Heather White, Anne Thomas (teacher) , David Nicholson, Jack Hofmann. The winning team from

Sir John Deane's College in Northwich

2nd Place:Arnold School, Blackpool

3rd Place:North Halifax Grammar School , Halifax

“It was a little bit more challenging than what we have done before but this is good!” - Anna Haycock (Ysgol Brynrefail School)

Poster produced by Year 10 work experience students Mariya Geneshka and Jose Dean-Lewis between June 20th to June 24th 2011

Leighton Park School

The Final TaskThe judges took into account the analytical skills of the team as well as the results gained. The teams had to produce a detailed analytical report including a breakdown of their results and a solution to the problem.

Whilst the judges decided on the winners, the competitors were entertained with a lecture by Dr Matthew Almond on spectroscopy and the uses of chemistry in space.

The Chemistry Department

Natalie Smyth Friend's School

Ben Nicholson,Lord Lawson of Beamish School

Tiffany Shum, Chigwell School

Johannes Kangur Stamford Endowed School

From RU Regular

From RU Pain3