task 210 – subsurface site investigation … no. 314-5332 ... whether the proposed construction...

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An Employee-Owned Company

TASK 210 – SUBSURFACE SITE INVESTIGATION REPORT

CONNECTICUT DEPARTMENT OF TRANSPORTATION

CAPACITY & OPERATIONAL IMPROVEMENTS ON ROUTE 69

IN THE VICINITY OF ROUTE 15

NEW HAVEN & WOODBRIDGE, CONNECTICUT

Prepared for:

Connecticut Department of Transportation

Division of Environmental Compliance

2800 Berlin Turnpike

Newington, Connecticut 06111

Prepared by:

BL Companies, Inc.

355 Research Parkway

Meriden, Connecticut 06450

BL Companies Project Number 14EC0047

ConnDOT Project No. 92-0672

Assignment No. 314-5332

January 2017

This report was prepared by the individuals listed below. Any questions or comments regarding

the information provided herein should be directed to these individuals.

Prepared by:

Joy P. Kloss, LEP, CHMM

Sr. Environmental Scientist

Reviewed by:

Aaron L. Silva, LEP

Project Manager

Task 210 – Subsurface Site Investigation -i- Project No.14EC0047

Improvements on Route 69 In the Vicinity of Route 15 January 2017

State Project No. 92-0672; Assignment No. 314-5332

TABLE OF CONTENTS

1.0 INTRODUCTION.............................................................................................................. 1

1.1 BACKGROUND AND PURPOSE ............................................................................................. 1

1.2 PREVIOUS ENVIRONMENTAL REPORTS ............................................................................... 1

1.3 SCOPE OF WORK ................................................................................................................. 3

2.0 LOCAL ENVIRONMENT AND RECEPTORS ............................................................ 5

2.1 SURFICIAL GEOLOGY .......................................................................................................... 5

2.2 BEDROCK GEOLOGY ........................................................................................................... 5

2.3 GROUNDWATER .................................................................................................................. 5

2.4 SURFACE WATER ................................................................................................................ 5

3.0 FIELD INVESTIGATION AND SAMPLING METHODS .......................................... 6

3.1 SOIL BORING INSTALLATION AND SAMPLING .................................................................... 6

3.2 GROUNDWATER SAMPLING ................................................................................................ 6

4.0 REGULATORY CRITERIA ............................................................................................ 7

4.1 SOIL CRITERIA .................................................................................................................... 7

4.2 GROUNDWATER CRITERIA .................................................................................................. 8

5.0 SUMMARY AND EVALUATION OF ANALYTICAL DATA .................................... 9

5.1 SOIL SAMPLE ANALYTICAL RESULTS ................................................................................. 9

5.2 GROUNDWATER SAMPLE ANALYTICAL RESULTS ............................................................ 11

5.3 QUALITY ASSURANCE (QA)/QUALITY CONTROL (QC) RESULTS .................................... 11

6.0 POTENTIAL SOURCES OF CONTAMINATION, RECEPTORS, AND

IDENTIFIED PRELIMINARY AREAS OF ENVIRONMENTAL CONCERN ...... 13

7.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................... 14

8.0 LIMITATIONS ................................................................................................................ 15

9.0 REFERENCES ................................................................................................................. 16

APPENDIX A – FIGURES

Figure 1 Site Location Map

ENV-01 through ENV-03 Site Investigation Plan

APPENDIX B – TABLES

Table 1 Sample Location Rationale and Selected Analyses

Table 2 Soil Analytical Results

Table 3 Groundwater Analytical Results

APPENDIX C – BORING LOGS

APPENDIX D – LABORATORY ANALYTICAL REPORT

Task 210 – Subsurface Site Investigation -1- Project No.14EC0047



1.0 INTRODUCTION

BL Companies was retained by the State of Connecticut Department of Transportation

(ConnDOT) to conduct a Task 210 Subsurface Site Investigation (SSI) in support of ConnDOT

Project No. 92-0672, Capacity and Operational Improvements on Route 69 in the Vicinity of

Route 15 in New Haven and Woodbridge, Connecticut. This report provides a brief description

and history of the project area, a discussion of the local environment and receptors, the

investigation rationale, a summary of the data obtained during the investigation, an interpretation

of the results with respect to the appropriate regulatory criteria, and recommendations.

1.1 Background and Purpose

The project corridor is located along Route 69 between Lucy Street in Woodbridge, Connecticut

and Glen View Terrace in New Haven, Connecticut. The primary purpose of this project is to

improve capacity and operation deficiencies on Route 69 in the vicinity of the Route 15

Interchange 59. This project involves minor widening on Route 69 in the northbound and

southbound direction and Route 15 exit ramps to alleviate delays and queue lengths. In addition,

the project includes the installation of new sidewalks, ramps, and crosswalks to facilitate

pedestrian movement along Route 69, and on Route 69 at the Route 63 intersection. The Site’s

location and pertinent features are depicted on the enclosed Site Location Map (Figure 1) and

Site Investigation Plans (ENV-01 through ENV-03) in Appendix A.

The purpose of this Task 210 SSI is to collect soil and groundwater data in order to evaluate

whether the proposed construction activities require management of contaminated soil and

groundwater.

1.2 Previous Environmental Reports

Prior to the preparation of this Task 210 SSI, BL Companies was retained by ConnDOT to

conduct a Task 110 for the improvements on Route 69 in the vicinity of Route 15 in New Haven

and Woodbridge, CT. The findings of this report are briefly summarized below:

Task 110 Corridor Land Use Evaluation, Improvements on Route 69 in the Vicinity of Route 15,

New Haven and Woodbridge, Connecticut, BL Companies, dated May 2016

The objective of the Task 110 was to assess the relative environmental risk associated with

current and former land uses within the project corridor and vicinity; to evaluate whether the

project activities may encounter hazardous wastes, contaminated materials, or other regulated

substances; and to evaluate whether further investigation of the project corridor is warranted.

The Task 110 included the evaluation of 35 parcels, of which 11 were assigned a “high risk” and

4 were assigned a “moderate risk”, and 20 were assigned a “low risk” designation. The high,

moderate, and low risk parcels include the following:




High Risk Parcels

Parcel 1 – 1475 Whalley Avenue – Establishment as defined by the CTA.

Parcel 3 – 1460 Whalley Avenue – Historical dry cleaning facility.

Parcel 5 – 1474 Whalley Avenue – Establishment as defined by the CTA.

Parcel 6 – Whalley Avenue – Historical industrial operations associated with The Pond Lily Dye

Company.

Parcel 9 – 1522 Whalley Avenue – Historic commercial/industrial operations.

Parcel 10 – 1536 Whalley Avenue – LUST and CPCS listing.

Parcel 13 – 1570 Whalley Avenue – Historical use as a gas station, a leaking UST, hazardous

waste generation, and documented releases.

Parcel 17 – 149 Amity Road – Historical use as a gas station with a leaking UST.

Parcel 18 – 1655 Litchfield Turnpike – Historical use as a gas station, with a leaking UST, and

documented releases.

Parcel 22 – 1660 Litchfield Turnpike – Historical use as a gas station with a leaking UST.

Parcel 25 – 1670 Litchfield Turnpike – Historical dry cleaning facility.

Moderate Risk Parcels

Parcel 7 – 1500 Whalley Avenue – Historical commercial use with a car wash operation.

Parcel 8 – 1516 Whalley Avenue – Historical commercial use with a contractor’s storage

operation.

Parcel 12 – 1560 Whalley Avenue – Historical commercial use with a UST removal.

Parcel 20 – 1659 Litchfield Turnpike – Historical storage of truck trailers.

Low Risk Parcels

Parcel 2 – 1440 Whalley Avenue – Historical use as residential and low-risk commercial activity.

Parcel 4 – 2 Amity Road – Historical use as residential and low-risk commercial activity.

Parcel 11 – 75 Amity Road – Vacant parcel and restaurant, historically utilized as parking and/or

entrance.

Parcel 14 – 1595 Whalley Avenue – Vacant parcel, historically undeveloped.

Parcel 15 – 109 Amity Road – Vacant parcel, historically undeveloped.

Parcel 16 – Whalley Avenue – Vacant parcel, historically undeveloped.

Parcel 19 – 1663 Litchfield Turnpike – Historical low-risk commercial activity.






Parcel 24 – 1668 Litchfield Turnpike – Historical residential use.





Parcel 30 – 1677 Litchfield Turnpike – Vacant parcel, historically undeveloped.



Parcel 33 – 1671 Litchfield Turnpike – Vacant parcel, historically undeveloped.



Based upon these findings, BL Companies recommended that a Task 210 SSI be performed in

areas of anticipated intrusive construction activities and/or right-of-way acquisitions adjacent to

the low, moderate, and high risk parcels.

1.3 Scope of Work

BL Companies completed a Task 210 SSI work plan, dated October 19, 2016, which was

approved by ConnDOT. The scope of work included the following tasks:

• Pre-drilling activities (1) obtain a ConnDOT Encroachment Permit, (2) mark

proposed drilling locations and contact Call-Before-You-Dig to request mark outs of

subsurface utilities, and (3) discuss proposed drilling locations with representatives of

ConnDOT, and other utility companies/agencies;

• Completion of seven soil borings to depths of 5 to 15 feet below grade (ftbg) using a

Geoprobe direct push rig;

• Completion of six soil borings to a depth of 2 ftbg using a hand auger;

• Installation of two temporary groundwater monitoring wells;

• Recording lithology and field screening soil samples with a photoionization detector

(PID);

• Collection and laboratory analysis of up to 20 soil samples for one or more of the

following:

o Volatile Organic Compounds (VOCs) by EPA Method 8260;

o Semi-Volatile Organic Compounds by EPA Method 8270;

o Extractable Total Petroleum Hydrocarbons (ETPH) by CT ETPH Method;

o Total RCRA 8 Metals by EPA Methods 6010/ 7471;

o Leachable RCRA 8 Metals using the toxicity characteristic leaching

procedure (TCLP);

o Polychlorinated Biphenyls (PCBs) by EPA Method 8082;

o Pesticides by EPA Method 8081; and

o Ignitability; Reactivity; and pH.




• Collection and laboratory analysis of groundwater samples from two temporary wells

for the following:

o VOCs by EPA Method 8260;

o SVOCs by EPA Method 8270;

o ETPH by CT ETPH Method;

o PCBs by EPA Method 8082;

o Pesticides by EPA Method 8081; and

o Total and Dissolved RCRA 8 Metals, Copper, and Zinc by EPA Method

6010/7471.




2.0 LOCAL ENVIRONMENT AND RECEPTORS

2.1 Surficial Geology

According to the United States Geologic Society (U.S.G.S.) Surficial Materials Map of

Connecticut, dated 1992, the surficial geology of the project corridor consists of sand and gravel

overlying sand. Sand and gravel is generally less than 20 feet thick, horizontally bedded, and

overlies thicker, inclined layers of sand.

Based on observations during boring installation, surficial materials consist of brown fine to

coarse sand with silt and varying amounts for fine to coarse gravel, which is underlain with

red/brown fine to coarse sand with fine to coarse gravel and silt. Petroleum staining and odor

were observed in boring B-4, between 1 and 10 ftbg. Boring logs are included as Appendix C.

2.2 Bedrock Geology

According to the “Bedrock Geological Map of Connecticut”, dated 1985, bedrock beneath the

project area is mapped as New Haven Arkose, which is characterized by red, pink, and gray

coarse-grained, locally conglomeratic, poorly sorted and indurated arkose, interbedded with

brick-red micaceous, locally shaly siltstone and fine-grained feldspathic clayey sandstone.

Bedrock was not encountered during this investigation.

2.3 Groundwater

According to the Connecticut Department of Energy and Environmental Protection (CTDEEP)

Water Quality Classifications Map of New Haven, Connecticut (November 2016), groundwater

within the southernmost portion of the project, from Route 15 and south, is located in an area

with “GA/GAA” classified groundwater. “GA/GAA” classified groundwater is considered

suitable for direct human consumption without the need for treatment; however, the water quality

within this area may not be meeting current standards. Groundwater within the remaining

portion of the project, from Route 15 and north, is classified as “GA”, which is located within an

area of existing and potential private or public water supply wells. The Site is not located in an

Aquifer Protection Area. During this Task 210 SSI, groundwater was encountered at

approximately 7 to 9 ftbg.

Based on the presence of the West River, the general direction of groundwater flow is inferred to

be south/southeast.

2.4 Surface Water

Lily Pond and West River run adjacent to the project area to the east. According to the above

referenced CTDEEP map, Lily Pond and West River are classified as a Class “A” surface waters.

The designated uses for Class “A” surface waters are existing or proposed drinking water

supplies, habitat for fish and other aquatic life and wildlife, recreation, navigation, water supply

for agriculture and industry.




3.0 FIELD INVESTIGATION AND SAMPLING METHODS

This Task 210 SSI included the advancement of 13 soil borings, installation of two temporary

monitoring wells, and collection and laboratory analysis of 20 soil samples and two groundwater

samples. BL Companies subcontracted Cummins Envirotech, Inc. (CEI) of Old Lyme,

Connecticut to advance borings and install the temporary wells. The soil boring locations are

depicted on ENV-01 through ENV-03.

Soil and groundwater samples were analyzed for regulated constituents of concern associated

with the historical use of adjacent properties. Table 1 in Appendix B provides a summary of the

sampling rationale and the laboratory analyses requested for each soil and groundwater sample.

The following sections summarize the field investigation and sampling methodologies used

during this investigation.

3.1 Soil Boring Installation and Sampling

On November 16, 2016, seven soil borings, identified as B-1 through B-7, were advanced to

depths ranging from 5 to 15 ftbg using a track-mounted Geoprobe direct-push drill rig. Soil

samples were obtained continuously during advancement of borings using a 2-inch diameter,

5-foot long, thin-walled, sampling device equipped with disposable acetate liners. Six borings,

identified as HA-1 through HA-6, were advanced utilizing a hand auger to a depth of two ftbg.

A representative portion of each soil core was screened with a PID to detect estimated quantities

of total VOCs in vapor emitted from the soil. The PID was equipped with a 10.6 eV bulb and

was calibrated to isobutylene standard gas (100 parts per million (ppm)). The results of the PID

screening were 0.0 ppm for all samples screened with the exception of B-4 which exhibited

elevated PID readings ranging from 300 to 2,341 ppm. Petroleum staining and odor were also

observed throughout the soil boring. PID readings are provided on the boring logs in

Appendix C.

Soil samples were selected for laboratory analysis based the anticipated depth of construction

activities, observations (physical evidence of contamination and/or lithology change), and the

results of the field screening. The samples were submitted under proper chain-of-custody to

Accutest New England (Accutest) of Marlborough, Massachusetts, a State of Connecticut

Department of Public Health certified environmental testing laboratory.

3.2 Groundwater Sampling

Following soil sampling, a 1-inch diameter PVC screen and riser pipe were inserted into borings

B-1 and B-3, as temporary sampling wells. After the groundwater in the temporary wells was

allowed to equilibrate, the wells were sampled at a low-flow rate using a peristaltic pump.

Groundwater was pumped directly into appropriate sample containers provided by the laboratory

and placed in a cooler with ice. The groundwater samples were submitted to Accutest under

proper chain-of-custody control.




4.0 REGULATORY CRITERIA

The soil analytical results were compared to the numeric criteria listed in the Connecticut DEEP

Remediation Standard Regulations (RSRs), sections 22a-133k-1 through 22a-133k-3 of the

Regulations of Connecticut State Agencies, dated June 2013, and also compared to the published

2015 numeric criteria for additional polluting substances not promulgated in the June 2013

RSRs. The RSRs were developed by the DEEP to define the remediation performance standards

for soil and groundwater to be protective of human health and the environment.

The RSRs apply specifically to sites at which remedial actions are required by the DEEP under

Chapters 445 or 446k of the Connecticut General Statutes (CGS) such as under an administrative

order, subsequent to a transfer of an establishment under CGS Section 22a-134a, and to sites that

are enrolled in a Voluntary Remediation Program under CGS Sections 22a-133x or 22a-133y.

The project limits are not currently regulated under any of these State statutes. However, BL

Companies used the numeric criteria stated above as guidance to evaluate the data regarding

concentrations of regulated compounds detected in soil. DEEP defines polluted soil as

containing any substance at a concentration above the analytical detection limit. Contaminated

soil is defined as any substance whose concentration exceeds the numeric criteria of the RSRs.

Both classifications require special handling, re-use, and disposal requirements.

Based on discussions between ConnDOT and DEEP, the numeric criteria in the RSRs do not

provide the best method for construction projects to determine whether treatment of groundwater

is necessary prior to discharge. In accordance with DEEP guidance, groundwater analytical

results were compared to the effluent limits established under both DEEP General Permits for the

Discharge of Groundwater Remediation Wastewater (to Sanitary or Surface Water) for the

purpose of groundwater management.

The following sections provide a brief summary of the soil and groundwater criteria utilized

during this Task 210 SSI.

4.1 Soil Criteria

Direct Exposure Criteria (DEC)

The DEC are designed to protect human health from risks associated with exposure to pollutants

in contaminated soil within 15 feet of the ground surface.

The RSRs provide two sets of DEC, one for residential land use (RES DEC) and another for

industrial/commercial land use (I/C DEC). The CTDEEP RSRs define “residential activity”

under CGS Section 22a-133k-1(a) to include any activity related to a residence or dwelling, or to

a school, hospital, day care center, playground, or outdoor recreation area. Remediation to the

RES DEC is required unless an ELUR is recorded that restricts residential use. For this project,

BL Companies compared the soil analytical results to both the RES DEC and I/C DEC.




Pollutant Mobility Criteria (PMC)

The PMC are designed to protect groundwater quality by reducing or eliminating the potential

for migration of pollutants to groundwater from contaminated soil. The RSRs provide two sets

of PMC based on the groundwater classification of the Site, as designated by DEEP. In a “GA”

groundwater classification area, the GA PMC apply to soil located from the ground surface to the

depth of the seasonal low water table. As the project area is in a “GA” area, BL Companies

compared the soil analytical results to the GA PMC.

4.2 Groundwater Criteria

Maximum Concentration Limits (MCLs) Established in DEEP General Permits for Discharge of

Groundwater Remediation Wastewater Directly to Surface Water or Sanitary Sewer

Maximum Concentration Limits (MCLs) established in DEEP General Permits for Discharge of

Groundwater Remediation Wastewater Directly to Surface Water or Sanitary Sewer apply to

impacted groundwater that is discharged to surface water or sanitary sewer during construction.

In order to evaluate whether construction dewatering would require treatment prior to discharge,

BL Companies compared the groundwater analytical results to the Remediation Waste Water

Discharge MCLs.




5.0 SUMMARY AND EVALUATION OF ANALYTICAL DATA

5.1 Soil Sample Analytical Results

Soil analytical results are summarized in Table 2 in Appendix B along with the regulatory

criteria. The soil analytical laboratory reports are included in Appendix D.

VOCs

All soil samples were analyzed for VOCs by EPA Method 8260. Several VOCs were detected in

soil samples B-4 (1-3’) and B-4 (7-10’) at concentrations above the GA PMC. The VOC,

tetrachloroethene, was detected in sample B-1 (0-5’) at concentrations below the RSR criteria.

VOCs were not detected in the remaining samples analyzed.

SVOCs

All soil samples were analyzed for SVOCs by EPA Method 8270. SVOCs were detected in soil

samples B-4 (1-3’), B-4 (7-10’), B-6 (0-2’), B-7 (2-4’), HA-1 (0-2’), HA-4 (0-2’), and HA-5 (0-

2’) at concentrations above the RES DEC, I/C DEC, and/or GA PMC. SVOCs were detected in

soil samples B-1 (0-5’), B-2 (0-2’), B-3 (0-2’), B-5 (0-2’), B-7 (0-2’), HA-2 (0-2’), HA-3 (0-2’),

and HA-6 (0-2’) at concentrations below the RSR criteria. SVOCs were not detected in the

remaining samples analyzed.

ETPH

All soil samples were analyzed for ETPH by CT ETPH Method. ETPH was detected in soil

samples B-4 (1-3’), B-6 (0-2’), HA-4 (0-2’), and HA-5 (0-2’) at concentrations above the RES

DEC and GA PMC of 500 milligrams per kilogram (mg/kg). ETPH was detected in soil sample

B-1 (0-5’), B-2 (0-2’), B-3 (0-2’), B-4 (7-10’), B-5 (0-2’), B-7 (0-2’), B-7 (2-4’), HA-1 (0-2’),

HA-2 (0-2’), HA-3 (0-2’), and HA-6 (0-2’) at concentrations below the RSR criteria. ETPH was

not detected in the remaining samples analyzed.

Metals

All soil samples were analyzed for total RCRA 8 metals.

• Arsenic was detected in all soil samples at concentrations ranging from 1.4 mg/kg to

5.9 mg/kg, which are below the RES DEC and I/C DEC.

• Barium was detected in all soil samples at concentrations ranging from 18.5 mg/kg to


• Cadmium was detected in soil samples B-4 (1-3’), HA-1 (0-2’), and HA-5 (0-2’) at

concentrations ranging from 0.38 mg/kg to 0.43 mg/kg, which are below the RES DEC

and I/C DEC.

• Chromium was detected in all soil samples at concentrations ranging from 4.7 mg/kg to





• Mercury was detected in ten soil samples at concentrations ranging from 0.041 mg/kg to


• Lead was detected in soil samples B-4 (1-3’) and HA-1 (0-2’) at concentrations above

the RES DEC of 400 mg/kg. Lead was detected in all the remaining soil samples at

concentrations ranging from 4 mg/kg to 263 mg/kg, which are below the RES DEC and

I/C DEC.

• Selenium and silver were not detected in any of the samples analyzed.

The soil samples were additionally analyzed for leachable RCRA 8 metals by TCLP for

comparison to the GA PMC.

• TCLP barium was detected in soil sample B-1 (0-5’), B-1 (6-8’), and B-4 (1-3’) at

concentrations below the GA PMC.

• TCLP cadmium was detected in soil sample HA-1 (0-2’) at a concentration above the

GA PMC of 0.005 mg/L. TCLP cadmium was detected in sample B-1 (0-5’) at a

concentration below the GA PMC.

• TCLP chromium was detected in soil samples B-2 (6-8’) and B-4 (7-10’) at

concentrations below the GA PMC.

• TCLP lead was detected in soil samples B-1 (0-5’), B-2 (0-2’), B-2 (6-8’), B-3 (0-2’),

B-4 (1-3’), B-4 (7-10’), B-5 (0-2’), B-6 (0-2’), HA-1 (0-2’), HA-2 (0-2’), HA-3 (0-2’),

HA-4 (0-2’), HA-5 (0-2’), and HA-6 (0-2’) at concentrations above the GA PMC.

• TCLP arsenic, mercury, selenium, and silver were not detected in any of the samples

analyzed.

• Additionally, soil represented by these samples does not contain hazardous levels of

metals.

PCBs

All soil samples were analyzed for PCBs by EPA Method 8082. PCBs were detected in soil

samples B-4 (1-3’), B-5 (0-2’), B-7 (2-4’), HA-1 (0-2’), HA-2 (0-2’), HA-3 (0-2’), HA-4 (2-4’),

and HA-5 (0-2’) at concentrations below the RSR criteria. PCBs were not detected in the

remaining samples analyzed.

Pesticides

All soil samples were analyzed for pesticides by EPA Method 8081. 4,4-DDD was detected in

soil samples B-7 (0-2’), B-7 (2-4’), HA-1 (0-2’), and HA-5 (0-2’) at concentrations above the

GA PMC of 0.003 mg/kg. 4,4-DDE was detected in soil samples B-7 (0-2’), B-7 (2-4’), HA-1

(0-2’), HA-2 (0-2’), HA-3 (0-2’), HA-4 (0-2’), and HA-6 (0-2’) at concentrations above the GA

PMC of 0.003 mg/kg. 4-DDT was detected in soil samples B-1 (0-5’), B-4 (1-3’), B-5 (0-2’),

B-6 (0-2’), B-7 (0-2’), B-7 (2-4’), HA-1 (0-2’), HA-2 (0-2’), HA-3 (0-2’), HA-4 (0-2’), HA-5

(0-2’), and HA-6 (0-2’) above the GA PMC of 0.003 mg/kg. Pesticides were not detected above

the reportable detection limits in any other soil samples.




Reactivity, Ignitability, and Corrosivity

All soil samples were analyzed for reactive cyanide and sulfide, ignitability, and pH. Based on

the laboratory results, the soil does not exhibit hazardous characteristics of reactivity,

ignitability, and corrosivity.

5.2 Groundwater Sample Analytical Results

Two groundwater samples were submitted for laboratory analysis of VOCs, SVOCs, ETPH,

PCBs, pesticides, and total and dissolved RCRA 8 metals, copper, and zinc during this Task 210

SSI. Groundwater analytical results in comparison to the General Permit Discharge MCLs are

summarized in Table 3 in Appendix B. The groundwater analytical laboratory report is

included in Appendix D.

VOCs

Benzene was detected in groundwater sample B-3/GW at a concentration below the Surface

Water and Sanitary Sewer MCLs. VOCs were not detected above the detection limits in the

groundwater sample B-1/GW.

Metals

• Total arsenic, copper, and lead were detected in groundwater sample B-1/GW at

concentrations above their respective Surface Water Discharge MCLs, but below their

respective Sanitary Sewer Discharge MCL. Dissolved arsenic, copper, and lead were

not detected in either sample.

• Total chromium and zinc were detected in groundwater sample B-1/GW at

concentrations below the DEEP General Discharge Permit MCLs. Dissolved chromium

and zinc were not detected in either sample.

• Total and dissolved barium were detected in groundwater samples B-1/GW and

B-3/GW at concentrations below the DEEP General Discharge Permit MCLs.

ETPH, SVOCs, Pesticides, and PCBs

ETPH, SVOCs, pesticides, and PCBs were not detected above the detection limits in either of the

groundwater samples.

5.3 Quality Assurance (QA)/Quality Control (QC) Results

All samples were analyzed using the DEEP Reasonable Confidence Protocol (RCP), where

applicable, and meet the RCP requirements. BL Companies also thoroughly reviewed the

laboratory RCP Certification Report to evaluate the reliability of the analytical data. The case

narratives do not indicate any non-conformances that would affect the usability of the data. All

reportable detection limits were below RSR criteria and DEEP General Discharge Permit MCLs.




Soil

Trip blank samples were prepared at the laboratory and accompanied the sample containers from

the laboratory, to the Site, and back to the laboratory. The purpose of the trip blank samples was

to evaluate the potential for cross-contamination from the surrounding environment during

transport. The trip blank samples were analyzed for VOCs. VOCs were not detected in the trip

blank samples, indicating that there was likely no cross-contamination of the samples during

transportation.

A duplicate soil sample was obtained from one randomly selected soil sample location to

evaluate the accuracy of the laboratory analytical data, measured as Relative Percent Difference

(RPD) as defined by the DEEP Laboratory Quality Assurance and Quality Control Guidance

Document, dated May 2009, revised December 2010. The duplicate was obtained from sample

HA-6 (0-2’) and analyzed for VOCs, ETPH, PCBs, pesticides, and total and TCLP RCRA 8

metals. All RPDs were lower than the 50 RPD acceptable limit for non-aqueous samples.

Groundwater

A field blank sample was collected by running de-ionized water through the sampling equipment

and into the laboratory provided sample containers. The purpose of a field blank sample is to

evaluate the potential for cross-contamination due to the sampling equipment or technique. The

field blank sample was analyzed for VOCs, SVOCs, ETPH, PCBs, pesticides, and total and

dissolved metals. No constituents were detected in the field blank sample.

Trip blank samples were prepared at the laboratory and accompanied the sample containers from

the laboratory, to the Site, and back to the laboratory. The purpose of the trip blank samples was

to evaluate the potential for cross-contamination from the surrounding environment during

transport. The trip blank samples were analyzed for VOCs. VOCs were not detected in the trip

blank samples, indicating that there was likely no cross-contamination of the samples during

transportation.

A duplicate sample was collected from B-3/GW to evaluate the accuracy of the laboratory

analytical data, measured as RPD. The duplicate sample was analyzed for VOCs, SVOCs,

ETPH, PCBs, pesticides, and total and dissolved RCRA 8 metals, copper, and zinc. All RPDs

were lower than the 30 RPD acceptable limit for aqueous samples.




6.0 POTENTIAL SOURCES OF CONTAMINATION, RECEPTORS, AND

IDENTIFIED PRELIMINARY AREAS OF ENVIRONMENTAL CONCERN

The following provides a summary of the potential sources of soil and groundwater

contamination identified during completion of this Task 210 SSI, an evaluation of potential

pathways for migration, and the identification of a preliminary Area of Environmental Concern

(AOEC) and Groundwater Area of Environmental Concern (GW AOEC) within the project area.

AOEC 1 (Site-Wide)– Contaminated Soil in the Vicinity of Borings B-1 through B-7 and

HA-1 through HA-6

ETPH, VOCs, SVOCs pesticides and lead were detected at concentrations exceeding the RES

DEC, I/C DEC, and/or GA PMC in soil samples collected at depths ranging from 0 to 10 ftbg.

The source of the contamination is likely historical uses of adjacent parcels, incidental release

from vehicles or run off from Route 69, and urban fill containing coal, ash, and slag.

Proposed work within AOEC 1 includes new road construction, relocation/reconstruction of existing

roadways and sidewalks, drainage improvements, utility relocations, and excavations in excess of

three feet in depth. Therefore, any soil removed from AOEC 1 should be reused onsite or

handled as controlled material. Potential receptors of the impacted soil include workers involved

in the construction activities, particularly during excavation activities.

GW AOEC – Contaminated Groundwater in the Vicinity of Borings B-1.

Total arsenic, copper, and lead were detected at concentrations above the Surface Water

Discharge MCL in the groundwater sample collected from boring B-1.

It is unknown whether excavations will be performed below the water table during the project.

However, based on the results of this investigation, if groundwater within the GW AOEC

requires dewatering, it will require special management or treatment. Potential receptors of the

impacted groundwater include workers involved in the dewatering activities.




7.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the analytical data collected by BL Companies, a preliminary AOEC and GW AOEC

were identified within the project area, as summarized below:

• Soil within AOEC 1 (Site-Wide) contains ETPH, SVOCs, VOCs, pesticides, and lead

at concentrations exceeding RSR numeric criteria and therefore classified as

contaminated material. This contaminated material must be managed and handled as

controlled material per ConnDOT specifications.

• Groundwater within GW AOEC contains total arsenic, copper, and lead above the

General Permit MCL for Surface Water. Therefore, groundwater within GW AOEC

will require special management or treatment if encountered during excavations for

the project.

Based on the results of this Task 210 SSI, BL Companies recommends that a Task 310 – Plans,

Specifications, and Estimates be assigned to prepare plans and specifications for the proper

management and/or disposal of contaminated materials (soil and groundwater) that may be

reused, removed, handled, transported, or disposed of during construction activities and for the

establishment of appropriate worker health and safety protocols.




8.0 LIMITATIONS

The conclusions stated above are based solely on the information described in this report. The

data and observations generated during this investigation reflect the conditions found on the

project site on the dates and at the locations specified. Where visual observations are included in

the report, they represent conditions at the time of investigation, and may not be indicative of

past or future conditions. The data cannot be extrapolated to locations on the Site that were not

tested, or to compounds for which tests were not conducted.

Latent conditions and other information may become evident in the future based on currently

unavailable evidence. BL Companies assumes no responsibility for such conditions or for the

inspection, engineering, or repair that might be required to discover or correct such factors.

Should such evidence arise, it should be forwarded to BL Companies so that additional

conclusions and recommendations may be evaluated as necessary.

This report has been completed solely for the benefit and individual use of the client. No part

thereof, nor any copy of the same, shall be used for any purpose by anyone other than the client.

No disclosure or reliance of this report may be made without the prior written consent of BL

Companies.




9.0 REFERENCES

1. State of Connecticut Department of Energy and Environmental Protection (CTDEEP),

Remediation Standard Regulations, Sections 22a-133k-1 through –3 of the Regulations of

Connecticut State Agencies, June 2013.

2. CTDEEP, “Water Quality Classifications Map of New Haven”, November 2016.

3. CTDEEP, “Recommended Numeric Criteria for Common Additional Polluting Substances

and Certain Alternative Criteria”, December 10, 2015.

4. State of Connecticut Department of Transportation, Division of Environmental Compliance,

“On-Call Contaminated Soil/Ground Water Scopes” manual, dated 2010.

5. Rogers, John, USGS, “Bedrock Geological Map of Connecticut”, dated 1985.

6. Stone, J., USGS, “Surficial Materials Map of Connecticut”, dated 1992.

APPENDIX A

FIGURES

Figure 1 – Site Location Map

ENV-01 through ENV-03 – Site Investigation Plans

SITE

LOCATION

FIGURE 1

SITE LOCATION MAP

Capacity & Operational Improvements on Route 69

In the Vicinity of Route 15 New Haven & Woodbridge, CT

Project No. 14EC0047

Base map is a reproduction of the U.S.G.S. 7.5 Minute New Haven Quadrangle – Map 95

B-2B-1

B-3

B-4

B-5

HA-1

DESIGNER/DRAFTER:

CHECKED BY:

PROJECT TITLE: TOWN:

DRAWING TITLE:

PROJECT NO.

DRAWING NO.

SHEET NO.

Filename:SHEET NO.REVISION DESCRIPTIONDATEREV.

DEPARTMENT OF TRANSPORTATION

STATE OF CONNECTICUT

SCALE 1"=40'

40 800

SCALE IN FEETOF WORK WHICH WILL BE REQUIRED.

THE CONDITIONS OF ACTUAL QUANTITIES

IN NO WAY WARRANTED TO INDICATE

INVESTIGATIONS BY THE STATE AND IS

SHEETS IS BASED ON LIMITED

QUANTITIES OF WORK, SHOWN ON THESE

THE INFORMATION, INCLUDING ESTIMATED

1/16/2017

BLOCK:

SIGNATURE/

...\DD_MSH_ENV_92-672_01.dgnPlotted Date:

CONNECTICU

T

DE

PA

RT

ME

NT

O F TRANS

PO

RT

ATI

ON

ENV-01JK

92-672JO

LAND SURVEYING

ENVIRONMENTAL

ENGINEERING

ARCHITECTURE

EN

V-02

INVESTIGATION PLAN

CAPCITY & OPERATIONAL

IN THE VICINITY OF ROUTE 15

IMPROVEMENTS ON ROUTE 69

NEW HAVENWOODBRIDGE

LEGEND

B-2

B-1

HA-1

SITE

GEOPROBE BORING

GEOPROBE BORING / GROUNDWATER SAMPLE

HAND AUGER BORING

GWAOEC

ENTIRE PROJECT AREA IS A SOIL AREA OF ENVIRONMENTAL CONCERN (AOEC)

GROUNDWATER AREA OF ENVIRONMENTAL CONCERN (GWAOEC)

HA-2

HA-3 HA-4

HA-5HA-6

B-6

DESIGNER/DRAFTER:

CHECKED BY:


DRAWING TITLE:

PROJECT NO.

DRAWING NO.

SHEET NO.




SCALE 1"=40'

40 800








1/16/2017

BLOCK:

SIGNATURE/


CONNECTICU

T

DE

PA

RT

ME

NT

O F TRANS

PO

RT

ATI

ON

ENV-02JK

92-672JO

LAND SURVEYING

ENVIRONMENTAL

ENGINEERING

ARCHITECTURE

EN

V-03

INVESTIGATION PLANIN THE VICINITY OF ROUTE 15

EN

V-01

CAPACITY & OPERANTIONAL


NEW HAVENWOODBRIDGE

LEGEND

B-2

B-1

HA-1

SITE

GEOPROBE BORING


HAND AUGER BORING


B-7

DESIGNER/DRAFTER:

CHECKED BY:


DRAWING TITLE:

PROJECT NO.

DRAWING NO.

SHEET NO.




SCALE 1"=40'

40 800








1/16/2017

BLOCK:

SIGNATURE/


CONNECTICU

T

DE

PA

RT

ME

NT

O F TRANS

PO

RT

ATI

ON

ENV-03JK

92-672JO

LAND SURVEYING

ENVIRONMENTAL

ENGINEERING

ARCHITECTURE

LEGEND

INVESTIGATION PLANIN THE VICINITY OF ROUTE 15

EN

V-02

CAPACITY & OPERATIONAL


NEW HAVENWOODBRIDGE

B-2

B-1

HA-1

SITE

GEOPROBE BORING


HAND AUGER BORING


APPENDIX B

TABLES

Table 1 – Sample Location Rationale and Selected Analyses

Table 2 – Soil Analytical Results

Table 3 – Groundwater Analytical Results

Table 1

Sample Location Rationale and Selected Analyses

Improvements on Route 69 In the Vicinity of Route 15

New Haven and Woodbridge, CT


Sample

IdentificationMatrix

Sample

IntervalLocation Rationale

VOCs

(8260)

SVOCs

(8270)ETPH

PCBs

(8082)

Pesticides

(8081)

Total

RCRA 8

Metals

TCLP

RCRA 8

Metals

Ignitability,

Reactivity, pH

0-5' X X X X X X X X





8-10' X X X X X X X X


7-10' X X X X X X X X





0-2' X X X X X X X


HA-1 Soil 0-2' Cut and sidewalk construction area X X X X X X X

HA-2 Soil 0-2' Sidewalk construction area X X X X X X X X

HA-3 Soil 0-2' Sidewalk construction area X X X X X X X


HA-5 Soil 0-2' Sidewalk construction area X X X X X X X X


Sample

IdentificationMatrix

Sample

Collection

Method

Location RationaleVOCs

(8260)

SVOCs

(8270)ETPH

PCBs

(8082)

Pesticides

(8081)

Total

RCRA 8

Metals, Cu

& Zn

B-1/GW Groundwater Grab Cut area northeast of high risk parcel

1670 Litchfield TurnpikeX X X X X X

B-3/GW Groundwater Grab Cut and drainage area west of high risk

parcel 1655 Litchfield TurnpikeX X X X X X

B-6 Soil Cut and sidewalk construction area

X

SoilAdjacent to high risk parcel 1655

Litchfield Turnpike

B-5 Soil Cut and sidewalk ramp construction area

B-7 Soil West side of southern bridge abutment

Dissolved

RCRA 8

Metals, Cu & Zn

X

B-3 SoilCut and drainage area west of high risk

parcel 1655 Litchfield Turnpike

B-4

B-1 SoilCut area northeast of high risk parcel

1670 Litchfield Turnpike

B-2 Soil Cut and drainage area

BL Companies Project No. 14EC0047 1 of 1 January 2017

Table 2

Soil Analytical Results




B-1 (0-5') B-1 (6-8') B-2 (0-2') B-2 (6-8') B-3 (0-2') B-3 (8-10') B-4 (1-3') B-4 (7-10') B-5 (0-2') B-5 (6-8') B-6 (0-2') B-6 (2-4') B-7 (0-2') B-7 (2-4') HA-1 (0-2') HA-2 (0-2') HA-3 (0-2') HA-4 (0-2') HA-5 (0-2') HA-6 (0-2')

HA-6 (0-2')

Duplicate TRIP BLANK

11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016 11/16/2016

500 2,500 500 116 ND 48.7 ND 79.5 ND 2,140 372 115 ND 620 ND 171 288 403 242 428 567 740 100 98.9 NA

VOCs (mg/kg)

Benzene 21 200 0.02 ND ND ND ND ND ND 0.19 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

n-Butylbenzene 500* 1,000* 7* ND ND ND ND ND ND 3.6 1.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

sec-Butylbenzene 500* 1,000* 7* ND ND ND ND ND ND 1.83 0.631 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Ethylbenzene 500 1,000 10.1 ND ND ND ND ND ND 0.65 4.26 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Isopropylbenzene 500* 1,000* 0.5* ND ND ND ND ND ND 5.23 1.53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

p-Isopropyltoluene 500* 1,000* 0.5* ND ND ND ND ND ND ND 0.388 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Naphthalene 1,000 2,500 5.6 ND ND ND ND ND ND 0.5 2.39 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

n-Propylbenzene 500* 1,000* 1* ND ND ND ND ND ND 16.3 5.27 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Carbon Disulfide 500* 1,000* 0.8* ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Tetrachloroethene 12 110 0.1 0.0075 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

1,2,4-Trimethylbenzene 500* 1,000* 2.8* ND ND ND ND ND ND ND 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

1,3,5-Trimethylbenzene 500* 1,000* 2.8* ND ND ND ND ND ND ND 4.35 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Total Xylenes 500* 1,000* 19.5* ND ND ND ND ND ND 0.316 10.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

SVOCs (mg/kg)

Acenaphthene 1,000* 2,500* 8.4* ND ND ND ND ND ND ND 0.111 ND ND ND ND ND 0.154 ND ND ND ND NA ND NA NA

Acenaphthylene 1,000 2,500 8.4 ND ND ND ND ND ND 10.6 ND ND ND 0.808 ND ND ND 0.826 0.121 0.361 ND 1.59 0.134 NA NA

Anthracene 1,000 2,500 40 ND ND ND ND ND ND 6.33 ND ND ND 0.326 ND ND 0.392 ND ND 0.191 ND 0.748 ND NA NA

Benzo(a)anthracene 1 7.8 1 0.326 ND ND ND ND ND 21.6 ND ND ND 1.99 ND 0.202 1.31 1.33 0.263 0.673 1.17 2.17 0.469 NA NA

Benzo(a)pyrene 1 1 1 0.388 ND ND ND ND ND 21.6 ND ND ND 2.03 ND ND 1.13 1.67 0.294 0.726 ND 2.53 0.5 NA NA

Benzo(b)fluoranthene 1 7.8 1 0.389 ND ND ND ND ND 20.1 ND ND ND 1.9 ND 0.191 1.08 1.46 0.336 0.752 1.27 2.51 0.481 NA NA

Benzo(g,h,i)perylene 8.4* 78* 1* 0.284 ND ND ND ND ND 14.4 ND ND ND 1.34 ND 0.132 0.663 1.5 0.235 0.537 1.24 1.93 0.379 NA NA

Benzo(k)fluoranthene 8.4 78 1 0.390 ND ND ND ND ND 18.6 ND ND ND 1.69 ND 0.161 0.96 1.42 0.282 0.675 1.22 2.37 0.473 NA NA

Carbazole 31 290 0.2 ND ND ND ND ND ND 2.84 ND ND ND ND ND ND 0.228 ND ND ND ND ND ND NA NA

Chrysene 84* 780* 1* 0.436 ND ND ND ND ND 29.5 ND ND ND 2.47 ND 0.226 1.46 1.71 0.371 0.956 1.53 3.02 0.565 NA NA

Dibenz(a,h)anthracene 1* 1* 1* ND ND ND ND ND ND 3.65 ND ND ND 0.334 ND ND 0.177 ND ND 0.133 ND ND ND NA NA

Dibenzofuran 68* 1,000* 0.2* ND ND ND ND ND ND 1.36 ND ND ND ND ND ND 0.111 ND ND ND ND ND ND NA NA

Fluoranthene 1,000 2,500 5.6 0.718 ND 0.129 ND 0.119 ND 59.5 0.133 0.184 ND 3.97 ND 0.408 3.1 2.95 0.567 1.46 2.62 4.38 1.09 NA NA

Fluorene 1,000 2,500 5.6 ND ND ND ND ND ND 5.28 0.152 ND ND ND ND ND 0.138 ND ND ND ND ND ND NA NA

Indeno(1,2,3-cd)pyrene 1* 7.8* 1* ND ND ND ND ND ND 14.1 ND ND ND 1.29 ND ND 0.674 ND ND 0.508 ND 1.88 0.362 NA NA

2-Methylnaphthalene 270* 1,000* 0.56* ND ND ND ND ND ND 1.19 5.44 ND ND ND ND ND ND ND ND ND ND ND ND NA NA

Naphthalene 1,000 2,500 5.6 ND ND ND ND ND ND ND 7.69 ND ND ND ND ND ND ND ND ND ND ND ND NA NA

Phenanthrene 1,000 2,500 4 0.395 ND ND ND ND ND 40.3 0.289 ND ND 1.39 ND 0.226 2.27 1.32 0.24 0.719 1.19 1.91 0.447 NA NA

Pyrene 1,000 2,500 4 0.738 ND 0.136 ND 0.121 ND 57.0 ND 0.189 ND 4.33 ND 0.386 2.83 2.74 0.553 1.53 2.46 4.28 0.918 NA NA

PCBs (mg/kg) 1 10 -- ND ND ND ND ND ND 0.06 ND 0.0321 ND ND ND ND 0.0837 0.104 0.1015 0.0623 0.114 0.047 ND ND NA

Pesticides (mg/kg)

4,4'-DDD 1.8* 17* 0.003* ND ND ND ND ND ND ND ND ND ND ND ND 0.0448 0.0093 0.0051 ND ND ND 0.0079 ND ND NA

4,4'-DDE 1.8* 17* 0.003* ND ND ND ND ND ND ND ND ND ND ND ND 0.278 0.0878 0.0643 0.05 0.0166 0.0094 ND 0.0128 0.0109 NA

4,4'-DDT 1.8* 17* 0.003* 0.0131 ND ND ND ND ND 0.0182 ND 0.0091 ND 0.0153 ND 0.575 0.190 0.263 0.0527 0.0642 0.197 0.0277 0.0216 0.021 NA

Total RCRA 8 Metals (mg/kg)

Arsenic 10 10 -- 3.7 1.9 1.7 1.7 1.4 1.7 3.9 1.8 3.7 2.1 3.9 1.5 5.7 5.8 2.1 5.9 2.8 2.2 4.6 4 3.8 NA

Barium 4,700 140,000 -- 90.1 37.9 18.5 35.8 27 28 68.3 35.5 74.2 18.7 66.1 21.6 74 52.7 40.5 72.8 41.8 27.6 42.4 61.6 52.6 NA

Cadmium 34 1,000 -- ND ND ND ND ND ND 0.43 ND ND ND ND ND ND ND 0.43 ND ND ND 0.38 ND ND NA

Chromium, Total 100** 100** -- 22.3 11.1 10.6 14.8 10.6 17.2 15.1 27.9 15.7 4.7 11.3 10.9 16.4 13.7 12.4 14.6 14 20.6 16.6 15.6 16.6 NA

Lead 400 1,000 -- 94.2 4.9 19.5 27.4 5.8 4.4 543 7.6 59.5 4 90.5 4.2 35.9 27.2 598 153 263 185 222 67.3 78.8 NA

Mercury 20 610 -- 0.28 ND ND ND ND ND 0.082 ND 0.12 ND 0.047 ND 1.6 0.67 ND 0.076 0.041 ND 0.12 0.047 0.056 NA

TCLP RCRA 8 Metals (mg/L)

Barium -- -- 1 0.68 0.56 ND ND ND ND 0.68 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Cadmium -- -- 0.005 0.0042 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.006 ND ND ND ND ND ND NA

Chromium -- -- 0.05 ND ND ND 0.013 ND ND ND 0.022 ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Lead -- -- 0.015 0.29 ND 0.19 0.03 0.017 ND 1.5 0.031 0.047 ND 0.017 ND ND ND 1.3 0.058 0.31 0.5 0.081 0.042 0.040 NA

Ignitability (Flashpoint) (degrees F) -- -- -- >230 >230 >230 >230 >230 >230 >230 >230 >230 >230 >230 >230 NA >230 NA >230 NA NA >230 NA NA NA

pH (SU) -- -- -- 7.6 7.7 7.5 7.2 7 6.9 7 7.8 7 8.7 7.7 7.8 NA 6.8 NA 7 NA NA 7.2 NA NA NA

Reactivity Cyanide (mg/kg) -- -- -- ND ND ND ND ND ND ND ND ND ND ND ND NA ND NA ND NA NA ND NA NA NA

Reactivity Sulfide (mg/kg) -- -- -- ND ND ND ND ND ND ND ND ND ND ND ND NA ND NA ND NA NA ND NA NA NA

CTDEEP = Connecticut Department of Energy and Environmental Protection

RSR = Remediation Standard Regulations

RES DEC = Residential Direct Exposure Criteria

I/C DEC = Industrial-Commercial Direct Exposure Criteria

GA PMC = GA Pollutant Mobility Criteria

mg/kg = milligrams per kilogram

mg/L = milligrams per liters

ND = Not detected above laboratory reporting limits

NA = Not Analyzed

* = published 2015 numeric criteria for additional polluting substances not established in 2013 RSRs

** = hexavalent chromium criteria

-- = criteria does not apply

Only compounds detected are listed in table

Shade/Bold

Concentration of Compound in Sample

= Exceeds Numeric Criteria

Parameters

CTDEEP RSR

Numeric Criteria

I/C DECRES DEC GA PMC

ETPH (mg/kg)

BL Companies Project No. 14EC0047 page 1 of 1 January 2017

Table 3

Groundwater Analytical Results




B-1/GW B-3/GW

B3/GW

Duplicate

Equipment

Blank Trip Blank

11/16/16 11/16/16 11/16/16 11/16/16 11/16/16

5,000 100,000 ND ND ND ND NA

50 5,000 ND 0.6 0.59 ND ND

Benzene NE NE ND 0.6 0.59 ND ND

Total PAHs 5 500 ND ND ND ND NA

PCBs (µg/L) 0.1 1 ND ND ND ND NA

* * ND ND ND ND NA

Total RCRA 8 Metals (µg/L)

Arsenic 0.021 100 9.5 ND ND ND NA

Barium NE 5,000 421 72.2 70.3 ND NA

Chromium 342 1,000 46.3 ND ND ND NA

Copper 48 1,000 120 ND ND ND NA

Lead 9.8 100 25.9 ND ND ND NA

Zinc 322 1,000 67 ND ND ND NA

Dissolved RCRA 8 Metals (µg/L)

Barium NE 5,000 72.5 60.9 61.2 ND NA

MCL = maximum concentration limits listed in the DEEP General Permit for Discharge of Remediation Wastewater

µg/L = micrograms per liter

ND = Not Detected above the Laboratory Reporting Limit

NE = None Established

NA = Not Analyzed

* = Limits Established for Individual Compounds

Only compounds detected are listed in tableShade & Bold

General Permit MCLs

Surface WaterSanitary

Sewer

Concentration of Compound in Sample

ETPH (ug/L)

Parameters

Total VOCs (µg/L)

= Exceeds General Discharge Permit MCL

SVOCs (µg/L)

Pesticides (µg/L)

BL Companies Project No. 14EC0047 January 2017

APPENDIX C

BORING LOGS

GRASS/TOPSOIL.Brown fine to medium SAND and SILT, some fine tocoarse gravel.

Brown SILT, trace fine to medium gravel.

Brown fine to coarse SAND, some fine to coarse gravel,trace silt.Red fine to coarse SAND, some fine to medium gravel,trace silt. Saturated at 7 ftbg.

Red/brown fine to coarse SAND, trace fine to mediumgravel and silt, saturated.

End of exploration, temporary well set at 14 ftbg.

5

10

15

30

36

54

0.0

0.0

0.0

Sample collected at 0-5

ftbg.


ftbg.

Temporary well screened

4-14 ftbg and removed

after sampling.

B-1/GW

11/16/16

14EC0047

Doug Miller/ Wes Johnson

Date:

Borehole Dia: 2 Inches

Drill Rig: Geotech 7822DT

Architecture

Engineering

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Proportions Used: Trace = 1 to 10%, Little = 10 to 20%, Some = 20 to 30%, And = 30 to 50%

Drill Method: Direct Push

PID

Environmental Science

Land Surveying

BORING LOG Boring No.:

Project No.:

Site Name: Route 69 Improvements

Weather: Sunny, 50°F

Boring Co.:

GRASS/TOPSOIL.Brown SILT and SAND.

Brown fine to coarse SAND and GRAVEL, trace silt.

Brown fine to coarse SAND, some fine to coarse gravel,trace silt.

Red/brown fine to coarse SAND and GRAVEL, trace silt.Damp at 9.5 ftbg.

End of exploration at 10 ftbg.

5

10

15

48

48

0.0

0.0


ftbg.


ftbg.

B-2

11/16/16

14EC0047


Date:



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PID


Land Surveying


Project No.:



Boring Co.:

GRASS/TOPSOIL.Brown SILT and fine SAND.

Brown fine to coarse SAND, some fine to coarse roundedgravel.

Brown fine to coarse SAND, some fine to coarse roundedgravel, trace cobbles.Red/brown fine to coarse SAND, saturated at 9 ftbg.

Red/brown fine to coarse SAND, some fine to coarserounded gravel, saturated.

Red/brown fine to medium SAND, saturated.

End of exploration, temporary well set at 15 ftbg.

5

10

15

42

48

40

0.0

0.0

0.0


ftbg.


ftbg.

Temporary well screened

5-15 ftbg and removed

after sampling.

B-3/GW

11/16/16

14EC0047


Date:



Architecture

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PID


Land Surveying


Project No.:



Boring Co.:

ASPHALTBrown fine to medium SAND and SILT, some fine tomedium gravel.

Dark brown SILT, some fine SAND, trace fine gravel,strong petroleum odor and staining.

Brown SILT and fine to coarse SAND, some fine to coarsegravel, strong petroleum odor and staining.

Brown fine to coarse SAND and GRAVEL, trace silt,damp at 9.5 ftbg. Petroleum odor and staining.


5

10

15

38

30

2,321

300


ftbg.


ftbg.

B-4

11/16/16

14EC0047


Date:



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Remarks



PID


Land Surveying


Project No.:



Boring Co.:

GRASS/TOPSOIL.Brown SILT, some fine sand, trace fine to medium gravel.

COBBLES.

Red/brown fine to coarse SAND, some fine to coarsegravel, trace silt. Saturated at 8 ftbg.


5

10

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20

37

36

0.0

0.0


ftbg.


ftbg.

B-5

11/16/16

14EC0047


Date:



Architecture

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PID


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Project No.:



Boring Co.:

GRASS/TOPSOIL.Brown SILT, some fine to medium sand, trace fine tocoarse gravel.

Brown fine to medium SAND and SILT, trace fine tocoarse gravel.


5

10

15

29

0.0


ftbg.


ftbg.

B-6

11/16/16

14EC0047


Date:



Architecture

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PID


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Project No.:



Boring Co.:

GRASS/TOPSOIL.Brown/dark brown fine to medium SAND, trace coal, slag,and fine to coarse gravel.


5

10

15

48

0.0


ftbg.


ftbg.

B-7

11/16/16

14EC0047


Date:


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Drill Method: Air Knife

PID


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Project No.:



Boring Co.:

APPENDIX D

LABORATORY ANALYTICAL REPORTS

12/02/16

Technical Report for

BL Companies

Route 69 Improvements, New Haven, CT

14EC0047

SGS Accutest Job Number: MC48821

Sampling Date: 11/16/16

Report to:

BL Companies355 Research ParkwayMeriden, CT [email protected]

ATTN: Joy Kloss

Total number of pages in report:

Certifications: MA (M-MA136,SW846 NELAC) CT (PH-0109) NH (250210) RI (00071) FL (E87579) NY (11791)

NJ (MA926) PA (6801121) ND (R-188) CO (MA00136) MN (11546AA) NC (653) IL (002337) WI (399080220)

DoD ELAP (L-A-B L2235)

This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.

Test results relate only to samples analyzed.

New England • 50 D'Angelo Drive • Building 1 • Marlborough, MA 01752 • tel: 508-481-6200 • fax: 508-481-7753 • http://www.accutest.com

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Program

and/or state specific certification programs as applicable.

Client Service contact: Jeremy Vienneau 508-481-6200

H. (Brad) MadadianLab Director

New England 12/02/16

e-Hardcopy 2.0Automated Report

555

SGS Accutest is the sole authority for authorizing edits or modifications to this document.Unauthorized modification of this report is strictly prohibited.

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Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 5Section 2: Case Narrative/Conformance Summary .............................................................. 10Section 3: Summary of Hits .................................................................................................... 19Section 4: Sample Results ........................................................................................................ 32

4.1: MC48821-1: B-1(0-5') .................................................................................................. 334.2: MC48821-1A: B-1(0-5') ............................................................................................... 444.3: MC48821-2: B-1(6-8') .................................................................................................. 454.4: MC48821-2A: B-1(6-8') ............................................................................................... 564.5: MC48821-3: B-2(0-2') .................................................................................................. 574.6: MC48821-3A: B-2(0-2') ............................................................................................... 684.7: MC48821-4: B-2(6-8') .................................................................................................. 694.8: MC48821-4A: B-2(6-8') ............................................................................................... 804.9: MC48821-5: B-3(0-2') .................................................................................................. 814.10: MC48821-5A: B-3(0-2') ............................................................................................. 924.11: MC48821-6: B-3(8-10') .............................................................................................. 934.12: MC48821-6A: B-3(8-10') ........................................................................................... 1044.13: MC48821-7: B-4(1-3') ................................................................................................ 1054.14: MC48821-7A: B-4(1-3') ............................................................................................. 1164.15: MC48821-8: B-4(7-10') .............................................................................................. 1174.16: MC48821-8A: B-4(7-10') ........................................................................................... 1284.17: MC48821-9: B-5(0-2') ................................................................................................ 1294.18: MC48821-9A: B-5(0-2') ............................................................................................. 1404.19: MC48821-10: B-5(6-8') .............................................................................................. 1414.20: MC48821-10A: B-5(6-8') ........................................................................................... 1524.21: MC48821-11: B-6(0-2') .............................................................................................. 1534.22: MC48821-11A: B-6(0-2') ........................................................................................... 1644.23: MC48821-12: B-6(2-4') .............................................................................................. 1654.24: MC48821-12A: B-6(2-4') ........................................................................................... 1764.25: MC48821-13: B-7(0-2') .............................................................................................. 1774.26: MC48821-13A: B-7(0-2') ........................................................................................... 1874.27: MC48821-14: B-7(2-4') .............................................................................................. 1884.28: MC48821-14A: B-7(2-4') ........................................................................................... 1994.29: MC48821-15: HA-1(0-2') ........................................................................................... 2004.30: MC48821-15A: HA-1(0-2') ........................................................................................ 2104.31: MC48821-16: HA-2(0-2') ........................................................................................... 2114.32: MC48821-16A: HA-2(0-2') ........................................................................................ 2224.33: MC48821-17: HA-3(0-2') ........................................................................................... 2234.34: MC48821-17A: HA-3(0-2') ........................................................................................ 2334.35: MC48821-18: HA-4(0-2') ........................................................................................... 2344.36: MC48821-18A: HA-4(0-2') ........................................................................................ 2444.37: MC48821-19: HA-5(0-2') ........................................................................................... 2454.38: MC48821-19A: HA-5(0-2') ........................................................................................ 256

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4.39: MC48821-20: HA-6(0-2') ........................................................................................... 2574.40: MC48821-20A: HA-6(0-2') ........................................................................................ 2674.41: MC48821-21: HA-6(0-2')DUP ................................................................................... 2684.42: MC48821-21A: HA-6(0-2')DUP ................................................................................ 2754.43: MC48821-22: B-1/GW ............................................................................................... 2764.44: MC48821-22F: B-1/GW ............................................................................................. 2864.45: MC48821-23: B-3/GW ............................................................................................... 2874.46: MC48821-23F: B-3/GW ............................................................................................. 2974.47: MC48821-24: B-3/GW DUP ...................................................................................... 2984.48: MC48821-24F: B-3/GW DUP .................................................................................... 3084.49: MC48821-25: TRIP BLANK ..................................................................................... 3094.50: MC48821-26: TRIP BLANK ..................................................................................... 3124.51: MC48821-26A: TRIP BLANK ................................................................................... 3154.52: MC48821-27: EQUIPMENT BLANK ....................................................................... 3184.53: MC48821-27F: EQUIPMENT BLANK ..................................................................... 328

Section 5: Misc. Forms ............................................................................................................ 3295.1: Chain of Custody ........................................................................................................... 3305.2: RCP Form ...................................................................................................................... 3345.3: Sample Tracking Chronicle ........................................................................................... 3355.4: QC Evaluation: CT RCP Limits .................................................................................... 349

Section 6: GC/MS Volatiles - QC Data Summaries .............................................................. 3866.1: Method Blank Summary ................................................................................................ 3876.2: Blank Spike Summary ................................................................................................... 3996.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 4056.4: Internal Standard Area Summaries ................................................................................ 4116.5: Surrogate Recovery Summaries ..................................................................................... 417

Section 7: GC/MS Semi-volatiles - QC Data Summaries ..................................................... 4207.1: Method Blank Summary ................................................................................................ 4217.2: Blank Spike Summary ................................................................................................... 4307.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 4337.4: Internal Standard Area Summaries ................................................................................ 4397.5: Surrogate Recovery Summaries ..................................................................................... 445

Section 8: GC Semi-volatiles - QC Data Summaries ............................................................ 4488.1: Method Blank Summary ................................................................................................ 4498.2: Blank Spike Summary ................................................................................................... 4598.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 4678.4: DDT/Endrin Breakdown Checks ................................................................................... 4698.5: Surrogate Recovery Summaries ..................................................................................... 474

Section 9: Metals Analysis - QC Data Summaries ................................................................ 4809.1: Prep QC MP27038: As,Ba,Cd,Cr,Cu,Pb,Se,Ag,Zn ....................................................... 4819.2: Prep QC MP27041: As,Ba,Cd,Cr,Cu,Pb,Se,Ag,Zn ....................................................... 4879.3: Prep QC MP27043: As,Ba,Cd,Cr,Pb,Se,Ag .................................................................. 493

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9.4: Prep QC MP27045: Hg .................................................................................................. 5059.5: Prep QC MP27050: Hg .................................................................................................. 5109.6: Prep QC MP27053: As,Ba,Cd,Cr,Pb,Se,Ag .................................................................. 5149.7: Prep QC MP27055: As,Ba,Cd,Cr,Pb,Se,Ag .................................................................. 5229.8: Prep QC MP27057: Hg .................................................................................................. 5329.9: Prep QC MP27058: As,Ba,Cd,Cr,Pb,Se,Ag .................................................................. 5369.10: Prep QC MP27059: Hg ................................................................................................ 5469.11: Prep QC MP27060: Hg ................................................................................................ 550

Section 10: General Chemistry - QC Data Summaries ........................................................ 55310.1: Method Blank and Spike Results Summary ................................................................ 55410.2: Duplicate Results Summary ........................................................................................ 555

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Sample Summary

BL CompaniesJob No: MC48821

Route 69 Improvements, New Haven, CTProject No: 14EC0047

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

MC48821-1 11/16/16 00:00 DSM 11/18/16 SO Soil B-1(0-5')

MC48821-1A 11/16/16 00:00 DSM 11/18/16 SO Soil B-1(0-5')

MC48821-2 11/16/16 00:00 DSM 11/18/16 SO Soil B-1(6-8')

MC48821-2A 11/16/16 00:00 DSM 11/18/16 SO Soil B-1(6-8')

MC48821-3 11/16/16 00:00 DSM 11/18/16 SO Soil B-2(0-2')

MC48821-3A 11/16/16 00:00 DSM 11/18/16 SO Soil B-2(0-2')

MC48821-4 11/16/16 00:00 DSM 11/18/16 SO Soil B-2(6-8')

MC48821-4A 11/16/16 00:00 DSM 11/18/16 SO Soil B-2(6-8')

MC48821-5 11/16/16 00:00 DSM 11/18/16 SO Soil B-3(0-2')

MC48821-5A 11/16/16 00:00 DSM 11/18/16 SO Soil B-3(0-2')

MC48821-6 11/16/16 00:00 DSM 11/18/16 SO Soil B-3(8-10')

MC48821-6A 11/16/16 00:00 DSM 11/18/16 SO Soil B-3(8-10')

MC48821-7 11/16/16 00:00 DSM 11/18/16 SO Soil B-4(1-3')

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

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Sample Summary(continued)




MC48821-7A 11/16/16 00:00 DSM 11/18/16 SO Soil B-4(1-3')

MC48821-8 11/16/16 00:00 DSM 11/18/16 SO Soil B-4(7-10')

MC48821-8A 11/16/16 00:00 DSM 11/18/16 SO Soil B-4(7-10')

MC48821-9 11/16/16 00:00 DSM 11/18/16 SO Soil B-5(0-2')

MC48821-9A 11/16/16 00:00 DSM 11/18/16 SO Soil B-5(0-2')

MC48821-10 11/16/16 00:00 DSM 11/18/16 SO Soil B-5(6-8')

MC48821-10A11/16/16 00:00 DSM 11/18/16 SO Soil B-5(6-8')

MC48821-11 11/16/16 00:00 DSM 11/18/16 SO Soil B-6(0-2')

MC48821-11A11/16/16 00:00 DSM 11/18/16 SO Soil B-6(0-2')

MC48821-12 11/16/16 00:00 DSM 11/18/16 SO Soil B-6(2-4')

MC48821-12A11/16/16 00:00 DSM 11/18/16 SO Soil B-6(2-4')

MC48821-13 11/16/16 00:00 DSM 11/18/16 SO Soil B-7(0-2')

MC48821-13A11/16/16 00:00 DSM 11/18/16 SO Soil B-7(0-2')


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MC48821-14 11/16/16 00:00 DSM 11/18/16 SO Soil B-7(2-4')

MC48821-14A11/16/16 00:00 DSM 11/18/16 SO Soil B-7(2-4')

MC48821-15 11/16/16 00:00 DSM 11/18/16 SO Soil HA-1(0-2')

MC48821-15A11/16/16 00:00 DSM 11/18/16 SO Soil HA-1(0-2')

MC48821-16 11/16/16 00:00 DSM 11/18/16 SO Soil HA-2(0-2')

MC48821-16A11/16/16 00:00 DSM 11/18/16 SO Soil HA-2(0-2')

MC48821-17 11/16/16 00:00 DSM 11/18/16 SO Soil HA-3(0-2')

MC48821-17A11/16/16 00:00 DSM 11/18/16 SO Soil HA-3(0-2')

MC48821-18 11/16/16 00:00 DSM 11/18/16 SO Soil HA-4(0-2')

MC48821-18A11/16/16 00:00 DSM 11/18/16 SO Soil HA-4(0-2')

MC48821-19 11/16/16 00:00 DSM 11/18/16 SO Soil HA-5(0-2')

MC48821-19A11/16/16 00:00 DSM 11/18/16 SO Soil HA-5(0-2')

MC48821-20 11/16/16 00:00 DSM 11/18/16 SO Soil HA-6(0-2')


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MC48821-20A11/16/16 00:00 DSM 11/18/16 SO Soil HA-6(0-2')

MC48821-21 11/16/16 00:00 DSM 11/18/16 SO Soil HA-6(0-2')DUP

MC48821-21A11/16/16 00:00 DSM 11/18/16 SO Soil HA-6(0-2')DUP

MC48821-22 11/16/16 00:00 DSM 11/18/16 AQ Ground Water B-1/GW

MC48821-22F11/16/16 00:00 DSM 11/18/16 AQ Groundwater Filtered B-1/GW

MC48821-23 11/16/16 00:00 DSM 11/18/16 AQ Ground Water B-3/GW

MC48821-23F11/16/16 00:00 DSM 11/18/16 AQ Groundwater Filtered B-3/GW

MC48821-24 11/16/16 00:00 DSM 11/18/16 AQ Ground Water B-3/GW DUP

MC48821-24F11/16/16 00:00 DSM 11/18/16 AQ Groundwater Filtered B-3/GW DUP

MC48821-25 11/16/16 00:00 DSM 11/18/16 AQ Trip Blank Water TRIP BLANK

MC48821-26 11/16/16 00:00 DSM 11/18/16 SO Trip Blank Methanol TRIP BLANK

MC48821-26A11/16/16 00:00 DSM 11/18/16 SO Trip Blank Soil TRIP BLANK

MC48821-27 11/16/16 00:00 DSM 11/18/16 AQ Equipment Blank EQUIPMENT BLANK


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MC48821-27F11/16/16 00:00 DSM 11/18/16 AQ Equip Blank Filtered EQUIPMENT BLANK


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1

25 Sample(s), 3 Trip Blank(s) were collected on 11/16/2016 and were received at SGS Accutest New England on 11/18/2016 properly preserved, at 3 Deg. C and intact. These Samples received a job number of MC48821. A listing of the Laboratory Sample ID, Client Sample ID and dates of collection are presented in the Results Summary Section of this report.

Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more information, please refer to QC summary pages.

Client: BL Companies

Site: Route 69 Improvements, New Haven, CT

Job No MC48821

Report Date 12/2/2016 11:33:30 A

SAMPLE DELIVERY GROUP CASE NARRATIVE

Volatiles by GCMS By Method SW846 8260CMatrix: AQ Batch ID: MSV1905

All samples were analyzed within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Minimum response factor for 2-Butanone less than 0.05 in MSV1890-ICC1890.

Blank Spike Duplicate is being reported but is not required for RCP criteria.

MSV1905-BS for Chloromethane: Outside control limits. Associated samples are non-detect for this compound.

Continuing Calibration for Methylene chloride, freon-113, 1,1-dichloroethene, trans-1,2-Dichloroethene, carbon disulfide, bromoform, Trans-1,4-Dichloro-2-Butene, 1,2-dibromo-3-chloropropane exceed 20% difference (biased low). Reporting Limit response verified by low-level standard.

Continuing calibration check standard for chloromethane, vinyl chloride, bromomethane, trichlorofluoromethane exceeds 20% Difference (biased high). Associated samples are non-detect for this compound.

Initial Calibration Verification MSV1890-ICV1890 for Acetone, 2-butanone, 2-hexanone exceed 30% difference (biased high). Sample result may be biased high or non-detect for this compound.

MSV1905-BS for Acetone, Bromoform, Bromomethane, 2-Butanone (MEK), Dichlorodifluoromethane, Freon 113, 2-Hexanone, Trichlorofluoromethane, Vinyl chloride: Outside RCP control limits.

Matrix: SO Batch ID: MSL4388



Blank Spike Recovery(s) for 1,2,4-Trimethylbenzene are outside in-house control limits, but within RCP control limits.


Continuing Calibration for 1,1-Dichloroethene exceed 20% Difference (biased low). Reporting Limit response verified by low-level standard.

Minimum response factor for Acetone, 2-Butanone is less than 0.05 in MSL4387-ICC4387.

Continuing Calibration for 1,2,4-Trimethylbenzene exceed 20% Difference (biased high). Result may be biased high or sample is non-detect for this compound..

MSL4388-BS for Dichlorodifluoromethane: Outside RCP control limits.

Matrix: SO Batch ID: MSM2944



Continuing Calibration for freon-113, 1,1-dichloroethene, carbon disulfide exceed 20% Difference (biased low). Reporting Limit response verified by low-level standard.

MSM2944-BS for Methylene chloride: Outside in house control limits, but within RCP control limits. Associated samples are non-detect for this compound.

MC48821-13,14,15,16 for Dibromofluoromethane: Outside RCP control limits.

MC48821-1,3,9,11,13,14,15,16 has internal standards outside control limits due to possible matrix interference. Confirmed by reanalysis.


Friday, December 02, 2016 Page 1 of 9

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Volatiles by GCMS By Method SW846 8260CMatrix: SO Batch ID: MSM2945

MC48821-1,3,9,11,13,14,15,16 has internal standards outside control limits due to possible matrix interference. Confirmed by reanalysis.

MC48821-1,3,9,11,13,14,15,16: Confirmation run for internal standard areas.




MC48821-17,18,19,20,21 has internal standards outside control limits due to possible matrix interference. Confirmed by reanalysis.

Continuing Calibration for dichlorodifluoromethane, Chloromethane, bromomethane, chloroethane exceed 20% Difference (biased low). Reporting Limit response verified by low-level standard.

MC48821-19 for 4-Bromofluorobenzene: Outside control limits due to possible matrix interference. Confirmed by reanalysis.

Continuing Calibration for Acetone outside of acceptance criteria (biased high). Associated samples are non-detect for this compound.

MSM2946-BS for 2-Butanone (MEK): Outside control limits. Associated samples are non-detect for this compound.

MC48821-18 for 4-Bromofluorobenzene: Outside RCP control limits.

MSM2946-BS for Acetone: Outside RCP control limits.


MC48821-17,18,19,20,21 has internal standards outside control limits due to possible matrix interference. Confirmed by reanalysis.

MC48821-17: Confirmation run for internal standard areas.


MC48821-19: Confirmation run.




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Extractables by GCMS By Method SW846 8270DMatrix: AQ Batch ID: OP49189

All samples were extracted within the recommended method holding time.



Blank Spike Recovery(s) for 1,2,4-Trichlorobenzene, 2,4-Dinitrotoluene, 2,6-Dinitrotoluene, 4-Bromophenyl phenyl ether, 4-Chlorophenyl phenyl ether, Di-n-butyl phthalate, Diethyl phthalate, Hexachlorobutadiene, Hexachloroethane are outside control limits. Meets program technical requirements.

Continuing Calibration MSW1264-CC1235 for Hexachlorocyclopentadiene, bis(2-Chloroethyl)ether, bis(2-chloroisopropyl)ether exceed 20% Difference (biased low). Reporting Limit Response verified by low-level standard.

Quadratic regression is employed for initial calibration standard MSW1235-ICC1235 for 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol.


Matrix: SO Batch ID: OP49183





Quadratic regression is employed for initial calibration standard MSR1877-ICC1877 for 2,4-Dinitrophenol

Continuing Calibration MSR1897-CC1877 for 4-Nitrophenol, Pentachlorophenol exceed 20% Difference (biased low). Reporting Limit Response verified by low-level standard.

OP49183-BS for Aniline, 4-Chloroaniline, 3,3'-Dichlorobenzidine: Outside RCP control limits.





Blank Spike Recovery(s) for 4-Chlorophenyl phenyl ether, Diethyl phthalate, Dimethyl phthalate are outside control limits.

MC48821-18: Elevated RL due to dilution required for matrix interference.



Continuing Calibration MSR1900-CC1877 for Hexachlorocyclopentadiene, 2,4-Dinitrophenol, 4,6-Dinitro-2-methylphenol, Pentachlorophenol exceed 20% Difference (biased low). Reporting Limit Response verified by low-level standard.

Extractables by GCMS By Method SW846 8270D BY SIMMatrix: AQ Batch ID: OP49190




Only PAHs requested.

Quadratic regression is employed for initial calibration standard MSI3929-ICC3929 for Benzo[b]fluoranthene, Benzo[a]pyrene, Indeno[1,2,3-cd]pyrene, Dibenz[a,h]anthracene.


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Extractables by GC By Method CT-ETPH 7/06Matrix: AQ Batch ID: OP49181

















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Extractables by GC By Method SW846 8081BMatrix: AQ Batch ID: OP49191




Quadratic regression is employed for initial calibration standard GBE2691-ICC2691, signal #1 for 4,4'-DDT, Methoxychlor.

OP49191-MB for Decachlorobiphenyl: Outside control limits.

OP49191-BS for delta-BHC, Endrin aldehyde; OP49191-BS and MC48821-22,-23,-24,-27 for Decachlorobiphenyl (sig#1) : Outside RCP control limits.

Continuing calibration check standard GBE2691-ECC2691, signal #1 for Alpha-BHC, Beta-BHC, Aldrin, Heptachlor Epoxide, Dieldrin, Endrin exceed 20% Difference (biased high). Associated samples are non-detect for this compound.





Quadratic regression is employed for initial calibration standard GBE2693-ICC2693, signal #1 for Heptachlor, Endosulfan-I, Endrin, Methoxychlor, Endrin Keton and signal #2 for 4,4'-DDT, Methoxychlor.

MC48821-17 for 4,4'-DDT: Confirmation value >40% RPD.

MC48821-20 for 4,4'-DDE: Confirmation value >40% RPD.

MC48821-19 for Decachlorobiphenyl: Outside control limits due to possible matrix interference.


MC48821-11 for Decachlorobiphenyl: Outside control limits due to possible matrix interference.




Calibration check standard GBE2693-ECC2693 for 4,4'-DDT, Methoxychlor exceed 20% Difference. Outside control limits due to possible residual matrix interference. Confirmed by reanalysis.

OP49201-BS for delta-BHC; MC48821-14,-15,-18 for Decachlorobiphenyl (sig#2): Outside RCP control limits.

Calibration check standard GBE2693-CC2693, signal #1, file BE53530 for Endosulfan Sulfate exceed 20% difference. Endosulfan Sulfate is reported from singl #2.





Quadratic regression is employed for initial calibration standard GBE2694-ICC2694, signal #1 for Endrin, Endosulfan-I, Endrin Aldehyde, Methoxychlor, Endrin Keton.


MC48821-1,7 for Decachlorobiphenyl: Outside control limits due to possible matrix interference.

MC48821-21 for 4,4'-DDT: Confirmation value >40% RPD.

Continuing calibration check standard GBE2694-CC2694 (signal #1), file BE53559, BE53564 for Endrin Aldehyde, Endosulfan Sulfate, Methoxychlor, 4,4'-DDT, DCB exceed 20% Difference. Outside control limits due to possible residual matrix interference. Confirmed by reanalysis.


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Extractables by GC By Method SW846 8082AMatrix: AQ Batch ID: OP49179




Continuing calibration check standard GBK1999-CC1999, file BK63238, signal #1 for DCB exceed 20% difference.Target analytes are satisfactory.





MC48821-16 for Aroclor 1254: Estimated value due to the presence of other Aroclor pattern.Confirmation value >40% RPD





MC48821-9 for Aroclor 1260: Confirmation value >40% RPD.

Continuing calibration check standard GBK2004-ECC2002, signal #1 for DCB exceed 20% difference.Target analytes are satisfactory.


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Metals By Method SW846 6010CMatrix: AQ Batch ID: MP27038

All samples were digested within the recommended method holding time.



Sample(s) MC48790-3SDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Chromium, Copper are outside control limits for sample MP27038-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

Only selected metals requested.

Matrix: AQ Batch ID: MP27041




Sample(s) MC48764-6FSDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Chromium, Zinc are outside control limits for sample MP27041-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).


Matrix: LEACHATE Batch ID: MP27055




Sample(s) MC48821-1AMS, MC48821-1AMSD, MC48821-1ASDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Cadmium, Chromium, Selenium are outside control limits for sample MP27055-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).






Sample(s) MC48821-21AMS, MC48821-21AMSD, MC48821-21ASDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Cadmium, Chromium, Lead, Selenium are outside control limits for sample MP27058-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).


Matrix: SO Batch ID: MP27043




Sample(s) MC48821-9MS, MC48821-9MSD, MC48821-9SDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Arsenic, Cadmium, Selenium are outside control limits for sample MP27043-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).







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Metals By Method SW846 6010CMatrix: SO Batch ID: MP27053

Sample(s) MC48869-2SDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Cadmium, Silver are outside control limits for sample MP27053-SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).


Metals By Method SW846 7470AMatrix: AQ Batch ID: MP27050




Sample(s) MC48821-22FMS, MC48821-22FMSD were used as the QC samples for metals.





Sample(s) MC48821-1AMS, MC48821-1AMSD were used as the QC samples for metals.





Sample(s) MC48821-21AMSD, MC48821-21AMS were used as the QC samples for metals.

Matrix Spike Recovery(s) for Mercury are outside control limits. Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.

Metals By Method SW846 7471BMatrix: SO Batch ID: MP27045




Sample(s) MC48821-2MS, MC48821-2MSD were used as the QC samples for metals.





Wet Chemistry By Method SM 2540G-97 MODMatrix: SO Batch ID: GN55387

Sample(s) MC48821-1DUP were used as the QC samples for Solids, Percent.

Wet Chemistry By Method SW846 9045DMatrix: SO Batch ID: GN55423

Sample(s) MC48821-1DUP were used as the QC samples for pH.


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Wet Chemistry By Method SW846 CHAP7Matrix: SO Batch ID: GP21131

All samples were distilled within the recommended method holding time.



Sample(s) MC48821-3DUP were used as the QC samples for Cyanide Reactivity.

Matrix: SO Batch ID: GP21132

All samples were distilled within the recommended method holding time.



Sample(s) MC48821-3DUP were used as the QC samples for Sulfide Reactivity.

SGS Accutest New England certifies that all analysis were performed within method specification. It is further recommended that this report to be used in its entirety.The Laboratory Director for SGS Accutest New England or assignee as verified by the signature on the cover page has authorized the release of this report(MC48821).


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Summary of Hits Page 1 of 13 Job Number: MC48821Account: BL CompaniesProject: Route 69 Improvements, New Haven, CTCollected: 11/16/16

Lab Sample ID Client Sample ID Result/Analyte Qual RL MDL Units Method

MC48821-1 B-1(0-5')

Tetrachloroethene 7.5 2.9 ug/kg SW846 8260CBenzo(a)anthracene 326 130 ug/kg SW846 8270DBenzo(a)pyrene 388 320 ug/kg SW846 8270DBenzo(b)fluoranthene 389 130 ug/kg SW846 8270DBenzo(g,h,i)perylene 284 130 ug/kg SW846 8270DBenzo(k)fluoranthene 390 130 ug/kg SW846 8270DChrysene 436 130 ug/kg SW846 8270DFluoranthene 718 130 ug/kg SW846 8270DPhenanthrene 395 130 ug/kg SW846 8270DPyrene 738 130 ug/kg SW846 8270DCT-ETPH (C9-C36) 116 22 mg/kg CT-ETPH 7/064,4'-DDT 13.1 6.4 ug/kg SW846 8081BArsenic 3.7 1.0 mg/kg SW846 6010CBarium 90.1 5.2 mg/kg SW846 6010CChromium 22.3 1.0 mg/kg SW846 6010CLead 94.2 1.0 mg/kg SW846 6010CMercury 0.28 0.041 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.6 su SW846 9045D

MC48821-1A B-1(0-5')

Barium 0.68 0.50 mg/l SW846 6010CCadmium 0.0042 0.0040 mg/l SW846 6010CLead 0.29 0.010 mg/l SW846 6010C

MC48821-2 B-1(6-8')

Arsenic 1.9 0.88 mg/kg SW846 6010CBarium 37.9 4.4 mg/kg SW846 6010CChromium 11.1 0.88 mg/kg SW846 6010CLead 4.9 0.88 mg/kg SW846 6010CIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.7 su SW846 9045D

MC48821-2A B-1(6-8')

Barium 0.56 0.50 mg/l SW846 6010C

MC48821-3 B-2(0-2')

Fluoranthene 129 110 ug/kg SW846 8270DPyrene 136 110 ug/kg SW846 8270D

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CT-ETPH (C9-C36) 48.7 17 mg/kg CT-ETPH 7/06Arsenic 1.7 0.87 mg/kg SW846 6010CBarium 18.5 4.4 mg/kg SW846 6010CChromium 10.6 0.87 mg/kg SW846 6010CLead 19.5 0.87 mg/kg SW846 6010CIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.5 su SW846 9045D

MC48821-3A B-2(0-2')

Lead 0.19 0.010 mg/l SW846 6010C

MC48821-4 B-2(6-8')


MC48821-4A B-2(6-8')

Chromium 0.013 0.010 mg/l SW846 6010CLead 0.030 0.010 mg/l SW846 6010C

MC48821-5 B-3(0-2')

Fluoranthene 119 100 ug/kg SW846 8270DPyrene 121 100 ug/kg SW846 8270DCT-ETPH (C9-C36) 79.5 17 mg/kg CT-ETPH 7/06Arsenic 1.4 0.83 mg/kg SW846 6010CBarium 27.0 4.2 mg/kg SW846 6010CChromium 10.6 0.83 mg/kg SW846 6010CLead 5.8 0.83 mg/kg SW846 6010CIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.0 su SW846 9045D

MC48821-5A B-3(0-2')

Lead 0.017 0.010 mg/l SW846 6010C

MC48821-6 B-3(8-10')

Arsenic 1.7 0.91 mg/kg SW846 6010C

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Barium 28.0 4.5 mg/kg SW846 6010CChromium 17.2 0.91 mg/kg SW846 6010CLead 4.4 0.91 mg/kg SW846 6010CIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 6.9 su SW846 9045D

MC48821-6A B-3(8-10')

No hits reported in this sample.

MC48821-7 B-4(1-3')

Benzene 190 63 ug/kg SW846 8260Cn-Butylbenzene 3600 310 ug/kg SW846 8260Csec-Butylbenzene 1830 310 ug/kg SW846 8260CEthylbenzene 650 130 ug/kg SW846 8260CIsopropylbenzene 5230 310 ug/kg SW846 8260CNaphthalene 500 310 ug/kg SW846 8260Cn-Propylbenzene 16300 310 ug/kg SW846 8260Cm,p-Xylene 316 130 ug/kg SW846 8260CAcenaphthylene 10600 1100 ug/kg SW846 8270DAnthracene 6330 1100 ug/kg SW846 8270DBenzo(a)anthracene 21600 1100 ug/kg SW846 8270DBenzo(a)pyrene 21600 2900 ug/kg SW846 8270DBenzo(b)fluoranthene 20100 1100 ug/kg SW846 8270DBenzo(g,h,i)perylene 14400 1100 ug/kg SW846 8270DBenzo(k)fluoranthene 18600 1100 ug/kg SW846 8270DCarbazole 2840 1100 ug/kg SW846 8270DChrysene 29500 1100 ug/kg SW846 8270DDibenzo(a,h)anthracene 3650 1100 ug/kg SW846 8270DDibenzofuran 1360 1100 ug/kg SW846 8270DFluoranthene 59500 1100 ug/kg SW846 8270DFluorene 5280 1100 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene 14100 2900 ug/kg SW846 8270D2-Methylnaphthalene 1190 1100 ug/kg SW846 8270DPhenanthrene 40300 1100 ug/kg SW846 8270DPyrene 57000 1100 ug/kg SW846 8270DCT-ETPH (C9-C36) 2140 98 mg/kg CT-ETPH 7/064,4'-DDT 18.2 5.9 ug/kg SW846 8081BAroclor 1262 60.0 29 ug/kg SW846 8082AArsenic 3.9 0.97 mg/kg SW846 6010CBarium 68.3 4.8 mg/kg SW846 6010CCadmium 0.43 0.39 mg/kg SW846 6010CChromium 15.1 0.97 mg/kg SW846 6010CLead 543 0.97 mg/kg SW846 6010C

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Mercury 0.082 0.038 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.0 su SW846 9045D

MC48821-7A B-4(1-3')

Barium 0.68 0.50 mg/l SW846 6010CLead 1.5 0.010 mg/l SW846 6010C

MC48821-8 B-4(7-10')

n-Butylbenzene 1700 300 ug/kg SW846 8260Csec-Butylbenzene 631 300 ug/kg SW846 8260CEthylbenzene 4260 120 ug/kg SW846 8260CIsopropylbenzene 1530 300 ug/kg SW846 8260Cp-Isopropyltoluene 388 300 ug/kg SW846 8260CNaphthalene 2390 300 ug/kg SW846 8260Cn-Propylbenzene 5270 300 ug/kg SW846 8260C1,2,4-Trimethylbenzene a 15000 300 ug/kg SW846 8260C1,3,5-Trimethylbenzene 4350 300 ug/kg SW846 8260Cm,p-Xylene 8070 120 ug/kg SW846 8260Co-Xylene 2430 120 ug/kg SW846 8260CAcenaphthene 111 110 ug/kg SW846 8270DFluoranthene 133 110 ug/kg SW846 8270DFluorene 152 110 ug/kg SW846 8270D2-Methylnaphthalene 5440 110 ug/kg SW846 8270DNaphthalene 7690 110 ug/kg SW846 8270DPhenanthrene 289 110 ug/kg SW846 8270DCT-ETPH (C9-C36) 372 18 mg/kg CT-ETPH 7/06Arsenic 1.8 0.89 mg/kg SW846 6010CBarium 35.5 4.5 mg/kg SW846 6010CChromium 27.9 0.89 mg/kg SW846 6010CLead 7.6 0.89 mg/kg SW846 6010CIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.8 su SW846 9045D

MC48821-8A B-4(7-10')

Chromium 0.022 0.010 mg/l SW846 6010CLead 0.031 0.010 mg/l SW846 6010C

MC48821-9 B-5(0-2')

Fluoranthene 184 110 ug/kg SW846 8270DPyrene 189 110 ug/kg SW846 8270D

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CT-ETPH (C9-C36) 115 18 mg/kg CT-ETPH 7/064,4'-DDT 9.1 5.3 ug/kg SW846 8081BAroclor 1260 b 32.1 26 ug/kg SW846 8082AArsenic 3.7 0.88 mg/kg SW846 6010CBarium 74.2 4.4 mg/kg SW846 6010CChromium 15.7 0.88 mg/kg SW846 6010CLead 59.5 0.88 mg/kg SW846 6010CMercury 0.12 0.034 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.0 su SW846 9045D

MC48821-9A B-5(0-2')

Lead 0.047 0.010 mg/l SW846 6010C

MC48821-10 B-5(6-8')


MC48821-10A B-5(6-8')


MC48821-11 B-6(0-2')

Acenaphthylene 808 120 ug/kg SW846 8270DAnthracene 326 120 ug/kg SW846 8270DBenzo(a)anthracene 1990 120 ug/kg SW846 8270DBenzo(a)pyrene 2030 290 ug/kg SW846 8270DBenzo(b)fluoranthene 1900 120 ug/kg SW846 8270DBenzo(g,h,i)perylene 1340 120 ug/kg SW846 8270DBenzo(k)fluoranthene 1690 120 ug/kg SW846 8270DChrysene 2470 120 ug/kg SW846 8270DDibenzo(a,h)anthracene 334 120 ug/kg SW846 8270DFluoranthene 3970 120 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene 1290 290 ug/kg SW846 8270DPhenanthrene 1390 120 ug/kg SW846 8270DPyrene 4330 120 ug/kg SW846 8270DCT-ETPH (C9-C36) 620 95 mg/kg CT-ETPH 7/064,4'-DDT 15.3 5.9 ug/kg SW846 8081B

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Arsenic 3.9 0.96 mg/kg SW846 6010CBarium 66.1 4.8 mg/kg SW846 6010CChromium 11.3 0.96 mg/kg SW846 6010CLead 90.5 0.96 mg/kg SW846 6010CMercury 0.047 0.035 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.7 su SW846 9045D

MC48821-11A B-6(0-2')

Lead 0.017 0.010 mg/l SW846 6010C

MC48821-12 B-6(2-4')


MC48821-12A B-6(2-4')


MC48821-13 B-7(0-2')

Benzo(a)anthracene 202 110 ug/kg SW846 8270DBenzo(b)fluoranthene 191 110 ug/kg SW846 8270DBenzo(g,h,i)perylene 132 110 ug/kg SW846 8270DBenzo(k)fluoranthene 161 110 ug/kg SW846 8270DChrysene 226 110 ug/kg SW846 8270DFluoranthene 408 110 ug/kg SW846 8270DPhenanthrene 226 110 ug/kg SW846 8270DPyrene 386 110 ug/kg SW846 8270DCT-ETPH (C9-C36) 171 18 mg/kg CT-ETPH 7/064,4'-DDD 44.8 5.6 ug/kg SW846 8081B4,4'-DDE b 278 28 ug/kg SW846 8081B4,4'-DDT 575 28 ug/kg SW846 8081BArsenic 5.7 0.90 mg/kg SW846 6010CBarium 74.0 4.5 mg/kg SW846 6010CChromium 16.4 0.90 mg/kg SW846 6010CLead 35.9 0.90 mg/kg SW846 6010CMercury 1.6 0.18 mg/kg SW846 7471B

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MC48821-13A B-7(0-2')


MC48821-14 B-7(2-4')

Acenaphthene 154 100 ug/kg SW846 8270DAnthracene 392 100 ug/kg SW846 8270DBenzo(a)anthracene 1310 100 ug/kg SW846 8270DBenzo(a)pyrene 1130 260 ug/kg SW846 8270DBenzo(b)fluoranthene 1080 100 ug/kg SW846 8270DBenzo(g,h,i)perylene 663 100 ug/kg SW846 8270DBenzo(k)fluoranthene 960 100 ug/kg SW846 8270DCarbazole 228 100 ug/kg SW846 8270DChrysene 1460 100 ug/kg SW846 8270DDibenzo(a,h)anthracene 177 100 ug/kg SW846 8270DDibenzofuran 111 100 ug/kg SW846 8270DFluoranthene 3100 100 ug/kg SW846 8270DFluorene 138 100 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene 674 260 ug/kg SW846 8270DPhenanthrene 2270 100 ug/kg SW846 8270DPyrene 2830 100 ug/kg SW846 8270DCT-ETPH (C9-C36) 288 17 mg/kg CT-ETPH 7/064,4'-DDD 9.3 5.1 ug/kg SW846 8081B4,4'-DDE b 87.8 26 ug/kg SW846 8081B4,4'-DDT 190 26 ug/kg SW846 8081BAroclor 1242 83.7 26 ug/kg SW846 8082AArsenic 5.8 0.87 mg/kg SW846 6010CBarium 52.7 4.3 mg/kg SW846 6010CChromium 13.7 0.87 mg/kg SW846 6010CLead 27.2 0.87 mg/kg SW846 6010CMercury 0.67 0.032 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 6.8 su SW846 9045D

MC48821-14A B-7(2-4')


MC48821-15 HA-1(0-2')

Acenaphthylene c 826 520 ug/kg SW846 8270DBenzo(a)anthracene c 1330 520 ug/kg SW846 8270DBenzo(a)pyrene c 1670 1300 ug/kg SW846 8270DBenzo(b)fluoranthene c 1460 520 ug/kg SW846 8270D

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Benzo(g,h,i)perylene c 1500 520 ug/kg SW846 8270DBenzo(k)fluoranthene c 1420 520 ug/kg SW846 8270DChrysene c 1710 520 ug/kg SW846 8270DFluoranthene c 2950 520 ug/kg SW846 8270DPhenanthrene c 1320 520 ug/kg SW846 8270DPyrene c 2740 520 ug/kg SW846 8270DCT-ETPH (C9-C36) 403 82 mg/kg CT-ETPH 7/064,4'-DDD 5.1 5.1 ug/kg SW846 8081B4,4'-DDE b 64.3 26 ug/kg SW846 8081B4,4'-DDT 263 26 ug/kg SW846 8081BAroclor 1260 104 26 ug/kg SW846 8082AArsenic 2.1 0.84 mg/kg SW846 6010CBarium 40.5 4.2 mg/kg SW846 6010CCadmium 0.43 0.34 mg/kg SW846 6010CChromium 12.4 0.84 mg/kg SW846 6010CLead 598 0.84 mg/kg SW846 6010C

MC48821-15A HA-1(0-2')

Cadmium 0.0060 0.0040 mg/l SW846 6010CLead 1.3 0.010 mg/l SW846 6010C

MC48821-16 HA-2(0-2')

Acenaphthylene 121 120 ug/kg SW846 8270DBenzo(a)anthracene 263 120 ug/kg SW846 8270DBenzo(a)pyrene 294 290 ug/kg SW846 8270DBenzo(b)fluoranthene 336 120 ug/kg SW846 8270DBenzo(g,h,i)perylene 235 120 ug/kg SW846 8270DBenzo(k)fluoranthene 282 120 ug/kg SW846 8270DChrysene 371 120 ug/kg SW846 8270DFluoranthene 567 120 ug/kg SW846 8270DPhenanthrene 240 120 ug/kg SW846 8270DPyrene 553 120 ug/kg SW846 8270DCT-ETPH (C9-C36) 242 97 mg/kg CT-ETPH 7/064,4'-DDE b 50.0 5.8 ug/kg SW846 8081B4,4'-DDT 52.7 5.8 ug/kg SW846 8081BAroclor 1254 d 32.7 29 ug/kg SW846 8082AAroclor 1260 68.8 29 ug/kg SW846 8082AArsenic 5.9 0.95 mg/kg SW846 6010CBarium 72.8 4.7 mg/kg SW846 6010CChromium 14.6 0.95 mg/kg SW846 6010CLead 153 0.95 mg/kg SW846 6010CMercury 0.076 0.038 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020

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pH 7.0 su SW846 9045D

MC48821-16A HA-2(0-2')

Lead 0.058 0.010 mg/l SW846 6010C

MC48821-17 HA-3(0-2')

Acenaphthylene 361 110 ug/kg SW846 8270DAnthracene 191 110 ug/kg SW846 8270DBenzo(a)anthracene 673 110 ug/kg SW846 8270DBenzo(a)pyrene 726 280 ug/kg SW846 8270DBenzo(b)fluoranthene 752 110 ug/kg SW846 8270DBenzo(g,h,i)perylene 537 110 ug/kg SW846 8270DBenzo(k)fluoranthene 675 110 ug/kg SW846 8270DChrysene 956 110 ug/kg SW846 8270DDibenzo(a,h)anthracene 133 110 ug/kg SW846 8270DFluoranthene 1460 110 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene 508 280 ug/kg SW846 8270DPhenanthrene 719 110 ug/kg SW846 8270DPyrene 1530 110 ug/kg SW846 8270DCT-ETPH (C9-C36) 428 90 mg/kg CT-ETPH 7/064,4'-DDE 16.6 5.6 ug/kg SW846 8081B4,4'-DDT b 64.2 5.6 ug/kg SW846 8081BAroclor 1260 62.3 28 ug/kg SW846 8082AArsenic 2.8 0.93 mg/kg SW846 6010CBarium 41.8 4.6 mg/kg SW846 6010CChromium 14.0 0.93 mg/kg SW846 6010CLead 263 0.93 mg/kg SW846 6010CMercury 0.041 0.036 mg/kg SW846 7471B

MC48821-17A HA-3(0-2')

Lead 0.31 0.010 mg/l SW846 6010C

MC48821-18 HA-4(0-2')

Benzo(a)anthracene c 1170 550 ug/kg SW846 8270DBenzo(b)fluoranthene c 1270 550 ug/kg SW846 8270DBenzo(g,h,i)perylene c 1240 550 ug/kg SW846 8270DBenzo(k)fluoranthene c 1220 550 ug/kg SW846 8270DChrysene c 1530 550 ug/kg SW846 8270DFluoranthene c 2620 550 ug/kg SW846 8270DPhenanthrene c 1190 550 ug/kg SW846 8270DPyrene c 2460 550 ug/kg SW846 8270D

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CT-ETPH (C9-C36) 567 89 mg/kg CT-ETPH 7/064,4'-DDE 9.4 5.6 ug/kg SW846 8081B4,4'-DDT 197 28 ug/kg SW846 8081BAroclor 1260 114 28 ug/kg SW846 8082AArsenic 2.2 0.88 mg/kg SW846 6010CBarium 27.6 4.4 mg/kg SW846 6010CChromium 20.6 0.88 mg/kg SW846 6010CLead 185 0.88 mg/kg SW846 6010C

MC48821-18A HA-4(0-2')

Lead 0.50 0.010 mg/l SW846 6010C

MC48821-19 HA-5(0-2')

Acenaphthylene c 1590 570 ug/kg SW846 8270DAnthracene c 748 570 ug/kg SW846 8270DBenzo(a)anthracene c 2170 570 ug/kg SW846 8270DBenzo(a)pyrene c 2530 1400 ug/kg SW846 8270DBenzo(b)fluoranthene c 2510 570 ug/kg SW846 8270DBenzo(g,h,i)perylene c 1930 570 ug/kg SW846 8270DBenzo(k)fluoranthene c 2370 570 ug/kg SW846 8270DChrysene c 3020 570 ug/kg SW846 8270DFluoranthene c 4380 570 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene c 1880 1400 ug/kg SW846 8270DPhenanthrene c 1910 570 ug/kg SW846 8270DPyrene c 4280 570 ug/kg SW846 8270DCT-ETPH (C9-C36) 740 94 mg/kg CT-ETPH 7/064,4'-DDD 7.9 5.8 ug/kg SW846 8081B4,4'-DDT 27.7 5.8 ug/kg SW846 8081BAroclor 1260 47.0 29 ug/kg SW846 8082AArsenic 4.6 0.94 mg/kg SW846 6010CBarium 42.4 4.7 mg/kg SW846 6010CCadmium 0.38 0.38 mg/kg SW846 6010CChromium 16.6 0.94 mg/kg SW846 6010CLead 222 0.94 mg/kg SW846 6010CMercury 0.12 0.035 mg/kg SW846 7471BIgnitability (Flashpoint) >230 Deg. F SW846 1020pH 7.2 su SW846 9045D

MC48821-19A HA-5(0-2')

Lead 0.081 0.010 mg/l SW846 6010C

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MC48821-20 HA-6(0-2')

Acenaphthylene 134 110 ug/kg SW846 8270DBenzo(a)anthracene 469 110 ug/kg SW846 8270DBenzo(a)pyrene 500 270 ug/kg SW846 8270DBenzo(b)fluoranthene 481 110 ug/kg SW846 8270DBenzo(g,h,i)perylene 379 110 ug/kg SW846 8270DBenzo(k)fluoranthene 473 110 ug/kg SW846 8270DChrysene 565 110 ug/kg SW846 8270DFluoranthene 1090 110 ug/kg SW846 8270DIndeno(1,2,3-cd)pyrene 362 270 ug/kg SW846 8270DPhenanthrene 447 110 ug/kg SW846 8270DPyrene 918 110 ug/kg SW846 8270DCT-ETPH (C9-C36) 100 19 mg/kg CT-ETPH 7/064,4'-DDE b 12.8 5.7 ug/kg SW846 8081B4,4'-DDT 21.6 5.7 ug/kg SW846 8081BArsenic 4.0 0.93 mg/kg SW846 6010CBarium 61.6 4.6 mg/kg SW846 6010CChromium 15.6 0.93 mg/kg SW846 6010CLead 67.3 0.93 mg/kg SW846 6010CMercury 0.047 0.037 mg/kg SW846 7471B

MC48821-20A HA-6(0-2')

Lead 0.042 0.010 mg/l SW846 6010C

MC48821-21 HA-6(0-2')DUP

CT-ETPH (C9-C36) 98.9 19 mg/kg CT-ETPH 7/064,4'-DDE b 10.9 5.4 ug/kg SW846 8081B4,4'-DDT b 21.0 5.4 ug/kg SW846 8081BArsenic 3.8 0.93 mg/kg SW846 6010CBarium 52.6 4.6 mg/kg SW846 6010CChromium 16.6 0.93 mg/kg SW846 6010CLead 78.8 0.93 mg/kg SW846 6010CMercury 0.056 0.034 mg/kg SW846 7471B

MC48821-21A HA-6(0-2')DUP

Lead 0.040 0.010 mg/l SW846 6010C

MC48821-22 B-1/GW

Arsenic 9.5 4.0 ug/l SW846 6010CBarium 421 50 ug/l SW846 6010C

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Chromium 46.3 10 ug/l SW846 6010CCopper 120 25 ug/l SW846 6010CLead 25.9 5.0 ug/l SW846 6010CZinc 67.0 20 ug/l SW846 6010C

MC48821-22F B-1/GW

Barium 72.5 50 ug/l SW846 6010C

MC48821-23 B-3/GW

Benzene 0.60 0.50 ug/l SW846 8260CBarium 72.2 50 ug/l SW846 6010C

MC48821-23F B-3/GW

Barium 60.9 50 ug/l SW846 6010C

MC48821-24 B-3/GW DUP

Benzene 0.59 0.50 ug/l SW846 8260CBarium 70.3 50 ug/l SW846 6010C

MC48821-24F B-3/GW DUP

Barium 61.2 50 ug/l SW846 6010C

MC48821-25 TRIP BLANK


MC48821-26 TRIP BLANK


MC48821-26A TRIP BLANK


MC48821-27 EQUIPMENT BLANK


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(a) Continuing Calibration outside of acceptance criteria. Result may be biased high.(b) Confirmation value >40% RPD.(c) Elevated RL due to dilution required for matrix interference.(d) Estimated value due to the presence of other Aroclor pattern.Confirmation value >40% RPD

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Sample Results

Report of Analysis

New EnglandSection 4

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Report of Analysis Page 1 of 3

Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8260C Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 M82087.D 1 11/23/16 KP n/a n/a MSM2944Run #2 a M82128.D 1 11/23/16 KP n/a n/a MSM2945

Initial Weight Final VolumeRun #1 4.50 g 5.0 mlRun #2 5.29 g 5.0 ml

VOA RCP List

CAS No. Compound Result RL Units Q

67-64-1 Acetone ND 15 ug/kg107-13-1 Acrylonitrile ND 37 ug/kg71-43-2 Benzene ND 1.5 ug/kg108-86-1 Bromobenzene ND 7.3 ug/kg75-27-4 Bromodichloromethane ND 2.9 ug/kg75-25-2 Bromoform ND 2.9 ug/kg74-83-9 Bromomethane ND 15 ug/kg78-93-3 2-Butanone (MEK) ND 15 ug/kg104-51-8 n-Butylbenzene ND 7.3 ug/kg135-98-8 sec-Butylbenzene ND 7.3 ug/kg98-06-6 tert-Butylbenzene ND 7.3 ug/kg75-15-0 Carbon disulfide b ND 7.3 ug/kg56-23-5 Carbon tetrachloride ND 2.9 ug/kg108-90-7 Chlorobenzene ND 2.9 ug/kg75-00-3 Chloroethane ND 15 ug/kg67-66-3 Chloroform ND 2.9 ug/kg74-87-3 Chloromethane ND 7.3 ug/kg95-49-8 o-Chlorotoluene ND 7.3 ug/kg106-43-4 p-Chlorotoluene ND 7.3 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 7.3 ug/kg124-48-1 Dibromochloromethane ND 7.3 ug/kg106-93-4 1,2-Dibromoethane ND 2.9 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.9 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.9 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.9 ug/kg75-71-8 Dichlorodifluoromethane ND 7.3 ug/kg75-34-3 1,1-Dichloroethane ND 2.9 ug/kg107-06-2 1,2-Dichloroethane ND 2.9 ug/kg75-35-4 1,1-Dichloroethene b ND 2.9 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.9 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.9 ug/kg78-87-5 1,2-Dichloropropane ND 2.9 ug/kg

ND = Not detected J = Indicates an estimated valueRL = Reporting Limit B = Indicates analyte found in associated method blankE = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

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VOA RCP List


142-28-9 1,3-Dichloropropane ND 7.3 ug/kg594-20-7 2,2-Dichloropropane ND 7.3 ug/kg563-58-6 1,1-Dichloropropene ND 7.3 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.9 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.9 ug/kg100-41-4 Ethylbenzene ND 2.9 ug/kg76-13-1 Freon 113 b ND 7.3 ug/kg87-68-3 Hexachlorobutadiene ND 7.3 ug/kg591-78-6 2-Hexanone ND 7.3 ug/kg98-82-8 Isopropylbenzene ND 7.3 ug/kg99-87-6 p-Isopropyltoluene ND 7.3 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.9 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 7.3 ug/kg74-95-3 Methylene bromide ND 7.3 ug/kg75-09-2 Methylene chloride ND 2.9 ug/kg91-20-3 Naphthalene ND 7.3 ug/kg103-65-1 n-Propylbenzene ND 7.3 ug/kg100-42-5 Styrene ND 7.3 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.9 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 7.3 ug/kg127-18-4 Tetrachloroethene 7.5 2.9 ug/kg109-99-9 Tetrahydrofuran ND 15 ug/kg108-88-3 Toluene ND 7.3 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 15 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 7.3 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 7.3 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.9 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.9 ug/kg79-01-6 Trichloroethene ND 2.9 ug/kg75-69-4 Trichlorofluoromethane ND 2.9 ug/kg96-18-4 1,2,3-Trichloropropane ND 7.3 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 7.3 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 7.3 ug/kg75-01-4 Vinyl chloride ND 15 ug/kg

m,p-Xylene ND 2.9 ug/kg95-47-6 o-Xylene ND 2.9 ug/kg

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 124% 106% 65-141%


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2037-26-5 Toluene-D8 103% 99% 65-129%460-00-4 4-Bromofluorobenzene 115% 131% 63-137%

(a) Confirmation run for internal standard areas.(b) Continuing Calibration outside of acceptance criteria. Reporting Limit response verified by low-level

standard.


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8270D SW846 3546 Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 R50884.D 1 11/26/16 DRY 11/22/16 OP49183 MSR1897Run #2

Initial Weight Final VolumeRun #1 20.6 g 1.0 mlRun #2

ABN RCP List


95-57-8 2-Chlorophenol ND 320 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 640 ug/kg120-83-2 2,4-Dichlorophenol ND 640 ug/kg105-67-9 2,4-Dimethylphenol ND 640 ug/kg51-28-5 2,4-Dinitrophenol ND 640 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 640 ug/kg95-48-7 2-Methylphenol ND 640 ug/kg106-44-5 4-Methylphenol ND 640 ug/kg88-75-5 2-Nitrophenol ND 640 ug/kg100-02-7 4-Nitrophenol a ND 640 ug/kg87-86-5 Pentachlorophenol a ND 640 ug/kg108-95-2 Phenol ND 320 ug/kg95-95-4 2,4,5-Trichlorophenol ND 640 ug/kg88-06-2 2,4,6-Trichlorophenol ND 640 ug/kg83-32-9 Acenaphthene ND 130 ug/kg208-96-8 Acenaphthylene ND 130 ug/kg62-53-3 Aniline ND 640 ug/kg120-12-7 Anthracene ND 130 ug/kg56-55-3 Benzo(a)anthracene 326 130 ug/kg50-32-8 Benzo(a)pyrene 388 320 ug/kg205-99-2 Benzo(b)fluoranthene 389 130 ug/kg191-24-2 Benzo(g,h,i)perylene 284 130 ug/kg207-08-9 Benzo(k)fluoranthene 390 130 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 320 ug/kg85-68-7 Butyl benzyl phthalate ND 320 ug/kg91-58-7 2-Chloronaphthalene ND 320 ug/kg106-47-8 4-Chloroaniline ND 640 ug/kg86-74-8 Carbazole ND 130 ug/kg218-01-9 Chrysene 436 130 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 320 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 320 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 320 ug/kg


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ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 320 ug/kg121-14-2 2,4-Dinitrotoluene ND 640 ug/kg606-20-2 2,6-Dinitrotoluene ND 640 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 640 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 130 ug/kg132-64-9 Dibenzofuran ND 130 ug/kg84-74-2 Di-n-butyl phthalate ND 320 ug/kg117-84-0 Di-n-octyl phthalate ND 320 ug/kg84-66-2 Diethyl phthalate ND 320 ug/kg131-11-3 Dimethyl phthalate ND 320 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 320 ug/kg206-44-0 Fluoranthene 718 130 ug/kg86-73-7 Fluorene ND 130 ug/kg118-74-1 Hexachlorobenzene ND 320 ug/kg87-68-3 Hexachlorobutadiene ND 320 ug/kg77-47-4 Hexachlorocyclopentadiene ND 640 ug/kg67-72-1 Hexachloroethane ND 320 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 320 ug/kg78-59-1 Isophorone ND 320 ug/kg91-57-6 2-Methylnaphthalene ND 130 ug/kg88-74-4 2-Nitroaniline ND 640 ug/kg99-09-2 3-Nitroaniline ND 640 ug/kg100-01-6 4-Nitroaniline ND 640 ug/kg91-20-3 Naphthalene ND 130 ug/kg98-95-3 Nitrobenzene ND 320 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 320 ug/kg86-30-6 N-Nitrosodiphenylamine ND 320 ug/kg82-68-8 Pentachloronitrobenzene ND 640 ug/kg85-01-8 Phenanthrene 395 130 ug/kg129-00-0 Pyrene 738 130 ug/kg110-86-1 Pyridine ND 640 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 640 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 320 ug/kg


367-12-4 2-Fluorophenol 72% 25-109%4165-62-2 Phenol-d5 73% 29-113%118-79-6 2,4,6-Tribromophenol 86% 20-141%4165-60-0 Nitrobenzene-d5 72% 27-115%


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ABN RCP List


321-60-8 2-Fluorobiphenyl 88% 34-118%1718-51-0 Terphenyl-d14 100% 42-139%

(a) Continuing Calibration outside of acceptance criteria. Reporting Limit Response verified by low-levelstandard.


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8081B SW846 3546 Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 BE53561.D 1 11/30/16 TA 11/29/16 OP49219 GBE2694Run #2


Pesticide RCP List


15972-60-8 Alachlor ND 64 ug/kg309-00-2 Aldrin ND 6.4 ug/kg319-84-6 alpha-BHC ND 6.4 ug/kg319-85-7 beta-BHC ND 6.4 ug/kg319-86-8 delta-BHC ND 6.4 ug/kg58-89-9 gamma-BHC (Lindane) ND 6.4 ug/kg12789-03-6 Chlordane ND 64 ug/kg60-57-1 Dieldrin ND 6.4 ug/kg72-54-8 4,4'-DDD ND 6.4 ug/kg72-55-9 4,4'-DDE ND 6.4 ug/kg50-29-3 4,4'-DDT 13.1 6.4 ug/kg72-20-8 Endrin ND 6.4 ug/kg1031-07-8 Endosulfan sulfate ND 6.4 ug/kg7421-93-4 Endrin aldehyde ND 6.4 ug/kg959-98-8 Endosulfan-I ND 6.4 ug/kg33213-65-9 Endosulfan-II ND 6.4 ug/kg76-44-8 Heptachlor ND 6.4 ug/kg1024-57-3 Heptachlor epoxide ND 6.4 ug/kg72-43-5 Methoxychlor ND 6.4 ug/kg53494-70-5 Endrin ketone ND 6.4 ug/kg8001-35-2 Toxaphene ND 64 ug/kg


877-09-8 Tetrachloro-m-xylene 61% 10-143%877-09-8 Tetrachloro-m-xylene 77% 10-143%2051-24-3 Decachlorobiphenyl 78% 10-172%2051-24-3 Decachlorobiphenyl 250% a 10-172%

(a) Outside control limits due to possible matrix interference.


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8082A SW846 3546 Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 BK63355.D 1 11/30/16 TA 11/29/16 OP49218 GBK2004Run #2


CT Polychlorinated Biphenyls RCP List


12674-11-2 Aroclor 1016 ND 32 ug/kg11104-28-2 Aroclor 1221 ND 32 ug/kg11141-16-5 Aroclor 1232 ND 32 ug/kg53469-21-9 Aroclor 1242 ND 32 ug/kg12672-29-6 Aroclor 1248 ND 32 ug/kg11097-69-1 Aroclor 1254 ND 32 ug/kg11096-82-5 Aroclor 1260 ND 32 ug/kg37324-23-5 Aroclor 1262 ND 32 ug/kg11100-14-4 Aroclor 1268 ND 32 ug/kg


877-09-8 Tetrachloro-m-xylene 59% 25-145%877-09-8 Tetrachloro-m-xylene 52% 25-145%2051-24-3 Decachlorobiphenyl 83% 25-179%2051-24-3 Decachlorobiphenyl 73% 25-179%


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3546 Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 CF5410.D 1 11/25/16 MD 11/22/16 OP49193 GCF1344Run #2



CT-ETPH (C9-C36) 116 22 mg/kg


84-15-1 o-Terphenyl 80% 50-137%


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16

Percent Solids: 75.9 Project: Route 69 Improvements, New Haven, CT

Metals Analysis

Analyte Result RL Units DF Prep Analyzed By Method Prep Method

Arsenic 3.7 1.0 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Barium 90.1 5.2 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Cadmium <0.41 0.41 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Chromium 22.3 1.0 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Lead 94.2 1.0 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Mercury 0.28 0.041 mg/kg 1 11/22/16 11/23/16 EAL SW846 7471B 2 SW846 7471B 4

Selenium <1.0 1.0 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

Silver <0.52 0.52 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3

(1) Instrument QC Batch: MA19639(2) Instrument QC Batch: MA19641(3) Prep QC Batch: MP27043(4) Prep QC Batch: MP27045

RL = Reporting Limit

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General Chemistry

Analyte Result RL Units DF Analyzed By Method

Cyanide Reactivity <2.0 2.0 mg/kg 1 11/23/16 15:10 HS SW846 CHAP7

Ignitability (Flashpoint) >230 Deg. F 1 11/23/16 HS SW846 1020

Solids, Percent 75.9 % 1 11/21/16 HS SM 2540G-97 MOD

Sulfide Reactivity <65 65 mg/kg 1 11/22/16 CF SW846 CHAP7

pH 7.6 su 1 11/26/16 13:32 EL SW846 9045D


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Client Sample ID: B-1(0-5') Lab Sample ID: MC48821-1A Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16


Metals Analysis, TCLP Leachate SW846 1311

Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method

Arsenic <0.010 D004 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Barium 0.68 D005 100 0.50 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Cadmium 0.0042 D006 1.0 0.0040 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Chromium <0.010 D007 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Lead 0.29 D008 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Mercury <0.00020 D009 0.20 0.00020mg/l 1 11/23/16 11/28/16 JM SW846 7470A 2 SW846 7470A 4

Selenium <0.025 D010 1.0 0.025 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3

Silver <0.0050 D011 5.0 0.0050 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3


RL = Reporting LimitMCL = Maximum Contamination Level (40 CFR 261 6/96)

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File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 M82088.D 1 11/23/16 KP n/a n/a MSM2944Run #2


VOA RCP List


67-64-1 Acetone ND 9.5 ug/kg107-13-1 Acrylonitrile ND 24 ug/kg71-43-2 Benzene ND 0.95 ug/kg108-86-1 Bromobenzene ND 4.8 ug/kg75-27-4 Bromodichloromethane ND 1.9 ug/kg75-25-2 Bromoform ND 1.9 ug/kg74-83-9 Bromomethane ND 9.5 ug/kg78-93-3 2-Butanone (MEK) ND 9.5 ug/kg104-51-8 n-Butylbenzene ND 4.8 ug/kg135-98-8 sec-Butylbenzene ND 4.8 ug/kg98-06-6 tert-Butylbenzene ND 4.8 ug/kg75-15-0 Carbon disulfide a ND 4.8 ug/kg56-23-5 Carbon tetrachloride ND 1.9 ug/kg108-90-7 Chlorobenzene ND 1.9 ug/kg75-00-3 Chloroethane ND 9.5 ug/kg67-66-3 Chloroform ND 1.9 ug/kg74-87-3 Chloromethane ND 4.8 ug/kg95-49-8 o-Chlorotoluene ND 4.8 ug/kg106-43-4 p-Chlorotoluene ND 4.8 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 4.8 ug/kg124-48-1 Dibromochloromethane ND 4.8 ug/kg106-93-4 1,2-Dibromoethane ND 1.9 ug/kg95-50-1 1,2-Dichlorobenzene ND 1.9 ug/kg541-73-1 1,3-Dichlorobenzene ND 1.9 ug/kg106-46-7 1,4-Dichlorobenzene ND 1.9 ug/kg75-71-8 Dichlorodifluoromethane ND 4.8 ug/kg75-34-3 1,1-Dichloroethane ND 1.9 ug/kg107-06-2 1,2-Dichloroethane ND 1.9 ug/kg75-35-4 1,1-Dichloroethene a ND 1.9 ug/kg156-59-2 cis-1,2-Dichloroethene ND 1.9 ug/kg156-60-5 trans-1,2-Dichloroethene ND 1.9 ug/kg78-87-5 1,2-Dichloropropane ND 1.9 ug/kg


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VOA RCP List


142-28-9 1,3-Dichloropropane ND 4.8 ug/kg594-20-7 2,2-Dichloropropane ND 4.8 ug/kg563-58-6 1,1-Dichloropropene ND 4.8 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 1.9 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 1.9 ug/kg100-41-4 Ethylbenzene ND 1.9 ug/kg76-13-1 Freon 113 a ND 4.8 ug/kg87-68-3 Hexachlorobutadiene ND 4.8 ug/kg591-78-6 2-Hexanone ND 4.8 ug/kg98-82-8 Isopropylbenzene ND 4.8 ug/kg99-87-6 p-Isopropyltoluene ND 4.8 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 1.9 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 4.8 ug/kg74-95-3 Methylene bromide ND 4.8 ug/kg75-09-2 Methylene chloride ND 1.9 ug/kg91-20-3 Naphthalene ND 4.8 ug/kg103-65-1 n-Propylbenzene ND 4.8 ug/kg100-42-5 Styrene ND 4.8 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 1.9 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 4.8 ug/kg127-18-4 Tetrachloroethene ND 1.9 ug/kg109-99-9 Tetrahydrofuran ND 9.5 ug/kg108-88-3 Toluene ND 4.8 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 9.5 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 4.8 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 4.8 ug/kg71-55-6 1,1,1-Trichloroethane ND 1.9 ug/kg79-00-5 1,1,2-Trichloroethane ND 1.9 ug/kg79-01-6 Trichloroethene ND 1.9 ug/kg75-69-4 Trichlorofluoromethane ND 1.9 ug/kg96-18-4 1,2,3-Trichloropropane ND 4.8 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 4.8 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 4.8 ug/kg75-01-4 Vinyl chloride ND 9.5 ug/kg



1868-53-7 Dibromofluoromethane 117% 65-141%


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2037-26-5 Toluene-D8 104% 65-129%460-00-4 4-Bromofluorobenzene 96% 63-137%

(a) Continuing Calibration outside of acceptance criteria. Reporting Limit response verified by low-levelstandard.


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File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 R50920.D 1 11/29/16 MR 11/23/16 OP49195 MSR1899Run #2


ABN RCP List


95-57-8 2-Chlorophenol ND 270 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 550 ug/kg120-83-2 2,4-Dichlorophenol ND 550 ug/kg105-67-9 2,4-Dimethylphenol ND 550 ug/kg51-28-5 2,4-Dinitrophenol ND 550 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 550 ug/kg95-48-7 2-Methylphenol ND 550 ug/kg106-44-5 4-Methylphenol ND 550 ug/kg88-75-5 2-Nitrophenol ND 550 ug/kg100-02-7 4-Nitrophenol ND 550 ug/kg87-86-5 Pentachlorophenol ND 550 ug/kg108-95-2 Phenol ND 270 ug/kg95-95-4 2,4,5-Trichlorophenol ND 550 ug/kg88-06-2 2,4,6-Trichlorophenol ND 550 ug/kg83-32-9 Acenaphthene ND 110 ug/kg208-96-8 Acenaphthylene ND 110 ug/kg62-53-3 Aniline ND 550 ug/kg120-12-7 Anthracene ND 110 ug/kg56-55-3 Benzo(a)anthracene ND 110 ug/kg50-32-8 Benzo(a)pyrene ND 270 ug/kg205-99-2 Benzo(b)fluoranthene ND 110 ug/kg191-24-2 Benzo(g,h,i)perylene ND 110 ug/kg207-08-9 Benzo(k)fluoranthene ND 110 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 270 ug/kg85-68-7 Butyl benzyl phthalate ND 270 ug/kg91-58-7 2-Chloronaphthalene ND 270 ug/kg106-47-8 4-Chloroaniline ND 550 ug/kg86-74-8 Carbazole ND 110 ug/kg218-01-9 Chrysene ND 110 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 270 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 270 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 270 ug/kg


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ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 270 ug/kg121-14-2 2,4-Dinitrotoluene ND 550 ug/kg606-20-2 2,6-Dinitrotoluene ND 550 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 550 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 110 ug/kg132-64-9 Dibenzofuran ND 110 ug/kg84-74-2 Di-n-butyl phthalate ND 270 ug/kg117-84-0 Di-n-octyl phthalate ND 270 ug/kg84-66-2 Diethyl phthalate ND 270 ug/kg131-11-3 Dimethyl phthalate ND 270 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 270 ug/kg206-44-0 Fluoranthene ND 110 ug/kg86-73-7 Fluorene ND 110 ug/kg118-74-1 Hexachlorobenzene ND 270 ug/kg87-68-3 Hexachlorobutadiene ND 270 ug/kg77-47-4 Hexachlorocyclopentadiene ND 550 ug/kg67-72-1 Hexachloroethane ND 270 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 270 ug/kg78-59-1 Isophorone ND 270 ug/kg91-57-6 2-Methylnaphthalene ND 110 ug/kg88-74-4 2-Nitroaniline ND 550 ug/kg99-09-2 3-Nitroaniline ND 550 ug/kg100-01-6 4-Nitroaniline ND 550 ug/kg91-20-3 Naphthalene ND 110 ug/kg98-95-3 Nitrobenzene ND 270 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 270 ug/kg86-30-6 N-Nitrosodiphenylamine ND 270 ug/kg82-68-8 Pentachloronitrobenzene ND 550 ug/kg85-01-8 Phenanthrene ND 110 ug/kg129-00-0 Pyrene ND 110 ug/kg110-86-1 Pyridine ND 550 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 550 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 270 ug/kg




49 of 555

MC48821

44.3

SGS Accutest



ABN RCP List




50 of 555

MC48821

44.3

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 54 ug/kg309-00-2 Aldrin ND 5.4 ug/kg319-84-6 alpha-BHC ND 5.4 ug/kg319-85-7 beta-BHC ND 5.4 ug/kg319-86-8 delta-BHC ND 5.4 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.4 ug/kg12789-03-6 Chlordane ND 54 ug/kg60-57-1 Dieldrin ND 5.4 ug/kg72-54-8 4,4'-DDD ND 5.4 ug/kg72-55-9 4,4'-DDE ND 5.4 ug/kg50-29-3 4,4'-DDT ND 5.4 ug/kg72-20-8 Endrin ND 5.4 ug/kg1031-07-8 Endosulfan sulfate ND 5.4 ug/kg7421-93-4 Endrin aldehyde ND 5.4 ug/kg959-98-8 Endosulfan-I ND 5.4 ug/kg33213-65-9 Endosulfan-II ND 5.4 ug/kg76-44-8 Heptachlor ND 5.4 ug/kg1024-57-3 Heptachlor epoxide ND 5.4 ug/kg72-43-5 Methoxychlor ND 5.4 ug/kg53494-70-5 Endrin ketone ND 5.4 ug/kg8001-35-2 Toxaphene ND 54 ug/kg




51 of 555

MC48821

44.3

SGS Accutest











52 of 555

MC48821

44.3

SGS Accutest






CT-ETPH (C9-C36) ND 18 mg/kg


84-15-1 o-Terphenyl 94% 50-137%


53 of 555

MC48821

44.3

SGS Accutest




Metals Analysis







Mercury <0.033 0.033 mg/kg 1 11/22/16 11/23/16 EAL SW846 7471B 2 SW846 7471B 4





54 of 555

MC48821

44.3

SGS Accutest




General Chemistry






pH 7.7 su 1 11/26/16 13:32 EL SW846 9045D


55 of 555

MC48821

44.3

SGS Accutest








Cadmium <0.0040 D006 1.0 0.0040 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3


Lead <0.010 D008 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3






56 of 555

MC48821

44.4

SGS Accutest





VOA RCP List




57 of 555

MC48821

44.5

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 5.2 ug/kg594-20-7 2,2-Dichloropropane ND 5.2 ug/kg563-58-6 1,1-Dichloropropene ND 5.2 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.1 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.1 ug/kg100-41-4 Ethylbenzene ND 2.1 ug/kg76-13-1 Freon 113 b ND 5.2 ug/kg87-68-3 Hexachlorobutadiene ND 5.2 ug/kg591-78-6 2-Hexanone ND 5.2 ug/kg98-82-8 Isopropylbenzene ND 5.2 ug/kg99-87-6 p-Isopropyltoluene ND 5.2 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.1 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.2 ug/kg74-95-3 Methylene bromide ND 5.2 ug/kg75-09-2 Methylene chloride ND 2.1 ug/kg91-20-3 Naphthalene ND 5.2 ug/kg103-65-1 n-Propylbenzene ND 5.2 ug/kg100-42-5 Styrene ND 5.2 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.1 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.2 ug/kg127-18-4 Tetrachloroethene ND 2.1 ug/kg109-99-9 Tetrahydrofuran ND 10 ug/kg108-88-3 Toluene ND 5.2 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 10 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.2 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.2 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.1 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.1 ug/kg79-01-6 Trichloroethene ND 2.1 ug/kg75-69-4 Trichlorofluoromethane ND 2.1 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.2 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.2 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.2 ug/kg75-01-4 Vinyl chloride ND 10 ug/kg





58 of 555

MC48821

44.5

SGS Accutest



VOA RCP List




standard.


59 of 555

MC48821

44.5

SGS Accutest





ABN RCP List




60 of 555

MC48821

44.5

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 270 ug/kg121-14-2 2,4-Dinitrotoluene ND 540 ug/kg606-20-2 2,6-Dinitrotoluene ND 540 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 540 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 110 ug/kg132-64-9 Dibenzofuran ND 110 ug/kg84-74-2 Di-n-butyl phthalate ND 270 ug/kg117-84-0 Di-n-octyl phthalate ND 270 ug/kg84-66-2 Diethyl phthalate ND 270 ug/kg131-11-3 Dimethyl phthalate ND 270 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 270 ug/kg206-44-0 Fluoranthene 129 110 ug/kg86-73-7 Fluorene ND 110 ug/kg118-74-1 Hexachlorobenzene ND 270 ug/kg87-68-3 Hexachlorobutadiene ND 270 ug/kg77-47-4 Hexachlorocyclopentadiene ND 540 ug/kg67-72-1 Hexachloroethane ND 270 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 270 ug/kg78-59-1 Isophorone ND 270 ug/kg91-57-6 2-Methylnaphthalene ND 110 ug/kg88-74-4 2-Nitroaniline ND 540 ug/kg99-09-2 3-Nitroaniline ND 540 ug/kg100-01-6 4-Nitroaniline ND 540 ug/kg91-20-3 Naphthalene ND 110 ug/kg98-95-3 Nitrobenzene ND 270 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 270 ug/kg86-30-6 N-Nitrosodiphenylamine ND 270 ug/kg82-68-8 Pentachloronitrobenzene ND 540 ug/kg85-01-8 Phenanthrene ND 110 ug/kg129-00-0 Pyrene 136 110 ug/kg110-86-1 Pyridine ND 540 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 540 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 270 ug/kg




61 of 555

MC48821

44.5

SGS Accutest



ABN RCP List




62 of 555

MC48821

44.5

SGS Accutest





Pesticide RCP List






63 of 555

MC48821

44.5

SGS Accutest











64 of 555

MC48821

44.5

SGS Accutest






CT-ETPH (C9-C36) 48.7 17 mg/kg


84-15-1 o-Terphenyl 81% 50-137%


65 of 555

MC48821

44.5

SGS Accutest




Metals Analysis












66 of 555

MC48821

44.5

SGS Accutest




General Chemistry






pH 7.5 su 1 11/26/16 13:32 EL SW846 9045D


67 of 555

MC48821

44.5

SGS Accutest







Barium <0.50 D005 100 0.50 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3









68 of 555

MC48821

44.6

SGS Accutest





VOA RCP List


67-64-1 Acetone ND 11 ug/kg107-13-1 Acrylonitrile ND 27 ug/kg71-43-2 Benzene ND 1.1 ug/kg108-86-1 Bromobenzene ND 5.5 ug/kg75-27-4 Bromodichloromethane ND 2.2 ug/kg75-25-2 Bromoform ND 2.2 ug/kg74-83-9 Bromomethane ND 11 ug/kg78-93-3 2-Butanone (MEK) ND 11 ug/kg104-51-8 n-Butylbenzene ND 5.5 ug/kg135-98-8 sec-Butylbenzene ND 5.5 ug/kg98-06-6 tert-Butylbenzene ND 5.5 ug/kg75-15-0 Carbon disulfide a ND 5.5 ug/kg56-23-5 Carbon tetrachloride ND 2.2 ug/kg108-90-7 Chlorobenzene ND 2.2 ug/kg75-00-3 Chloroethane ND 11 ug/kg67-66-3 Chloroform ND 2.2 ug/kg74-87-3 Chloromethane ND 5.5 ug/kg95-49-8 o-Chlorotoluene ND 5.5 ug/kg106-43-4 p-Chlorotoluene ND 5.5 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.5 ug/kg124-48-1 Dibromochloromethane ND 5.5 ug/kg106-93-4 1,2-Dibromoethane ND 2.2 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.2 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.2 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.2 ug/kg75-71-8 Dichlorodifluoromethane ND 5.5 ug/kg75-34-3 1,1-Dichloroethane ND 2.2 ug/kg107-06-2 1,2-Dichloroethane ND 2.2 ug/kg75-35-4 1,1-Dichloroethene a ND 2.2 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.2 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.2 ug/kg78-87-5 1,2-Dichloropropane ND 2.2 ug/kg


69 of 555

MC48821

44.7

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 5.5 ug/kg594-20-7 2,2-Dichloropropane ND 5.5 ug/kg563-58-6 1,1-Dichloropropene ND 5.5 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.2 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.2 ug/kg100-41-4 Ethylbenzene ND 2.2 ug/kg76-13-1 Freon 113 a ND 5.5 ug/kg87-68-3 Hexachlorobutadiene ND 5.5 ug/kg591-78-6 2-Hexanone ND 5.5 ug/kg98-82-8 Isopropylbenzene ND 5.5 ug/kg99-87-6 p-Isopropyltoluene ND 5.5 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.2 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.5 ug/kg74-95-3 Methylene bromide ND 5.5 ug/kg75-09-2 Methylene chloride ND 2.2 ug/kg91-20-3 Naphthalene ND 5.5 ug/kg103-65-1 n-Propylbenzene ND 5.5 ug/kg100-42-5 Styrene ND 5.5 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.2 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 ug/kg127-18-4 Tetrachloroethene ND 2.2 ug/kg109-99-9 Tetrahydrofuran ND 11 ug/kg108-88-3 Toluene ND 5.5 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 11 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.5 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.5 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.2 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.2 ug/kg79-01-6 Trichloroethene ND 2.2 ug/kg75-69-4 Trichlorofluoromethane ND 2.2 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.5 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.5 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.5 ug/kg75-01-4 Vinyl chloride ND 11 ug/kg





70 of 555

MC48821

44.7

SGS Accutest



VOA RCP List





71 of 555

MC48821

44.7

SGS Accutest





ABN RCP List




72 of 555

MC48821

44.7

SGS Accutest



ABN RCP List






73 of 555

MC48821

44.7

SGS Accutest



ABN RCP List




74 of 555

MC48821

44.7

SGS Accutest





Pesticide RCP List






75 of 555

MC48821

44.7

SGS Accutest











76 of 555

MC48821

44.7

SGS Accutest








84-15-1 o-Terphenyl 83% 50-137%


77 of 555

MC48821

44.7

SGS Accutest




Metals Analysis












78 of 555

MC48821

44.7

SGS Accutest




General Chemistry






pH 7.2 su 1 11/26/16 13:32 EL SW846 9045D


79 of 555

MC48821

44.7

SGS Accutest









Chromium 0.013 D007 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3







80 of 555

MC48821

44.8

SGS Accutest





VOA RCP List




81 of 555

MC48821

44.9

SGS Accutest



VOA RCP List







82 of 555

MC48821

44.9

SGS Accutest



VOA RCP List





83 of 555

MC48821

44.9

SGS Accutest





ABN RCP List




84 of 555

MC48821

44.9

SGS Accutest



ABN RCP List






85 of 555

MC48821

44.9

SGS Accutest



ABN RCP List




86 of 555

MC48821

44.9

SGS Accutest





Pesticide RCP List






87 of 555

MC48821

44.9

SGS Accutest











88 of 555

MC48821

44.9

SGS Accutest








84-15-1 o-Terphenyl 84% 50-137%


89 of 555

MC48821

44.9

SGS Accutest




Metals Analysis












90 of 555

MC48821

44.9

SGS Accutest




General Chemistry






pH 7.0 su 1 11/26/16 13:32 EL SW846 9045D


91 of 555

MC48821

44.9

SGS Accutest
















92 of 555

MC48821

44.10

SGS Accutest





VOA RCP List


67-64-1 Acetone ND 10 ug/kg107-13-1 Acrylonitrile ND 25 ug/kg71-43-2 Benzene ND 1.0 ug/kg108-86-1 Bromobenzene ND 5.1 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane ND 10 ug/kg78-93-3 2-Butanone (MEK) ND 10 ug/kg104-51-8 n-Butylbenzene ND 5.1 ug/kg135-98-8 sec-Butylbenzene ND 5.1 ug/kg98-06-6 tert-Butylbenzene ND 5.1 ug/kg75-15-0 Carbon disulfide a ND 5.1 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane ND 10 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane ND 5.1 ug/kg95-49-8 o-Chlorotoluene ND 5.1 ug/kg106-43-4 p-Chlorotoluene ND 5.1 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.1 ug/kg124-48-1 Dibromochloromethane ND 5.1 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane ND 5.1 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene a ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg


93 of 555

MC48821

44.11

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 5.1 ug/kg594-20-7 2,2-Dichloropropane ND 5.1 ug/kg563-58-6 1,1-Dichloropropene ND 5.1 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.0 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.0 ug/kg100-41-4 Ethylbenzene ND 2.0 ug/kg76-13-1 Freon 113 a ND 5.1 ug/kg87-68-3 Hexachlorobutadiene ND 5.1 ug/kg591-78-6 2-Hexanone ND 5.1 ug/kg98-82-8 Isopropylbenzene ND 5.1 ug/kg99-87-6 p-Isopropyltoluene ND 5.1 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.1 ug/kg74-95-3 Methylene bromide ND 5.1 ug/kg75-09-2 Methylene chloride ND 2.0 ug/kg91-20-3 Naphthalene ND 5.1 ug/kg103-65-1 n-Propylbenzene ND 5.1 ug/kg100-42-5 Styrene ND 5.1 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.1 ug/kg127-18-4 Tetrachloroethene ND 2.0 ug/kg109-99-9 Tetrahydrofuran ND 10 ug/kg108-88-3 Toluene ND 5.1 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 10 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.1 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.1 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.0 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.0 ug/kg79-01-6 Trichloroethene ND 2.0 ug/kg75-69-4 Trichlorofluoromethane ND 2.0 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.1 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.1 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.1 ug/kg75-01-4 Vinyl chloride ND 10 ug/kg





94 of 555

MC48821

44.11

SGS Accutest



VOA RCP List





95 of 555

MC48821

44.11

SGS Accutest





ABN RCP List




96 of 555

MC48821

44.11

SGS Accutest



ABN RCP List






97 of 555

MC48821

44.11

SGS Accutest



ABN RCP List




98 of 555

MC48821

44.11

SGS Accutest





Pesticide RCP List






99 of 555

MC48821

44.11

SGS Accutest











100 of 555

MC48821

44.11

SGS Accutest








84-15-1 o-Terphenyl 93% 50-137%


101 of 555

MC48821

44.11

SGS Accutest




Metals Analysis












102 of 555

MC48821

44.11

SGS Accutest




General Chemistry






pH 6.9 su 1 11/26/16 13:32 EL SW846 9045D


103 of 555

MC48821

44.11

SGS Accutest
















104 of 555

MC48821

44.12

SGS Accutest



File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 L101714.D 1 11/23/16 TB n/a n/a MSL4388Run #2

Initial Weight Final Volume Methanol AliquotRun #1 11.5 g 10.0 ml 100 ulRun #2

VOA RCP List


67-64-1 Acetone ND 630 ug/kg107-13-1 Acrylonitrile ND 1600 ug/kg71-43-2 Benzene 190 63 ug/kg108-86-1 Bromobenzene ND 310 ug/kg75-27-4 Bromodichloromethane ND 130 ug/kg75-25-2 Bromoform ND 130 ug/kg74-83-9 Bromomethane ND 630 ug/kg78-93-3 2-Butanone (MEK) ND 630 ug/kg104-51-8 n-Butylbenzene 3600 310 ug/kg135-98-8 sec-Butylbenzene 1830 310 ug/kg98-06-6 tert-Butylbenzene ND 310 ug/kg75-15-0 Carbon disulfide ND 310 ug/kg56-23-5 Carbon tetrachloride ND 130 ug/kg108-90-7 Chlorobenzene ND 130 ug/kg75-00-3 Chloroethane ND 630 ug/kg67-66-3 Chloroform ND 130 ug/kg74-87-3 Chloromethane ND 310 ug/kg95-49-8 o-Chlorotoluene ND 310 ug/kg106-43-4 p-Chlorotoluene ND 310 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 310 ug/kg124-48-1 Dibromochloromethane ND 310 ug/kg106-93-4 1,2-Dibromoethane ND 130 ug/kg95-50-1 1,2-Dichlorobenzene ND 130 ug/kg541-73-1 1,3-Dichlorobenzene ND 130 ug/kg106-46-7 1,4-Dichlorobenzene ND 130 ug/kg75-71-8 Dichlorodifluoromethane ND 310 ug/kg75-34-3 1,1-Dichloroethane ND 130 ug/kg107-06-2 1,2-Dichloroethane ND 130 ug/kg75-35-4 1,1-Dichloroethene a ND 130 ug/kg156-59-2 cis-1,2-Dichloroethene ND 130 ug/kg156-60-5 trans-1,2-Dichloroethene ND 130 ug/kg78-87-5 1,2-Dichloropropane ND 130 ug/kg


105 of 555

MC48821

44.13

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 310 ug/kg594-20-7 2,2-Dichloropropane ND 310 ug/kg563-58-6 1,1-Dichloropropene ND 310 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 130 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 130 ug/kg100-41-4 Ethylbenzene 650 130 ug/kg76-13-1 Freon 113 ND 310 ug/kg87-68-3 Hexachlorobutadiene ND 310 ug/kg591-78-6 2-Hexanone ND 310 ug/kg98-82-8 Isopropylbenzene 5230 310 ug/kg99-87-6 p-Isopropyltoluene ND 310 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 130 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 310 ug/kg74-95-3 Methylene bromide ND 310 ug/kg75-09-2 Methylene chloride ND 130 ug/kg91-20-3 Naphthalene 500 310 ug/kg103-65-1 n-Propylbenzene 16300 310 ug/kg100-42-5 Styrene ND 310 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 130 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 310 ug/kg127-18-4 Tetrachloroethene ND 130 ug/kg109-99-9 Tetrahydrofuran ND 630 ug/kg108-88-3 Toluene ND 310 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 630 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 310 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 310 ug/kg71-55-6 1,1,1-Trichloroethane ND 130 ug/kg79-00-5 1,1,2-Trichloroethane ND 130 ug/kg79-01-6 Trichloroethene ND 130 ug/kg75-69-4 Trichlorofluoromethane ND 130 ug/kg96-18-4 1,2,3-Trichloropropane ND 310 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 310 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 310 ug/kg75-01-4 Vinyl chloride ND 630 ug/kg

m,p-Xylene 316 130 ug/kg95-47-6 o-Xylene ND 130 ug/kg




106 of 555

MC48821

44.13

SGS Accutest



VOA RCP List





107 of 555

MC48821

44.13

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 2900 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 5700 ug/kg120-83-2 2,4-Dichlorophenol ND 5700 ug/kg105-67-9 2,4-Dimethylphenol ND 5700 ug/kg51-28-5 2,4-Dinitrophenol ND 5700 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 5700 ug/kg95-48-7 2-Methylphenol ND 5700 ug/kg106-44-5 4-Methylphenol ND 5700 ug/kg88-75-5 2-Nitrophenol ND 5700 ug/kg100-02-7 4-Nitrophenol ND 5700 ug/kg87-86-5 Pentachlorophenol ND 5700 ug/kg108-95-2 Phenol ND 2900 ug/kg95-95-4 2,4,5-Trichlorophenol ND 5700 ug/kg88-06-2 2,4,6-Trichlorophenol ND 5700 ug/kg83-32-9 Acenaphthene ND 1100 ug/kg208-96-8 Acenaphthylene 10600 1100 ug/kg62-53-3 Aniline ND 5700 ug/kg120-12-7 Anthracene 6330 1100 ug/kg56-55-3 Benzo(a)anthracene 21600 1100 ug/kg50-32-8 Benzo(a)pyrene 21600 2900 ug/kg205-99-2 Benzo(b)fluoranthene 20100 1100 ug/kg191-24-2 Benzo(g,h,i)perylene 14400 1100 ug/kg207-08-9 Benzo(k)fluoranthene 18600 1100 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 2900 ug/kg85-68-7 Butyl benzyl phthalate ND 2900 ug/kg91-58-7 2-Chloronaphthalene ND 2900 ug/kg106-47-8 4-Chloroaniline ND 5700 ug/kg86-74-8 Carbazole 2840 1100 ug/kg218-01-9 Chrysene 29500 1100 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 2900 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 2900 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 2900 ug/kg


108 of 555

MC48821

44.13

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 2900 ug/kg121-14-2 2,4-Dinitrotoluene ND 5700 ug/kg606-20-2 2,6-Dinitrotoluene ND 5700 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 5700 ug/kg53-70-3 Dibenzo(a,h)anthracene 3650 1100 ug/kg132-64-9 Dibenzofuran 1360 1100 ug/kg84-74-2 Di-n-butyl phthalate ND 2900 ug/kg117-84-0 Di-n-octyl phthalate ND 2900 ug/kg84-66-2 Diethyl phthalate ND 2900 ug/kg131-11-3 Dimethyl phthalate ND 2900 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 2900 ug/kg206-44-0 Fluoranthene 59500 1100 ug/kg86-73-7 Fluorene 5280 1100 ug/kg118-74-1 Hexachlorobenzene ND 2900 ug/kg87-68-3 Hexachlorobutadiene ND 2900 ug/kg77-47-4 Hexachlorocyclopentadiene ND 5700 ug/kg67-72-1 Hexachloroethane ND 2900 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 14100 2900 ug/kg78-59-1 Isophorone ND 2900 ug/kg91-57-6 2-Methylnaphthalene 1190 1100 ug/kg88-74-4 2-Nitroaniline ND 5700 ug/kg99-09-2 3-Nitroaniline ND 5700 ug/kg100-01-6 4-Nitroaniline ND 5700 ug/kg91-20-3 Naphthalene ND 1100 ug/kg98-95-3 Nitrobenzene ND 2900 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 2900 ug/kg86-30-6 N-Nitrosodiphenylamine ND 2900 ug/kg82-68-8 Pentachloronitrobenzene ND 5700 ug/kg85-01-8 Phenanthrene 40300 1100 ug/kg129-00-0 Pyrene 57000 1100 ug/kg110-86-1 Pyridine ND 5700 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 5700 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 2900 ug/kg




109 of 555

MC48821

44.13

SGS Accutest



ABN RCP List




110 of 555

MC48821

44.13

SGS Accutest





Pesticide RCP List







111 of 555

MC48821

44.13

SGS Accutest







12674-11-2 Aroclor 1016 ND 29 ug/kg11104-28-2 Aroclor 1221 ND 29 ug/kg11141-16-5 Aroclor 1232 ND 29 ug/kg53469-21-9 Aroclor 1242 ND 29 ug/kg12672-29-6 Aroclor 1248 ND 29 ug/kg11097-69-1 Aroclor 1254 ND 29 ug/kg11096-82-5 Aroclor 1260 ND 29 ug/kg37324-23-5 Aroclor 1262 60.0 29 ug/kg11100-14-4 Aroclor 1268 ND 29 ug/kg




112 of 555

MC48821

44.13

SGS Accutest








84-15-1 o-Terphenyl 96% 50-137%


113 of 555

MC48821

44.13

SGS Accutest




Metals Analysis




Cadmium 0.43 0.39 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3


Lead 543 0.97 mg/kg 1 11/22/16 11/22/16 EAL SW846 6010C 1 SW846 3050B 3






114 of 555

MC48821

44.13

SGS Accutest




General Chemistry






pH 7.0 su 1 11/26/16 13:32 EL SW846 9045D


115 of 555

MC48821

44.13

SGS Accutest
















116 of 555

MC48821

44.14

SGS Accutest





VOA RCP List


67-64-1 Acetone ND 600 ug/kg107-13-1 Acrylonitrile ND 1500 ug/kg71-43-2 Benzene ND 60 ug/kg108-86-1 Bromobenzene ND 300 ug/kg75-27-4 Bromodichloromethane ND 120 ug/kg75-25-2 Bromoform ND 120 ug/kg74-83-9 Bromomethane ND 600 ug/kg78-93-3 2-Butanone (MEK) ND 600 ug/kg104-51-8 n-Butylbenzene 1700 300 ug/kg135-98-8 sec-Butylbenzene 631 300 ug/kg98-06-6 tert-Butylbenzene ND 300 ug/kg75-15-0 Carbon disulfide ND 300 ug/kg56-23-5 Carbon tetrachloride ND 120 ug/kg108-90-7 Chlorobenzene ND 120 ug/kg75-00-3 Chloroethane ND 600 ug/kg67-66-3 Chloroform ND 120 ug/kg74-87-3 Chloromethane ND 300 ug/kg95-49-8 o-Chlorotoluene ND 300 ug/kg106-43-4 p-Chlorotoluene ND 300 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 300 ug/kg124-48-1 Dibromochloromethane ND 300 ug/kg106-93-4 1,2-Dibromoethane ND 120 ug/kg95-50-1 1,2-Dichlorobenzene ND 120 ug/kg541-73-1 1,3-Dichlorobenzene ND 120 ug/kg106-46-7 1,4-Dichlorobenzene ND 120 ug/kg75-71-8 Dichlorodifluoromethane ND 300 ug/kg75-34-3 1,1-Dichloroethane ND 120 ug/kg107-06-2 1,2-Dichloroethane ND 120 ug/kg75-35-4 1,1-Dichloroethene a ND 120 ug/kg156-59-2 cis-1,2-Dichloroethene ND 120 ug/kg156-60-5 trans-1,2-Dichloroethene ND 120 ug/kg78-87-5 1,2-Dichloropropane ND 120 ug/kg


117 of 555

MC48821

44.15

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 300 ug/kg594-20-7 2,2-Dichloropropane ND 300 ug/kg563-58-6 1,1-Dichloropropene ND 300 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 120 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 120 ug/kg100-41-4 Ethylbenzene 4260 120 ug/kg76-13-1 Freon 113 ND 300 ug/kg87-68-3 Hexachlorobutadiene ND 300 ug/kg591-78-6 2-Hexanone ND 300 ug/kg98-82-8 Isopropylbenzene 1530 300 ug/kg99-87-6 p-Isopropyltoluene 388 300 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 120 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 300 ug/kg74-95-3 Methylene bromide ND 300 ug/kg75-09-2 Methylene chloride ND 120 ug/kg91-20-3 Naphthalene 2390 300 ug/kg103-65-1 n-Propylbenzene 5270 300 ug/kg100-42-5 Styrene ND 300 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 120 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 300 ug/kg127-18-4 Tetrachloroethene ND 120 ug/kg109-99-9 Tetrahydrofuran ND 600 ug/kg108-88-3 Toluene ND 300 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 600 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 300 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 300 ug/kg71-55-6 1,1,1-Trichloroethane ND 120 ug/kg79-00-5 1,1,2-Trichloroethane ND 120 ug/kg79-01-6 Trichloroethene ND 120 ug/kg75-69-4 Trichlorofluoromethane ND 120 ug/kg96-18-4 1,2,3-Trichloropropane ND 300 ug/kg95-63-6 1,2,4-Trimethylbenzene b 15000 300 ug/kg108-67-8 1,3,5-Trimethylbenzene 4350 300 ug/kg75-01-4 Vinyl chloride ND 600 ug/kg

m,p-Xylene 8070 120 ug/kg95-47-6 o-Xylene 2430 120 ug/kg




118 of 555

MC48821

44.15

SGS Accutest



VOA RCP List




(b) Continuing Calibration outside of acceptance criteria. Result may be biased high.


119 of 555

MC48821

44.15

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 270 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 540 ug/kg120-83-2 2,4-Dichlorophenol ND 540 ug/kg105-67-9 2,4-Dimethylphenol ND 540 ug/kg51-28-5 2,4-Dinitrophenol ND 540 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 540 ug/kg95-48-7 2-Methylphenol ND 540 ug/kg106-44-5 4-Methylphenol ND 540 ug/kg88-75-5 2-Nitrophenol ND 540 ug/kg100-02-7 4-Nitrophenol ND 540 ug/kg87-86-5 Pentachlorophenol ND 540 ug/kg108-95-2 Phenol ND 270 ug/kg95-95-4 2,4,5-Trichlorophenol ND 540 ug/kg88-06-2 2,4,6-Trichlorophenol ND 540 ug/kg83-32-9 Acenaphthene 111 110 ug/kg208-96-8 Acenaphthylene ND 110 ug/kg62-53-3 Aniline ND 540 ug/kg120-12-7 Anthracene ND 110 ug/kg56-55-3 Benzo(a)anthracene ND 110 ug/kg50-32-8 Benzo(a)pyrene ND 270 ug/kg205-99-2 Benzo(b)fluoranthene ND 110 ug/kg191-24-2 Benzo(g,h,i)perylene ND 110 ug/kg207-08-9 Benzo(k)fluoranthene ND 110 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 270 ug/kg85-68-7 Butyl benzyl phthalate ND 270 ug/kg91-58-7 2-Chloronaphthalene ND 270 ug/kg106-47-8 4-Chloroaniline ND 540 ug/kg86-74-8 Carbazole ND 110 ug/kg218-01-9 Chrysene ND 110 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 270 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 270 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 270 ug/kg


120 of 555

MC48821

44.15

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 270 ug/kg121-14-2 2,4-Dinitrotoluene ND 540 ug/kg606-20-2 2,6-Dinitrotoluene ND 540 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 540 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 110 ug/kg132-64-9 Dibenzofuran ND 110 ug/kg84-74-2 Di-n-butyl phthalate ND 270 ug/kg117-84-0 Di-n-octyl phthalate ND 270 ug/kg84-66-2 Diethyl phthalate ND 270 ug/kg131-11-3 Dimethyl phthalate ND 270 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 270 ug/kg206-44-0 Fluoranthene 133 110 ug/kg86-73-7 Fluorene 152 110 ug/kg118-74-1 Hexachlorobenzene ND 270 ug/kg87-68-3 Hexachlorobutadiene ND 270 ug/kg77-47-4 Hexachlorocyclopentadiene ND 540 ug/kg67-72-1 Hexachloroethane ND 270 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 270 ug/kg78-59-1 Isophorone ND 270 ug/kg91-57-6 2-Methylnaphthalene 5440 110 ug/kg88-74-4 2-Nitroaniline ND 540 ug/kg99-09-2 3-Nitroaniline ND 540 ug/kg100-01-6 4-Nitroaniline ND 540 ug/kg91-20-3 Naphthalene 7690 110 ug/kg98-95-3 Nitrobenzene ND 270 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 270 ug/kg86-30-6 N-Nitrosodiphenylamine ND 270 ug/kg82-68-8 Pentachloronitrobenzene ND 540 ug/kg85-01-8 Phenanthrene 289 110 ug/kg129-00-0 Pyrene ND 110 ug/kg110-86-1 Pyridine ND 540 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 540 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 270 ug/kg




121 of 555

MC48821

44.15

SGS Accutest



ABN RCP List




122 of 555

MC48821

44.15

SGS Accutest





Pesticide RCP List






123 of 555

MC48821

44.15

SGS Accutest











124 of 555

MC48821

44.15

SGS Accutest








84-15-1 o-Terphenyl 91% 50-137%


125 of 555

MC48821

44.15

SGS Accutest




Metals Analysis












126 of 555

MC48821

44.15

SGS Accutest




General Chemistry






pH 7.8 su 1 11/26/16 13:32 EL SW846 9045D


127 of 555

MC48821

44.15

SGS Accutest









Chromium 0.022 D007 5.0 0.010 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3







128 of 555

MC48821

44.16

SGS Accutest





VOA RCP List




129 of 555

MC48821

44.17

SGS Accutest



VOA RCP List







130 of 555

MC48821

44.17

SGS Accutest



VOA RCP List




standard.


131 of 555

MC48821

44.17

SGS Accutest





ABN RCP List




132 of 555

MC48821

44.17

SGS Accutest



ABN RCP List






133 of 555

MC48821

44.17

SGS Accutest



ABN RCP List




134 of 555

MC48821

44.17

SGS Accutest





Pesticide RCP List






135 of 555

MC48821

44.17

SGS Accutest







12674-11-2 Aroclor 1016 ND 26 ug/kg11104-28-2 Aroclor 1221 ND 26 ug/kg11141-16-5 Aroclor 1232 ND 26 ug/kg53469-21-9 Aroclor 1242 ND 26 ug/kg12672-29-6 Aroclor 1248 ND 26 ug/kg11097-69-1 Aroclor 1254 ND 26 ug/kg11096-82-5 Aroclor 1260 a 32.1 26 ug/kg37324-23-5 Aroclor 1262 ND 26 ug/kg11100-14-4 Aroclor 1268 ND 26 ug/kg



(a) Confirmation value >40% RPD.


136 of 555

MC48821

44.17

SGS Accutest








84-15-1 o-Terphenyl 87% 50-137%


137 of 555

MC48821

44.17

SGS Accutest




Metals Analysis












138 of 555

MC48821

44.17

SGS Accutest




General Chemistry






pH 7.0 su 1 11/26/16 13:32 EL SW846 9045D


139 of 555

MC48821

44.17

SGS Accutest
















140 of 555

MC48821

44.18

SGS Accutest





VOA RCP List




141 of 555

MC48821

44.19

SGS Accutest



VOA RCP List







142 of 555

MC48821

44.19

SGS Accutest



VOA RCP List





143 of 555

MC48821

44.19

SGS Accutest





ABN RCP List




144 of 555

MC48821

44.19

SGS Accutest



ABN RCP List






145 of 555

MC48821

44.19

SGS Accutest



ABN RCP List




146 of 555

MC48821

44.19

SGS Accutest





Pesticide RCP List






147 of 555

MC48821

44.19

SGS Accutest











148 of 555

MC48821

44.19

SGS Accutest








84-15-1 o-Terphenyl 84% 50-137%


149 of 555

MC48821

44.19

SGS Accutest




Metals Analysis












150 of 555

MC48821

44.19

SGS Accutest




General Chemistry






pH 8.7 su 1 11/26/16 13:32 EL SW846 9045D


151 of 555

MC48821

44.19

SGS Accutest
















152 of 555

MC48821

44.20

SGS Accutest





VOA RCP List




153 of 555

MC48821

44.21

SGS Accutest



VOA RCP List







154 of 555

MC48821

44.21

SGS Accutest



VOA RCP List




standard.


155 of 555

MC48821

44.21

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 290 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 580 ug/kg120-83-2 2,4-Dichlorophenol ND 580 ug/kg105-67-9 2,4-Dimethylphenol ND 580 ug/kg51-28-5 2,4-Dinitrophenol ND 580 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 580 ug/kg95-48-7 2-Methylphenol ND 580 ug/kg106-44-5 4-Methylphenol ND 580 ug/kg88-75-5 2-Nitrophenol ND 580 ug/kg100-02-7 4-Nitrophenol ND 580 ug/kg87-86-5 Pentachlorophenol ND 580 ug/kg108-95-2 Phenol ND 290 ug/kg95-95-4 2,4,5-Trichlorophenol ND 580 ug/kg88-06-2 2,4,6-Trichlorophenol ND 580 ug/kg83-32-9 Acenaphthene ND 120 ug/kg208-96-8 Acenaphthylene 808 120 ug/kg62-53-3 Aniline ND 580 ug/kg120-12-7 Anthracene 326 120 ug/kg56-55-3 Benzo(a)anthracene 1990 120 ug/kg50-32-8 Benzo(a)pyrene 2030 290 ug/kg205-99-2 Benzo(b)fluoranthene 1900 120 ug/kg191-24-2 Benzo(g,h,i)perylene 1340 120 ug/kg207-08-9 Benzo(k)fluoranthene 1690 120 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 290 ug/kg85-68-7 Butyl benzyl phthalate ND 290 ug/kg91-58-7 2-Chloronaphthalene ND 290 ug/kg106-47-8 4-Chloroaniline ND 580 ug/kg86-74-8 Carbazole ND 120 ug/kg218-01-9 Chrysene 2470 120 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 290 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 290 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 290 ug/kg


156 of 555

MC48821

44.21

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 290 ug/kg121-14-2 2,4-Dinitrotoluene ND 580 ug/kg606-20-2 2,6-Dinitrotoluene ND 580 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 580 ug/kg53-70-3 Dibenzo(a,h)anthracene 334 120 ug/kg132-64-9 Dibenzofuran ND 120 ug/kg84-74-2 Di-n-butyl phthalate ND 290 ug/kg117-84-0 Di-n-octyl phthalate ND 290 ug/kg84-66-2 Diethyl phthalate ND 290 ug/kg131-11-3 Dimethyl phthalate ND 290 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 290 ug/kg206-44-0 Fluoranthene 3970 120 ug/kg86-73-7 Fluorene ND 120 ug/kg118-74-1 Hexachlorobenzene ND 290 ug/kg87-68-3 Hexachlorobutadiene ND 290 ug/kg77-47-4 Hexachlorocyclopentadiene ND 580 ug/kg67-72-1 Hexachloroethane ND 290 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 1290 290 ug/kg78-59-1 Isophorone ND 290 ug/kg91-57-6 2-Methylnaphthalene ND 120 ug/kg88-74-4 2-Nitroaniline ND 580 ug/kg99-09-2 3-Nitroaniline ND 580 ug/kg100-01-6 4-Nitroaniline ND 580 ug/kg91-20-3 Naphthalene ND 120 ug/kg98-95-3 Nitrobenzene ND 290 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 290 ug/kg86-30-6 N-Nitrosodiphenylamine ND 290 ug/kg82-68-8 Pentachloronitrobenzene ND 580 ug/kg85-01-8 Phenanthrene 1390 120 ug/kg129-00-0 Pyrene 4330 120 ug/kg110-86-1 Pyridine ND 580 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 580 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 290 ug/kg




157 of 555

MC48821

44.21

SGS Accutest



ABN RCP List




158 of 555

MC48821

44.21

SGS Accutest





Pesticide RCP List




877-09-8 Tetrachloro-m-xylene 41% 10-143%877-09-8 Tetrachloro-m-xylene 51% 10-143%2051-24-3 Decachlorobiphenyl 176% a 10-172%2051-24-3 Decachlorobiphenyl 275% a 10-172%



159 of 555

MC48821

44.21

SGS Accutest



File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 BB70557.D 1 11/28/16 TA 11/23/16 OP49200 GBB3722Run #2








160 of 555

MC48821

44.21

SGS Accutest








84-15-1 o-Terphenyl 108% 50-137%


161 of 555

MC48821

44.21

SGS Accutest




Metals Analysis












162 of 555

MC48821

44.21

SGS Accutest




General Chemistry






pH 7.7 su 1 11/26/16 13:32 EL SW846 9045D


163 of 555

MC48821

44.21

SGS Accutest
















164 of 555

MC48821

44.22

SGS Accutest





VOA RCP List




165 of 555

MC48821

44.23

SGS Accutest



VOA RCP List







166 of 555

MC48821

44.23

SGS Accutest



VOA RCP List





167 of 555

MC48821

44.23

SGS Accutest





ABN RCP List




168 of 555

MC48821

44.23

SGS Accutest



ABN RCP List






169 of 555

MC48821

44.23

SGS Accutest



ABN RCP List




170 of 555

MC48821

44.23

SGS Accutest





Pesticide RCP List






171 of 555

MC48821

44.23

SGS Accutest











172 of 555

MC48821

44.23

SGS Accutest








84-15-1 o-Terphenyl 87% 50-137%


173 of 555

MC48821

44.23

SGS Accutest




Metals Analysis












174 of 555

MC48821

44.23

SGS Accutest




General Chemistry






pH 7.8 su 1 11/26/16 13:32 EL SW846 9045D


175 of 555

MC48821

44.23

SGS Accutest
















176 of 555

MC48821

44.24

SGS Accutest





VOA RCP List




177 of 555

MC48821

44.25

SGS Accutest



VOA RCP List







178 of 555

MC48821

44.25

SGS Accutest



VOA RCP List




standard.


179 of 555

MC48821

44.25

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 270 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 540 ug/kg120-83-2 2,4-Dichlorophenol ND 540 ug/kg105-67-9 2,4-Dimethylphenol ND 540 ug/kg51-28-5 2,4-Dinitrophenol ND 540 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 540 ug/kg95-48-7 2-Methylphenol ND 540 ug/kg106-44-5 4-Methylphenol ND 540 ug/kg88-75-5 2-Nitrophenol ND 540 ug/kg100-02-7 4-Nitrophenol ND 540 ug/kg87-86-5 Pentachlorophenol ND 540 ug/kg108-95-2 Phenol ND 270 ug/kg95-95-4 2,4,5-Trichlorophenol ND 540 ug/kg88-06-2 2,4,6-Trichlorophenol ND 540 ug/kg83-32-9 Acenaphthene ND 110 ug/kg208-96-8 Acenaphthylene ND 110 ug/kg62-53-3 Aniline ND 540 ug/kg120-12-7 Anthracene ND 110 ug/kg56-55-3 Benzo(a)anthracene 202 110 ug/kg50-32-8 Benzo(a)pyrene ND 270 ug/kg205-99-2 Benzo(b)fluoranthene 191 110 ug/kg191-24-2 Benzo(g,h,i)perylene 132 110 ug/kg207-08-9 Benzo(k)fluoranthene 161 110 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 270 ug/kg85-68-7 Butyl benzyl phthalate ND 270 ug/kg91-58-7 2-Chloronaphthalene ND 270 ug/kg106-47-8 4-Chloroaniline ND 540 ug/kg86-74-8 Carbazole ND 110 ug/kg218-01-9 Chrysene 226 110 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 270 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 270 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 270 ug/kg


180 of 555

MC48821

44.25

SGS Accutest



ABN RCP List






181 of 555

MC48821

44.25

SGS Accutest



ABN RCP List




182 of 555

MC48821

44.25

SGS Accutest



File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 BE53534.D 1 11/29/16 TA 11/23/16 OP49201 GBE2693Run #2 BE53522.D 5 11/29/16 TA 11/23/16 OP49201 GBE2693


Pesticide RCP List


15972-60-8 Alachlor ND 56 ug/kg309-00-2 Aldrin ND 5.6 ug/kg319-84-6 alpha-BHC ND 5.6 ug/kg319-85-7 beta-BHC ND 5.6 ug/kg319-86-8 delta-BHC ND 5.6 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.6 ug/kg12789-03-6 Chlordane ND 56 ug/kg60-57-1 Dieldrin ND 5.6 ug/kg72-54-8 4,4'-DDD 44.8 5.6 ug/kg72-55-9 4,4'-DDE a 278 b 28 ug/kg50-29-3 4,4'-DDT 575 b 28 ug/kg72-20-8 Endrin ND 5.6 ug/kg1031-07-8 Endosulfan sulfate ND 5.6 ug/kg7421-93-4 Endrin aldehyde ND 5.6 ug/kg959-98-8 Endosulfan-I ND 5.6 ug/kg33213-65-9 Endosulfan-II ND 5.6 ug/kg76-44-8 Heptachlor ND 5.6 ug/kg1024-57-3 Heptachlor epoxide ND 5.6 ug/kg72-43-5 Methoxychlor ND 5.6 ug/kg53494-70-5 Endrin ketone ND 5.6 ug/kg8001-35-2 Toxaphene ND 56 ug/kg


877-09-8 Tetrachloro-m-xylene 62% 84% 10-143%877-09-8 Tetrachloro-m-xylene 61% 77% 10-143%2051-24-3 Decachlorobiphenyl 60% 126% 10-172%2051-24-3 Decachlorobiphenyl 71% 115% 10-172%

(a) Confirmation value >40% RPD.(b) Result is from Run# 2


183 of 555

MC48821

44.25

SGS Accutest











184 of 555

MC48821

44.25

SGS Accutest








84-15-1 o-Terphenyl 93% 50-137%


185 of 555

MC48821

44.25

SGS Accutest




Metals Analysis












186 of 555

MC48821

44.25

SGS Accutest
















187 of 555

MC48821

44.26

SGS Accutest





VOA RCP List




188 of 555

MC48821

44.27

SGS Accutest



VOA RCP List







189 of 555

MC48821

44.27

SGS Accutest



VOA RCP List




standard.


190 of 555

MC48821

44.27

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 260 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 510 ug/kg120-83-2 2,4-Dichlorophenol ND 510 ug/kg105-67-9 2,4-Dimethylphenol ND 510 ug/kg51-28-5 2,4-Dinitrophenol ND 510 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 510 ug/kg95-48-7 2-Methylphenol ND 510 ug/kg106-44-5 4-Methylphenol ND 510 ug/kg88-75-5 2-Nitrophenol ND 510 ug/kg100-02-7 4-Nitrophenol ND 510 ug/kg87-86-5 Pentachlorophenol ND 510 ug/kg108-95-2 Phenol ND 260 ug/kg95-95-4 2,4,5-Trichlorophenol ND 510 ug/kg88-06-2 2,4,6-Trichlorophenol ND 510 ug/kg83-32-9 Acenaphthene 154 100 ug/kg208-96-8 Acenaphthylene ND 100 ug/kg62-53-3 Aniline ND 510 ug/kg120-12-7 Anthracene 392 100 ug/kg56-55-3 Benzo(a)anthracene 1310 100 ug/kg50-32-8 Benzo(a)pyrene 1130 260 ug/kg205-99-2 Benzo(b)fluoranthene 1080 100 ug/kg191-24-2 Benzo(g,h,i)perylene 663 100 ug/kg207-08-9 Benzo(k)fluoranthene 960 100 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 260 ug/kg85-68-7 Butyl benzyl phthalate ND 260 ug/kg91-58-7 2-Chloronaphthalene ND 260 ug/kg106-47-8 4-Chloroaniline ND 510 ug/kg86-74-8 Carbazole 228 100 ug/kg218-01-9 Chrysene 1460 100 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 260 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 260 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 260 ug/kg


191 of 555

MC48821

44.27

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 260 ug/kg121-14-2 2,4-Dinitrotoluene ND 510 ug/kg606-20-2 2,6-Dinitrotoluene ND 510 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 510 ug/kg53-70-3 Dibenzo(a,h)anthracene 177 100 ug/kg132-64-9 Dibenzofuran 111 100 ug/kg84-74-2 Di-n-butyl phthalate ND 260 ug/kg117-84-0 Di-n-octyl phthalate ND 260 ug/kg84-66-2 Diethyl phthalate ND 260 ug/kg131-11-3 Dimethyl phthalate ND 260 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 260 ug/kg206-44-0 Fluoranthene 3100 100 ug/kg86-73-7 Fluorene 138 100 ug/kg118-74-1 Hexachlorobenzene ND 260 ug/kg87-68-3 Hexachlorobutadiene ND 260 ug/kg77-47-4 Hexachlorocyclopentadiene ND 510 ug/kg67-72-1 Hexachloroethane ND 260 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 674 260 ug/kg78-59-1 Isophorone ND 260 ug/kg91-57-6 2-Methylnaphthalene ND 100 ug/kg88-74-4 2-Nitroaniline ND 510 ug/kg99-09-2 3-Nitroaniline ND 510 ug/kg100-01-6 4-Nitroaniline ND 510 ug/kg91-20-3 Naphthalene ND 100 ug/kg98-95-3 Nitrobenzene ND 260 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 260 ug/kg86-30-6 N-Nitrosodiphenylamine ND 260 ug/kg82-68-8 Pentachloronitrobenzene ND 510 ug/kg85-01-8 Phenanthrene 2270 100 ug/kg129-00-0 Pyrene 2830 100 ug/kg110-86-1 Pyridine ND 510 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 510 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 260 ug/kg




192 of 555

MC48821

44.27

SGS Accutest



ABN RCP List




193 of 555

MC48821

44.27

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 51 ug/kg309-00-2 Aldrin ND 5.1 ug/kg319-84-6 alpha-BHC ND 5.1 ug/kg319-85-7 beta-BHC ND 5.1 ug/kg319-86-8 delta-BHC ND 5.1 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.1 ug/kg12789-03-6 Chlordane ND 51 ug/kg60-57-1 Dieldrin ND 5.1 ug/kg72-54-8 4,4'-DDD 9.3 5.1 ug/kg72-55-9 4,4'-DDE a 87.8 b 26 ug/kg50-29-3 4,4'-DDT 190 b 26 ug/kg72-20-8 Endrin ND 5.1 ug/kg1031-07-8 Endosulfan sulfate ND 5.1 ug/kg7421-93-4 Endrin aldehyde ND 5.1 ug/kg959-98-8 Endosulfan-I ND 5.1 ug/kg33213-65-9 Endosulfan-II ND 5.1 ug/kg76-44-8 Heptachlor ND 5.1 ug/kg1024-57-3 Heptachlor epoxide ND 5.1 ug/kg72-43-5 Methoxychlor ND 5.1 ug/kg53494-70-5 Endrin ketone ND 5.1 ug/kg8001-35-2 Toxaphene ND 51 ug/kg





194 of 555

MC48821

44.27

SGS Accutest







12674-11-2 Aroclor 1016 ND 26 ug/kg11104-28-2 Aroclor 1221 ND 26 ug/kg11141-16-5 Aroclor 1232 ND 26 ug/kg53469-21-9 Aroclor 1242 83.7 26 ug/kg12672-29-6 Aroclor 1248 ND 26 ug/kg11097-69-1 Aroclor 1254 ND 26 ug/kg11096-82-5 Aroclor 1260 ND 26 ug/kg37324-23-5 Aroclor 1262 ND 26 ug/kg11100-14-4 Aroclor 1268 ND 26 ug/kg




195 of 555

MC48821

44.27

SGS Accutest








84-15-1 o-Terphenyl 89% 50-137%


196 of 555

MC48821

44.27

SGS Accutest




Metals Analysis












197 of 555

MC48821

44.27

SGS Accutest




General Chemistry






pH 6.8 su 1 11/26/16 13:32 EL SW846 9045D


198 of 555

MC48821

44.27

SGS Accutest
















199 of 555

MC48821

44.28

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8260C Percent Solids: 95.5 Project: Route 69 Improvements, New Haven, CT



VOA RCP List


67-64-1 Acetone ND 9.0 ug/kg107-13-1 Acrylonitrile ND 23 ug/kg71-43-2 Benzene ND 0.90 ug/kg108-86-1 Bromobenzene ND 4.5 ug/kg75-27-4 Bromodichloromethane ND 1.8 ug/kg75-25-2 Bromoform ND 1.8 ug/kg74-83-9 Bromomethane ND 9.0 ug/kg78-93-3 2-Butanone (MEK) ND 9.0 ug/kg104-51-8 n-Butylbenzene ND 4.5 ug/kg135-98-8 sec-Butylbenzene ND 4.5 ug/kg98-06-6 tert-Butylbenzene ND 4.5 ug/kg75-15-0 Carbon disulfide b ND 4.5 ug/kg56-23-5 Carbon tetrachloride ND 1.8 ug/kg108-90-7 Chlorobenzene ND 1.8 ug/kg75-00-3 Chloroethane ND 9.0 ug/kg67-66-3 Chloroform ND 1.8 ug/kg74-87-3 Chloromethane ND 4.5 ug/kg95-49-8 o-Chlorotoluene ND 4.5 ug/kg106-43-4 p-Chlorotoluene ND 4.5 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 4.5 ug/kg124-48-1 Dibromochloromethane ND 4.5 ug/kg106-93-4 1,2-Dibromoethane ND 1.8 ug/kg95-50-1 1,2-Dichlorobenzene ND 1.8 ug/kg541-73-1 1,3-Dichlorobenzene ND 1.8 ug/kg106-46-7 1,4-Dichlorobenzene ND 1.8 ug/kg75-71-8 Dichlorodifluoromethane ND 4.5 ug/kg75-34-3 1,1-Dichloroethane ND 1.8 ug/kg107-06-2 1,2-Dichloroethane ND 1.8 ug/kg75-35-4 1,1-Dichloroethene b ND 1.8 ug/kg156-59-2 cis-1,2-Dichloroethene ND 1.8 ug/kg156-60-5 trans-1,2-Dichloroethene ND 1.8 ug/kg78-87-5 1,2-Dichloropropane ND 1.8 ug/kg


200 of 555

MC48821

44.29

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 4.5 ug/kg594-20-7 2,2-Dichloropropane ND 4.5 ug/kg563-58-6 1,1-Dichloropropene ND 4.5 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 1.8 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 1.8 ug/kg100-41-4 Ethylbenzene ND 1.8 ug/kg76-13-1 Freon 113 b ND 4.5 ug/kg87-68-3 Hexachlorobutadiene ND 4.5 ug/kg591-78-6 2-Hexanone ND 4.5 ug/kg98-82-8 Isopropylbenzene ND 4.5 ug/kg99-87-6 p-Isopropyltoluene ND 4.5 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 1.8 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 4.5 ug/kg74-95-3 Methylene bromide ND 4.5 ug/kg75-09-2 Methylene chloride ND 1.8 ug/kg91-20-3 Naphthalene ND 4.5 ug/kg103-65-1 n-Propylbenzene ND 4.5 ug/kg100-42-5 Styrene ND 4.5 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 1.8 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 4.5 ug/kg127-18-4 Tetrachloroethene ND 1.8 ug/kg109-99-9 Tetrahydrofuran ND 9.0 ug/kg108-88-3 Toluene ND 4.5 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 9.0 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 4.5 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 4.5 ug/kg71-55-6 1,1,1-Trichloroethane ND 1.8 ug/kg79-00-5 1,1,2-Trichloroethane ND 1.8 ug/kg79-01-6 Trichloroethene ND 1.8 ug/kg75-69-4 Trichlorofluoromethane ND 1.8 ug/kg96-18-4 1,2,3-Trichloropropane ND 4.5 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 4.5 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 4.5 ug/kg75-01-4 Vinyl chloride ND 9.0 ug/kg





201 of 555

MC48821

44.29

SGS Accutest



VOA RCP List




standard.


202 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8270D SW846 3546 Percent Solids: 95.5 Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 a R50933.D 5 11/29/16 MR 11/23/16 OP49195 MSR1899Run #2


ABN RCP List


95-57-8 2-Chlorophenol ND 1300 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 2600 ug/kg120-83-2 2,4-Dichlorophenol ND 2600 ug/kg105-67-9 2,4-Dimethylphenol ND 2600 ug/kg51-28-5 2,4-Dinitrophenol ND 2600 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 2600 ug/kg95-48-7 2-Methylphenol ND 2600 ug/kg106-44-5 4-Methylphenol ND 2600 ug/kg88-75-5 2-Nitrophenol ND 2600 ug/kg100-02-7 4-Nitrophenol ND 2600 ug/kg87-86-5 Pentachlorophenol ND 2600 ug/kg108-95-2 Phenol ND 1300 ug/kg95-95-4 2,4,5-Trichlorophenol ND 2600 ug/kg88-06-2 2,4,6-Trichlorophenol ND 2600 ug/kg83-32-9 Acenaphthene ND 520 ug/kg208-96-8 Acenaphthylene 826 520 ug/kg62-53-3 Aniline ND 2600 ug/kg120-12-7 Anthracene ND 520 ug/kg56-55-3 Benzo(a)anthracene 1330 520 ug/kg50-32-8 Benzo(a)pyrene 1670 1300 ug/kg205-99-2 Benzo(b)fluoranthene 1460 520 ug/kg191-24-2 Benzo(g,h,i)perylene 1500 520 ug/kg207-08-9 Benzo(k)fluoranthene 1420 520 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 1300 ug/kg85-68-7 Butyl benzyl phthalate ND 1300 ug/kg91-58-7 2-Chloronaphthalene ND 1300 ug/kg106-47-8 4-Chloroaniline ND 2600 ug/kg86-74-8 Carbazole ND 520 ug/kg218-01-9 Chrysene 1710 520 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 1300 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 1300 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 1300 ug/kg


203 of 555

MC48821

44.29

SGS Accutest



ABN RCP List






204 of 555

MC48821

44.29

SGS Accutest



ABN RCP List



(a) Elevated RL due to dilution required for matrix interference.


205 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8081B SW846 3546 Percent Solids: 95.5 Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List


15972-60-8 Alachlor ND 51 ug/kg309-00-2 Aldrin ND 5.1 ug/kg319-84-6 alpha-BHC ND 5.1 ug/kg319-85-7 beta-BHC ND 5.1 ug/kg319-86-8 delta-BHC ND 5.1 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.1 ug/kg12789-03-6 Chlordane ND 51 ug/kg60-57-1 Dieldrin ND 5.1 ug/kg72-54-8 4,4'-DDD 5.1 5.1 ug/kg72-55-9 4,4'-DDE a 64.3 b 26 ug/kg50-29-3 4,4'-DDT 263 b 26 ug/kg72-20-8 Endrin ND 5.1 ug/kg1031-07-8 Endosulfan sulfate ND 5.1 ug/kg7421-93-4 Endrin aldehyde ND 5.1 ug/kg959-98-8 Endosulfan-I ND 5.1 ug/kg33213-65-9 Endosulfan-II ND 5.1 ug/kg76-44-8 Heptachlor ND 5.1 ug/kg1024-57-3 Heptachlor epoxide ND 5.1 ug/kg72-43-5 Methoxychlor ND 5.1 ug/kg53494-70-5 Endrin ketone ND 5.1 ug/kg8001-35-2 Toxaphene ND 51 ug/kg





206 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8082A SW846 3546 Percent Solids: 95.5 Project: Route 69 Improvements, New Haven, CT





12674-11-2 Aroclor 1016 ND 26 ug/kg11104-28-2 Aroclor 1221 ND 26 ug/kg11141-16-5 Aroclor 1232 ND 26 ug/kg53469-21-9 Aroclor 1242 ND 26 ug/kg12672-29-6 Aroclor 1248 ND 26 ug/kg11097-69-1 Aroclor 1254 ND 26 ug/kg11096-82-5 Aroclor 1260 104 26 ug/kg37324-23-5 Aroclor 1262 ND 26 ug/kg11100-14-4 Aroclor 1268 ND 26 ug/kg




207 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3546 Percent Solids: 95.5 Project: Route 69 Improvements, New Haven, CT






84-15-1 o-Terphenyl 82% 50-137%


208 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16


Metals Analysis












209 of 555

MC48821

44.29

SGS Accutest


Client Sample ID: HA-1(0-2') Lab Sample ID: MC48821-15A Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16






Cadmium 0.0060 D006 1.0 0.0040 mg/l 1 11/23/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 3








210 of 555

MC48821

44.30

SGS Accutest





VOA RCP List




211 of 555

MC48821

44.31

SGS Accutest



VOA RCP List







212 of 555

MC48821

44.31

SGS Accutest



VOA RCP List




standard.


213 of 555

MC48821

44.31

SGS Accutest





ABN RCP List




214 of 555

MC48821

44.31

SGS Accutest



ABN RCP List






215 of 555

MC48821

44.31

SGS Accutest



ABN RCP List




216 of 555

MC48821

44.31

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 58 ug/kg309-00-2 Aldrin ND 5.8 ug/kg319-84-6 alpha-BHC ND 5.8 ug/kg319-85-7 beta-BHC ND 5.8 ug/kg319-86-8 delta-BHC ND 5.8 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.8 ug/kg12789-03-6 Chlordane ND 58 ug/kg60-57-1 Dieldrin ND 5.8 ug/kg72-54-8 4,4'-DDD ND 5.8 ug/kg72-55-9 4,4'-DDE a 50.0 5.8 ug/kg50-29-3 4,4'-DDT 52.7 5.8 ug/kg72-20-8 Endrin ND 5.8 ug/kg1031-07-8 Endosulfan sulfate ND 5.8 ug/kg7421-93-4 Endrin aldehyde ND 5.8 ug/kg959-98-8 Endosulfan-I ND 5.8 ug/kg33213-65-9 Endosulfan-II ND 5.8 ug/kg76-44-8 Heptachlor ND 5.8 ug/kg1024-57-3 Heptachlor epoxide ND 5.8 ug/kg72-43-5 Methoxychlor ND 5.8 ug/kg53494-70-5 Endrin ketone ND 5.8 ug/kg8001-35-2 Toxaphene ND 58 ug/kg





217 of 555

MC48821

44.31

SGS Accutest







12674-11-2 Aroclor 1016 ND 29 ug/kg11104-28-2 Aroclor 1221 ND 29 ug/kg11141-16-5 Aroclor 1232 ND 29 ug/kg53469-21-9 Aroclor 1242 ND 29 ug/kg12672-29-6 Aroclor 1248 ND 29 ug/kg11097-69-1 Aroclor 1254 a 32.7 29 ug/kg11096-82-5 Aroclor 1260 68.8 29 ug/kg37324-23-5 Aroclor 1262 ND 29 ug/kg11100-14-4 Aroclor 1268 ND 29 ug/kg



(a) Estimated value due to the presence of other Aroclor pattern.Confirmation value >40% RPD


218 of 555

MC48821

44.31

SGS Accutest








84-15-1 o-Terphenyl 68% 50-137%


219 of 555

MC48821

44.31

SGS Accutest




Metals Analysis












220 of 555

MC48821

44.31

SGS Accutest




General Chemistry




Solids, Percent 83 % 1 11/21/16 HS SM 2540G-97 MOD


pH 7.0 su 1 11/26/16 13:32 EL SW846 9045D


221 of 555

MC48821

44.31

SGS Accutest
















222 of 555

MC48821

44.32

SGS Accutest



File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 M82152.D 1 11/26/16 DRY n/a n/a MSM2946Run #2 a M82166.D 1 11/28/16 CB n/a n/a MSM2947


VOA RCP List


67-64-1 Acetone ND 10 ug/kg107-13-1 Acrylonitrile ND 26 ug/kg71-43-2 Benzene ND 1.0 ug/kg108-86-1 Bromobenzene ND 5.2 ug/kg75-27-4 Bromodichloromethane ND 2.1 ug/kg75-25-2 Bromoform ND 2.1 ug/kg74-83-9 Bromomethane b ND 10 ug/kg78-93-3 2-Butanone (MEK) ND 10 ug/kg104-51-8 n-Butylbenzene ND 5.2 ug/kg135-98-8 sec-Butylbenzene ND 5.2 ug/kg98-06-6 tert-Butylbenzene ND 5.2 ug/kg75-15-0 Carbon disulfide ND 5.2 ug/kg56-23-5 Carbon tetrachloride ND 2.1 ug/kg108-90-7 Chlorobenzene ND 2.1 ug/kg75-00-3 Chloroethane b ND 10 ug/kg67-66-3 Chloroform ND 2.1 ug/kg74-87-3 Chloromethane b ND 5.2 ug/kg95-49-8 o-Chlorotoluene ND 5.2 ug/kg106-43-4 p-Chlorotoluene ND 5.2 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.2 ug/kg124-48-1 Dibromochloromethane ND 5.2 ug/kg106-93-4 1,2-Dibromoethane ND 2.1 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.1 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.1 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.1 ug/kg75-71-8 Dichlorodifluoromethane b ND 5.2 ug/kg75-34-3 1,1-Dichloroethane ND 2.1 ug/kg107-06-2 1,2-Dichloroethane ND 2.1 ug/kg75-35-4 1,1-Dichloroethene ND 2.1 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.1 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.1 ug/kg78-87-5 1,2-Dichloropropane ND 2.1 ug/kg


223 of 555

MC48821

44.33

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 5.2 ug/kg594-20-7 2,2-Dichloropropane ND 5.2 ug/kg563-58-6 1,1-Dichloropropene ND 5.2 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.1 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.1 ug/kg100-41-4 Ethylbenzene ND 2.1 ug/kg76-13-1 Freon 113 ND 5.2 ug/kg87-68-3 Hexachlorobutadiene ND 5.2 ug/kg591-78-6 2-Hexanone ND 5.2 ug/kg98-82-8 Isopropylbenzene ND 5.2 ug/kg99-87-6 p-Isopropyltoluene ND 5.2 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.1 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.2 ug/kg74-95-3 Methylene bromide ND 5.2 ug/kg75-09-2 Methylene chloride ND 2.1 ug/kg91-20-3 Naphthalene ND 5.2 ug/kg103-65-1 n-Propylbenzene ND 5.2 ug/kg100-42-5 Styrene ND 5.2 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.1 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.2 ug/kg127-18-4 Tetrachloroethene ND 2.1 ug/kg109-99-9 Tetrahydrofuran ND 10 ug/kg108-88-3 Toluene ND 5.2 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 10 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.2 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.2 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.1 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.1 ug/kg79-01-6 Trichloroethene ND 2.1 ug/kg75-69-4 Trichlorofluoromethane ND 2.1 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.2 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.2 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.2 ug/kg75-01-4 Vinyl chloride ND 10 ug/kg





224 of 555

MC48821

44.33

SGS Accutest



VOA RCP List




standard.


225 of 555

MC48821

44.33

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 280 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 560 ug/kg120-83-2 2,4-Dichlorophenol ND 560 ug/kg105-67-9 2,4-Dimethylphenol ND 560 ug/kg51-28-5 2,4-Dinitrophenol ND 560 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 560 ug/kg95-48-7 2-Methylphenol ND 560 ug/kg106-44-5 4-Methylphenol ND 560 ug/kg88-75-5 2-Nitrophenol ND 560 ug/kg100-02-7 4-Nitrophenol ND 560 ug/kg87-86-5 Pentachlorophenol ND 560 ug/kg108-95-2 Phenol ND 280 ug/kg95-95-4 2,4,5-Trichlorophenol ND 560 ug/kg88-06-2 2,4,6-Trichlorophenol ND 560 ug/kg83-32-9 Acenaphthene ND 110 ug/kg208-96-8 Acenaphthylene 361 110 ug/kg62-53-3 Aniline ND 560 ug/kg120-12-7 Anthracene 191 110 ug/kg56-55-3 Benzo(a)anthracene 673 110 ug/kg50-32-8 Benzo(a)pyrene 726 280 ug/kg205-99-2 Benzo(b)fluoranthene 752 110 ug/kg191-24-2 Benzo(g,h,i)perylene 537 110 ug/kg207-08-9 Benzo(k)fluoranthene 675 110 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 280 ug/kg85-68-7 Butyl benzyl phthalate ND 280 ug/kg91-58-7 2-Chloronaphthalene ND 280 ug/kg106-47-8 4-Chloroaniline ND 560 ug/kg86-74-8 Carbazole ND 110 ug/kg218-01-9 Chrysene 956 110 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 280 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 280 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 280 ug/kg


226 of 555

MC48821

44.33

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 280 ug/kg121-14-2 2,4-Dinitrotoluene ND 560 ug/kg606-20-2 2,6-Dinitrotoluene ND 560 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 560 ug/kg53-70-3 Dibenzo(a,h)anthracene 133 110 ug/kg132-64-9 Dibenzofuran ND 110 ug/kg84-74-2 Di-n-butyl phthalate ND 280 ug/kg117-84-0 Di-n-octyl phthalate ND 280 ug/kg84-66-2 Diethyl phthalate ND 280 ug/kg131-11-3 Dimethyl phthalate ND 280 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 280 ug/kg206-44-0 Fluoranthene 1460 110 ug/kg86-73-7 Fluorene ND 110 ug/kg118-74-1 Hexachlorobenzene ND 280 ug/kg87-68-3 Hexachlorobutadiene ND 280 ug/kg77-47-4 Hexachlorocyclopentadiene ND 560 ug/kg67-72-1 Hexachloroethane ND 280 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 508 280 ug/kg78-59-1 Isophorone ND 280 ug/kg91-57-6 2-Methylnaphthalene ND 110 ug/kg88-74-4 2-Nitroaniline ND 560 ug/kg99-09-2 3-Nitroaniline ND 560 ug/kg100-01-6 4-Nitroaniline ND 560 ug/kg91-20-3 Naphthalene ND 110 ug/kg98-95-3 Nitrobenzene ND 280 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 280 ug/kg86-30-6 N-Nitrosodiphenylamine ND 280 ug/kg82-68-8 Pentachloronitrobenzene ND 560 ug/kg85-01-8 Phenanthrene 719 110 ug/kg129-00-0 Pyrene 1530 110 ug/kg110-86-1 Pyridine ND 560 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 560 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 280 ug/kg




227 of 555

MC48821

44.33

SGS Accutest



ABN RCP List




228 of 555

MC48821

44.33

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 56 ug/kg309-00-2 Aldrin ND 5.6 ug/kg319-84-6 alpha-BHC ND 5.6 ug/kg319-85-7 beta-BHC ND 5.6 ug/kg319-86-8 delta-BHC ND 5.6 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.6 ug/kg12789-03-6 Chlordane ND 56 ug/kg60-57-1 Dieldrin ND 5.6 ug/kg72-54-8 4,4'-DDD ND 5.6 ug/kg72-55-9 4,4'-DDE 16.6 5.6 ug/kg50-29-3 4,4'-DDT a 64.2 5.6 ug/kg72-20-8 Endrin ND 5.6 ug/kg1031-07-8 Endosulfan sulfate ND 5.6 ug/kg7421-93-4 Endrin aldehyde ND 5.6 ug/kg959-98-8 Endosulfan-I ND 5.6 ug/kg33213-65-9 Endosulfan-II ND 5.6 ug/kg76-44-8 Heptachlor ND 5.6 ug/kg1024-57-3 Heptachlor epoxide ND 5.6 ug/kg72-43-5 Methoxychlor ND 5.6 ug/kg53494-70-5 Endrin ketone ND 5.6 ug/kg8001-35-2 Toxaphene ND 56 ug/kg





229 of 555

MC48821

44.33

SGS Accutest







12674-11-2 Aroclor 1016 ND 28 ug/kg11104-28-2 Aroclor 1221 ND 28 ug/kg11141-16-5 Aroclor 1232 ND 28 ug/kg53469-21-9 Aroclor 1242 ND 28 ug/kg12672-29-6 Aroclor 1248 ND 28 ug/kg11097-69-1 Aroclor 1254 ND 28 ug/kg11096-82-5 Aroclor 1260 62.3 28 ug/kg37324-23-5 Aroclor 1262 ND 28 ug/kg11100-14-4 Aroclor 1268 ND 28 ug/kg




230 of 555

MC48821

44.33

SGS Accutest








84-15-1 o-Terphenyl 108% 50-137%


231 of 555

MC48821

44.33

SGS Accutest




Metals Analysis












232 of 555

MC48821

44.33

SGS Accutest
















233 of 555

MC48821

44.34

SGS Accutest





VOA RCP List


67-64-1 Acetone ND 9.8 ug/kg107-13-1 Acrylonitrile ND 25 ug/kg71-43-2 Benzene ND 0.98 ug/kg108-86-1 Bromobenzene ND 4.9 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane b ND 9.8 ug/kg78-93-3 2-Butanone (MEK) ND 9.8 ug/kg104-51-8 n-Butylbenzene ND 4.9 ug/kg135-98-8 sec-Butylbenzene ND 4.9 ug/kg98-06-6 tert-Butylbenzene ND 4.9 ug/kg75-15-0 Carbon disulfide ND 4.9 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane b ND 9.8 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane b ND 4.9 ug/kg95-49-8 o-Chlorotoluene ND 4.9 ug/kg106-43-4 p-Chlorotoluene ND 4.9 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 4.9 ug/kg124-48-1 Dibromochloromethane ND 4.9 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane b ND 4.9 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg


234 of 555

MC48821

44.35

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 4.9 ug/kg594-20-7 2,2-Dichloropropane ND 4.9 ug/kg563-58-6 1,1-Dichloropropene ND 4.9 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.0 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.0 ug/kg100-41-4 Ethylbenzene ND 2.0 ug/kg76-13-1 Freon 113 ND 4.9 ug/kg87-68-3 Hexachlorobutadiene ND 4.9 ug/kg591-78-6 2-Hexanone ND 4.9 ug/kg98-82-8 Isopropylbenzene ND 4.9 ug/kg99-87-6 p-Isopropyltoluene ND 4.9 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 4.9 ug/kg74-95-3 Methylene bromide ND 4.9 ug/kg75-09-2 Methylene chloride ND 2.0 ug/kg91-20-3 Naphthalene ND 4.9 ug/kg103-65-1 n-Propylbenzene ND 4.9 ug/kg100-42-5 Styrene ND 4.9 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 ug/kg127-18-4 Tetrachloroethene ND 2.0 ug/kg109-99-9 Tetrahydrofuran ND 9.8 ug/kg108-88-3 Toluene ND 4.9 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 9.8 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 4.9 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 4.9 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.0 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.0 ug/kg79-01-6 Trichloroethene ND 2.0 ug/kg75-69-4 Trichlorofluoromethane ND 2.0 ug/kg96-18-4 1,2,3-Trichloropropane ND 4.9 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 4.9 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 4.9 ug/kg75-01-4 Vinyl chloride ND 9.8 ug/kg





235 of 555

MC48821

44.35

SGS Accutest



VOA RCP List




standard.


236 of 555

MC48821

44.35

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 1400 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 2700 ug/kg120-83-2 2,4-Dichlorophenol ND 2700 ug/kg105-67-9 2,4-Dimethylphenol ND 2700 ug/kg51-28-5 2,4-Dinitrophenol b ND 2700 ug/kg534-52-1 4,6-Dinitro-o-cresol b ND 2700 ug/kg95-48-7 2-Methylphenol ND 2700 ug/kg106-44-5 4-Methylphenol ND 2700 ug/kg88-75-5 2-Nitrophenol ND 2700 ug/kg100-02-7 4-Nitrophenol ND 2700 ug/kg87-86-5 Pentachlorophenol b ND 2700 ug/kg108-95-2 Phenol ND 1400 ug/kg95-95-4 2,4,5-Trichlorophenol ND 2700 ug/kg88-06-2 2,4,6-Trichlorophenol ND 2700 ug/kg83-32-9 Acenaphthene ND 550 ug/kg208-96-8 Acenaphthylene ND 550 ug/kg62-53-3 Aniline ND 2700 ug/kg120-12-7 Anthracene ND 550 ug/kg56-55-3 Benzo(a)anthracene 1170 550 ug/kg50-32-8 Benzo(a)pyrene ND 1400 ug/kg205-99-2 Benzo(b)fluoranthene 1270 550 ug/kg191-24-2 Benzo(g,h,i)perylene 1240 550 ug/kg207-08-9 Benzo(k)fluoranthene 1220 550 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 1400 ug/kg85-68-7 Butyl benzyl phthalate ND 1400 ug/kg91-58-7 2-Chloronaphthalene ND 1400 ug/kg106-47-8 4-Chloroaniline ND 2700 ug/kg86-74-8 Carbazole ND 550 ug/kg218-01-9 Chrysene 1530 550 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 1400 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 1400 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 1400 ug/kg


237 of 555

MC48821

44.35

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 1400 ug/kg121-14-2 2,4-Dinitrotoluene ND 2700 ug/kg606-20-2 2,6-Dinitrotoluene ND 2700 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 2700 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 550 ug/kg132-64-9 Dibenzofuran ND 550 ug/kg84-74-2 Di-n-butyl phthalate ND 1400 ug/kg117-84-0 Di-n-octyl phthalate ND 1400 ug/kg84-66-2 Diethyl phthalate ND 1400 ug/kg131-11-3 Dimethyl phthalate ND 1400 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 1400 ug/kg206-44-0 Fluoranthene 2620 550 ug/kg86-73-7 Fluorene ND 550 ug/kg118-74-1 Hexachlorobenzene ND 1400 ug/kg87-68-3 Hexachlorobutadiene ND 1400 ug/kg77-47-4 Hexachlorocyclopentadiene b ND 2700 ug/kg67-72-1 Hexachloroethane ND 1400 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 1400 ug/kg78-59-1 Isophorone ND 1400 ug/kg91-57-6 2-Methylnaphthalene ND 550 ug/kg88-74-4 2-Nitroaniline ND 2700 ug/kg99-09-2 3-Nitroaniline ND 2700 ug/kg100-01-6 4-Nitroaniline ND 2700 ug/kg91-20-3 Naphthalene ND 550 ug/kg98-95-3 Nitrobenzene ND 1400 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 1400 ug/kg86-30-6 N-Nitrosodiphenylamine ND 1400 ug/kg82-68-8 Pentachloronitrobenzene ND 2700 ug/kg85-01-8 Phenanthrene 1190 550 ug/kg129-00-0 Pyrene 2460 550 ug/kg110-86-1 Pyridine ND 2700 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 2700 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 1400 ug/kg




238 of 555

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SGS Accutest



ABN RCP List



(a) Elevated RL due to dilution required for matrix interference.(b) Continuing Calibration outside of acceptance criteria. Reporting Limit Response verified by low-level

standard.


239 of 555

MC48821

44.35

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 56 ug/kg309-00-2 Aldrin ND 5.6 ug/kg319-84-6 alpha-BHC ND 5.6 ug/kg319-85-7 beta-BHC ND 5.6 ug/kg319-86-8 delta-BHC ND 5.6 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.6 ug/kg12789-03-6 Chlordane ND 56 ug/kg60-57-1 Dieldrin ND 5.6 ug/kg72-54-8 4,4'-DDD ND 5.6 ug/kg72-55-9 4,4'-DDE 9.4 5.6 ug/kg50-29-3 4,4'-DDT 197 a 28 ug/kg72-20-8 Endrin ND 5.6 ug/kg1031-07-8 Endosulfan sulfate ND 5.6 ug/kg7421-93-4 Endrin aldehyde ND 5.6 ug/kg959-98-8 Endosulfan-I ND 5.6 ug/kg33213-65-9 Endosulfan-II ND 5.6 ug/kg76-44-8 Heptachlor ND 5.6 ug/kg1024-57-3 Heptachlor epoxide ND 5.6 ug/kg72-43-5 Methoxychlor ND 5.6 ug/kg53494-70-5 Endrin ketone ND 5.6 ug/kg8001-35-2 Toxaphene ND 56 ug/kg



(a) Result is from Run# 2


240 of 555

MC48821

44.35

SGS Accutest







12674-11-2 Aroclor 1016 ND 28 ug/kg11104-28-2 Aroclor 1221 ND 28 ug/kg11141-16-5 Aroclor 1232 ND 28 ug/kg53469-21-9 Aroclor 1242 ND 28 ug/kg12672-29-6 Aroclor 1248 ND 28 ug/kg11097-69-1 Aroclor 1254 ND 28 ug/kg11096-82-5 Aroclor 1260 114 28 ug/kg37324-23-5 Aroclor 1262 ND 28 ug/kg11100-14-4 Aroclor 1268 ND 28 ug/kg




241 of 555

MC48821

44.35

SGS Accutest








84-15-1 o-Terphenyl 115% 50-137%


242 of 555

MC48821

44.35

SGS Accutest




Metals Analysis












243 of 555

MC48821

44.35

SGS Accutest
















244 of 555

MC48821

44.36

SGS Accutest





VOA RCP List




245 of 555

MC48821

44.37

SGS Accutest



VOA RCP List







246 of 555

MC48821

44.37

SGS Accutest



VOA RCP List


2037-26-5 Toluene-D8 94% 104% 65-129%460-00-4 4-Bromofluorobenzene 155% c 107% 63-137%

(a) Confirmation run.(b) Continuing Calibration outside of acceptance criteria. Reporting Limit response verified by low-level

standard.(c) Outside control limits due to possible matrix interference. Confirmed by reanalysis.


247 of 555

MC48821

44.37

SGS Accutest





ABN RCP List


95-57-8 2-Chlorophenol ND 1400 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 2900 ug/kg120-83-2 2,4-Dichlorophenol ND 2900 ug/kg105-67-9 2,4-Dimethylphenol ND 2900 ug/kg51-28-5 2,4-Dinitrophenol b ND 2900 ug/kg534-52-1 4,6-Dinitro-o-cresol b ND 2900 ug/kg95-48-7 2-Methylphenol ND 2900 ug/kg106-44-5 4-Methylphenol ND 2900 ug/kg88-75-5 2-Nitrophenol ND 2900 ug/kg100-02-7 4-Nitrophenol ND 2900 ug/kg87-86-5 Pentachlorophenol b ND 2900 ug/kg108-95-2 Phenol ND 1400 ug/kg95-95-4 2,4,5-Trichlorophenol ND 2900 ug/kg88-06-2 2,4,6-Trichlorophenol ND 2900 ug/kg83-32-9 Acenaphthene ND 570 ug/kg208-96-8 Acenaphthylene 1590 570 ug/kg62-53-3 Aniline ND 2900 ug/kg120-12-7 Anthracene 748 570 ug/kg56-55-3 Benzo(a)anthracene 2170 570 ug/kg50-32-8 Benzo(a)pyrene 2530 1400 ug/kg205-99-2 Benzo(b)fluoranthene 2510 570 ug/kg191-24-2 Benzo(g,h,i)perylene 1930 570 ug/kg207-08-9 Benzo(k)fluoranthene 2370 570 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 1400 ug/kg85-68-7 Butyl benzyl phthalate ND 1400 ug/kg91-58-7 2-Chloronaphthalene ND 1400 ug/kg106-47-8 4-Chloroaniline ND 2900 ug/kg86-74-8 Carbazole ND 570 ug/kg218-01-9 Chrysene 3020 570 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 1400 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 1400 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 1400 ug/kg


248 of 555

MC48821

44.37

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 1400 ug/kg121-14-2 2,4-Dinitrotoluene ND 2900 ug/kg606-20-2 2,6-Dinitrotoluene ND 2900 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 2900 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 570 ug/kg132-64-9 Dibenzofuran ND 570 ug/kg84-74-2 Di-n-butyl phthalate ND 1400 ug/kg117-84-0 Di-n-octyl phthalate ND 1400 ug/kg84-66-2 Diethyl phthalate ND 1400 ug/kg131-11-3 Dimethyl phthalate ND 1400 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 1400 ug/kg206-44-0 Fluoranthene 4380 570 ug/kg86-73-7 Fluorene ND 570 ug/kg118-74-1 Hexachlorobenzene ND 1400 ug/kg87-68-3 Hexachlorobutadiene ND 1400 ug/kg77-47-4 Hexachlorocyclopentadiene b ND 2900 ug/kg67-72-1 Hexachloroethane ND 1400 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 1880 1400 ug/kg78-59-1 Isophorone ND 1400 ug/kg91-57-6 2-Methylnaphthalene ND 570 ug/kg88-74-4 2-Nitroaniline ND 2900 ug/kg99-09-2 3-Nitroaniline ND 2900 ug/kg100-01-6 4-Nitroaniline ND 2900 ug/kg91-20-3 Naphthalene ND 570 ug/kg98-95-3 Nitrobenzene ND 1400 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 1400 ug/kg86-30-6 N-Nitrosodiphenylamine ND 1400 ug/kg82-68-8 Pentachloronitrobenzene ND 2900 ug/kg85-01-8 Phenanthrene 1910 570 ug/kg129-00-0 Pyrene 4280 570 ug/kg110-86-1 Pyridine ND 2900 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 2900 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 1400 ug/kg




249 of 555

MC48821

44.37

SGS Accutest



ABN RCP List



(a) Elevated RL due to dilution required for matrix interference.(b) Continuing Calibration outside of acceptance criteria. Reporting Limit Response verified by low-level

standard.


250 of 555

MC48821

44.37

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 58 ug/kg309-00-2 Aldrin ND 5.8 ug/kg319-84-6 alpha-BHC ND 5.8 ug/kg319-85-7 beta-BHC ND 5.8 ug/kg319-86-8 delta-BHC ND 5.8 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.8 ug/kg12789-03-6 Chlordane ND 58 ug/kg60-57-1 Dieldrin ND 5.8 ug/kg72-54-8 4,4'-DDD 7.9 5.8 ug/kg72-55-9 4,4'-DDE ND 5.8 ug/kg50-29-3 4,4'-DDT 27.7 5.8 ug/kg72-20-8 Endrin ND 5.8 ug/kg1031-07-8 Endosulfan sulfate ND 5.8 ug/kg7421-93-4 Endrin aldehyde ND 5.8 ug/kg959-98-8 Endosulfan-I ND 5.8 ug/kg33213-65-9 Endosulfan-II ND 5.8 ug/kg76-44-8 Heptachlor ND 5.8 ug/kg1024-57-3 Heptachlor epoxide ND 5.8 ug/kg72-43-5 Methoxychlor ND 5.8 ug/kg53494-70-5 Endrin ketone ND 5.8 ug/kg8001-35-2 Toxaphene ND 58 ug/kg





251 of 555

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12674-11-2 Aroclor 1016 ND 29 ug/kg11104-28-2 Aroclor 1221 ND 29 ug/kg11141-16-5 Aroclor 1232 ND 29 ug/kg53469-21-9 Aroclor 1242 ND 29 ug/kg12672-29-6 Aroclor 1248 ND 29 ug/kg11097-69-1 Aroclor 1254 ND 29 ug/kg11096-82-5 Aroclor 1260 47.0 29 ug/kg37324-23-5 Aroclor 1262 ND 29 ug/kg11100-14-4 Aroclor 1268 ND 29 ug/kg




252 of 555

MC48821

44.37

SGS Accutest








84-15-1 o-Terphenyl 111% 50-137%


253 of 555

MC48821

44.37

SGS Accutest




Metals Analysis












254 of 555

MC48821

44.37

SGS Accutest




General Chemistry






pH 7.2 su 1 11/26/16 13:32 EL SW846 9045D


255 of 555

MC48821

44.37

SGS Accutest
















256 of 555

MC48821

44.38

SGS Accutest





VOA RCP List




257 of 555

MC48821

44.39

SGS Accutest



VOA RCP List







258 of 555

MC48821

44.39

SGS Accutest



VOA RCP List




standard.


259 of 555

MC48821

44.39

SGS Accutest





ABN RCP List




260 of 555

MC48821

44.39

SGS Accutest



ABN RCP List


7005-72-3 4-Chlorophenyl phenyl ether ND 270 ug/kg121-14-2 2,4-Dinitrotoluene ND 550 ug/kg606-20-2 2,6-Dinitrotoluene ND 550 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 550 ug/kg53-70-3 Dibenzo(a,h)anthracene ND 110 ug/kg132-64-9 Dibenzofuran ND 110 ug/kg84-74-2 Di-n-butyl phthalate ND 270 ug/kg117-84-0 Di-n-octyl phthalate ND 270 ug/kg84-66-2 Diethyl phthalate ND 270 ug/kg131-11-3 Dimethyl phthalate ND 270 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 270 ug/kg206-44-0 Fluoranthene 1090 110 ug/kg86-73-7 Fluorene ND 110 ug/kg118-74-1 Hexachlorobenzene ND 270 ug/kg87-68-3 Hexachlorobutadiene ND 270 ug/kg77-47-4 Hexachlorocyclopentadiene ND 550 ug/kg67-72-1 Hexachloroethane ND 270 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene 362 270 ug/kg78-59-1 Isophorone ND 270 ug/kg91-57-6 2-Methylnaphthalene ND 110 ug/kg88-74-4 2-Nitroaniline ND 550 ug/kg99-09-2 3-Nitroaniline ND 550 ug/kg100-01-6 4-Nitroaniline ND 550 ug/kg91-20-3 Naphthalene ND 110 ug/kg98-95-3 Nitrobenzene ND 270 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 270 ug/kg86-30-6 N-Nitrosodiphenylamine ND 270 ug/kg82-68-8 Pentachloronitrobenzene ND 550 ug/kg85-01-8 Phenanthrene 447 110 ug/kg129-00-0 Pyrene 918 110 ug/kg110-86-1 Pyridine ND 550 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 550 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 270 ug/kg




261 of 555

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ABN RCP List




262 of 555

MC48821

44.39

SGS Accutest





Pesticide RCP List


15972-60-8 Alachlor ND 57 ug/kg309-00-2 Aldrin ND 5.7 ug/kg319-84-6 alpha-BHC ND 5.7 ug/kg319-85-7 beta-BHC ND 5.7 ug/kg319-86-8 delta-BHC ND 5.7 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.7 ug/kg12789-03-6 Chlordane ND 57 ug/kg60-57-1 Dieldrin ND 5.7 ug/kg72-54-8 4,4'-DDD ND 5.7 ug/kg72-55-9 4,4'-DDE a 12.8 5.7 ug/kg50-29-3 4,4'-DDT 21.6 5.7 ug/kg72-20-8 Endrin ND 5.7 ug/kg1031-07-8 Endosulfan sulfate ND 5.7 ug/kg7421-93-4 Endrin aldehyde ND 5.7 ug/kg959-98-8 Endosulfan-I ND 5.7 ug/kg33213-65-9 Endosulfan-II ND 5.7 ug/kg76-44-8 Heptachlor ND 5.7 ug/kg1024-57-3 Heptachlor epoxide ND 5.7 ug/kg72-43-5 Methoxychlor ND 5.7 ug/kg53494-70-5 Endrin ketone ND 5.7 ug/kg8001-35-2 Toxaphene ND 57 ug/kg





263 of 555

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264 of 555

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84-15-1 o-Terphenyl 86% 50-137%


265 of 555

MC48821

44.39

SGS Accutest




Metals Analysis












266 of 555

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267 of 555

MC48821

44.40

SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8260C Percent Solids: 88.2 Project: Route 69 Improvements, New Haven, CT



VOA RCP List


67-64-1 Acetone ND 9.8 ug/kg107-13-1 Acrylonitrile ND 24 ug/kg71-43-2 Benzene ND 0.98 ug/kg108-86-1 Bromobenzene ND 4.9 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane b ND 9.8 ug/kg78-93-3 2-Butanone (MEK) ND 9.8 ug/kg104-51-8 n-Butylbenzene ND 4.9 ug/kg135-98-8 sec-Butylbenzene ND 4.9 ug/kg98-06-6 tert-Butylbenzene ND 4.9 ug/kg75-15-0 Carbon disulfide ND 4.9 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane b ND 9.8 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane b ND 4.9 ug/kg95-49-8 o-Chlorotoluene ND 4.9 ug/kg106-43-4 p-Chlorotoluene ND 4.9 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 4.9 ug/kg124-48-1 Dibromochloromethane ND 4.9 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane b ND 4.9 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg


268 of 555

MC48821

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SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 4.9 ug/kg594-20-7 2,2-Dichloropropane ND 4.9 ug/kg563-58-6 1,1-Dichloropropene ND 4.9 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.0 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 2.0 ug/kg100-41-4 Ethylbenzene ND 2.0 ug/kg76-13-1 Freon 113 ND 4.9 ug/kg87-68-3 Hexachlorobutadiene ND 4.9 ug/kg591-78-6 2-Hexanone ND 4.9 ug/kg98-82-8 Isopropylbenzene ND 4.9 ug/kg99-87-6 p-Isopropyltoluene ND 4.9 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 4.9 ug/kg74-95-3 Methylene bromide ND 4.9 ug/kg75-09-2 Methylene chloride ND 2.0 ug/kg91-20-3 Naphthalene ND 4.9 ug/kg103-65-1 n-Propylbenzene ND 4.9 ug/kg100-42-5 Styrene ND 4.9 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 4.9 ug/kg127-18-4 Tetrachloroethene ND 2.0 ug/kg109-99-9 Tetrahydrofuran ND 9.8 ug/kg108-88-3 Toluene ND 4.9 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 9.8 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 4.9 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 4.9 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.0 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.0 ug/kg79-01-6 Trichloroethene ND 2.0 ug/kg75-69-4 Trichlorofluoromethane ND 2.0 ug/kg96-18-4 1,2,3-Trichloropropane ND 4.9 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 4.9 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 4.9 ug/kg75-01-4 Vinyl chloride ND 9.8 ug/kg





269 of 555

MC48821

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SGS Accutest



VOA RCP List




standard.


270 of 555

MC48821

44.41

SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8081B SW846 3546 Percent Solids: 88.2 Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List


15972-60-8 Alachlor ND 54 ug/kg309-00-2 Aldrin ND 5.4 ug/kg319-84-6 alpha-BHC ND 5.4 ug/kg319-85-7 beta-BHC ND 5.4 ug/kg319-86-8 delta-BHC ND 5.4 ug/kg58-89-9 gamma-BHC (Lindane) ND 5.4 ug/kg12789-03-6 Chlordane ND 54 ug/kg60-57-1 Dieldrin ND 5.4 ug/kg72-54-8 4,4'-DDD ND 5.4 ug/kg72-55-9 4,4'-DDE a 10.9 5.4 ug/kg50-29-3 4,4'-DDT a 21.0 5.4 ug/kg72-20-8 Endrin ND 5.4 ug/kg1031-07-8 Endosulfan sulfate ND 5.4 ug/kg7421-93-4 Endrin aldehyde ND 5.4 ug/kg959-98-8 Endosulfan-I ND 5.4 ug/kg33213-65-9 Endosulfan-II ND 5.4 ug/kg76-44-8 Heptachlor ND 5.4 ug/kg1024-57-3 Heptachlor epoxide ND 5.4 ug/kg72-43-5 Methoxychlor ND 5.4 ug/kg53494-70-5 Endrin ketone ND 5.4 ug/kg8001-35-2 Toxaphene ND 54 ug/kg





271 of 555

MC48821

44.41

SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: SW846 8082A SW846 3546 Percent Solids: 88.2 Project: Route 69 Improvements, New Haven, CT









272 of 555

MC48821

44.41

SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3546 Percent Solids: 88.2 Project: Route 69 Improvements, New Haven, CT






84-15-1 o-Terphenyl 71% 50-137%


273 of 555

MC48821

44.41

SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21 Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16


Metals Analysis












274 of 555

MC48821

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SGS Accutest


Client Sample ID: HA-6(0-2')DUP Lab Sample ID: MC48821-21A Date Sampled: 11/16/16 Matrix: SO - Soil Date Received: 11/18/16














275 of 555

MC48821

44.42

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 V51612.D 1 11/22/16 KP n/a n/a MSV1905Run #2

Purge VolumeRun #1 5.0 mlRun #2

VOA RCP List


67-64-1 Acetone ND 10 ug/l107-13-1 Acrylonitrile ND 5.0 ug/l71-43-2 Benzene ND 0.50 ug/l108-86-1 Bromobenzene ND 5.0 ug/l75-27-4 Bromodichloromethane ND 1.0 ug/l75-25-2 Bromoform a ND 1.0 ug/l74-83-9 Bromomethane ND 2.0 ug/l78-93-3 2-Butanone (MEK) ND 10 ug/l104-51-8 n-Butylbenzene ND 5.0 ug/l135-98-8 sec-Butylbenzene ND 5.0 ug/l98-06-6 tert-Butylbenzene ND 5.0 ug/l75-15-0 Carbon disulfide a ND 5.0 ug/l56-23-5 Carbon tetrachloride ND 1.0 ug/l108-90-7 Chlorobenzene ND 1.0 ug/l75-00-3 Chloroethane ND 2.0 ug/l67-66-3 Chloroform ND 1.0 ug/l74-87-3 Chloromethane ND 2.0 ug/l95-49-8 o-Chlorotoluene ND 5.0 ug/l106-43-4 p-Chlorotoluene ND 5.0 ug/l96-12-8 1,2-Dibromo-3-chloropropan a ND 5.0 ug/l124-48-1 Dibromochloromethane ND 1.0 ug/l106-93-4 1,2-Dibromoethane ND 1.0 ug/l95-50-1 1,2-Dichlorobenzene ND 1.0 ug/l541-73-1 1,3-Dichlorobenzene ND 1.0 ug/l106-46-7 1,4-Dichlorobenzene ND 1.0 ug/l75-71-8 Dichlorodifluoromethane ND 2.0 ug/l75-34-3 1,1-Dichloroethane ND 1.0 ug/l107-06-2 1,2-Dichloroethane ND 1.0 ug/l75-35-4 1,1-Dichloroethene a ND 1.0 ug/l156-59-2 cis-1,2-Dichloroethene ND 1.0 ug/l156-60-5 trans-1,2-Dichloroethene a ND 1.0 ug/l78-87-5 1,2-Dichloropropane ND 2.0 ug/l


276 of 555

MC48821

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SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 5.0 ug/l594-20-7 2,2-Dichloropropane ND 5.0 ug/l563-58-6 1,1-Dichloropropene ND 5.0 ug/l10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/l10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/l100-41-4 Ethylbenzene ND 1.0 ug/l76-13-1 Freon 113 a ND 5.0 ug/l87-68-3 Hexachlorobutadiene ND 5.0 ug/l591-78-6 2-Hexanone ND 10 ug/l98-82-8 Isopropylbenzene ND 5.0 ug/l99-87-6 p-Isopropyltoluene ND 5.0 ug/l1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.0 ug/l74-95-3 Methylene bromide ND 5.0 ug/l75-09-2 Methylene chloride a ND 2.0 ug/l91-20-3 Naphthalene ND 5.0 ug/l103-65-1 n-Propylbenzene ND 5.0 ug/l100-42-5 Styrene ND 5.0 ug/l630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/l127-18-4 Tetrachloroethene ND 1.0 ug/l109-99-9 Tetrahydrofuran ND 10 ug/l108-88-3 Toluene ND 1.0 ug/l110-57-6 Trans-1,4-Dichloro-2-Butene a ND 5.0 ug/l87-61-6 1,2,3-Trichlorobenzene ND 5.0 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/l71-55-6 1,1,1-Trichloroethane ND 1.0 ug/l79-00-5 1,1,2-Trichloroethane ND 1.0 ug/l79-01-6 Trichloroethene ND 1.0 ug/l75-69-4 Trichlorofluoromethane ND 1.0 ug/l96-18-4 1,2,3-Trichloropropane ND 5.0 ug/l95-63-6 1,2,4-Trimethylbenzene ND 1.0 ug/l108-67-8 1,3,5-Trimethylbenzene ND 1.0 ug/l75-01-4 Vinyl chloride ND 1.0 ug/l

m,p-Xylene ND 1.0 ug/l95-47-6 o-Xylene ND 1.0 ug/l




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VOA RCP List





278 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 W31136.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264Run #2

Initial Volume Final VolumeRun #1 980 ml 1.0 mlRun #2

ABN RCP List(without PAH)


95-57-8 2-Chlorophenol ND 5.1 ug/l59-50-7 4-Chloro-3-methyl phenol ND 10 ug/l120-83-2 2,4-Dichlorophenol ND 10 ug/l105-67-9 2,4-Dimethylphenol ND 10 ug/l51-28-5 2,4-Dinitrophenol ND 20 ug/l534-52-1 4,6-Dinitro-o-cresol ND 10 ug/l95-48-7 2-Methylphenol ND 10 ug/l106-44-5 4-Methylphenol ND 10 ug/l88-75-5 2-Nitrophenol ND 10 ug/l100-02-7 4-Nitrophenol ND 20 ug/l87-86-5 Pentachlorophenol ND 10 ug/l108-95-2 Phenol ND 5.1 ug/l95-95-4 2,4,5-Trichlorophenol ND 10 ug/l88-06-2 2,4,6-Trichlorophenol ND 10 ug/l62-53-3 Aniline ND 10 ug/l101-55-3 4-Bromophenyl phenyl ether ND 5.1 ug/l85-68-7 Butyl benzyl phthalate ND 5.1 ug/l91-58-7 2-Chloronaphthalene ND 5.1 ug/l106-47-8 4-Chloroaniline ND 10 ug/l86-74-8 Carbazole ND 2.0 ug/l111-91-1 bis(2-Chloroethoxy)methane ND 5.1 ug/l111-44-4 bis(2-Chloroethyl)ether a ND 5.1 ug/l108-60-1 bis(2-Chloroisopropyl)ether a ND 5.1 ug/l7005-72-3 4-Chlorophenyl phenyl ether ND 5.1 ug/l121-14-2 2,4-Dinitrotoluene ND 10 ug/l606-20-2 2,6-Dinitrotoluene ND 10 ug/l91-94-1 3,3'-Dichlorobenzidine ND 5.1 ug/l132-64-9 Dibenzofuran ND 2.0 ug/l84-74-2 Di-n-butyl phthalate ND 5.1 ug/l117-84-0 Di-n-octyl phthalate ND 5.1 ug/l84-66-2 Diethyl phthalate ND 5.1 ug/l131-11-3 Dimethyl phthalate ND 5.1 ug/l


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MC48821

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SGS Accutest





117-81-7 bis(2-Ethylhexyl)phthalate ND 2.0 ug/l118-74-1 Hexachlorobenzene ND 5.1 ug/l87-68-3 Hexachlorobutadiene ND 5.1 ug/l77-47-4 Hexachlorocyclopentadiene a ND 10 ug/l67-72-1 Hexachloroethane ND 5.1 ug/l78-59-1 Isophorone ND 5.1 ug/l91-57-6 2-Methylnaphthalene ND 2.0 ug/l88-74-4 2-Nitroaniline ND 10 ug/l99-09-2 3-Nitroaniline ND 10 ug/l100-01-6 4-Nitroaniline ND 10 ug/l98-95-3 Nitrobenzene ND 5.1 ug/l621-64-7 N-Nitroso-di-n-propylamine ND 5.1 ug/l86-30-6 N-Nitrosodiphenylamine ND 10 ug/l82-68-8 Pentachloronitrobenzene ND 10 ug/l110-86-1 Pyridine ND 10 ug/l95-94-3 1,2,4,5-Tetrachlorobenzene ND 10 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.1 ug/l


367-12-4 2-Fluorophenol 48% 10-80%4165-62-2 Phenol-d5 29% 10-72%118-79-6 2,4,6-Tribromophenol 103% 42-134%4165-60-0 Nitrobenzene-d5 76% 25-117%321-60-8 2-Fluorobiphenyl 86% 24-112%1718-51-0 Terphenyl-d14 108% 48-133%



280 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D BY SIM SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 I103758.D 1 11/29/16 AA 11/22/16 OP49190 MSI3935Run #2


BN PAH List


83-32-9 Acenaphthene ND 0.10 ug/l208-96-8 Acenaphthylene ND 0.10 ug/l120-12-7 Anthracene ND 0.10 ug/l56-55-3 Benzo(a)anthracene ND 0.051 ug/l50-32-8 Benzo(a)pyrene ND 0.10 ug/l205-99-2 Benzo(b)fluoranthene ND 0.051 ug/l191-24-2 Benzo(g,h,i)perylene ND 0.10 ug/l207-08-9 Benzo(k)fluoranthene ND 0.10 ug/l218-01-9 Chrysene ND 0.10 ug/l53-70-3 Dibenzo(a,h)anthracene ND 0.10 ug/l206-44-0 Fluoranthene ND 0.10 ug/l86-73-7 Fluorene ND 0.10 ug/l193-39-5 Indeno(1,2,3-cd)pyrene ND 0.10 ug/l91-57-6 2-Methylnaphthalene ND 2.0 ug/l91-20-3 Naphthalene ND 2.0 ug/l85-01-8 Phenanthrene ND 0.051 ug/l129-00-0 Pyrene ND 0.10 ug/l


4165-60-0 Nitrobenzene-d5 77% 26-121%321-60-8 2-Fluorobiphenyl 62% 28-107%1718-51-0 Terphenyl-d14 87% 29-129%


281 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List


15972-60-8 Alachlor ND 0.10 ug/l309-00-2 Aldrin ND 0.010 ug/l319-84-6 alpha-BHC ND 0.010 ug/l319-85-7 beta-BHC ND 0.010 ug/l319-86-8 delta-BHC ND 0.010 ug/l58-89-9 gamma-BHC (Lindane) ND 0.010 ug/l12789-03-6 Chlordane ND 0.10 ug/l60-57-1 Dieldrin ND 0.0020 ug/l72-54-8 4,4'-DDD ND 0.010 ug/l72-55-9 4,4'-DDE ND 0.010 ug/l50-29-3 4,4'-DDT ND 0.010 ug/l72-20-8 Endrin ND 0.010 ug/l1031-07-8 Endosulfan sulfate ND 0.010 ug/l7421-93-4 Endrin aldehyde ND 0.010 ug/l53494-70-5 Endrin ketone ND 0.010 ug/l959-98-8 Endosulfan-I ND 0.010 ug/l33213-65-9 Endosulfan-II ND 0.010 ug/l76-44-8 Heptachlor ND 0.010 ug/l1024-57-3 Heptachlor epoxide ND 0.010 ug/l72-43-5 Methoxychlor ND 0.010 ug/l8001-35-2 Toxaphene ND 0.51 ug/l




282 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8082A SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT





12674-11-2 Aroclor 1016 ND 0.26 ug/l11104-28-2 Aroclor 1221 ND 0.26 ug/l11141-16-5 Aroclor 1232 ND 0.26 ug/l53469-21-9 Aroclor 1242 ND 0.26 ug/l12672-29-6 Aroclor 1248 ND 0.26 ug/l11097-69-1 Aroclor 1254 ND 0.26 ug/l11096-82-5 Aroclor 1260 ND 0.26 ug/l37324-23-5 Aroclor 1262 ND 0.26 ug/l11100-14-4 Aroclor 1268 ND 0.26 ug/l




283 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 IR3292.D 1 11/23/16 MD 11/21/16 OP49181 GIR229Run #2



CT-ETPH (C9-C36) ND 0.10 mg/l


84-15-1 o-Terphenyl 73% 50-149%


284 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16

Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

Total Metals Analysis


Arsenic 9.5 4.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Barium 421 50 ug/l 1 11/21/16 11/28/16 EAL SW846 6010C 3 SW846 3010A 4

Cadmium <4.0 4.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Chromium 46.3 10 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Copper 120 25 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Lead 25.9 5.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Mercury <0.20 0.20 ug/l 1 11/22/16 11/23/16 EAL SW846 7470A 2 SW846 7470A 5

Selenium <10 10 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Silver <5.0 5.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Zinc 67.0 20 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

(1) Instrument QC Batch: MA19640(2) Instrument QC Batch: MA19643(3) Instrument QC Batch: MA19646(4) Prep QC Batch: MP27038(5) Prep QC Batch: MP27050


285 of 555

MC48821

44.43

SGS Accutest


Client Sample ID: B-1/GW Lab Sample ID: MC48821-22F Date Sampled: 11/16/16 Matrix: AQ - Groundwater Filtered Date Received: 11/18/16


Dissolved Metals Analysis


Arsenic <4.0 4.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Barium 72.5 50 ug/l 1 11/21/16 11/28/16 EAL SW846 6010C 3 SW846 3010A 4


Chromium <10 10 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Copper <25 25 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4

Lead <5.0 5.0 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4




Zinc <20 20 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 1 SW846 3010A 4



286 of 555

MC48821

44.44

SGS Accutest





VOA RCP List


67-64-1 Acetone ND 10 ug/l107-13-1 Acrylonitrile ND 5.0 ug/l71-43-2 Benzene 0.60 0.50 ug/l108-86-1 Bromobenzene ND 5.0 ug/l75-27-4 Bromodichloromethane ND 1.0 ug/l75-25-2 Bromoform a ND 1.0 ug/l74-83-9 Bromomethane ND 2.0 ug/l78-93-3 2-Butanone (MEK) ND 10 ug/l104-51-8 n-Butylbenzene ND 5.0 ug/l135-98-8 sec-Butylbenzene ND 5.0 ug/l98-06-6 tert-Butylbenzene ND 5.0 ug/l75-15-0 Carbon disulfide a ND 5.0 ug/l56-23-5 Carbon tetrachloride ND 1.0 ug/l108-90-7 Chlorobenzene ND 1.0 ug/l75-00-3 Chloroethane ND 2.0 ug/l67-66-3 Chloroform ND 1.0 ug/l74-87-3 Chloromethane ND 2.0 ug/l95-49-8 o-Chlorotoluene ND 5.0 ug/l106-43-4 p-Chlorotoluene ND 5.0 ug/l96-12-8 1,2-Dibromo-3-chloropropan a ND 5.0 ug/l124-48-1 Dibromochloromethane ND 1.0 ug/l106-93-4 1,2-Dibromoethane ND 1.0 ug/l95-50-1 1,2-Dichlorobenzene ND 1.0 ug/l541-73-1 1,3-Dichlorobenzene ND 1.0 ug/l106-46-7 1,4-Dichlorobenzene ND 1.0 ug/l75-71-8 Dichlorodifluoromethane ND 2.0 ug/l75-34-3 1,1-Dichloroethane ND 1.0 ug/l107-06-2 1,2-Dichloroethane ND 1.0 ug/l75-35-4 1,1-Dichloroethene a ND 1.0 ug/l156-59-2 cis-1,2-Dichloroethene ND 1.0 ug/l156-60-5 trans-1,2-Dichloroethene a ND 1.0 ug/l78-87-5 1,2-Dichloropropane ND 2.0 ug/l


287 of 555

MC48821

44.45

SGS Accutest



VOA RCP List







288 of 555

MC48821

44.45

SGS Accutest



VOA RCP List





289 of 555

MC48821

44.45

SGS Accutest









290 of 555

MC48821

44.45

SGS Accutest










291 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D BY SIM SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



BN PAH List






292 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List






293 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8082A SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT









294 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT






84-15-1 o-Terphenyl 84% 50-149%


295 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16
















296 of 555

MC48821

44.45

SGS Accutest


Client Sample ID: B-3/GW Lab Sample ID: MC48821-23F Date Sampled: 11/16/16 Matrix: AQ - Groundwater Filtered Date Received: 11/18/16
















297 of 555

MC48821

44.46

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



VOA RCP List


67-64-1 Acetone ND 10 ug/l107-13-1 Acrylonitrile ND 5.0 ug/l71-43-2 Benzene 0.59 0.50 ug/l108-86-1 Bromobenzene ND 5.0 ug/l75-27-4 Bromodichloromethane ND 1.0 ug/l75-25-2 Bromoform a ND 1.0 ug/l74-83-9 Bromomethane ND 2.0 ug/l78-93-3 2-Butanone (MEK) ND 10 ug/l104-51-8 n-Butylbenzene ND 5.0 ug/l135-98-8 sec-Butylbenzene ND 5.0 ug/l98-06-6 tert-Butylbenzene ND 5.0 ug/l75-15-0 Carbon disulfide a ND 5.0 ug/l56-23-5 Carbon tetrachloride ND 1.0 ug/l108-90-7 Chlorobenzene ND 1.0 ug/l75-00-3 Chloroethane ND 2.0 ug/l67-66-3 Chloroform ND 1.0 ug/l74-87-3 Chloromethane ND 2.0 ug/l95-49-8 o-Chlorotoluene ND 5.0 ug/l106-43-4 p-Chlorotoluene ND 5.0 ug/l96-12-8 1,2-Dibromo-3-chloropropan a ND 5.0 ug/l124-48-1 Dibromochloromethane ND 1.0 ug/l106-93-4 1,2-Dibromoethane ND 1.0 ug/l95-50-1 1,2-Dichlorobenzene ND 1.0 ug/l541-73-1 1,3-Dichlorobenzene ND 1.0 ug/l106-46-7 1,4-Dichlorobenzene ND 1.0 ug/l75-71-8 Dichlorodifluoromethane ND 2.0 ug/l75-34-3 1,1-Dichloroethane ND 1.0 ug/l107-06-2 1,2-Dichloroethane ND 1.0 ug/l75-35-4 1,1-Dichloroethene a ND 1.0 ug/l156-59-2 cis-1,2-Dichloroethene ND 1.0 ug/l156-60-5 trans-1,2-Dichloroethene a ND 1.0 ug/l78-87-5 1,2-Dichloropropane ND 2.0 ug/l


298 of 555

MC48821

44.47

SGS Accutest



VOA RCP List







299 of 555

MC48821

44.47

SGS Accutest



VOA RCP List





300 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT







301 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT








302 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8270D BY SIM SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



BN PAH List






303 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List






304 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: SW846 8082A SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT









305 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT






84-15-1 o-Terphenyl 72% 50-149%


306 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24 Date Sampled: 11/16/16 Matrix: AQ - Ground Water Date Received: 11/18/16
















307 of 555

MC48821

44.47

SGS Accutest


Client Sample ID: B-3/GW DUP Lab Sample ID: MC48821-24F Date Sampled: 11/16/16 Matrix: AQ - Groundwater Filtered Date Received: 11/18/16
















308 of 555

MC48821

44.48

SGS Accutest


Client Sample ID: TRIP BLANK Lab Sample ID: MC48821-25 Date Sampled: 11/16/16 Matrix: AQ - Trip Blank Water Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



VOA RCP List




309 of 555

MC48821

44.49

SGS Accutest



VOA RCP List







310 of 555

MC48821

44.49

SGS Accutest



VOA RCP List





311 of 555

MC48821

44.49

SGS Accutest


Client Sample ID: TRIP BLANK Lab Sample ID: MC48821-26 Date Sampled: 11/16/16 Matrix: SO - Trip Blank Methanol Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



VOA RCP List


67-64-1 Acetone ND 250 ug/kg107-13-1 Acrylonitrile ND 630 ug/kg71-43-2 Benzene ND 25 ug/kg108-86-1 Bromobenzene ND 130 ug/kg75-27-4 Bromodichloromethane ND 50 ug/kg75-25-2 Bromoform ND 50 ug/kg74-83-9 Bromomethane ND 250 ug/kg78-93-3 2-Butanone (MEK) ND 250 ug/kg104-51-8 n-Butylbenzene ND 130 ug/kg135-98-8 sec-Butylbenzene ND 130 ug/kg98-06-6 tert-Butylbenzene ND 130 ug/kg75-15-0 Carbon disulfide ND 130 ug/kg56-23-5 Carbon tetrachloride ND 50 ug/kg108-90-7 Chlorobenzene ND 50 ug/kg75-00-3 Chloroethane ND 250 ug/kg67-66-3 Chloroform ND 50 ug/kg74-87-3 Chloromethane ND 130 ug/kg95-49-8 o-Chlorotoluene ND 130 ug/kg106-43-4 p-Chlorotoluene ND 130 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 130 ug/kg124-48-1 Dibromochloromethane ND 130 ug/kg106-93-4 1,2-Dibromoethane ND 50 ug/kg95-50-1 1,2-Dichlorobenzene ND 50 ug/kg541-73-1 1,3-Dichlorobenzene ND 50 ug/kg106-46-7 1,4-Dichlorobenzene ND 50 ug/kg75-71-8 Dichlorodifluoromethane ND 130 ug/kg75-34-3 1,1-Dichloroethane ND 50 ug/kg107-06-2 1,2-Dichloroethane ND 50 ug/kg75-35-4 1,1-Dichloroethene a ND 50 ug/kg156-59-2 cis-1,2-Dichloroethene ND 50 ug/kg156-60-5 trans-1,2-Dichloroethene ND 50 ug/kg78-87-5 1,2-Dichloropropane ND 50 ug/kg


312 of 555

MC48821

44.50

SGS Accutest



VOA RCP List


142-28-9 1,3-Dichloropropane ND 130 ug/kg594-20-7 2,2-Dichloropropane ND 130 ug/kg563-58-6 1,1-Dichloropropene ND 130 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 50 ug/kg10061-02-6 trans-1,3-Dichloropropene ND 50 ug/kg100-41-4 Ethylbenzene ND 50 ug/kg76-13-1 Freon 113 ND 130 ug/kg87-68-3 Hexachlorobutadiene ND 130 ug/kg591-78-6 2-Hexanone ND 130 ug/kg98-82-8 Isopropylbenzene ND 130 ug/kg99-87-6 p-Isopropyltoluene ND 130 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 50 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 130 ug/kg74-95-3 Methylene bromide ND 130 ug/kg75-09-2 Methylene chloride ND 50 ug/kg91-20-3 Naphthalene ND 130 ug/kg103-65-1 n-Propylbenzene ND 130 ug/kg100-42-5 Styrene ND 130 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 50 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 130 ug/kg127-18-4 Tetrachloroethene ND 50 ug/kg109-99-9 Tetrahydrofuran ND 250 ug/kg108-88-3 Toluene ND 130 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 250 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 130 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 130 ug/kg71-55-6 1,1,1-Trichloroethane ND 50 ug/kg79-00-5 1,1,2-Trichloroethane ND 50 ug/kg79-01-6 Trichloroethene ND 50 ug/kg75-69-4 Trichlorofluoromethane ND 50 ug/kg96-18-4 1,2,3-Trichloropropane ND 130 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 130 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 130 ug/kg75-01-4 Vinyl chloride ND 250 ug/kg

m,p-Xylene ND 50 ug/kg95-47-6 o-Xylene ND 50 ug/kg




313 of 555

MC48821

44.50

SGS Accutest



VOA RCP List





314 of 555

MC48821

44.50

SGS Accutest


Client Sample ID: TRIP BLANK Lab Sample ID: MC48821-26A Date Sampled: 11/16/16 Matrix: SO - Trip Blank Soil Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 M82146.D 1 11/26/16 DRY n/a n/a MSM2946Run #2


VOA RCP List


67-64-1 Acetone ND 10 ug/kg107-13-1 Acrylonitrile ND 25 ug/kg71-43-2 Benzene ND 1.0 ug/kg108-86-1 Bromobenzene ND 5.0 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane a ND 10 ug/kg78-93-3 2-Butanone (MEK) ND 10 ug/kg104-51-8 n-Butylbenzene ND 5.0 ug/kg135-98-8 sec-Butylbenzene ND 5.0 ug/kg98-06-6 tert-Butylbenzene ND 5.0 ug/kg75-15-0 Carbon disulfide ND 5.0 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane a ND 10 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane a ND 5.0 ug/kg95-49-8 o-Chlorotoluene ND 5.0 ug/kg106-43-4 p-Chlorotoluene ND 5.0 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 ug/kg124-48-1 Dibromochloromethane ND 5.0 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane a ND 5.0 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg


315 of 555

MC48821

44.51

SGS Accutest



VOA RCP List







316 of 555

MC48821

44.51

SGS Accutest



VOA RCP List





317 of 555

MC48821

44.51

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8260C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



VOA RCP List




318 of 555

MC48821

44.52

SGS Accutest



VOA RCP List







319 of 555

MC48821

44.52

SGS Accutest



VOA RCP List





320 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT







321 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT








322 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8270D BY SIM SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



BN PAH List






323 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT



Pesticide RCP List






324 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: SW846 8082A SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT









325 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16 Method: CT-ETPH 7/06 SW846 3510C Percent Solids: n/a Project: Route 69 Improvements, New Haven, CT






84-15-1 o-Terphenyl 71% 50-149%


326 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27 Date Sampled: 11/16/16 Matrix: AQ - Equipment Blank Date Received: 11/18/16





Barium <50 50 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 2 SW846 3010A 3











327 of 555

MC48821

44.52

SGS Accutest


Client Sample ID: EQUIPMENT BLANK Lab Sample ID: MC48821-27F Date Sampled: 11/16/16 Matrix: AQ - Equip Blank Filtered Date Received: 11/18/16





Barium <50 50 ug/l 1 11/21/16 11/23/16 EAL SW846 6010C 2 SW846 3010A 3











328 of 555

MC48821

44.53

SGS Accutest

Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Chain of Custody• RCP Form• Sample Tracking Chronicle• QC Evaluation: CT RCP Limits


329 of 555

MC48821

5

MC48821: Chain of CustodyPage 1 of 4

330 of 555

MC48821

55.1


331 of 555

MC48821

55.1


332 of 555

MC48821

55.1

SGS Accutest Sample Receipt Summary

Job Number: MC48821 Client: BL COMP.

Date / Time Received: 11/18/2016 7:00:00 PM Delivery Method: SGS

Project: RTE 69

4. No. Coolers: 3

Airbill #'s:

Cooler Security

1. Custody Seals Present:

Y or N

2. Custody Seals Intact:

3. COC Present:

4. Smpl Dates/Time OK

2. Thermometer ID:

Cooler Temperature Y or N

1. Temp criteria achieved:

3. Cooler media:

IRGUN1;

Ice (Bag)

Quality Control Preservation Y or N N/A

1. Trip Blank present / cooler:

2. Trip Blank listed on COC:

3. Samples preserved properly:

4. VOCs headspace free:

Sample Integrity - Documentation Y or N

1. Sample labels present on bottles:

2. Container labeling complete:

3. Sample container label / COC agree:

Sample Integrity - Condition Y or N

1. Sample recvd within HT:

3. Condition of sample:

2. All containers accounted for:

Sample Integrity - Instructions

1. Analysis requested is clear:

2. Bottles received for unspecified tests

3. Sufficient volume recvd for analysis:

4. Compositing instructions clear:

5. Filtering instructions clear:

Intact

Y or N

Comments

Y or N N/A

Cooler Temps (Initial/Adjusted): #1: (3/3); #2: (2.9/2.9); #3: (3/3);


333 of 555

MC48821

55.1

Laboratory Name: Client:

Project Location: Project Number:

Sampling Date(s):

Laboratory Sample ID(s):

Methods:

1 Yes No

1A Yes No

1B Yes No

NA

2 Yes No

3 Yes No

4 Yes No

5 Yes No

Yes No

6 Yes No

7 Yes No

Authorized

Signature: Position: Lab Director

Printed Name: H. (Brad) Madadian Date:

Accutest New England

Are project-specific matrix spikes and laboratory duplicates included in this

data set?

Note: For all questions to which the response was "No" (with the exception of question #7), additional

information must be provided in an attached narrative. If the answer to question #1, #1A or #1B is "No", the

data package does not meet the requirements for "Reasonable Confidence".

I, the undersigned, attest under pains and penalties of perjury that, to the best of my knowledge and belief

and based upon my personal inquiry of those responsible for providing the information contained in this

analytical report, such information is accurate and complete.

Reza Tand

12/2/2016

Were all samples received by the laboratory in a condition consistent with

that described on the associated chain-of-custody document(s)?

Were samples received at an appropriate temperature (<6° C)?

Were all QA/QC performance criteria specified in the CTDEP Reasonable

Confidence Protocol documents achieved?

a) Were reporting limits specified or referenced on the chain-of-custody?

b) Were these reporting limits met?

For each analytical method referenced in this laboratory report package,

were results reported for all constituents identified in the method-specific

analyte lists presented in the Reasonable Confidence Protocol documents?

11/16/2016

MC48821-26A, MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5,

MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11,

MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16, MC48821-17,

MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-22, MC48821-23,

MC48821-24, MC48821-25, MC48821-26, MC48821-27, MC48821-1A, MC48821-2A,

MC48821-3A, MC48821-4A, MC48821-5A, MC48821-6A, MC48821-7A, MC48821-8A,

MC48821-9A, MC48821-10A, MC48821-11A, MC48821-12A, MC48821-13A, MC48821-

14A, MC48821-15A, MC48821-16A, MC48821-17A, MC48821-18A, MC48821-19A,

MC48821-20A, MC48821-21A, MC48821-22F, MC48821-23F, MC48821-24F, MC48821-

27FRefer to case narrative.

For each analytical method referenced in this laboratory report package, were all

specified QA/QC performance criteria followed, including the requirement to explain any

criteria falling outside of acceptable guidelines, as specified in the CTDEP method-specific

Reasonable Confidence Protocol

documents)?

Where all the method specified preservation and holding time requirements met?

VPH and EPH mehods only: Was the VPH or EPH method conducted without significant

modifications (See section 11.3 of respective methods)

Reasonable Confidence Protocol

Laboratory Analysis

QA/QC Certification Form

Accutest New England BL Companies

Route 69 Improvements, New Haven, CT 14EC0047

334 of 555

MC48821

55.2

SGS Accutest

Internal Sample Tracking Chronicle



SampleNumber Method Analyzed By Prepped By Test Codes

MC48821-1 Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-1(0-5')

MC48821-1 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-1 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-1 SW846 6010C 22-NOV-16 19:25 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-1 SW846 1020 23-NOV-16 HS IGNMC48821-1 SW846 8260C 23-NOV-16 01:57 KP V8260RCPMC48821-1 SW846 7471B 23-NOV-16 13:31 EAL 22-NOV-16 EM HGMC48821-1 SW846 CHAP7 23-NOV-16 15:10 HS 22-NOV-16 HS CREACMC48821-1 SW846 8260C 23-NOV-16 22:02 KP V8260RCPMC48821-1 CT-ETPH 7/06 25-NOV-16 11:58 MD 22-NOV-16 AJ BCTTPHMC48821-1 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-1 SW846 8270D 26-NOV-16 16:31 DRY 22-NOV-16 PA AB8270RCPMC48821-1 SW846 8082A 30-NOV-16 09:42 TA 29-NOV-16 PA P8082RCPMC48821-1 SW846 8081B 30-NOV-16 11:10 TA 29-NOV-16 PA P8081RCP


MC48821-2 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-2 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-2 SW846 6010C 22-NOV-16 19:30 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-2 SW846 1020 23-NOV-16 HS IGNMC48821-2 SW846 8260C 23-NOV-16 02:25 KP V8260RCPMC48821-2 SW846 7471B 23-NOV-16 13:26 EAL 22-NOV-16 EM HGMC48821-2 SW846 CHAP7 23-NOV-16 15:10 HS 22-NOV-16 HS CREACMC48821-2 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-2 CT-ETPH 7/06 28-NOV-16 11:29 MD 23-NOV-16 PA BCTTPHMC48821-2 SW846 8270D 29-NOV-16 14:45 MR 23-NOV-16 PA AB8270RCPMC48821-2 SW846 8081B 30-NOV-16 08:44 TA 29-NOV-16 PA P8081RCPMC48821-2 SW846 8082A 30-NOV-16 09:57 TA 29-NOV-16 PA P8082RCP


MC48821-3 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-3 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-3 SW846 6010C 22-NOV-16 19:45 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-3 SW846 1020 23-NOV-16 HS IGN

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MC48821

55.3

SGS Accutest





MC48821-3 SW846 8260C 23-NOV-16 02:53 KP V8260RCPMC48821-3 SW846 7471B 23-NOV-16 13:38 EAL 22-NOV-16 EM HGMC48821-3 SW846 CHAP7 23-NOV-16 15:10 HS 22-NOV-16 HS CREACMC48821-3 SW846 8260C 23-NOV-16 22:30 KP V8260RCPMC48821-3 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-3 CT-ETPH 7/06 28-NOV-16 12:01 MD 23-NOV-16 PA BCTTPHMC48821-3 SW846 8270D 29-NOV-16 15:11 MR 23-NOV-16 PA AB8270RCPMC48821-3 SW846 8081B 30-NOV-16 09:57 TA 29-NOV-16 PA P8081RCPMC48821-3 SW846 8082A 30-NOV-16 10:13 TA 29-NOV-16 PA P8082RCP




MC48821-5 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-5 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-5 SW846 6010C 22-NOV-16 19:55 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-5 SW846 1020 23-NOV-16 HS IGNMC48821-5 SW846 8260C 23-NOV-16 03:48 KP V8260RCPMC48821-5 SW846 7471B 23-NOV-16 13:42 EAL 22-NOV-16 EM HGMC48821-5 SW846 CHAP7 23-NOV-16 15:10 HS 22-NOV-16 HS CREACMC48821-5 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-5 CT-ETPH 7/06 28-NOV-16 14:06 MD 23-NOV-16 PA BCTTPHMC48821-5 SW846 8270D 29-NOV-16 16:02 MR 23-NOV-16 PA AB8270RCPMC48821-5 SW846 8081B 30-NOV-16 10:26 TA 29-NOV-16 PA P8081RCP

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MC48821

55.3

SGS Accutest





MC48821-5 SW846 8082A 30-NOV-16 10:45 TA 29-NOV-16 PA P8082RCP




MC48821-7 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-7 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-7 SW846 6010C 22-NOV-16 20:05 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-7 SW846 1020 23-NOV-16 HS IGNMC48821-7 SW846 7471B 23-NOV-16 13:47 EAL 22-NOV-16 EM HGMC48821-7 SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-7 SW846 8260C 23-NOV-16 22:30 TB V8260RCPMC48821-7 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-7 CT-ETPH 7/06 28-NOV-16 21:25 MD 23-NOV-16 PA BCTTPHMC48821-7 SW846 8270D 29-NOV-16 16:54 MR 23-NOV-16 PA AB8270RCPMC48821-7 SW846 8082A 30-NOV-16 11:16 TA 29-NOV-16 PA P8082RCPMC48821-7 SW846 8081B 30-NOV-16 11:24 TA 29-NOV-16 PA P8081RCP


MC48821-8 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-8 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-8 SW846 6010C 22-NOV-16 20:10 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SE

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MC48821

55.3

SGS Accutest





MC48821-8 SW846 1020 23-NOV-16 HS IGNMC48821-8 SW846 7471B 23-NOV-16 13:49 EAL 22-NOV-16 EM HGMC48821-8 SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-8 SW846 8260C 23-NOV-16 21:11 TB V8260RCPMC48821-8 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-8 CT-ETPH 7/06 28-NOV-16 13:03 MD 23-NOV-16 PA BCTTPHMC48821-8 SW846 8270D 29-NOV-16 17:20 MR 23-NOV-16 PA AB8270RCPMC48821-8 SW846 8081B 30-NOV-16 09:27 TA 29-NOV-16 PA P8081RCPMC48821-8 SW846 8082A 30-NOV-16 11:48 TA 29-NOV-16 PA P8082RCP


MC48821-9 SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-9 SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-9 SW846 6010C 22-NOV-16 19:10 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-9 SW846 1020 23-NOV-16 HS IGNMC48821-9 SW846 8260C 23-NOV-16 04:43 KP V8260RCPMC48821-9 SW846 7471B 23-NOV-16 13:51 EAL 22-NOV-16 EM HGMC48821-9 SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-9 SW846 8260C 23-NOV-16 22:57 KP V8260RCPMC48821-9 SW846 9045D 26-NOV-16 13:32 EL PHMC48821-9 CT-ETPH 7/06 28-NOV-16 15:09 MD 23-NOV-16 PA BCTTPHMC48821-9 SW846 8270D 29-NOV-16 17:46 MR 23-NOV-16 PA AB8270RCPMC48821-9 SW846 8081B 30-NOV-16 10:11 TA 29-NOV-16 PA P8081RCPMC48821-9 SW846 8082A 30-NOV-16 12:04 TA 29-NOV-16 PA P8082RCP

MC48821-10Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-5(6-8')

MC48821-10SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-10SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-10SW846 6010C 22-NOV-16 20:15 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-10SW846 1020 23-NOV-16 HS IGNMC48821-10SW846 8260C 23-NOV-16 05:11 KP V8260RCPMC48821-10SW846 7471B 23-NOV-16 13:54 EAL 22-NOV-16 EM HGMC48821-10SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-10SW846 9045D 26-NOV-16 13:32 EL PHMC48821-10CT-ETPH 7/06 28-NOV-16 10:58 MD 23-NOV-16 PA BCTTPHMC48821-10SW846 8270D 29-NOV-16 18:12 MR 23-NOV-16 PA AB8270RCP

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MC48821

55.3

SGS Accutest





MC48821-10SW846 8081B 30-NOV-16 09:41 TA 29-NOV-16 PA P8081RCPMC48821-10SW846 8082A 30-NOV-16 12:20 TA 29-NOV-16 PA P8082RCP


MC48821-11SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-11SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-11SW846 6010C 22-NOV-16 20:20 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-11SW846 1020 23-NOV-16 HS IGNMC48821-11SW846 8260C 23-NOV-16 05:38 KP V8260RCPMC48821-11SW846 7471B 23-NOV-16 13:56 EAL 22-NOV-16 EM HGMC48821-11SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-11SW846 8260C 23-NOV-16 23:26 KP V8260RCPMC48821-11SW846 9045D 26-NOV-16 13:32 EL PHMC48821-11SW846 8082A 28-NOV-16 16:40 TA 23-NOV-16 AJ P8082RCPMC48821-11CT-ETPH 7/06 28-NOV-16 18:48 MD 23-NOV-16 PA BCTTPHMC48821-11SW846 8081B 29-NOV-16 12:57 TA 23-NOV-16 AJ P8081RCPMC48821-11SW846 8270D 29-NOV-16 18:38 MR 23-NOV-16 PA AB8270RCP


MC48821-12SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-12SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-12SW846 6010C 22-NOV-16 20:25 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-12SW846 1020 23-NOV-16 HS IGNMC48821-12SW846 8260C 23-NOV-16 06:06 KP V8260RCPMC48821-12SW846 7471B 23-NOV-16 13:58 EAL 22-NOV-16 EM HGMC48821-12SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-12SW846 9045D 26-NOV-16 13:32 EL PHMC48821-12CT-ETPH 7/06 28-NOV-16 13:35 MD 23-NOV-16 PA BCTTPHMC48821-12SW846 8082A 28-NOV-16 16:57 TA 23-NOV-16 AJ P8082RCPMC48821-12SW846 8081B 29-NOV-16 12:42 TA 23-NOV-16 AJ P8081RCPMC48821-12SW846 8270D 29-NOV-16 19:04 MR 23-NOV-16 PA AB8270RCP


MC48821-13SM 2540G-97 MOD 21-NOV-16 HS %SOL

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MC48821

55.3

SGS Accutest





MC48821-13SW846 6010C 22-NOV-16 20:30 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-13SW846 8260C 23-NOV-16 06:34 KP V8260RCPMC48821-13SW846 7471B 23-NOV-16 14:24 EAL 22-NOV-16 EM HGMC48821-13SW846 8260C 23-NOV-16 23:54 KP V8260RCPMC48821-13CT-ETPH 7/06 28-NOV-16 15:41 MD 23-NOV-16 PA BCTTPHMC48821-13SW846 8082A 28-NOV-16 17:14 TA 23-NOV-16 AJ P8082RCPMC48821-13SW846 8081B 29-NOV-16 11:44 TA 23-NOV-16 AJ P8081RCPMC48821-13SW846 8081B 29-NOV-16 14:39 TA 23-NOV-16 AJ P8081RCPMC48821-13SW846 8270D 29-NOV-16 19:30 MR 23-NOV-16 PA AB8270RCP


MC48821-14SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-14SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-14SW846 6010C 22-NOV-16 20:45 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-14SW846 1020 23-NOV-16 HS IGNMC48821-14SW846 8260C 23-NOV-16 07:01 KP V8260RCPMC48821-14SW846 7471B 23-NOV-16 14:07 EAL 22-NOV-16 EM HGMC48821-14SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-14SW846 8260C 24-NOV-16 00:21 KP V8260RCPMC48821-14SW846 9045D 26-NOV-16 13:32 EL PHMC48821-14CT-ETPH 7/06 28-NOV-16 16:12 MD 23-NOV-16 PA BCTTPHMC48821-14SW846 8082A 28-NOV-16 17:30 TA 23-NOV-16 AJ P8082RCPMC48821-14SW846 8081B 29-NOV-16 11:59 TA 23-NOV-16 AJ P8081RCPMC48821-14SW846 8081B 29-NOV-16 14:54 TA 23-NOV-16 AJ P8081RCPMC48821-14SW846 8270D 29-NOV-16 19:56 MR 23-NOV-16 PA AB8270RCP

MC48821-15Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAHA-1(0-2')

MC48821-15SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-15SW846 6010C 22-NOV-16 20:50 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-15SW846 8260C 23-NOV-16 07:29 KP V8260RCPMC48821-15SW846 7471B 23-NOV-16 14:10 EAL 22-NOV-16 EM HGMC48821-15SW846 8260C 24-NOV-16 00:49 KP V8260RCPMC48821-15SW846 8082A 28-NOV-16 17:47 TA 23-NOV-16 AJ P8082RCPMC48821-15CT-ETPH 7/06 28-NOV-16 19:19 MD 23-NOV-16 PA BCTTPHMC48821-15SW846 8081B 29-NOV-16 12:13 TA 23-NOV-16 AJ P8081RCPMC48821-15SW846 8081B 29-NOV-16 15:08 TA 23-NOV-16 AJ P8081RCP

Page 6 of 14

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MC48821

55.3

SGS Accutest





MC48821-15SW846 8270D 29-NOV-16 20:22 MR 23-NOV-16 PA AB8270RCP


MC48821-16SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-16SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-16SW846 6010C 22-NOV-16 20:55 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-16SW846 1020 23-NOV-16 HS IGNMC48821-16SW846 8260C 23-NOV-16 07:57 KP V8260RCPMC48821-16SW846 7471B 23-NOV-16 14:13 EAL 22-NOV-16 EM HGMC48821-16SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-16SW846 8260C 24-NOV-16 01:17 KP V8260RCPMC48821-16SW846 9045D 26-NOV-16 13:32 EL PHMC48821-16SW846 8082A 28-NOV-16 18:03 TA 23-NOV-16 AJ P8082RCPMC48821-16CT-ETPH 7/06 28-NOV-16 18:16 MD 23-NOV-16 PA BCTTPHMC48821-16SW846 8081B 29-NOV-16 13:11 TA 23-NOV-16 AJ P8081RCPMC48821-16SW846 8270D 29-NOV-16 20:48 MR 23-NOV-16 PA AB8270RCP


MC48821-17SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-17SW846 6010C 22-NOV-16 21:00 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-17SW846 7471B 23-NOV-16 14:15 EAL 22-NOV-16 EM HGMC48821-17SW846 8260C 26-NOV-16 17:14 DRY V8260RCPMC48821-17SW846 8260C 28-NOV-16 14:35 CB V8260RCPMC48821-17SW846 8082A 28-NOV-16 18:37 TA 23-NOV-16 AJ P8082RCPMC48821-17CT-ETPH 7/06 28-NOV-16 19:51 MD 23-NOV-16 PA BCTTPHMC48821-17SW846 8081B 29-NOV-16 13:26 TA 23-NOV-16 AJ P8081RCPMC48821-17SW846 8270D 29-NOV-16 21:14 MR 23-NOV-16 PA AB8270RCP


MC48821-18SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-18SW846 6010C 22-NOV-16 21:05 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-18SW846 7471B 23-NOV-16 14:17 EAL 22-NOV-16 EM HGMC48821-18SW846 8260C 26-NOV-16 17:42 DRY V8260RCPMC48821-18SW846 8260C 28-NOV-16 15:03 CB V8260RCP

Page 7 of 14

341 of 555

MC48821

55.3

SGS Accutest





MC48821-18SW846 8082A 28-NOV-16 18:53 TA 23-NOV-16 AJ P8082RCPMC48821-18CT-ETPH 7/06 28-NOV-16 20:22 MD 23-NOV-16 PA BCTTPHMC48821-18SW846 8081B 29-NOV-16 12:28 TA 23-NOV-16 AJ P8081RCPMC48821-18SW846 8081B 29-NOV-16 15:23 TA 23-NOV-16 AJ P8081RCPMC48821-18SW846 8270D 30-NOV-16 14:09 MR 23-NOV-16 PA AB8270RCP


MC48821-19SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-19SW846 CHAP7 22-NOV-16 CF 22-NOV-16 HS SREACMC48821-19SW846 6010C 22-NOV-16 21:10 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-19SW846 1020 23-NOV-16 HS IGNMC48821-19SW846 7471B 23-NOV-16 14:20 EAL 22-NOV-16 EM HGMC48821-19SW846 CHAP7 23-NOV-16 15:17 HS 22-NOV-16 HS CREACMC48821-19SW846 9045D 26-NOV-16 13:32 EL PHMC48821-19SW846 8260C 26-NOV-16 18:09 DRY V8260RCPMC48821-19SW846 8260C 28-NOV-16 15:59 CB V8260RCPMC48821-19SW846 8082A 28-NOV-16 19:10 TA 23-NOV-16 AJ P8082RCPMC48821-19CT-ETPH 7/06 28-NOV-16 20:54 MD 23-NOV-16 PA BCTTPHMC48821-19SW846 8081B 29-NOV-16 14:09 TA 23-NOV-16 AJ P8081RCPMC48821-19SW846 8270D 30-NOV-16 14:34 MR 23-NOV-16 PA AB8270RCP

MC48821-1ACollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-1(0-5')

MC48821-1ASW846 6010C 23-NOV-16 21:37 EAL 23-NOV-16 EM EAG,EAS,EBA,ECD,ECR,EPB,ESEMC48821-1ASW846 7470A 28-NOV-16 15:17 JM 23-NOV-16 EM EHG


MC48821-20SM 2540G-97 MOD 21-NOV-16 HS %SOLMC48821-20SW846 6010C 22-NOV-16 21:15 EAL 22-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-20SW846 7471B 23-NOV-16 14:22 EAL 22-NOV-16 EM HGMC48821-20SW846 8260C 26-NOV-16 18:37 DRY V8260RCPMC48821-20SW846 8260C 28-NOV-16 16:26 CB V8260RCPMC48821-20CT-ETPH 7/06 28-NOV-16 16:44 MD 23-NOV-16 PA BCTTPHMC48821-20SW846 8082A 28-NOV-16 19:27 TA 23-NOV-16 AJ P8082RCPMC48821-20SW846 8081B 29-NOV-16 14:25 TA 23-NOV-16 AJ P8081RCP

Page 8 of 14

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MC48821

55.3

SGS Accutest





MC48821-20SW846 8270D 29-NOV-16 22:31 MR 23-NOV-16 PA AB8270RCP

MC48821-21Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAHA-6(0-2')DUP

MC48821-21SW846 6010C 23-NOV-16 20:22 EAL 23-NOV-16 EM AG,AS,BA,CD,CR,PB,SEMC48821-21SW846 8260C 26-NOV-16 19:05 DRY V8260RCPMC48821-21SM 2540G-97 MOD 28-NOV-16 JM %SOLMC48821-21SW846 8260C 28-NOV-16 16:54 CB V8260RCPMC48821-21SW846 7471B 29-NOV-16 12:58 EAL 28-NOV-16 EM HGMC48821-21SW846 8081B 30-NOV-16 11:39 TA 29-NOV-16 PA P8081RCPMC48821-21CT-ETPH 7/06 30-NOV-16 11:49 MD 29-NOV-16 PA BCTTPHMC48821-21SW846 8082A 30-NOV-16 12:35 TA 29-NOV-16 PA P8082RCP

MC48821-22Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-1/GW

MC48821-22SW846 8260C 22-NOV-16 21:19 KP V8260RCPMC48821-22SW846 8082A 22-NOV-16 22:45 TA 21-NOV-16 PA P8082RCPMC48821-22SW846 6010C 23-NOV-16 11:37 EAL 21-NOV-16 EM AG,AS,CD,CR,CU,PB,SE,ZNMC48821-22SW846 7470A 23-NOV-16 17:09 EAL 22-NOV-16 EM HGMC48821-22SW846 8081B 23-NOV-16 21:09 TA 22-NOV-16 PA P8081RCPMC48821-22CT-ETPH 7/06 23-NOV-16 23:52 MD 21-NOV-16 AJ BCTTPHMC48821-22SW846 6010C 28-NOV-16 11:03 EAL 21-NOV-16 EM BAMC48821-22SW846 8270D BY SIM 29-NOV-16 11:12 AA 22-NOV-16 PA B8270SIMPAHMC48821-22SW846 8270D 29-NOV-16 12:43 MR 22-NOV-16 PA AB8270RCP-PAH

MC48821-23Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-3/GW


Page 9 of 14

343 of 555

MC48821

55.3

SGS Accutest





MC48821-24Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-3/GW DUP


MC48821-25Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BATRIP BLANK

MC48821-25SW846 8260C 22-NOV-16 14:46 KP V8260RCP

MC48821-26Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BATRIP BLANK

MC48821-26SW846 8260C 23-NOV-16 15:48 TB V8260RCP

MC48821-27Collected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAEQUIPMENT BLANK

MC48821-27SW846 8260C 22-NOV-16 15:14 KP V8260RCPMC48821-27SW846 8082A 22-NOV-16 23:32 TA 21-NOV-16 PA P8082RCPMC48821-27SW846 7470A 23-NOV-16 17:18 EAL 22-NOV-16 EM HGMC48821-27SW846 6010C 23-NOV-16 19:23 EAL 21-NOV-16 VY AG,AS,BA,CD,CR,CU,PB,SE,ZNMC48821-27SW846 8081B 23-NOV-16 21:53 TA 22-NOV-16 PA P8081RCPMC48821-27CT-ETPH 7/06 24-NOV-16 01:16 MD 21-NOV-16 AJ BCTTPHMC48821-27SW846 8270D BY SIM 29-NOV-16 12:31 AA 22-NOV-16 PA B8270SIMPAHMC48821-27SW846 8270D 29-NOV-16 14:02 MR 22-NOV-16 PA AB8270RCP-PAH


MC48821-2ASW846 6010C 23-NOV-16 21:47 EAL 23-NOV-16 EM EAG,EAS,EBA,ECD,ECR,EPB,ESE

Page 10 of 14

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MC48821

55.3

SGS Accutest





MC48821-2ASW846 7470A 28-NOV-16 15:19 JM 23-NOV-16 EM EHG













Page 11 of 14

345 of 555

MC48821

55.3

SGS Accutest

















MC48821-15ACollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAHA-1(0-2')

Page 12 of 14

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MC48821

55.3

SGS Accutest
















MC48821-21ACollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAHA-6(0-2')DUP


Page 13 of 14

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MC48821

55.3

SGS Accutest





MC48821-22FCollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-1/GW

MC48821-22FSW846 6010C 23-NOV-16 11:42 EAL 21-NOV-16 EM AG,AS,CD,CR,CU,PB,SE,ZNMC48821-22FSW846 7470A 23-NOV-16 16:31 EAL 22-NOV-16 EM HGMC48821-22FSW846 6010C 28-NOV-16 11:08 EAL 21-NOV-16 EM BA

MC48821-23FCollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-3/GW


MC48821-24FCollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAB-3/GW DUP


MC48821-26ACollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BATRIP BLANK

MC48821-26ASW846 8260C 26-NOV-16 14:26 DRY V8260RCP

MC48821-27FCollected: 16-NOV-16 00:00 By: DSM Received: 18-NOV-16 By: BAEQUIPMENT BLANK

MC48821-27FSW846 7470A 23-NOV-16 17:21 EAL 22-NOV-16 EM HGMC48821-27FSW846 6010C 23-NOV-16 19:28 EAL 21-NOV-16 VY AG,AS,BA,CD,CR,CU,PB,SE,ZN

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QC Evaluation: CT RCP Limits Page 1 of 37 Job Number: MC48821Account: BL CompaniesProject: Route 69 Improvements, New Haven, CTCollected: 11/16/16

QC Sample ID CAS# Analyte Sample Result Result Units LimitsType Type

MSL4388 SW846 8260C

MSL4388-BS 67-64-1 Acetone BSP REC 79 % 70-130MSL4388-BS 107-13-1 Acrylonitrile BSP REC 81 % 70-130MSL4388-BS 71-43-2 Benzene BSP REC 95 % 70-130MSL4388-BS 108-86-1 Bromobenzene BSP REC 109 % 70-130MSL4388-BS 75-27-4 Bromodichloromethane BSP REC 100 % 70-130MSL4388-BS 75-25-2 Bromoform BSP REC 107 % 70-130MSL4388-BS 74-83-9 Bromomethane BSP REC 109 % 70-130MSL4388-BS 78-93-3 2-Butanone (MEK) BSP REC 89 % 70-130MSL4388-BS 104-51-8 n-Butylbenzene BSP REC 116 % 70-130MSL4388-BS 135-98-8 sec-Butylbenzene BSP REC 115 % 70-130MSL4388-BS 98-06-6 tert-Butylbenzene BSP REC 113 % 70-130MSL4388-BS 75-15-0 Carbon disulfide BSP REC 85 % 70-130MSL4388-BS 56-23-5 Carbon tetrachloride BSP REC 100 % 70-130MSL4388-BS 108-90-7 Chlorobenzene BSP REC 104 % 70-130MSL4388-BS 75-00-3 Chloroethane BSP REC 113 % 70-130MSL4388-BS 67-66-3 Chloroform BSP REC 94 % 70-130MSL4388-BS 74-87-3 Chloromethane BSP REC 118 % 70-130MSL4388-BS 95-49-8 o-Chlorotoluene BSP REC 109 % 70-130MSL4388-BS 106-43-4 p-Chlorotoluene BSP REC 110 % 70-130MSL4388-BS 96-12-8 1,2-Dibromo-3-chloropropane BSP REC 105 % 70-130MSL4388-BS 124-48-1 Dibromochloromethane BSP REC 106 % 70-130MSL4388-BS 106-93-4 1,2-Dibromoethane BSP REC 105 % 70-130MSL4388-BS 95-50-1 1,2-Dichlorobenzene BSP REC 106 % 70-130MSL4388-BS 541-73-1 1,3-Dichlorobenzene BSP REC 104 % 70-130MSL4388-BS 106-46-7 1,4-Dichlorobenzene BSP REC 101 % 70-130MSL4388-BS 75-71-8 Dichlorodifluoromethane BSP REC 131 % 70-130MSL4388-BS 75-34-3 1,1-Dichloroethane BSP REC 85 % 70-130MSL4388-BS 107-06-2 1,2-Dichloroethane BSP REC 94 % 70-130MSL4388-BS 75-35-4 1,1-Dichloroethene BSP REC 82 % 70-130MSL4388-BS 156-59-2 cis-1,2-Dichloroethene BSP REC 92 % 70-130MSL4388-BS 156-60-5 trans-1,2-Dichloroethene BSP REC 81 % 70-130MSL4388-BS 78-87-5 1,2-Dichloropropane BSP REC 98 % 70-130MSL4388-BS 142-28-9 1,3-Dichloropropane BSP REC 106 % 70-130MSL4388-BS 594-20-7 2,2-Dichloropropane BSP REC 108 % 70-130MSL4388-BS 563-58-6 1,1-Dichloropropene BSP REC 101 % 70-130MSL4388-BS 10061-01-5 cis-1,3-Dichloropropene BSP REC 108 % 70-130MSL4388-BS 10061-02-6 trans-1,3-Dichloropropene BSP REC 106 % 70-130MSL4388-BS 100-41-4 Ethylbenzene BSP REC 108 % 70-130MSL4388-BS 76-13-1 Freon 113 BSP REC 88 % 70-130MSL4388-BS 87-68-3 Hexachlorobutadiene BSP REC 118 % 70-130MSL4388-BS 591-78-6 2-Hexanone BSP REC 114 % 70-130MSL4388-BS 98-82-8 Isopropylbenzene BSP REC 116 % 70-130

* Sample used for QC is not from job MC48821

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MSL4388-BS 99-87-6 p-Isopropyltoluene BSP REC 109 % 70-130MSL4388-BS 1634-04-4 Methyl Tert Butyl Ether BSP REC 96 % 70-130MSL4388-BS 108-10-1 4-Methyl-2-pentanone (MIBK) BSP REC 103 % 70-130MSL4388-BS 74-95-3 Methylene bromide BSP REC 100 % 70-130MSL4388-BS 75-09-2 Methylene chloride BSP REC 78 % 70-130MSL4388-BS 91-20-3 Naphthalene BSP REC 104 % 70-130MSL4388-BS 103-65-1 n-Propylbenzene BSP REC 111 % 70-130MSL4388-BS 100-42-5 Styrene BSP REC 105 % 70-130MSL4388-BS 630-20-6 1,1,1,2-Tetrachloroethane BSP REC 107 % 70-130MSL4388-BS 79-34-5 1,1,2,2-Tetrachloroethane BSP REC 99 % 70-130MSL4388-BS 127-18-4 Tetrachloroethene BSP REC 102 % 70-130MSL4388-BS 109-99-9 Tetrahydrofuran BSP REC 92 % 70-130MSL4388-BS 108-88-3 Toluene BSP REC 98 % 70-130MSL4388-BS 110-57-6 Trans-1,4-Dichloro-2-Butene BSP REC 104 % 70-130MSL4388-BS 87-61-6 1,2,3-Trichlorobenzene BSP REC 108 % 70-130MSL4388-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 107 % 70-130MSL4388-BS 71-55-6 1,1,1-Trichloroethane BSP REC 105 % 70-130MSL4388-BS 79-00-5 1,1,2-Trichloroethane BSP REC 101 % 70-130MSL4388-BS 79-01-6 Trichloroethene BSP REC 98 % 70-130MSL4388-BS 75-69-4 Trichlorofluoromethane BSP REC 105 % 70-130MSL4388-BS 96-18-4 1,2,3-Trichloropropane BSP REC 103 % 70-130MSL4388-BS 95-63-6 1,2,4-Trimethylbenzene BSP REC 120 a % 70-130MSL4388-BS 108-67-8 1,3,5-Trimethylbenzene BSP REC 118 % 70-130MSL4388-BS 75-01-4 Vinyl chloride BSP REC 128 % 70-130MSL4388-BS m,p-Xylene BSP REC 114 % 70-130MSL4388-BS 95-47-6 o-Xylene BSP REC 116 % 70-130MSL4388-BS 1868-53-7 Dibromofluoromethane BSP SURR 92 % 70-130MSL4388-BS 2037-26-5 Toluene-D8 BSP SURR 100 % 70-130MSL4388-BS 460-00-4 4-Bromofluorobenzene BSP SURR 100 % 70-130MSL4388-BSD 67-64-1 Acetone BSD REC 100 % 70-130MSL4388-BSD 67-64-1 Acetone BSD RPD 24 % 20MSL4388-BSD 107-13-1 Acrylonitrile BSD REC 97 % 70-130MSL4388-BSD 107-13-1 Acrylonitrile BSD RPD 18 % 20MSL4388-BSD 71-43-2 Benzene BSD REC 94 % 70-130MSL4388-BSD 71-43-2 Benzene BSD RPD 1 % 20MSL4388-BSD 108-86-1 Bromobenzene BSD REC 110 % 70-130MSL4388-BSD 108-86-1 Bromobenzene BSD RPD 1 % 20MSL4388-BSD 75-27-4 Bromodichloromethane BSD REC 99 % 70-130MSL4388-BSD 75-27-4 Bromodichloromethane BSD RPD 0 % 20MSL4388-BSD 75-25-2 Bromoform BSD REC 108 % 70-130MSL4388-BSD 75-25-2 Bromoform BSD RPD 1 % 20MSL4388-BSD 74-83-9 Bromomethane BSD REC 87 % 70-130MSL4388-BSD 74-83-9 Bromomethane BSD RPD 22 % 20MSL4388-BSD 78-93-3 2-Butanone (MEK) BSD REC 104 % 70-130MSL4388-BSD 78-93-3 2-Butanone (MEK) BSD RPD 16 % 20


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MSL4388-BSD 104-51-8 n-Butylbenzene BSD REC 113 % 70-130MSL4388-BSD 104-51-8 n-Butylbenzene BSD RPD 2 % 20MSL4388-BSD 135-98-8 sec-Butylbenzene BSD REC 112 % 70-130MSL4388-BSD 135-98-8 sec-Butylbenzene BSD RPD 2 % 20MSL4388-BSD 98-06-6 tert-Butylbenzene BSD REC 110 % 70-130MSL4388-BSD 98-06-6 tert-Butylbenzene BSD RPD 3 % 20MSL4388-BSD 75-15-0 Carbon disulfide BSD REC 99 % 70-130MSL4388-BSD 75-15-0 Carbon disulfide BSD RPD 15 % 20MSL4388-BSD 56-23-5 Carbon tetrachloride BSD REC 100 % 70-130MSL4388-BSD 56-23-5 Carbon tetrachloride BSD RPD 0 % 20MSL4388-BSD 108-90-7 Chlorobenzene BSD REC 104 % 70-130MSL4388-BSD 108-90-7 Chlorobenzene BSD RPD 0 % 20MSL4388-BSD 75-00-3 Chloroethane BSD REC 92 % 70-130MSL4388-BSD 75-00-3 Chloroethane BSD RPD 20 % 20MSL4388-BSD 67-66-3 Chloroform BSD REC 92 % 70-130MSL4388-BSD 67-66-3 Chloroform BSD RPD 3 % 20MSL4388-BSD 74-87-3 Chloromethane BSD REC 97 % 70-130MSL4388-BSD 74-87-3 Chloromethane BSD RPD 19 % 20MSL4388-BSD 95-49-8 o-Chlorotoluene BSD REC 108 % 70-130MSL4388-BSD 95-49-8 o-Chlorotoluene BSD RPD 1 % 20MSL4388-BSD 106-43-4 p-Chlorotoluene BSD REC 109 % 70-130MSL4388-BSD 106-43-4 p-Chlorotoluene BSD RPD 1 % 20MSL4388-BSD 96-12-8 1,2-Dibromo-3-chloropropane BSD REC 108 % 70-130MSL4388-BSD 96-12-8 1,2-Dibromo-3-chloropropane BSD RPD 3 % 20MSL4388-BSD 124-48-1 Dibromochloromethane BSD REC 106 % 70-130MSL4388-BSD 124-48-1 Dibromochloromethane BSD RPD 1 % 20MSL4388-BSD 106-93-4 1,2-Dibromoethane BSD REC 107 % 70-130MSL4388-BSD 106-93-4 1,2-Dibromoethane BSD RPD 2 % 20MSL4388-BSD 95-50-1 1,2-Dichlorobenzene BSD REC 106 % 70-130MSL4388-BSD 95-50-1 1,2-Dichlorobenzene BSD RPD 0 % 20MSL4388-BSD 541-73-1 1,3-Dichlorobenzene BSD REC 104 % 70-130MSL4388-BSD 541-73-1 1,3-Dichlorobenzene BSD RPD 0 % 20MSL4388-BSD 106-46-7 1,4-Dichlorobenzene BSD REC 102 % 70-130MSL4388-BSD 106-46-7 1,4-Dichlorobenzene BSD RPD 0 % 20MSL4388-BSD 75-71-8 Dichlorodifluoromethane BSD REC 104 % 70-130MSL4388-BSD 75-71-8 Dichlorodifluoromethane BSD RPD 23 % 20MSL4388-BSD 75-34-3 1,1-Dichloroethane BSD REC 90 % 70-130MSL4388-BSD 75-34-3 1,1-Dichloroethane BSD RPD 6 % 20MSL4388-BSD 107-06-2 1,2-Dichloroethane BSD REC 93 % 70-130MSL4388-BSD 107-06-2 1,2-Dichloroethane BSD RPD 1 % 20MSL4388-BSD 75-35-4 1,1-Dichloroethene BSD REC 96 % 70-130MSL4388-BSD 75-35-4 1,1-Dichloroethene BSD RPD 16 % 20MSL4388-BSD 156-59-2 cis-1,2-Dichloroethene BSD REC 98 % 70-130MSL4388-BSD 156-59-2 cis-1,2-Dichloroethene BSD RPD 6 % 20MSL4388-BSD 156-60-5 trans-1,2-Dichloroethene BSD REC 95 % 70-130


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MSL4388-BSD 156-60-5 trans-1,2-Dichloroethene BSD RPD 16 % 20MSL4388-BSD 78-87-5 1,2-Dichloropropane BSD REC 98 % 70-130MSL4388-BSD 78-87-5 1,2-Dichloropropane BSD RPD 0 % 20MSL4388-BSD 142-28-9 1,3-Dichloropropane BSD REC 108 % 70-130MSL4388-BSD 142-28-9 1,3-Dichloropropane BSD RPD 1 % 20MSL4388-BSD 594-20-7 2,2-Dichloropropane BSD REC 102 % 70-130MSL4388-BSD 594-20-7 2,2-Dichloropropane BSD RPD 6 % 20MSL4388-BSD 563-58-6 1,1-Dichloropropene BSD REC 103 % 70-130MSL4388-BSD 563-58-6 1,1-Dichloropropene BSD RPD 2 % 20MSL4388-BSD 10061-01-5 cis-1,3-Dichloropropene BSD REC 110 % 70-130MSL4388-BSD 10061-01-5 cis-1,3-Dichloropropene BSD RPD 1 % 20MSL4388-BSD 10061-02-6 trans-1,3-Dichloropropene BSD REC 108 % 70-130MSL4388-BSD 10061-02-6 trans-1,3-Dichloropropene BSD RPD 2 % 20MSL4388-BSD 100-41-4 Ethylbenzene BSD REC 108 % 70-130MSL4388-BSD 100-41-4 Ethylbenzene BSD RPD 0 % 20MSL4388-BSD 76-13-1 Freon 113 BSD REC 98 % 70-130MSL4388-BSD 76-13-1 Freon 113 BSD RPD 12 % 20MSL4388-BSD 87-68-3 Hexachlorobutadiene BSD REC 114 % 70-130MSL4388-BSD 87-68-3 Hexachlorobutadiene BSD RPD 3 % 20MSL4388-BSD 591-78-6 2-Hexanone BSD REC 114 % 70-130MSL4388-BSD 591-78-6 2-Hexanone BSD RPD 0 % 20MSL4388-BSD 98-82-8 Isopropylbenzene BSD REC 115 % 70-130MSL4388-BSD 98-82-8 Isopropylbenzene BSD RPD 1 % 20MSL4388-BSD 99-87-6 p-Isopropyltoluene BSD REC 106 % 70-130MSL4388-BSD 99-87-6 p-Isopropyltoluene BSD RPD 3 % 20MSL4388-BSD 1634-04-4 Methyl Tert Butyl Ether BSD REC 103 % 70-130MSL4388-BSD 1634-04-4 Methyl Tert Butyl Ether BSD RPD 8 % 20MSL4388-BSD 108-10-1 4-Methyl-2-pentanone (MIBK) BSD REC 104 % 70-130MSL4388-BSD 108-10-1 4-Methyl-2-pentanone (MIBK) BSD RPD 1 % 20MSL4388-BSD 74-95-3 Methylene bromide BSD REC 101 % 70-130MSL4388-BSD 74-95-3 Methylene bromide BSD RPD 1 % 20MSL4388-BSD 75-09-2 Methylene chloride BSD REC 91 % 70-130MSL4388-BSD 75-09-2 Methylene chloride BSD RPD 16 % 20MSL4388-BSD 91-20-3 Naphthalene BSD REC 103 % 70-130MSL4388-BSD 91-20-3 Naphthalene BSD RPD 1 % 20MSL4388-BSD 103-65-1 n-Propylbenzene BSD REC 112 % 70-130MSL4388-BSD 103-65-1 n-Propylbenzene BSD RPD 0 % 20MSL4388-BSD 100-42-5 Styrene BSD REC 107 % 70-130MSL4388-BSD 100-42-5 Styrene BSD RPD 2 % 20MSL4388-BSD 630-20-6 1,1,1,2-Tetrachloroethane BSD REC 107 % 70-130MSL4388-BSD 630-20-6 1,1,1,2-Tetrachloroethane BSD RPD 0 % 20MSL4388-BSD 79-34-5 1,1,2,2-Tetrachloroethane BSD REC 102 % 70-130MSL4388-BSD 79-34-5 1,1,2,2-Tetrachloroethane BSD RPD 3 % 20MSL4388-BSD 127-18-4 Tetrachloroethene BSD REC 100 % 70-130MSL4388-BSD 127-18-4 Tetrachloroethene BSD RPD 2 % 20


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MSL4388-BSD 109-99-9 Tetrahydrofuran BSD REC 99 % 70-130MSL4388-BSD 109-99-9 Tetrahydrofuran BSD RPD 7 % 20MSL4388-BSD 108-88-3 Toluene BSD REC 98 % 70-130MSL4388-BSD 108-88-3 Toluene BSD RPD 1 % 20MSL4388-BSD 110-57-6 Trans-1,4-Dichloro-2-Butene BSD REC 102 % 70-130MSL4388-BSD 110-57-6 Trans-1,4-Dichloro-2-Butene BSD RPD 2 % 20MSL4388-BSD 87-61-6 1,2,3-Trichlorobenzene BSD REC 108 % 70-130MSL4388-BSD 87-61-6 1,2,3-Trichlorobenzene BSD RPD 0 % 20MSL4388-BSD 120-82-1 1,2,4-Trichlorobenzene BSD REC 107 % 70-130MSL4388-BSD 120-82-1 1,2,4-Trichlorobenzene BSD RPD 0 % 20MSL4388-BSD 71-55-6 1,1,1-Trichloroethane BSD REC 94 % 70-130MSL4388-BSD 71-55-6 1,1,1-Trichloroethane BSD RPD 11 % 20MSL4388-BSD 79-00-5 1,1,2-Trichloroethane BSD REC 101 % 70-130MSL4388-BSD 79-00-5 1,1,2-Trichloroethane BSD RPD 0 % 20MSL4388-BSD 79-01-6 Trichloroethene BSD REC 96 % 70-130MSL4388-BSD 79-01-6 Trichloroethene BSD RPD 1 % 20MSL4388-BSD 75-69-4 Trichlorofluoromethane BSD REC 88 % 70-130MSL4388-BSD 75-69-4 Trichlorofluoromethane BSD RPD 18 % 20MSL4388-BSD 96-18-4 1,2,3-Trichloropropane BSD REC 103 % 70-130MSL4388-BSD 96-18-4 1,2,3-Trichloropropane BSD RPD 0 % 20MSL4388-BSD 95-63-6 1,2,4-Trimethylbenzene BSD REC 117 % 70-130MSL4388-BSD 95-63-6 1,2,4-Trimethylbenzene BSD RPD 2 % 20MSL4388-BSD 108-67-8 1,3,5-Trimethylbenzene BSD REC 116 % 70-130MSL4388-BSD 108-67-8 1,3,5-Trimethylbenzene BSD RPD 1 % 20MSL4388-BSD 75-01-4 Vinyl chloride BSD REC 107 % 70-130MSL4388-BSD 75-01-4 Vinyl chloride BSD RPD 18 % 20MSL4388-BSD m,p-Xylene BSD REC 114 % 70-130MSL4388-BSD m,p-Xylene BSD RPD 0 % 20MSL4388-BSD 95-47-6 o-Xylene BSD REC 116 % 70-130MSL4388-BSD 95-47-6 o-Xylene BSD RPD 1 % 20MSL4388-BSD 1868-53-7 Dibromofluoromethane BSD SURR 89 % 70-130MSL4388-BSD 2037-26-5 Toluene-D8 BSD SURR 100 % 70-130MSL4388-BSD 460-00-4 4-Bromofluorobenzene BSD SURR 101 % 70-130MSL4388-MB 1868-53-7 Dibromofluoromethane MB SURR 103 % 70-130MSL4388-MB 2037-26-5 Toluene-D8 MB SURR 101 % 70-130MSL4388-MB 460-00-4 4-Bromofluorobenzene MB SURR 110 % 70-130MC48821-7 1868-53-7 Dibromofluoromethane SAMP SURR 86 % 70-130MC48821-7 2037-26-5 Toluene-D8 SAMP SURR 108 % 70-130MC48821-7 460-00-4 4-Bromofluorobenzene SAMP SURR 102 % 70-130MC48821-8 1868-53-7 Dibromofluoromethane SAMP SURR 101 % 70-130MC48821-8 2037-26-5 Toluene-D8 SAMP SURR 109 % 70-130MC48821-8 460-00-4 4-Bromofluorobenzene SAMP SURR 97 % 70-130MC48821-26 1868-53-7 Dibromofluoromethane SAMP SURR 98 % 70-130MC48821-26 2037-26-5 Toluene-D8 SAMP SURR 99 % 70-130MC48821-26 460-00-4 4-Bromofluorobenzene SAMP SURR 104 % 70-130


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MSM2944 SW846 8260C

MSM2944-BS 67-64-1 Acetone BSP REC 81 % 70-130MSM2944-BS 107-13-1 Acrylonitrile BSP REC 108 % 70-130MSM2944-BS 71-43-2 Benzene BSP REC 113 % 70-130MSM2944-BS 108-86-1 Bromobenzene BSP REC 102 % 70-130MSM2944-BS 75-27-4 Bromodichloromethane BSP REC 110 % 70-130MSM2944-BS 75-25-2 Bromoform BSP REC 102 % 70-130MSM2944-BS 74-83-9 Bromomethane BSP REC 80 % 70-130MSM2944-BS 78-93-3 2-Butanone (MEK) BSP REC 87 % 70-130MSM2944-BS 104-51-8 n-Butylbenzene BSP REC 100 % 70-130MSM2944-BS 135-98-8 sec-Butylbenzene BSP REC 100 % 70-130MSM2944-BS 98-06-6 tert-Butylbenzene BSP REC 104 % 70-130MSM2944-BS 75-15-0 Carbon disulfide BSP REC 123 % 70-130MSM2944-BS 56-23-5 Carbon tetrachloride BSP REC 118 % 70-130MSM2944-BS 108-90-7 Chlorobenzene BSP REC 99 % 70-130MSM2944-BS 75-00-3 Chloroethane BSP REC 82 % 70-130MSM2944-BS 67-66-3 Chloroform BSP REC 116 % 70-130MSM2944-BS 74-87-3 Chloromethane BSP REC 107 % 70-130MSM2944-BS 95-49-8 o-Chlorotoluene BSP REC 103 % 70-130MSM2944-BS 106-43-4 p-Chlorotoluene BSP REC 101 % 70-130MSM2944-BS 96-12-8 1,2-Dibromo-3-chloropropane BSP REC 97 % 70-130MSM2944-BS 124-48-1 Dibromochloromethane BSP REC 100 % 70-130MSM2944-BS 106-93-4 1,2-Dibromoethane BSP REC 97 % 70-130MSM2944-BS 95-50-1 1,2-Dichlorobenzene BSP REC 97 % 70-130MSM2944-BS 541-73-1 1,3-Dichlorobenzene BSP REC 97 % 70-130MSM2944-BS 106-46-7 1,4-Dichlorobenzene BSP REC 96 % 70-130MSM2944-BS 75-71-8 Dichlorodifluoromethane BSP REC 78 % 70-130MSM2944-BS 75-34-3 1,1-Dichloroethane BSP REC 113 % 70-130MSM2944-BS 107-06-2 1,2-Dichloroethane BSP REC 117 % 70-130MSM2944-BS 75-35-4 1,1-Dichloroethene BSP REC 113 % 70-130MSM2944-BS 156-59-2 cis-1,2-Dichloroethene BSP REC 118 % 70-130MSM2944-BS 156-60-5 trans-1,2-Dichloroethene BSP REC 104 % 70-130MSM2944-BS 78-87-5 1,2-Dichloropropane BSP REC 110 % 70-130MSM2944-BS 142-28-9 1,3-Dichloropropane BSP REC 106 % 70-130MSM2944-BS 594-20-7 2,2-Dichloropropane BSP REC 120 % 70-130MSM2944-BS 563-58-6 1,1-Dichloropropene BSP REC 116 % 70-130MSM2944-BS 10061-01-5 cis-1,3-Dichloropropene BSP REC 105 % 70-130MSM2944-BS 10061-02-6 trans-1,3-Dichloropropene BSP REC 105 % 70-130MSM2944-BS 100-41-4 Ethylbenzene BSP REC 105 % 70-130MSM2944-BS 76-13-1 Freon 113 BSP REC 119 % 70-130MSM2944-BS 87-68-3 Hexachlorobutadiene BSP REC 99 % 70-130MSM2944-BS 591-78-6 2-Hexanone BSP REC 85 % 70-130MSM2944-BS 98-82-8 Isopropylbenzene BSP REC 99 % 70-130


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MSM2944-BS 99-87-6 p-Isopropyltoluene BSP REC 99 % 70-130MSM2944-BS 1634-04-4 Methyl Tert Butyl Ether BSP REC 108 % 70-130MSM2944-BS 108-10-1 4-Methyl-2-pentanone (MIBK) BSP REC 100 % 70-130MSM2944-BS 74-95-3 Methylene bromide BSP REC 109 % 70-130MSM2944-BS 75-09-2 Methylene chloride BSP REC 126 b % 70-130MSM2944-BS 91-20-3 Naphthalene BSP REC 88 % 70-130MSM2944-BS 103-65-1 n-Propylbenzene BSP REC 100 % 70-130MSM2944-BS 100-42-5 Styrene BSP REC 101 % 70-130MSM2944-BS 630-20-6 1,1,1,2-Tetrachloroethane BSP REC 106 % 70-130MSM2944-BS 79-34-5 1,1,2,2-Tetrachloroethane BSP REC 102 % 70-130MSM2944-BS 127-18-4 Tetrachloroethene BSP REC 98 % 70-130MSM2944-BS 109-99-9 Tetrahydrofuran BSP REC 97 % 70-130MSM2944-BS 108-88-3 Toluene BSP REC 113 % 70-130MSM2944-BS 110-57-6 Trans-1,4-Dichloro-2-Butene BSP REC 100 % 70-130MSM2944-BS 87-61-6 1,2,3-Trichlorobenzene BSP REC 95 % 70-130MSM2944-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 89 % 70-130MSM2944-BS 71-55-6 1,1,1-Trichloroethane BSP REC 117 % 70-130MSM2944-BS 79-00-5 1,1,2-Trichloroethane BSP REC 108 % 70-130MSM2944-BS 79-01-6 Trichloroethene BSP REC 107 % 70-130MSM2944-BS 75-69-4 Trichlorofluoromethane BSP REC 103 % 70-130MSM2944-BS 96-18-4 1,2,3-Trichloropropane BSP REC 102 % 70-130MSM2944-BS 95-63-6 1,2,4-Trimethylbenzene BSP REC 101 % 70-130MSM2944-BS 108-67-8 1,3,5-Trimethylbenzene BSP REC 106 % 70-130MSM2944-BS 75-01-4 Vinyl chloride BSP REC 87 % 70-130MSM2944-BS m,p-Xylene BSP REC 103 % 70-130MSM2944-BS 95-47-6 o-Xylene BSP REC 103 % 70-130MSM2944-BS 1868-53-7 Dibromofluoromethane BSP SURR 106 % 70-130MSM2944-BS 2037-26-5 Toluene-D8 BSP SURR 102 % 70-130MSM2944-BS 460-00-4 4-Bromofluorobenzene BSP SURR 96 % 70-130MSM2944-MB 1868-53-7 Dibromofluoromethane MB SURR 120 % 70-130MSM2944-MB 2037-26-5 Toluene-D8 MB SURR 105 % 70-130MSM2944-MB 460-00-4 4-Bromofluorobenzene MB SURR 96 % 70-130MC48821-1 1868-53-7 Dibromofluoromethane SAMP SURR 124 % 70-130MC48821-1 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-1 460-00-4 4-Bromofluorobenzene SAMP SURR 115 % 70-130MC48821-2 1868-53-7 Dibromofluoromethane SAMP SURR 117 % 70-130MC48821-2 2037-26-5 Toluene-D8 SAMP SURR 104 % 70-130MC48821-2 460-00-4 4-Bromofluorobenzene SAMP SURR 96 % 70-130MC48821-3 1868-53-7 Dibromofluoromethane SAMP SURR 127 % 70-130MC48821-3 2037-26-5 Toluene-D8 SAMP SURR 102 % 70-130MC48821-3 460-00-4 4-Bromofluorobenzene SAMP SURR 122 % 70-130MC48821-4 1868-53-7 Dibromofluoromethane SAMP SURR 121 % 70-130MC48821-4 2037-26-5 Toluene-D8 SAMP SURR 108 % 70-130MC48821-4 460-00-4 4-Bromofluorobenzene SAMP SURR 101 % 70-130MC48821-5 1868-53-7 Dibromofluoromethane SAMP SURR 127 % 70-130


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MC48821-5 2037-26-5 Toluene-D8 SAMP SURR 108 % 70-130MC48821-5 460-00-4 4-Bromofluorobenzene SAMP SURR 96 % 70-130MC48821-6 1868-53-7 Dibromofluoromethane SAMP SURR 125 % 70-130MC48821-6 2037-26-5 Toluene-D8 SAMP SURR 107 % 70-130MC48821-6 460-00-4 4-Bromofluorobenzene SAMP SURR 97 % 70-130MC48821-9 1868-53-7 Dibromofluoromethane SAMP SURR 129 % 70-130MC48821-9 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-9 460-00-4 4-Bromofluorobenzene SAMP SURR 127 % 70-130MC48821-10 1868-53-7 Dibromofluoromethane SAMP SURR 129 % 70-130MC48821-10 2037-26-5 Toluene-D8 SAMP SURR 107 % 70-130MC48821-10 460-00-4 4-Bromofluorobenzene SAMP SURR 95 % 70-130MC48821-11 1868-53-7 Dibromofluoromethane SAMP SURR 126 % 70-130MC48821-11 2037-26-5 Toluene-D8 SAMP SURR 106 % 70-130MC48821-11 460-00-4 4-Bromofluorobenzene SAMP SURR 106 % 70-130MC48821-12 1868-53-7 Dibromofluoromethane SAMP SURR 126 % 70-130MC48821-12 2037-26-5 Toluene-D8 SAMP SURR 107 % 70-130MC48821-12 460-00-4 4-Bromofluorobenzene SAMP SURR 96 % 70-130MC48821-13 1868-53-7 Dibromofluoromethane SAMP SURR 136 % 70-130MC48821-13 2037-26-5 Toluene-D8 SAMP SURR 108 % 70-130MC48821-13 460-00-4 4-Bromofluorobenzene SAMP SURR 106 % 70-130MC48821-14 1868-53-7 Dibromofluoromethane SAMP SURR 133 % 70-130MC48821-14 2037-26-5 Toluene-D8 SAMP SURR 102 % 70-130MC48821-14 460-00-4 4-Bromofluorobenzene SAMP SURR 123 % 70-130MC48821-15 1868-53-7 Dibromofluoromethane SAMP SURR 138 % 70-130MC48821-15 2037-26-5 Toluene-D8 SAMP SURR 104 % 70-130MC48821-15 460-00-4 4-Bromofluorobenzene SAMP SURR 120 % 70-130MC48821-16 1868-53-7 Dibromofluoromethane SAMP SURR 132 % 70-130MC48821-16 2037-26-5 Toluene-D8 SAMP SURR 105 % 70-130MC48821-16 460-00-4 4-Bromofluorobenzene SAMP SURR 123 % 70-130

MSM2946 SW846 8260C

MSM2946-BS 67-64-1 Acetone BSP REC 174 % 70-130MSM2946-BS 107-13-1 Acrylonitrile BSP REC 104 % 70-130MSM2946-BS 71-43-2 Benzene BSP REC 95 % 70-130MSM2946-BS 108-86-1 Bromobenzene BSP REC 88 % 70-130MSM2946-BS 75-27-4 Bromodichloromethane BSP REC 90 % 70-130MSM2946-BS 75-25-2 Bromoform BSP REC 88 % 70-130MSM2946-BS 74-83-9 Bromomethane BSP REC 73 % 70-130MSM2946-BS 78-93-3 2-Butanone (MEK) BSP REC 154 b % 70-130MSM2946-BS 104-51-8 n-Butylbenzene BSP REC 103 % 70-130MSM2946-BS 135-98-8 sec-Butylbenzene BSP REC 100 % 70-130MSM2946-BS 98-06-6 tert-Butylbenzene BSP REC 96 % 70-130MSM2946-BS 75-15-0 Carbon disulfide BSP REC 109 % 70-130MSM2946-BS 56-23-5 Carbon tetrachloride BSP REC 95 % 70-130


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MSM2946-BS 108-90-7 Chlorobenzene BSP REC 87 % 70-130MSM2946-BS 75-00-3 Chloroethane BSP REC 78 % 70-130MSM2946-BS 67-66-3 Chloroform BSP REC 92 % 70-130MSM2946-BS 74-87-3 Chloromethane BSP REC 112 % 70-130MSM2946-BS 95-49-8 o-Chlorotoluene BSP REC 95 % 70-130MSM2946-BS 106-43-4 p-Chlorotoluene BSP REC 94 % 70-130MSM2946-BS 96-12-8 1,2-Dibromo-3-chloropropane BSP REC 88 % 70-130MSM2946-BS 124-48-1 Dibromochloromethane BSP REC 88 % 70-130MSM2946-BS 106-93-4 1,2-Dibromoethane BSP REC 91 % 70-130MSM2946-BS 95-50-1 1,2-Dichlorobenzene BSP REC 87 % 70-130MSM2946-BS 541-73-1 1,3-Dichlorobenzene BSP REC 88 % 70-130MSM2946-BS 106-46-7 1,4-Dichlorobenzene BSP REC 83 % 70-130MSM2946-BS 75-71-8 Dichlorodifluoromethane BSP REC 103 % 70-130MSM2946-BS 75-34-3 1,1-Dichloroethane BSP REC 96 % 70-130MSM2946-BS 107-06-2 1,2-Dichloroethane BSP REC 92 % 70-130MSM2946-BS 75-35-4 1,1-Dichloroethene BSP REC 111 % 70-130MSM2946-BS 156-59-2 cis-1,2-Dichloroethene BSP REC 104 % 70-130MSM2946-BS 156-60-5 trans-1,2-Dichloroethene BSP REC 93 % 70-130MSM2946-BS 78-87-5 1,2-Dichloropropane BSP REC 94 % 70-130MSM2946-BS 142-28-9 1,3-Dichloropropane BSP REC 95 % 70-130MSM2946-BS 594-20-7 2,2-Dichloropropane BSP REC 101 % 70-130MSM2946-BS 563-58-6 1,1-Dichloropropene BSP REC 100 % 70-130MSM2946-BS 10061-01-5 cis-1,3-Dichloropropene BSP REC 96 % 70-130MSM2946-BS 10061-02-6 trans-1,3-Dichloropropene BSP REC 90 % 70-130MSM2946-BS 100-41-4 Ethylbenzene BSP REC 98 % 70-130MSM2946-BS 76-13-1 Freon 113 BSP REC 109 % 70-130MSM2946-BS 87-68-3 Hexachlorobutadiene BSP REC 92 % 70-130MSM2946-BS 591-78-6 2-Hexanone BSP REC 124 % 70-130MSM2946-BS 98-82-8 Isopropylbenzene BSP REC 99 % 70-130MSM2946-BS 99-87-6 p-Isopropyltoluene BSP REC 96 % 70-130MSM2946-BS 1634-04-4 Methyl Tert Butyl Ether BSP REC 109 % 70-130MSM2946-BS 108-10-1 4-Methyl-2-pentanone (MIBK) BSP REC 101 % 70-130MSM2946-BS 74-95-3 Methylene bromide BSP REC 89 % 70-130MSM2946-BS 75-09-2 Methylene chloride BSP REC 98 % 70-130MSM2946-BS 91-20-3 Naphthalene BSP REC 86 % 70-130MSM2946-BS 103-65-1 n-Propylbenzene BSP REC 93 % 70-130MSM2946-BS 100-42-5 Styrene BSP REC 101 % 70-130MSM2946-BS 630-20-6 1,1,1,2-Tetrachloroethane BSP REC 93 % 70-130MSM2946-BS 79-34-5 1,1,2,2-Tetrachloroethane BSP REC 87 % 70-130MSM2946-BS 127-18-4 Tetrachloroethene BSP REC 88 % 70-130MSM2946-BS 109-99-9 Tetrahydrofuran BSP REC 99 % 70-130MSM2946-BS 108-88-3 Toluene BSP REC 91 % 70-130MSM2946-BS 110-57-6 Trans-1,4-Dichloro-2-Butene BSP REC 95 % 70-130MSM2946-BS 87-61-6 1,2,3-Trichlorobenzene BSP REC 96 % 70-130MSM2946-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 95 % 70-130


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MSM2946-BS 71-55-6 1,1,1-Trichloroethane BSP REC 98 % 70-130MSM2946-BS 79-00-5 1,1,2-Trichloroethane BSP REC 91 % 70-130MSM2946-BS 79-01-6 Trichloroethene BSP REC 89 % 70-130MSM2946-BS 75-69-4 Trichlorofluoromethane BSP REC 93 % 70-130MSM2946-BS 96-18-4 1,2,3-Trichloropropane BSP REC 83 % 70-130MSM2946-BS 95-63-6 1,2,4-Trimethylbenzene BSP REC 98 % 70-130MSM2946-BS 108-67-8 1,3,5-Trimethylbenzene BSP REC 105 % 70-130MSM2946-BS 75-01-4 Vinyl chloride BSP REC 94 % 70-130MSM2946-BS m,p-Xylene BSP REC 101 % 70-130MSM2946-BS 95-47-6 o-Xylene BSP REC 105 % 70-130MSM2946-BS 1868-53-7 Dibromofluoromethane BSP SURR 98 % 70-130MSM2946-BS 2037-26-5 Toluene-D8 BSP SURR 102 % 70-130MSM2946-BS 460-00-4 4-Bromofluorobenzene BSP SURR 98 % 70-130MSM2946-MB 1868-53-7 Dibromofluoromethane MB SURR 110 % 70-130MSM2946-MB 2037-26-5 Toluene-D8 MB SURR 103 % 70-130MSM2946-MB 460-00-4 4-Bromofluorobenzene MB SURR 100 % 70-130MC48821-17 1868-53-7 Dibromofluoromethane SAMP SURR 120 % 70-130MC48821-17 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-17 460-00-4 4-Bromofluorobenzene SAMP SURR 128 % 70-130MC48821-18 1868-53-7 Dibromofluoromethane SAMP SURR 122 % 70-130MC48821-18 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-18 460-00-4 4-Bromofluorobenzene SAMP SURR 133 % 70-130MC48821-19 1868-53-7 Dibromofluoromethane SAMP SURR 129 % 70-130MC48821-19 2037-26-5 Toluene-D8 SAMP SURR 94 % 70-130MC48821-19 460-00-4 4-Bromofluorobenzene SAMP SURR 155 c % 70-130MC48821-20 1868-53-7 Dibromofluoromethane SAMP SURR 120 % 70-130MC48821-20 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-20 460-00-4 4-Bromofluorobenzene SAMP SURR 121 % 70-130MC48821-21 1868-53-7 Dibromofluoromethane SAMP SURR 123 % 70-130MC48821-21 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-21 460-00-4 4-Bromofluorobenzene SAMP SURR 121 % 70-130MC48821-26A 1868-53-7 Dibromofluoromethane SAMP SURR 114 % 70-130MC48821-26A 2037-26-5 Toluene-D8 SAMP SURR 103 % 70-130MC48821-26A 460-00-4 4-Bromofluorobenzene SAMP SURR 102 % 70-130

MSV1905 SW846 8260C

MSV1905-BS 67-64-1 Acetone BSP REC 155 % 70-130MSV1905-BS 107-13-1 Acrylonitrile BSP REC 116 % 70-130MSV1905-BS 71-43-2 Benzene BSP REC 101 % 70-130MSV1905-BS 108-86-1 Bromobenzene BSP REC 105 % 70-130MSV1905-BS 75-27-4 Bromodichloromethane BSP REC 97 % 70-130MSV1905-BS 75-25-2 Bromoform BSP REC 67 % 70-130MSV1905-BS 74-83-9 Bromomethane BSP REC 143 % 70-130MSV1905-BS 78-93-3 2-Butanone (MEK) BSP REC 139 % 70-130


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MSV1905-BS 104-51-8 n-Butylbenzene BSP REC 118 % 70-130MSV1905-BS 135-98-8 sec-Butylbenzene BSP REC 114 % 70-130MSV1905-BS 98-06-6 tert-Butylbenzene BSP REC 110 % 70-130MSV1905-BS 75-15-0 Carbon disulfide BSP REC 119 % 70-130MSV1905-BS 56-23-5 Carbon tetrachloride BSP REC 110 % 70-130MSV1905-BS 108-90-7 Chlorobenzene BSP REC 95 % 70-130MSV1905-BS 75-00-3 Chloroethane BSP REC 117 % 70-130MSV1905-BS 67-66-3 Chloroform BSP REC 114 % 70-130MSV1905-BS 74-87-3 Chloromethane BSP REC 169 b % 70-130MSV1905-BS 95-49-8 o-Chlorotoluene BSP REC 114 % 70-130MSV1905-BS 106-43-4 p-Chlorotoluene BSP REC 113 % 70-130MSV1905-BS 96-12-8 1,2-Dibromo-3-chloropropane BSP REC 81 % 70-130MSV1905-BS 124-48-1 Dibromochloromethane BSP REC 82 % 70-130MSV1905-BS 106-93-4 1,2-Dibromoethane BSP REC 94 % 70-130MSV1905-BS 95-50-1 1,2-Dichlorobenzene BSP REC 101 % 70-130MSV1905-BS 541-73-1 1,3-Dichlorobenzene BSP REC 100 % 70-130MSV1905-BS 106-46-7 1,4-Dichlorobenzene BSP REC 100 % 70-130MSV1905-BS 75-71-8 Dichlorodifluoromethane BSP REC 146 % 70-130MSV1905-BS 75-34-3 1,1-Dichloroethane BSP REC 112 % 70-130MSV1905-BS 107-06-2 1,2-Dichloroethane BSP REC 112 % 70-130MSV1905-BS 75-35-4 1,1-Dichloroethene BSP REC 117 % 70-130MSV1905-BS 156-59-2 cis-1,2-Dichloroethene BSP REC 113 % 70-130MSV1905-BS 156-60-5 trans-1,2-Dichloroethene BSP REC 104 % 70-130MSV1905-BS 78-87-5 1,2-Dichloropropane BSP REC 105 % 70-130MSV1905-BS 142-28-9 1,3-Dichloropropane BSP REC 106 % 70-130MSV1905-BS 594-20-7 2,2-Dichloropropane BSP REC 129 % 70-130MSV1905-BS 563-58-6 1,1-Dichloropropene BSP REC 113 % 70-130MSV1905-BS 10061-01-5 cis-1,3-Dichloropropene BSP REC 93 % 70-130MSV1905-BS 10061-02-6 trans-1,3-Dichloropropene BSP REC 92 % 70-130MSV1905-BS 100-41-4 Ethylbenzene BSP REC 104 % 70-130MSV1905-BS 76-13-1 Freon 113 BSP REC 136 % 70-130MSV1905-BS 87-68-3 Hexachlorobutadiene BSP REC 107 % 70-130MSV1905-BS 591-78-6 2-Hexanone BSP REC 140 % 70-130MSV1905-BS 98-82-8 Isopropylbenzene BSP REC 110 % 70-130MSV1905-BS 99-87-6 p-Isopropyltoluene BSP REC 114 % 70-130MSV1905-BS 1634-04-4 Methyl Tert Butyl Ether BSP REC 108 % 70-130MSV1905-BS 108-10-1 4-Methyl-2-pentanone (MIBK) BSP REC 106 % 70-130MSV1905-BS 74-95-3 Methylene bromide BSP REC 104 % 70-130MSV1905-BS 75-09-2 Methylene chloride BSP REC 111 % 70-130MSV1905-BS 91-20-3 Naphthalene BSP REC 90 % 70-130MSV1905-BS 103-65-1 n-Propylbenzene BSP REC 113 % 70-130MSV1905-BS 100-42-5 Styrene BSP REC 101 % 70-130MSV1905-BS 630-20-6 1,1,1,2-Tetrachloroethane BSP REC 95 % 70-130MSV1905-BS 79-34-5 1,1,2,2-Tetrachloroethane BSP REC 108 % 70-130MSV1905-BS 127-18-4 Tetrachloroethene BSP REC 92 % 70-130


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MSV1905-BS 109-99-9 Tetrahydrofuran BSP REC 102 % 70-130MSV1905-BS 108-88-3 Toluene BSP REC 105 % 70-130MSV1905-BS 110-57-6 Trans-1,4-Dichloro-2-Butene BSP REC 73 % 70-130MSV1905-BS 87-61-6 1,2,3-Trichlorobenzene BSP REC 106 % 70-130MSV1905-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 100 % 70-130MSV1905-BS 71-55-6 1,1,1-Trichloroethane BSP REC 122 % 70-130MSV1905-BS 79-00-5 1,1,2-Trichloroethane BSP REC 102 % 70-130MSV1905-BS 79-01-6 Trichloroethene BSP REC 95 % 70-130MSV1905-BS 75-69-4 Trichlorofluoromethane BSP REC 135 % 70-130MSV1905-BS 96-18-4 1,2,3-Trichloropropane BSP REC 113 % 70-130MSV1905-BS 95-63-6 1,2,4-Trimethylbenzene BSP REC 111 % 70-130MSV1905-BS 108-67-8 1,3,5-Trimethylbenzene BSP REC 116 % 70-130MSV1905-BS 75-01-4 Vinyl chloride BSP REC 134 % 70-130MSV1905-BS m,p-Xylene BSP REC 100 % 70-130MSV1905-BS 95-47-6 o-Xylene BSP REC 99 % 70-130MSV1905-BS 1868-53-7 Dibromofluoromethane BSP SURR 112 % 70-130MSV1905-BS 2037-26-5 Toluene-D8 BSP SURR 103 % 70-130MSV1905-BS 460-00-4 4-Bromofluorobenzene BSP SURR 104 % 70-130MSV1905-BSD 67-64-1 Acetone BSD REC 146 % 70-130MSV1905-BSD 67-64-1 Acetone BSD RPD 6 % 20MSV1905-BSD 107-13-1 Acrylonitrile BSD REC 112 % 70-130MSV1905-BSD 107-13-1 Acrylonitrile BSD RPD 4 % 20MSV1905-BSD 71-43-2 Benzene BSD REC 99 % 70-130MSV1905-BSD 71-43-2 Benzene BSD RPD 2 % 20MSV1905-BSD 108-86-1 Bromobenzene BSD REC 105 % 70-130MSV1905-BSD 108-86-1 Bromobenzene BSD RPD 0 % 20MSV1905-BSD 75-27-4 Bromodichloromethane BSD REC 95 % 70-130MSV1905-BSD 75-27-4 Bromodichloromethane BSD RPD 2 % 20MSV1905-BSD 75-25-2 Bromoform BSD REC 69 % 70-130MSV1905-BSD 75-25-2 Bromoform BSD RPD 4 % 20MSV1905-BSD 74-83-9 Bromomethane BSD REC 127 % 70-130MSV1905-BSD 74-83-9 Bromomethane BSD RPD 12 % 20MSV1905-BSD 78-93-3 2-Butanone (MEK) BSD REC 131 % 70-130MSV1905-BSD 78-93-3 2-Butanone (MEK) BSD RPD 5 % 20MSV1905-BSD 104-51-8 n-Butylbenzene BSD REC 117 % 70-130MSV1905-BSD 104-51-8 n-Butylbenzene BSD RPD 0 % 20MSV1905-BSD 135-98-8 sec-Butylbenzene BSD REC 111 % 70-130MSV1905-BSD 135-98-8 sec-Butylbenzene BSD RPD 2 % 20MSV1905-BSD 98-06-6 tert-Butylbenzene BSD REC 108 % 70-130MSV1905-BSD 98-06-6 tert-Butylbenzene BSD RPD 2 % 20MSV1905-BSD 75-15-0 Carbon disulfide BSD REC 113 % 70-130MSV1905-BSD 75-15-0 Carbon disulfide BSD RPD 5 % 20MSV1905-BSD 56-23-5 Carbon tetrachloride BSD REC 110 % 70-130MSV1905-BSD 56-23-5 Carbon tetrachloride BSD RPD 0 % 20MSV1905-BSD 108-90-7 Chlorobenzene BSD REC 96 % 70-130


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MSV1905-BSD 108-90-7 Chlorobenzene BSD RPD 1 % 20MSV1905-BSD 75-00-3 Chloroethane BSD REC 112 % 70-130MSV1905-BSD 75-00-3 Chloroethane BSD RPD 4 % 20MSV1905-BSD 67-66-3 Chloroform BSD REC 109 % 70-130MSV1905-BSD 67-66-3 Chloroform BSD RPD 4 % 20MSV1905-BSD 74-87-3 Chloromethane BSD REC 165 b % 70-130MSV1905-BSD 74-87-3 Chloromethane BSD RPD 3 % 20MSV1905-BSD 95-49-8 o-Chlorotoluene BSD REC 111 % 70-130MSV1905-BSD 95-49-8 o-Chlorotoluene BSD RPD 3 % 20MSV1905-BSD 106-43-4 p-Chlorotoluene BSD REC 112 % 70-130MSV1905-BSD 106-43-4 p-Chlorotoluene BSD RPD 1 % 20MSV1905-BSD 96-12-8 1,2-Dibromo-3-chloropropane BSD REC 85 % 70-130MSV1905-BSD 96-12-8 1,2-Dibromo-3-chloropropane BSD RPD 5 % 20MSV1905-BSD 124-48-1 Dibromochloromethane BSD REC 84 % 70-130MSV1905-BSD 124-48-1 Dibromochloromethane BSD RPD 2 % 20MSV1905-BSD 106-93-4 1,2-Dibromoethane BSD REC 95 % 70-130MSV1905-BSD 106-93-4 1,2-Dibromoethane BSD RPD 1 % 20MSV1905-BSD 95-50-1 1,2-Dichlorobenzene BSD REC 100 % 70-130MSV1905-BSD 95-50-1 1,2-Dichlorobenzene BSD RPD 2 % 20MSV1905-BSD 541-73-1 1,3-Dichlorobenzene BSD REC 100 % 70-130MSV1905-BSD 541-73-1 1,3-Dichlorobenzene BSD RPD 0 % 20MSV1905-BSD 106-46-7 1,4-Dichlorobenzene BSD REC 100 % 70-130MSV1905-BSD 106-46-7 1,4-Dichlorobenzene BSD RPD 0 % 20MSV1905-BSD 75-71-8 Dichlorodifluoromethane BSD REC 144 % 70-130MSV1905-BSD 75-71-8 Dichlorodifluoromethane BSD RPD 1 % 20MSV1905-BSD 75-34-3 1,1-Dichloroethane BSD REC 107 % 70-130MSV1905-BSD 75-34-3 1,1-Dichloroethane BSD RPD 5 % 20MSV1905-BSD 107-06-2 1,2-Dichloroethane BSD REC 113 % 70-130MSV1905-BSD 107-06-2 1,2-Dichloroethane BSD RPD 1 % 20MSV1905-BSD 75-35-4 1,1-Dichloroethene BSD REC 111 % 70-130MSV1905-BSD 75-35-4 1,1-Dichloroethene BSD RPD 6 % 20MSV1905-BSD 156-59-2 cis-1,2-Dichloroethene BSD REC 108 % 70-130MSV1905-BSD 156-59-2 cis-1,2-Dichloroethene BSD RPD 5 % 20MSV1905-BSD 156-60-5 trans-1,2-Dichloroethene BSD REC 100 % 70-130MSV1905-BSD 156-60-5 trans-1,2-Dichloroethene BSD RPD 4 % 20MSV1905-BSD 78-87-5 1,2-Dichloropropane BSD REC 104 % 70-130MSV1905-BSD 78-87-5 1,2-Dichloropropane BSD RPD 1 % 20MSV1905-BSD 142-28-9 1,3-Dichloropropane BSD REC 107 % 70-130MSV1905-BSD 142-28-9 1,3-Dichloropropane BSD RPD 1 % 20MSV1905-BSD 594-20-7 2,2-Dichloropropane BSD REC 124 % 70-130MSV1905-BSD 594-20-7 2,2-Dichloropropane BSD RPD 4 % 20MSV1905-BSD 563-58-6 1,1-Dichloropropene BSD REC 111 % 70-130MSV1905-BSD 563-58-6 1,1-Dichloropropene BSD RPD 2 % 20MSV1905-BSD 10061-01-5 cis-1,3-Dichloropropene BSD REC 93 % 70-130MSV1905-BSD 10061-01-5 cis-1,3-Dichloropropene BSD RPD 0 % 20


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MSV1905-BSD 10061-02-6 trans-1,3-Dichloropropene BSD REC 91 % 70-130MSV1905-BSD 10061-02-6 trans-1,3-Dichloropropene BSD RPD 1 % 20MSV1905-BSD 100-41-4 Ethylbenzene BSD REC 103 % 70-130MSV1905-BSD 100-41-4 Ethylbenzene BSD RPD 0 % 20MSV1905-BSD 76-13-1 Freon 113 BSD REC 132 % 70-130MSV1905-BSD 76-13-1 Freon 113 BSD RPD 3 % 20MSV1905-BSD 87-68-3 Hexachlorobutadiene BSD REC 110 % 70-130MSV1905-BSD 87-68-3 Hexachlorobutadiene BSD RPD 2 % 20MSV1905-BSD 591-78-6 2-Hexanone BSD REC 141 % 70-130MSV1905-BSD 591-78-6 2-Hexanone BSD RPD 1 % 20MSV1905-BSD 98-82-8 Isopropylbenzene BSD REC 109 % 70-130MSV1905-BSD 98-82-8 Isopropylbenzene BSD RPD 1 % 20MSV1905-BSD 99-87-6 p-Isopropyltoluene BSD REC 111 % 70-130MSV1905-BSD 99-87-6 p-Isopropyltoluene BSD RPD 3 % 20MSV1905-BSD 1634-04-4 Methyl Tert Butyl Ether BSD REC 106 % 70-130MSV1905-BSD 1634-04-4 Methyl Tert Butyl Ether BSD RPD 1 % 20MSV1905-BSD 108-10-1 4-Methyl-2-pentanone (MIBK) BSD REC 108 % 70-130MSV1905-BSD 108-10-1 4-Methyl-2-pentanone (MIBK) BSD RPD 1 % 20MSV1905-BSD 74-95-3 Methylene bromide BSD REC 105 % 70-130MSV1905-BSD 74-95-3 Methylene bromide BSD RPD 2 % 20MSV1905-BSD 75-09-2 Methylene chloride BSD REC 107 % 70-130MSV1905-BSD 75-09-2 Methylene chloride BSD RPD 4 % 20MSV1905-BSD 91-20-3 Naphthalene BSD REC 91 % 70-130MSV1905-BSD 91-20-3 Naphthalene BSD RPD 1 % 20MSV1905-BSD 103-65-1 n-Propylbenzene BSD REC 112 % 70-130MSV1905-BSD 103-65-1 n-Propylbenzene BSD RPD 1 % 20MSV1905-BSD 100-42-5 Styrene BSD REC 102 % 70-130MSV1905-BSD 100-42-5 Styrene BSD RPD 1 % 20MSV1905-BSD 630-20-6 1,1,1,2-Tetrachloroethane BSD REC 97 % 70-130MSV1905-BSD 630-20-6 1,1,1,2-Tetrachloroethane BSD RPD 2 % 20MSV1905-BSD 79-34-5 1,1,2,2-Tetrachloroethane BSD REC 107 % 70-130MSV1905-BSD 79-34-5 1,1,2,2-Tetrachloroethane BSD RPD 1 % 20MSV1905-BSD 127-18-4 Tetrachloroethene BSD REC 94 % 70-130MSV1905-BSD 127-18-4 Tetrachloroethene BSD RPD 2 % 20MSV1905-BSD 109-99-9 Tetrahydrofuran BSD REC 101 % 70-130MSV1905-BSD 109-99-9 Tetrahydrofuran BSD RPD 0 % 20MSV1905-BSD 108-88-3 Toluene BSD REC 102 % 70-130MSV1905-BSD 108-88-3 Toluene BSD RPD 3 % 20MSV1905-BSD 110-57-6 Trans-1,4-Dichloro-2-Butene BSD REC 75 % 70-130MSV1905-BSD 110-57-6 Trans-1,4-Dichloro-2-Butene BSD RPD 2 % 20MSV1905-BSD 87-61-6 1,2,3-Trichlorobenzene BSD REC 106 % 70-130MSV1905-BSD 87-61-6 1,2,3-Trichlorobenzene BSD RPD 1 % 25MSV1905-BSD 120-82-1 1,2,4-Trichlorobenzene BSD REC 101 % 70-130MSV1905-BSD 120-82-1 1,2,4-Trichlorobenzene BSD RPD 1 % 20MSV1905-BSD 71-55-6 1,1,1-Trichloroethane BSD REC 120 % 70-130


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MSV1905-BSD 71-55-6 1,1,1-Trichloroethane BSD RPD 2 % 20MSV1905-BSD 79-00-5 1,1,2-Trichloroethane BSD REC 101 % 70-130MSV1905-BSD 79-00-5 1,1,2-Trichloroethane BSD RPD 1 % 20MSV1905-BSD 79-01-6 Trichloroethene BSD REC 95 % 70-130MSV1905-BSD 79-01-6 Trichloroethene BSD RPD 0 % 20MSV1905-BSD 75-69-4 Trichlorofluoromethane BSD REC 131 % 70-130MSV1905-BSD 75-69-4 Trichlorofluoromethane BSD RPD 3 % 20MSV1905-BSD 96-18-4 1,2,3-Trichloropropane BSD REC 113 % 70-130MSV1905-BSD 96-18-4 1,2,3-Trichloropropane BSD RPD 0 % 20MSV1905-BSD 95-63-6 1,2,4-Trimethylbenzene BSD REC 109 % 70-130MSV1905-BSD 95-63-6 1,2,4-Trimethylbenzene BSD RPD 2 % 20MSV1905-BSD 108-67-8 1,3,5-Trimethylbenzene BSD REC 115 % 70-130MSV1905-BSD 108-67-8 1,3,5-Trimethylbenzene BSD RPD 1 % 20MSV1905-BSD 75-01-4 Vinyl chloride BSD REC 131 % 70-130MSV1905-BSD 75-01-4 Vinyl chloride BSD RPD 2 % 20MSV1905-BSD m,p-Xylene BSD REC 100 % 70-130MSV1905-BSD m,p-Xylene BSD RPD 0 % 20MSV1905-BSD 95-47-6 o-Xylene BSD REC 99 % 70-130MSV1905-BSD 95-47-6 o-Xylene BSD RPD 0 % 20MSV1905-BSD 1868-53-7 Dibromofluoromethane BSD SURR 109 % 70-130MSV1905-BSD 2037-26-5 Toluene-D8 BSD SURR 102 % 70-130MSV1905-BSD 460-00-4 4-Bromofluorobenzene BSD SURR 102 % 70-130MSV1905-MB 1868-53-7 Dibromofluoromethane MB SURR 110 % 70-130MSV1905-MB 2037-26-5 Toluene-D8 MB SURR 101 % 70-130MSV1905-MB 460-00-4 4-Bromofluorobenzene MB SURR 102 % 70-130MC48821-22 1868-53-7 Dibromofluoromethane SAMP SURR 120 % 70-130MC48821-22 2037-26-5 Toluene-D8 SAMP SURR 101 % 70-130MC48821-22 460-00-4 4-Bromofluorobenzene SAMP SURR 101 % 70-130MC48821-23 1868-53-7 Dibromofluoromethane SAMP SURR 117 % 70-130MC48821-23 2037-26-5 Toluene-D8 SAMP SURR 104 % 70-130MC48821-23 460-00-4 4-Bromofluorobenzene SAMP SURR 102 % 70-130MC48821-24 1868-53-7 Dibromofluoromethane SAMP SURR 119 % 70-130MC48821-24 2037-26-5 Toluene-D8 SAMP SURR 102 % 70-130MC48821-24 460-00-4 4-Bromofluorobenzene SAMP SURR 102 % 70-130MC48821-25 1868-53-7 Dibromofluoromethane SAMP SURR 115 % 70-130MC48821-25 2037-26-5 Toluene-D8 SAMP SURR 102 % 70-130MC48821-25 460-00-4 4-Bromofluorobenzene SAMP SURR 103 % 70-130MC48821-27 1868-53-7 Dibromofluoromethane SAMP SURR 116 % 70-130MC48821-27 2037-26-5 Toluene-D8 SAMP SURR 104 % 70-130MC48821-27 460-00-4 4-Bromofluorobenzene SAMP SURR 104 % 70-130

OP49183 SW846 8270D

OP49183-BS 95-57-8 2-Chlorophenol BSP REC 66 % 30-130OP49183-BS 59-50-7 4-Chloro-3-methyl phenol BSP REC 76 % 30-130


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OP49183-BS 120-83-2 2,4-Dichlorophenol BSP REC 76 % 30-130OP49183-BS 105-67-9 2,4-Dimethylphenol BSP REC 73 % 30-130OP49183-BS 51-28-5 2,4-Dinitrophenol BSP REC 56 % 30-130OP49183-BS 534-52-1 4,6-Dinitro-o-cresol BSP REC 77 % 30-130OP49183-BS 95-48-7 2-Methylphenol BSP REC 70 % 30-130OP49183-BS 106-44-5 4-Methylphenol BSP REC 71 % 30-130OP49183-BS 88-75-5 2-Nitrophenol BSP REC 67 % 30-130OP49183-BS 100-02-7 4-Nitrophenol BSP REC 92 % 30-130OP49183-BS 87-86-5 Pentachlorophenol BSP REC 71 % 30-130OP49183-BS 108-95-2 Phenol BSP REC 66 % 30-130OP49183-BS 95-95-4 2,4,5-Trichlorophenol BSP REC 90 % 30-130OP49183-BS 88-06-2 2,4,6-Trichlorophenol BSP REC 88 % 30-130OP49183-BS 83-32-9 Acenaphthene BSP REC 84 % 40-140OP49183-BS 208-96-8 Acenaphthylene BSP REC 78 % 40-140OP49183-BS 62-53-3 Aniline BSP REC 31 % 40-140OP49183-BS 120-12-7 Anthracene BSP REC 81 % 40-140OP49183-BS 56-55-3 Benzo(a)anthracene BSP REC 85 % 40-140OP49183-BS 50-32-8 Benzo(a)pyrene BSP REC 84 % 40-140OP49183-BS 205-99-2 Benzo(b)fluoranthene BSP REC 84 % 40-140OP49183-BS 191-24-2 Benzo(g,h,i)perylene BSP REC 86 % 40-140OP49183-BS 207-08-9 Benzo(k)fluoranthene BSP REC 84 % 40-140OP49183-BS 101-55-3 4-Bromophenyl phenyl ether BSP REC 96 % 40-140OP49183-BS 85-68-7 Butyl benzyl phthalate BSP REC 92 % 40-140OP49183-BS 91-58-7 2-Chloronaphthalene BSP REC 84 % 40-140OP49183-BS 106-47-8 4-Chloroaniline BSP REC 28 % 40-140OP49183-BS 86-74-8 Carbazole BSP REC 84 % 40-140OP49183-BS 218-01-9 Chrysene BSP REC 83 % 40-140OP49183-BS 111-91-1 bis(2-Chloroethoxy)methane BSP REC 68 % 40-140OP49183-BS 111-44-4 bis(2-Chloroethyl)ether BSP REC 66 % 40-140OP49183-BS 108-60-1 bis(2-Chloroisopropyl)ether BSP REC 71 % 40-140OP49183-BS 7005-72-3 4-Chlorophenyl phenyl ether BSP REC 101 % 40-140OP49183-BS 121-14-2 2,4-Dinitrotoluene BSP REC 97 % 40-140OP49183-BS 606-20-2 2,6-Dinitrotoluene BSP REC 90 % 40-140OP49183-BS 91-94-1 3,3'-Dichlorobenzidine BSP REC 34 % 40-140OP49183-BS 53-70-3 Dibenzo(a,h)anthracene BSP REC 84 % 40-140OP49183-BS 132-64-9 Dibenzofuran BSP REC 88 % 40-140OP49183-BS 84-74-2 Di-n-butyl phthalate BSP REC 93 % 40-140OP49183-BS 117-84-0 Di-n-octyl phthalate BSP REC 82 % 40-140OP49183-BS 84-66-2 Diethyl phthalate BSP REC 100 % 40-140OP49183-BS 131-11-3 Dimethyl phthalate BSP REC 99 % 40-140OP49183-BS 117-81-7 bis(2-Ethylhexyl)phthalate BSP REC 86 % 40-140OP49183-BS 206-44-0 Fluoranthene BSP REC 89 % 40-140OP49183-BS 86-73-7 Fluorene BSP REC 94 % 40-140OP49183-BS 118-74-1 Hexachlorobenzene BSP REC 88 % 40-140OP49183-BS 87-68-3 Hexachlorobutadiene BSP REC 68 % 40-140


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OP49183-BS 77-47-4 Hexachlorocyclopentadiene BSP REC 53 % 40-140OP49183-BS 67-72-1 Hexachloroethane BSP REC 60 % 40-140OP49183-BS 193-39-5 Indeno(1,2,3-cd)pyrene BSP REC 84 % 40-140OP49183-BS 78-59-1 Isophorone BSP REC 72 % 40-140OP49183-BS 91-57-6 2-Methylnaphthalene BSP REC 73 % 40-140OP49183-BS 88-74-4 2-Nitroaniline BSP REC 87 % 40-140OP49183-BS 99-09-2 3-Nitroaniline BSP REC 48 % 40-140OP49183-BS 100-01-6 4-Nitroaniline BSP REC 80 % 40-140OP49183-BS 91-20-3 Naphthalene BSP REC 84 % 40-140OP49183-BS 98-95-3 Nitrobenzene BSP REC 65 % 40-140OP49183-BS 621-64-7 N-Nitroso-di-n-propylamine BSP REC 79 % 40-140OP49183-BS 86-30-6 N-Nitrosodiphenylamine BSP REC 81 % 40-140OP49183-BS 82-68-8 Pentachloronitrobenzene BSP REC 91 % 40-140OP49183-BS 85-01-8 Phenanthrene BSP REC 86 % 40-140OP49183-BS 129-00-0 Pyrene BSP REC 87 % 40-140OP49183-BS 110-86-1 Pyridine BSP REC 40 % 40-140OP49183-BS 95-94-3 1,2,4,5-Tetrachlorobenzene BSP REC 78 % 40-140OP49183-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 72 % 40-140OP49183-BS 367-12-4 2-Fluorophenol BSP SURR 56 % 30-130OP49183-BS 4165-62-2 Phenol-d5 BSP SURR 62 % 30-130OP49183-BS 118-79-6 2,4,6-Tribromophenol BSP SURR 76 % 30-130OP49183-BS 4165-60-0 Nitrobenzene-d5 BSP SURR 57 % 30-130OP49183-BS 321-60-8 2-Fluorobiphenyl BSP SURR 74 % 30-130OP49183-BS 1718-51-0 Terphenyl-d14 BSP SURR 78 % 30-130OP49183-BSD 95-57-8 2-Chlorophenol BSD REC 74 % 30-130OP49183-BSD 95-57-8 2-Chlorophenol BSD RPD 8 % 30OP49183-BSD 59-50-7 4-Chloro-3-methyl phenol BSD REC 76 % 30-130OP49183-BSD 59-50-7 4-Chloro-3-methyl phenol BSD RPD 3 % 30OP49183-BSD 120-83-2 2,4-Dichlorophenol BSD REC 78 % 30-130OP49183-BSD 120-83-2 2,4-Dichlorophenol BSD RPD 0 % 30OP49183-BSD 105-67-9 2,4-Dimethylphenol BSD REC 75 % 30-130OP49183-BSD 105-67-9 2,4-Dimethylphenol BSD RPD 0 % 30OP49183-BSD 51-28-5 2,4-Dinitrophenol BSD REC 23 % 30-130OP49183-BSD 51-28-5 2,4-Dinitrophenol BSD RPD 86 d % 30OP49183-BSD 534-52-1 4,6-Dinitro-o-cresol BSD REC 30 % 30-130OP49183-BSD 534-52-1 4,6-Dinitro-o-cresol BSD RPD 89 d % 30OP49183-BSD 95-48-7 2-Methylphenol BSD REC 77 % 30-130OP49183-BSD 95-48-7 2-Methylphenol BSD RPD 7 % 30OP49183-BSD 106-44-5 4-Methylphenol BSD REC 75 % 30-130OP49183-BSD 106-44-5 4-Methylphenol BSD RPD 3 % 30OP49183-BSD 88-75-5 2-Nitrophenol BSD REC 72 % 30-130OP49183-BSD 88-75-5 2-Nitrophenol BSD RPD 4 % 30OP49183-BSD 100-02-7 4-Nitrophenol BSD REC 78 % 30-130OP49183-BSD 100-02-7 4-Nitrophenol BSD RPD 19 % 30OP49183-BSD 87-86-5 Pentachlorophenol BSD REC 69 % 30-130


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OP49183-BSD 87-86-5 Pentachlorophenol BSD RPD 6 % 30OP49183-BSD 108-95-2 Phenol BSD REC 71 % 30-130OP49183-BSD 108-95-2 Phenol BSD RPD 5 % 30OP49183-BSD 95-95-4 2,4,5-Trichlorophenol BSD REC 89 % 30-130OP49183-BSD 95-95-4 2,4,5-Trichlorophenol BSD RPD 4 % 30OP49183-BSD 88-06-2 2,4,6-Trichlorophenol BSD REC 87 % 30-130OP49183-BSD 88-06-2 2,4,6-Trichlorophenol BSD RPD 3 % 30OP49183-BSD 83-32-9 Acenaphthene BSD REC 81 % 40-140OP49183-BSD 83-32-9 Acenaphthene BSD RPD 7 % 30OP49183-BSD 208-96-8 Acenaphthylene BSD REC 76 % 40-140OP49183-BSD 208-96-8 Acenaphthylene BSD RPD 4 % 30OP49183-BSD 62-53-3 Aniline BSD REC 29 % 40-140OP49183-BSD 62-53-3 Aniline BSD RPD 10 % 30OP49183-BSD 120-12-7 Anthracene BSD REC 79 % 40-140OP49183-BSD 120-12-7 Anthracene BSD RPD 6 % 30OP49183-BSD 56-55-3 Benzo(a)anthracene BSD REC 84 % 40-140OP49183-BSD 56-55-3 Benzo(a)anthracene BSD RPD 4 % 30OP49183-BSD 50-32-8 Benzo(a)pyrene BSD REC 81 % 40-140OP49183-BSD 50-32-8 Benzo(a)pyrene BSD RPD 6 % 30OP49183-BSD 205-99-2 Benzo(b)fluoranthene BSD REC 78 % 40-140OP49183-BSD 205-99-2 Benzo(b)fluoranthene BSD RPD 10 % 30OP49183-BSD 191-24-2 Benzo(g,h,i)perylene BSD REC 78 % 40-140OP49183-BSD 191-24-2 Benzo(g,h,i)perylene BSD RPD 12 % 30OP49183-BSD 207-08-9 Benzo(k)fluoranthene BSD REC 81 % 40-140OP49183-BSD 207-08-9 Benzo(k)fluoranthene BSD RPD 6 % 30OP49183-BSD 101-55-3 4-Bromophenyl phenyl ether BSD REC 93 % 40-140OP49183-BSD 101-55-3 4-Bromophenyl phenyl ether BSD RPD 6 % 30OP49183-BSD 85-68-7 Butyl benzyl phthalate BSD REC 93 % 40-140OP49183-BSD 85-68-7 Butyl benzyl phthalate BSD RPD 2 % 30OP49183-BSD 91-58-7 2-Chloronaphthalene BSD REC 83 % 40-140OP49183-BSD 91-58-7 2-Chloronaphthalene BSD RPD 4 % 30OP49183-BSD 106-47-8 4-Chloroaniline BSD REC 25 % 40-140OP49183-BSD 106-47-8 4-Chloroaniline BSD RPD 17 % 30OP49183-BSD 86-74-8 Carbazole BSD REC 81 % 40-140OP49183-BSD 86-74-8 Carbazole BSD RPD 6 % 30OP49183-BSD 218-01-9 Chrysene BSD REC 80 % 40-140OP49183-BSD 218-01-9 Chrysene BSD RPD 6 % 30OP49183-BSD 111-91-1 bis(2-Chloroethoxy)methane BSD REC 71 % 40-140OP49183-BSD 111-91-1 bis(2-Chloroethoxy)methane BSD RPD 2 % 30OP49183-BSD 111-44-4 bis(2-Chloroethyl)ether BSD REC 75 % 40-140OP49183-BSD 111-44-4 bis(2-Chloroethyl)ether BSD RPD 9 % 30OP49183-BSD 108-60-1 bis(2-Chloroisopropyl)ether BSD REC 81 % 40-140OP49183-BSD 108-60-1 bis(2-Chloroisopropyl)ether BSD RPD 11 % 30OP49183-BSD 7005-72-3 4-Chlorophenyl phenyl ether BSD REC 96 % 40-140OP49183-BSD 7005-72-3 4-Chlorophenyl phenyl ether BSD RPD 7 % 30


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OP49183-BSD 121-14-2 2,4-Dinitrotoluene BSD REC 92 % 40-140OP49183-BSD 121-14-2 2,4-Dinitrotoluene BSD RPD 7 % 30OP49183-BSD 606-20-2 2,6-Dinitrotoluene BSD REC 87 % 40-140OP49183-BSD 606-20-2 2,6-Dinitrotoluene BSD RPD 7 % 30OP49183-BSD 91-94-1 3,3'-Dichlorobenzidine BSD REC 55 % 40-140OP49183-BSD 91-94-1 3,3'-Dichlorobenzidine BSD RPD 44 d % 30OP49183-BSD 53-70-3 Dibenzo(a,h)anthracene BSD REC 79 % 40-140OP49183-BSD 53-70-3 Dibenzo(a,h)anthracene BSD RPD 8 % 30OP49183-BSD 132-64-9 Dibenzofuran BSD REC 83 % 40-140OP49183-BSD 132-64-9 Dibenzofuran BSD RPD 9 % 30OP49183-BSD 84-74-2 Di-n-butyl phthalate BSD REC 91 % 40-140OP49183-BSD 84-74-2 Di-n-butyl phthalate BSD RPD 4 % 30OP49183-BSD 117-84-0 Di-n-octyl phthalate BSD REC 81 % 40-140OP49183-BSD 117-84-0 Di-n-octyl phthalate BSD RPD 4 % 30OP49183-BSD 84-66-2 Diethyl phthalate BSD REC 98 % 40-140OP49183-BSD 84-66-2 Diethyl phthalate BSD RPD 5 % 30OP49183-BSD 131-11-3 Dimethyl phthalate BSD REC 96 % 40-140OP49183-BSD 131-11-3 Dimethyl phthalate BSD RPD 5 % 30OP49183-BSD 117-81-7 bis(2-Ethylhexyl)phthalate BSD REC 89 % 40-140OP49183-BSD 117-81-7 bis(2-Ethylhexyl)phthalate BSD RPD 0 % 30OP49183-BSD 206-44-0 Fluoranthene BSD REC 84 % 40-140OP49183-BSD 206-44-0 Fluoranthene BSD RPD 8 % 30OP49183-BSD 86-73-7 Fluorene BSD REC 89 % 40-140OP49183-BSD 86-73-7 Fluorene BSD RPD 8 % 30OP49183-BSD 118-74-1 Hexachlorobenzene BSD REC 86 % 40-140OP49183-BSD 118-74-1 Hexachlorobenzene BSD RPD 6 % 30OP49183-BSD 87-68-3 Hexachlorobutadiene BSD REC 70 % 40-140OP49183-BSD 87-68-3 Hexachlorobutadiene BSD RPD 1 % 30OP49183-BSD 77-47-4 Hexachlorocyclopentadiene BSD REC 7 e % 40-140OP49183-BSD 77-47-4 Hexachlorocyclopentadiene BSD RPD 153 e % 30OP49183-BSD 67-72-1 Hexachloroethane BSD REC 57 % 40-140OP49183-BSD 67-72-1 Hexachloroethane BSD RPD 8 % 30OP49183-BSD 193-39-5 Indeno(1,2,3-cd)pyrene BSD REC 79 % 40-140OP49183-BSD 193-39-5 Indeno(1,2,3-cd)pyrene BSD RPD 9 % 30OP49183-BSD 78-59-1 Isophorone BSD REC 76 % 40-140OP49183-BSD 78-59-1 Isophorone BSD RPD 2 % 30OP49183-BSD 91-57-6 2-Methylnaphthalene BSD REC 75 % 40-140OP49183-BSD 91-57-6 2-Methylnaphthalene BSD RPD 0 % 30OP49183-BSD 88-74-4 2-Nitroaniline BSD REC 86 % 40-140OP49183-BSD 88-74-4 2-Nitroaniline BSD RPD 3 % 30OP49183-BSD 99-09-2 3-Nitroaniline BSD REC 46 % 40-140OP49183-BSD 99-09-2 3-Nitroaniline BSD RPD 8 % 30OP49183-BSD 100-01-6 4-Nitroaniline BSD REC 69 % 40-140OP49183-BSD 100-01-6 4-Nitroaniline BSD RPD 18 % 30OP49183-BSD 91-20-3 Naphthalene BSD REC 98 % 40-140


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OP49183-BSD 91-20-3 Naphthalene BSD RPD 13 % 30OP49183-BSD 98-95-3 Nitrobenzene BSD REC 70 % 40-140OP49183-BSD 98-95-3 Nitrobenzene BSD RPD 5 % 30OP49183-BSD 621-64-7 N-Nitroso-di-n-propylamine BSD REC 81 % 40-140OP49183-BSD 621-64-7 N-Nitroso-di-n-propylamine BSD RPD 1 % 30OP49183-BSD 86-30-6 N-Nitrosodiphenylamine BSD REC 81 % 40-140OP49183-BSD 86-30-6 N-Nitrosodiphenylamine BSD RPD 4 % 30OP49183-BSD 82-68-8 Pentachloronitrobenzene BSD REC 86 % 40-140OP49183-BSD 82-68-8 Pentachloronitrobenzene BSD RPD 8 % 30OP49183-BSD 85-01-8 Phenanthrene BSD REC 83 % 40-140OP49183-BSD 85-01-8 Phenanthrene BSD RPD 6 % 30OP49183-BSD 129-00-0 Pyrene BSD REC 85 % 40-140OP49183-BSD 129-00-0 Pyrene BSD RPD 5 % 30OP49183-BSD 110-86-1 Pyridine BSD REC 48 % 40-140OP49183-BSD 110-86-1 Pyridine BSD RPD 14 % 30OP49183-BSD 95-94-3 1,2,4,5-Tetrachlorobenzene BSD REC 77 % 40-140OP49183-BSD 95-94-3 1,2,4,5-Tetrachlorobenzene BSD RPD 4 % 30OP49183-BSD 120-82-1 1,2,4-Trichlorobenzene BSD REC 76 % 40-140OP49183-BSD 120-82-1 1,2,4-Trichlorobenzene BSD RPD 3 % 30OP49183-BSD 367-12-4 2-Fluorophenol BSD SURR 64 % 30-130OP49183-BSD 4165-62-2 Phenol-d5 BSD SURR 68 % 30-130OP49183-BSD 118-79-6 2,4,6-Tribromophenol BSD SURR 74 % 30-130OP49183-BSD 4165-60-0 Nitrobenzene-d5 BSD SURR 62 % 30-130OP49183-BSD 321-60-8 2-Fluorobiphenyl BSD SURR 73 % 30-130OP49183-BSD 1718-51-0 Terphenyl-d14 BSD SURR 76 % 30-130OP49183-MB 367-12-4 2-Fluorophenol MB SURR 66 % 30-130OP49183-MB 4165-62-2 Phenol-d5 MB SURR 69 % 30-130OP49183-MB 118-79-6 2,4,6-Tribromophenol MB SURR 71 % 30-130OP49183-MB 4165-60-0 Nitrobenzene-d5 MB SURR 62 % 30-130OP49183-MB 321-60-8 2-Fluorobiphenyl MB SURR 75 % 30-130OP49183-MB 1718-51-0 Terphenyl-d14 MB SURR 83 % 30-130MC48821-1 367-12-4 2-Fluorophenol SAMP SURR 72 % 30-130MC48821-1 4165-62-2 Phenol-d5 SAMP SURR 73 % 30-130MC48821-1 118-79-6 2,4,6-Tribromophenol SAMP SURR 86 % 30-130MC48821-1 4165-60-0 Nitrobenzene-d5 SAMP SURR 72 % 30-130MC48821-1 321-60-8 2-Fluorobiphenyl SAMP SURR 88 % 30-130MC48821-1 1718-51-0 Terphenyl-d14 SAMP SURR 100 % 30-130

OP49189 SW846 8270D

OP49189-BS 95-57-8 2-Chlorophenol BSP REC 87 % 30-130OP49189-BS 59-50-7 4-Chloro-3-methyl phenol BSP REC 90 % 30-130OP49189-BS 120-83-2 2,4-Dichlorophenol BSP REC 104 % 30-130OP49189-BS 105-67-9 2,4-Dimethylphenol BSP REC 54 % 30-130OP49189-BS 51-28-5 2,4-Dinitrophenol BSP REC 106 % 30-130


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OP49189-BS 534-52-1 4,6-Dinitro-o-cresol BSP REC 116 % 30-130OP49189-BS 95-48-7 2-Methylphenol BSP REC 67 % 30-130OP49189-BS 106-44-5 4-Methylphenol BSP REC 63 % 30-130OP49189-BS 88-75-5 2-Nitrophenol BSP REC 107 % 30-130OP49189-BS 100-02-7 4-Nitrophenol BSP REC 34 % 30-130OP49189-BS 87-86-5 Pentachlorophenol BSP REC 90 % 30-130OP49189-BS 108-95-2 Phenol BSP REC 33 % 30-130OP49189-BS 95-95-4 2,4,5-Trichlorophenol BSP REC 118 % 30-130OP49189-BS 88-06-2 2,4,6-Trichlorophenol BSP REC 115 % 30-130OP49189-BS 62-53-3 Aniline BSP REC 59 % 40-140OP49189-BS 101-55-3 4-Bromophenyl phenyl ether BSP REC 133 f % 40-140OP49189-BS 85-68-7 Butyl benzyl phthalate BSP REC 118 % 40-140OP49189-BS 91-58-7 2-Chloronaphthalene BSP REC 120 % 40-140OP49189-BS 106-47-8 4-Chloroaniline BSP REC 94 % 40-140OP49189-BS 86-74-8 Carbazole BSP REC 112 % 40-140OP49189-BS 111-91-1 bis(2-Chloroethoxy)methane BSP REC 93 % 40-140OP49189-BS 111-44-4 bis(2-Chloroethyl)ether BSP REC 94 % 40-140OP49189-BS 108-60-1 bis(2-Chloroisopropyl)ether BSP REC 89 % 40-140OP49189-BS 7005-72-3 4-Chlorophenyl phenyl ether BSP REC 142 f % 40-140OP49189-BS 121-14-2 2,4-Dinitrotoluene BSP REC 130 f % 40-140OP49189-BS 606-20-2 2,6-Dinitrotoluene BSP REC 127 f % 40-140OP49189-BS 91-94-1 3,3'-Dichlorobenzidine BSP REC 80 % 40-140OP49189-BS 132-64-9 Dibenzofuran BSP REC 118 % 40-140OP49189-BS 84-74-2 Di-n-butyl phthalate BSP REC 123 f % 40-140OP49189-BS 117-84-0 Di-n-octyl phthalate BSP REC 98 % 40-140OP49189-BS 84-66-2 Diethyl phthalate BSP REC 131 f % 40-140OP49189-BS 131-11-3 Dimethyl phthalate BSP REC 131 % 40-140OP49189-BS 117-81-7 bis(2-Ethylhexyl)phthalate BSP REC 108 % 40-140OP49189-BS 118-74-1 Hexachlorobenzene BSP REC 124 % 40-140OP49189-BS 87-68-3 Hexachlorobutadiene BSP REC 116 f % 40-140OP49189-BS 77-47-4 Hexachlorocyclopentadiene BSP REC 61 % 40-140OP49189-BS 67-72-1 Hexachloroethane BSP REC 101 f % 40-140OP49189-BS 78-59-1 Isophorone BSP REC 100 % 40-140OP49189-BS 91-57-6 2-Methylnaphthalene BSP REC 112 % 40-140OP49189-BS 88-74-4 2-Nitroaniline BSP REC 118 % 40-140OP49189-BS 99-09-2 3-Nitroaniline BSP REC 107 % 40-140OP49189-BS 100-01-6 4-Nitroaniline BSP REC 109 % 40-140OP49189-BS 98-95-3 Nitrobenzene BSP REC 95 % 40-140OP49189-BS 621-64-7 N-Nitroso-di-n-propylamine BSP REC 104 % 40-140OP49189-BS 86-30-6 N-Nitrosodiphenylamine BSP REC 109 % 40-140OP49189-BS 82-68-8 Pentachloronitrobenzene BSP REC 113 % 40-140OP49189-BS 110-86-1 Pyridine BSP REC 44 % 40-140OP49189-BS 95-94-3 1,2,4,5-Tetrachlorobenzene BSP REC 117 % 40-140OP49189-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 124 f % 40-140OP49189-BS 367-12-4 2-Fluorophenol BSP SURR 42 % 15-110


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OP49189-BS 4165-62-2 Phenol-d5 BSP SURR 26 % 15-110OP49189-BS 118-79-6 2,4,6-Tribromophenol BSP SURR 106 % 15-110OP49189-BS 4165-60-0 Nitrobenzene-d5 BSP SURR 85 % 30-130OP49189-BS 321-60-8 2-Fluorobiphenyl BSP SURR 94 % 30-130OP49189-BS 1718-51-0 Terphenyl-d14 BSP SURR 102 % 30-130OP49189-BSD 95-57-8 2-Chlorophenol BSD REC 90 % 30-130OP49189-BSD 95-57-8 2-Chlorophenol BSD RPD 3 % 20OP49189-BSD 59-50-7 4-Chloro-3-methyl phenol BSD REC 94 % 30-130OP49189-BSD 59-50-7 4-Chloro-3-methyl phenol BSD RPD 4 % 20OP49189-BSD 120-83-2 2,4-Dichlorophenol BSD REC 98 % 30-130OP49189-BSD 120-83-2 2,4-Dichlorophenol BSD RPD 6 % 20OP49189-BSD 105-67-9 2,4-Dimethylphenol BSD REC 69 % 30-130OP49189-BSD 105-67-9 2,4-Dimethylphenol BSD RPD 25 f % 20OP49189-BSD 51-28-5 2,4-Dinitrophenol BSD REC 111 % 30-130OP49189-BSD 51-28-5 2,4-Dinitrophenol BSD RPD 5 % 20OP49189-BSD 534-52-1 4,6-Dinitro-o-cresol BSD REC 124 % 30-130OP49189-BSD 534-52-1 4,6-Dinitro-o-cresol BSD RPD 6 % 20OP49189-BSD 95-48-7 2-Methylphenol BSD REC 79 % 30-130OP49189-BSD 95-48-7 2-Methylphenol BSD RPD 17 % 20OP49189-BSD 106-44-5 4-Methylphenol BSD REC 74 % 30-130OP49189-BSD 106-44-5 4-Methylphenol BSD RPD 17 % 20OP49189-BSD 88-75-5 2-Nitrophenol BSD REC 99 % 30-130OP49189-BSD 88-75-5 2-Nitrophenol BSD RPD 8 % 20OP49189-BSD 100-02-7 4-Nitrophenol BSD REC 47 % 30-130OP49189-BSD 100-02-7 4-Nitrophenol BSD RPD 32 f % 20OP49189-BSD 87-86-5 Pentachlorophenol BSD REC 92 % 30-130OP49189-BSD 87-86-5 Pentachlorophenol BSD RPD 3 % 20OP49189-BSD 108-95-2 Phenol BSD REC 42 % 30-130OP49189-BSD 108-95-2 Phenol BSD RPD 24 f % 20OP49189-BSD 95-95-4 2,4,5-Trichlorophenol BSD REC 116 % 30-130OP49189-BSD 95-95-4 2,4,5-Trichlorophenol BSD RPD 1 % 20OP49189-BSD 88-06-2 2,4,6-Trichlorophenol BSD REC 112 % 30-130OP49189-BSD 88-06-2 2,4,6-Trichlorophenol BSD RPD 3 % 20OP49189-BSD 62-53-3 Aniline BSD REC 44 % 40-140OP49189-BSD 62-53-3 Aniline BSD RPD 29 f % 20OP49189-BSD 101-55-3 4-Bromophenyl phenyl ether BSD REC 137 f % 40-140OP49189-BSD 101-55-3 4-Bromophenyl phenyl ether BSD RPD 3 % 20OP49189-BSD 85-68-7 Butyl benzyl phthalate BSD REC 120 % 40-140OP49189-BSD 85-68-7 Butyl benzyl phthalate BSD RPD 2 % 20OP49189-BSD 91-58-7 2-Chloronaphthalene BSD REC 114 % 40-140OP49189-BSD 91-58-7 2-Chloronaphthalene BSD RPD 5 % 20OP49189-BSD 106-47-8 4-Chloroaniline BSD REC 84 % 40-140OP49189-BSD 106-47-8 4-Chloroaniline BSD RPD 12 % 20OP49189-BSD 86-74-8 Carbazole BSD REC 117 % 40-140OP49189-BSD 86-74-8 Carbazole BSD RPD 4 % 20


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OP49189-BSD 111-91-1 bis(2-Chloroethoxy)methane BSD REC 87 % 40-140OP49189-BSD 111-91-1 bis(2-Chloroethoxy)methane BSD RPD 7 % 20OP49189-BSD 111-44-4 bis(2-Chloroethyl)ether BSD REC 89 % 40-140OP49189-BSD 111-44-4 bis(2-Chloroethyl)ether BSD RPD 5 % 20OP49189-BSD 108-60-1 bis(2-Chloroisopropyl)ether BSD REC 82 % 40-140OP49189-BSD 108-60-1 bis(2-Chloroisopropyl)ether BSD RPD 7 % 20OP49189-BSD 7005-72-3 4-Chlorophenyl phenyl ether BSD REC 142 f % 40-140OP49189-BSD 7005-72-3 4-Chlorophenyl phenyl ether BSD RPD 0 % 20OP49189-BSD 121-14-2 2,4-Dinitrotoluene BSD REC 137 f % 40-140OP49189-BSD 121-14-2 2,4-Dinitrotoluene BSD RPD 5 % 20OP49189-BSD 606-20-2 2,6-Dinitrotoluene BSD REC 128 f % 40-140OP49189-BSD 606-20-2 2,6-Dinitrotoluene BSD RPD 1 % 20OP49189-BSD 91-94-1 3,3'-Dichlorobenzidine BSD REC 85 % 40-140OP49189-BSD 91-94-1 3,3'-Dichlorobenzidine BSD RPD 6 % 20OP49189-BSD 132-64-9 Dibenzofuran BSD REC 116 % 40-140OP49189-BSD 132-64-9 Dibenzofuran BSD RPD 2 % 20OP49189-BSD 84-74-2 Di-n-butyl phthalate BSD REC 129 f % 40-140OP49189-BSD 84-74-2 Di-n-butyl phthalate BSD RPD 5 % 20OP49189-BSD 117-84-0 Di-n-octyl phthalate BSD REC 102 % 40-140OP49189-BSD 117-84-0 Di-n-octyl phthalate BSD RPD 4 % 20OP49189-BSD 84-66-2 Diethyl phthalate BSD REC 135 f % 40-140OP49189-BSD 84-66-2 Diethyl phthalate BSD RPD 3 % 20OP49189-BSD 131-11-3 Dimethyl phthalate BSD REC 135 % 40-140OP49189-BSD 131-11-3 Dimethyl phthalate BSD RPD 3 % 20OP49189-BSD 117-81-7 bis(2-Ethylhexyl)phthalate BSD REC 112 % 40-140OP49189-BSD 117-81-7 bis(2-Ethylhexyl)phthalate BSD RPD 4 % 20OP49189-BSD 118-74-1 Hexachlorobenzene BSD REC 128 f % 40-140OP49189-BSD 118-74-1 Hexachlorobenzene BSD RPD 3 % 20OP49189-BSD 87-68-3 Hexachlorobutadiene BSD REC 104 % 40-140OP49189-BSD 87-68-3 Hexachlorobutadiene BSD RPD 11 % 20OP49189-BSD 77-47-4 Hexachlorocyclopentadiene BSD REC 58 % 40-140OP49189-BSD 77-47-4 Hexachlorocyclopentadiene BSD RPD 5 % 20OP49189-BSD 67-72-1 Hexachloroethane BSD REC 91 % 40-140OP49189-BSD 67-72-1 Hexachloroethane BSD RPD 10 % 20OP49189-BSD 78-59-1 Isophorone BSD REC 92 % 40-140OP49189-BSD 78-59-1 Isophorone BSD RPD 8 % 20OP49189-BSD 91-57-6 2-Methylnaphthalene BSD REC 104 % 40-140OP49189-BSD 91-57-6 2-Methylnaphthalene BSD RPD 7 % 20OP49189-BSD 88-74-4 2-Nitroaniline BSD REC 120 % 40-140OP49189-BSD 88-74-4 2-Nitroaniline BSD RPD 1 % 20OP49189-BSD 99-09-2 3-Nitroaniline BSD REC 105 % 40-140OP49189-BSD 99-09-2 3-Nitroaniline BSD RPD 2 % 20OP49189-BSD 100-01-6 4-Nitroaniline BSD REC 109 % 40-140OP49189-BSD 100-01-6 4-Nitroaniline BSD RPD 0 % 20OP49189-BSD 98-95-3 Nitrobenzene BSD REC 89 % 40-140


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OP49189-BSD 98-95-3 Nitrobenzene BSD RPD 6 % 20OP49189-BSD 621-64-7 N-Nitroso-di-n-propylamine BSD REC 96 % 40-140OP49189-BSD 621-64-7 N-Nitroso-di-n-propylamine BSD RPD 7 % 20OP49189-BSD 86-30-6 N-Nitrosodiphenylamine BSD REC 116 f % 40-140OP49189-BSD 86-30-6 N-Nitrosodiphenylamine BSD RPD 6 % 20OP49189-BSD 82-68-8 Pentachloronitrobenzene BSD REC 120 % 40-140OP49189-BSD 82-68-8 Pentachloronitrobenzene BSD RPD 6 % 20OP49189-BSD 110-86-1 Pyridine BSD REC 20 % 40-140OP49189-BSD 110-86-1 Pyridine BSD RPD 75 f % 20OP49189-BSD 95-94-3 1,2,4,5-Tetrachlorobenzene BSD REC 108 % 40-140OP49189-BSD 95-94-3 1,2,4,5-Tetrachlorobenzene BSD RPD 7 % 20OP49189-BSD 120-82-1 1,2,4-Trichlorobenzene BSD REC 113 f % 40-140OP49189-BSD 120-82-1 1,2,4-Trichlorobenzene BSD RPD 9 % 20OP49189-BSD 367-12-4 2-Fluorophenol BSD SURR 52 % 15-110OP49189-BSD 4165-62-2 Phenol-d5 BSD SURR 35 % 15-110OP49189-BSD 118-79-6 2,4,6-Tribromophenol BSD SURR 112 % 15-110OP49189-BSD 4165-60-0 Nitrobenzene-d5 BSD SURR 78 % 30-130OP49189-BSD 321-60-8 2-Fluorobiphenyl BSD SURR 88 % 30-130OP49189-BSD 1718-51-0 Terphenyl-d14 BSD SURR 103 % 30-130OP49189-MB 367-12-4 2-Fluorophenol MB SURR 55 % 15-110OP49189-MB 4165-62-2 Phenol-d5 MB SURR 36 % 15-110OP49189-MB 118-79-6 2,4,6-Tribromophenol MB SURR 102 % 15-110OP49189-MB 4165-60-0 Nitrobenzene-d5 MB SURR 81 % 30-130OP49189-MB 321-60-8 2-Fluorobiphenyl MB SURR 97 % 30-130OP49189-MB 1718-51-0 Terphenyl-d14 MB SURR 107 % 30-130MC48821-22 367-12-4 2-Fluorophenol SAMP SURR 48 % 15-110MC48821-22 4165-62-2 Phenol-d5 SAMP SURR 29 % 15-110MC48821-22 118-79-6 2,4,6-Tribromophenol SAMP SURR 103 % 15-110MC48821-22 4165-60-0 Nitrobenzene-d5 SAMP SURR 76 % 30-130MC48821-22 321-60-8 2-Fluorobiphenyl SAMP SURR 86 % 30-130MC48821-22 1718-51-0 Terphenyl-d14 SAMP SURR 108 % 30-130MC48821-23 367-12-4 2-Fluorophenol SAMP SURR 47 % 15-110MC48821-23 4165-62-2 Phenol-d5 SAMP SURR 30 % 15-110MC48821-23 118-79-6 2,4,6-Tribromophenol SAMP SURR 108 % 15-110MC48821-23 4165-60-0 Nitrobenzene-d5 SAMP SURR 79 % 30-130MC48821-23 321-60-8 2-Fluorobiphenyl SAMP SURR 89 % 30-130MC48821-23 1718-51-0 Terphenyl-d14 SAMP SURR 106 % 30-130MC48821-24 367-12-4 2-Fluorophenol SAMP SURR 41 % 15-110MC48821-24 4165-62-2 Phenol-d5 SAMP SURR 26 % 15-110MC48821-24 118-79-6 2,4,6-Tribromophenol SAMP SURR 99 % 15-110MC48821-24 4165-60-0 Nitrobenzene-d5 SAMP SURR 68 % 30-130MC48821-24 321-60-8 2-Fluorobiphenyl SAMP SURR 75 % 30-130MC48821-24 1718-51-0 Terphenyl-d14 SAMP SURR 105 % 30-130MC48821-27 367-12-4 2-Fluorophenol SAMP SURR 45 % 15-110MC48821-27 4165-62-2 Phenol-d5 SAMP SURR 28 % 15-110


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MC48821-27 118-79-6 2,4,6-Tribromophenol SAMP SURR 107 % 15-110MC48821-27 4165-60-0 Nitrobenzene-d5 SAMP SURR 77 % 30-130MC48821-27 321-60-8 2-Fluorobiphenyl SAMP SURR 88 % 30-130MC48821-27 1718-51-0 Terphenyl-d14 SAMP SURR 107 % 30-130

OP49195 SW846 8270D

OP49195-BS 95-57-8 2-Chlorophenol BSP REC 86 % 30-130OP49195-BS 59-50-7 4-Chloro-3-methyl phenol BSP REC 88 % 30-130OP49195-BS 120-83-2 2,4-Dichlorophenol BSP REC 90 % 30-130OP49195-BS 105-67-9 2,4-Dimethylphenol BSP REC 85 % 30-130OP49195-BS 51-28-5 2,4-Dinitrophenol BSP REC 45 % 30-130OP49195-BS 534-52-1 4,6-Dinitro-o-cresol BSP REC 77 % 30-130OP49195-BS 95-48-7 2-Methylphenol BSP REC 89 % 30-130OP49195-BS 106-44-5 4-Methylphenol BSP REC 87 % 30-130OP49195-BS 88-75-5 2-Nitrophenol BSP REC 84 % 30-130OP49195-BS 100-02-7 4-Nitrophenol BSP REC 96 % 30-130OP49195-BS 87-86-5 Pentachlorophenol BSP REC 73 % 30-130OP49195-BS 108-95-2 Phenol BSP REC 85 % 30-130OP49195-BS 95-95-4 2,4,5-Trichlorophenol BSP REC 102 % 30-130OP49195-BS 88-06-2 2,4,6-Trichlorophenol BSP REC 100 % 30-130OP49195-BS 83-32-9 Acenaphthene BSP REC 97 % 40-140OP49195-BS 208-96-8 Acenaphthylene BSP REC 90 % 40-140OP49195-BS 62-53-3 Aniline BSP REC 46 % 40-140OP49195-BS 120-12-7 Anthracene BSP REC 93 % 40-140OP49195-BS 56-55-3 Benzo(a)anthracene BSP REC 98 % 40-140OP49195-BS 50-32-8 Benzo(a)pyrene BSP REC 89 % 40-140OP49195-BS 205-99-2 Benzo(b)fluoranthene BSP REC 89 % 40-140OP49195-BS 191-24-2 Benzo(g,h,i)perylene BSP REC 81 % 40-140OP49195-BS 207-08-9 Benzo(k)fluoranthene BSP REC 91 % 40-140OP49195-BS 101-55-3 4-Bromophenyl phenyl ether BSP REC 110 % 40-140OP49195-BS 85-68-7 Butyl benzyl phthalate BSP REC 115 % 40-140OP49195-BS 91-58-7 2-Chloronaphthalene BSP REC 99 % 40-140OP49195-BS 106-47-8 4-Chloroaniline BSP REC 50 % 40-140OP49195-BS 86-74-8 Carbazole BSP REC 97 % 40-140OP49195-BS 218-01-9 Chrysene BSP REC 94 % 40-140OP49195-BS 111-91-1 bis(2-Chloroethoxy)methane BSP REC 84 % 40-140OP49195-BS 111-44-4 bis(2-Chloroethyl)ether BSP REC 92 % 40-140OP49195-BS 108-60-1 bis(2-Chloroisopropyl)ether BSP REC 96 % 40-140OP49195-BS 7005-72-3 4-Chlorophenyl phenyl ether BSP REC 115 g % 40-140OP49195-BS 121-14-2 2,4-Dinitrotoluene BSP REC 109 % 40-140OP49195-BS 606-20-2 2,6-Dinitrotoluene BSP REC 101 % 40-140OP49195-BS 91-94-1 3,3'-Dichlorobenzidine BSP REC 58 % 40-140OP49195-BS 53-70-3 Dibenzo(a,h)anthracene BSP REC 81 % 40-140OP49195-BS 132-64-9 Dibenzofuran BSP REC 98 % 40-140


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OP49195-BS 84-74-2 Di-n-butyl phthalate BSP REC 107 % 40-140OP49195-BS 117-84-0 Di-n-octyl phthalate BSP REC 98 % 40-140OP49195-BS 84-66-2 Diethyl phthalate BSP REC 114 g % 40-140OP49195-BS 131-11-3 Dimethyl phthalate BSP REC 112 g % 40-140OP49195-BS 117-81-7 bis(2-Ethylhexyl)phthalate BSP REC 103 % 40-140OP49195-BS 206-44-0 Fluoranthene BSP REC 98 % 40-140OP49195-BS 86-73-7 Fluorene BSP REC 106 % 40-140OP49195-BS 118-74-1 Hexachlorobenzene BSP REC 100 % 40-140OP49195-BS 87-68-3 Hexachlorobutadiene BSP REC 88 % 40-140OP49195-BS 77-47-4 Hexachlorocyclopentadiene BSP REC 56 % 40-140OP49195-BS 67-72-1 Hexachloroethane BSP REC 85 % 40-140OP49195-BS 193-39-5 Indeno(1,2,3-cd)pyrene BSP REC 80 % 40-140OP49195-BS 78-59-1 Isophorone BSP REC 88 % 40-140OP49195-BS 91-57-6 2-Methylnaphthalene BSP REC 89 % 40-140OP49195-BS 88-74-4 2-Nitroaniline BSP REC 102 % 40-140OP49195-BS 99-09-2 3-Nitroaniline BSP REC 71 % 40-140OP49195-BS 100-01-6 4-Nitroaniline BSP REC 92 % 40-140OP49195-BS 91-20-3 Naphthalene BSP REC 118 % 40-140OP49195-BS 98-95-3 Nitrobenzene BSP REC 84 % 40-140OP49195-BS 621-64-7 N-Nitroso-di-n-propylamine BSP REC 95 % 40-140OP49195-BS 86-30-6 N-Nitrosodiphenylamine BSP REC 95 % 40-140OP49195-BS 82-68-8 Pentachloronitrobenzene BSP REC 99 % 40-140OP49195-BS 85-01-8 Phenanthrene BSP REC 98 % 40-140OP49195-BS 129-00-0 Pyrene BSP REC 106 % 40-140OP49195-BS 110-86-1 Pyridine BSP REC 62 % 40-140OP49195-BS 95-94-3 1,2,4,5-Tetrachlorobenzene BSP REC 92 % 40-140OP49195-BS 120-82-1 1,2,4-Trichlorobenzene BSP REC 95 % 40-140OP49195-BS 367-12-4 2-Fluorophenol BSP SURR 75 % 30-130OP49195-BS 4165-62-2 Phenol-d5 BSP SURR 80 % 30-130OP49195-BS 118-79-6 2,4,6-Tribromophenol BSP SURR 86 % 30-130OP49195-BS 4165-60-0 Nitrobenzene-d5 BSP SURR 73 % 30-130OP49195-BS 321-60-8 2-Fluorobiphenyl BSP SURR 84 % 30-130OP49195-BS 1718-51-0 Terphenyl-d14 BSP SURR 95 % 30-130OP49195-MB 367-12-4 2-Fluorophenol MB SURR 68 % 30-130OP49195-MB 4165-62-2 Phenol-d5 MB SURR 69 % 30-130OP49195-MB 118-79-6 2,4,6-Tribromophenol MB SURR 64 % 30-130OP49195-MB 4165-60-0 Nitrobenzene-d5 MB SURR 67 % 30-130OP49195-MB 321-60-8 2-Fluorobiphenyl MB SURR 74 % 30-130OP49195-MB 1718-51-0 Terphenyl-d14 MB SURR 87 % 30-130MC48821-2 367-12-4 2-Fluorophenol SAMP SURR 77 % 30-130MC48821-2 4165-62-2 Phenol-d5 SAMP SURR 76 % 30-130MC48821-2 118-79-6 2,4,6-Tribromophenol SAMP SURR 81 % 30-130MC48821-2 4165-60-0 Nitrobenzene-d5 SAMP SURR 72 % 30-130MC48821-2 321-60-8 2-Fluorobiphenyl SAMP SURR 82 % 30-130MC48821-2 1718-51-0 Terphenyl-d14 SAMP SURR 96 % 30-130


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MC48821-3 367-12-4 2-Fluorophenol SAMP SURR 79 % 30-130MC48821-3 4165-62-2 Phenol-d5 SAMP SURR 78 % 30-130MC48821-3 118-79-6 2,4,6-Tribromophenol SAMP SURR 86 % 30-130MC48821-3 4165-60-0 Nitrobenzene-d5 SAMP SURR 75 % 30-130MC48821-3 321-60-8 2-Fluorobiphenyl SAMP SURR 87 % 30-130MC48821-3 1718-51-0 Terphenyl-d14 SAMP SURR 99 % 30-130MC48821-4 367-12-4 2-Fluorophenol SAMP SURR 71 % 30-130MC48821-4 4165-62-2 Phenol-d5 SAMP SURR 71 % 30-130MC48821-4 118-79-6 2,4,6-Tribromophenol SAMP SURR 75 % 30-130MC48821-4 4165-60-0 Nitrobenzene-d5 SAMP SURR 65 % 30-130MC48821-4 321-60-8 2-Fluorobiphenyl SAMP SURR 78 % 30-130MC48821-4 1718-51-0 Terphenyl-d14 SAMP SURR 87 % 30-130MC48821-5 367-12-4 2-Fluorophenol SAMP SURR 66 % 30-130MC48821-5 4165-62-2 Phenol-d5 SAMP SURR 64 % 30-130MC48821-5 118-79-6 2,4,6-Tribromophenol SAMP SURR 73 % 30-130MC48821-5 4165-60-0 Nitrobenzene-d5 SAMP SURR 63 % 30-130MC48821-5 321-60-8 2-Fluorobiphenyl SAMP SURR 73 % 30-130MC48821-5 1718-51-0 Terphenyl-d14 SAMP SURR 83 % 30-130MC48821-6 367-12-4 2-Fluorophenol SAMP SURR 78 % 30-130MC48821-6 4165-62-2 Phenol-d5 SAMP SURR 77 % 30-130MC48821-6 118-79-6 2,4,6-Tribromophenol SAMP SURR 83 % 30-130MC48821-6 4165-60-0 Nitrobenzene-d5 SAMP SURR 76 % 30-130MC48821-6 321-60-8 2-Fluorobiphenyl SAMP SURR 85 % 30-130MC48821-6 1718-51-0 Terphenyl-d14 SAMP SURR 96 % 30-130MC48821-7 367-12-4 2-Fluorophenol SAMP SURR 69 % 30-130MC48821-7 4165-62-2 Phenol-d5 SAMP SURR 78 % 30-130MC48821-7 118-79-6 2,4,6-Tribromophenol SAMP SURR 109 % 30-130MC48821-7 4165-60-0 Nitrobenzene-d5 SAMP SURR 74 % 30-130MC48821-7 321-60-8 2-Fluorobiphenyl SAMP SURR 89 % 30-130MC48821-7 1718-51-0 Terphenyl-d14 SAMP SURR 97 % 30-130MC48821-8 367-12-4 2-Fluorophenol SAMP SURR 69 % 30-130MC48821-8 4165-62-2 Phenol-d5 SAMP SURR 69 % 30-130MC48821-8 118-79-6 2,4,6-Tribromophenol SAMP SURR 78 % 30-130MC48821-8 4165-60-0 Nitrobenzene-d5 SAMP SURR 70 % 30-130MC48821-8 321-60-8 2-Fluorobiphenyl SAMP SURR 79 % 30-130MC48821-8 1718-51-0 Terphenyl-d14 SAMP SURR 87 % 30-130MC48821-9 367-12-4 2-Fluorophenol SAMP SURR 67 % 30-130MC48821-9 4165-62-2 Phenol-d5 SAMP SURR 67 % 30-130MC48821-9 118-79-6 2,4,6-Tribromophenol SAMP SURR 74 % 30-130MC48821-9 4165-60-0 Nitrobenzene-d5 SAMP SURR 63 % 30-130MC48821-9 321-60-8 2-Fluorobiphenyl SAMP SURR 72 % 30-130MC48821-9 1718-51-0 Terphenyl-d14 SAMP SURR 81 % 30-130MC48821-10 367-12-4 2-Fluorophenol SAMP SURR 66 % 30-130MC48821-10 4165-62-2 Phenol-d5 SAMP SURR 65 % 30-130MC48821-10 118-79-6 2,4,6-Tribromophenol SAMP SURR 72 % 30-130


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MC48821

55.4



MC48821-10 4165-60-0 Nitrobenzene-d5 SAMP SURR 65 % 30-130MC48821-10 321-60-8 2-Fluorobiphenyl SAMP SURR 73 % 30-130MC48821-10 1718-51-0 Terphenyl-d14 SAMP SURR 83 % 30-130MC48821-11 367-12-4 2-Fluorophenol SAMP SURR 69 % 30-130MC48821-11 4165-62-2 Phenol-d5 SAMP SURR 71 % 30-130MC48821-11 118-79-6 2,4,6-Tribromophenol SAMP SURR 83 % 30-130MC48821-11 4165-60-0 Nitrobenzene-d5 SAMP SURR 68 % 30-130MC48821-11 321-60-8 2-Fluorobiphenyl SAMP SURR 80 % 30-130MC48821-11 1718-51-0 Terphenyl-d14 SAMP SURR 91 % 30-130MC48821-12 367-12-4 2-Fluorophenol SAMP SURR 72 % 30-130MC48821-12 4165-62-2 Phenol-d5 SAMP SURR 71 % 30-130MC48821-12 118-79-6 2,4,6-Tribromophenol SAMP SURR 79 % 30-130MC48821-12 4165-60-0 Nitrobenzene-d5 SAMP SURR 69 % 30-130MC48821-12 321-60-8 2-Fluorobiphenyl SAMP SURR 80 % 30-130MC48821-12 1718-51-0 Terphenyl-d14 SAMP SURR 92 % 30-130MC48821-13 367-12-4 2-Fluorophenol SAMP SURR 68 % 30-130MC48821-13 4165-62-2 Phenol-d5 SAMP SURR 68 % 30-130MC48821-13 118-79-6 2,4,6-Tribromophenol SAMP SURR 79 % 30-130MC48821-13 4165-60-0 Nitrobenzene-d5 SAMP SURR 68 % 30-130MC48821-13 321-60-8 2-Fluorobiphenyl SAMP SURR 78 % 30-130MC48821-13 1718-51-0 Terphenyl-d14 SAMP SURR 86 % 30-130MC48821-14 367-12-4 2-Fluorophenol SAMP SURR 61 % 30-130MC48821-14 4165-62-2 Phenol-d5 SAMP SURR 61 % 30-130MC48821-14 118-79-6 2,4,6-Tribromophenol SAMP SURR 81 % 30-130MC48821-14 4165-60-0 Nitrobenzene-d5 SAMP SURR 59 % 30-130MC48821-14 321-60-8 2-Fluorobiphenyl SAMP SURR 72 % 30-130MC48821-14 1718-51-0 Terphenyl-d14 SAMP SURR 88 % 30-130MC48821-15 367-12-4 2-Fluorophenol SAMP SURR 74 % 30-130MC48821-15 4165-62-2 Phenol-d5 SAMP SURR 74 % 30-130MC48821-15 118-79-6 2,4,6-Tribromophenol SAMP SURR 98 % 30-130MC48821-15 4165-60-0 Nitrobenzene-d5 SAMP SURR 70 % 30-130MC48821-15 321-60-8 2-Fluorobiphenyl SAMP SURR 88 % 30-130MC48821-15 1718-51-0 Terphenyl-d14 SAMP SURR 95 % 30-130MC48821-16 367-12-4 2-Fluorophenol SAMP SURR 65 % 30-130MC48821-16 4165-62-2 Phenol-d5 SAMP SURR 64 % 30-130MC48821-16 118-79-6 2,4,6-Tribromophenol SAMP SURR 78 % 30-130MC48821-16 4165-60-0 Nitrobenzene-d5 SAMP SURR 63 % 30-130MC48821-16 321-60-8 2-Fluorobiphenyl SAMP SURR 75 % 30-130MC48821-16 1718-51-0 Terphenyl-d14 SAMP SURR 79 % 30-130MC48821-17 367-12-4 2-Fluorophenol SAMP SURR 69 % 30-130MC48821-17 4165-62-2 Phenol-d5 SAMP SURR 69 % 30-130MC48821-17 118-79-6 2,4,6-Tribromophenol SAMP SURR 82 % 30-130MC48821-17 4165-60-0 Nitrobenzene-d5 SAMP SURR 66 % 30-130MC48821-17 321-60-8 2-Fluorobiphenyl SAMP SURR 80 % 30-130MC48821-17 1718-51-0 Terphenyl-d14 SAMP SURR 84 % 30-130


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MC48821-18 367-12-4 2-Fluorophenol SAMP SURR 62 % 30-130MC48821-18 4165-62-2 Phenol-d5 SAMP SURR 58 % 30-130MC48821-18 118-79-6 2,4,6-Tribromophenol SAMP SURR 89 % 30-130MC48821-18 4165-60-0 Nitrobenzene-d5 SAMP SURR 58 % 30-130MC48821-18 321-60-8 2-Fluorobiphenyl SAMP SURR 76 % 30-130MC48821-18 1718-51-0 Terphenyl-d14 SAMP SURR 84 % 30-130MC48821-19 367-12-4 2-Fluorophenol SAMP SURR 70 % 30-130MC48821-19 4165-62-2 Phenol-d5 SAMP SURR 69 % 30-130MC48821-19 118-79-6 2,4,6-Tribromophenol SAMP SURR 94 % 30-130MC48821-19 4165-60-0 Nitrobenzene-d5 SAMP SURR 68 % 30-130MC48821-19 321-60-8 2-Fluorobiphenyl SAMP SURR 88 % 30-130MC48821-19 1718-51-0 Terphenyl-d14 SAMP SURR 95 % 30-130MC48821-20 367-12-4 2-Fluorophenol SAMP SURR 58 % 30-130MC48821-20 4165-62-2 Phenol-d5 SAMP SURR 63 % 30-130MC48821-20 118-79-6 2,4,6-Tribromophenol SAMP SURR 82 % 30-130MC48821-20 4165-60-0 Nitrobenzene-d5 SAMP SURR 55 % 30-130MC48821-20 321-60-8 2-Fluorobiphenyl SAMP SURR 67 % 30-130MC48821-20 1718-51-0 Terphenyl-d14 SAMP SURR 84 % 30-130

OP49179 SW846 8082A

OP49179-BS 12674-11-2 Aroclor 1016 BSP REC 105 % 40-140OP49179-BS 11096-82-5 Aroclor 1260 BSP REC 110 % 40-140OP49179-BS 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 85 % 30-150OP49179-BS 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 89 % 30-150OP49179-BS 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 70 % 30-150OP49179-BS 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 69 % 30-150OP49179-BSD 12674-11-2 Aroclor 1016 BSD REC 95 % 40-140OP49179-BSD 12674-11-2 Aroclor 1016 BSD RPD 10 % 20OP49179-BSD 11104-28-2 Aroclor 1221 BSD RPD 0 % 20OP49179-BSD 11141-16-5 Aroclor 1232 BSD RPD 0 % 20OP49179-BSD 53469-21-9 Aroclor 1242 BSD RPD 0 % 20OP49179-BSD 12672-29-6 Aroclor 1248 BSD RPD 0 % 20OP49179-BSD 11097-69-1 Aroclor 1254 BSD RPD 0 % 20OP49179-BSD 11096-82-5 Aroclor 1260 BSD REC 95 % 40-140OP49179-BSD 11096-82-5 Aroclor 1260 BSD RPD 15 % 20OP49179-BSD 37324-23-5 Aroclor 1262 BSD RPD 0 % 20OP49179-BSD 11100-14-4 Aroclor 1268 BSD RPD 0 % 20OP49179-BSD 877-09-8 Tetrachloro-m-xylene (sig#1) BSD SURR 81 % 30-150OP49179-BSD 877-09-8 Tetrachloro-m-xylene (sig#2) BSD SURR 85 % 30-150OP49179-BSD 2051-24-3 Decachlorobiphenyl (sig#1) BSD SURR 72 % 30-150OP49179-BSD 2051-24-3 Decachlorobiphenyl (sig#2) BSD SURR 72 % 30-150OP49179-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 94 % 30-150OP49179-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 97 % 30-150OP49179-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 77 % 30-150


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OP49179-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 77 % 30-150MC48821-22 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 86 % 30-150MC48821-22 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 84 % 30-150MC48821-22 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 86 % 30-150MC48821-22 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 87 % 30-150MC48821-23 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 93 % 30-150MC48821-23 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 93 % 30-150MC48821-23 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 114 % 30-150MC48821-23 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 111 % 30-150MC48821-24 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 90 % 30-150MC48821-24 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 90 % 30-150MC48821-24 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 104 % 30-150MC48821-24 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 100 % 30-150MC48821-27 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 92 % 30-150MC48821-27 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 90 % 30-150MC48821-27 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 123 % 30-150MC48821-27 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 122 % 30-150

OP49191 SW846 8081B

OP49191-BS 15972-60-8 Alachlor BSP REC 67 % 40-140OP49191-BS 309-00-2 Aldrin BSP REC 53 % 40-140OP49191-BS 319-84-6 alpha-BHC BSP REC 57 % 40-140OP49191-BS 319-85-7 beta-BHC BSP REC 68 % 40-140OP49191-BS 319-86-8 delta-BHC BSP REC 33 % 40-140OP49191-BS 58-89-9 gamma-BHC (Lindane) BSP REC 58 % 40-140OP49191-BS 60-57-1 Dieldrin BSP REC 71 % 40-140OP49191-BS 72-54-8 4,4'-DDD BSP REC 54 % 40-140OP49191-BS 72-55-9 4,4'-DDE BSP REC 51 % 40-140OP49191-BS 50-29-3 4,4'-DDT BSP REC 75 % 40-140OP49191-BS 72-20-8 Endrin BSP REC 78 % 40-140OP49191-BS 1031-07-8 Endosulfan sulfate BSP REC 58 % 40-140OP49191-BS 7421-93-4 Endrin aldehyde BSP REC 32 % 40-140OP49191-BS 53494-70-5 Endrin ketone BSP REC 60 % 40-140OP49191-BS 959-98-8 Endosulfan-I BSP REC 46 % 40-140OP49191-BS 33213-65-9 Endosulfan-II BSP REC 63 % 40-140OP49191-BS 76-44-8 Heptachlor BSP REC 66 % 40-140OP49191-BS 1024-57-3 Heptachlor epoxide BSP REC 67 % 40-140OP49191-BS 72-43-5 Methoxychlor BSP REC 99 % 40-140OP49191-BS 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 58 % 30-150OP49191-BS 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 57 % 30-150OP49191-BS 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 11 % 30-150OP49191-BS 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 46 % 30-150OP49191-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 41 % 30-150OP49191-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 43 % 30-150


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OP49191-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 8 h % 30-150OP49191-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 31 % 30-150MC48821-22 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 44 % 30-150MC48821-22 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 45 % 30-150MC48821-22 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 19 % 30-150MC48821-22 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 56 % 30-150MC48821-23 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 35 % 30-150MC48821-23 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 38 % 30-150MC48821-23 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 16 % 30-150MC48821-23 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 50 % 30-150MC48821-24 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 42 % 30-150MC48821-24 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 44 % 30-150MC48821-24 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 17 % 30-150MC48821-24 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 55 % 30-150MC48821-27 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 58 % 30-150MC48821-27 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 44 % 30-150MC48821-27 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 19 % 30-150MC48821-27 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 71 % 30-150

OP49200 SW846 8082A

OP49200-BS 12674-11-2 Aroclor 1016 BSP REC 93 % 40-140OP49200-BS 11096-82-5 Aroclor 1260 BSP REC 94 % 40-140OP49200-BS 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 85 % 30-150OP49200-BS 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 91 % 30-150OP49200-BS 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 97 % 30-150OP49200-BS 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 103 % 30-150OP49200-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 95 % 30-150OP49200-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 100 % 30-150OP49200-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 104 % 30-150OP49200-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 112 % 30-150MC48821-11 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 65 % 30-150MC48821-11 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 58 % 30-150MC48821-11 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 145 % 30-150MC48821-11 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 59 % 30-150MC48821-12 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 84 % 30-150MC48821-12 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 76 % 30-150MC48821-12 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 69 % 30-150MC48821-12 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 60 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 81 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 78 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 94 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 76 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 68 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 56 % 30-150


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MC48821-14 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 113 % 30-150MC48821-14 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 71 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 77 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 66 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 99 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 71 % 30-150MC48821-16 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 82 % 30-150MC48821-16 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 75 % 30-150MC48821-16 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 91 % 30-150MC48821-16 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 82 % 30-150MC48821-17 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 77 % 30-150MC48821-17 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 68 % 30-150MC48821-17 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 107 % 30-150MC48821-17 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 80 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 81 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 72 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 108 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 83 % 30-150MC48821-19 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 72 % 30-150MC48821-19 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 64 % 30-150MC48821-19 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 119 % 30-150MC48821-19 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 78 % 30-150MC48821-20 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 79 % 30-150MC48821-20 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 72 % 30-150MC48821-20 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 86 % 30-150MC48821-20 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 74 % 30-150

OP49201 SW846 8081B

OP49201-BS 15972-60-8 Alachlor BSP REC 55 % 40-140OP49201-BS 309-00-2 Aldrin BSP REC 57 % 40-140OP49201-BS 319-84-6 alpha-BHC BSP REC 54 % 40-140OP49201-BS 319-85-7 beta-BHC BSP REC 57 % 40-140OP49201-BS 319-86-8 delta-BHC BSP REC 27 % 40-140OP49201-BS 58-89-9 gamma-BHC (Lindane) BSP REC 55 % 40-140OP49201-BS 60-57-1 Dieldrin BSP REC 59 % 40-140OP49201-BS 72-54-8 4,4'-DDD BSP REC 63 % 40-140OP49201-BS 72-55-9 4,4'-DDE BSP REC 63 % 40-140OP49201-BS 50-29-3 4,4'-DDT BSP REC 66 % 40-140OP49201-BS 72-20-8 Endrin BSP REC 61 % 40-140OP49201-BS 1031-07-8 Endosulfan sulfate BSP REC 68 % 40-140OP49201-BS 7421-93-4 Endrin aldehyde BSP REC 66 % 40-140OP49201-BS 959-98-8 Endosulfan-I BSP REC 62 % 40-140OP49201-BS 33213-65-9 Endosulfan-II BSP REC 67 % 40-140OP49201-BS 76-44-8 Heptachlor BSP REC 63 % 40-140


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OP49201-BS 1024-57-3 Heptachlor epoxide BSP REC 58 % 40-140OP49201-BS 72-43-5 Methoxychlor BSP REC 75 % 40-140OP49201-BS 53494-70-5 Endrin ketone BSP REC 72 % 40-140OP49201-BS 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 63 % 30-150OP49201-BS 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 60 % 30-150OP49201-BS 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 58 % 30-150OP49201-BS 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 73 % 30-150OP49201-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 78 % 30-150OP49201-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 78 % 30-150OP49201-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 78 % 30-150OP49201-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 100 % 30-150MC48821-11 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 41 % 30-150MC48821-11 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 51 % 30-150MC48821-11 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 176 i % 30-150MC48821-11 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 275 i % 30-150MC48821-12 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 85 % 30-150MC48821-12 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 92 % 30-150MC48821-12 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 96 % 30-150MC48821-12 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 104 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 62 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 84 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 61 % 30-150MC48821-13 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 77 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 126 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 60 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 115 % 30-150MC48821-13 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 71 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 51 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 59 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 65 % 30-150MC48821-14 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 60 % 30-150MC48821-14 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 57 % 30-150MC48821-14 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 105 % 30-150MC48821-14 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 123 % 30-150MC48821-14 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 158 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 82 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 61 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 76 % 30-150MC48821-15 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 67 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 115 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 87 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 153 % 30-150MC48821-15 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 165 % 30-150MC48821-16 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 63 % 30-150MC48821-16 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 62 % 30-150


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MC48821

55.4



MC48821-16 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 71 % 30-150MC48821-16 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 81 % 30-150MC48821-17 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 47 % 30-150MC48821-17 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 55 % 30-150MC48821-17 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 71 % 30-150MC48821-17 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 116 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 63 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 73 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 62 % 30-150MC48821-18 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 66 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 117 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 68 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 152 % 30-150MC48821-18 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 145 % 30-150MC48821-19 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 55 % 30-150MC48821-19 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 55 % 30-150MC48821-19 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 114 % 30-150MC48821-19 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 213 i % 30-150MC48821-20 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 52 % 30-150MC48821-20 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 58 % 30-150MC48821-20 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 57 % 30-150MC48821-20 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 77 % 30-150

OP49218 SW846 8082A

OP49218-BS 12674-11-2 Aroclor 1016 BSP REC 104 % 40-140OP49218-BS 11096-82-5 Aroclor 1260 BSP REC 113 % 40-140OP49218-BS 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 84 % 30-150OP49218-BS 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 87 % 30-150OP49218-BS 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 112 % 30-150OP49218-BS 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 111 % 30-150OP49218-BSD 12674-11-2 Aroclor 1016 BSD REC 103 % 40-140OP49218-BSD 12674-11-2 Aroclor 1016 BSD RPD 3 % 30OP49218-BSD 11104-28-2 Aroclor 1221 BSD RPD 0 % 30OP49218-BSD 11141-16-5 Aroclor 1232 BSD RPD 0 % 30OP49218-BSD 53469-21-9 Aroclor 1242 BSD RPD 0 % 30OP49218-BSD 12672-29-6 Aroclor 1248 BSD RPD 0 % 30OP49218-BSD 11097-69-1 Aroclor 1254 BSD RPD 0 % 30OP49218-BSD 11096-82-5 Aroclor 1260 BSD REC 111 % 40-140OP49218-BSD 11096-82-5 Aroclor 1260 BSD RPD 4 % 30OP49218-BSD 37324-23-5 Aroclor 1262 BSD RPD 0 % 30OP49218-BSD 11100-14-4 Aroclor 1268 BSD RPD 0 % 30OP49218-BSD 877-09-8 Tetrachloro-m-xylene (sig#1) BSD SURR 85 % 30-150OP49218-BSD 877-09-8 Tetrachloro-m-xylene (sig#2) BSD SURR 88 % 30-150OP49218-BSD 2051-24-3 Decachlorobiphenyl (sig#1) BSD SURR 110 % 30-150


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OP49218-BSD 2051-24-3 Decachlorobiphenyl (sig#2) BSD SURR 107 % 30-150OP49218-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 93 % 30-150OP49218-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 96 % 30-150OP49218-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 128 % 30-150OP49218-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 123 % 30-150MC48821-1 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 59 % 30-150MC48821-1 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 52 % 30-150MC48821-1 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 83 % 30-150MC48821-1 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 73 % 30-150MC48821-2 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 69 % 30-150MC48821-2 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 73 % 30-150MC48821-2 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 95 % 30-150MC48821-2 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 91 % 30-150MC48821-3 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 83 % 30-150MC48821-3 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 101 % 30-150MC48821-3 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 118 % 30-150MC48821-3 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 107 % 30-150MC48821-4 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 96 % 30-150MC48821-4 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 107 % 30-150MC48821-4 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 134 % 30-150MC48821-4 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 128 % 30-150MC48821-5 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 78 % 30-150MC48821-5 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 81 % 30-150MC48821-5 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 111 % 30-150MC48821-5 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 106 % 30-150MC48821-6 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 68 % 30-150MC48821-6 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 72 % 30-150MC48821-6 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 88 % 30-150MC48821-6 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 85 % 30-150MC48821-7 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 74 % 30-150MC48821-7 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 56 % 30-150MC48821-7 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 106 % 30-150MC48821-7 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 79 % 30-150MC48821-8 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 76 % 30-150MC48821-8 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 70 % 30-150MC48821-8 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 107 % 30-150MC48821-8 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 104 % 30-150MC48821-9 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 95 % 30-150MC48821-9 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 92 % 30-150MC48821-9 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 131 % 30-150MC48821-9 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 118 % 30-150MC48821-10 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 100 % 30-150MC48821-10 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 99 % 30-150MC48821-10 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 119 % 30-150MC48821-10 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 114 % 30-150


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55.4



MC48821-21 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 76 % 30-150MC48821-21 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 76 % 30-150MC48821-21 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 107 % 30-150MC48821-21 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 98 % 30-150

OP49219 SW846 8081B

OP49219-BS1 15972-60-8 Alachlor BSP REC 107 % 40-140OP49219-BS1 309-00-2 Aldrin BSP REC 93 % 40-140OP49219-BS1 319-84-6 alpha-BHC BSP REC 91 % 40-140OP49219-BS1 319-85-7 beta-BHC BSP REC 102 % 40-140OP49219-BS1 319-86-8 delta-BHC BSP REC 47 % 40-140OP49219-BS1 58-89-9 gamma-BHC (Lindane) BSP REC 93 % 40-140OP49219-BS1 60-57-1 Dieldrin BSP REC 98 % 40-140OP49219-BS1 72-54-8 4,4'-DDD BSP REC 97 % 40-140OP49219-BS1 72-55-9 4,4'-DDE BSP REC 98 % 40-140OP49219-BS1 50-29-3 4,4'-DDT BSP REC 98 % 40-140OP49219-BS1 72-20-8 Endrin BSP REC 99 % 40-140OP49219-BS1 1031-07-8 Endosulfan sulfate BSP REC 107 % 40-140OP49219-BS1 7421-93-4 Endrin aldehyde BSP REC 94 % 40-140OP49219-BS1 959-98-8 Endosulfan-I BSP REC 100 % 40-140OP49219-BS1 33213-65-9 Endosulfan-II BSP REC 102 % 40-140OP49219-BS1 76-44-8 Heptachlor BSP REC 96 % 40-140OP49219-BS1 1024-57-3 Heptachlor epoxide BSP REC 97 % 40-140OP49219-BS1 72-43-5 Methoxychlor BSP REC 99 % 40-140OP49219-BS1 53494-70-5 Endrin ketone BSP REC 107 % 40-140OP49219-BS1 877-09-8 Tetrachloro-m-xylene (sig#1) BSP SURR 82 % 30-150OP49219-BS1 877-09-8 Tetrachloro-m-xylene (sig#2) BSP SURR 81 % 30-150OP49219-BS1 2051-24-3 Decachlorobiphenyl (sig#1) BSP SURR 77 % 30-150OP49219-BS1 2051-24-3 Decachlorobiphenyl (sig#2) BSP SURR 100 % 30-150OP49219-MB 877-09-8 Tetrachloro-m-xylene (sig#1) MB SURR 75 % 30-150OP49219-MB 877-09-8 Tetrachloro-m-xylene (sig#2) MB SURR 78 % 30-150OP49219-MB 2051-24-3 Decachlorobiphenyl (sig#1) MB SURR 85 % 30-150OP49219-MB 2051-24-3 Decachlorobiphenyl (sig#2) MB SURR 104 % 30-150MC48821-1 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 61 % 30-150MC48821-1 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 77 % 30-150MC48821-1 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 78 % 30-150MC48821-1 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 250 i % 30-150MC48821-2 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 58 % 30-150MC48821-2 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 64 % 30-150MC48821-2 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 54 % 30-150MC48821-2 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 84 % 30-150MC48821-3 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 61 % 30-150MC48821-3 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 69 % 30-150MC48821-3 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 50 % 30-150


384 of 555

MC48821

55.4



MC48821-3 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 97 % 30-150MC48821-4 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 43 % 30-150MC48821-4 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 50 % 30-150MC48821-4 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 52 % 30-150MC48821-4 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 67 % 30-150MC48821-5 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 56 % 30-150MC48821-5 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 72 % 30-150MC48821-5 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 60 % 30-150MC48821-5 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 87 % 30-150MC48821-6 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 48 % 30-150MC48821-6 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 55 % 30-150MC48821-6 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 52 % 30-150MC48821-6 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 75 % 30-150MC48821-7 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 40 % 30-150MC48821-7 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 54 % 30-150MC48821-7 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 133 % 30-150MC48821-7 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 826 i % 30-150MC48821-8 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 47 % 30-150MC48821-8 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 63 % 30-150MC48821-8 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 64 % 30-150MC48821-8 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 98 % 30-150MC48821-9 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 40 % 30-150MC48821-9 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 51 % 30-150MC48821-9 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 36 % 30-150MC48821-9 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 72 % 30-150MC48821-10 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 60 % 30-150MC48821-10 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 73 % 30-150MC48821-10 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 51 % 30-150MC48821-10 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 87 % 30-150MC48821-21 877-09-8 Tetrachloro-m-xylene (sig#1) SAMP SURR 58 % 30-150MC48821-21 877-09-8 Tetrachloro-m-xylene (sig#2) SAMP SURR 72 % 30-150MC48821-21 2051-24-3 Decachlorobiphenyl (sig#1) SAMP SURR 41 % 30-150MC48821-21 2051-24-3 Decachlorobiphenyl (sig#2) SAMP SURR 98 % 30-150

(a) Outside control limits. Refer to Blank Spike Duplicate.(b) Outside control limits. Associated samples are non-detect for this compound.(c) Outside control limits due to possible matrix interference. Confirmed by reanalysis.(d) Outside control limits. Individual spike recoveries within acceptance limits.(e) Outside control limits. Refer to Blank Spike.(f) Outside control limits. Meets program technical requirements.(g) Outside control limits. Blank Spike meets program technical requirements.(h) Outside control limits.(i) Outside control limits due to possible matrix interference.


385 of 555

MC48821

55.4

SGS Accutest

GC/MS Volatiles

QC Data Summaries


• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries• Internal Standard Area Summaries• Surrogate Recovery Summaries


386 of 555

MC48821

6

Method Blank Summary Page 1 of 3 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSV1905-MB V51594.D 1 11/22/16 KP n/a n/a MSV1905

The QC reported here applies to the following samples: Method: SW846 8260C

MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27


67-64-1 Acetone ND 10 ug/l107-13-1 Acrylonitrile ND 5.0 ug/l71-43-2 Benzene ND 0.50 ug/l108-86-1 Bromobenzene ND 5.0 ug/l75-27-4 Bromodichloromethane ND 1.0 ug/l75-25-2 Bromoform ND 1.0 ug/l74-83-9 Bromomethane ND 2.0 ug/l78-93-3 2-Butanone (MEK) ND 10 ug/l104-51-8 n-Butylbenzene ND 5.0 ug/l135-98-8 sec-Butylbenzene ND 5.0 ug/l98-06-6 tert-Butylbenzene ND 5.0 ug/l75-15-0 Carbon disulfide ND 5.0 ug/l56-23-5 Carbon tetrachloride ND 1.0 ug/l108-90-7 Chlorobenzene ND 1.0 ug/l75-00-3 Chloroethane ND 2.0 ug/l67-66-3 Chloroform ND 1.0 ug/l74-87-3 Chloromethane ND 2.0 ug/l95-49-8 o-Chlorotoluene ND 5.0 ug/l106-43-4 p-Chlorotoluene ND 5.0 ug/l96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 ug/l124-48-1 Dibromochloromethane ND 1.0 ug/l106-93-4 1,2-Dibromoethane ND 1.0 ug/l95-50-1 1,2-Dichlorobenzene ND 1.0 ug/l541-73-1 1,3-Dichlorobenzene ND 1.0 ug/l106-46-7 1,4-Dichlorobenzene ND 1.0 ug/l75-71-8 Dichlorodifluoromethane ND 2.0 ug/l75-34-3 1,1-Dichloroethane ND 1.0 ug/l107-06-2 1,2-Dichloroethane ND 1.0 ug/l75-35-4 1,1-Dichloroethene ND 1.0 ug/l156-59-2 cis-1,2-Dichloroethene ND 1.0 ug/l156-60-5 trans-1,2-Dichloroethene ND 1.0 ug/l78-87-5 1,2-Dichloropropane ND 2.0 ug/l142-28-9 1,3-Dichloropropane ND 5.0 ug/l594-20-7 2,2-Dichloropropane ND 5.0 ug/l563-58-6 1,1-Dichloropropene ND 5.0 ug/l10061-01-5 cis-1,3-Dichloropropene ND 0.50 ug/l

387 of 555

MC48821

66.1.1




MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27


10061-02-6 trans-1,3-Dichloropropene ND 0.50 ug/l100-41-4 Ethylbenzene ND 1.0 ug/l76-13-1 Freon 113 ND 5.0 ug/l87-68-3 Hexachlorobutadiene ND 5.0 ug/l591-78-6 2-Hexanone ND 10 ug/l98-82-8 Isopropylbenzene ND 5.0 ug/l99-87-6 p-Isopropyltoluene ND 5.0 ug/l1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.0 ug/l74-95-3 Methylene bromide ND 5.0 ug/l75-09-2 Methylene chloride ND 2.0 ug/l91-20-3 Naphthalene ND 5.0 ug/l103-65-1 n-Propylbenzene ND 5.0 ug/l100-42-5 Styrene ND 5.0 ug/l630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 ug/l127-18-4 Tetrachloroethene ND 1.0 ug/l109-99-9 Tetrahydrofuran ND 10 ug/l108-88-3 Toluene ND 1.0 ug/l110-57-6 Trans-1,4-Dichloro-2-Butene ND 5.0 ug/l87-61-6 1,2,3-Trichlorobenzene ND 5.0 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/l71-55-6 1,1,1-Trichloroethane ND 1.0 ug/l79-00-5 1,1,2-Trichloroethane ND 1.0 ug/l79-01-6 Trichloroethene ND 1.0 ug/l75-69-4 Trichlorofluoromethane ND 1.0 ug/l96-18-4 1,2,3-Trichloropropane ND 5.0 ug/l95-63-6 1,2,4-Trimethylbenzene ND 1.0 ug/l108-67-8 1,3,5-Trimethylbenzene ND 1.0 ug/l75-01-4 Vinyl chloride ND 1.0 ug/l


388 of 555

MC48821

66.1.1




MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27

CAS No. Surrogate Recoveries Limits

1868-53-7 Dibromofluoromethane 110% 76-129%2037-26-5 Toluene-D8 101% 83-114%460-00-4 4-Bromofluorobenzene 102% 75-124%

389 of 555

MC48821

66.1.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSM2944-MB M82084.D 1 11/23/16 KP n/a n/a MSM2944


MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-9, MC48821-10, MC48821-11,MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16


67-64-1 Acetone ND 10 ug/kg107-13-1 Acrylonitrile ND 25 ug/kg71-43-2 Benzene ND 1.0 ug/kg108-86-1 Bromobenzene ND 5.0 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane ND 10 ug/kg78-93-3 2-Butanone (MEK) ND 10 ug/kg104-51-8 n-Butylbenzene ND 5.0 ug/kg135-98-8 sec-Butylbenzene ND 5.0 ug/kg98-06-6 tert-Butylbenzene ND 5.0 ug/kg75-15-0 Carbon disulfide ND 5.0 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane ND 10 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane ND 5.0 ug/kg95-49-8 o-Chlorotoluene ND 5.0 ug/kg106-43-4 p-Chlorotoluene ND 5.0 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 ug/kg124-48-1 Dibromochloromethane ND 5.0 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane ND 5.0 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg142-28-9 1,3-Dichloropropane ND 5.0 ug/kg594-20-7 2,2-Dichloropropane ND 5.0 ug/kg563-58-6 1,1-Dichloropropene ND 5.0 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.0 ug/kg

390 of 555

MC48821

66.1.2






10061-02-6 trans-1,3-Dichloropropene ND 2.0 ug/kg100-41-4 Ethylbenzene ND 2.0 ug/kg76-13-1 Freon 113 ND 5.0 ug/kg87-68-3 Hexachlorobutadiene ND 5.0 ug/kg591-78-6 2-Hexanone ND 5.0 ug/kg98-82-8 Isopropylbenzene ND 5.0 ug/kg99-87-6 p-Isopropyltoluene ND 5.0 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.0 ug/kg74-95-3 Methylene bromide ND 5.0 ug/kg75-09-2 Methylene chloride ND 2.0 ug/kg91-20-3 Naphthalene ND 5.0 ug/kg103-65-1 n-Propylbenzene ND 5.0 ug/kg100-42-5 Styrene ND 5.0 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 ug/kg127-18-4 Tetrachloroethene ND 2.0 ug/kg109-99-9 Tetrahydrofuran ND 10 ug/kg108-88-3 Toluene 0.78 5.0 ug/kg J110-57-6 Trans-1,4-Dichloro-2-Butene ND 10 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.0 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.0 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.0 ug/kg79-01-6 Trichloroethene ND 2.0 ug/kg75-69-4 Trichlorofluoromethane ND 2.0 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.0 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.0 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.0 ug/kg75-01-4 Vinyl chloride ND 10 ug/kg


391 of 555

MC48821

66.1.2







392 of 555

MC48821

66.1.2


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSL4388-MB L101697.D 1 11/23/16 TB n/a n/a MSL4388


MC48821-7, MC48821-8, MC48821-26


67-64-1 Acetone ND 500 ug/kg107-13-1 Acrylonitrile ND 1300 ug/kg71-43-2 Benzene ND 50 ug/kg108-86-1 Bromobenzene ND 250 ug/kg75-27-4 Bromodichloromethane ND 100 ug/kg75-25-2 Bromoform ND 100 ug/kg74-83-9 Bromomethane ND 500 ug/kg78-93-3 2-Butanone (MEK) ND 500 ug/kg104-51-8 n-Butylbenzene ND 250 ug/kg135-98-8 sec-Butylbenzene ND 250 ug/kg98-06-6 tert-Butylbenzene ND 250 ug/kg75-15-0 Carbon disulfide ND 250 ug/kg56-23-5 Carbon tetrachloride ND 100 ug/kg108-90-7 Chlorobenzene ND 100 ug/kg75-00-3 Chloroethane ND 500 ug/kg67-66-3 Chloroform ND 100 ug/kg74-87-3 Chloromethane ND 250 ug/kg95-49-8 o-Chlorotoluene ND 250 ug/kg106-43-4 p-Chlorotoluene ND 250 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 250 ug/kg124-48-1 Dibromochloromethane ND 250 ug/kg106-93-4 1,2-Dibromoethane ND 100 ug/kg95-50-1 1,2-Dichlorobenzene ND 100 ug/kg541-73-1 1,3-Dichlorobenzene ND 100 ug/kg106-46-7 1,4-Dichlorobenzene ND 100 ug/kg75-71-8 Dichlorodifluoromethane ND 250 ug/kg75-34-3 1,1-Dichloroethane ND 100 ug/kg107-06-2 1,2-Dichloroethane ND 100 ug/kg75-35-4 1,1-Dichloroethene ND 100 ug/kg156-59-2 cis-1,2-Dichloroethene ND 100 ug/kg156-60-5 trans-1,2-Dichloroethene ND 100 ug/kg78-87-5 1,2-Dichloropropane ND 100 ug/kg142-28-9 1,3-Dichloropropane ND 250 ug/kg594-20-7 2,2-Dichloropropane ND 250 ug/kg563-58-6 1,1-Dichloropropene ND 250 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 100 ug/kg

393 of 555

MC48821

66.1.3




MC48821-7, MC48821-8, MC48821-26


10061-02-6 trans-1,3-Dichloropropene ND 100 ug/kg100-41-4 Ethylbenzene ND 100 ug/kg76-13-1 Freon 113 ND 250 ug/kg87-68-3 Hexachlorobutadiene ND 250 ug/kg591-78-6 2-Hexanone ND 250 ug/kg98-82-8 Isopropylbenzene ND 250 ug/kg99-87-6 p-Isopropyltoluene ND 250 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 100 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 250 ug/kg74-95-3 Methylene bromide ND 250 ug/kg75-09-2 Methylene chloride ND 100 ug/kg91-20-3 Naphthalene ND 250 ug/kg103-65-1 n-Propylbenzene ND 250 ug/kg100-42-5 Styrene ND 250 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 100 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 250 ug/kg127-18-4 Tetrachloroethene ND 100 ug/kg109-99-9 Tetrahydrofuran ND 500 ug/kg108-88-3 Toluene ND 250 ug/kg110-57-6 Trans-1,4-Dichloro-2-Butene ND 500 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 250 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 250 ug/kg71-55-6 1,1,1-Trichloroethane ND 100 ug/kg79-00-5 1,1,2-Trichloroethane ND 100 ug/kg79-01-6 Trichloroethene ND 100 ug/kg75-69-4 Trichlorofluoromethane ND 100 ug/kg96-18-4 1,2,3-Trichloropropane ND 250 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 250 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 250 ug/kg75-01-4 Vinyl chloride ND 500 ug/kg

m,p-Xylene ND 100 ug/kg95-47-6 o-Xylene ND 100 ug/kg

394 of 555

MC48821

66.1.3




MC48821-7, MC48821-8, MC48821-26



395 of 555

MC48821

66.1.3


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSM2946-MB M82145.D 1 11/26/16 DRY n/a n/a MSM2946


MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A


67-64-1 Acetone ND 10 ug/kg107-13-1 Acrylonitrile ND 25 ug/kg71-43-2 Benzene ND 1.0 ug/kg108-86-1 Bromobenzene ND 5.0 ug/kg75-27-4 Bromodichloromethane ND 2.0 ug/kg75-25-2 Bromoform ND 2.0 ug/kg74-83-9 Bromomethane ND 10 ug/kg78-93-3 2-Butanone (MEK) ND 10 ug/kg104-51-8 n-Butylbenzene ND 5.0 ug/kg135-98-8 sec-Butylbenzene ND 5.0 ug/kg98-06-6 tert-Butylbenzene ND 5.0 ug/kg75-15-0 Carbon disulfide ND 5.0 ug/kg56-23-5 Carbon tetrachloride ND 2.0 ug/kg108-90-7 Chlorobenzene ND 2.0 ug/kg75-00-3 Chloroethane ND 10 ug/kg67-66-3 Chloroform ND 2.0 ug/kg74-87-3 Chloromethane ND 5.0 ug/kg95-49-8 o-Chlorotoluene ND 5.0 ug/kg106-43-4 p-Chlorotoluene ND 5.0 ug/kg96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 ug/kg124-48-1 Dibromochloromethane ND 5.0 ug/kg106-93-4 1,2-Dibromoethane ND 2.0 ug/kg95-50-1 1,2-Dichlorobenzene ND 2.0 ug/kg541-73-1 1,3-Dichlorobenzene ND 2.0 ug/kg106-46-7 1,4-Dichlorobenzene ND 2.0 ug/kg75-71-8 Dichlorodifluoromethane ND 5.0 ug/kg75-34-3 1,1-Dichloroethane ND 2.0 ug/kg107-06-2 1,2-Dichloroethane ND 2.0 ug/kg75-35-4 1,1-Dichloroethene ND 2.0 ug/kg156-59-2 cis-1,2-Dichloroethene ND 2.0 ug/kg156-60-5 trans-1,2-Dichloroethene ND 2.0 ug/kg78-87-5 1,2-Dichloropropane ND 2.0 ug/kg142-28-9 1,3-Dichloropropane ND 5.0 ug/kg594-20-7 2,2-Dichloropropane ND 5.0 ug/kg563-58-6 1,1-Dichloropropene ND 5.0 ug/kg10061-01-5 cis-1,3-Dichloropropene ND 2.0 ug/kg

396 of 555

MC48821

66.1.4




MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A


10061-02-6 trans-1,3-Dichloropropene ND 2.0 ug/kg100-41-4 Ethylbenzene ND 2.0 ug/kg76-13-1 Freon 113 ND 5.0 ug/kg87-68-3 Hexachlorobutadiene ND 5.0 ug/kg591-78-6 2-Hexanone ND 5.0 ug/kg98-82-8 Isopropylbenzene ND 5.0 ug/kg99-87-6 p-Isopropyltoluene ND 5.0 ug/kg1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/kg108-10-1 4-Methyl-2-pentanone (MIBK) ND 5.0 ug/kg74-95-3 Methylene bromide ND 5.0 ug/kg75-09-2 Methylene chloride ND 2.0 ug/kg91-20-3 Naphthalene 2.1 5.0 ug/kg J103-65-1 n-Propylbenzene ND 5.0 ug/kg100-42-5 Styrene ND 5.0 ug/kg630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/kg79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 ug/kg127-18-4 Tetrachloroethene ND 2.0 ug/kg109-99-9 Tetrahydrofuran ND 10 ug/kg108-88-3 Toluene 2.6 5.0 ug/kg J110-57-6 Trans-1,4-Dichloro-2-Butene ND 10 ug/kg87-61-6 1,2,3-Trichlorobenzene ND 5.0 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/kg71-55-6 1,1,1-Trichloroethane ND 2.0 ug/kg79-00-5 1,1,2-Trichloroethane ND 2.0 ug/kg79-01-6 Trichloroethene ND 2.0 ug/kg75-69-4 Trichlorofluoromethane ND 2.0 ug/kg96-18-4 1,2,3-Trichloropropane ND 5.0 ug/kg95-63-6 1,2,4-Trimethylbenzene ND 5.0 ug/kg108-67-8 1,3,5-Trimethylbenzene ND 5.0 ug/kg75-01-4 Vinyl chloride ND 10 ug/kg


397 of 555

MC48821

66.1.4




MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A



398 of 555

MC48821

66.1.4

Blank Spike Summary Page 1 of 3 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSM2944-BS M82081.D 1 11/22/16 KP n/a n/a MSM2944



Spike BSP BSPCAS No. Compound ug/kg ug/kg % Limits

67-64-1 Acetone 50 40.5 81 24-179107-13-1 Acrylonitrile 50 54.1 108 52-15971-43-2 Benzene 50 56.3 113 73-115108-86-1 Bromobenzene 50 50.9 102 76-12175-27-4 Bromodichloromethane 50 55.1 110 76-12275-25-2 Bromoform 50 50.9 102 67-15174-83-9 Bromomethane 50 40.0 80 52-13978-93-3 2-Butanone (MEK) 50 43.3 87 32-151104-51-8 n-Butylbenzene 50 49.9 100 71-124135-98-8 sec-Butylbenzene 50 50.2 100 71-12498-06-6 tert-Butylbenzene 50 51.9 104 66-12575-15-0 Carbon disulfide 50 61.7 123 57-14356-23-5 Carbon tetrachloride 50 58.9 118 73-129108-90-7 Chlorobenzene 50 49.6 99 79-12375-00-3 Chloroethane 50 40.9 82 51-15967-66-3 Chloroform 50 58.1 116 72-12274-87-3 Chloromethane 50 53.4 107 57-14395-49-8 o-Chlorotoluene 50 51.6 103 68-121106-43-4 p-Chlorotoluene 50 50.4 101 68-11996-12-8 1,2-Dibromo-3-chloropropane 50 48.3 97 52-132124-48-1 Dibromochloromethane 50 50.2 100 74-139106-93-4 1,2-Dibromoethane 50 48.7 97 76-13095-50-1 1,2-Dichlorobenzene 50 48.3 97 73-122541-73-1 1,3-Dichlorobenzene 50 48.6 97 74-119106-46-7 1,4-Dichlorobenzene 50 48.1 96 75-11875-71-8 Dichlorodifluoromethane 50 39.0 78 11-18375-34-3 1,1-Dichloroethane 50 56.7 113 70-128107-06-2 1,2-Dichloroethane 50 58.3 117 70-12675-35-4 1,1-Dichloroethene 50 56.7 113 71-136156-59-2 cis-1,2-Dichloroethene 50 59.0 118 78-128156-60-5 trans-1,2-Dichloroethene 50 52.2 104 71-13178-87-5 1,2-Dichloropropane 50 55.1 110 79-124142-28-9 1,3-Dichloropropane 50 53.2 106 78-128594-20-7 2,2-Dichloropropane 50 59.8 120 54-145563-58-6 1,1-Dichloropropene 50 58.0 116 67-12510061-01-5 cis-1,3-Dichloropropene 50 52.3 105 75-126

* = Outside of Control Limits.

399 of 555

MC48821

66.2.1






10061-02-6 trans-1,3-Dichloropropene 50 52.5 105 75-128100-41-4 Ethylbenzene 50 52.5 105 76-12276-13-1 Freon 113 50 59.7 119 70-13787-68-3 Hexachlorobutadiene 50 49.5 99 73-137591-78-6 2-Hexanone 50 42.3 85 26-16998-82-8 Isopropylbenzene 50 49.6 99 69-12499-87-6 p-Isopropyltoluene 50 49.7 99 73-1241634-04-4 Methyl Tert Butyl Ether 50 54.0 108 58-133108-10-1 4-Methyl-2-pentanone (MIBK) 50 50.0 100 43-16674-95-3 Methylene bromide 50 54.4 109 76-12575-09-2 Methylene chloride 50 63.0 126* a 74-12591-20-3 Naphthalene 50 43.9 88 39-158103-65-1 n-Propylbenzene 50 50.0 100 69-121100-42-5 Styrene 50 50.6 101 79-124630-20-6 1,1,1,2-Tetrachloroethane 50 53.1 106 75-13679-34-5 1,1,2,2-Tetrachloroethane 50 50.8 102 66-134127-18-4 Tetrachloroethene 50 49.1 98 76-125109-99-9 Tetrahydrofuran 50 48.5 97 34-177108-88-3 Toluene 50 56.6 113 76-119110-57-6 Trans-1,4-Dichloro-2-Butene 50 50.1 100 57-14087-61-6 1,2,3-Trichlorobenzene 50 47.6 95 52-146120-82-1 1,2,4-Trichlorobenzene 50 44.4 89 66-13371-55-6 1,1,1-Trichloroethane 50 58.7 117 70-13079-00-5 1,1,2-Trichloroethane 50 54.0 108 75-12479-01-6 Trichloroethene 50 53.7 107 74-12775-69-4 Trichlorofluoromethane 50 51.4 103 48-15696-18-4 1,2,3-Trichloropropane 50 51.1 102 65-13095-63-6 1,2,4-Trimethylbenzene 50 50.5 101 69-119108-67-8 1,3,5-Trimethylbenzene 50 52.9 106 69-12375-01-4 Vinyl chloride 50 43.6 87 33-166

m,p-Xylene 100 103 103 78-12295-47-6 o-Xylene 50 51.5 103 77-123


400 of 555

MC48821

66.2.1





CAS No. Surrogate Recoveries BSP Limits


(a) Outside control limits. Associated samples are non-detect for this compound.


401 of 555

MC48821

66.2.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSM2946-BS M82141.D 1 11/26/16 DRY n/a n/a MSM2946


MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A


67-64-1 Acetone 50 87.1 174 24-179107-13-1 Acrylonitrile 50 51.9 104 52-15971-43-2 Benzene 50 47.6 95 73-115108-86-1 Bromobenzene 50 43.8 88 76-12175-27-4 Bromodichloromethane 50 44.8 90 76-12275-25-2 Bromoform 50 44.0 88 67-15174-83-9 Bromomethane 50 36.3 73 52-13978-93-3 2-Butanone (MEK) 50 76.9 154* a 32-151104-51-8 n-Butylbenzene 50 51.7 103 71-124135-98-8 sec-Butylbenzene 50 49.8 100 71-12498-06-6 tert-Butylbenzene 50 47.9 96 66-12575-15-0 Carbon disulfide 50 54.5 109 57-14356-23-5 Carbon tetrachloride 50 47.7 95 73-129108-90-7 Chlorobenzene 50 43.4 87 79-12375-00-3 Chloroethane 50 39.0 78 51-15967-66-3 Chloroform 50 46.1 92 72-12274-87-3 Chloromethane 50 55.9 112 57-14395-49-8 o-Chlorotoluene 50 47.4 95 68-121106-43-4 p-Chlorotoluene 50 46.9 94 68-11996-12-8 1,2-Dibromo-3-chloropropane 50 44.2 88 52-132124-48-1 Dibromochloromethane 50 43.9 88 74-139106-93-4 1,2-Dibromoethane 50 45.3 91 76-13095-50-1 1,2-Dichlorobenzene 50 43.7 87 73-122541-73-1 1,3-Dichlorobenzene 50 43.8 88 74-119106-46-7 1,4-Dichlorobenzene 50 41.4 83 75-11875-71-8 Dichlorodifluoromethane 50 51.5 103 11-18375-34-3 1,1-Dichloroethane 50 47.9 96 70-128107-06-2 1,2-Dichloroethane 50 46.2 92 70-12675-35-4 1,1-Dichloroethene 50 55.5 111 71-136156-59-2 cis-1,2-Dichloroethene 50 52.0 104 78-128156-60-5 trans-1,2-Dichloroethene 50 46.5 93 71-13178-87-5 1,2-Dichloropropane 50 47.2 94 79-124142-28-9 1,3-Dichloropropane 50 47.4 95 78-128594-20-7 2,2-Dichloropropane 50 50.7 101 54-145563-58-6 1,1-Dichloropropene 50 49.9 100 67-12510061-01-5 cis-1,3-Dichloropropene 50 47.9 96 75-126


402 of 555

MC48821

66.2.2




MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A


10061-02-6 trans-1,3-Dichloropropene 50 45.2 90 75-128100-41-4 Ethylbenzene 50 49.0 98 76-12276-13-1 Freon 113 50 54.3 109 70-13787-68-3 Hexachlorobutadiene 50 45.8 92 73-137591-78-6 2-Hexanone 50 61.9 124 26-16998-82-8 Isopropylbenzene 50 49.7 99 69-12499-87-6 p-Isopropyltoluene 50 48.2 96 73-1241634-04-4 Methyl Tert Butyl Ether 50 54.3 109 58-133108-10-1 4-Methyl-2-pentanone (MIBK) 50 50.3 101 43-16674-95-3 Methylene bromide 50 44.7 89 76-12575-09-2 Methylene chloride 50 48.9 98 74-12591-20-3 Naphthalene 50 43.1 86 39-158103-65-1 n-Propylbenzene 50 46.6 93 69-121100-42-5 Styrene 50 50.3 101 79-124630-20-6 1,1,1,2-Tetrachloroethane 50 46.6 93 75-13679-34-5 1,1,2,2-Tetrachloroethane 50 43.3 87 66-134127-18-4 Tetrachloroethene 50 44.2 88 76-125109-99-9 Tetrahydrofuran 50 49.3 99 34-177108-88-3 Toluene 50 45.7 91 76-119110-57-6 Trans-1,4-Dichloro-2-Butene 50 47.3 95 57-14087-61-6 1,2,3-Trichlorobenzene 50 48.0 96 52-146120-82-1 1,2,4-Trichlorobenzene 50 47.6 95 66-13371-55-6 1,1,1-Trichloroethane 50 49.2 98 70-13079-00-5 1,1,2-Trichloroethane 50 45.5 91 75-12479-01-6 Trichloroethene 50 44.5 89 74-12775-69-4 Trichlorofluoromethane 50 46.3 93 48-15696-18-4 1,2,3-Trichloropropane 50 41.7 83 65-13095-63-6 1,2,4-Trimethylbenzene 50 49.0 98 69-119108-67-8 1,3,5-Trimethylbenzene 50 52.3 105 69-12375-01-4 Vinyl chloride 50 47.0 94 33-166

m,p-Xylene 100 101 101 78-12295-47-6 o-Xylene 50 52.5 105 77-123


403 of 555

MC48821

66.2.2




MC48821-17, MC48821-18, MC48821-19, MC48821-20, MC48821-21, MC48821-26A





404 of 555

MC48821

66.2.2

Blank Spike/Blank Spike Duplicate Summary Page 1 of 3 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSV1905-BS V51591.D 1 11/22/16 KP n/a n/a MSV1905MSV1905-BSD V51592.D 1 11/22/16 KP n/a n/a MSV1905


MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27

Spike BSP BSP BSD BSD LimitsCAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD

67-64-1 Acetone 50 77.4 155 73.0 146 6 24-200/25107-13-1 Acrylonitrile 50 58.1 116 55.8 112 4 47-147/2571-43-2 Benzene 50 50.7 101 49.7 99 2 66-123/25108-86-1 Bromobenzene 50 52.7 105 52.5 105 0 73-124/2575-27-4 Bromodichloromethane 50 48.5 97 47.6 95 2 68-130/2575-25-2 Bromoform 50 33.4 67 34.6 69 4 61-149/2574-83-9 Bromomethane 50 71.5 143 63.3 127 12 52-151/2578-93-3 2-Butanone (MEK) 50 69.4 139 65.7 131 5 45-171/25104-51-8 n-Butylbenzene 50 58.8 118 58.6 117 0 80-134/30135-98-8 sec-Butylbenzene 50 56.8 114 55.5 111 2 77-132/2598-06-6 tert-Butylbenzene 50 54.8 110 53.9 108 2 71-130/2575-15-0 Carbon disulfide 50 59.4 119 56.5 113 5 24-164/2556-23-5 Carbon tetrachloride 50 55.0 110 54.8 110 0 54-151/25108-90-7 Chlorobenzene 50 47.7 95 48.1 96 1 75-117/2575-00-3 Chloroethane 50 58.3 117 56.2 112 4 54-160/2567-66-3 Chloroform 50 56.9 114 54.6 109 4 65-127/2574-87-3 Chloromethane 50 84.5 169* a 82.4 165* a 3 43-154/2595-49-8 o-Chlorotoluene 50 57.0 114 55.4 111 3 71-128/25106-43-4 p-Chlorotoluene 50 56.4 113 55.9 112 1 71-125/2596-12-8 1,2-Dibromo-3-chloropropane 50 40.7 81 42.6 85 5 53-145/25124-48-1 Dibromochloromethane 50 40.9 82 41.9 84 2 67-137/25106-93-4 1,2-Dibromoethane 50 47.2 94 47.6 95 1 73-126/2595-50-1 1,2-Dichlorobenzene 50 50.7 101 49.9 100 2 75-124/25541-73-1 1,3-Dichlorobenzene 50 50.1 100 50.0 100 0 76-120/25106-46-7 1,4-Dichlorobenzene 50 50.2 100 50.0 100 0 77-117/2575-71-8 Dichlorodifluoromethane 50 73.0 146 72.0 144 1 20-161/2575-34-3 1,1-Dichloroethane 50 55.9 112 53.3 107 5 55-128/25107-06-2 1,2-Dichloroethane 50 56.1 112 56.4 113 1 68-126/2575-35-4 1,1-Dichloroethene 50 58.7 117 55.5 111 6 44-148/25156-59-2 cis-1,2-Dichloroethene 50 56.6 113 54.1 108 5 63-132/25156-60-5 trans-1,2-Dichloroethene 50 51.9 104 50.0 100 4 54-127/2578-87-5 1,2-Dichloropropane 50 52.4 105 52.0 104 1 68-123/25142-28-9 1,3-Dichloropropane 50 53.0 106 53.3 107 1 75-130/25594-20-7 2,2-Dichloropropane 50 64.4 129 62.1 124 4 47-156/25563-58-6 1,1-Dichloropropene 50 56.5 113 55.4 111 2 65-123/2510061-01-5 cis-1,3-Dichloropropene 50 46.7 93 46.7 93 0 61-145/25


405 of 555

MC48821

66.3.1




MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27


10061-02-6 trans-1,3-Dichloropropene 50 45.8 92 45.5 91 1 60-134/25100-41-4 Ethylbenzene 50 51.8 104 51.7 103 0 74-127/2576-13-1 Freon 113 50 68.1 136 66.1 132 3 39-154/2587-68-3 Hexachlorobutadiene 50 53.6 107 54.9 110 2 71-141/25591-78-6 2-Hexanone 50 70.1 140 70.7 141 1 44-166/2598-82-8 Isopropylbenzene 50 55.0 110 54.3 109 1 70-131/2599-87-6 p-Isopropyltoluene 50 57.1 114 55.6 111 3 79-131/251634-04-4 Methyl Tert Butyl Ether 50 53.8 108 53.0 106 1 59-135/25108-10-1 4-Methyl-2-pentanone (MIBK) 50 53.2 106 53.8 108 1 63-138/2574-95-3 Methylene bromide 50 51.8 104 52.6 105 2 70-124/2575-09-2 Methylene chloride 50 55.7 111 53.7 107 4 54-132/2591-20-3 Naphthalene 50 45.2 90 45.5 91 1 37-145/25103-65-1 n-Propylbenzene 50 56.6 113 55.8 112 1 71-128/25100-42-5 Styrene 50 50.5 101 51.0 102 1 76-130/25630-20-6 1,1,1,2-Tetrachloroethane 50 47.5 95 48.5 97 2 71-139/2579-34-5 1,1,2,2-Tetrachloroethane 50 54.1 108 53.5 107 1 62-130/25127-18-4 Tetrachloroethene 50 46.1 92 47.1 94 2 68-133/25109-99-9 Tetrahydrofuran 50 50.8 102 50.6 101 0 52-131/25108-88-3 Toluene 50 52.5 105 51.2 102 3 73-124/25110-57-6 Trans-1,4-Dichloro-2-Butene 50 36.7 73 37.5 75 2 26-163/2587-61-6 1,2,3-Trichlorobenzene 50 52.8 106 53.1 106 1 58-144/25120-82-1 1,2,4-Trichlorobenzene 50 50.0 100 50.4 101 1 63-137/2571-55-6 1,1,1-Trichloroethane 50 61.2 122 60.2 120 2 60-135/2579-00-5 1,1,2-Trichloroethane 50 50.8 102 50.5 101 1 72-125/2579-01-6 Trichloroethene 50 47.7 95 47.6 95 0 73-120/2575-69-4 Trichlorofluoromethane 50 67.3 135 65.3 131 3 52-152/2596-18-4 1,2,3-Trichloropropane 50 56.5 113 56.4 113 0 56-136/2595-63-6 1,2,4-Trimethylbenzene 50 55.4 111 54.3 109 2 76-125/25108-67-8 1,3,5-Trimethylbenzene 50 58.2 116 57.4 115 1 76-132/2575-01-4 Vinyl chloride 50 67.0 134 65.7 131 2 49-154/25

m,p-Xylene 100 99.6 100 99.8 100 0 73-129/2595-47-6 o-Xylene 50 49.7 99 49.5 99 0 73-128/25


406 of 555

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66.3.1




MC48821-22, MC48821-23, MC48821-24, MC48821-25, MC48821-27

CAS No. Surrogate Recoveries BSP BSD Limits

1868-53-7 Dibromofluoromethane 112% 109% 76-129%2037-26-5 Toluene-D8 103% 102% 83-114%460-00-4 4-Bromofluorobenzene 104% 102% 75-124%



407 of 555

MC48821

66.3.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchMSL4388-BS L101693.D 1 11/23/16 TB n/a n/a MSL4388MSL4388-BSD L101694.D 1 11/23/16 TB n/a n/a MSL4388


MC48821-7, MC48821-8, MC48821-26

Spike BSP BSP BSD BSD LimitsCAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD

67-64-1 Acetone 2500 1970 79 2500 100 24 24-179/25107-13-1 Acrylonitrile 2500 2020 81 2430 97 18 52-159/2571-43-2 Benzene 2500 2370 95 2350 94 1 73-115/25108-86-1 Bromobenzene 2500 2730 109 2750 110 1 76-121/2575-27-4 Bromodichloromethane 2500 2490 100 2480 99 0 76-122/2575-25-2 Bromoform 2500 2670 107 2700 108 1 67-151/2574-83-9 Bromomethane 2500 2730 109 2180 87 22 52-139/2578-93-3 2-Butanone (MEK) 2500 2220 89 2610 104 16 32-151/25104-51-8 n-Butylbenzene 2500 2890 116 2830 113 2 71-124/25135-98-8 sec-Butylbenzene 2500 2870 115 2810 112 2 71-124/2598-06-6 tert-Butylbenzene 2500 2820 113 2750 110 3 66-125/2575-15-0 Carbon disulfide 2500 2120 85 2470 99 15 57-143/2556-23-5 Carbon tetrachloride 2500 2510 100 2500 100 0 73-129/25108-90-7 Chlorobenzene 2500 2600 104 2600 104 0 79-123/2575-00-3 Chloroethane 2500 2820 113 2310 92 20 51-159/2567-66-3 Chloroform 2500 2350 94 2290 92 3 72-122/2574-87-3 Chloromethane 2500 2950 118 2430 97 19 57-143/2595-49-8 o-Chlorotoluene 2500 2730 109 2700 108 1 68-121/25106-43-4 p-Chlorotoluene 2500 2740 110 2720 109 1 68-119/2596-12-8 1,2-Dibromo-3-chloropropane 2500 2630 105 2700 108 3 52-132/25124-48-1 Dibromochloromethane 2500 2640 106 2660 106 1 74-139/25106-93-4 1,2-Dibromoethane 2500 2630 105 2680 107 2 76-130/2595-50-1 1,2-Dichlorobenzene 2500 2640 106 2640 106 0 73-122/25541-73-1 1,3-Dichlorobenzene 2500 2600 104 2600 104 0 74-119/25106-46-7 1,4-Dichlorobenzene 2500 2530 101 2540 102 0 75-118/2575-71-8 Dichlorodifluoromethane 2500 3270 131 2600 104 23 11-183/2575-34-3 1,1-Dichloroethane 2500 2120 85 2240 90 6 70-128/25107-06-2 1,2-Dichloroethane 2500 2350 94 2320 93 1 70-126/2575-35-4 1,1-Dichloroethene 2500 2040 82 2400 96 16 71-136/25156-59-2 cis-1,2-Dichloroethene 2500 2290 92 2440 98 6 78-128/25156-60-5 trans-1,2-Dichloroethene 2500 2020 81 2380 95 16 71-131/2578-87-5 1,2-Dichloropropane 2500 2460 98 2450 98 0 79-124/25142-28-9 1,3-Dichloropropane 2500 2660 106 2690 108 1 78-128/25594-20-7 2,2-Dichloropropane 2500 2710 108 2550 102 6 54-145/25563-58-6 1,1-Dichloropropene 2500 2530 101 2570 103 2 67-125/2510061-01-5 cis-1,3-Dichloropropene 2500 2710 108 2750 110 1 75-126/25


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MC48821

66.3.2




MC48821-7, MC48821-8, MC48821-26


10061-02-6 trans-1,3-Dichloropropene 2500 2650 106 2700 108 2 75-128/25100-41-4 Ethylbenzene 2500 2690 108 2690 108 0 76-122/2576-13-1 Freon 113 2500 2190 88 2460 98 12 70-137/2587-68-3 Hexachlorobutadiene 2500 2940 118 2860 114 3 73-137/25591-78-6 2-Hexanone 2500 2860 114 2850 114 0 26-169/2598-82-8 Isopropylbenzene 2500 2890 116 2870 115 1 69-124/2599-87-6 p-Isopropyltoluene 2500 2730 109 2660 106 3 73-124/251634-04-4 Methyl Tert Butyl Ether 2500 2390 96 2580 103 8 58-133/25108-10-1 4-Methyl-2-pentanone (MIBK) 2500 2580 103 2610 104 1 43-166/2574-95-3 Methylene bromide 2500 2510 100 2530 101 1 76-125/2575-09-2 Methylene chloride 2500 1940 78 2270 91 16 74-125/2591-20-3 Naphthalene 2500 2610 104 2580 103 1 39-158/25103-65-1 n-Propylbenzene 2500 2780 111 2790 112 0 69-121/25100-42-5 Styrene 2500 2630 105 2670 107 2 79-124/25630-20-6 1,1,1,2-Tetrachloroethane 2500 2670 107 2670 107 0 75-136/2579-34-5 1,1,2,2-Tetrachloroethane 2500 2470 99 2540 102 3 66-134/25127-18-4 Tetrachloroethene 2500 2550 102 2510 100 2 76-125/25109-99-9 Tetrahydrofuran 2500 2300 92 2470 99 7 34-177/25108-88-3 Toluene 2500 2460 98 2440 98 1 76-119/25110-57-6 Trans-1,4-Dichloro-2-Butene 2500 2600 104 2550 102 2 57-140/2587-61-6 1,2,3-Trichlorobenzene 2500 2700 108 2700 108 0 52-146/25120-82-1 1,2,4-Trichlorobenzene 2500 2670 107 2680 107 0 66-133/2571-55-6 1,1,1-Trichloroethane 2500 2620 105 2340 94 11 70-130/2579-00-5 1,1,2-Trichloroethane 2500 2520 101 2530 101 0 75-124/2579-01-6 Trichloroethene 2500 2440 98 2410 96 1 74-127/2575-69-4 Trichlorofluoromethane 2500 2630 105 2190 88 18 48-156/2596-18-4 1,2,3-Trichloropropane 2500 2580 103 2580 103 0 65-130/2595-63-6 1,2,4-Trimethylbenzene 2500 2990 120* a 2920 117 2 69-119/25108-67-8 1,3,5-Trimethylbenzene 2500 2940 118 2900 116 1 69-123/2575-01-4 Vinyl chloride 2500 3210 128 2680 107 18 33-166/25

m,p-Xylene 5000 5720 114 5700 114 0 78-122/2595-47-6 o-Xylene 2500 2890 116 2910 116 1 77-123/25


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66.3.2




MC48821-7, MC48821-8, MC48821-26


1868-53-7 Dibromofluoromethane 92% 89% 65-141%2037-26-5 Toluene-D8 100% 100% 65-129%460-00-4 4-Bromofluorobenzene 100% 101% 63-137%

(a) Outside control limits. Refer to Blank Spike Duplicate.


410 of 555

MC48821

66.3.2

Volatile Internal Standard Area Summary Page 1 of 1 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Check Std: MSL4388-CC4387 Injection Date: 11/23/16Lab File ID: L101692.D Injection Time: 12:38 Instrument ID: GCMSL Method: SW846 8260C

IS 1 IS 2 IS 3 IS 4 IS 5AREA RT AREA RT AREA RT AREA RT AREA RT

Check Std 194485 9.56 290915 10.45 170489 13.65 175552 16.23 49904 7.54Upper Limit a 388970 10.06 581830 10.95 340978 14.15 351104 16.73 99808 8.04Lower Limit b 97243 9.06 145458 9.95 85245 13.15 87776 15.73 24952 7.04

Lab IS 1 IS 2 IS 3 IS 4 IS 5Sample ID AREA RT AREA RT AREA RT AREA RT AREA RT

MSL4388-BS 171087 9.56 300621 10.45 172698 13.65 180532 16.23 42400 7.54MSL4388-BSD 212056 9.56 312992 10.45 179559 13.65 186197 16.23 58508 7.54MSL4388-MB 145960 9.56 226022 10.45 129453 13.65 118965 16.23 41733 7.52ZZZZZZ 149396 9.55 223211 10.45 125811 13.65 120165 16.23 42201 7.54MC48821-26 151228 9.55 228807 10.45 126119 13.65 122275 16.23 41536 7.57ZZZZZZ 119166 9.55 186806 10.45 106714 13.65 104988 16.23 44641 7.68ZZZZZZ 124390 9.55 194479 10.45 110762 13.65 104131 16.23 18537c 7.61ZZZZZZ 105118 9.56 177380 10.45 100934 13.65 95302 16.23 11596c 7.53MC48808-3 108615 9.56 172154 10.45 98551 13.65 91399 16.23 12617c 7.53ZZZZZZ 103048 9.56 162638 10.45 93693 13.65 88177 16.23 14609c 7.52MC48821-8 112037 9.56 180850 10.45 120418 13.65 135564 16.23 16306c 7.53ZZZZZZ 152573 9.55 235506 10.45 159638 13.65 165672 16.23 30702 7.53ZZZZZZ 194122 9.55 288192 10.45 183058 13.65 198904 16.22 37793 7.53MC48821-7 226256 9.55 330737 10.45 196728 13.65 207462 16.22 48555 7.53ZZZZZZ 224535 9.55 325917 10.45 203338 13.65 216569 16.22 43718 7.53MC48808-3MS 241886 9.55 347271 10.45 202908 13.65 218438 16.22 45634 7.52MC48808-3MSD 252095 9.55 354502 10.45 205129 13.65 218072 16.22 51936 7.53

IS 1 = PentafluorobenzeneIS 2 = 1,4-DifluorobenzeneIS 3 = Chlorobenzene-D5IS 4 = 1,4-Dichlorobenzene-d4IS 5 = Tert Butyl Alcohol-D9

(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Outside control limits. Target analytes not associated with this internal standard.

411 of 555

MC48821

66.4.1


Check Std: MSM2944-CC2932 Injection Date: 11/22/16Lab File ID: M82080.D Injection Time: 22:44 Instrument ID: GCMSM Method: SW846 8260C




MSM2944-BS 110859 9.77 179320 10.67 94106 13.90 101582 16.48 56394 7.69MSM2944-MB 82590 9.77 133525 10.67 72608 13.90 72932 16.49 43359 7.68ZZZZZZ 89170 9.77 150965 10.67 73174 13.89 54164 16.49 59403 7.68ZZZZZZ 85476 9.77 141545 10.67 76956 13.90 76666 16.49 65340 7.68MC48821-1 80519 9.77 131324 10.67 63475 13.90 44232c 16.48 40399 7.68MC48821-2 85577 9.77 139251 10.67 74985 13.89 74716 16.49 42841 7.68MC48821-3 69242 9.77 114325 10.67 55641 13.90 37190c 16.49 33310 7.68MC48821-4 81159 9.77 129714 10.67 70547 13.89 64247 16.49 45383 7.68MC48821-5 74711 9.77 120756 10.67 67615 13.90 65367 16.49 41626 7.68MC48821-6 85354 9.77 141382 10.67 78731 13.90 76594 16.49 43574 7.68MC48821-9 78118 9.77 124960 10.67 57854 13.90 32682c 16.48 32022 7.68MC48821-10 79464 9.77 133228 10.67 74403 13.89 72692 16.48 40515 7.68MC48821-11 71724 9.77 114973 10.67 60911 13.90 48457c 16.48 26740 7.68MC48821-12 77319 9.77 128082 10.67 70338 13.89 66234 16.49 40284 7.68MC48821-13 56698 9.77 93010 10.67 49572 13.90 37793c 16.48 30459 7.68MC48821-14 69837 9.77 118991 10.67 52860 13.89 31481c 16.48 42038 7.67MC48821-15 66571 9.77 110763 10.67 54430 13.90 34080c 16.49 35437 7.68MC48821-16 71098 9.77 118684 10.67 58813 13.90 35630c 16.49 32915 7.67


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Outside control limits due to possible matrix interference. Confirmed by reanalysis.

412 of 555

MC48821

66.4.2


Check Std: MSM2945-ICC2945 Injection Date: 11/23/16Lab File ID: M82116.D Injection Time: 16:29 Instrument ID: GCMSM Method: SW846 8260C




MSM2945-BS 115902 9.77 185121 10.67 94791 13.89 102544 16.48 60792 7.69MSM2945-MB 102380 9.77 164464 10.67 84638 13.90 86298 16.48 47370 7.68ZZZZZZ 92523 9.77 149880 10.67 72329 13.89 57717 16.48 70763 7.68ZZZZZZ 89546 9.77 144602 10.67 73958 13.89 64568 16.48 76533 7.68ZZZZZZ 82143 9.77 133511 10.67 68694 13.89 58125 16.48 57123 7.67MC48821-1 c 77110 9.77 122322 10.67 55489 13.89 33784d 16.48 28359 7.68MC48821-3 c 68525 9.77 112145 10.67 55392 13.89 39948d 16.48 35680 7.68MC48821-9 c 79432 9.77 128820 10.67 59588 13.89 39586d 16.48 31835 7.68MC48821-11 c 77655 9.77 124146 10.67 53549 13.89 29790d 16.48 35462 7.67MC48821-13 c 62581 9.77 102996 10.67 49974 13.89 36255d 16.48 29511 7.67MC48821-14 c 34151e 9.77 54979e 10.67 24301e 13.90 13452d 16.48 21808e 7.67MC48821-15 c 61229 9.77 100402 10.67 48368 13.89 30946d 16.48 35081 7.67MC48821-16 c 68119 9.77 110883 10.67 54544 13.90 36366d 16.48 26535 7.68


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Confirmation run for internal standard areas.(d) Outside control limits due to possible matrix interference. Confirmed by reanalysis.(e) Outside control limits. Sample results confirmed by reanalysis.

413 of 555

MC48821

66.4.3






MSM2946-BS 97533 9.77 160491 10.67 87541 13.90 99345 16.49 55827 7.70MSM2946-MB 80494 9.77 133727 10.67 72919 13.90 72614 16.49 41386 7.68MC48821-26A 79813 9.77 134441 10.67 72673 13.89 71641 16.49 41745 7.68ZZZZZZ 71278 9.77 121116 10.67 68197 13.89 67131 16.49 40589 7.67MC48869-1 71549 9.77 120089 10.67 67790 13.90 66673 16.48 40630 7.67ZZZZZZ 70229 9.77 117789 10.67 65666 13.90 64381 16.49 40368 7.68ZZZZZZ 59830 9.77 96810 10.67 54070 13.90 52317 16.49 29459 7.69ZZZZZZ 21571c 9.77 32791c 10.67 20825c 13.89 18737c 16.48 14804d 7.68MC48821-17 68702 9.77 114724 10.67 56817 13.90 36214c 16.48 35808 7.68MC48821-18 65730 9.77 110163 10.67 55707 13.90 33717c 16.49 36470 7.68MC48821-19 49667 9.77 74447c 10.67 24011c 13.90 8486c 16.48 30722 7.67MC48821-20 66158 9.77 112947 10.67 57855 13.89 39904c 16.49 33577 7.68MC48821-21 60112 9.77 100998 10.67 50388 13.90 34497c 16.49 28703 7.68ZZZZZZ 63992 9.77 111199 10.67 60818 13.89 53336 16.49 33482 7.67MC48869-1MS 92101 9.77 150075 10.67 81800 13.89 87979 16.48 42404 7.69MC48869-1MSD 96509 9.77 156279 10.67 81533 13.90 86106 16.48 48382 7.69


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Outside control limits due to possible matrix interference. Confirmed by reanalysis.(d) Outside control limits. Target analytes not associated with this internal standard.

414 of 555

MC48821

66.4.4






MSM2947-BS 102594 9.77 168057 10.67 92309 13.90 101185 16.48 56019 7.69MSM2947-MB 92924 9.77 155211 10.67 84057 13.89 83172 16.49 50853 7.68ZZZZZZ 4944c 9.77 7250c 10.68 4292c 13.90 3971c 16.49 1571d 7.68MC48821-17 e 74436 9.77 124019 10.67 62189 13.89 43114c 16.48 30239 7.68MC48821-18 e 68982 9.77 115971 10.67 56906 13.89 37213c 16.48 37437 7.68ZZZZZZ 79270 9.77 134889 10.67 72349 13.89 80858 16.48 39744 7.68MC48821-19 f 36586c 9.77 57327c 10.67 32899c 13.90 27626c 16.48 30745 7.68MC48821-20 e 71104 9.77 120090 10.67 60414 13.89 42786c 16.48 35279 7.68MC48821-21 e 62922 9.77 110244 10.67 57361 13.89 44858c 16.48 38327 7.68ZZZZZZ 71012 9.77 122370 10.67 69958 13.89 71472 16.48 36910 7.68ZZZZZZ 75765 9.77 128957 10.67 74636 13.89 78424 16.48 43736 7.68ZZZZZZ 78427 9.77 134255 10.67 74059 13.90 75787 16.48 40295 7.68MC48853-3 77502 9.77 128906 10.67 72357 13.90 76424 16.48 41176 7.68ZZZZZZ 79632 9.77 135798 10.67 75101 13.90 78888 16.48 37028 7.68ZZZZZZ 89743 9.77 150923 10.67 83149 13.90 86387 16.48 53601 7.68ZZZZZZ 82631 9.77 140023 10.67 75416 13.89 80161 16.48 49599 7.68ZZZZZZ 76456 9.77 125158 10.67 69315 13.89 66019 16.48 38389 7.67ZZZZZZ 74316 9.77 123690 10.67 67257 13.90 65583 16.48 38393 7.67ZZZZZZ 76487 9.77 128432 10.67 67140 13.90 53519 16.48 37093 7.68MC48853-3MS 85401 9.77 136382 10.67 75805 13.89 84914 16.48 44779 7.70MC48853-3MSD 109676 9.77 175608 10.67 95038 13.90 103663 16.48 51710 7.70


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Outside control limits due to possible matrix interference. Confirmed by reanalysis.(d) Outside control limits. Target analytes not associated with this internal standard.(e) Confirmation run for internal standard areas.(f) Confirmation run.

415 of 555

MC48821

66.4.5


Check Std: MSV1905-CC1890 Injection Date: 11/22/16Lab File ID: V51590.D Injection Time: 10:59 Instrument ID: GCMSV Method: SW846 8260C




MSV1905-BS 216481 8.93 361200 9.83 184151 13.08 216092 15.68 117658 6.87MSV1905-BSD 217774 8.93 357696 9.83 180098 13.07 215061 15.68 118401 6.87MSV1905-MB 208961 8.93 355859 9.83 175487 13.07 207814 15.68 109827 6.87ZZZZZZ 196342 8.93 332050 9.83 164052 13.07 187653 15.68 101637 6.87MC48821-25 197930 8.93 333581 9.83 164511 13.07 191223 15.68 97024 6.87MC48821-27 186887 8.93 318524 9.83 163714 13.07 187061 15.68 100566 6.87ZZZZZZ 192131 8.93 333525 9.83 165639 13.07 200925 15.68 102162 6.87ZZZZZZ 213339 8.93 358194 9.82 175070 13.07 204609 15.68 115467 6.87ZZZZZZ 205652 8.93 357685 9.82 165427 13.07 183630 15.68 103747 6.87ZZZZZZ 196285 8.93 326243 9.82 160712 13.07 184901 15.68 98121 6.87ZZZZZZ 198554 8.93 326857 9.82 159295 13.07 183804 15.68 116415 6.87ZZZZZZ 206067 8.93 345242 9.82 173739 13.07 200256 15.68 109229 6.86ZZZZZZ 189288 8.92 322296 9.82 164825 13.07 182073 15.68 99616 6.86ZZZZZZ 185310 8.92 318473 9.82 153493 13.07 180683 15.68 103185 6.86ZZZZZZ 183333 8.92 306009 9.82 151854 13.07 176279 15.68 100176 6.86ZZZZZZ 168737 8.92 296100 9.82 144664 13.07 167956 15.68 92127 6.86ZZZZZZ 171024 8.92 293720 9.82 147130 13.07 170196 15.68 93783 6.86ZZZZZZ 178227 8.92 310244 9.82 157291 13.07 180148 15.68 94652 6.86MC48821-22 177844 8.92 306566 9.82 152047 13.07 175936 15.68 92178 6.86MC48821-23 178349 8.92 308426 9.82 159432 13.07 179111 15.68 94689 6.86MC48821-24 174590 8.92 301385 9.82 152656 13.07 173603 15.68 90813 6.86


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.

416 of 555

MC48821

66.4.6

Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Method: SW846 8260C Matrix: AQ

Samples and QC shown here apply to the above method

Lab LabSample ID File ID S1 S2 S3

MC48821-22 V51612.D 120 101 101MC48821-23 V51613.D 117 104 102MC48821-24 V51614.D 119 102 102MC48821-25 V51598.D 115 102 103MC48821-27 V51599.D 116 104 104MSV1905-BS V51591.D 112 103 104MSV1905-BSD V51592.D 109 102 102MSV1905-MB V51594.D 110 101 102

Surrogate RecoveryCompounds Limits

S1 = Dibromofluoromethane 76-129%S2 = Toluene-D8 83-114%S3 = 4-Bromofluorobenzene 75-124%

417 of 555

MC48821

66.5.1


Method: SW846 8260C Matrix: SO



MC48821-1 M82128.D 106 99 131MC48821-1 M82087.D 124 103 115MC48821-2 M82088.D 117 104 96MC48821-3 M82129.D 109 102 123MC48821-3 M82089.D 127 102 122MC48821-4 M82090.D 121 108 101MC48821-5 M82091.D 127 108 96MC48821-6 M82092.D 125 107 97MC48821-7 L101714.D 86 108 102MC48821-8 L101711.D 101 109 97MC48821-9 M82130.D 110 101 122MC48821-9 M82093.D 129 103 127MC48821-10 M82094.D 129 107 95MC48821-11 M82131.D 112 98 135MC48821-11 M82095.D 126 106 106MC48821-12 M82096.D 126 107 96MC48821-13 M82132.D 115 101 116MC48821-13 M82097.D 136 108 106MC48821-14 M82133.D 120 96 134MC48821-14 M82098.D 133 102 123MC48821-15 M82134.D 120 101 129MC48821-15 M82099.D 138 104 120MC48821-16 M82100.D 132 105 123MC48821-16 M82135.D 117 102 124MC48821-17 M82152.D 120 103 128MC48821-17 M82166.D 115 101 123MC48821-18 M82153.D 122 103 133MC48821-18 M82167.D 118 99 127MC48821-19 M82154.D 129 94 155* aMC48821-19 M82169.D 121 104 107MC48821-20 M82170.D 118 101 119MC48821-20 M82155.D 120 103 121MC48821-21 M82156.D 123 103 121MC48821-21 M82171.D 128 101 112MC48821-26 L101699.D 98 99 104MC48821-26A M82146.D 114 103 102MSL4388-BS L101693.D 92 100 100MSL4388-BSD L101694.D 89 100 101MSL4388-MB L101697.D 103 101 110MSM2944-BS M82081.D 106 102 96

418 of 555

MC48821

66.5.2


Method: SW846 8260C Matrix: SO



MSM2944-MB M82084.D 120 105 96MSM2946-BS M82141.D 98 102 98MSM2946-MB M82145.D 110 103 100


S1 = Dibromofluoromethane 65-141%S2 = Toluene-D8 65-129%S3 = 4-Bromofluorobenzene 63-137%

(a) Outside control limits due to possible matrix interference. Confirmed by reanalysis.

419 of 555

MC48821

66.5.2

SGS Accutest

GC/MS Semi-volatiles

QC Data Summaries


• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries• Internal Standard Area Summaries• Surrogate Recovery Summaries


420 of 555

MC48821

7


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49183-MB R50814.D 1 11/22/16 MR 11/21/16 OP49183 MSR1895

The QC reported here applies to the following samples: Method: SW846 8270D

MC48821-1


95-57-8 2-Chlorophenol ND 250 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 490 ug/kg120-83-2 2,4-Dichlorophenol ND 490 ug/kg105-67-9 2,4-Dimethylphenol ND 490 ug/kg51-28-5 2,4-Dinitrophenol ND 490 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 490 ug/kg95-48-7 2-Methylphenol ND 490 ug/kg106-44-5 4-Methylphenol ND 490 ug/kg88-75-5 2-Nitrophenol ND 490 ug/kg100-02-7 4-Nitrophenol ND 490 ug/kg87-86-5 Pentachlorophenol ND 490 ug/kg108-95-2 Phenol ND 250 ug/kg95-95-4 2,4,5-Trichlorophenol ND 490 ug/kg88-06-2 2,4,6-Trichlorophenol ND 490 ug/kg83-32-9 Acenaphthene ND 99 ug/kg208-96-8 Acenaphthylene ND 99 ug/kg62-53-3 Aniline ND 490 ug/kg120-12-7 Anthracene ND 99 ug/kg56-55-3 Benzo(a)anthracene ND 99 ug/kg50-32-8 Benzo(a)pyrene ND 250 ug/kg205-99-2 Benzo(b)fluoranthene ND 99 ug/kg191-24-2 Benzo(g,h,i)perylene 19.3 99 ug/kg J207-08-9 Benzo(k)fluoranthene ND 99 ug/kg101-55-3 4-Bromophenyl phenyl ether ND 250 ug/kg85-68-7 Butyl benzyl phthalate ND 250 ug/kg91-58-7 2-Chloronaphthalene ND 250 ug/kg106-47-8 4-Chloroaniline ND 490 ug/kg86-74-8 Carbazole ND 99 ug/kg218-01-9 Chrysene ND 99 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 250 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 250 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 250 ug/kg7005-72-3 4-Chlorophenyl phenyl ether ND 250 ug/kg121-14-2 2,4-Dinitrotoluene ND 490 ug/kg606-20-2 2,6-Dinitrotoluene ND 490 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 490 ug/kg

421 of 555

MC48821

77.1.1




MC48821-1


53-70-3 Dibenzo(a,h)anthracene 17.1 99 ug/kg J132-64-9 Dibenzofuran ND 99 ug/kg84-74-2 Di-n-butyl phthalate ND 250 ug/kg117-84-0 Di-n-octyl phthalate 101 250 ug/kg J84-66-2 Diethyl phthalate ND 250 ug/kg131-11-3 Dimethyl phthalate ND 250 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 250 ug/kg206-44-0 Fluoranthene ND 99 ug/kg86-73-7 Fluorene ND 99 ug/kg118-74-1 Hexachlorobenzene ND 250 ug/kg87-68-3 Hexachlorobutadiene ND 250 ug/kg77-47-4 Hexachlorocyclopentadiene ND 490 ug/kg67-72-1 Hexachloroethane ND 250 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 250 ug/kg78-59-1 Isophorone ND 250 ug/kg91-57-6 2-Methylnaphthalene ND 99 ug/kg88-74-4 2-Nitroaniline ND 490 ug/kg99-09-2 3-Nitroaniline ND 490 ug/kg100-01-6 4-Nitroaniline ND 490 ug/kg91-20-3 Naphthalene ND 99 ug/kg98-95-3 Nitrobenzene ND 250 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 250 ug/kg86-30-6 N-Nitrosodiphenylamine ND 250 ug/kg82-68-8 Pentachloronitrobenzene ND 490 ug/kg85-01-8 Phenanthrene ND 99 ug/kg129-00-0 Pyrene ND 99 ug/kg110-86-1 Pyridine ND 490 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 490 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 250 ug/kg


367-12-4 2-Fluorophenol 66% 25-109%4165-62-2 Phenol-d5 69% 29-113%118-79-6 2,4,6-Tribromophenol 71% 20-141%

422 of 555

MC48821

77.1.1




MC48821-1



423 of 555

MC48821

77.1.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49189-MB W31133.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264


MC48821-22, MC48821-23, MC48821-24, MC48821-27


95-57-8 2-Chlorophenol ND 5.0 ug/l59-50-7 4-Chloro-3-methyl phenol ND 10 ug/l120-83-2 2,4-Dichlorophenol ND 10 ug/l105-67-9 2,4-Dimethylphenol ND 10 ug/l51-28-5 2,4-Dinitrophenol ND 20 ug/l534-52-1 4,6-Dinitro-o-cresol ND 10 ug/l95-48-7 2-Methylphenol ND 10 ug/l106-44-5 4-Methylphenol ND 10 ug/l88-75-5 2-Nitrophenol ND 10 ug/l100-02-7 4-Nitrophenol ND 20 ug/l87-86-5 Pentachlorophenol ND 10 ug/l108-95-2 Phenol ND 5.0 ug/l95-95-4 2,4,5-Trichlorophenol ND 10 ug/l88-06-2 2,4,6-Trichlorophenol ND 10 ug/l62-53-3 Aniline ND 10 ug/l101-55-3 4-Bromophenyl phenyl ether ND 5.0 ug/l85-68-7 Butyl benzyl phthalate ND 5.0 ug/l91-58-7 2-Chloronaphthalene ND 5.0 ug/l106-47-8 4-Chloroaniline ND 10 ug/l86-74-8 Carbazole ND 2.0 ug/l111-91-1 bis(2-Chloroethoxy)methane ND 5.0 ug/l111-44-4 bis(2-Chloroethyl)ether ND 5.0 ug/l108-60-1 bis(2-Chloroisopropyl)ether ND 5.0 ug/l7005-72-3 4-Chlorophenyl phenyl ether ND 5.0 ug/l121-14-2 2,4-Dinitrotoluene ND 10 ug/l606-20-2 2,6-Dinitrotoluene ND 10 ug/l91-94-1 3,3'-Dichlorobenzidine ND 5.0 ug/l132-64-9 Dibenzofuran ND 2.0 ug/l84-74-2 Di-n-butyl phthalate ND 5.0 ug/l117-84-0 Di-n-octyl phthalate ND 5.0 ug/l84-66-2 Diethyl phthalate ND 5.0 ug/l131-11-3 Dimethyl phthalate ND 5.0 ug/l117-81-7 bis(2-Ethylhexyl)phthalate ND 2.0 ug/l118-74-1 Hexachlorobenzene ND 5.0 ug/l87-68-3 Hexachlorobutadiene ND 5.0 ug/l77-47-4 Hexachlorocyclopentadiene ND 10 ug/l

424 of 555

MC48821

77.1.2


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49189-MB W31133.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264


MC48821-22, MC48821-23, MC48821-24, MC48821-27


67-72-1 Hexachloroethane ND 5.0 ug/l78-59-1 Isophorone ND 5.0 ug/l91-57-6 2-Methylnaphthalene ND 2.0 ug/l88-74-4 2-Nitroaniline ND 10 ug/l99-09-2 3-Nitroaniline ND 10 ug/l100-01-6 4-Nitroaniline ND 10 ug/l98-95-3 Nitrobenzene ND 5.0 ug/l621-64-7 N-Nitroso-di-n-propylamine ND 5.0 ug/l86-30-6 N-Nitrosodiphenylamine ND 10 ug/l82-68-8 Pentachloronitrobenzene ND 10 ug/l110-86-1 Pyridine ND 10 ug/l95-94-3 1,2,4,5-Tetrachlorobenzene ND 10 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/l



425 of 555

MC48821

77.1.2




MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10,MC48821-11, MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16, MC48821-17, MC48821-18,MC48821-19, MC48821-20


95-57-8 2-Chlorophenol ND 240 ug/kg59-50-7 4-Chloro-3-methyl phenol ND 480 ug/kg120-83-2 2,4-Dichlorophenol ND 480 ug/kg105-67-9 2,4-Dimethylphenol ND 480 ug/kg51-28-5 2,4-Dinitrophenol ND 480 ug/kg534-52-1 4,6-Dinitro-o-cresol ND 480 ug/kg95-48-7 2-Methylphenol ND 480 ug/kg106-44-5 4-Methylphenol ND 480 ug/kg88-75-5 2-Nitrophenol ND 480 ug/kg100-02-7 4-Nitrophenol ND 480 ug/kg87-86-5 Pentachlorophenol ND 480 ug/kg108-95-2 Phenol ND 240 ug/kg95-95-4 2,4,5-Trichlorophenol ND 480 ug/kg88-06-2 2,4,6-Trichlorophenol ND 480 ug/kg83-32-9 Acenaphthene ND 96 ug/kg208-96-8 Acenaphthylene ND 96 ug/kg62-53-3 Aniline ND 480 ug/kg120-12-7 Anthracene ND 96 ug/kg56-55-3 Benzo(a)anthracene ND 96 ug/kg50-32-8 Benzo(a)pyrene 15.7 240 ug/kg J205-99-2 Benzo(b)fluoranthene 11.5 96 ug/kg J191-24-2 Benzo(g,h,i)perylene ND 96 ug/kg207-08-9 Benzo(k)fluoranthene 14.9 96 ug/kg J101-55-3 4-Bromophenyl phenyl ether ND 240 ug/kg85-68-7 Butyl benzyl phthalate ND 240 ug/kg91-58-7 2-Chloronaphthalene ND 240 ug/kg106-47-8 4-Chloroaniline ND 480 ug/kg86-74-8 Carbazole ND 96 ug/kg218-01-9 Chrysene ND 96 ug/kg111-91-1 bis(2-Chloroethoxy)methane ND 240 ug/kg111-44-4 bis(2-Chloroethyl)ether ND 240 ug/kg108-60-1 bis(2-Chloroisopropyl)ether ND 240 ug/kg7005-72-3 4-Chlorophenyl phenyl ether ND 240 ug/kg121-14-2 2,4-Dinitrotoluene ND 480 ug/kg606-20-2 2,6-Dinitrotoluene ND 480 ug/kg91-94-1 3,3'-Dichlorobenzidine ND 480 ug/kg

426 of 555

MC48821

77.1.3






53-70-3 Dibenzo(a,h)anthracene ND 96 ug/kg132-64-9 Dibenzofuran ND 96 ug/kg84-74-2 Di-n-butyl phthalate 19.5 240 ug/kg J117-84-0 Di-n-octyl phthalate 105 240 ug/kg J84-66-2 Diethyl phthalate ND 240 ug/kg131-11-3 Dimethyl phthalate ND 240 ug/kg117-81-7 bis(2-Ethylhexyl)phthalate ND 240 ug/kg206-44-0 Fluoranthene ND 96 ug/kg86-73-7 Fluorene ND 96 ug/kg118-74-1 Hexachlorobenzene ND 240 ug/kg87-68-3 Hexachlorobutadiene ND 240 ug/kg77-47-4 Hexachlorocyclopentadiene ND 480 ug/kg67-72-1 Hexachloroethane ND 240 ug/kg193-39-5 Indeno(1,2,3-cd)pyrene ND 240 ug/kg78-59-1 Isophorone ND 240 ug/kg91-57-6 2-Methylnaphthalene ND 96 ug/kg88-74-4 2-Nitroaniline ND 480 ug/kg99-09-2 3-Nitroaniline ND 480 ug/kg100-01-6 4-Nitroaniline ND 480 ug/kg91-20-3 Naphthalene ND 96 ug/kg98-95-3 Nitrobenzene ND 240 ug/kg621-64-7 N-Nitroso-di-n-propylamine ND 240 ug/kg86-30-6 N-Nitrosodiphenylamine ND 240 ug/kg82-68-8 Pentachloronitrobenzene ND 480 ug/kg85-01-8 Phenanthrene ND 96 ug/kg129-00-0 Pyrene ND 96 ug/kg110-86-1 Pyridine ND 480 ug/kg95-94-3 1,2,4,5-Tetrachlorobenzene ND 480 ug/kg120-82-1 1,2,4-Trichlorobenzene ND 240 ug/kg



427 of 555

MC48821

77.1.3







428 of 555

MC48821

77.1.3


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49190-MB I103755.D 1 11/29/16 AA 11/22/16 OP49190 MSI3935

The QC reported here applies to the following samples: Method: SW846 8270D BY SIM

MC48821-22, MC48821-23, MC48821-24, MC48821-27





429 of 555

MC48821

77.1.4


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49195-BS R50919.D 1 11/29/16 MR 11/23/16 OP49195 MSR1899




95-57-8 2-Chlorophenol 2480 2140 86 39-10459-50-7 4-Chloro-3-methyl phenol 2480 2180 88 51-110120-83-2 2,4-Dichlorophenol 2480 2240 90 47-109105-67-9 2,4-Dimethylphenol 2480 2100 85 43-10551-28-5 2,4-Dinitrophenol 2480 1110 45 10-130534-52-1 4,6-Dinitro-o-cresol 2480 1910 77 16-14095-48-7 2-Methylphenol 2480 2200 89 40-105106-44-5 4-Methylphenol 4960 4300 87 38-11488-75-5 2-Nitrophenol 2480 2080 84 41-112100-02-7 4-Nitrophenol 2480 2390 96 28-13487-86-5 Pentachlorophenol 2480 1820 73 22-123108-95-2 Phenol 2480 2120 85 40-10795-95-4 2,4,5-Trichlorophenol 2480 2530 102 54-11588-06-2 2,4,6-Trichlorophenol 2480 2490 100 51-11083-32-9 Acenaphthene 2480 2400 97 49-108208-96-8 Acenaphthylene 2480 2240 90 37-10262-53-3 Aniline 2480 1150 46 10-90120-12-7 Anthracene 2480 2300 93 54-11156-55-3 Benzo(a)anthracene 2480 2430 98 56-11750-32-8 Benzo(a)pyrene 2480 2200 89 57-117205-99-2 Benzo(b)fluoranthene 2480 2210 89 55-122191-24-2 Benzo(g,h,i)perylene 2480 2010 81 52-123207-08-9 Benzo(k)fluoranthene 2480 2250 91 54-117101-55-3 4-Bromophenyl phenyl ether 2480 2730 110 54-11885-68-7 Butyl benzyl phthalate 2480 2850 115 54-12191-58-7 2-Chloronaphthalene 2480 2450 99 46-114106-47-8 4-Chloroaniline 2480 1230 50 12-8886-74-8 Carbazole 2480 2400 97 56-116218-01-9 Chrysene 2480 2320 94 56-114111-91-1 bis(2-Chloroethoxy)methane 2480 2090 84 41-106111-44-4 bis(2-Chloroethyl)ether 2480 2290 92 28-113108-60-1 bis(2-Chloroisopropyl)ether 2480 2390 96 30-1327005-72-3 4-Chlorophenyl phenyl ether 2480 2840 115* a 54-114121-14-2 2,4-Dinitrotoluene 2480 2700 109 50-121606-20-2 2,6-Dinitrotoluene 2480 2510 101 52-11591-94-1 3,3'-Dichlorobenzidine 2480 1450 58 17-120


430 of 555

MC48821

77.2.1






53-70-3 Dibenzo(a,h)anthracene 2480 2010 81 54-121132-64-9 Dibenzofuran 2480 2440 98 52-10984-74-2 Di-n-butyl phthalate 2480 2650 107 55-113117-84-0 Di-n-octyl phthalate 2480 2440 98 53-12684-66-2 Diethyl phthalate 2480 2820 114* a 54-111131-11-3 Dimethyl phthalate 2480 2790 112* a 53-111117-81-7 bis(2-Ethylhexyl)phthalate 2480 2560 103 55-125206-44-0 Fluoranthene 2480 2440 98 55-11686-73-7 Fluorene 2480 2620 106 52-111118-74-1 Hexachlorobenzene 2480 2490 100 52-11787-68-3 Hexachlorobutadiene 2480 2180 88 36-10877-47-4 Hexachlorocyclopentadiene 2480 1380 56 10-9967-72-1 Hexachloroethane 2480 2100 85 33-100193-39-5 Indeno(1,2,3-cd)pyrene 2480 1990 80 55-12078-59-1 Isophorone 2480 2190 88 37-10191-57-6 2-Methylnaphthalene 2480 2200 89 38-11488-74-4 2-Nitroaniline 2480 2530 102 55-12099-09-2 3-Nitroaniline 2480 1770 71 31-103100-01-6 4-Nitroaniline 2480 2270 92 50-11291-20-3 Naphthalene 2480 2920 118 27-12898-95-3 Nitrobenzene 2480 2080 84 33-108621-64-7 N-Nitroso-di-n-propylamine 2480 2350 95 37-11286-30-6 N-Nitrosodiphenylamine 2480 2360 95 47-11482-68-8 Pentachloronitrobenzene 2480 2460 99 50-12585-01-8 Phenanthrene 2480 2430 98 54-112129-00-0 Pyrene 2480 2640 106 54-118110-86-1 Pyridine 2480 1530 62 23-8195-94-3 1,2,4,5-Tetrachlorobenzene 2480 2290 92 43-113120-82-1 1,2,4-Trichlorobenzene 2480 2360 95 38-105




431 of 555

MC48821

77.2.1







(a) Outside control limits. Blank Spike meets program technical requirements.


432 of 555

MC48821

77.2.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49183-BS R50815.D 1 11/22/16 MR 11/21/16 OP49183 MSR1895OP49183-BSD R50823.D 1 11/22/16 MR 11/21/16 OP49183 MSR1895


MC48821-1


95-57-8 2-Chlorophenol 2490 1640 66 1780 74 8 39-104/3059-50-7 4-Chloro-3-methyl phenol 2490 1900 76 1850 76 3 51-110/30120-83-2 2,4-Dichlorophenol 2490 1890 76 1890 78 0 47-109/30105-67-9 2,4-Dimethylphenol 2490 1820 73 1820 75 0 43-105/3051-28-5 2,4-Dinitrophenol 2490 1390 56 557 23 86* a 10-130/30534-52-1 4,6-Dinitro-o-cresol 2490 1920 77 736 30 89* a 16-140/3095-48-7 2-Methylphenol 2490 1740 70 1870 77 7 40-105/30106-44-5 4-Methylphenol 4970 3530 71 3620 75 3 38-114/3088-75-5 2-Nitrophenol 2490 1670 67 1730 72 4 41-112/30100-02-7 4-Nitrophenol 2490 2290 92 1890 78 19 28-134/3087-86-5 Pentachlorophenol 2490 1770 71 1660 69 6 22-123/30108-95-2 Phenol 2490 1630 66 1720 71 5 40-107/3095-95-4 2,4,5-Trichlorophenol 2490 2230 90 2150 89 4 54-115/3088-06-2 2,4,6-Trichlorophenol 2490 2180 88 2110 87 3 51-110/3083-32-9 Acenaphthene 2490 2100 84 1960 81 7 49-108/30208-96-8 Acenaphthylene 2490 1930 78 1850 76 4 37-102/3062-53-3 Aniline 2490 769 31 693 29 10 10-90/30120-12-7 Anthracene 2490 2020 81 1900 79 6 54-111/3056-55-3 Benzo(a)anthracene 2490 2110 85 2020 84 4 56-117/3050-32-8 Benzo(a)pyrene 2490 2090 84 1960 81 6 57-117/30205-99-2 Benzo(b)fluoranthene 2490 2080 84 1880 78 10 55-122/30191-24-2 Benzo(g,h,i)perylene 2490 2130 86 1880 78 12 52-123/30207-08-9 Benzo(k)fluoranthene 2490 2080 84 1950 81 6 54-117/30101-55-3 4-Bromophenyl phenyl ether 2490 2380 96 2250 93 6 54-118/3085-68-7 Butyl benzyl phthalate 2490 2290 92 2250 93 2 54-121/3091-58-7 2-Chloronaphthalene 2490 2090 84 2000 83 4 46-114/30106-47-8 4-Chloroaniline 2490 707 28 598 25 17 12-88/3086-74-8 Carbazole 2490 2100 84 1970 81 6 56-116/30218-01-9 Chrysene 2490 2060 83 1940 80 6 56-114/30111-91-1 bis(2-Chloroethoxy)methane 2490 1690 68 1720 71 2 41-106/30111-44-4 bis(2-Chloroethyl)ether 2490 1650 66 1810 75 9 28-113/30108-60-1 bis(2-Chloroisopropyl)ether 2490 1760 71 1960 81 11 30-132/307005-72-3 4-Chlorophenyl phenyl ether 2490 2500 101 2330 96 7 54-114/30121-14-2 2,4-Dinitrotoluene 2490 2400 97 2230 92 7 50-121/30606-20-2 2,6-Dinitrotoluene 2490 2250 90 2100 87 7 52-115/3091-94-1 3,3'-Dichlorobenzidine 2490 856 34 1340 55 44* a 17-120/30


433 of 555

MC48821

77.3.1




MC48821-1


53-70-3 Dibenzo(a,h)anthracene 2490 2080 84 1920 79 8 54-121/30132-64-9 Dibenzofuran 2490 2190 88 2010 83 9 52-109/3084-74-2 Di-n-butyl phthalate 2490 2300 93 2200 91 4 55-113/30117-84-0 Di-n-octyl phthalate 2490 2050 82 1970 81 4 53-126/3084-66-2 Diethyl phthalate 2490 2480 100 2370 98 5 54-111/30131-11-3 Dimethyl phthalate 2490 2460 99 2330 96 5 53-111/30117-81-7 bis(2-Ethylhexyl)phthalate 2490 2140 86 2150 89 0 55-125/30206-44-0 Fluoranthene 2490 2210 89 2040 84 8 55-116/3086-73-7 Fluorene 2490 2330 94 2160 89 8 52-111/30118-74-1 Hexachlorobenzene 2490 2200 88 2080 86 6 52-117/3087-68-3 Hexachlorobutadiene 2490 1680 68 1690 70 1 36-108/3077-47-4 Hexachlorocyclopentadiene 2490 1310 53 176 7* b 153* b 10-99/3067-72-1 Hexachloroethane 2490 1480 60 1370 57 8 33-100/30193-39-5 Indeno(1,2,3-cd)pyrene 2490 2090 84 1910 79 9 55-120/3078-59-1 Isophorone 2490 1800 72 1830 76 2 37-101/3091-57-6 2-Methylnaphthalene 2490 1810 73 1810 75 0 38-114/3088-74-4 2-Nitroaniline 2490 2160 87 2090 86 3 55-120/3099-09-2 3-Nitroaniline 2490 1200 48 1110 46 8 31-103/30100-01-6 4-Nitroaniline 2490 2000 80 1670 69 18 50-112/3091-20-3 Naphthalene 2490 2080 84 2360 98 13 27-128/3098-95-3 Nitrobenzene 2490 1620 65 1700 70 5 33-108/30621-64-7 N-Nitroso-di-n-propylamine 2490 1960 79 1950 81 1 37-112/3086-30-6 N-Nitrosodiphenylamine 2490 2020 81 1950 81 4 47-114/3082-68-8 Pentachloronitrobenzene 2490 2270 91 2090 86 8 50-125/3085-01-8 Phenanthrene 2490 2130 86 2000 83 6 54-112/30129-00-0 Pyrene 2490 2160 87 2060 85 5 54-118/30110-86-1 Pyridine 2490 996 40 1150 48 14 23-81/3095-94-3 1,2,4,5-Tetrachlorobenzene 2490 1940 78 1870 77 4 43-113/30120-82-1 1,2,4-Trichlorobenzene 2490 1800 72 1850 76 3 38-105/30


367-12-4 2-Fluorophenol 56% 64% 25-109%4165-62-2 Phenol-d5 62% 68% 29-113%118-79-6 2,4,6-Tribromophenol 76% 74% 20-141%


434 of 555

MC48821

77.3.1




MC48821-1


4165-60-0 Nitrobenzene-d5 57% 62% 27-115%321-60-8 2-Fluorobiphenyl 74% 73% 34-118%1718-51-0 Terphenyl-d14 78% 76% 42-139%

(a) Outside control limits. Individual spike recoveries within acceptance limits.(b) Outside control limits. Refer to Blank Spike.


435 of 555

MC48821

77.3.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49189-BS W31134.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264OP49189-BSD W31135.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264


MC48821-22, MC48821-23, MC48821-24, MC48821-27


95-57-8 2-Chlorophenol 50 43.5 87 45.0 90 3 39-100/2059-50-7 4-Chloro-3-methyl phenol 50 44.9 90 46.8 94 4 43-112/20120-83-2 2,4-Dichlorophenol 50 52.1 104 49.2 98 6 44-113/20105-67-9 2,4-Dimethylphenol 50 26.8 54 34.3 69 25* a 21-108/2051-28-5 2,4-Dinitrophenol 50 52.9 106 55.7 111 5 22-128/20534-52-1 4,6-Dinitro-o-cresol 50 58.1 116 61.8 124 6 42-132/2095-48-7 2-Methylphenol 50 33.3 67 39.4 79 17 34-91/20106-44-5 4-Methylphenol 100 62.6 63 74.4 74 17 31-90/2088-75-5 2-Nitrophenol 50 53.3 107 49.4 99 8 40-118/20100-02-7 4-Nitrophenol 50 17.1 34 23.7 47 32* a 10-71/2087-86-5 Pentachlorophenol 50 44.8 90 46.0 92 3 33-123/20108-95-2 Phenol 50 16.3 33 20.8 42 24* a 11-57/2095-95-4 2,4,5-Trichlorophenol 50 58.9 118 58.2 116 1 50-122/2088-06-2 2,4,6-Trichlorophenol 50 57.5 115 55.9 112 3 48-118/2062-53-3 Aniline 50 29.7 59 22.2 44 29* a 18-90/20101-55-3 4-Bromophenyl phenyl ether 50 66.4 133* a 68.4 137* a 3 55-126/2085-68-7 Butyl benzyl phthalate 50 58.9 118 60.2 120 2 56-124/2091-58-7 2-Chloronaphthalene 50 60.1 120 57.0 114 5 45-123/20106-47-8 4-Chloroaniline 50 47.1 94 41.8 84 12 35-111/2086-74-8 Carbazole 50 56.0 112 58.5 117 4 60-121/20111-91-1 bis(2-Chloroethoxy)methane 50 46.7 93 43.4 87 7 41-117/20111-44-4 bis(2-Chloroethyl)ether 50 46.8 94 44.6 89 5 31-114/20108-60-1 bis(2-Chloroisopropyl)ether 50 44.4 89 41.2 82 7 33-135/207005-72-3 4-Chlorophenyl phenyl ether 50 70.8 142* a 70.9 142* a 0 52-124/20121-14-2 2,4-Dinitrotoluene 50 65.2 130* a 68.5 137* a 5 52-128/20606-20-2 2,6-Dinitrotoluene 50 63.7 127* a 64.2 128* a 1 50-126/2091-94-1 3,3'-Dichlorobenzidine 50 40.0 80 42.5 85 6 46-134/20132-64-9 Dibenzofuran 50 59.2 118 57.8 116 2 51-118/2084-74-2 Di-n-butyl phthalate 50 61.4 123* a 64.7 129* a 5 57-120/20117-84-0 Di-n-octyl phthalate 50 49.2 98 51.1 102 4 58-125/2084-66-2 Diethyl phthalate 50 65.6 131* a 67.4 135* a 3 40-125/20131-11-3 Dimethyl phthalate 50 65.6 131 67.7 135 3 10-145/20117-81-7 bis(2-Ethylhexyl)phthalate 50 53.8 108 55.8 112 4 60-126/20118-74-1 Hexachlorobenzene 50 61.9 124 64.0 128* a 3 53-127/2087-68-3 Hexachlorobutadiene 50 57.8 116* a 51.8 104 11 17-110/2077-47-4 Hexachlorocyclopentadiene 50 30.6 61 29.2 58 5 10-75/20


436 of 555

MC48821

77.3.2


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49189-BS W31134.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264OP49189-BSD W31135.D 1 11/29/16 MR 11/22/16 OP49189 MSW1264


MC48821-22, MC48821-23, MC48821-24, MC48821-27


67-72-1 Hexachloroethane 50 50.7 101* a 45.7 91 10 15-98/2078-59-1 Isophorone 50 50.1 100 46.2 92 8 36-106/2091-57-6 2-Methylnaphthalene 50 56.1 112 52.1 104 7 41-112/2088-74-4 2-Nitroaniline 50 59.0 118 59.8 120 1 52-130/2099-09-2 3-Nitroaniline 50 53.5 107 52.7 105 2 47-120/20100-01-6 4-Nitroaniline 50 54.4 109 54.5 109 0 51-121/2098-95-3 Nitrobenzene 50 47.3 95 44.4 89 6 27-120/20621-64-7 N-Nitroso-di-n-propylamine 50 51.9 104 48.2 96 7 37-123/2086-30-6 N-Nitrosodiphenylamine 50 54.5 109 57.8 116* a 6 50-112/2082-68-8 Pentachloronitrobenzene 50 56.5 113 59.9 120 6 54-129/20110-86-1 Pyridine 50 22.0 44 10 20 75* a 10-72/2095-94-3 1,2,4,5-Tetrachlorobenzene 50 58.3 117 54.1 108 7 39-119/20120-82-1 1,2,4-Trichlorobenzene 50 61.8 124* a 56.7 113* a 9 27-107/20


367-12-4 2-Fluorophenol 42% 52% 10-80%4165-62-2 Phenol-d5 26% 35% 10-72%118-79-6 2,4,6-Tribromophenol 106% 112% 42-134%4165-60-0 Nitrobenzene-d5 85% 78% 25-117%321-60-8 2-Fluorobiphenyl 94% 88% 24-112%1718-51-0 Terphenyl-d14 102% 103% 48-133%

(a) Outside control limits. Meets program technical requirements.


437 of 555

MC48821

77.3.2


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49190-BS I103756.D 1 11/29/16 AA 11/22/16 OP49190 MSI3935OP49190-BSD I103757.D 1 11/29/16 AA 11/22/16 OP49190 MSI3935

The QC reported here applies to the following samples: Method: SW846 8270D BY SIM

MC48821-22, MC48821-23, MC48821-24, MC48821-27


83-32-9 Acenaphthene 50 44.7 89 41.1 82 8 45-116/30208-96-8 Acenaphthylene 50 45.3 91 41.2 82 9 34-110/30120-12-7 Anthracene 50 46.4 93 44.6 89 4 50-117/3056-55-3 Benzo(a)anthracene 50 52.7 105 51.5 103 2 55-139/3050-32-8 Benzo(a)pyrene 50 47.2 94 46.3 93 2 48-131/30205-99-2 Benzo(b)fluoranthene 50 47.8 96 47.0 94 2 49-141/30191-24-2 Benzo(g,h,i)perylene 50 49.0 98 47.8 96 2 60-130/30207-08-9 Benzo(k)fluoranthene 50 46.6 93 45.0 90 3 49-133/30218-01-9 Chrysene 50 46.3 93 44.7 89 4 52-128/3053-70-3 Dibenzo(a,h)anthracene 50 50.5 101 49.2 98 3 60-136/30206-44-0 Fluoranthene 50 48.6 97 46.7 93 4 46-132/3086-73-7 Fluorene 50 43.6 87 41.0 82 6 53-120/30193-39-5 Indeno(1,2,3-cd)pyrene 50 49.2 98 48.2 96 2 57-134/3091-57-6 2-Methylnaphthalene 50 43.8 88 38.8 78 12 36-111/3091-20-3 Naphthalene 50 44.9 90 40.4 81 11 32-116/3085-01-8 Phenanthrene 50 42.9 86 42.6 85 1 50-120/30129-00-0 Pyrene 50 48.2 96 46.3 93 4 48-127/30


4165-60-0 Nitrobenzene-d5 90% 81% 26-121%321-60-8 2-Fluorobiphenyl 76% 66% 28-107%1718-51-0 Terphenyl-d14 87% 83% 29-129%


438 of 555

MC48821

77.3.3

Semivolatile Internal Standard Area Summary Page 1 of 1 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Check Std: MSI3935-CC3929 Injection Date: 11/29/16Lab File ID: I103752.D Injection Time: 08:25 Instrument ID: GCMSI Method: SW846 8270D BY SIM

IS 1 IS 2 IS 3 IS 4 IS 5 IS 6AREA RT AREA RT AREA RT AREA RT AREA RT AREA RT

Check Std 23885 4.22 68550 5.26 57070 6.79 61793 8.09 49187 11.15 90795 14.44Upper Limit a 47770 4.72 137100 5.76 114140 7.29 123586 8.59 98374 11.65 181590 14.94Lower Limit b 11943 3.72 34275 4.76 28535 6.29 30897 7.59 24594 10.65 45398 13.94

Lab IS 1 IS 2 IS 3 IS 4 IS 5 IS 6Sample ID AREA RT AREA RT AREA RT AREA RT AREA RT AREA RT

ZZZZZZ 20681 4.22 61073 5.26 48059 6.79 55783 8.09 41405 11.15 78185 14.44ZZZZZZ 24613 4.22 71872 5.27 57124 6.79 72858 8.09 52807 11.15 106794 14.44OP49190-MB 23943 4.22 70327 5.26 54245 6.79 62705 8.09 48028 11.15 93139 14.44OP49190-BS 22718 4.23 68191 5.27 52091 6.79 59309 8.09 48184 11.16 94173 14.44OP49190-BSD 24340 4.23 72745 5.27 56117 6.79 63760 8.10 52407 11.16 103009 14.44MC48821-22 24485 4.22 73094 5.26 55908 6.79 63957 8.09 50057 11.15 97965 14.44MC48821-23 20842 4.23 62456 5.26 49240 6.79 57726 8.09 45135 11.15 89543 14.44MC48821-24 23250 4.22 70172 5.26 53896 6.79 61771 8.09 47844 11.15 94714 14.44MC48821-27 22169 4.22 65629 5.26 50675 6.79 58847 8.09 45200 11.15 89038 14.44ZZZZZZ 23697 4.22 70123 5.26 55017 6.79 63125 8.09 50566 11.15 104914 14.44ZZZZZZ 25297 4.22 74839 5.26 57930 6.79 67304 8.09 52281 11.15 105943 14.44ZZZZZZ 22451 4.23 66854 5.26 51950 6.79 61515 8.09 47663 11.15 97500 14.44ZZZZZZ 24718 4.22 75693 5.27 59300 6.79 65247 8.10 52573 11.16 109874 14.44ZZZZZZ 22209 4.23 66681 5.26 52257 6.79 60811 8.09 48584 11.15 99703 14.44ZZZZZZ 21282 4.23 63840 5.26 49678 6.79 57502 8.09 46431 11.15 94397 14.44ZZZZZZ 23180 4.22 68933 5.26 53043 6.79 60222 8.09 47604 11.15 94519 14.44ZZZZZZ 24450 4.23 71893 5.27 54750 6.79 62545 8.09 47866 11.15 94611 14.44ZZZZZZ 21744 4.23 64996 5.26 49773 6.79 57788 8.09 44722 11.15 87685 14.44ZZZZZZ 21440 4.22 64940 5.26 49687 6.79 56728 8.09 43916 11.15 85143 14.44ZZZZZZ 21783 4.23 64792 5.26 50942 6.79 58437 8.09 45510 11.15 87339 14.44

IS 1 = 1,4-Dichlorobenzene-d4IS 2 = Naphthalene-d8IS 3 = Acenaphthene-D10IS 4 = Phenanthrene-d10IS 5 = Chrysene-d12IS 6 = Perylene-d12


439 of 555

MC48821

77.4.1


Check Std: MSR1895-CC1877 Injection Date: 11/22/16Lab File ID: R50813.D Injection Time: 16:46 Instrument ID: GCMSR Method: SW846 8270D




OP49183-MB 442881 4.02 1658006 5.07 953019 6.59 1830497 7.87 1893296 10.72 1665222 13.85OP49183-BS 469748 4.02 1757106 5.07 1007925 6.60 1932558 7.88 2023808 10.73 1769541 13.85ZZZZZZ 365129 4.02 1338745 5.07 755251 6.59 1420945 7.88 1435858 10.73 1340699 13.86ZZZZZZ 444319 4.02 1630308 5.07 912299 6.59 1732444 7.87 1763604 10.72 1628508 13.85ZZZZZZ 346799 4.02 1273679 5.07 714823 6.59 1378088 7.87 1380865 10.72 1257437 13.84ZZZZZZ 494355 4.02 1837234 5.07 1042651 6.59 1996592 7.87 2045760 10.73 1813592 13.86OP49183-MS 369873 4.02 1399916 5.07 798288 6.60 1491727 7.88 1629629 10.74 1513584 13.89OP49183-MSD 395864 4.02 1489266 5.07 843534 6.60 1585334 7.88 1739618 10.74 1560459 13.91MC48772-6 406330 4.02 1538491 5.07 884275 6.60 1664870 7.88 1792170 10.74 1616890 13.89OP49183-BSD 404112 4.03 1541567 5.08 883484 6.60 1636244 7.88 1651436 10.74 1523348 13.87ZZZZZZ 418665 4.03 1707268 5.09 1025410 6.64 1690879 7.93 1693121 10.75 1542946 13.88ZZZZZZ 411072 4.03 1779867 5.09 1104437 6.63 1842598 7.92 1752524 10.75 1540971 13.88OP49128-MB 337337 4.02 1246421 5.07 695240 6.60 1312203 7.88 1322186 10.73 1253551 13.86OP49128-BS 331400 4.02 1242107 5.07 698419 6.60 1297532 7.88 1321172 10.74 1251661 13.86OP49128-MS 449496 4.02 1646962 5.08 931828 6.60 1765873 7.88 1819173 10.74 1670746 13.87OP49128-MSD 378161 4.02 1405494 5.07 807795 6.60 1471535 7.88 1512622 10.74 1445826 13.87MC48662-15 316416 4.02 1175688 5.07 670050 6.60 1275163 7.88 1350302 10.73 1276217 13.86ZZZZZZ 444088 4.02 1606534 5.07 898509 6.60 1701997 7.88 1749114 10.73 1684518 13.87ZZZZZZ 320692 4.02 1177960 5.07 661577 6.60 1247959 7.88 1289818 10.73 1240312 13.85ZZZZZZ 406748 4.02 1500316 5.07 842506 6.60 1589983 7.88 1639969 10.73 1555049 13.86ZZZZZZ 329722 4.02 1218991 5.07 689182 6.60 1303403 7.88 1377754 10.73 1313747 13.86ZZZZZZ 434848 4.02 1568789 5.07 890859 6.60 1736381 7.88 1804989 10.73 1683960 13.86ZZZZZZ 341724 4.02 1250594 5.07 703415 6.60 1336196 7.88 1373101 10.73 1314757 13.85ZZZZZZ 408645 4.02 1494516 5.07 849680 6.60 1614521 7.88 1733455 10.73 1664020 13.86ZZZZZZ 335700 4.02 1245615 5.07 695048 6.60 1337908 7.88 1397704 10.73 1373911 13.86



440 of 555

MC48821

77.4.2






OP49206-MB 359604 4.02 1323342 5.07 738955 6.60 1385113 7.88 1405713 10.74 1279542 13.87OP49206-BS 405401 4.02 1460227 5.08 800841 6.60 1447207 7.88 1453787 10.74 1306366 13.87OP49206-BSD 385196 4.02 1383847 5.07 765605 6.60 1410910 7.88 1427661 10.74 1290728 13.87ZZZZZZ 362073 4.02 1339642 5.07 748017 6.60 1415194 7.88 1424406 10.74 1292782 13.87ZZZZZZ 381782 4.02 1410937 5.07 788667 6.60 1468850 7.88 1503286 10.74 1387592 13.87OP49119-LB1 382462 4.02 1397452 5.07 786120 6.60 1472909 7.88 1477319 10.74 1354159 13.87OP49119-MB1 382462 4.02 1397452 5.07 786120 6.60 1472909 7.88 1477319 10.74 1354159 13.87OP49119-BS1 380613 4.02 1364424 5.07 753507 6.60 1379734 7.88 1391736 10.74 1256937 13.87OP49119-LS1 383349 4.02 1340179 5.08 734481 6.60 1322282 7.88 1333458 10.74 1194339 13.87ZZZZZZ 365556 4.02 1365817 5.07 771076 6.60 1464762 7.88 1503809 10.73 1387542 13.87ZZZZZZ 362593 4.02 1354756 5.07 781132 6.60 1501737 7.88 1543719 10.74 1399274 13.87ZZZZZZ 358911 4.02 1326064 5.07 762332 6.60 1476428 7.88 1511962 10.73 1376259 13.87MC48821-1 471241 4.02 1704740 5.07 931631 6.60 1616894 7.88 1441487 10.73 1252121 13.87ZZZZZZ 476254 4.02 1701587 5.07 905816 6.60 1559197 7.88 1443103 10.74 1348700 13.88ZZZZZZ 416700 4.02 1484765 5.07 790950 6.60 1398073 7.88 1356919 10.74 1306853 13.87ZZZZZZ 478407 4.02 1713884 5.07 895969 6.60 1544766 7.88 1459009 10.74 1364189 13.89ZZZZZZ 467051 4.02 1667771 5.07 882039 6.60 1522208 7.88 1372838 10.74 1256415 13.87ZZZZZZ 475496 4.02 1658047 5.07 868211 6.60 1501300 7.88 1397245 10.74 1313981 13.87ZZZZZZ 411618 4.02 1461238 5.07 767697 6.60 1359802 7.88 1374290 10.74 1213566 13.88ZZZZZZ 415250 4.02 1454731 5.07 757032 6.60 1319344 7.88 1342118 10.74 1152749 13.90ZZZZZZ 426288 4.02 1475047 5.07 773378 6.60 1345548 7.88 1371074 10.74 1195295 13.89



441 of 555

MC48821

77.4.3






OP49199-MB 441251 4.00 1640322 5.05 920821 6.57 1754699 7.85 1593307 10.69 1389769 13.80OP49199-BS 399295 4.00 1487946 5.05 848882 6.57 1571131 7.86 1490647 10.69 1268870 13.80ZZZZZZ 421542 4.00 1569902 5.05 883742 6.57 1647717 7.85 1473415 10.69 1225154 13.79OP49195-MB 420801 4.00 1552816 5.05 887937 6.57 1653940 7.85 1525104 10.69 1288999 13.79OP49195-BS 420558 4.00 1580933 5.05 897424 6.58 1684880 7.86 1589292 10.69 1348750 13.80MC48821-2 386190 4.00 1445221 5.05 820922 6.57 1563933 7.85 1456397 10.68 1245522 13.79MC48821-3 435939 4.00 1618112 5.05 907334 6.57 1696406 7.85 1539744 10.69 1288730 13.79MC48821-4 401360 4.00 1501538 5.05 847110 6.57 1611517 7.85 1513875 10.69 1279634 13.79MC48821-5 377042 4.00 1384238 5.05 784405 6.57 1495876 7.85 1411446 10.68 1210545 13.79MC48821-6 408464 4.00 1495414 5.05 852211 6.57 1604915 7.85 1513848 10.68 1238844 13.79MC48821-7 299924 4.00 1121733 5.05 647320 6.57 1251553 7.85 1310528 10.69 1242395 13.81MC48821-8 377781 4.01 1399998 5.06 757859 6.57 1441660 7.85 1434809 10.69 1260523 13.79MC48821-9 376962 4.00 1413908 5.05 798849 6.57 1485258 7.85 1444139 10.69 1283185 13.79MC48821-10 402327 4.00 1471955 5.05 832764 6.57 1571258 7.85 1512662 10.69 1286942 13.78MC48821-11 390107 4.00 1422063 5.05 801074 6.57 1463359 7.85 1412811 10.69 1342791 13.81MC48821-12 441025 4.00 1622695 5.05 919670 6.57 1692727 7.85 1534887 10.69 1350323 13.79MC48821-13 432114 4.00 1579158 5.05 884195 6.57 1607273 7.85 1487739 10.69 1378569 13.79MC48821-14 420785 4.00 1539604 5.05 846757 6.57 1511608 7.85 1448382 10.69 1374238 13.80MC48821-15 c 313202 4.00 1156473 5.05 661324 6.57 1266675 7.85 1334226 10.69 1235738 13.79MC48821-16 423928 4.00 1563923 5.05 847161 6.57 1526156 7.85 1469196 10.69 1401255 13.80MC48821-17 455010 4.00 1651956 5.05 899916 6.57 1628040 7.85 1595005 10.69 1447938 13.81MC48821-20 313917 4.00 1177833 5.05 680029 6.57 1332100 7.85 1409218 10.69 1338969 13.80


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Elevated RL due to dilution required for matrix interference.

442 of 555

MC48821

77.4.4






OP49165-MB 403598 4.00 1513205 5.05 898419 6.57 1768107 7.85 1884396 10.69 1767026 13.80OP49165-BS 366534 4.00 1385342 5.05 817116 6.57 1554247 7.86 1675009 10.70 1573231 13.81MC48821-18 c 321527 4.00 1211222 5.05 710232 6.57 1360844 7.85 1399170 10.69 1306296 13.80MC48821-19 c 324993 4.00 1221786 5.05 702430 6.57 1361829 7.85 1391146 10.69 1300688 13.80OP49165-MS 348385 4.00 1340555 5.05 800616 6.57 1534601 7.86 1600582 10.70 1495305 13.81OP49165-MSD 356506 4.00 1352633 5.05 811595 6.57 1571782 7.86 1653861 10.70 1529184 13.81MC48769-1 402728 4.00 1517094 5.05 907378 6.57 1739397 7.85 1751554 10.69 1618519 13.80ZZZZZZ 362993 4.00 1383673 5.05 822945 6.57 1603663 7.85 1698070 10.69 1588484 13.80ZZZZZZ 370293 4.00 1408158 5.05 835624 6.57 1629809 7.85 1709848 10.69 1606436 13.80ZZZZZZ 393315 4.00 1492425 5.05 875365 6.57 1724740 7.85 1716949 10.69 1576080 13.80ZZZZZZ 378530 4.00 1443373 5.05 861428 6.57 1641814 7.85 1712700 10.69 1587249 13.80ZZZZZZ 355724 4.00 1348877 5.05 789717 6.57 1538163 7.85 1593501 10.69 1468448 13.80ZZZZZZ 379583 4.00 1443208 5.05 853135 6.57 1658248 7.85 1741178 10.69 1623900 13.80ZZZZZZ 371481 4.00 1406766 5.05 837467 6.57 1645375 7.85 1713452 10.69 1569814 13.80ZZZZZZ 370166 4.00 1417566 5.05 848474 6.57 1675950 7.85 1857313 10.69 1764746 13.80ZZZZZZ 362887 4.00 1374282 5.05 826773 6.57 1610862 7.85 1693692 10.69 1590148 13.80ZZZZZZ 360005 4.00 1383429 5.05 809508 6.57 1568700 7.85 1623792 10.69 1518400 13.79ZZZZZZ 356201 4.00 1361440 5.05 796041 6.57 1583377 7.85 1689909 10.69 1552419 13.79


(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.(c) Elevated RL due to dilution required for matrix interference.

443 of 555

MC48821

77.4.5


Check Std: MSW1264-CC1235 Injection Date: 11/29/16Lab File ID: W31130.D Injection Time: 10:05 Instrument ID: GCMSW Method: SW846 8270D




OP49189-MB 60439 3.90 227882 4.95 152940 6.48 310744 7.76 376977 10.56 381898 13.61OP49189-BS 60901 3.90 226501 4.95 155453 6.48 319017 7.76 386663 10.57 378043 13.62OP49189-BSD 61981 3.90 230988 4.95 155670 6.48 315283 7.76 389301 10.57 380466 13.62MC48821-22 62091 3.90 231014 4.95 154449 6.48 312430 7.76 387183 10.56 395072 13.62MC48821-23 61058 3.90 225816 4.95 153483 6.48 308641 7.76 382912 10.56 385008 13.61MC48821-24 59925 3.90 223424 4.95 149556 6.48 301200 7.76 374614 10.56 374725 13.61MC48821-27 59934 3.90 222173 4.95 148969 6.48 303319 7.76 374591 10.56 378512 13.62OP49203-MB 59202 3.90 225956 4.95 149739 6.48 309025 7.76 375886 10.56 371130 13.61OP49203-BS 59558 3.90 221554 4.95 154836 6.48 308674 7.76 388458 10.57 380526 13.62OP49203-BSD 63267 3.90 237007 4.95 161343 6.48 328956 7.76 391757 10.57 387241 13.62ZZZZZZ 61575 3.90 228806 4.95 151328 6.48 310559 7.76 381318 10.56 388583 13.62ZZZZZZ 59447 3.90 218058 4.95 143390 6.48 287242 7.76 347328 10.56 351111 13.62ZZZZZZ 62988 3.90 237098 4.95 162077 6.48 319951 7.77 373226 10.56 373044 13.61ZZZZZZ 62892 3.90 234082 4.95 153947 6.48 310890 7.76 366449 10.56 365754 13.62ZZZZZZ 63618 3.90 234751 4.95 157333 6.48 319105 7.76 387622 10.56 385979 13.62ZZZZZZ 62245 3.90 234535 4.95 155731 6.48 315520 7.76 383387 10.56 382959 13.62ZZZZZZ 62770 3.90 236499 4.95 160635 6.48 310980 7.77 372320 10.57 373029 13.62ZZZZZZ 64399 3.90 239209 4.95 156428 6.48 320078 7.76 382665 10.57 375935 13.62ZZZZZZ 70381 3.90 258674 4.95 176195 6.48 359679 7.76 436631 10.56 434482 13.62ZZZZZZ 68580 3.90 258024 4.95 171352 6.48 353006 7.76 423579 10.56 415962 13.61ZZZZZZ 68263 3.90 256555 4.95 172920 6.48 350771 7.76 429046 10.56 424984 13.62ZZZZZZ 68518 3.90 253836 4.95 168703 6.48 346502 7.76 420807 10.57 420389 13.62



444 of 555

MC48821

77.4.6

Semivolatile Surrogate Recovery Summary Page 1 of 1 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Method: SW846 8270D Matrix: AQ


Lab LabSample ID File ID S1 S2 S3 S4 S5 S6

MC48821-22 W31136.D 48 29 103 76 86 108MC48821-23 W31137.D 47 30 108 79 89 106MC48821-24 W31138.D 41 26 99 68 75 105MC48821-27 W31139.D 45 28 107 77 88 107OP49189-BS W31134.D 42 26 106 85 94 102OP49189-BSD W31135.D 52 35 112 78 88 103OP49189-MB W31133.D 55 36 102 81 97 107


S1 = 2-Fluorophenol 10-80%S2 = Phenol-d5 10-72%S3 = 2,4,6-Tribromophenol 42-134%S4 = Nitrobenzene-d5 25-117%S5 = 2-Fluorobiphenyl 24-112%S6 = Terphenyl-d14 48-133%

445 of 555

MC48821

77.5.1


Method: SW846 8270D Matrix: SO


Lab LabSample ID File ID S1 S2 S3 S4 S5 S6

MC48821-1 R50884.D 72 73 86 72 88 100MC48821-2 R50920.D 77 76 81 72 82 96MC48821-3 R50921.D 79 78 86 75 87 99MC48821-4 R50922.D 71 71 75 65 78 87MC48821-5 R50923.D 66 64 73 63 73 83MC48821-6 R50924.D 78 77 83 76 85 96MC48821-7 R50925.D 69 78 109 74 89 97MC48821-8 R50926.D 69 69 78 70 79 87MC48821-9 R50927.D 67 67 74 63 72 81MC48821-10 R50928.D 66 65 72 65 73 83MC48821-11 R50929.D 69 71 83 68 80 91MC48821-12 R50930.D 72 71 79 69 80 92MC48821-13 R50931.D 68 68 79 68 78 86MC48821-14 R50932.D 61 61 81 59 72 88MC48821-15 R50933.D 74 74 98 70 88 95MC48821-16 R50934.D 65 64 78 63 75 79MC48821-17 R50935.D 69 69 82 66 80 84MC48821-18 R50947.D 62 58 89 58 76 84MC48821-19 R50948.D 70 69 94 68 88 95MC48821-20 R50938.D 58 63 82 55 67 84OP49183-BS R50815.D 56 62 76 57 74 78OP49183-BSD R50823.D 64 68 74 62 73 76OP49183-MB R50814.D 66 69 71 62 75 83OP49195-BS R50919.D 75 80 86 73 84 95OP49195-MB R50918.D 68 69 64 67 74 87


S1 = 2-Fluorophenol 25-109%S2 = Phenol-d5 29-113%S3 = 2,4,6-Tribromophenol 20-141%S4 = Nitrobenzene-d5 27-115%S5 = 2-Fluorobiphenyl 34-118%S6 = Terphenyl-d14 42-139%

446 of 555

MC48821

77.5.2


Method: SW846 8270D BY SIM Matrix: AQ



MC48821-22 I103758.D 77 62 87MC48821-23 I103759.D 86 70 94MC48821-24 I103760.D 69 57 89MC48821-27 I103761.D 85 69 96OP49190-BS I103756.D 90 76 87OP49190-BSD I103757.D 81 66 83OP49190-MB I103755.D 87 73 94


S1 = Nitrobenzene-d5 26-121%S2 = 2-Fluorobiphenyl 28-107%S3 = Terphenyl-d14 29-129%

447 of 555

MC48821

77.5.3

SGS Accutest

GC Semi-volatiles

QC Data Summaries


• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries• DDT/Endrin Breakdown Checks• Surrogate Recovery Summaries


448 of 555

MC48821

8


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49181-MB IR3279.D 1 11/23/16 MD 11/21/16 OP49181 GIR229

The QC reported here applies to the following samples: Method: CT-ETPH 7/06

MC48821-22, MC48821-23, MC48821-24, MC48821-27




84-15-1 o-Terphenyl 72% 50-149%

449 of 555

MC48821

88.1.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49193-MB CF5383.D 1 11/23/16 MD 11/22/16 OP49193 GCF1344


MC48821-1




84-15-1 o-Terphenyl 79% 50-137%

450 of 555

MC48821

88.1.2








84-15-1 o-Terphenyl 80% 50-137%

451 of 555

MC48821

88.1.3




MC48821-21




84-15-1 o-Terphenyl 66% 50-137%

452 of 555

MC48821

88.1.4


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49191-MB BE53463.D 1 11/23/16 TA 11/22/16 OP49191 GBE2691

The QC reported here applies to the following samples: Method: SW846 8081B

MC48821-22, MC48821-23, MC48821-24, MC48821-27




877-09-8 Tetrachloro-m-xylene 41% 23-134%877-09-8 Tetrachloro-m-xylene 43% 23-134%2051-24-3 Decachlorobiphenyl 8%* a 10-127%2051-24-3 Decachlorobiphenyl 31% 10-127%

(a) Outside control limits.

453 of 555

MC48821

88.1.5




MC48821-11, MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16, MC48821-17, MC48821-18,MC48821-19, MC48821-20





454 of 555

MC48821

88.1.6




MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9,MC48821-10, MC48821-21





455 of 555

MC48821

88.1.7


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49179-MB BK63217.D 1 11/22/16 TA 11/21/16 OP49179 GBK1999

The QC reported here applies to the following samples: Method: SW846 8082A

MC48821-22, MC48821-23, MC48821-24, MC48821-27





456 of 555

MC48821

88.1.8


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49200-MB BB70553.D 1 11/28/16 TA 11/23/16 OP49200 GBB3722







457 of 555

MC48821

88.1.9


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49218-MB BK63352.D 1 11/30/16 TA 11/29/16 OP49218 GBK2004







458 of 555

MC48821

88.1.10


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49181-BS IR3280.D 1 11/23/16 MD 11/21/16 OP49181 GIR229


MC48821-22, MC48821-23, MC48821-24, MC48821-27

Spike BSP BSPCAS No. Compound mg/l mg/l % Limits

CT-ETPH (C9-C36) 0.7 0.531 76 60-120


84-15-1 o-Terphenyl 69% 50-149%


459 of 555

MC48821

88.2.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49193-BS CF5384.D 1 11/23/16 MD 11/22/16 OP49193 GCF1344


MC48821-1

Spike BSP BSPCAS No. Compound mg/kg mg/kg % Limits

CT-ETPH (C9-C36) 43.8 33.5 76 60-120


84-15-1 o-Terphenyl 89% 50-137%


460 of 555

MC48821

88.2.2






CT-ETPH (C9-C36) 44.2 32.0 72 60-120


84-15-1 o-Terphenyl 67% 50-137%


461 of 555

MC48821

88.2.3




MC48821-21


CT-ETPH (C9-C36) 44 28.3 64 60-120


84-15-1 o-Terphenyl 65% 50-137%


462 of 555

MC48821

88.2.4


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49191-BS BE53464.D 1 11/23/16 TA 11/22/16 OP49191 GBE2691


MC48821-22, MC48821-23, MC48821-24, MC48821-27

Spike BSP BSPCAS No. Compound ug/l ug/l % Limits

15972-60-8 Alachlor 1 0.67 67 33-181309-00-2 Aldrin 0.1 0.053 53 21-166319-84-6 alpha-BHC 0.1 0.057 57 24-175319-85-7 beta-BHC 0.1 0.068 68 27-179319-86-8 delta-BHC 0.1 0.033 33 12-17658-89-9 gamma-BHC (Lindane) 0.1 0.058 58 27-17660-57-1 Dieldrin 0.1 0.071 71 29-19072-54-8 4,4'-DDD 0.1 0.054 54 35-17872-55-9 4,4'-DDE 0.1 0.051 51 33-17350-29-3 4,4'-DDT 0.1 0.075 75 26-19072-20-8 Endrin 0.1 0.078 78 32-1921031-07-8 Endosulfan sulfate 0.1 0.058 58 32-1857421-93-4 Endrin aldehyde 0.1 0.032 32 29-16453494-70-5 Endrin ketone 0.1 0.060 60 37-191959-98-8 Endosulfan-I 0.1 0.046 46 34-18433213-65-9 Endosulfan-II 0.1 0.063 63 35-18576-44-8 Heptachlor 0.1 0.066 66 26-1681024-57-3 Heptachlor epoxide 0.1 0.067 67 35-18172-43-5 Methoxychlor 0.1 0.099 99 26-199




463 of 555

MC48821

88.2.5


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49201-BS BE53521.D 1 11/29/16 TA 11/23/16 OP49201 GBE2693




15972-60-8 Alachlor 319 175 55 40-164309-00-2 Aldrin 31.9 18.1 57 37-165319-84-6 alpha-BHC 31.9 17.1 54 32-157319-85-7 beta-BHC 31.9 18.1 57 41-159319-86-8 delta-BHC 31.9 8.6 27 26-15758-89-9 gamma-BHC (Lindane) 31.9 17.5 55 34-15660-57-1 Dieldrin 31.9 18.7 59 42-17172-54-8 4,4'-DDD 31.9 20.0 63 41-16872-55-9 4,4'-DDE 31.9 20.2 63 42-16750-29-3 4,4'-DDT 31.9 21.2 66 37-17272-20-8 Endrin 31.9 19.5 61 30-1911031-07-8 Endosulfan sulfate 31.9 21.6 68 41-1627421-93-4 Endrin aldehyde 31.9 21.0 66 32-161959-98-8 Endosulfan-I 31.9 19.7 62 42-16833213-65-9 Endosulfan-II 31.9 21.3 67 41-16676-44-8 Heptachlor 31.9 20.0 63 43-1591024-57-3 Heptachlor epoxide 31.9 18.4 58 42-16772-43-5 Methoxychlor 31.9 24.1 75 28-18753494-70-5 Endrin ketone 31.9 23.0 72 32-170




464 of 555

MC48821

88.2.6


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49219-BS1 BE53550.D 1 11/30/16 TA 11/29/16 OP49219 GBE2694




15972-60-8 Alachlor 316 337 107 40-164309-00-2 Aldrin 31.6 29.3 93 37-165319-84-6 alpha-BHC 31.6 28.6 91 32-157319-85-7 beta-BHC 31.6 32.1 102 41-159319-86-8 delta-BHC 31.6 14.9 47 26-15758-89-9 gamma-BHC (Lindane) 31.6 29.4 93 34-15660-57-1 Dieldrin 31.6 30.8 98 42-17172-54-8 4,4'-DDD 31.6 30.6 97 41-16872-55-9 4,4'-DDE 31.6 30.8 98 42-16750-29-3 4,4'-DDT 31.6 31.1 98 37-17272-20-8 Endrin 31.6 31.3 99 30-1911031-07-8 Endosulfan sulfate 31.6 33.7 107 41-1627421-93-4 Endrin aldehyde 31.6 29.7 94 32-161959-98-8 Endosulfan-I 31.6 31.7 100 42-16833213-65-9 Endosulfan-II 31.6 32.1 102 41-16676-44-8 Heptachlor 31.6 30.4 96 43-1591024-57-3 Heptachlor epoxide 31.6 30.7 97 42-16772-43-5 Methoxychlor 31.6 31.3 99 28-18753494-70-5 Endrin ketone 31.6 33.7 107 32-170




465 of 555

MC48821

88.2.7


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49200-BS BB70554.D 1 11/28/16 TA 11/23/16 OP49200 GBB3722




12674-11-2 Aroclor 1016 260 242 93 47-14411104-28-2 Aroclor 1221 ND 40-14011141-16-5 Aroclor 1232 ND 40-14053469-21-9 Aroclor 1242 ND 40-14012672-29-6 Aroclor 1248 ND 40-14011097-69-1 Aroclor 1254 ND 40-14011096-82-5 Aroclor 1260 260 245 94 45-15637324-23-5 Aroclor 1262 ND 40-14011100-14-4 Aroclor 1268 ND 40-140




466 of 555

MC48821

88.2.8


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49179-BS BK63218.D 1 11/22/16 TA 11/21/16 OP49179 GBK1999OP49179-BSD BK63219.D 1 11/22/16 TA 11/21/16 OP49179 GBK1999


MC48821-22, MC48821-23, MC48821-24, MC48821-27


12674-11-2 Aroclor 1016 2 2.1 105 1.9 95 10 34-139/2011104-28-2 Aroclor 1221 ND ND nc 40-140/2011141-16-5 Aroclor 1232 ND ND nc 40-140/2053469-21-9 Aroclor 1242 ND ND nc 40-140/2012672-29-6 Aroclor 1248 ND ND nc 40-140/2011097-69-1 Aroclor 1254 ND ND nc 40-140/2011096-82-5 Aroclor 1260 2 2.2 110 1.9 95 15 37-147/2037324-23-5 Aroclor 1262 ND ND nc 40-140/2011100-14-4 Aroclor 1268 ND ND nc 40-140/20




467 of 555

MC48821

88.3.1


Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP49218-BS BK63353.D 1 11/30/16 TA 11/29/16 OP49218 GBK2004OP49218-BSD BK63354.D 1 11/30/16 TA 11/29/16 OP49218 GBK2004




12674-11-2 Aroclor 1016 264 274 104 266 103 3 47-144/3011104-28-2 Aroclor 1221 ND ND nc 40-140/3011141-16-5 Aroclor 1232 ND ND nc 40-140/3053469-21-9 Aroclor 1242 ND ND nc 40-140/3012672-29-6 Aroclor 1248 ND ND nc 40-140/3011097-69-1 Aroclor 1254 ND ND nc 40-140/3011096-82-5 Aroclor 1260 264 298 113 285 111 4 45-156/3037324-23-5 Aroclor 1262 ND ND nc 40-140/3011100-14-4 Aroclor 1268 ND ND nc 40-140/30




468 of 555

MC48821

88.3.2

DDT/Endrin Breakdown Check Page 1 of 1 Job Number: MC48821Account: BLCTM BL CompaniesProject: Route 69 Improvements, New Haven, CT

Sample: GBE2691-DDT Injection Date: 11/23/16Lab File ID: BE53452.D Injection Time: 18:01 Instrument ID: GCBE

Response ResponseCompound Signal 1 Signal 2

4,4'-DDD 27343026 13745194,4'-DDE 15399707 9057744,4'-DDT 1416451403 96111561

DDT Breakdown a 2.9 % 2.3 %

Endrin aldehyde 16595998 661175Endrin ketone 37052919 1741977Endrin 753448501 53993836

Endrin Breakdown b 6.6 % 4.3 %

(a) Calculated as: (DDD + DDE) / (DDD + DDE + DDT) x 100(b) Calculated as: (Endrin Aldehyde + Endrin Ketone) / (Endrin Aldehyde + Endrin Ketone + Endrin) x 100

This check applies to the following Samples, MS, MSD, Blanks, and Standards:

Lab Lab Date Time Hours ClientSample ID File ID Analyzed Analyzed Lapsed Sample ID

GBE2691-IC2691 BE53453.D 11/23/16 18:16 00:15 Initial cal 2GBE2691-IC2691 BE53454.D 11/23/16 18:30 00:29 Initial cal 5GBE2691-IC2691 BE53455.D 11/23/16 18:45 00:44 Initial cal 10GBE2691-IC2691 BE53456.D 11/23/16 18:59 00:58 Initial cal 50GBE2691-ICC2691 BE53457.D 11/23/16 19:14 01:12 Initial cal 100GBE2691-IC2691 BE53458.D 11/23/16 19:28 01:27 Initial cal 125GBE2691-IC2691 BE53459.D 11/23/16 19:43 01:41 Initial cal 250GBE2691-IC2691 BE53460.D 11/23/16 19:57 01:56 Initial cal 1000GBE2691-IC2691 BE53461.D 11/23/16 20:12 02:10 Initial cal 500GBE2691-ICV2691 BE53462.D 11/23/16 20:26 02:25 Initial cal verification 100OP49191-MB BE53463.D 11/23/16 20:40 02:39 Method BlankOP49191-BS BE53464.D 11/23/16 20:55 02:54 Blank SpikeMC48821-22 BE53465.D 11/23/16 21:09 03:08 B-1/GWMC48821-23 BE53466.D 11/23/16 21:24 03:23 B-3/GWMC48821-24 BE53467.D 11/23/16 21:38 03:37 B-3/GW DUPMC48821-27 BE53468.D 11/23/16 21:53 03:52 EQUIPMENT BLANKGBE2691-ECC2691 BE53469.D 11/23/16 22:07 04:06 Ending cal 100

469 of 555

MC48821

88.4.1




4,4'-DDD 8345107 4028734,4'-DDE 5554975 2271694,4'-DDT 1546562613 100232384



Endrin Breakdown b 6.9 % 5 %




GBE2693-IC2693 BE53511.D 11/29/16 09:05 00:14 Initial cal 5GBE2693-IC2693 BE53512.D 11/29/16 09:20 00:30 Initial cal 10GBE2693-IC2693 BE53513.D 11/29/16 09:34 00:44 Initial cal 50GBE2693-ICC2693 BE53514.D 11/29/16 09:49 00:59 Initial cal 100GBE2693-IC2693 BE53515.D 11/29/16 10:03 01:13 Initial cal 125GBE2693-IC2693 BE53516.D 11/29/16 10:18 01:28 Initial cal 250GBE2693-IC2693 BE53517.D 11/29/16 10:32 01:42 Initial cal 1000GBE2693-IC2693 BE53518.D 11/29/16 10:47 01:56 Initial cal 500GBE2693-ICV2693 BE53519.D 11/29/16 11:01 02:11 Initial cal verification 100OP49201-MB BE53520.D 11/29/16 11:15 02:25 Method BlankOP49201-BS BE53521.D 11/29/16 11:30 02:40 Blank SpikeMC48821-13 BE53522.D 11/29/16 11:44 02:54 B-7(0-2')MC48821-14 BE53523.D 11/29/16 11:59 03:09 B-7(2-4')MC48821-15 BE53524.D 11/29/16 12:13 03:23 HA-1(0-2')MC48821-18 BE53525.D 11/29/16 12:28 03:38 HA-4(0-2')MC48821-12 BE53526.D 11/29/16 12:42 03:52 B-6(2-4')MC48821-11 BE53527.D 11/29/16 12:57 04:07 B-6(0-2')MC48821-16 BE53528.D 11/29/16 13:11 04:21 HA-2(0-2')MC48821-17 BE53529.D 11/29/16 13:26 04:36 HA-3(0-2')GBE2693-CC2693 BE53530.D 11/29/16 13:40 04:50 Continuing cal 100

470 of 555

MC48821

88.4.2




4,4'-DDD 43811202 20224364,4'-DDE 3354563 2705324,4'-DDT 1611645091 110098510

DDT Breakdown a 2.8 % 2 %






MC48821-19 BE53532.D 11/29/16 14:09 00:14 HA-5(0-2')MC48821-20 BE53533.D 11/29/16 14:25 00:30 HA-6(0-2')MC48821-13 BE53534.D 11/29/16 14:39 00:45 B-7(0-2')MC48821-14 BE53535.D 11/29/16 14:54 00:59 B-7(2-4')MC48821-15 BE53536.D 11/29/16 15:08 01:14 HA-1(0-2')MC48821-18 BE53537.D 11/29/16 15:23 01:28 HA-4(0-2')GBE2693-ECC2693 BE53538.D 11/29/16 15:37 01:43 Ending cal 100

471 of 555

MC48821

88.4.3




4,4'-DDD 10851431 16203184,4'-DDE 3833414 2483714,4'-DDT 2381505184 135852841







GBE2694-IC2694 BE53540.D 11/30/16 04:46 00:14 Initial cal 5GBE2694-IC2694 BE53541.D 11/30/16 05:00 00:28 Initial cal 10GBE2694-IC2694 BE53542.D 11/30/16 05:14 00:43 Initial cal 50GBE2694-ICC2694 BE53543.D 11/30/16 05:28 00:57 Initial cal 100GBE2694-IC2694 BE53544.D 11/30/16 05:43 01:11 Initial cal 125GBE2694-IC2694 BE53545.D 11/30/16 05:57 01:25 Initial cal 250GBE2694-IC2694 BE53546.D 11/30/16 06:11 01:40 Initial cal 1000GBE2694-IC2694 BE53547.D 11/30/16 06:25 01:54 Initial cal 500GBE2694-ICV2694 BE53548.D 11/30/16 06:39 02:08 Initial cal verification 100OP49219-MB BE53549.D 11/30/16 08:16 03:44 Method BlankOP49219-BS1 BE53550.D 11/30/16 08:30 03:58 Blank SpikeMC48821-2 BE53551.D 11/30/16 08:44 04:13 B-1(6-8')MC48821-4 BE53552.D 11/30/16 08:58 04:27 B-2(6-8')MC48821-6 BE53553.D 11/30/16 09:13 04:41 B-3(8-10')MC48821-8 BE53554.D 11/30/16 09:27 04:56 B-4(7-10')MC48821-10 BE53555.D 11/30/16 09:41 05:10 B-5(6-8')MC48821-3 BE53556.D 11/30/16 09:57 05:26 B-2(0-2')MC48821-9 BE53557.D 11/30/16 10:11 05:40 B-5(0-2')MC48821-5 BE53558.D 11/30/16 10:26 05:54 B-3(0-2')GBE2694-CC2694 BE53559.D 11/30/16 10:41 06:10 Continuing cal 100

472 of 555

MC48821

88.4.4




4,4'-DDD 71759363 34085214,4'-DDE 3731774 2746514,4'-DDT 1798346964 112498666

DDT Breakdown a 4 % 3.2 %






MC48821-1 BE53561.D 11/30/16 11:10 00:14 B-1(0-5')MC48821-7 BE53562.D 11/30/16 11:24 00:29 B-4(1-3')MC48821-21 BE53563.D 11/30/16 11:39 00:43 HA-6(0-2')DUPGBE2694-ECC2694 BE53564.D 11/30/16 11:53 00:57 Ending cal 100

473 of 555

MC48821

88.4.5


Method: SW846 8081B Matrix: AQ


Lab LabSample ID File ID S1 a S1 b S2 a S2 b

MC48821-22 BE53465.D 44 45 19 56MC48821-23 BE53466.D 35 38 16 50MC48821-24 BE53467.D 42 44 17 55MC48821-27 BE53468.D 58 44 19 71OP49191-BS BE53464.D 58 57 11 46OP49191-MB BE53463.D 41 43 8* c 31


S1 = Tetrachloro-m-xylene 23-134%S2 = Decachlorobiphenyl 10-127%

(a) Recovery from GC signal #1(b) Recovery from GC signal #2(c) Outside control limits.

474 of 555

MC48821

88.5.1


Method: SW846 8081B Matrix: SO



MC48821-1 BE53561.D 61 77 78 250* cMC48821-2 BE53551.D 58 64 54 84MC48821-3 BE53556.D 61 69 50 97MC48821-4 BE53552.D 43 50 52 67MC48821-5 BE53558.D 56 72 60 87MC48821-6 BE53553.D 48 55 52 75MC48821-7 BE53562.D 40 54 133 826* cMC48821-8 BE53554.D 47 63 64 98MC48821-9 BE53557.D 40 51 36 72MC48821-10 BE53555.D 60 73 51 87MC48821-11 BE53527.D 41 51 176* c 275* c

MC48821-12 BE53526.D 85 92 96 104MC48821-13 BE53522.D 84 77 126 115MC48821-13 BE53534.D 62 61 60 71MC48821-14 BE53523.D 59 65 105 158MC48821-14 BE53535.D 51 60 57 123MC48821-15 BE53524.D 82 76 115 153MC48821-15 BE53536.D 61 67 87 165MC48821-16 BE53528.D 63 62 71 81MC48821-17 BE53529.D 47 55 71 116MC48821-18 BE53525.D 73 66 117 145MC48821-18 BE53537.D 63 62 68 152MC48821-19 BE53532.D 55 55 114 213* c

MC48821-20 BE53533.D 52 58 57 77MC48821-21 BE53563.D 58 72 41 98OP49201-BS BE53521.D 63 60 58 73OP49201-MB BE53520.D 78 78 78 100OP49219-BS1 BE53550.D 82 81 77 100OP49219-MB BE53549.D 75 78 85 104



(a) Recovery from GC signal #1(b) Recovery from GC signal #2(c) Outside control limits due to possible matrix interference.

475 of 555

MC48821

88.5.2


Method: SW846 8082A Matrix: AQ



MC48821-22 BK63228.D 86 84 86 87MC48821-23 BK63229.D 93 93 114 111MC48821-24 BK63230.D 90 90 104 100MC48821-27 BK63231.D 92 90 123 122OP49179-BS BK63218.D 85 89 70 69OP49179-BSD BK63219.D 81 85 72 72OP49179-MB BK63217.D 94 97 77 77



(a) Recovery from GC signal #1(b) Recovery from GC signal #2

476 of 555

MC48821

88.5.3


Method: SW846 8082A Matrix: SO



MC48821-1 BK63355.D 59 52 83 73MC48821-2 BK63356.D 69 73 95 91MC48821-3 BK63357.D 83 101 118 107MC48821-4 BK63358.D 96 107 134 128MC48821-5 BK63359.D 78 81 111 106MC48821-6 BK63360.D 68 72 88 85MC48821-7 BK63361.D 74 56 106 79MC48821-8 BK63363.D 76 70 107 104MC48821-9 BK63364.D 95 92 131 118MC48821-10 BK63365.D 100 99 119 114MC48821-11 BB70557.D 65 58 145 59MC48821-12 BB70558.D 84 76 69 60MC48821-13 BB70559.D 81 78 94 76MC48821-14 BB70560.D 68 56 113 71MC48821-15 BB70561.D 77 66 99 71MC48821-16 BB70562.D 82 75 91 82MC48821-17 BB70564.D 77 68 107 80MC48821-18 BB70565.D 81 72 108 83MC48821-19 BB70566.D 72 64 119 78MC48821-20 BB70567.D 79 72 86 74MC48821-21 BK63366.D 76 76 107 98OP49200-BS BB70554.D 85 91 97 103OP49200-MB BB70553.D 95 100 104 112OP49218-BS BK63353.D 84 87 112 111OP49218-BSD BK63354.D 85 88 110 107OP49218-MB BK63352.D 93 96 128 123



(a) Recovery from GC signal #1(b) Recovery from GC signal #2

477 of 555

MC48821

88.5.4


Method: CT-ETPH 7/06 Matrix: AQ


Lab LabSample ID File ID S1 a

MC48821-22 IR3292.D 73MC48821-23 IR3293.D 84MC48821-24 IR3294.D 72MC48821-27 IR3295.D 71OP49181-BS IR3280.D 69OP49181-MB IR3279.D 72


S1 = o-Terphenyl 50-149%

(a) Recovery from GC signal #1

478 of 555

MC48821

88.5.5


Method: CT-ETPH 7/06 Matrix: SO


Lab LabSample ID File ID S1 a

MC48821-1 CF5410.D 80MC48821-2 CF5418.D 94MC48821-3 CF5419.D 81MC48821-4 CF5420.D 83MC48821-5 CF5423.D 84MC48821-6 CF5416.D 93MC48821-7 CF5436.D 96MC48821-8 CF5421.D 91MC48821-9 CF5425.D 87MC48821-10 CF5417.D 84MC48821-11 CF5431.D 108MC48821-12 CF5422.D 87MC48821-13 CF5426.D 93MC48821-14 CF5427.D 89MC48821-15 CF5432.D 82MC48821-16 CF5430.D 68MC48821-17 CF5433.D 108MC48821-18 CF5434.D 115MC48821-19 CF5435.D 111MC48821-20 CF5428.D 86MC48821-21 CF5470.D 71OP49193-BS CF5384.D 89OP49193-MB CF5383.D 79OP49196-BS CF5415.D 67OP49196-MB CF5414.D 80OP49224-BS CF5466.D 65OP49224-MB CF5465.D 66


S1 = o-Terphenyl 50-137%

(a) Recovery from GC signal #1

479 of 555

MC48821

88.5.6

SGS Accutest

Metals Analysis

QC Data Summaries


• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries


480 of 555

MC48821

9

BLANK RESULTS SUMMARY Part 2 - Method Blanks

Login Number: MC48821 Account: BLCTM - BL Companies

Project: Route 69 Improvements, New Haven, CT

QC Batch ID: MP27038 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l

Prep Date: 11/21/16

MB Metal RL IDL MDL raw final

Aluminum 200 11 25

Antimony 6.0 1.3 1.2

Arsenic 4.0 1.5 2 0.0 <4.0

Barium 50 .19 .57 0.10 <50

Beryllium 4.0 .16 .34

Bismuth 50 .95 1.8

Boron 100 9.7 2.3

Cadmium 4.0 .19 .3 -0.20 <4.0

Calcium 5000 7.6 18

Chromium 10 .39 1.1 0.0 <10

Cobalt 50 .21 .41

Copper 25 .55 4.2 0.90 <25

Gold 50 .91 1.3

Iron 100 1.9 16

Lead 5.0 1.1 1.1 -0.50 <5.0

Lithium 500 1.3 1.8

Magnesium 5000 25 56

Manganese 15 .11 .41

Molybdenum 100 .17 16

Nickel 40 .33 .35

Palladium 50 1.9 1.4

Platinum 50 3.1 4.7

Potassium 5000 27 78

Selenium 10 1.8 3.4 -1.0 <10

Silicon 100 6.3 11

Silver 5.0 .27 1.4 0.0 <5.0

Sodium 5000 5.1 35

Sulfur 50 2.2 3.3

Strontium 10 .079 .17

Thallium 5.0 1.3 1.8

Tin 100 .8 2.2

Titanium 50 .32 .99

Tungsten 100 3.3 23

_________________________________________________________________________________________________________

Page 1

481 of 555

MC48821

99.1.1





Prep Date: 11/21/16


Vanadium 10 .37 .4

Zinc 20 1.2 1 -0.10 <20

Zirconium 50 .32 2.6

Associated samples MP27038: MC48821-22, MC48821-23, MC48821-24, MC48821-22F, MC48821-23F, MC48821-24F

Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 2

482 of 555

MC48821

99.1.1

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY




Prep Date: 11/21/16 11/21/16

BSP Spikelot QC BSD Spikelot BSD QC Metal Result MPICP7 % Rec Limits Result MPICP7 % Rec RPD Limit

Aluminum

Antimony

Arsenic 482 500 96.4 80-120 485 500 97.0 0.6 20

Barium 1910 2000 95.5 80-120 1910 2000 95.5 0.0 20

Beryllium anr

Bismuth

Boron

Cadmium 489 500 97.8 80-120 491 500 98.2 0.4 20

Calcium

Chromium 474 500 94.8 80-120 475 500 95.0 0.2 20

Cobalt

Copper 458 500 91.6 80-120 459 500 91.8 0.2 20

Gold

Iron

Lead 972 1000 97.2 80-120 974 1000 97.4 0.2 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel anr

Palladium

Platinum

Potassium

Selenium 483 500 96.6 80-120 484 500 96.8 0.2 20

Silicon

Silver 179 200 89.5 80-120 179 200 89.5 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

483 of 555

MC48821

99.1.2





Prep Date: 11/21/16 11/21/16


Vanadium

Zinc 478 500 95.6 80-120 478 500 95.6 0.0 20

Zirconium



_________________________________________________________________________________________________________

Page 2

484 of 555

MC48821

99.1.2

SERIAL DILUTION RESULTS SUMMARY




Prep Date: 11/21/16

MC48790-3 QC Metal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic 0.00 0.00 NC 0-10

Barium 65.6 66.1 0.8 0-10

Beryllium anr

Bismuth

Boron

Cadmium 0.00 0.00 NC 0-10

Calcium

Chromium 0.400 0.00 100.0(a) 0-10

Cobalt

Copper 1.50 3.70 146.7(a) 0-10

Gold

Iron

Lead 0.00 0.00 NC 0-10

Lithium

Magnesium

Manganese

Molybdenum

Nickel anr

Palladium

Platinum

Potassium

Selenium 0.00 0.00 NC 0-10

Silicon

Silver 0.00 0.00 NC 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

485 of 555

MC48821

99.1.3





Prep Date: 11/21/16


Vanadium

Zinc 0.00 0.00 NC 0-10

Zirconium


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

_________________________________________________________________________________________________________

Page 2

486 of 555

MC48821

99.1.3





Prep Date: 11/21/16


Aluminum 200 11 25

Antimony 6.0 1.3 1.2

Arsenic 4.0 1.5 2 -0.50 <4.0

Barium 50 .19 .57 0.0 <50

Beryllium 4.0 .16 .34

Bismuth 50 .95 1.8

Boron 100 9.7 2.3

Cadmium 4.0 .19 .3 -0.10 <4.0

Calcium 5000 7.6 18

Chromium 10 .39 1.1 0.30 <10

Cobalt 50 .21 .41

Copper 25 .55 4.2 0.20 <25

Gold 50 .91 1.3

Iron 100 1.9 16

Lead 5.0 1.1 1.1 0.20 <5.0

Lithium 500 1.3 1.8

Magnesium 5000 25 56

Manganese 15 .11 .41

Molybdenum 100 .17 16

Nickel 40 .33 .35

Palladium 50 1.9 1.4

Platinum 50 3.1 4.7

Potassium 5000 27 78

Selenium 10 1.8 3.4 0.50 <10

Silicon 100 6.3 11

Silver 5.0 .27 1.4 -0.20 <5.0

Sodium 5000 5.1 35

Sulfur 50 2.2 3.3

Strontium 10 .079 .17

Thallium 5.0 1.3 1.8

Tin 100 .8 2.2

Titanium 50 .32 .99

Tungsten 100 3.3 23

_________________________________________________________________________________________________________

Page 1

487 of 555

MC48821

99.2.1





Prep Date: 11/21/16


Vanadium 10 .37 .4

Zinc 20 1.2 1 0.0 <20

Zirconium 50 .32 2.6

Associated samples MP27041: MC48821-27, MC48821-27F


_________________________________________________________________________________________________________

Page 2

488 of 555

MC48821

99.2.1





Prep Date: 11/21/16 11/21/16


Aluminum

Antimony

Arsenic 496 500 99.2 80-120 498 500 99.6 0.4 20

Barium 1860 2000 93.0 80-120 1870 2000 93.5 0.5 20

Beryllium

Bismuth

Boron

Cadmium 498 500 99.6 80-120 500 500 100.0 0.4 20

Calcium

Chromium 488 500 97.6 80-120 489 500 97.8 0.2 20

Cobalt

Copper 466 500 93.2 80-120 468 500 93.6 0.4 20

Gold

Iron anr

Lead 985 1000 98.5 80-120 987 1000 98.7 0.2 20

Lithium

Magnesium

Manganese anr

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 490 500 98.0 80-120 493 500 98.6 0.6 20

Silicon

Silver 181 200 90.5 80-120 181 200 90.5 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

489 of 555

MC48821

99.2.2





Prep Date: 11/21/16 11/21/16


Vanadium

Zinc 495 500 99.0 80-120 495 500 99.0 0.0 20

Zirconium



_________________________________________________________________________________________________________

Page 2

490 of 555

MC48821

99.2.2





Prep Date: 11/21/16

MC48764-6F QC Metal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic 0.00 0.00 NC 0-10

Barium 100 101 1.3 0-10

Beryllium

Bismuth

Boron

Cadmium 0.00 0.00 NC 0-10

Calcium

Chromium 1.50 0.00 100.0(a) 0-10

Cobalt

Copper 0.00 0.00 NC 0-10

Gold

Iron anr

Lead 0.00 0.00 NC 0-10

Lithium

Magnesium

Manganese anr

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.00 0.00 NC 0-10

Silicon

Silver 0.00 0.00 NC 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

491 of 555

MC48821

99.2.3





Prep Date: 11/21/16

MC48764-6F QC Metal Original SDL 1:5 %DIF Limits

Vanadium

Zinc 1.60 0.00 100.0(a) 0-10

Zirconium



_________________________________________________________________________________________________________

Page 2

492 of 555

MC48821

99.2.3




QC Batch ID: MP27043 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg

Prep Date: 11/22/16


Aluminum 20 1.1 1.2

Antimony 1.0 .13 .17

Arsenic 1.0 .15 .2 0.010 <1.0

Barium 5.0 .019 .076 0.020 <5.0

Beryllium 0.40 .016 .015

Bismuth 5.0 .095 .15

Boron 10 .97 .13

Cadmium 0.40 .019 .031 -0.010 <0.40

Calcium 500 .76 .86

Chromium 1.0 .039 .047 0.060 <1.0

Cobalt 5.0 .021 .031

Copper 2.5 .055 .1

Gold 5.0 .091 .11

Iron 10 .19 .44

Lead 1.0 .11 .11 -0.010 <1.0

Lithium 50 .13 .18

Magnesium 500 2.5 4

Manganese 1.5 .011 .047

Molybdenum 10 .017 .51

Nickel 4.0 .033 .057

Palladium 5.0 .19 .14

Platinum 5.0 .31 .54

Potassium 500 2.7 3.4

Selenium 1.0 .18 .3 0.0 <1.0

Silicon 10 .63 .51

Silver 0.50 .027 .061 -0.010 <0.50

Sodium 500 .51 1.2

Sulfur 5.0 .22 .31

Strontium 1.0 .0079 .022

Thallium 1.0 .13 .11

Tin 10 .08 .078

Titanium 5.0 .032 .054

Tungsten 10 .33 .93

_________________________________________________________________________________________________________

Page 1

493 of 555

MC48821

99.3.1





Prep Date: 11/22/16


Vanadium 1.0 .037 .04

Zinc 2.0 .12 .17

Zirconium 5.0 .032 .17

Associated samples MP27043: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7,MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16,MC48821-17, MC48821-18, MC48821-19, MC48821-20


_________________________________________________________________________________________________________

Page 2

494 of 555

MC48821

99.3.1

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY




Prep Date: 11/22/16

MC48821-9 Spikelot QC Metal Original MS MPICP7 % Rec Limits

Aluminum

Antimony

Arsenic 3.7 42.5 43.8 88.5 75-125

Barium 74.2 232 175 90.0 75-125

Beryllium

Bismuth

Boron

Cadmium 0.070 40.0 43.8 91.1 75-125

Calcium

Chromium 15.7 56.5 43.8 93.0 75-125

Cobalt

Copper

Gold

Iron

Lead 59.5 139 87.7 90.7 75-125

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.25 38.6 43.8 87.5 75-125

Silicon

Silver 0.0 15.2 17.5 86.7 75-125

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

495 of 555

MC48821

99.3.2





Prep Date: 11/22/16

MC48821-9 Spikelot QC Metal Original MS MPICP7 % Rec Limits

Vanadium

Zinc

Zirconium


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 2

496 of 555

MC48821

99.3.2





Prep Date: 11/22/16

MC48821-9 Spikelot MSD QC Metal Original MSD MPICP7 % Rec RPD Limit

Aluminum

Antimony

Arsenic 3.7 44.8 44.2 93.0 5.3 20

Barium 74.2 250 177 99.4 7.5 20

Beryllium

Bismuth

Boron

Cadmium 0.070 42.2 44.2 95.3 5.4 20

Calcium

Chromium 15.7 60.4 44.2 101.1 6.7 20

Cobalt

Copper

Gold

Iron

Lead 59.5 146 88.4 97.9 4.9 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.25 40.5 44.2 91.1 4.8 20

Silicon

Silver 0.0 15.9 17.7 89.9 4.5 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 3

497 of 555

MC48821

99.3.2





Prep Date: 11/22/16

MC48821-9 Spikelot MSD QC Metal Original MSD MPICP7 % Rec RPD Limit

Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 4

498 of 555

MC48821

99.3.2





Prep Date: 11/22/16 11/22/16


Aluminum

Antimony

Arsenic 47.6 50 95.2 80-120 47.5 50 95.0 0.2 20

Barium 190 200 95.0 80-120 189 200 94.5 0.5 20

Beryllium

Bismuth

Boron

Cadmium 48.4 50 96.8 80-120 48.1 50 96.2 0.6 20

Calcium

Chromium 48.1 50 96.2 80-120 47.9 50 95.8 0.4 20

Cobalt

Copper

Gold

Iron

Lead 99.4 100 99.4 80-120 98.1 100 98.1 1.3 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 48.0 50 96.0 80-120 47.7 50 95.4 0.6 20

Silicon

Silver 17.9 20 89.5 80-120 17.8 20 89.0 0.6 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

499 of 555

MC48821

99.3.3





Prep Date: 11/22/16 11/22/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

500 of 555

MC48821

99.3.3





Prep Date: 11/22/16

LCS Spikelot QC Metal Result MPLCS86 % Rec Limits

Aluminum

Antimony

Arsenic 89.7 97.5 92.0 78-122

Barium 273 306 89.2 83-117

Beryllium

Bismuth

Boron

Cadmium 72.8 76.6 95.0 82-118

Calcium

Chromium 94.3 103 91.6 80-121

Cobalt

Copper

Gold

Iron

Lead 91.0 96.7 94.1 82-118

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 152 161 94.4 78-123

Silicon

Silver 43.5 49.3 88.2 75-125

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 3

501 of 555

MC48821

99.3.3





Prep Date: 11/22/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 4

502 of 555

MC48821

99.3.3




QC Batch ID: MP27043 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l

Prep Date: 11/22/16


Aluminum

Antimony

Arsenic 42.2 46.7 10.7 (a) 0-10

Barium 847 905 6.9 0-10

Beryllium

Bismuth

Boron

Cadmium 0.800 0.00 100.0(a) 0-10

Calcium

Chromium 180 194 7.8 0-10

Cobalt

Copper

Gold

Iron

Lead 679 711 4.8 0-10

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 2.90 0.00 100.0(a) 0-10

Silicon

Silver 0.00 0.00 NC 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

503 of 555

MC48821

99.3.4





Prep Date: 11/22/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

504 of 555

MC48821

99.3.4




QC Batch ID: MP27045 Methods: SW846 7471B Matrix Type: SOLID Units: mg/kg

Prep Date: 11/22/16


Mercury 0.033 .0011 .0057 -0.0070 <0.033



_________________________________________________________________________________________________________

Page 1

505 of 555

MC48821

99.4.1





Prep Date: 11/22/16

MC48821-2 Spikelot QC Metal Original MS HGRWS1 % Rec Limits

Mercury 0.0 0.47 0.492 95.6 80-120



_________________________________________________________________________________________________________

Page 1

506 of 555

MC48821

99.4.2





Prep Date: 11/22/16

MC48821-2 Spikelot MSD QC Metal Original MSD HGRWS1 % Rec RPD Limit

Mercury 0.0 0.49 0.499 98.2 4.2 20



_________________________________________________________________________________________________________

Page 2

507 of 555

MC48821

99.4.2





Prep Date: 11/22/16 11/22/16

BSP Spikelot QC BSD Spikelot BSD QC Metal Result HGRWS1 % Rec Limits Result HGRWS1 % Rec RPD Limit

Mercury 0.46 0.5 92.0 80-120 0.46 0.5 92.0 0.0 20



_________________________________________________________________________________________________________

Page 1

508 of 555

MC48821

99.4.3





Prep Date: 11/22/16

LCS Spikelot QC Metal Result HGLCS86 % Rec Limits

Mercury 18.3 20.2 90.6 71-129



_________________________________________________________________________________________________________

Page 2

509 of 555

MC48821

99.4.3




QC Batch ID: MP27050 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l

Prep Date: 11/22/16


Mercury 0.20 .0068 .034 -0.071 <0.20

Associated samples MP27050: MC48821-22, MC48821-23, MC48821-24, MC48821-27, MC48821-22F, MC48821-23F,MC48821-24F, MC48821-27F


_________________________________________________________________________________________________________

Page 1

510 of 555

MC48821

99.5.1





Prep Date: 11/22/16

MC48821-22F Spikelot QC Metal Original MS HGRWS1 % Rec Limits

Mercury 0.0 3.3 3 110.0 75-125



_________________________________________________________________________________________________________

Page 1

511 of 555

MC48821

99.5.2





Prep Date: 11/22/16

MC48821-22F Spikelot MSD QC Metal Original MSD HGRWS1 % Rec RPD Limit

Mercury 0.0 3.1 3 103.3 6.2 20



_________________________________________________________________________________________________________

Page 2

512 of 555

MC48821

99.5.2





Prep Date: 11/22/16 11/22/16


Mercury 3.0 3 100.0 80-120 3.0 3 100.0 0.0 20



_________________________________________________________________________________________________________

Page 1

513 of 555

MC48821

99.5.3





Prep Date: 11/23/16


Aluminum 20 1.1 1.2

Antimony 1.0 .13 .17

Arsenic 1.0 .15 .2 -0.040 <1.0

Barium 5.0 .019 .076 0.020 <5.0

Beryllium 0.40 .016 .015

Bismuth 5.0 .095 .15

Boron 10 .97 .13

Cadmium 0.40 .019 .031 -0.040 <0.40

Calcium 500 .76 .86

Chromium 1.0 .039 .047 0.0 <1.0

Cobalt 5.0 .021 .031

Copper 2.5 .055 .1

Gold 5.0 .091 .11

Iron 10 .19 .44

Lead 1.0 .11 .11 -0.030 <1.0

Lithium 50 .13 .18

Magnesium 500 2.5 4

Manganese 1.5 .011 .047

Molybdenum 10 .017 .51

Nickel 4.0 .033 .057

Palladium 5.0 .19 .14

Platinum 5.0 .31 .54

Potassium 500 2.7 3.4

Selenium 1.0 .18 .3 -0.010 <1.0

Silicon 10 .63 .51

Silver 0.50 .027 .061 0.010 <0.50

Sodium 500 .51 1.2

Sulfur 5.0 .22 .31

Strontium 1.0 .0079 .022

Thallium 1.0 .13 .11

Tin 10 .08 .078

Titanium 5.0 .032 .054

Tungsten 10 .33 .93

_________________________________________________________________________________________________________

Page 1

514 of 555

MC48821

99.6.1





Prep Date: 11/23/16


Vanadium 1.0 .037 .04

Zinc 2.0 .12 .17

Zirconium 5.0 .032 .17

Associated samples MP27053: MC48821-21


_________________________________________________________________________________________________________

Page 2

515 of 555

MC48821

99.6.1





Prep Date: 11/23/16 11/23/16


Aluminum

Antimony

Arsenic 45.6 50 91.2 80-120 45.5 50 91.0 0.2 20

Barium 181 200 90.5 80-120 180 200 90.0 0.6 20

Beryllium

Bismuth

Boron

Cadmium 47.1 50 94.2 80-120 46.5 50 93.0 1.3 20

Calcium

Chromium 45.3 50 90.6 80-120 45.0 50 90.0 0.7 20

Cobalt

Copper

Gold

Iron

Lead 93.1 100 93.1 80-120 92.3 100 92.3 0.9 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 45.4 50 90.8 80-120 44.9 50 89.8 1.1 20

Silicon

Silver 17.0 20 85.0 80-120 16.9 20 84.5 0.6 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

516 of 555

MC48821

99.6.2





Prep Date: 11/23/16 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

517 of 555

MC48821

99.6.2





Prep Date: 11/23/16


Aluminum

Antimony

Arsenic 84.9 97.5 87.1 78-122

Barium 266 306 86.9 83-117

Beryllium

Bismuth

Boron

Cadmium 70.6 76.6 92.2 82-118

Calcium

Chromium 90.8 103 88.2 80-121

Cobalt

Copper

Gold

Iron

Lead 84.0 96.7 86.9 82-118

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 141 161 87.6 78-123

Silicon

Silver 40.6 49.3 82.4 75-125

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 3

518 of 555

MC48821

99.6.2





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 4

519 of 555

MC48821

99.6.2





Prep Date: 11/23/16


Aluminum

Antimony

Arsenic 17.5 19.0 8.6 0-10

Barium 141 145 2.9 0-10

Beryllium

Bismuth

Boron

Cadmium 0.200 0.00 100.0(a) 0-10

Calcium

Chromium 106 108 1.3 0-10

Cobalt

Copper

Gold

Iron

Lead 56.4 57.4 1.8 0-10

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.00 0.00 NC 0-10

Silicon

Silver 1.30 3.10 138.5(a) 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

520 of 555

MC48821

99.6.3





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

521 of 555

MC48821

99.6.3




QC Batch ID: MP27055 Methods: SW846 6010C Matrix Type: LEACHATE Units: mg/l

Prep Date: 11/23/16


Aluminum 0.20 .011 .025

Antimony 0.0060 .0013 .0012

Arsenic 0.010 .0015 .002 -0.00050 <0.010

Barium 0.50 .00019 .00057 -0.00030 <0.50

Beryllium 0.0040 .00016 .00034

Bismuth 0.050 .00095 .0018

Boron 0.10 .0097 .0023

Cadmium 0.0040 .00019 .0003 -0.00050 <0.0040

Calcium 5.0 .0076 .018

Chromium 0.010 .00039 .0011 -0.00060 <0.010

Cobalt 0.050 .00021 .00041

Copper 0.025 .00055 .0042

Gold 0.050 .00091 .0013

Iron 0.10 .0019 .016

Lead 0.010 .0011 .0011 -0.00040 <0.010

Lithium 0.50 .0013 .0018

Magnesium 5.0 .025 .056

Manganese 0.015 .00011 .00041

Molybdenum 0.10 .00017 .016

Nickel 0.040 .00033 .00035

Palladium 0.050 .0019 .0014

Platinum 0.050 .0031 .0047

Potassium 5.0 .027 .078

Selenium 0.025 .0018 .0034 -0.00060 <0.025

Silicon 0.10 .0063 .03

Silver 0.0050 .00027 .0014 0.00010 <0.0050

Sodium 5.0 .0051 .035

Sulfur 0.050 .0022 .0033

Strontium 0.010 .000079 .00017

Thallium 0.0050 .0013 .0018

Tin 0.10 .0008 .0022

Titanium 0.050 .00032 .00099

Tungsten 0.10 .0033 .023

_________________________________________________________________________________________________________

Page 1

522 of 555

MC48821

99.7.1





Prep Date: 11/23/16


Vanadium 0.010 .00037 .0004

Zinc 0.10 .0012 .001

Zirconium 0.050 .00032 .0026

Associated samples MP27055: MC48821-1A, MC48821-2A, MC48821-3A, MC48821-4A, MC48821-5A, MC48821-6A,MC48821-7A, MC48821-8A, MC48821-9A, MC48821-10A, MC48821-11A, MC48821-12A, MC48821-13A, MC48821-14A,MC48821-15A, MC48821-16A, MC48821-17A, MC48821-18A, MC48821-19A, MC48821-20A


_________________________________________________________________________________________________________

Page 2

523 of 555

MC48821

99.7.1





Prep Date: 11/23/16

MC48821-1A Spikelot QC Metal Original MS MPICP7 % Rec Limits

Aluminum

Antimony

Arsenic 0.0 0.49 0.50 98.0 75-125

Barium 0.68 2.5 2.0 91.0 75-125

Beryllium

Bismuth

Boron

Cadmium 0.0042 0.50 0.50 99.2 75-125

Calcium

Chromium 0.0053 0.45 0.50 88.9 75-125

Cobalt

Copper

Gold

Iron

Lead 0.29 1.2 1.0 91.0 75-125

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.0025 0.50 0.50 99.5 75-125

Silicon

Silver 0.0 0.19 0.20 95.0 75-125

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

524 of 555

MC48821

99.7.2





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

525 of 555

MC48821

99.7.2





Prep Date: 11/23/16

MC48821-1A Spikelot MSD QC Metal Original MSD MPICP7 % Rec RPD Limit

Aluminum

Antimony

Arsenic 0.0 0.49 0.50 98.0 0.0 20

Barium 0.68 2.5 2.0 91.0 0.0 20

Beryllium

Bismuth

Boron

Cadmium 0.0042 0.51 0.50 101.2 2.0 20

Calcium

Chromium 0.0053 0.45 0.50 88.9 0.0 20

Cobalt

Copper

Gold

Iron

Lead 0.29 1.2 1.0 91.0 0.0 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.0025 0.50 0.50 99.5 0.0 20

Silicon

Silver 0.0 0.19 0.20 95.0 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 3

526 of 555

MC48821

99.7.2





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 4

527 of 555

MC48821

99.7.2





Prep Date: 11/23/16 11/23/16


Aluminum

Antimony

Arsenic 0.49 0.50 98.0 80-120 0.49 0.50 98.0 0.0 20

Barium 1.8 2.0 90.0 80-120 1.8 2.0 90.0 0.0 20

Beryllium

Bismuth

Boron

Cadmium 0.50 0.50 100.0 80-120 0.50 0.50 100.0 0.0 20

Calcium

Chromium 0.45 0.50 90.0 80-120 0.45 0.50 90.0 0.0 20

Cobalt

Copper

Gold

Iron

Lead 0.93 1.0 93.0 80-120 0.94 1.0 94.0 1.1 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.51 0.50 102.0 80-120 0.51 0.50 102.0 0.0 20

Silicon

Silver 0.19 0.20 95.0 80-120 0.19 0.20 95.0 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

528 of 555

MC48821

99.7.3





Prep Date: 11/23/16 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

529 of 555

MC48821

99.7.3




QC Batch ID: MP27055 Methods: SW846 6010C Matrix Type: LEACHATE Units: ug/l

Prep Date: 11/23/16

MC48821-1A QC Metal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic 0.00 0.00 NC 0-10

Barium 682 698 2.3 0-10

Beryllium

Bismuth

Boron

Cadmium 4.20 2.50 40.5 (a) 0-10

Calcium

Chromium 5.30 3.80 28.3 (a) 0-10

Cobalt

Copper

Gold

Iron

Lead 287 290 1.2 0-10

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 2.50 0.00 100.0(a) 0-10

Silicon

Silver 0.00 0.00 NC 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

530 of 555

MC48821

99.7.4





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

531 of 555

MC48821

99.7.4




QC Batch ID: MP27057 Methods: SW846 7470A Matrix Type: LEACHATE Units: mg/l

Prep Date: 11/23/16


Mercury 0.00020 .000023 .000034 -0.000055<0.00020



_________________________________________________________________________________________________________

Page 1

532 of 555

MC48821

99.8.1





Prep Date: 11/23/16

MC48821-1A Spikelot QC Metal Original MS HGRWS1 % Rec Limits

Mercury 0.0 0.0027 0.0030 90.0 75-125



_________________________________________________________________________________________________________

Page 1

533 of 555

MC48821

99.8.2





Prep Date: 11/23/16

MC48821-1A Spikelot MSD QC Metal Original MSD HGRWS1 % Rec RPD Limit

Mercury 0.0 0.0027 0.0030 90.0 0.0



_________________________________________________________________________________________________________

Page 2

534 of 555

MC48821

99.8.2





Prep Date: 11/23/16 11/23/16


Mercury 0.0028 0.0030 93.3 80-120 0.0028 0.0030 93.3 0.0



_________________________________________________________________________________________________________

Page 1

535 of 555

MC48821

99.8.3





Prep Date: 11/23/16


Aluminum 0.20 .011 .025

Antimony 0.0060 .0013 .0012

Arsenic 0.010 .0015 .002 -0.00060 <0.010

Barium 0.50 .00019 .00057 -0.00030 <0.50

Beryllium 0.0040 .00016 .00034

Bismuth 0.050 .00095 .0018

Boron 0.10 .0097 .0023

Cadmium 0.0040 .00019 .0003 -0.00050 <0.0040

Calcium 5.0 .0076 .018

Chromium 0.010 .00039 .0011 -0.00040 <0.010

Cobalt 0.050 .00021 .00041

Copper 0.025 .00055 .0042

Gold 0.050 .00091 .0013

Iron 0.10 .0019 .016

Lead 0.010 .0011 .0011 -0.00050 <0.010

Lithium 0.50 .0013 .0018

Magnesium 5.0 .025 .056

Manganese 0.015 .00011 .00041

Molybdenum 0.10 .00017 .016

Nickel 0.040 .00033 .00035

Palladium 0.050 .0019 .0014

Platinum 0.050 .0031 .0047

Potassium 5.0 .027 .078

Selenium 0.025 .0018 .0034 -0.0012 <0.025

Silicon 0.10 .0063 .03

Silver 0.0050 .00027 .0014 0.0 <0.0050

Sodium 5.0 .0051 .035

Sulfur 0.050 .0022 .0033

Strontium 0.010 .000079 .00017

Thallium 0.0050 .0013 .0018

Tin 0.10 .0008 .0022

Titanium 0.050 .00032 .00099

Tungsten 0.10 .0033 .023

_________________________________________________________________________________________________________

Page 1

536 of 555

MC48821

99.9.1





Prep Date: 11/23/16


Vanadium 0.010 .00037 .0004

Zinc 0.10 .0012 .001

Zirconium 0.050 .00032 .0026

Associated samples MP27058: MC48821-21A


_________________________________________________________________________________________________________

Page 2

537 of 555

MC48821

99.9.1





Prep Date: 11/23/16


Aluminum

Antimony

Arsenic 0.0 0.48 0.50 96.0 75-125

Barium 0.40 2.2 2.0 90.0 75-125

Beryllium

Bismuth

Boron

Cadmium 0.0022 0.51 0.50 101.6 75-125

Calcium

Chromium 0.00080 0.44 0.50 87.8 75-125

Cobalt

Copper

Gold

Iron

Lead 0.040 0.95 1.0 91.0 75-125

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.0031 0.49 0.50 97.4 75-125

Silicon

Silver 0.0 0.18 0.20 90.0 75-125

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

538 of 555

MC48821

99.9.2





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

539 of 555

MC48821

99.9.2





Prep Date: 11/23/16


Aluminum

Antimony

Arsenic 0.0 0.48 0.50 96.0 0.0 20

Barium 0.40 2.2 2.0 90.0 0.0 20

Beryllium

Bismuth

Boron

Cadmium 0.0022 0.51 0.50 101.6 0.0 20

Calcium

Chromium 0.00080 0.43 0.50 85.8 2.3 20

Cobalt

Copper

Gold

Iron

Lead 0.040 0.96 1.0 92.0 1.0 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.0031 0.50 0.50 99.4 2.0 20

Silicon

Silver 0.0 0.18 0.20 90.0 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 3

540 of 555

MC48821

99.9.2





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 4

541 of 555

MC48821

99.9.2





Prep Date: 11/23/16 11/23/16


Aluminum

Antimony

Arsenic 0.48 0.50 96.0 80-120 0.48 0.50 96.0 0.0 20

Barium 1.8 2.0 90.0 80-120 1.8 2.0 90.0 0.0 20

Beryllium

Bismuth

Boron

Cadmium 0.50 0.50 100.0 80-120 0.50 0.50 100.0 0.0 20

Calcium

Chromium 0.44 0.50 88.0 80-120 0.44 0.50 88.0 0.0 20

Cobalt

Copper

Gold

Iron

Lead 0.91 1.0 91.0 80-120 0.91 1.0 91.0 0.0 20

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 0.49 0.50 98.0 80-120 0.50 0.50 100.0 2.0 20

Silicon

Silver 0.18 0.20 90.0 80-120 0.18 0.20 90.0 0.0 20

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

542 of 555

MC48821

99.9.3





Prep Date: 11/23/16 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

543 of 555

MC48821

99.9.3





Prep Date: 11/23/16


Aluminum

Antimony

Arsenic 0.00 0.00 NC 0-10

Barium 404 419 3.6 0-10

Beryllium

Bismuth

Boron

Cadmium 2.20 0.00 100.0(a) 0-10

Calcium

Chromium 0.800 0.00 100.0(a) 0-10

Cobalt

Copper

Gold

Iron

Lead 39.8 35.3 11.3 (a) 0-10

Lithium

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium 3.10 0.00 100.0(a) 0-10

Silicon

Silver 0.00 0.00 NC 0-10

Sodium

Sulfur

Strontium

Thallium

Tin

Titanium

Tungsten

_________________________________________________________________________________________________________

Page 1

544 of 555

MC48821

99.9.4





Prep Date: 11/23/16


Vanadium

Zinc

Zirconium



_________________________________________________________________________________________________________

Page 2

545 of 555

MC48821

99.9.4





Prep Date: 11/23/16


Mercury 0.00020 .000023 .000034 -0.000053<0.00020



_________________________________________________________________________________________________________

Page 1

546 of 555

MC48821

99.10.1





Prep Date: 11/23/16

MC48821-21A Spikelot QC Metal Original MS HGRWS1 % Rec Limits

Mercury 0.0 0.0021 0.0030 70.0 (a) 75-125


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.

_________________________________________________________________________________________________________

Page 1

547 of 555

MC48821

99.10.2





Prep Date: 11/23/16

MC48821-21A Spikelot MSD QC Metal Original MSD HGRWS1 % Rec RPD Limit

Mercury 0.0 0.0024 0.0030 80.0 13.3



_________________________________________________________________________________________________________

Page 2

548 of 555

MC48821

99.10.2





Prep Date: 11/23/16 11/23/16


Mercury 0.0025 0.0030 83.3 80-120 0.0025 0.0030 83.3 0.0



_________________________________________________________________________________________________________

Page 1

549 of 555

MC48821

99.10.3





Prep Date: 11/28/16


Mercury 0.033 .0038 .0057 -0.0030 <0.033



_________________________________________________________________________________________________________

Page 1

550 of 555

MC48821

99.11.1





Prep Date: 11/28/16 11/28/16


Mercury 0.48 0.5 96.0 80-120 0.47 0.5 94.0 2.1 20



_________________________________________________________________________________________________________

Page 1

551 of 555

MC48821

99.11.2





Prep Date: 11/28/16

LCS Spikelot QC Metal Result HGLCS86 % Rec Limits

Mercury 18.8 20.2 93.1 71-129



_________________________________________________________________________________________________________

Page 2

552 of 555

MC48821

99.11.2

SGS Accutest

General Chemistry

QC Data Summaries


• Method Blank and Blank Spike Summaries• Duplicate Summaries• Matrix Spike Summaries


553 of 555

MC48821

10

METHOD BLANK AND SPIKE RESULTS SUMMARY GENERAL CHEMISTRY



MB Spike BSP BSP QC Analyte Batch ID RL Result Units Amount Result %Recov Limits

Cyanide Reactivity GP21131/GN55418 1.5 0.0 mg/kg Sulfide Reactivity GP21132/GN55407 50 0.0 mg/kg

Associated Samples: Batch GP21131: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-14, MC48821-16, MC48821-19Batch GP21132: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-14, MC48821-16, MC48821-19(*) Outside of QC limits

__________________________________________________________________________________________________________________________

Page 1

554 of 555

MC48821

1010.1

DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY



QC Original DUP QC Analyte Batch ID Sample Units Result Result RPD Limits

Cyanide Reactivity GP21131/GN55418 MC48821-3 mg/kg 0.0 0.0 0.0 0-20% Solids, Percent GN55387 MC48821-1 % 75.9 74.6 1.7 0-5% Sulfide Reactivity GP21132/GN55407 MC48821-3 mg/kg 0.0 0.0 0.0 0-20% pH GN55423 MC48821-1 su 7.6 7.6 0.0 0-20%

Associated Samples: Batch GN55387: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-13, MC48821-14, MC48821-15, MC48821-16, MC48821-17, MC48821-18, MC48821-19, MC48821-20Batch GN55423: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-14, MC48821-16, MC48821-19Batch GP21131: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-14, MC48821-16, MC48821-19Batch GP21132: MC48821-1, MC48821-2, MC48821-3, MC48821-4, MC48821-5, MC48821-6, MC48821-7, MC48821-8, MC48821-9, MC48821-10, MC48821-11, MC48821-12, MC48821-14, MC48821-16, MC48821-19(*) Outside of QC limits

__________________________________________________________________________________________________________________________

Page 1

555 of 555

MC48821

1010.2