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TABLE OF CONTENTS

I. GENERAL INFORMATION

1. Introduction 3

2. Mailing/shipping address 3

3. Contact information 3

4. How to use this directory 4

5. Discount program 4

II. INDUSTRIAL HYGIENE SERVICES AND FEES

1. General information and Policies 5

1.1. Standard Turnaround Time 5

1.2. Shipping, Billing and Rush Multipliers 5

1.3. Discounts for Multiple Analytes on Single Media 6

1.4. Blanks and Charges 6

1.5. Method Development 6

1.6. Media 6

1.7. Sampling Instructions 7

1.8. Analytical Reports 9

1.9. No Charge Loaner Pump Program 10

1.10. Laboratory Test Request (Chain of Custody) 12

2. Industrial Hygiene Test Catalog 13

2.1. How to Use the Test Catalog 13

2.2. Alphabetical Listing of Test Methods 16

2.3. Profiles 107

2.4. Media Table 110

III. PHARMACEUTICAL TESTING SERVICES 117

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IV. ENVIRONMENTAL SERVICES AND FEES 119

1. Introduction 119

2. Standard Turnaround Time 119

3. Billing and Rush Multipliers 119

4. Deliverable Multipliers 119

5. Certifications 119

6. Sample Containers/Shipping Kits 120

7. Sample Kit/Cooler Return Policy 120

8. Sample Kit/Cooler Temperatures 120

9. Sample Collection and Preservation Guidelines 120

10. How to Submit a Sample 121

11. Reports and Deliverables 122

12. Alphabetical Listing of Methods 125

V. MISCELLANEOUS SERVICES AND FEES 147

1. Introduction 147

2. Microbiology: Bacteria in Air 148

3. Microbiology: Bacteria in Water 148

4. Microbiology: Fungal 149

5. Air Quality Testing 150

VI. SERVICE GUIDE SUMMARY 150

1. Standard Terms and Conditions 150

2

I. General Information

1. IntroductionAnalytics has been a major supplier of industrial hygiene and environmental testing servicesto Fortune 500 companies, government agencies, and engineering firms since 1977. Thisexperience allows us to provide services that are both high in quality and cost effective.

Analytics is proud of the reputation we have earned over the last 30 years as a result ofproviding our customers the best quality analytical data available in the U.S. and more than30 countries abroad. We have over 1800 active clients and have done business with mostof them for over 10 years.

Analytics’ facility is one of the finest industrial hygiene and environmental laboratories in thecountry. We have in place the certifications, SOPs, insurance, and state-of-the art- instrumentation required to meet OSHA, NIOSH, and EPA analytical requirements.

Our standard turnaround time is 3 days for Industrial Hygiene samples, and 5 days forenvironmental samples. Analytics has no difficulty in meeting 24-hour turnaround time asmay be required.

2. Mailing/Shipping Addresses

Main Office & Laboratory

Analytics Corporation

10329 Stony Run Lane Ashland, VA 23005

800-888-8061 804-365-3000

804-365-3002 (Fax)

Remittance Address Analytics Corporation

PO Box 25249 Richmond, VA 23260

Website www.analyticscorp.com

Federal Tax ID #36-4359432 DUNS

#151052102

3. Contact Information

All personnel can be reached via our toll free number – 800-888-8061.

James McCarthy, President –5201 Jeffrey Spink, CEO – x5004

Andrew Teague, CIH, Industrial Hygiene Technical Laboratory Director – x5226 Dawn Casto, Environmental Technical Director – x5208

Jack Simila, Sales & No Charge Loaner Pumps – x5108 Customer Service – x0

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http://www.analyticscorp.com/

4. How to Use This Directory

This directory has been designed so you can find individual industrial hygiene analytes alphabetically and within profiles. Environmental analytes are sorted alphabetically and by regulation. Pharmaceutical APIs and surrogates are sorted alphabetically.

The following information is included in the alphabetical listings:

Industrial Hygiene: Analyte, CAS #, Recommended Media, Suggested Volume, Sampling Rate, LOQ, Analytical Method, Analytical Technique, Lab Code, and Comments.

Environmental: Analyte, Method, Sample Container and Volume Requirements, Preservation, Holding Times, and Limits of Quantitation.

Pharmaceutical: Compound, Media, Reporting Limit, Method.

Please refer to the Data Deliverables Section at the end of both the IH and Environmental Services and Fees sections for a complete listing of our data package options. We can provide your data via fax, e-mail, or CD-ROM. Our data package turnaround time is contingent upon the data package level required.

5. Discount Program

Please note that all prices listed in this Directory of Services are our list/non-discounted prices. Client discounts may be available and are based on your annual volume of business. Please contact our Sales personnel to discuss volume related discounting.

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II. Industrial Hygiene Services and Fees

1. General Information and Policies As you know, an industrial hygiene laboratory analyzes samples taken in the workplace environment. Since results of these analyses are used to determine the magnitude or presence of a problem in the workplace environment, it is vital that the laboratory analyzing the samples be proficient in producing high quality data on which important health decisions will be based. Our accreditation from AIHA is a mark of that capability. The AIHA accreditation shows that the laboratory has met defined standards for performance based on examination of a variety of criteria. When an IH laboratory is accredited by AIHA, it becomes part of a select group that have proven a high level of professional performance can be achieved and maintained.

1.1 Standard Turnaround Time

Analytics standard turnaround time for most industrial hygiene analyses is 3 business days from sample receipt at the laboratory. Faxed, e-mail, or verbal results are available by the close of business on the due date. A hard copy of the report will follow by mail.

1.2 Shipping, Billing and Rush Multipliers

Analytics will cover the cost of STANDARD OVERNIGHT FedEx return shipment to the laboratory of six (6) or more samples shipped within the United States. All other overnight delivery services charged on Analytics’ accounts will be billed at the courier’s published rate.

Clients may request monthly billing or individual invoices by sample group. Pricing is subject to change based on the current state of the economy. Billing by sample group is assumed unless otherwise requested. Billing terms are payable net 30. Acceptable forms

of payment include check, money order, wire transfer, VisaTM, MasterCardTM, DiscoverTM

or American ExpressTM.

Samples requiring rush or priority turnaround time must be scheduled prior to sample submission. The following charges will apply:

2 Day Turnaround Time 1.75 x price 1 Day Turnaround Time 2.00 x price Same Day Turnaround Time 3.00 x price Weekend Analysis 3.00 x price + $300 Holiday Analysis 3.00 x price + $300

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1.3 Discounts for Multiple Analytes on Single Media

Analysis of multiple compatible analytes captured on one medium is available at a discounted fee. The higher priced analyte is billed at the published fee with additional analytes discounted as follows:

Organics by GC 50% of the published fee Inorganics by ICP 50% of the published fee Inorganics by ICP/MS 50% of the published fee Inorganics by GFAA 50% of the published fee Analytes by IC/HPLC 50% of the published fee

Other discounts may apply based on the volume and types of samples.

1.4 Blanks and Charges

Blanks act as a control for analysis by accounting for contamination that can occur during handling, storage or shipment of samples. Therefore, they are recommended as standard industrial hygiene practice. Please handle them the same as samples, but draw no air through them. Submit one blank with each sample group of 10 or less, two blanks with 11-20 samples, etc. (i.e., 10% blanks). Since blanks are analyzed as any other sample in the laboratory, they are priced according to the analysis requested. Additional support documentation, including instrument calibration, chromatograms, etc. is available at a preparation charge of 20% of the total analytical cost.

Analytics reserves the right to refuse to process any sample, which is deemed by the laboratory to be non-compliant with the quality assurance requirements. In such cases, client services will notify the client. If sample issues cannot be resolved, the client may be billed a sample-handling fee for costs incurred up to that point.

1.5 Method Development

Analytics has over 500 methods currently in service. It has always been our policy to develop new routine methods at no charge, assuming adequate demand. In addition, we can develop very specific/one of a kind methods for a standard fee plus expenses.

1.6 Media

Standard filter cassettes, sorbent tubes, specialized filters and tubes are supplied free if the samples are returned for analysis. Fees for organics are based on small charcoal tube analysis – there is an additional charge of $8.00 for large charcoal tubes. Diffusive (passive) monitor fees are not included in the analytical unit price and are billed at the time of shipment. Media can be shipped via ground service at no charge. A purchase order or credit card authorization may be required prior to the shipment of media. Media that has been supplied free and not returned for analysis to our laboratory after thirty days will be billed at current manufacturer published prices. See Section 2.4 - Media Table, which provides part numbers, descriptions and pricing for sampling media.

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1.7 Sampling Instructions

The Analytics technical staff is available to discuss sampling strategies, sample requirements, and laboratory capabilities. Please direct inquiries through client services.

The volume of air to be collected for your samples is based on a number of factors, including:

• Threshold Limit Value (TLV) or Permissible Exposure Limit (PEL)

• Sensitivity of the analytical procedure

• Capacity of the collection device

• Concentration range to be measuredThe recommendations for air volumes, sampling rates and suggested media within this directory are provided for your convenience and are intended only as a guide to sample collection. With few exceptions, these air volumes enable the laboratory to report one-tenth of the TLV as the detection limit.

Fees for analyses of samples submitted on sorbent tubes include separate desorption, analysis, and reporting of both front and back sections.

Clearly label every tube, badge, vial, or sample container with your sample field number or your identification number. This number should also be printed on the chain of custody.

To facilitate testing and reporting, please type or clearly print all required information on the Laboratory Test Request/Chain of Custody (COC) form (an example immediately follows this section or our website www.analyticscorp.com). To initiate the COC, fill out and sign the appropriate sections designating time, date, and requested analysis. Submit the original with your samples and retain the copy for your records. The COC form should be submitted with each group of samples using a separate form for each sample type.

1.7.1 Solid Sorbent Tube Sampling Solid sorbent tubes include large and small charcoal tubes, porous polymer tubes such as XAD and XAD-7, large and small silica gel tubes, DNPH (dinitrophenyl hydrazine) tubes, Orbo tubes, Porapak Q, Tenax tubes, Firebrick tubes, Hydrar tubes and Florisil tubes. Sampling should be performed in the following manner:

1. Calibrate each pump at the recommended flow rate for the analyte of interest, using arepresentative solid-sorbent tube in-line. Calibrate each pump with a bubble meter orequivalent flow measuring device.

2. Break the ends of the solid sorbent tube immediately before sampling. The openingsshould be at least ½ of the internal diameter of the tube. Use a tube tip breaker or file.

3. Connect the solid sorbent tube to the tube holder, making sure the smaller sorbentsection (backup section) is nearest the pump. The air that is being sampled should notpass through any hose or tubing before entering the solid sorbent tube. To avoidchanneling and premature breakthrough, position the tube vertically during sampling.

4. Prepare field blanks by breaking the ends of tubes from the same lot as the tubes thatare being used for sampling. Handle the blanks in the same manner as the samples, but

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do not draw air through the blanks. 5. Sample at an accurately known flow rate for the length of time necessary to obtain the

specified air volume. Check the pump periodically during sampling to detect any changes in flow rate. If the accurate measurement of volume cannot be determined due to inconsistent flow rates, discard the sample.

6. Be sure to keep an accurate record of sampling data including sample location, beginning and ending times of air sampling, temperature, relative humidity, atmospheric pressure or

7. elevation above sea level, and name of employee. 8. Seal the ends of the tubes with plastic caps immediately after sampling. Clearly label

each sample with an appropriate identification number. Label each blank tube as a blank.

9. Pack the tubes tightly for shipment to the laboratory, with adequate packing to minimize the possibility of breakage. Enclose a completed sample analytical request form (chain of custody) with each batch.

10. Bulk samples are recommended when sampling chemical mixtures such as fuel oil, kerosene, etc. When it is necessary to ship a bulk sample along with the air samples, the bulk sample must be shipped in a separate package to avoid possible cross contamination.

1.7.2 Sampling Using Filters Filters include glass fiber filters, Teflon filters, mixed cellulose ester membranes, polyvinyl chloride filters, and treated filters and pads.

Sampling with filters can be done open or closed faced. Open-faced sampling is done with three (3) piece cassettes with just the top of the cassette removed. Closed-faced sampling is performed with only the buttons removed from the cassette. Open-faced sampling is used in situations where even dispersal of the analyte over the filter is desired, such as in asbestos sampling or on certain coated filters such as for isocyanate sampling. Closed-faced sampling is performed in most cases of particulate sampling, which deposits the analyte near the center of the cassette.

Sampling should be performed in the following manner:

1. Calibrate the sampling pump at the recommended flow rate with a representative filter

in line using a bubble meter or equivalent flow measuring device.

2. Remove the cassette buttons (closed faced sampling) or cassette top (open faced sampling). Air being sampled should not pass through any hose or tubing before entering the cassette.

3. Attach the cassette to the sampling pump using flexible tubing or a cassette holder, making sure the filter pad end of the cassette is closest to the pump.

4. Prepare field blanks using cassettes from the same lot by briefly removing and replacing cassette buttons and handling these blanks in the same manner as the samples, without drawing air through the blanks.

5. Sample at a known flow rate for the length of time necessary to obtain the specified air volume, or until there is evidence of excessive filter loading. Check the pump during sampling to detect any changes in flow rate. If the accurate measurement of volume cannot be determined due to inconsistent flow rates, discard the sample.

6. Disconnect the filter after sampling. Replace the buttons (or top) and properly label the

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sample and blanks. Be sure to keep an accurate record of sample data including sample location, beginning and ending times or air sampling, temperature, relative humidity, atmospheric pressure or elevation above sea level, and name of employee or area.

7. Ship the samples to the laboratory as soon as possible in a container designed to prevent damage in shipment. Enclose a completed chain of custody with each batch.

1.7.3 Sampling for Respirable Aerosols Respirable aerosol sampling is performed using a cyclone and filter sampler. Sampling for respirable aerosols should be performed in the same manner as sampling a filter except:

1. Calibrate each pump at the flow designated by the type of cyclone being used with a

representative cyclone and filter in line. Note that the filter is mounted upside down with the cyclone in place.

2. Inspect the interior of the cyclone. If there is visible scoring or damage inside, discard the cyclone since the dust separation characteristics may have been altered. Clean the interior of the cyclone.

3. Attach the cyclone to the filter according to the manufacturer’s instructions. Connect the assembly to the sampling pump. During sampling, make sure the cyclone hangs vertically and that the assembly does not get inverted during sampling. If an accurate and consistent flow rate cannot be maintained, discard the sample.

1.7.4 Sampling for Inhalable Aerosols We can provide pre-weighing of inhalable samplers, as well as post-weighing. Contact the laboratory for details on this relatively new technique.

1.8 Analytical Reports

Most clients have their data reported on our standard report, which includes total mass of analyte on each collector section, limits of quantitation, method reference and calculated air concentration. If you need additional data or would like a different format, please contact our customer service department at 800-888-8061, x0 and they will be able to assist you with your request. All laboratory reports, sample data and client proprietary information are held in confidence. Raw data for all analytical results will be retained for a period of 5 years. If data needs to be retained for a longer period, contact client services.

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1.9 No Charge Loaner Pump Program

Analytics offers a No Charge Loaner Pump Program. This program will provide you with everything you need for air sampling analysis–pumps, sample media, all accessories, and instructions, custom packaged to your requirements, shipped to you as you need it. You pay only for shipping and, of course, the analysis – there is absolutely no cost to use the pumps and accessories.

To order your pumps, all you need to do is contact Jack Simila at 800-888-8061, x5108.

Your order will include the pumps (as many as you need, all fully charged and pre-calibrated), tubing, sample media, sample media holders, pumps, chargers, instructions, cyclones, splitters, low flow regulators, tube breaker, tool kit, chain of custody form and calibrated field rotameter, all packed in a sturdy carrying case. Pumps are normally sent out the same day. Please keep in mind the more notice you provide, the less expensive shipping charges will be. Typical shipping costs for a sampling set that includes five pumps and is shipped across the country (VA to CA) with 2nd day delivery is about $40.

We use primarily SKC AirCheck 52 sampling pumps, which handle flows in the range of 25 to 3000 ml/min with a backpressure of 25" water at 2 liters per minute. They weigh 20 ounces and have a timer, flow fault feature and NiCad or NiMH battery with a battery-check feature. Other pumps are available on request. The pumps arrive fully charged and calibrated versus a primary standard, with a record of calibration in the shipment. A field rotameter, calibrated against a primary standard, is included in the sampling kit. Post calibration can be performed and reported if you request it on your chain of custody when you return the samples and pumps.

The pumps and all accessories can be kept for the duration of your sampling project. As long as you are collecting and submitting for analysis daily samples, you may use the pumps indefinitely. If your project is postponed, you will need to call to confirm availability. Depending on the length of the time delay, you may need to return everything to us, but we will re-ship the entire sampling kit to you for your new scheduled date.

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1.10 Laboratory Test Request (Chain of Custody)

Sample Custody is a set of procedures used to provide an accurate written record that can be used to trace the possession of a sample from the time of collection through its introduction into a data set. The Laboratory Test Request/Chain of Custody is used to record the transfer, possession, and custody of samples to ensure their integrity from collection through data reporting. Until you relinquish custody, you are responsible to ensure no one tampers with your samples. Custody is a critical part of the process because data reported without a complete and accurate chain of custody will not withstand legal challenge. The following items must be completed on the chain in order to ensure sample integrity and accurate analysis/reporting:

1. Date Shipping Samples

2. Total Number of Samples

3. Type of Media

4. Project Name or Number

5. PO or Release Number

6. Contact – Who the Report Will be Sent to

7. Telephone Number

8. Turnaround Time Required

9. Special Instructions, if needed

10. Where to fax/e-mail results

11. Sample ID or Sample Number

12. Sample Date

13. Sample volume

14. Analysis

15. Initiate COC

16. Laboratory Receipt Information (for laboratory use)

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LABORATORY TEST REQUESTACCOUNT NUMBER, NAME AND ADDRESS

10329 Stony Run Lane

Ashland, VA 23005

(804) 365-3000

TOLL FREE (800) 888-8061

FAX (804) 365-3002

SAMPLE DATE

SIGN HERE TO INITIATE CHAIN OF CUSTODY

CARRIER IF "ANALYTICS COURIER" SIGN HERE DATE

PLEASE RETAIN A COPY FOR YOUR RECORDS

SIGNATURE(SAMPLE RECEIVING)

SIGNATURE(SAMPLE ADMINISTRATION)

SIGNATURE(LAB)

SIGNATURE(LAB)

SAMPLES RECEIVED BY: SAMPLES RELEASED BY:

SIGNATURE(SAMPLE RECEIVING)

SIGNATURE(SAMPLE ADMINISTRATION)

SIGNATURE(LAB)

SIGNATURE(LAB)

DATE/TIME CONDITION OF SAMPLE

PURCHASE ORDER NO.

DATE SHIPPED

* o SAME DAY

* o 1 DAY

* oCALL FOR AVAILABILITY

SPECIAL INSTRUCTIONS AND/OR UNUSUAL CONDITIONS:TURN AROUND TIME

CONTACT

CHAIN OF CUSTODY RECORD

FOR LABORATORY USE ONLY

SAMPLES HAVE VEEN SEALED FOR TRANSPORT AND

DELIVERED TO LABORATORY VIA:

ANALYSS REQUESTED - PLEASE USE SEPARATE

LABORATORY TEST REQUEST FOR EACH SAMPLE TYPE

o FAX RESULTS FAX NUMBER:

( ) __________________

o EMAIL RESULTS - EMAIL:________________________

SAMPLE # OR SAMPLE AREASAMPLE

VOLUME/LITERS

*o2 DAY

oSTANDARD

*EXTRA CHARGE

PROJECT NAME OR NUMBER

TELEPHONE NUMBER

# OF SAMPLES SAMPLE TYPE/MEDIA

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ccatlyn

Line

2. Industrial Hygiene Test Catalog

2.1 How to Use the Test Catalog

This section is composed of several categories of information that allows the user to access the necessary parameters for industrial hygiene air sampling. The guide has been arranged to make it as easy as possible for the user. For many categories, abbreviations are used to facilitate a concise format. The following descriptions give the relevant information pertaining to each category in order of appearance in the guide.

Analyte & CAS# This category will give the name of the compound to be analyzed and the corresponding CAS#. In cases where there are other names for a compound, there may be a redirection to another place in the guide.

Recommended Media This category specifies the method recommended collection media for air sampling of the particular compound. Abbreviations used in this category are defined in the Section 2.4 Media Table.

Suggested Volume, L This category specifies the method recommended air volume to be sampled in liters. In many cases, this recommended volume can be at least doubled before breakthrough occurs. In high relative humidity locations or with very high volatile compounds, this recommended volume should not be exceeded.

Sampling Rate, LPM This sampling range indicates the minimum and maximum flow rate of the sampling pumps used in liters per minute.

LOQ (Limit of Quantitation) This category lists the lowest quantifiable sampling media loading (also known as Reporting Limit, RL) that will be reported (typically in micrograms) per sample. Samples measured below this loading will be reported as “<” values.

Method & Technique This category specifies the method used to analyze the compound listed in the test category. The “NIOSH” designation refers to methods described in the National Institute of Occupational Safety and Health Manual of Analytical Methods. The “OSHA” designation refers to methods described in the Occupational Safety and Health Administration Methods Manual. “SPM” designates a special method or an in-house method developed and validated by Analytics. An “M” in parentheses after the method designation refers to a modification of the method that has been validated by Analytics.

This category also gives abbreviations for the analytical technique and instrumentation used for the analysis of the compound listed in the test category.

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Lab Code (Compatibility) This category gives the option to the user of sampling more than one compound on a specific sampling media. In order to do so, not only must the same sampling media be specified for each compound, but the Compatibility letter designations given in this category must match for each test compound to be sampled. Particular attention must be given to other parameters of the individual compounds such as sample volume and flow rate in order to ensure sample validity. Care must be taken to make sure that no flow rate or air volume parameter for an individual compound is exceeded when sampling for two or more compounds. The exception to the Lab Code list is NC, which means the analyte is not compatible with other compounds.

Due to the frequency of questions on substance compatibility (analytes or compounds that can be sampled on the same collection media), we have included a compatibility code in this edition of the sampling guide. Please see the “Lab Code” column in the list of individual air contaminants for information on individual analytes and compounds. Listed below is the compatibility code key. When two or more substances have the same Recommended Media and same the Lab Code, they can be sampled together and are eligible for a discounted price (see terms and conditions section for details).

Code A

Desorbing Solution Carbon disulfide (CS2)

Code AA

Desorbing Solution Sodium Thiosulfate

B C

CS2 + 1% 2-Butanol CS2 + 1% 2-Propanol

CC EE

Toluene OSHA ID125G Acid Digestion

D CS2 + 5% 2-Propanol FF 0.1N Potassium Hydroxide E Methylene Chloride + 5% HH Acetone

Methanol F CS2 + 1% Dimethylformamide II Methylene Chloride + 15%

Methanol H CS2 + 1% Methanol JJ 50% Methanol + 50% Water I Methylene Chloride KK 50% Isopropanol + 50%

Toluene J Water-soluble Metals Prep LL CS2 + 2% Acetone K Methanol MM Benzene M Ethanol NN Di-n-Butylamine

Derivatization N Acetonitrile OO Aqua Regia Acid digestion O Acetonitrile + 10%

Dimethylsulfoxide P Isooctane Q Methanol + 20% water NC Prep Not Compatible With

Additional Tests S Hexane T NIOSH 7300M Acid Digestion U Bicarbonate/carbonate Eluent V Sodium borate Eluent W Tetrahydrofuran X 0.01N Sodium Hydroxide Y Methanesulfonic Acid Eluent

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2.2 Alphabetical Listing of Test Methods

Analytics is pleased to offer an extensive array of Industrial Hygiene analyses, including most OSHA, NIOSH, ASTM, and EPA methods and also numerous proprietary methods. Specific analytical tests are listed in the following sections. Lists of tests are presented in the Sections that follow here; Section 2.2 provides an alphabetical list by analyte, and Section 2.3 provides a listing of our profiles. Please note that for most tests Analytics does not require a minimum sample fee. Volume discounts are available depending on the annual volume or scope of your project. Please contact our sales department or your project manager for details.

15

Alphabetical Listing

of

Industrial Hygiene Tests

V01 06.2017 Toll Free: 800-888-8061 Find more info at www.analyticscorp.com 16

Analyte CAS # Recommended Media

Suggested

(minutes for passive

samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acenapthene

83-32-9 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116

Wrap cassettes with foil if sampling in bright sunlight.

Transfer filter to glass vial immediately after sampling, and

wrap tube and vial with aluminum foil to protect from light.

Store samples cold and ship samples cold for overnight

delivery.

Acenapthylene

208-96-8 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Acetaldehyde

75-07-0T-119

DNPH-Treated Silica Gel,

226-119

2 - 15 0.2 - 1.0 0.2EPA TO-11

HPLCN $116

Any ketone or aldehyde will react with the DNPH and is a

potential interference. Large concentrations of acetone or

MEK will compete with aldehyde and are therefore

potential negative interferences. Refrigerate media before

and after sampling and ship cold overnight. High ozone

level may necessitate ozone scrubber.

UMEX-100

SKC UMEX

Aldehyde PM 500-100

Up to 8 hours 0.0231 0.2EPA TO-11

HPLCN $116



MEK will compete with aldehyde and are therefore


and after sampling and ship cold overnight. High ozone

level may necessitate ozone scrubber.

Acetic Acid

64-19-7T-01

Charcoal, 226-015 - 48 0.2 Max 5

OSHA ID 186SG M

ICV $69

Preferred method. Use PTFE prefilter (PN C-29) to remove

particulate acetates, if present. Particulate acetates can be

measured on filter, otherwise discard after sampling.

Formic Acid can also be determined but must be stored and

shipped cold overnight.

T-10-03

Prewashed Silica Gel,

226-10-03

1 - 24 0.05 - 0.2 5NIOSH 2011M

ICV $69

Use PTFE prefilter (PN C-29) to remove particulate acetates,

if present. Particulate acetates can be measured on filter,

otherwise discard after sampling. Formic Acid can also be

determined.

Acetic Anhydride

108-24-7

C-28

GFFs (2), amine-treated,

37mm, 4PC

TWA 15 Max

STEL 7.5 Max

0.050 Max

0.50 Max10

OSHA 102M

HPLC/UVKK $100

Open face sampling. Interference from ketene and acetyl

chloride. Limited shelf life media; store cold. Ship samples

cold overnight to the lab.

Acetoin

573-86-0 T-183

(2 in Series) Custom Silica

Gel, 226-183

TWA 9 Max

STEL 3 Max

0.050 Max

0.20 Max0.4

OSHA Method 1012

GC-ECDNC $110

Protect from light during sampling and storage (wrap with

foil). Store and ship samples cold. Ship overnight. May be

sampled on same tube with diacetyl. Filter built into tube

faces incoming air streams. Samples stable at least 17 days.

A three (3) sample minimum charge will be applied.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acetone

67-64-1

T-01

Charcoal, 226-010.5 - 3 0.01 - 0.2 20

NIOSH 1300

GC/FIDA $56

O-91

Carbosieve S-III, Orbo 913 Max 0.05 Max 20

OSHA 69

GC/FIDF $56

M-3520

3M POVM 3520,

2-stage

2 Hours Max (at PEL) 0.0401 30NIOSH 1300M

GC/FIDA $56

Keep samples cold and expedite analysis for optimum

results.

M-02

SKC POVM, 575-0028 hours Max 0.0152 20

Proprietary,

IHGC-P029

GC/FID

A $77

T-09

Charcoal, 226-093 - 25 0.01 - 0.2 20

NIOSH 1606

GC/FIDII $56

M-01

SKC POVM, 575-00115 min - 8 hours 0.0224 10

NIOSH 1606M

GC/FIDII $56

M-3520

3M POVM 3520,

2-stage

2 Hours Max 0.0482 30NIOSH 1606M

GC/FIDII $56

Acetylene Tetrabromide

79-27-6 $-

See 1,1,2,2-Tetrabromoethane.

Acetylacetone

123-54-6

T-95

XAD-7, 226-95

TWA 24

STEL 3

TWA 0.05-0.1

CEIL 0.2 5

OSHA 7M

GC/FIDHH $77

Also known as 2,4-Pentandione.

Acid Mist (Inorganic Acid

Profile) See Inorganic Acid

Profile in Section 2.3

Profile includes Hydrobromic Acid, Hydrochloric Acid,

Hydrofluoric Acid, Nitric Acid, Phosphoric Acid, Sulfuric

Acid. Also see individual acids.

Acrolein

107-02-8T-119


226-119

2 - 30 0.2 - 1.0 0.25EPA TO-11M

HPLC/UVN $116

Result may be biased low due to instability of acrolein-

DNPH derivative. Any ketone or aldehyde will react with

the DNPH and is a potential interference. Large

concentrations of acetone or MEK will compete with

aldehyde and are therefore potential negative

interferences. Refrigerate media before and after sampling

and ship overnight.

T-117

HMP XAD-2,

226-117

TWA 48

STEL 3

TWA 0.1

STEL 0.2 1

OSHA 52

GC/NPDCC $102

Preferred method for compound stability. Not sensitive

enough to reach ACGIH TLV CEILING. Can also be analyzed

for formaldehyde. Store media cold be use.

UMEX-100

SKC UMEX Aldehyde

PM 500-100

Up to 8 hours 21.2 0.2EPA TO-11M

HPLC/UVN $116

Result may be biased low due to instability of acrolein-

DNPH derivative. Any ketone or aldehyde will react with


concentrations of acetone or MEK will compete with


interferences. Refrigerate media before and after sampling

and ship overnight.

Acetonitrile

75-05-8

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Acrylamide

79-06-1

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.40

Proprietary,

IHHPLC-P003

HPLC/UV

NC $160

Methylolacrylamide may also be tested along with

acrylamide.

T-57

GFF/XAD-7 OVS,

226-57

120 Max 1.0 Max 0.4OSHA PV2004

HPLC/UVNC $116

Acrylic Acid

79-10-7T-30-08 (2)

Anasorb 708, 226-30-08,

2 tubes in series

24 0.1 2OSHA PV2005

HPLC/UVK $116

Two identical tubes sampled in series. Low results due to

polymerization of acrylic acid on the sampling tube may

result from the presence of initiators collected. Methacrylic

acid may also be tested along with acrylic acid.

T-49-108

Chromosorb 108,

226-49-108

TWA 20

STEL 4.5

TWA 0.03-0.3

STEL 0.3 3

Proprietary,

IHHPLC-P005

HPLC/UV

JJ $160

Methacrylic acid can be collected and analyzed along with

acrylic acid using this sampling protocol (see lower

recommended sampling volume for methacrylic acid).

Acrylonitrile

107-13-1

T-01

Charcoal, 226-016 - 20 0.2 1

OSHA 37

GC/NPDHH $100

Preferred method.

M-3500

3M POVM, 350015 min - 8 hours 0.04 1.5

OSHA 37M

GC/NPDHH $100

M-02

SKC POVM, 575-002Up to 8 hours 0.0204 2.5

Proprietary,

IHGC-P029

GC/FID

A $77

T-81

Anasorb 747,

226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.25

Proprietary,

IHGC-P029

GC/FID

A $77

Aldehyde Profile See

Aldehyde Profile in

Section 2.3

T-119


226-119

16 - 30 0.2 - 1Varies with

compound

EPA TO-11

HPLC/UVN $254

Profile includes Acetaldehyde, Acrolein, Butyraldehyde,

Formaldehyde, Glutaraldehyde, and Isovaleraldehyde. For

STEL sampling, collect a 15-minute sample at 1 LPM. Ozone

may interfere - use ozone scrubber in known ozone

contaminated areas. Any ketone or aldehyde will react with


concentrations of acetone or MEK will compete with the


interferences. Refrigerate before and after sampling and

ship overnight. Media contains residual acetonitrile which

could interfere with acetonitrile monitoring.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Alkaline Dust

(as NaOH, KOH, other)

N/A

C-66

PTFE, 1um, 37mm, 2PC70 - 1000 1.0 - 4.0

40 NaOH,

56 KOH

NIOSH 7401

TitrationNC $69

This test provides a single cumulative measure of all

alkaline aerosols present in the exposure; e.g., sodium

hydroxide, potassium hydroxide, sodium bicarbonate,

calcium carbonate, etc. The acid-base titration test is not

compound-specific, but the result will be expressed in

terms of the alkaline compound identified on the test

request form. Acid compounds present in the sampling

environment will be negative interferences in the

measurement.

T-01

Charcoal, 226-014 - 50 0.01 - 0.2 5

NIOSH 1402

GC/FIDD $56

Also known as 2-Propenol.

M-3500

3M POVM, 3500Up to 8 hours 0.0404 7.5

NIOSH 1402M

GC/FIDI $56

Also known as 2-Propenol.

Allyl Chloride

107-05-1

T-01

Charcoal, 226-0116-100 0.01 - 1 5

NIOSH 1000

GC/FIDMM $77

Allyl Chloroformate

2937-50-0

T-153

Amine-treated XAD-2,

226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77

Store media and samples cold, ship samples cold overnight.

Samples must arrive at lab within 10 days of sampling.

Allyl Methacrylate

96-05-9

T-81

Anasorb 747,

226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min 0.012 2.6

Proprietary,

IHGC-P029

GC/FID

A $77

Aluminum

(metal dust and fume)

7429-90-5C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300M

ICP-OEST $40

Also see Welding Fume Profile. This analysis method is not

sufficient for analysis of the alpha-alumina form of

aluminum oxide which is commonly used in abrasives and

refractory materials (also known as corundum).

Ammonia

7664-41-7

T-10-06

H2SO4-Treated Silica Gel,

226-10-06

7.5 - 96 0.2 Max 2.5 NIOSH 6016 IC NC $69

Capacity reduced at high humidity. Prefilter (C-50) required

in presence of ammonium salt particulates.

T-29

Anasorb 747,

226-29

7 - 24 0.1 - 0.5 5.0

OSHA ID 188/

NIOSH 6015M

IC

NC $69

Sampling per OSHA ID188, analysis by NIOSH 6015M.

Capacity reduced at low humidity. Prefilter (C-50) required

in presence of ammonium salt particulates.

M-N584

Assay Ammonia PM,

AT N584

TWA Up to 8 hours

STEL 15 minutes0.0288 2.5

NIOSH 6016M

ICNC $69

Ship at ambient temperature to arrive at lab within 2 days.

Must be received by lab within 2 weeks of sampling. Store

unused samplers in refrigeration for maximum shelf life.

Ammonium Chloride

12125-02-9C-05

MCEF, 37mm, 0.8um, 3PC960 Max 2 Max 10

OSHA ID188M

ICNC $69

Sampling is for particulate ammonium salts, with analysis

for ammonium ion; ammonium chloride equivalent is

determined by calculation.

Allyl Alcohol

107-18-6

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ammonium Persulfate, as

Persulfate

7727-54-0C-10

PVC, 37mm, 5um, 3PC

TWA 480-960

STEL 60

TWA 1-4

STEL 4 2.7

NIOSH 6016M

ICNC $69

When submitting samples, “Ammonium Persulfate, AS

PERSULFATE” needs to be specified on the Analysis Request

Form in order to have results reported correctly as

persulfate. Analysis is for ammonium ion with “ammonium

persulfate, as persulfate” determined by calculation.

n-Amyl Acetate

628-63-7

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0260 30

NIOSH 1450M

GC/FIDA $56

M-01

SKC POVM, 575-01Up to 8 hours 0.0118 40

NIOSH 1450M

GC/FIDA $56

sec-Amyl Acetate

626-38-0

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

n-Amyl Alcohol

71-41-0

T-09

Charcoal, 226-093 - 48 0.05 - 0.2 3.3

OSHA 7

GC/FIDA $56

t-Amyl Methyl Ether

994-05-8

T-09

(2 in series) Charcoal,

226-09

96 Max 0.1-0.2 20NIOSH 1615M

GC/FIDA $56

Aniline

62-53-3

T-10

Silica Gel, 226-105 - 30 0.02 - 0.2 10

NIOSH 2002

GC/FIDM $56

C-15

GFFs (2), H2SO4-treated,

37mm, 3PC

5 - 50 0.1 - 0.2 20NIOSH 2017

GC/FIDM $102

This arrangement allows for collection of o-toluidine on the

same cassette, and a silica gel tube (226-15) may be

included downstream of the cassette to trap and include

nitro benzene in the analysis.

Anthracene

120-12-7 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Antimony and Compounds,

as Sb

7440-36-0

C-05

MCEF, 37mm, 0.8um, 3PC40 - 1000 1.0 - 3.0 2.0

OSHA ID 125

ICPEE $40

Also See Welding Fume Profile

Antimony - ICP-MS

7440-36-0C-05

MCEF, 37mm, 0.8um, 3PC2000 Max 1 - 4 0.05

NIOSH 7300M

ICP-MST $51

Antimony Trioxide,

as Sb

1309-64-4

C-05

MCEF, 37mm, 0.8um, 3PC240 0.5-3.0 1

OSHA ID-125

ICPEE $40

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Aromatic 100

N/A T-01

Charcoal, 226-01

TWA 5-20

STEL 3

TWA 0.01-0.2

STEL 0.2 50

NIOSH 1550

GC/FIDA $77

Ship 5 ml pure distillate in separate shipment for reference,

and note separate shipment of the bulk sample on the test

request form. Also known as High Flash Aromatic Naphtha.

Aromatic 150

N/AT-01

Charcoal, 226-01

TWA 5-20

STEL 3 0.01-0.2 50

NIOSH 1550

GC/FIDA $77



request form.

Aromatic 200

N/AT-01

Charcoal, 226-01

TWA 5-20

STEL 3 0.01-0.2 50

NIOSH 1550

GC/FIDA $77



request form.

Arsenic

7440-38-2C-05

MCEF, 37mm, 0.8um, 3PC800 - 1000 1.0 - 3.0 2

NIOSH 7300

ICPT $40

C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 0.05

NIOSH 7300M

ICP/MST $46

Arsenic Trioxide

(as Arsenic)

1327-53-3

C-18

MCEF/Treated Backup,

37mm, 3PC

30 - 1000 1.0 - 3.0 0.05OSHA ID105M

GFAANC $51

Particulate arsenic collects on the MCE filter, and arsenic

trioxide vapor collects on the treated pad. Particulate

arsenic may be tested from the MCE filter if needed.

C-18

MCEF/Treated Backup,

37mm, 3PC

30 - 1000 1.0 - 3.0 0.05OSHA ID105M

ICP-MSNC $51

Particulate arsenic collects on the MCE filter, and arsenic

trioxide vapor collects on the treated pad. Particulate

arsenic may be tested from the MCE filter if needed.

Arsine

(as Arsenic)

7784-42-1 T-01

Charcoal, 226-0110 Max 0.2 Max 0.01

NIOSH 6001M

GFAANC $51

Precede tube with arsenic trioxide cassette (see above) if

particulate arsenic and/or arsenic trioxide are present. This

treated filter/tube train can be tested for particulate

arsenic, arsenic trioxide vapor, and arsine if needed.

Samples are stable for at least 6 days at ambient

temperature.

T-09

Charcoal, 226-09120 - 240 0.5 Max 0.04

NIOSH 6001M

GFAANC $51

If particulate arsenic is present, precede tube with arsenic

trioxide cassette (see above) to trap particulate arsenic and

arsenic trioxide. This treated filter/tube train can be tested

for particulate arsenic, arsenic trioxide vapor, and arsine if

needed. The recommended sampling rate and maximum

volume included here are those described in the similar

method OSHA ID105. Samples are stable for at least 6 days

at ambient temperature.

Bulk sample, approx.

1 - 3 cubic inch volumeN/A 1.0%

EPA/600/M4- 82-

020, Dec. 1982

PLM

NC $17

Sample is assumed to be homogeneous

Bulk sample, approx.

1 - 3 cubic inch volumeN/A 1.0%

EPA- 600/R-93/116,

July 1993

PLM

NC $17

Price per layer

Asbestos Bulk ID

N/A

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Asbestos Bulk Point Count

N/ABulk sample, approx.

1 - 3 cubic inch volumeN/A <1.0%

EPA- 600/R-93/116,

July 1993

PLM

NC $51

Asbestos Fiber Count See Fiber Count.

Asbestos Wipe/

Vacuum Wipe

N/A

C-01

MCEF, 25mm, 0.8um, 3PC,

long cowl

N/A 10 - 16 LPM NA

EPA-600/M4- 82-

020, Dec. 1982

PLM

NC $28

Presence/absence measurement only for all forms of

asbestos; test requires a visible filter deposit be present.

Asphalt Fumes, measured

as Total Particulate and

Benzene Soluble Fraction

N/A

C-09

PTFE, Pre-weighed, 37mm,

2um, 2PC

28 - 400 1 - 4 30

NIOSH 5042

Gravimetric, with

extraction

MM $110

Ship refrigerated for overnight delivery. For benzene

solubles results above 0.2 mg/M3, client may elect to run

the PAH screen. If PAHs are desired, wrap cassette in foil

during sampling to protect from light. Includes total

particulate and benzene solubles reporting.

Barium

Total 7440-

39-3

C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300

ICPT $40

Barium Sulfate

Respirable

7727-43-7

- $-

See Particulates, Respirable. Sample may also be tested for

Total Barium, but test is not specific for barium sulfate.

Barium Sulfate

Total

7727-43-7

- $-

See Particulates, Total. Sample may also be tested for Total

Barium, but test is not specific for barium sulfate.

Barium,

Soluble Compounds

7440-39-3

C-05

MCEF, 37mm, 0.8um, 3PC300 1.5 3

NIOSH 7300M

ICPJ $68

Measurement of water-soluble barium compounds.

BCME

542-88-1- $-

See Bis(Chloromethyl)Ether

Benzaldehyde

100-52-7

T-119


226-119

2 - 30 0.2 - 1.0 1.00TO-11

HPLCN $116

Refrigerate before and after sampling and ship overnight.

Ozone may interfere - use ozone scrubber in known ozone





interferences. Media contains residual acetonitrile which


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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzene

71-43-2

T-01

Charcoal, 226-012 - 30 0.01 - 0.2 2

NIOSH 1501

GC/FIDA $56

M-01

SKC POVM, 575-00115 - 240 Min. 0.016 4.0

NIOSH 1501M

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0355 3

NIOSH 1501M

GC/FIDA $56

T-81

Anasorb 747, 226-81

TWA 30

STEL 3 0.03-0.2 1.1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-00215 - 240 Min. 0.0171 2.2

Proprietary,

IHGC-P029

GC/FID

A $77

M-N521

Assay Technology POVM,

N521

15 - 480 Min. 0.073 2.0 A $56

Benzene Soluble

Fraction N/AC-06

GFF, 37mm, 1um, 3PC960 1 - 2 30

OSHA 58

Gravimetric with

extraction

MM $116

This is the same test as Coal Tar Pitch Volatiles by OSHA 58.

Transfer filter into glass vial using tweezers immediately

after sampling; wrap vial in foil to protect from light.

Additional specific PAH analysis is available as follow-up if

needed for samples with BSF exceeding 0.2 mg/M3.

C-09

PTFE, Pre-weighed, 37mm,

2um, 3PC

28 - 400 1 - 4 30

NIOSH 5042

Gravimetric with

extraction

MM $116

Test includes measurement of Total Particulates and

Benzene Soluble Fraction. This is the NIOSH approach for

both Coal Tar Pitch Volatiles and Asphalt Fumes. Protect

samples from light if follow-up PAH analysis is needed.

Benzidine

92-87-5C-07

GFF, 13mm, 1um, 2PC

Swinnex

20 - 100 0.2 0.2NIOSH 5509

HPLCNC $116

Transfer filter and Teflon ring to vial after sampling. Store in

freezer, ship on dry ice for overnight delivery. Stable at

least 11 days at -15° C.

1,2-Benzisothiazolin-3-one

(BIT)

2634-33-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.3

IHO- HPLC-070

HPLC/UVK $160

Samples stable up to 21 days at ambient temperature.

Benzo(a)anthracene

56-55-3 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Benzo(b)fluoranthene

205-99-2 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzo(k)fluoranthene

207-8-9 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Benzo(g,h,i)perylene

191-24-1 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Benzo (a) pyrene

50-32-8 C-06

GFF, 37mm, 1um, 3PC960 2.0 3

OSHA 58

HPLC/FLMM $116

Place filter into glass vial using tweezers and wrap with foil

to protect from light. Ship refrigerated by overnight

delivery. Also see selected PNA Profile.

K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

Benzophenone

119-61-9

T-110

Chromosorb 106,

226-110

48 Max 0.2 Max 1.6OSHA PV2130

GC/FIDNC $56

Samples are stable at ambient temperature for at least 14

days.

Benzoyl Chloride

98-88-4T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC-FID

NN $77

Other chloroformates/acid chlorides may be tested from

the same sample. Store media and samples cold, ship

samples cold overnight. Samples must arrive at lab within

10 days of collection.

Benzoyl Peroxide

94-36-0C-05

MCEF, 37mm, 0.8um, 3PC40 - 400 1 - 3 1

NIOSH 5009

HPLC/UVNC $116

Ship refrigerated for overnight delivery.

Synonym: Dibenzoyl peroxide.

Benzoyl Peroxide

Inhalable

94-36-0

Call lab 960 Max 2.0 1NIOSH 5009M

HPLCNC $116

Important Note: 1. The IOM sampler should be operated

at 2 Lpm in order to correctly collect the particle size range

(up to 100 um) which comprises inhalable particles. 2. This

listing modifies NIOSH method 5009, which does not take

into account monitoring of inhalable particulates. The

maximum air volume of 400 L recommended in method

5009 has been increased to 960 L in this listing in order to

allow for a full-shift sample at the 2 Lpm sampling rate

required for the IOM sampler. However, if analytical results

show a filter loading of 1 to 2 milligrams or greater,

consider resampling for a shorter time period. 3. If

available, ship samples by overnight delivery to the lab in

an insulated container with cold pack (9% loss of material

from filter has been measured after 1 week @ 25 C).

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Benzyl Acetate

140-11-4

T-01

Charcoal, 226-0110 - 50 0.1 - 0.2 20

OSHA CSI

GC/FIDA $56

Benzyl Alcohol

100-51-6

T-01

Charcoal, 226-0110 - 24 0.01 - 0.2 20

NIOSH 1402M

GC/FIDD $56

T-95

XAD-7, 226-95

TWA 24

STEL 4.5

TWA 0.02- 0.1

STEL 0.3 2

OSHA 32M

HPLCK $116

Benzyl Chloride

100-44-7

T-01

Charcoal, 226-016 - 50 0.01 - 0.2 5

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0272 7.5

NIOSH 1003M

GC/FIDA $56

Benzylchloroformate

501-53-1

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77

Store media and samples cold, ship samples cold overnight.


Beryllium

7440-41-7

C-05

MCEF, 37mm, 0.8um, 3PC200 - 2000 1.0 - 4.0 0.005

NIOSH 7300M

ICP/MST $46

Not appropriate for monitoring “high-fired” beryllium

oxide. When monitoring “high-fired” beryllium oxide (such

as manufactured for use in ceramics in electronic

Applications, and in lasers), contact the lab prior to

sampling. The combination of digestion

technique/analytical technique/ method sensitivity must

be carefully chosen to obtain accurate results. Contact lab

for further information.

C-05

MCEF, 37mm, 0.8um, 3PC200 - 2000 1.0 - 4.0 0.05

OSHA ID125M

ICPEE $40

This approach is suitable for analysis of high-fired beryllium

oxide.

Beryllium

Wipe

7440-41-7

K-07

Ghost Wipe Kit100 cm2 - 0.01

NIOSH 7102M

GFAAT $51

This approach is NOT suitable for analysis of high-fired

beryllium oxide.

K-07

Ghost Wipe Kit100 cm2 - 0.1

OSHA ID125M

ICPEE $40

This approach is suitable for analysis of high-fired beryllium

oxide.

Biphenyl

92-52-4$-

See Diphenyl.

Bis (Chloromethyl) Ether

(BCME)

542-88-1

T-89

TCP-treated XAD- 4,

226-89

TWA 20

STEL 4.5 0.05-0.3 0.014

Proprietary,

IHGC-P011

GC/ECD

NC $153

Immediately after sampling heat treat tube(s) at 75°C for 45

minutes. Wrap in aluminum foil to protect from light.

Chloromethyl Methyl Ether can be determined on same

tube.

Bismuth

1304-82-1C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300M

ICPT $40

Bisphenol A

80-05-7

C-06

GFF, 37mm, 1um, 3PC300 1.6 2

NIOSH PCAM 333

HPLCN $116

Store samples in freezer. Ship cold overnight.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Boric Acid

(measured as Boron)

10043-35-3

C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 12

NIOSH 7300M

ICP-OEST $40

Samples are acid digested and tested for boron; equivalent

H3BO3 is calculated mathematically. Test is not specific for

boric acid.

Boron

7440-42-8C-05

MCEF, 37mm, 0.8um, 3PC50 - 500 1.0 - 3.0 2

NIOSH 7300M

ICPT $40

Bromine

7726-95-6

IMP-09

Impinger,

NaH- CO3/ Na2CO3

80 - 240 0.5 7.5OSHA ID 108

ICNC $69

Impinger solution available from laboratory.

C-16

Ag/PTFE, Cl2/Br2 Sampler,

25mm, 3PC

15 - 360 0.3 - 1.0 5.0NIOSH 6011

ICAA $69

Preferred method. Precleaning of filter required prior to

shipment. Cassette has short shelf life. Avoid direct sunlight

on filter during or after sampling. Chlorine can also be

measured as well as bromine.

Bromoethane

74-96-4- $-

See Ethyl Bromide

Bromoform

75-25-2

T-01

Charcoal, 226-014 - 70 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0293 30

NIOSH 1003M

GC/FIDA $56

Bromomethane

74-83-9$-

See Ethyl Bromide

1-Bromopropane

106-94-5T-01

Charcoal, 226-0112 Max 0.2 Max 0.5

NIOSH 1011M

GC/FIDA $56

The larger charcoal tube 226-09 may be used for greater

capacity at higher concentrations.

Synonym: n-Propyl bromide

M-3500

3M POVM, 3500Up to 8 hours 0.032 1.5

NIOSH 1011M

GC/FIDA $56

3M 3520 is recommended for 8-hour samples collected at

high humidity (>80%).

BTEX Profile

N/A T-01

Charcoal, 226-015 - 15 0.05 - 0.2

See

comments

NIOSH 1501

GC/FIDA $127

Profile includes Benzene (LOQ = 2 ug), Ethyl Benzene (LOQ

= 5 ug), Toluene (LOQ = 5 ug), Xylene (LOQ = 5 ug), Total

Hydrocarbons as Hexane (LOQ = 20 ug).

M-01 SKC POVM,

575-001Up to 8 hours Various

See

comments

NIOSH 1501M

GC/FIDA $127


= 10 ug), Toluene (LOQ = 10 ug), Xylene (LOQ = 10 ug), Total

Hydrocarbons as Hexane (LOQ = 40 ug).

M-3500

3M POVM, 3500Up to 8 hours Various

See

comments

NIOSH 1501M

GC/FIDA $127


= 7.5 ug), Toluene (LOQ = 7.5 ug), Xylene (LOQ = 7.5 ug),

Total Hydrocarbons as Hexane (LOQ = 30 ug).

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,3-Butadiene

106-99-0

T-73

TBC-Treated charcoal,

226-73

3 Max 0.01 - 0.05 2OSHA 56

GC/FIDA $56

Preferred method. Store collected samples under

refrigeration, and ship refrigerated overnight. Samples are

stable at least 17 days if stored cold.

T-09

(2) Charcoal, 226-095 - 25 0.01 - 0.5 8

NIOSH 1024

GC/FIDI $56

Two 226-09 tubes in series; cap separately after sampling.

Ship cold overnight, store in freezer after sampling.

M-3520

3M POVM 3520, 2-stageUp to 8 hours 0.0428 3

NIOSH 1024M

GC/FIDI $56

1,3-Butanediol

107-88-0- $-

See 1,3-Butylene Glycol

1,4-Butanediol

110-63-4- $-

See 1,4-Butylene Glycol

n-Butanol

71-36-3- $-

See n-Butyl alcohol

Sec-Butanol

78-92-2- $-

See sec-Butyl Alcohol.

t-Butanol

75-65-0- $-

See tert-Butyl alcohol.

2-Butanone

78-93-3- $-

See Methyl Ethyl Ketone.

2-Butoxyethanol

111-76-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.1 20

NIOSH 1403M

GC/FIDE $56

Also known as Butyl Cellosolve, Ethylene Glycol Monobutyl

Ether, and Dowanol EB

M-3500

3M POVM, 3500Up to 8 hours 0.0282 30

NIOSH 1403M

GC/FIDE $56

Also known as Butyl Cellosolve, Ethylene Glycol Monobutyl

Ether, and Dowanol EB

2-Butoxyethyl Acetate

112-07-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

OSHA 83

GC/FIDE $56

Also known as Butyl Cellosolve Acetate and Ethylene Glycol

Monobutyl Ether Acetate

M-3500

3M POVM, 3500Up to 8 hours 0.0243 30

OSHA 83M

GC/FIDE $56

Also known as Butyl Cellosolve Acetate and Ethylene Glycol


1-Butoxy-2-Propanol

5131-66-8-

See Propylene Glycol n-Butyl Ether

n-Butyl Acetate

123-86-4

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

T-81

Anasorb 747, 226-8110 0.03-0.2 1.1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min 0.013 2.2

Proprietary,

IHGC-P029

GC/FID

A $77

M-3500

3M POVM, 3500Up to 8 hours 0.0316 30

NIOSH 1450M

GC/FIDA $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

s-Butyl Acetate

105-46-4

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0286 30

NIOSH 1450M

GC/FIDA $56

t-Butyl Acetate

540-88-5

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0294 30

NIOSH 1450M

GC/FIDA $56

n-Butyl Acrylate

141-32-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1450M

GC/FIDA $56

Also see Acrylate Monomer Profile.

M-3500

3M POVM, 3500Up to 8 hours 0.0273 30

NIOSH 1450M

GC/FIDA $56

T-73


226-73

1 - 12 0.01 - 0.05 20OSHA CSI

GC/FIDA $56

M-02

SKC POVM, 575-00230 min - 8 hours 0.012 2.5

Proprietary,

IHGC-P029

GC/FID

A $77

Recommended passive sampling method.

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

n-Butyl Alcohol

71-36-3

T-01

Charcoal, 226-012 - 10 0.01 - 0.2 20

NIOSH 1401

GC/FIDC & A $56

M-3500

3M POVM, 3500Up to 8 hours 0.0343 30

NIOSH 1401M

GC/FIDC $56

sec-Butyl Alcohol

78-92-2

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2 20

NIOSH 1401

GC/FIDC $56

M-3500

3M POVM, 3500Up to 8 hours 0.0348 30

NIOSH 1401M

GC/FIDC $56

t-Butyl Alcohol

75-65-0

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2 20

NIOSH 1400

GC/FIDC $56

M-3500

3M POVM, 3500Up to 8 hours 0.0352 30

NIOSH 1400M

GC/FIDB $56

Butyl Carbitol

112-34-5- $-

See Diethylene Glycol Monobutyl Ether.

Butyl Carbitol Acetate

124-17-4- $-

See Diethylene Glycol Monobutyl Ether Acetate

Butyl Cellosolve

111-76-2- $-

See 2-Butoxyethanol.

Butyl Cellosolve Acetate

112-07-2- $-

See 2-Butoxyethyl Acetate.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

n-Butyl Glycidyl Ether

2426-08-6

T-01

Charcoal, 226-0115 - 30 0.01 - 0.2 20

NIOSH 1616

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0270 30

NIOSH 1616M

GC/FIDA $56

t-Butyl Glycidyl Ether

7665-72-7

T-01

Charcoal, 226-0115 - 30 0.01 - 0.2 20

NIOSH 1616M

GC/FIDA $56

tert-Butyl Hydrazine

Hydrochloride, as

Particulate

7400-27-3

C-11

PVC, Preweighed, 37mm,

5um, 2PC

TWA 960

STEL 60 1-4 50

NIOSH 0500

Gravimetric$21

Not chemical specific.

tert-Butyl Hydroperoxide

75-91-2

…BHP

T-47-01

Silica Gel, 226-47-01

TWA 10

STEL 3

TWA 0.05-0.2

STEL 0.22

IN-HOUSE

GC/MSK $160

Samples are stable at least 9 days. Three (3) sample

minimum.

Butyl Isocyanate

111-36-4

K-20

GFF, 2PP-treated, C-1415-30 1.0 Max 0.4

OSHA Stopgap

HPLC/UVO $116

Sample open faced. Refrigerate media before and after

sampling. Ship cold by overnight delivery. Testing is for

both 2,4- and 2,6-TDI isomers. Media has 2-month shelf life

(stored cold). OSHA National Emphasis Program specifies

field desorption immediately after sampling; the K-20 kit

includes C-14 cassette, V-04 vial with 3mL 90/10 (v/v)

acetonitrile/dimethyl sulfoxide, tweezers(2), rack,

instruction set, SDS for solution. Contact lab for more

specifics.

N-Butyl Lactate

138-22-7

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.21

OSHA PV2080

GC/FIDE $77

Butyl Mercaptan

109-79-5

C-48

GFF, Hg Acetate-Treated,

37mm, 2PC,

SKC PN 225-9007

TWA 20

STEL 3 - 150 Max0.2 Max -

NIOSH 2542

GC/FPDNC

Call for

pricing

Store media cold before use. Protect samples from light.

Subcontracted to an outside laboratory. Samples stable at

least 3 weeks at 25ºC.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Butyl Methacrylate

97-88-1

T-30-04

XAD-2, 226-30-041 - 8 0.05 - 0.1 20

NIOSH 2537M

GC/FIDDD $56 Also see Acrylate Monomer Profile.

T-81

Anasorb 747, 226-81TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1.3

Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002TWA 8 hr (Max)

STEL 15 min 0.01 2.6

Proprietary,

IHGC-P029

GC/FID

A $77 Recommended passive sampling method.

n-Butyl Phthalate

84-74-2- $- See Dibutyl Phthalate.

n-Butylamine

109-73-9

T-30-18

NITC-Treated XAD-2,

226-30-18

3 - 30 0.01 - 1.0 4NIOSH 2540M

HPLCN $116

Store media cold before sampling. Samples stable at

ambient temperature for at least 15 days.

1,3-Butylene Glycol

107-88-0T-57

GFF/XAD-7 OVS, 226-571 - 20 0.01 - 0.10 20

NIOSH 5523

GC/FIDK $77 Also see Glycol Profile.

1,4-Butylene Glycol

110-63-4T-57

GFF/XAD-7 OVS, 226-5760 - 1000 0.5 - 1.0 80

NIOSH 5523M

GC/FIDK $77

Butyraldehyde

123-72-8

T-119


226-119

2 - 30 0.2 - 1.0 0.8TO-11

HPLCN $116

Refrigerate before and after sampling and ship overnight.

Ozone may interfere - use ozone scrubber in known ozone





interferences. Media contains residual acetonitrile which


gamma- Butyrolactone

96-48-0

T-01

Charcoal, 226-0110 Max 1 Max 20

OSHA Stopgap

GC-FIDE $56

Cadmium

7440-43-9

C-05

MCEF, 37mm, 0.8um, 3PC 800 - 1000 1.0 - 3.0 0.5NIOSH 7300

ICPT $40

C-05

MCEF, 37mm, 0.8um, 3PC 800 - 1000 1.0 - 3.0 0.025NIOSH 7300M

ICP/MST $46

Calcium

7440-70-2C-05

MCEF, 37mm, 0.8um, 3PC100 - 1000 1.0 - 3.0 2

NIOSH 7300

ICPT $40 Consult TLV booklet for form of analyte.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Camphor

76-22-2

T-01

Charcoal, 226-011 - 25 0.01 - 0.2 10

NIOSH 1301

GC/FIDH $56

M-3500

3M POVM, 3500Up to 8 hours 0.0214 15

NIOSH 1301M

GC/FIDH $56

Caprolactam

Vapor

105-60-2

T-57

GFF/XAD-7 OVS,

226-57

100 1 Max 10OSHA PV2012

HPLCK $116 Vapor analysis only.

Caprolactam

Vapor + Particulate

105-60-2

T-57

GFF/XAD-7 OVS,

226-57

100 1 Max 10OSHA PV2012

HPLCK $160

Filter (particulate) and sorbent beds (vapor) are all tested

and reported separately; a cumulative result for all three

sections is also reported.

Carbitol (DGMEE)

111-90-0- $- See Diethylene Glycol Monoethyl Ether

Carbitol Acetate

112-15-2- $- See Diethlylene Glycol Ethyl Ether Acetate

Carbon Black

(as Total Particulate)

1333-86-4

C-11


5um, 2PC

100 - 960 1.0 - 2.0 50NIOSH 0500

GravimetricNC $21

Any and all other particulates will be a positive interference

with the gravimetric analysis. More specific analysis for

Carbon Black by OSHA ID196 is available as a subcontracted

analysis. Also see the entry for Elemental Carbon.

Carbon Dioxide

124-38-9Call Lab 3.5 - 500

OSHA ID172

GC/TCDNC $- Analysis is subcontracted.

Carbon Disulfide

75-15-0

T-44 & T-01

in series Drying Tube,

226-44, preceding

Charcoal, 226-01

25 Max 0.2 MaxNIOSH 1600

GC/FPDNC

Call for

pricing

Precede the charcoal tube with a drying tube (PN 226-44).

Store and ship cold, with drying tube still attached.

Subcontracted to outside laboratory.

Carbon Tetrabromide

558-13-4T-93

XAD-4, 226-93

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.2

OSHA Stopgap

GC/ECDNC

Call for

pricing

Important Note: Contact the laboratory before sampling in

order to allow time for set up. Subcontracted to outside

laboratory.

Tetrachloromethane

56-23-5

T-01

Charcoal, 226-013 - 150 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0302 30

NIOSH 1003M

GC/FIDA $56

Carbonyl Chloride

75-44-5- $- See Phosgene

Catechol

575-001

T-95

XAD-7, 226-9524 Max 0.1 Max 30

OSHA Stopgap

GC/FIDA $56

Cellosolve

110-80-5- $- See 2-Ethoxyethanol

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Cellosolve Acetate

111-15-9- $- See 2-Ethoxyethyl Acetate

Cerium Oxide

1306-38-3 C-05

MCEF, 37mm, 0.8um, 3PC960-1920 2-4 2.5 ICP T $77

Call to schedule analysis to ensure standard is in stock.

Three (3) sample minimum. Testing is for elemental cerium,

with mathematical calculation of cerian oxide.

Chlordane

57-74-9

T-30-16

GFF/XAD-2 OVS,

226-30-16

10-480 0.5 - 1.0 0.8OSHA 67

GC/ECDNC $102 Also see Chlorinated Pesticide Profile.

Chlorine

7782-50-5C-16

Ag/PTFE, Cl2 / Br2

Sampler, 25mm, 3PC

15 - 90 0.3 - 1.0 2.5NIOSH 6011

ICAA $69

Membrane has short shelf life. Protect from direct sunlight

or prolonged UV (fluorescent) light. Bromine vapor can also

be measured on same sampling device. Samples are stable

for at least 30 days after sampling.

Chlorine Dioxide

10049-04-4

IMP-04

MFGB, 15 mL 0.02% KI in

NaH-CO3/ Na2CO3

10 - 120 0.5 10OSHA ID 202

ICNC $153

Protect solution from light. Collection solution must stay

basic; a large concentration of acid gas (such as SO2) may

exceed the solution buffering capacity. Avoid this by

1) collecting smaller volume of air in such atmospheres, or

2) check solution pH after sampling and discard if acidic.

Midget Fritted Glass Bubbler (MFGB) Impinger solution is

available from the laboratory. Advance notice is required

due to instability of reagent. Collected samples are stable

at least 30 days.

5-Chloro-2-Methyl-4-Isothi-

azolin-3-One

(RH-651)

26172-55-4

K-12

Methanol-moistened

cotton-fabric swab Wipe 100 CM2 area N/A 1.20IHHPLC-P007

HPLC/UVJJ $160

Sampling media is methanol moistened cotton fabric swab

and requires immediate methanol extraction.

TexWipe®TX306, Fisher Scientific, Cat. # 18-308D cut in 2 in

x 2 in squares. Sampling media including methanol, vials,

pipette, and sampling instructions are available from

laboratory.

T-99

GFF/Silica Gel OVS,

226-99 TWA 50

STEL 7.5

0.2 TWA

0.5 STEL0.2

IHHPLC-P008

HPLC/UVJJ $160

Avoid and ensure that the outside of the OVS tube is not

contaminated when sampling atmospheres potentially

containing Kathon 886 ® Biocide as either a particulate or

aerosol. Component of Kathon 886 ® Biocide. Also see 2-

Methyl-4 Isothiazolin-3-one.

3-Chloro 2-Methyl-1-

Propene

563-47-3

T-81

Anasorb 747, 226-81

TWA 48

STEL 3 0.20 0.07

IN-HOUSE

GC/MSNC $160 Synonym: Methallyl Chloride

Chloroacetyl Chloride

79-04-9

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 10.00

AIHA J 12/1986,

pp 742-746

GC-FID

NN $77Store media and samples cold, ship samples cold overnight.

Samples must reach lab within 10 days of sampling.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Chloroacetic Acid See Monochloroacetic Acid

Chlorobenzene

108-90-7

T-01

Charcoal, 226-011.5 - 40 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0293 30

NIOSH 1003M

GC/FIDA $56

p-Chlorobenzotrifluoride

98-56-6

T-01

Charcoal, 226-0110 Max 0.2 Max 10

OSHA Stopgap

GC/FIDA $56

M-3520

3M POVM, 3520Up to 8 hours 0.0258 15

OSHA Stopgap

GC/FIDA $56

Chlorobromomethane

74-97-5

T-01

Charcoal, 226-010.5 - 8 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

Chlorodifluoromethane

75-45-6

M-3520

3M POVM 3520,

2-stage

Up to 8 hours 0.0413 50NIOSH 1018M

GC/FIDA $77 Note low air volumes.

O-91

Carbosieve S-III0.1 - 1.0 0.01 - 0.05 50

OSHA CSI

GC/FIDA $77 Note low air volumes.

T-09 (2)

Charcoal, 226-091 - 4 0.01 - 0.05 50

NIOSH 1018M

GC/FIDA $77

Sample with two tubes in series (back tube can be smaller

226-01). Note low air volumes.

Chloroethene See Vinyl chloride

1-Chloro-2,

3-epoxypropane

106-89-8

- $- See Epichlorohydrin

Chloroethane

75-00-3- $- See Ethyl Chloride

Chloroform

67-66-3

T-01

Charcoal, 226-011 - 50 0.01 - 0.2 10

NIOSH 1003

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0335 15

NIOSH 1003M

GC/FIDA $56

Chloromethane

74-87-3- $- See Methyl Chloride

Chloromethyl Benzene

100-44-7- $- See Benzyl chloride

Chloromethyl Methyl Ether

(CMME)

107-30-2

T-89

TCP-treated XAD-4,

226-89

TWA 20

STEL 4.5 0.05-0.3 0.018

Proprietary,

IHGC-P011

GC/ECD

NC $153Immediately after sampling heat treat tube(s) at 75°C for 45

minutes. Wrap in aluminum foil to protect from light. BCME

can be analyzed on same sample.

o-Chlorophenol

95-57-8T-10

Silica Gel, 226-10

TWA 10-40

STEL 3

TWA 0.05-0.2

STEL 0.2 2.00

NIOSH 2014

HPLC/UVN $116

V01 06.2017

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

o-Chloro-P-Nitroaniline

121-87-9 C-05

MCEF, 37mm, 0.8um, 3PC

TWA 480

STEL 60

TWA 1-4

STEL 4 10

NIOSH 5033

HPLC/UVNC

Call for

pricing

Subcontracted to outside laboratory. The referral

laboratory will analyze for o-chloro-p-nitroaniline on

request using the same method as p-nitroanaline.

Chloroprene

(beta-chloroprene)

126-99-8

T-01

Charcoal, 226-01 1.5 - 8 0.01 - 0.05 20NIOSH 1002

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0322 30

NIOSH 1002M

GC/FIDA $56

3-Chloropropene

107-05-1- $- See Allyl Chloride

o-Chlorotoluene

95-49-8

T-01


NIOSH 1003M

GC/FIDA $56

M-3500

3M POVM 3500Up to 8 hours 0.027 30

NIOSH 1003M

GC/FIDA $56

Chlorpyrifos

2921-88-2

T-30-16

GFF/XAD-2 OVS,

226-30-16

480 1.0 - 1.5 0.2OSHA 62M

GC/ECDNC $102

Chromium, Total

7440-47-3C-05

MCEF, 37mm, 0.8um, 3PC50 - 1000 1.0 - 3.0 2

NIOSH 7300M

ICPT $40 This method measures total chromium - metallic and salts.

Chromium, Low Level, Total

7440-47-3C-MCE-NN

MCE, Low Metals, 37mm,

0.8um, 2PC

50 - 1000 1.0 - 3.0 0.13NIOSH 7300M

ICP/MST $46

Chromium, Hexavalent

Different for each

compound

C-10

PVC, 37mm, 5um, 3PC30 - 960 2 0.025

OSHA ID215v2

ICNC $102

Recommended Method. Sample stability varies with

exposure source monitored. Identify operation sampled

(spray paint, chrome plating, welding, etc.) on Request for

Analysis form. Ship overnight within 24 hours of sampling

to meet all holding times. CrVI from acidic solutions, such

as plating, must be extracted in the lab within 6 days of

collection. CrVI from metalworking must be extracted in

the lab within 8 days of collection. 25 mm PVC filter

cassette (PN C-41) may be used to facilitate sampling under

a helmet or hood.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment


(Welding and Other Hot

Environments) Different for

each compound

C-53

PVC, 37mm, 5um, Quartz

support, 2PC

30 - 960 2 Max 0.025OSHA ID215v2

ICNC $102

Hot environments sometimes cause the 37mm cassettes to

expand resulting in leakage around the PVC filter onto the

backup pad. The quartz fiber backup pads in C-53 cassettes

are analyzed along with the PVC filters. See hold time

description included above.


Wipe

Different for each

compound

C-53

(PVC and/or quartz filter)

PVC, 37mm, 5um, Quartz

support, 2PC

100 cm2 N/A 0.025OSHA W4001M

ICNC $102

Cassette holds both PVC and Quartz filters; wipe samples

can be collected using either or both filters. Fold exposed

side in, and transfer into vial (PN V-15). Identify operation

sampled (spray paint, chrome plating, welding, etc.) on

Request for Analysis form. Ship overnight within 24 hours

of sampling to meet all holding times.

Chromium, Hexavalent Bulk

Sample Different for each

compound

1 gram Approx. N/A0.1 ug/g

Approx.

OSHA ID215v2

ICNC $102 Material must be homogenous and finely divided.

Chromic Acid - Soluble

Chromates

1333-82-0C-10

PVC, 37mm, 5um, 3PC1000 1.0 - 4.0 0.2

NIOSH 7600

SPECNC $69

OSHA ID215 is preferred method. Filter must be removed

from cassette and placed into a glass vial immediately after

sampling. Possible interferences include copper, iron,

nickel, and vanadium.

Chrysene

218-01-9 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

CMME

107-30-2$-

See Chloromethyl Methyl Ether. BCME can be analyzed on

same sample.

Coal Tar Pitch Volatiles,

measured as Benzene

Soluble Fraction (BSF)

65996-93-2

C-06

GFF, 37mm, 1um, 3PC960 2.0 60

OSHA 58

Grav/BZ SolMM $100





Cobalt

7440-48-4

C-05

MCEF, 37mm, 0.8um, 3PC 400 - 1000 1.0 - 3.0 2NIOSH 7300M

ICPT $40

May also be tested with tungsten per OSHA Method ID-

213.

C-05


ICP-MST $46

May also be tested with tungsten per OSHA Method ID-

213.

Coke Oven Emissions

67-63-0 C-06

GFF, 37mm, 1um, 3PC2.0 30

OSHA 58

Grav/BZ SolMM $100





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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Copper

7440-50-8

C-05

MCEF, 37mm, 0.8um, 3PC 40 - 1000 1.0 - 3.0 1NIOSH 7300

ICPT $40

C-05

MCEF, 37mm, 0.8um, 3PC 100 1-3 0.13NIOSH 7300M

ICP-MST $46 Analysis does not distinguish between dust and fume.

Cotton Dust

N/A

C-12


5um, 3PC

20 - 400 Elutriator 50 NC $21

Cresols, Total Isomers,

Vapor

1319-77-3

T-95

XAD-7, 226-9524 0.1 30

OSHA 32

HPLCK $116

Cresols and phenol can be sampled and analyzed from the

same sampler.

Cresols, Vapor and

Particulate

1319-77-3

T-57

GFF/XAD-7 OVS, 226-5748 0.1 30

OSHA 32M

HPLCK $116

Crotonaldehyde

4170-30-3

T-119


226-119

7.5 0.5 0.50EPA TO-11M

HPLC/UVN $116

Analysis is for a mix of cis- and trans- isomers. Refrigerate

before and after sampling and ship overnight. Ozone may

interfere - use ozone scrubber in known ozone contami-

nated areas. Any ketone or aldehyde will react with and

deplete the DNPH, and is a potential interference. ACGIH

states that if instantaneous monitoring is not feasible,

ceiling values “can be assessed by sampling over a period

that should not exceed 15 minutes, except for those

substances that may cause immediate irritation when

exposures are short.” Media contains residual acetonitrile

which could interfere with acetonitrile monitoring. Also see

Aldehyde profile.

Cumene

98-82-8

T-01

Charcoal, 226-0110 - 30 0.01 - 0.2 20

NIOSH 1501

GC/FIDA $53

M-3500

3M POVM, 3500Up to 8 hours 0.0245 30

NIOSH 1501M

GC/FIDA $56

T-81


STEL 3 0.03-0.2 1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02


STEL 15 min 0.013 2

Proprietary,

IHGC-P029

GC/FID

A $77

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Cupferron

135-20-6

IMP-11

Impinger, DI Water100.00 1.0 10

IN-HOUSE

HPLC/UVNC $160

Cyanides

Total VariousIMP-12

(order vials separately)

MFGB, 15 mL

0.1N KOH + 0.8um

PVC Prefilter

10 - 180 0.5 - 1.0 2.5NIOSH 7904

ISEFF $150

Analyze within five (5) days because particulate on filter

may liberate HCN gas; impinger samples are stable at least

30 days.

Cyanides, HCN and water-

soluble cyanide particulates T-28

Soda Lime, 226-282 - 90 0.2

2.6

(each

section)

NIOSH 6010M

ISENC $150

Before sampling, remove glass wool plug that precedes

glass fiber filter (stabilizes sampler during shipment).

Testing the prefilter for particulate cyanide allows this

sampler to provide both gaseous and particulate cyanide

results.

Cyanides - Gaseous (HCN)

See Hydrogen Cyanide - $- See Hydrogen Cyanide.

Cyanides - Water-soluble

Particulates, Various

C-05


ISEFF $69

Analyze within five (5) days because particulate on filter

may liberate HCN gas.

Cyclohexane

110-82-7

T-01

Charcoal, 226-012.5 - 5.0 0.01 - 0.2 20

NIOSH 1500

GC/FIDA $56

M-3500

3M POVM, 3500Up to 6 hours 0.0324 30

NIOSH 1500M

GC/FIDA $56

T-81

Anasorb 747,

226-81

TWA 10

STEL 3 0.03-0.2 1

Proprietary,

IHGC-P029

GC/FID

A $77

M02


STEL 15 min 0.02 2.1

Proprietary,

IHGC-P029

GC/FID

A $77

Cyclohexanol

108-93-0

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1402

GC/FIDD $56

M-3500

3M POVM, 3500Up to 8 hours 0.0295 30

NIOSH 1402M

GC/FIDD $56

T-81

Anasorb 747, 226-81 TWA 10 0.03-0.2 1.4

Proprietary,

IHGC-P029

GC/FID

A $77

M-02


STEL 15 min 0.01 2.7

Proprietary,

IHGC-P029

GC/FID

A $77

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Cyclohexanone

108-94-1

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1300

GC/FIDA $56

T-110

Chromosorb 106,

226-110

10 0.05 - 0.2 20OSHA 1

GC/FIDNC $56

M-3500

3M POVM, 3500Up to 8 hours 0.0289 30

NIOSH 1300M

GC/FIDA $56

T-81


STEL 3 0.03-0.2 1.4

Proprietary,

IHGC-P029

GC/FID

A $77

M-02


STEL 15 min 0.015 2.7

Proprietary,

IHGC-P029

GC/FID

A $77

Cyclohexene

110-83-8

T-01

Charcoal, 226-015 - 7 0.01 - 0.2 20

NIOSH 1500

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0323 30

NIOSH 1500M

GC/FIDA $56

T-81


STEL 3 0.03-0.2 1.1

Proprietary,

IHGC-P029

GC/FID

A $77

M-02


STEL 15 min 0.015 2.2

Proprietary,

IHGC-P029

GC/FID

A $77

Cyclohexylamine

108-91-8

T-30-18

NITC-Treated XAD-2, 226-

30-18

12 Max 0.1 Max 8NIOSH 2540M

HPLCN $116



Cyclopentadiene

542-92-7Call lab Maleic Andydride-

Treated Chromosorb 1043 0.01-0.05 -

NIOSH 2523

GC/FID- $- Sampling tube is treated Chromosorb-104 (special order).

Cyclopentane

287-92-3

T-01

Charcoal, 226-015 0.2 20

OSHA CSI

GC/FIDA $56

DBE (Dupont Dibasic

Esters™)

N/A

- $- See Dibasic Ester.

DBP

84-74-2- $- See Dibutyl Phthalate.

DDVP

62-73-7- $- See Dichlorvos.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Decafluoropentane

138495-42-8T-09

(2) Charcoal, 226-090.5 - 4 0.01 - 0.05 50

NIOSH 1018M

GC/FIDI $77

Two tubes in series; cap separately after sampling. Second

tube can be smaller 226-01. Store samples refrigerated,

ship cold overnight.

Decamethylcyclopentasi-

loxane

541-02-6

T-09

Charcoal, 226-09

TWA 96

STEL 30

TWA 0.2

STEL 2.0 10

IHGC-P040

GC/FIDA $77 Store samples in freezer, ship cold overnight.

n-Decane

124-18-5

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1500

GC/FIDA $56

M-3500


NIOSH 1500M

GC/FIDA $56

Desflurane

57041-67-5

T-81

Anasorb 747, 226-813 0.05 10

OSHA 106M

GC/FIDCC $69

Desmodur W

5124-30-1- $- See Methylene Bis(4-Cyclohexylisocyanate)

Di(2-Ethylhexyl) Phthalate

117-81-7T-56

GFF/Tenax OVS, 226-56

TWA 240

STEL 15 1.0 8

OSHA 104M

GC/FIDCC $81 Synonym: Di-sec-Octyl Phthalate, also DOP

Diacetone Alcohol

123-42-2

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1402

GC/FIDD $56 Synonym: 4-Hydroxy-4-methyl-2-pentanone

M-3500

3M POVM, 3500Up to 8 hours 0.0282 30

NIOSH 1402M

GC/FIDD $56

Diacetyl

431-03-8T-183

(2 in Series) Custom Silica

Gel, 226-183

TWA 9 Max

STEL 3 Max

0.050 Max

0.20 Max0.2

OSHA 1012

GC/ECDNC $110

Protect from light during sampling and storage wrapped

with aluminum foil). Store and ship samples cold. Ship

overnight. May be sampled on same tube with acetoin.

Filter built into tube faces incoming air stream. Samples

stable 17 days if stored cold. Three (3) sample minimum

charge will be applied.

Diatomaceous Earth,

Respirable as Particulate

61790-53-2- $- For speciation as amorphous silica, see Silica, Amorphous.

Diazinon

333-41-5T-57

GFF/XAD-7 OVS, 226-5712 - 240 0.2 - 1.0 0.02

OSHA 62

GC/ECDS $102

Dibasic Ester (DBE)

119-40-0T-01

Charcoal, 226-015 - 10 0.05 - 0.2 50

IHGC-P036

GC/FIDNC $77

Made from Dimethyl Adipates, Sebacates, and Glutarates.

Ship 5 ml sample of bulk material. DuPont product.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Dibenz(a,h)anthracene

53-70-3 K-06

PTFE + ORBO 43200-1000 2 3

NIOSH 5506

HPLCN $116





delivery.

DIBK - $- See Diisobutyl Ketone.

Diborane

19287-45-7

T-151

Oxidizer-Treated Charcoal,

226-151

60 - 260 0.5 - 1.0 5NIOSH 6006M

ICPNC $-

Samples are subcontracted to outside laboratory. PTFE

prefilter (C-45) required if particulate boron compounds

are present. Short shelf life media.

1,2-Dibromoethane

106-93-4- $- See Ethylene Dibromide.

Di-n-butylamine

111-92-2

T-30-18

NITC-Treated XAD-2,

226-30-18

10 0.1 2OSHA 60M

HPLC/UVN $116



Dibutyl Ether

142-96-1

T-01

Charcoal, 226-016 Max 0.01 - 0.2 10

NIOSH 1610 M

GC/FIDA $56

Dibutyl Phthalate

84-74-2

T-56

GFF/Tenax OVS, 226-56TWA 240

STEL 15 1.0 8

OSHA 104

GC/FIDCC $81

C-05

MCEF, 37mm, 0.8um, 3PC 10 - 200 1.0 - 3.0 20NIOSH 5020

GC/FIDA $56

1,1 Dichloroethene See Vinylidene Chloride

2,2-Dichloro-1,1,1-

Trifluoroethane

306-83-2

T-09 (2)

Charcoal, 226-090.25 - 3.0 0.01 - 0.05 40

NIOSH 2516M

GC/FIDI $77

4,5-Dichloro-2-N-Octyl-4-

Isothiazolin-3-one

64359-81-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.5

Proprietary,

IHHPLC-P002

HPLC/UV

NC $160Ensure outside of the sampler is clean before capping. Also

known as DCOIT, and RH-287. Sample may also be tested

for 2-n-Octyl-4-Isothiazolin-3-one.

o-Dichlorobenzene

95-50-1

T-01

Charcoal, 226-011 - 60 0.01 - 0.2 10

NIOSH 1003

GC/FIDA $56 Synonym: 1,2-Dichlorobenzene

M-3500

3M POVM, 3500Up to 8 hours 0.0278 15

NIOSH 1003M


p-Dichlorobenzene

106-46-7

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 10

NIOSH 1003


M-3500

3M POVM, 3500Up to 8 hours 0.0278 15

NIOSH 1003M


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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

3,4-Dichlorobenzotrifluo-

ride

328-84-7

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.2 4.8

OSHA Stopgap

GC/FIDA $77

Dichlorodifluoromethane

75-71-8

T-09 (2)

Charcoal, 226-091 - 4 0.01 - 0.05 50

NIOSH 1018

GC/FIDI $77

Two tubes in series. Second tube can be smaller 226-01

tube.

Dichlorodiphenyltrichlo-

roethane (DDT)

50-29-3

C-06

GFF, 37mm, 1um, 3PC100 1.5 0.2

NIOSH S274

GC/ECDS $102

1,1-Dichloroethane

75-34-3

T-01

Charcoal, 226-010.5 - 15 0.01 - 0.2 20

NIOSH 1003

GC/FIDA $56

M-3500


NIOSH 1003M

GC/FIDA $56

1,2-Dichloroethane

107-06-2- $- See Ethylene Dichloride.

1,2-Dichloroethene

540-59-0- $- See 1,2-Dichloroethylene, total.

1,1-Dichloroethene

75-35-4

T-01

Charcoal, 226-012.5 - 7.0 0.01 - 0.2 10

NIOSH 1015

GC/FIDA $56 Synonym; 1,1-Dichloroethylene

M-3500

3M POVM, 3500Up to 8 hours 0.0351 15

NIOSH 1015M

GC/FIDA $56

M-01

SKC POVM, 575-001Up to 8 hours 0.0123 20

NIOSH 1015M

GC/FIDA $56

1,1 Dichloroethylene See Vinylidene Chloride

1,2 Dichloroethylene, Total

(isomer mixture)

M-N566

Assay Technology POVM

AT N566

Up to 8 hours 0.00932 2.0NIOSH 1003M

GC/FIDRR $76

M-N521


AT N521

Up to 8 hours 0.0722NIOSH 1003M

GC/FIDA $76

M-01

SKC POVM, 575-00115 min. to 8 hours 0.0148 20

NIOSH 1003M

GC/FIDA $76

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,2-Dichloroethylene, total

(isomer mixture)

540-59-0, mixture of: trans-

1,2 156-60-5

cis-1,2 156-59-2

T-01

Charcoal, 226-01

0.2 - 5.0 0.01 - 0.2 10NIOSH 1003

GC/FIDA $76 Includes both -cis and -trans isomers.

M-3500


NIOSH 1003M

GC/FIDA $76

Also known as 1.2-Dichloroethene. Includes both -cis and -

trans.

1,1-Dichloro- 1-

fluoroethane

1717-00-6

T-09 (2)

Charcoal, 226-09 0.25 - 3.0 0.01 - 0.05 40NIOSH 2516M

GC/FIDNC $77 Also known as Refrigerant 141b. Two tubes in series.

O-91

Carbosieve S-III,

Orbo 91

1.0 0.05 Max 40OSHA 113

GC/FIDA $77 Also known as Refrigerant 141b. Two tubes in series.

Dichlorofluoromethane

75-43-4

T-09 (2)

Charcoal, 226-090.25 - 3.0 0.01 - 0.05 40

NIOSH 2516

GC/FIDA $77 Also known as Refrigerant 21. Two tubes in series.

Dichloromethane

75-09-2

T-01 (2)

Charcoal, 226-01 0.5 - 3 0.01 - 0.2 10NIOSH 1005

GC/FIDA $56

Also known as Methylene Chloride. Two tubes in series, cap

tubes separately after sampling and label front/rear.

Sample stable for 30 days at 5° C.

O-91

Carbosieve S-III,

Orbo 91

10 Max 0.01 - 0.1 10OSHA 80

GC/FIDNC $56

Also known as Methylene Chloride. Preferred active

sampling method.

M-01

SKC POVM, 575-0018 hours Max 0.0147 20

OSHA 80M

GC/FIDNC $56 Also known as Methylene Chloride.

M-3520

3M POVM 3520,

2-stage

Up to 8 hours

6 Hours Max in High

Humidity (80%)

0.0379 15NIOSH 1005M

GC/FIDA $56 Also known as Methylene Chloride.

4,5-Dichloro-2-N-Octyl-4-

Isothiazolin-3-one

64359-81-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0 0.5

IHHPLC-P002

HPLC/UVK $160 Synonyms: Kathon ® 930 Microbiocide, RH-287

Dichloropentafluoropro-

pane Ca & Cb- See Refrigerant 225 and AK225.

Dichloropentafluoropro-

pane- $- See Refrigerant 225 and AK225.

1,2-Dichloropropane

78-87-5- $- See Propylene dichloride.

1,2-Dichloro- 1,1,2,2-Tetra-

fluoroethane

76-14-2

T-09 (2)

Charcoal, 226-091 - 4 0.01 - 0.05 50

NIOSH 1018

GC/FIDI $77

Two tubes in series. Second tube can be smaller 226-01

tube. Synonym: R-114

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Dichlorvos

62-73-7

T-30-16

GFF/XAD-2 OVS,

226-30-16

120 1.0 0.2OSHA 62M

GC/ECDNC $102

Dicyclopentadiene

77-73-6

T-01

Charcoal, 226-0110.00 0.1 Max 5.0

OSHA 07

GC/FIDA $77

Diesel Exhaust Particulate

(<1 Um In Diameter)

7440-44-0- $- See Elemental Carbon.

Diesel Fuel

68334-30-5

T-01

Charcoal, 226-011 - 20 0.01 - 0.2 50

NIOSH 1550

GC/FIDA $77

Submit 5 ml of bulk in separate shipment with sample

number reference. Also see Kerosene.

Diethanolamine

111-42-2

T-30-18

NITC-Treated XAD-2,

226-30-18

10 0.1 2OSHA PV2018M

HPLCN $116

Store media cold before sampling. Samples are stable at


C-15

GFFs(2) H2SO4-treated,

37mm, 3PC

240 Max 1 Max 1J. Occ. Health,

2012, 54:340-343NC

Limited shelf live for sampler. Store samples in

refrigeration, ship cold overnight. Samples are stable at

least 5 days under refrigeration.

Diethyl Ether

60-29-7- $- See Ethyl Ether.

Diethylamine

109-89-7

T-96

NBD-chloride-treated

XAD-7, 226-96

10 0.2 2OSHA 41

HPLCW $116

T-30-18

NITC-Treated XAD-2,

226-30-18

10 0.1 2NIOSH 2540M

HPLCN $116 Store media cold before sampling.

Diethylaminoethanol

100-37-8

T-10-04


24 Max 0.2 Max 1

OSHA Stopgap

(NIOSH 2007M)

GC/NPD

NCCall for

pricing

Samples are subcontracted to outside laboratory.

Immediately after sampling, transfer each section of the

tube to separate vials containing 2 mL of 0.2 N HCl in

methanol: water (4:1). Obtain prepared vials from lab.

Synonym: 2-(Diethylamine)ethanol

T-98

H3PO4-treated XAD-7,

226-98

20 Max 0.2 Max -OSHA PV2060

GC/FIDNC

Call for

pricing

Store cold if not shipped immediately. Samples are

subcontracted to outside laboratory.

Diethylbenzene

(isomer mixture)

25340-17-4

T-01


NIOSH 1501M

GC/FIDA $56

Diethylene Glycol

111-46-6T-57

GFF/XAD-7 OVS, 226-5760 0.5 - 2.0 20

NIOSH 5523

GC/FIDJJ $77

Store and ship samples cold. Samples are stable at least 14

days. Also see Glycol Profile.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Diethylene Glycol

Chloroformate

106-75-2

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2 5

AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77Store media and samples cold, ship samples cold overnight.


Diethylene Glycol Dibutyl

Ether

112-73-2

T-01

Charcoal, 226-0110 0.01 - 0.05 20

NIOSH 1403M

GC/FIDE $56

Synonyms: 2-Butoxyethyl ether, also Bis(2-butoxyethyl)

ether, also Dibutyldiglycol

Diethylene Glycol Dimethyl

Ether

111-96-6

T-01

Charcoal, 226-0120 0.2 Max 20

NIOSH 1403M

GC/FIDE $56

Diethylene Glycol Ethyl

Ether Acetate

112-15-2

T-01

Charcoal, 226-0110 0.2 Max 20

NIOSH 1403M

GC/FIDE $56

Diethylene Glycol

Monobutyl Ether

112-34-5

M-3500

3M POVM, 3500 Up to 8 hours 0.0235 30NIOSH 1403M

GC/FIDE $56 Synonym: Butyl Carbitol

T-01

Charcoal, 226-012 - 10 0.01 - 0.05 20

NIOSH 1403M

GC/FIDE $56

Diethylene Glycol


124-17-4

T-01


NIOSH 1403M

GC/FIDE $56

Diethylene Glycol

Monoethyl Ether

111-90-0

T-01

Charcoal, 226-01 10 0.01 - 0.05 20NIOSH 1403M

GC/FIDE $56 Synonym: Carbitol

M-3500

3M POVM, 3500Up to 8 hours 0.0233 30

NIOSH 1403M

GC/FIDE $56

Diethylene Glycol

Monomethyl Ether

111-77-3

T-01

Charcoal, 226-01 10 0.2 Max 20NIOSH 1403M

GC/FIDE $56

M-3500

3M POVM, 3500Up to 8 hours 0.0235 30

NIOSH 1403M

GC/FIDE $56

Diethylenetriamine

111-40-0

T-30-18

NITC-Treated XAD-2,

226-30-18

TWA 10

STEL 3 STEL

TW 0.01-0.1

STEL 0.1 2

OSHA 60

HPLC/UVN $116



Diethylethanolamine

100-37-8- $- See diethylaminoethanol.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Diglycidyl Ether of

Bisphenol A

1675-54-3

C-06

GFF, 37mm, 1um, 3PC290 1.6 20

NIOSH P333

HPLCN $116 Store and ship cold after sampling.

Diglyme

111-96-6- $- See Diethylene Glycol dimethyl Ether.

Diisobutyl Ketone

108-83-8

T-01

Charcoal, 226-011 - 10 0.01 - 0.2 20

NIOSH 1300

GC/FIDA $56

T-81

Anasorb 747, 226-81TW 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1

Proprietary,

IHGC-P029

GC/FID

A $77

M-3500

3M POVM, 3500Up to 8 hours 0.0246 30

NIOSH 1300M

GC/FIDA $56

M-02


STEL 15 min 0.010 2

Proprietary,

IHGC-P029

GC/FID

A $77

Diisobutylene

25167-70-8

T-81

Anasorb 747,

226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2 1

Proprietary,

IHGC-P029

GC/FID

A $77Store media cold before sampling. Samples stable at


M-02


STEL 15 min 0.01 2

Proprietary,

IHGC-P029

GC/FID

A $77

Diisopropylamine

108-18-9

T-30-18

NITC-Treated XAD-2,

226-30-18

10 0.1 5OSHA 60M

HPLCN $116

Dimethoxymethane

109-87-5- $- See Methylal.

Dimethyl Adipate

627-93-0T-01

Charcoal, 226-0110 Max 0.2 20

Proprietary,

IHGC-P036

GC/FID

LL $56Refrigerate samples and ship cold overnight. Analyze within

2 weeks of collection.

Dimethyl Ether

115-10-6- See Methyl Ether

Dimethyl Ethylamine

598-56-1T-10

Silica Gel, 226-103 - 30 0.01 - 1.0 1

NIOSH 2007/2010

GC/FIDNC $- Samples are subcontracted to outside laboratory.

Dimethyl Glutarate

1119-40-0T-01

Charcoal, 226-0110 Max 0.2 20

Proprietary, IHGC-

P036 GC/FIDLL $56

Refrigerate samples and ship cold overnight. Analyze within


Dimethyl Phthalate

131-11-3

T-56

GFF/Tenax OVS,

226-56

TWA 240

STEL 15 1.0 20

OSHA 104

GC/FIDCC $81 Sample are stable for at least 2 weeks.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,1-Dimethyl propyl methyl

ether

994-05-8

- $- See Methyl tert-Amyl Ether.

Dimethyl Succinate

106-65-0T-01

Charcoal, 226-0110 Max 0.2 20

Proprietary,

IHGC-P036

GC/FID

LL $56Refrigerate samples and ship cold overnight. Analyze within


Dimethyl Sulfate

77-78-1T-115

Porapak-Q, 226-11535 Max 0.05 - 0.2 0.2

Proprietary,

IHGC-P006

GC/ECD

NC $160

Dimethyl Sulfoxide

67-68-5T-09

Charcoal, 226-09

TWA 3-24

STEL 3

TWA 0.05-0.1

STEL 0.2 3.9

OSHA 07

GC/FIDE $56

Dimethylacetamide

127-19-5

T-10

Silica Gel, 226-1015 - 80 0.01 - 1.0 20

NIOSH 2004

GC/FIDK $56

T-01

Charcoal, 226-0110 0.2 5

OSHA 66M

GC/FIDI $56

M-3500

3M POVM, 3500Up to 8 hours 0.0320 30

OSHA 66M

GC/FIDI $56

Dimethylacrylamide

(Vapor)

2680-03-7

T-10

Silica Gel, 226-10120 Max 1.0 Max 3.0

Preliminary HSE

MDHS 57M

HPLC/UV

NC $116Store and ship cold after sampling. Analyze within 2 weeks

of collection.

Dimethylamine

124-40-3

T-96


XAD-7, 226-96

10 0.2 2OSHA 34

HPLC UV OR FLW $116

T-30-18

NITC-Treated XAD-2,

226-30-18

20 Max 0.1 Max 4NIOSH 2540M

HPLC/UVN $116



Dimethylamine Borane

74-94-2

C-05


TWA 48-480

STEL 45

TWA 1

STEL 3 10.9

NIOSH 7300M

ICPT $40

This test is not chemically specific in that all sources of

Boron will contribute to the total result. On Analysis

Request form specify Boron analysis and request results

reported as PPM Dimethylamine Borane To convert Boron

results to Dimethylamine Borane in the same units,

multiply by 5.45.

N,N-Dimethylamine

75-64-9- $- See Dimethyl Ethylamine.

2-(Dimethylamino)ethanol

108-01-0 - $- See N,N-Dimethylethanolamine

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

3-Dimethylamino-1-propyl-

amine

109-55-7

T-95

XAD-7, 226-9524 Max 0.05 - 0.10 2

BASF AM-28

GC/FIDK $77

Store samples in freezer. Ship cold overnight within 24

hours of sampling.

N,N-Dimethylaniline

121-69-7

T-10

Silica Gel, 226-103 - 30 0.02 - 1.0 10

NIOSH 2002

GC/FIDM $56

2,3 Dimethyl-2,3-

Dinitrobutane

3964-18-9

T-35-03

Tenax, 226-35-032 - 4 0.02 - 0.05 0.4

NIOSH 2507M

GC/ECDNC $102

N,N-Dimethylethanolamine

108-01-0T-94

XAD-7, 226-94

TWA 10-24

STEL 1.5

TWA 0.02-0.1

STEL 0.1 2

NIOSH 2561M

GC-NPDNC $127

Synonym: N,N-Dimethyl-2-hydroxyethylamine, N,N-Di-

methylethanolamine, DMEA, Jeffcat DMEA

Dimethylformamide

68-12-2

T-10

Silica Gel, 226-1015 - 80 0.01 - 1.0 20

NIOSH 2004

GC/FIDK $56

M-3500

3M POVM, 3500Up to 8 hours 0.0355 7.5

OSHA 66

GC/NPDHH $56

T-01

Charcoal, 226-0110 0.2 1

OSHA 66

GC/NPDKK $127

Dimethylisopropylamine

996-35-0

T-94

XAD-7, 226-9410 - 24 0.02 - 0.1 5

NIOSH 2561M

GC/FIDK $127 Store and ship samples cold.

Dimethyltin Dichloride

753-71-1 T-30-16

GFF/XAD-2 OVS,

226-30-16

TWA 15-75

STEL 15 (Max)

TWA 0.25

STEL 1.0 0.1

NIOSH 5526

GC/FPDNC

Call for

pricing

Note: This is a labor-intensive analysis requiring a

dedicated instrument and there is a 3 sample minimum.

Analysis available for the following agents on one sample:

methyltin dichloride, dimethyltin dichloride, and

trimethyltin chloride. Samples are subcontracted to outside

laboratory.

Di-n-Octyl Phthalate

117-84-0T-56

GFF/Tenax OVS, 226-56240 1.0 50

OSHA 104

GC/FIDCC $81 Synonym: DNOP

Di-sec-Octyl Phthalate

(DOP)

117-81-7

$- See Di(2-Ethylhexyl) Phthalate.

1,4-Dioxane

123-91-1

T-01

Charcoal, 226-010.5 - 15 0.01 - 0.2 10

NIOSH 1602

GC/FIDA $56

M-3500

3M POVM, 3500Up to 8 hours 0.0345 15

NIOSH 1602M

GC/FIDA $56

1,3-Dioxolane

646-06-0

T-01


NIOSH 1602M

GC/FIDA $56 Validated only by recovery study.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Dipentene, a mixture of

s- and d-limonene isomers

138-86-3 $- See Limonene.

Diphenyl

92-52-4

T-35-01

Tenax RA, 226-35-0130 - 300 1.6 2

NIOSH 2530

GC/FIDNC $56

Diphenyl Ether

101-84-8$- See Phenyl Ether and Phenyl Ether/Diphenyl mixture

Diphenyl Ketone Vapor

119-61-9$- See Benzophenone.

Diphenyl Oxide

101-84-8$- See Phenyl Ether.

Dipropylene Glycol Methyl

Ether

34590-94-8

T-01

Charcoal, 226-01 5 - 10 0.01 - 0.1 20NIOSH 1403M

GC/FIDE $56 Synonym: Dipropylene glycol monomethyl ether

M-3500


NIOSH 1403M

GC/FIDE $56

Dipropylene Glycol Methyl

Ether Acetate

T-01


NIOSH 1403M

GC/FIDE $56

M-3500


NIOSH 1403M

GC/FIDE $56

Divinylbenzene

1321-74-0

T-73


226-73

12 0.05 7OSHA 89

GC/FIDNC $56

Commercial product routinely contains ethyl vinyl benzene

which may also warrant simultaneous monitoring.

DMAPA

109-55-7$- See 3-Dimethylamine-1-Propylamine.

1-Dodecanethiol

112-55-0$- See n-Dodecyl mercaptan.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Dodecyl Acrylate

2156-97-0

$- See lauryl Acrylate.

n-Dodecyl Mercaptan

112-55-0

T-10

Silica Gel, 226-10

6 0.4 Max 0.4 Proprietary

IHGC-P042

GC/MS

K $160

tert-Dodecyl Mercaptan

25103-58-6

T-30

XAD-2 Tube, 226-30

6 Ceiling

15 Max

0.4 Max 4 Proprietary

IHGC-P043

GC/MS

HH $160

Dodecyl Methacrylate

142-90-5

$- See Lauryl Methacrylate, C16-C18

DOP

117-81-7

$- See Di(2-Ethylhexyl) Phthalate.

Dowanol DM

111-77-3

$- See 2-(2-Methoxyethoxy) Ethanol

Dowanol DPM

34590-94-8

$- See Dipropylene Glycol Methyl Ether.

Dowanol EB

111-76-2

$- See 2-Butoxy Ethanol.

Dowtherm A

101-84-8 / 92-54-4

$- See Phenyl Ether / Biphenyl Mix.

DPGMEA $- See Dipropylene Glycol Monomethyl Ether Acetate.

Dursban

2921-88-2

$- See Chlorpyrifos.

Dust

Particulates Total

N/A

$- See Particulates, Total.

Dust

Particulates Respirable

N/A

$- See Particulates, respirable.

EEP Solvent

763-69-9

$- See Ethyl-3-Ethoxy Propionate.

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page 85


Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Elemental Carbon

7440-44-0

C-47

Quartz, heat-treated,

37mm, 3PC,

SKC PN 225-401

150 - 5000 2.0 - 4.0 1.3 NIOSH 5040

EGA/TOA

NC Call lab for

pricing

For mining applications use the cyclone+diesel particulate

matter cassette (jeweled impactor). Suitable cyclones

include the 10mm Dorr-Oliver nylon cyclone and SKC GS-1

conductive plastic cyclone, SKC225-105. The SKC cassette

has been tested for operation at 1.7 and 2.0 Lpm. For non-

mining applications a quartz filter (37 mm) without the

impactor may be used. Also, because more than 95% of

diesel particulates are less than 1 um in size, a size-

selective sampling device (cyclone) is not needed unless

there are other interference’s present, such as coal dust.


Epichlorohydrin

106-89-8

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.05-0.2

STEL 0.2

0.2 Proprietary

IHGC-P014

GC/FID

I $77

T-01

Charcoal, 226-01

2 - 30 0.01 - 0.2 10 NIOSH 1010M

GC/FID

A $56

M-3500

3M POVM, 3500

Up to 8 hours 0.0296 15 NIOSH 1010M

GC/FID

A $56

Ethanethiol

75-08-1

$- See Ethyl Mercaptan.

Ethanol

64-17-5

$- See Ethyl Alcohol.

Ethanolamine

(Monoethanolamine)

141-43-5

T-30-18

NITC-Treated XAD-2,

226-30-18

10 100 cc/min

Max

2 OSHA PV2111 N $116 Store media cold before sampling. Samples stable at


Synonym: 2-Aminoethanol

3-Ethenylpyridine

N/A

T-93

XAD-4, 226-93

600 1.5 Max 0.2 ASTM D5075

GC-NPD

NC $127 Used as indicator for Environmental Tobacco Smoke (ETS).

Store frozen, ship cold. May be sampled on same tube with

nicotine.

2-(2-ethoxy ethoxy) ethanol

111-90-0

$- See Diethylene glycol Monoethyl Ether.

2-Ethoxyethanol

110-80-5

T-01

Charcoal, 226-01

10 - 50 0.1 - 0.5 20 OSHA 79

GC/FID

E $56 Synonym: Cellosolve

M-3500

3M POVM, 3500

Up to 8 hours 0.0324 30 OSHA 79M

GC/FID

E $56

2-Ethoxyethyl Acetate

111-15-9

T-01

Charcoal, 226-01

10 - 50 0.1 - 0.5 20 OSHA 79

GC/FID

E $56

M-3500

3M POVM, 3500


GC/FID

E $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ethyl Acetate

141-78-6

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.1 Proprietary

IHGC-P029

GC/FID

A $77

M-3500

3M POVM, 3500

Up to 6 hours

(at PEL Concentration)

0.0345 30 NIOSH 1457M

GC/FID

A $56

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 20 NIOSH 1457

GC/FID

A $56

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min

0.014 2.2 Proprietary

IHGC-P029

GC/FID

A $77

Ethyl Acrylate

140-88-5

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.2 Proprietary

IHGC-P029

GC/FID

A $77 Preferred active sampling method. Also see Acrylate

Monomer Profile.

M-02

SKC POVM, 575-002

TWA 8hrs (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77 Preferred passive sampling method. Also see Acrylate

Monomer Profile.

T-01

Charcoal, 226-01

3 - 10 0.02 - 0.2 20 NIOSH 1450

GC/FID

A $56 Also see Acrylate Monomer Profile.

M-3500

3M POVM, 3500


GC/FID

A $56 Also see Acrylate Monomer Profile.

T-73


226-73

3 - 10 0.02 - 0.2 10 OSHA 92

GC/FID

NC $56 Also see Acrylate Monomer Profile.

Ethyl Alcohol

64-17-5

T-01

Charcoal, 226-01

0.1 - 1 0.01 - 0.2 20 NIOSH 1400

GC/FID

B $56 Ship cold for overnight delivery. Store in freezer.

Synonym: Ethanol

T-82 (2)

Anasorb 747, 226-82,

(2 in series)

5 - 12 0.01 - 0.05 20 OSHA 100

GC/FID

QQ $56

M-3520

3M POVM 3520, 2-stage

1 Hour Max (at PEL) 0.0437 30 NIOSH 1400M

GC/FID

B $56

Ethyl Amyl Ketone

541-85-5

T-01

Charcoal, 226-01

10 - 25 0.01 - 0.2 10 NIOSH 1301M

GC/FID

NC $56

Ethyl Benzene

100-41-4

T-01

Charcoal, 226-01

10 - 24 0.01 - 0.2 10 NIOSH 1501

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1 Proprietary

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

15 - 480 min. 0.013 2 Proprietary

IHGC-P029

GC/FID

A $77

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ethyl Bromide

74-96-4

T-01

Charcoal, 226-01

TWA 24

STEL 3

TWA 0.05-0.1

STEL 0.2

3 OSHA 07

GC/FID

NC $56

Ethyl Chloride

75-00-3

T-09 (2)

Charcoal, 226-09

0.5 - 3 0.02 - 0.05 50 NIOSH 2519

GC/FID

A $77 Synonym: Chloroethane

Ethyl Chloroformate

541-41-3

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID

NN $77 Store media and samples cold, ship samples cold overnight.


Ethyl Cyanoacrylate

7085-85-0

T-98


226-98

12 0.01 - 0.2 10 OSHA 55

HPLC

NC $116 Store samples in freezer or on ice after sampling. Ship cold

(dry ice if possible) by overnight delivery.

Ethyl Ether

60-29-7

T-01

Charcoal, 226-01

0.25 - 3 0.01 - 0.2 20 NIOSH 1610 GC/FID a $56 Ship refrigerated.

T-81

Anasorb 747, 226-81

0.25 - 3 0.01 - 0.2 20 OSHA Stopgap

GC/FID

NC $56 Ship refrigerated.

M-3520



GC/FID

A $56 Ship refrigerated.

Ethyl-3-Ethoxy Propionate

763-69-9

T-01

Charcoal, 226-01

5 - 10 0.01 - 0.1 20 OSHA PV2025

GC/FID

F $56

Ethyl Formate

109-94-4

T-01

Charcoal, 226-01

10 0.2 10 NIOSH 1452

GC/FID

A $56

2-Ethyl-1- Hexanol

104-76-7

T-01

Charcoal, 226-01

10 - 60 0.01 - 0.2 20 OSHA CSI

GC/FID

I $56

Ethyl Lactate

97-64-3

T-81

Anasorb 747, 226-81

TWA 6-24

STEL 3

TWA 0.05-0.1

STEL 0.2

3.4 OSHA 07

GC/FID

E $56

T-01

Charcoal, 226-01

10 Max 0.2 Max 20 OSHA PV2081

GC/FID

E $56

Ethyl Mercaptan

75-08-1

C-48


37mm, 2PC,

SKC PN 225-9007

10-150 0.1-0.2 4 NIOSH 2542M

HPLC

NC $- Samples are subcontracted to outside laboratory. Store

samplers cold before use. Collected samples are stable for

15 days at 25°C.

Ethyl Styrene

28106-30-1

T-73


226-73

TWA 12

STEL 3.75

TWA 0.05

STEL 0.25

6 OSHA 89

GC/FID

CC $56

Ethyl-2-Hydroxypropionate

97-64-3

$- See Ethyl lactate.

Ethylamine

75-04-7

T-30-18

NITC-Treated XAD-2,

226-30-18

10 Max 0.2 Max 3 OSHA 60M

HPLC

N $116 Store media cold before sampling. Samples stable at


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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ethylene Chlorohydrin

107-07-3

T-81A

Anasorb 747, 226-81

2 - 35 0.01 - 0.2 20 NIOSH 2513M

GC/FID

D $56

Ethylene Dibromide

106-93-4

T-01

Charcoal, 226-01

8 - 10 0.02 - 0.2 0.5 NIOSH 1008M

GC/ECD

NC $102

Ethylene Dichloride

107-06-2

T-01

Charcoal, 226-01

1 - 50 0.01 - 0.2 10 NIOSH 1003

GC/FID

A $56 Synonym: 1,2-Dichloroethane

M-3500

3M POVM, 3500


GC/FID

A $56

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.02-0.2

STEL 0.2

0.14 IHGC-P028

GC/FID

A $77

M-01

SKC POVM, 575-001

20 - 480 min 0.01 0.28 IHGC-P029

GC/FID

A $77

M-N566

Assay Technology N566

Up to 8 hours 0.00922 2.0 NIOSH 1003M

GC/FI

RR $56

Ethylene Glycol

107-21-1

T-57

GFF/XAD-7 OVS, 226-57

5 - 60 0.5 - 2.0 20 NIOSH 5523

GC/FID

JJ $77 Store samples cold, and ship samples cold overnight.

Ethylene Glycol Monobutyl

Ether

111-76-2

$- See 2-Butoxyethanol.

Ethylene Glycol Monobutyl

Ether Acetate

112-07-2

$- See 2-Butyoxylethyl Acetate

Ethylene Glycol Monoethyl

Ether

110-80-5

$- See 2-Ethoxyethanol.

Ethylene Glycol Monoethyl

Ether Acetate

111-15-9

$- See 2-Ethoxyethyl Acetate.

Ethylene Glycol

Monomethyl Ether Acetate

110-49-6

$- See 2-Methoxyethyl Acetate

Ethylene Glycol

Monomethyl Ether

109-86-4

$- See 2-Methoxyethanol.

Ethylene Glycol

Monopropyl Ether

2807-30-9

T-01

SKC Charcoal Tube,

226-01

10 Max 0.2 Max 20 NIOSH 1403M

GC/FID

E $56 See 2-Propoxyethanol

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Ethylene Oxide

75-21-8

M-06

SKC Ethylene Oxide PM,

575-005

15 min - 8 hours 0.0212 3 OSHA 1010M

GC/ECD

NC $102 Store sampling media cold. Store collected samples cold if

not shipped to the lab immediately after sampling. Ship

cold overnight.

T-178

HBR-treated

Anasorb 747, 226-178

TWA 12

STEL 0.75

0.05 2 OSHA 1010M

GC/ECD

NC $102 Store sampling media cold. Store collected samples cold if

not shipped to the lab immediately after sampling. Ship

cold overnight.

Ethylenediamine

107-15-3

T-30-18

NITC-Treated XAD-2,

226-30-18

TWA 12

STEL 3

TWA 0.025-0.1

STEL 0.2

3 OSHA 60

HPLC/UV



Ethylene Thiourea

96-45-7

C-56

GFFs(2), 37mm, 4PC

480 Max 2 Max 1 OSHA 95M

HPLC/UV

NC $138

Ethylhexanoic Acid

149-57-5

T-10-03


226-10-03

24 Max 0.2 Max 10 OSHA Stopgap

GC/FID

N $77

2-Ethylhexyl Acrylate

103-11-7

M-02

SKC POVM, 575-002

TWA 8 hrs

STEL 1.5 hrs (Min)

0.01 15 Proprietary

IHGC-P029

GC/FID

A $77

T-81

Anasorb 747, 226-81

TWA 10 TWA 0.03-0.2 2.8 Proprietary

IHGC-P029

GC/FID

A $77

Ethylhexyl Chloroformate

24468-13-1

T-153

Amine-treated XAD-2, 226-

153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



2-Ethylhexylnitrate

27247-96-7

T-09

SKC 226-09

2-48 0.1 - 0.2 5.0 Ethyl DII-3

10/29/89

GC/FID

A Tube capacity is approximately 1 mg of 2-ethylhexylnitrate.

No special handling requirements have been established.

Ethylvinylbenzene

28106-30-1

$- See Ethyl Styrene.

Fiber Count, Total

N/A

C-01


long cowl

480 - 1000

(adjust total volume to

optimize filter lading; see

reference method online)

0.5 - 16.0 Approx. 3100

F/F

NIOSH 7400,

A Rules PCM

NC $17 Sample open faced on black conductive cowled cassette.

Primary asbestos fiber counting method. ANALYSIS IS NOT

SPECIFIC FOR FIBER TYPE. Specify "A" counting rules when

exposure may contain asbestos. Specify "B" counting rules

when exposure a) does not contain asbestos, and b) may

contain certain man-made mineral fibers of larger

dimensions, such as synthetic vitreous fibers. Follow-up

analysis of the same filter by NIOSH Method 7402 (TEM)

can be used to provide differentiation of fiber types.

Fiber Count, Total

(“B” counting rules for

non-asbestos fibers)

N/A

C-01


long cowl

480 - 1000 0.5 - 16.0 Approx. 3100

F/F

NIOSH 7400,

B Rules PCM


“B” rules are used for counting certain non-asbestos fibers.

ANALYSIS IS NOT SPECIFIC FOR FIBER TYPE. Follow-up



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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Fibrous Glass

(Synthetic Vitreous)

N/A

C-01


long cowl

480 0.5 - 16.0 Approx. 3100

F/F

NIOSH 7400,

B Rules PCM


“B” rules are used for counting certain non-asbestos fibers.

ANALYSIS IS NOT SPECIFIC FOR FIBER TYPE. Follow-up



Fluoranthene

206-44-0

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC

N $116 Wrap cassettes with foil if sampling in bright sunlight.




delivery.

Fluorene

86-73-7

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC





delivery.

Fluorides,

Gaseous Only

16984-48-8

C-13

MCE/Treated Backup,

37mm, 3PC

50 - 800 1.0 - 2.0 5 NIOSH 7902

ISE

NC $69 Prefilter may be tested for particulate from of fluoride if

desired.

Fluorides,

Particulate Only

16984-48-8

C-05


50 - 800 1.0 - 2.0 5 NIOSH 7902

ISE

NC $81 Sample on C-13 cassette to test both gaseous and

particulate fluorides on a single sampler.

Fluorides, Total

16984-48-8

C-13

MCE/Treated Backup,

37mm, 3PC

50 - 800 1.0 - 2.0 10 NIOSH 7902

ISE

NC $150 Reporting includes separate results for gaseous fluoride,

particulate fluoride, and total fluoride

Forane

26675-46-7

T-81

Anasorb 747, 226-81

20 0.05 10 OSHA 103

GC/FID

A $56 Synonym: Isoflurane

M-02

SKC POVM, 575-002


GC/FID

A $56

M-3520



GC/FID

A $56

Formaldehyde

50-00-0

T-119


226-119

2 - 30 0.03 - 1.0 0.1 NIOSH 2016

HPLC

N $91 Preferred active sampling method. Refrigerate before and

after sampling and ship overnight. For STEL sampling,

collect a 15-minute sample at 1 LPM. Ozone may interfere -

use ozone scrubber in known ozone contaminated areas.



MEK will compete with the aldehyde and are therefore

potential negative interferences. Media contains residual

acetonitrile which could interfere with acetonitrile

monitoring.

Formaldehyde

Short Term

50-00-0

T-54

HMP-treated XAD- 2,

226-54

3 0.2 0.5 OSHA 52

GC/NPD

CC $91 For STEL sampling, collect a 15-minute sample at 0.2 LPM.

Keep fresh tubes in refrigerated storage. Sample using

same lot number for all samples. Field blank submission is

very important.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Formaldehyde

Long Term

50-00-0

T-117

HMP-Treated XAD-2,

226-117

24 0.1 0.5 OSHA 52

GC/NPD

CC $91 Keep fresh tubes in refrigerated storage. Sample using

same lot number for all samples. Field blank submission is

very important.

Formaldehyde

50-00-0

UMEX-100

SKC UMEX Aldehyde

PM 500-100


HPLC

NC $91 Preferred passive sampler for formaldehyde. OSHA reports

sampling rate bias for all diffusional formaldehyde

samplers when exposure source is methanol-stabilized

formalin. Any ketone or aldehyde will react with the DNPH

and is a potential interference. May be used for 24-hour

IAQ sampling. Large concentrations of acetone or MEK will

compete with the aldehyde and are therefore potential

negative interferences. Refrigerate before and after

sampling and ship overnight. Passive monitor cost is not

included in price. Samples may be stored up to 3 weeks if

refrigerated.

M-ATN571

Assay Aldehyde

PM ATN571


HPLC

NC $91

M-3721

3M Formaldehyde

PM 3721


SPEC

NC $91 Not suitable for short-term measurements. Submission of

field blank is strongly recommended.

Formaldehyde

50-00-0

IMP-02

Impinger, 1% Sodium

Bisulfite

1 - 100 0.2 - 1.0 2.5 NIOSH 3500M

SPEC

NC $91

Formaldehyde in Dust

50-00-0

Call lab IOM sampler 240 - 1050 2 4 NIOSH 5700

HPLC/UV

NC $160 Transfer IOM cassette to bottle after sampling, store and

ship cold.

Formamide

75-12-7

T-10

Silica Gel, 226-10

TWA 10

STEL 3

TWA 0.02-0.1

STEL 0.2

2 OSHA Stopgap

GC/NPD

K $127

T-10-03


226-10-03

TWA 10

STEL 3

TWA 0.02-0.1

STEL 0.2

5 OSHA Stopgap

GC/NPD

K $127

Formic Acid

64-18-6

T-10-03


226-10-03

1 - 24 0.05 - 0.2 5 NIOSH 2011

IC

V $69 PTFE prefilter (C-29) required in presence of formate salts;

discard cassette unless formic acid salts are to be

measured. Acetic acid can also be measured on the same

sample.T-01

Charcoal, 226-01

48 Max 0.2 Max 5 OSHA ID186 SG

IC

V $69 Store cold after sampling. Ship cold overnight for analysis

within 7 days of collection (82% recovery at 2 weeks of cold

storage). Use prefilter (C-29) if formate salts are present.

Acetic acid can also be measured on the same sample.

Submission of a field blank is essential.

Formic Acid Methyl Ester

107-31-3

$- See methyl formate.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Freon

N/A

$- See Individual Refrigerants

Fuel Oil See Kerosene.

Furfural

98-01-1

M-3500

3M POVM, 3500


GC/FID

I $56

T-117

HMP-Treated XAD-2,

226-117

1 - 12 0.01 - 0.05 50 NIOSH 2529

GC/FID

CC $77

Furfuryl Alcohol

98-00-0

T-115

Porapak-Q, 226-115

3 - 25 0.01 - 0.05 40 NIOSH 2505

GC/FID

NC $77

Gallium

12024-21-4

C-05

MCEF, 37mm, 0.8um,

3PC

1920 4 2.7 OSHA ID206

ICP

NC $77 NIOSH 7300 determines the amount of Gallium metal. Not

suitable for analysis of highly-insoluble gallium oxide.

Gasoline

8006-61-9

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 75 NIOSH 1550M

GC/FID

A $77

M-3500

3M POVM, 3500


GC/FID

A $77

Glass Fibers/ Synthetic

Vitreous Fibers

N/A

$- See Fiber Count, Synthetic

Glutaraldehyde

111-30-8

T-119


226-119

1 - 30 0.05 - 0.5 0.2 NIOSH 2532

HPLC/UV

N $116 Any ketone or aldehyde will react with the DNPH and is a



potential negative interferences. Refrigerate before and

after sampling and ship overnight. The C-20 treated filter

sampler should be used if there is aerosol exposure

potential.

C-20

GFFs (2), DNPH-treated,

37mm, 4PC

30-480 2 0.4 OSHA 64

HPLC/UV

N $116 Sample open faced. Any ketone or aldehyde will react with


concentrations of ozone, acetone or MEK will compete with

the aldehyde and are therefore potential negative


ship overnight. Minimum media order of 10 units.

UMEx-100

SKC UMEx Aldehyde PM,

500-100

Up to 8 hours 0.014 0.2 NIOSH

2532M

N $116

Glycidyl Methacrylate

106-91-2

T-09

Charcoal, 226-09

TWA 24

STEL 3

TWA 0.05-1

STEL 0.2

4.3 OSHA 07

GC/FID

A $77

Glycolic Acid

79-14-1

C-44

GFF Type A/B, 37mm, 1um,

3PC

300 Max 0.2 - 2.0 20 Proprietary

IHIC-P001

IC/Cond.

NC $86 Synonym: Hydroxyacetic Acid

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

GMAA

79-41-4

$- See Methacrylic Acid

Goal® Herbicide

42874-03-3

C-10

PVC, 37mm, 5um, 3PC

TWA 96

STEL 30

TWA 0.2

STEL 2.0

2 IN-HOUSE

HPLC/UV

N $145

Gold

7740-57-5

C-05

MCEF, 37mm, 0.8um,

3PC

200-400 1 - 2 2 NIOSH 7300M

ICP

NC

Graphite

7782-42-5

C-10

PVC, 37mm, 5um, 3PC

100 - 500 1.0 - 3.0 100 NIOSH 7500M

XRD

W $127 Quartz is a direct positive interference.

Graphite

Bulk

7782-42-5

2 - 5 grams 1% NIOSH 7500M

XRD

$127

Halothane

151-67-7

T-81

Anasorb 747, 226-81

12 Max 0.05 Max 75 OSHA 103

GC/FID

A $56

M-3520



GC/FID

A $56

HCFC 225

135151-96-1

$- See Refrigerant 225 ca & cb. Also known as AK 225 ™ and

dichloropentafluoropropane.

HCFC-123

306-83-2

$- See 2,2-Dichloro-1,1.1-Trifluoroethane

HDI

822-06-0

$- See Hexamethylene Diisocyanate

HDI Homopolymer

28182-81-2

$- See Hexamethylene Diisocyanate Homopolymer

Heptachlor

76-44-8

T-30-16

GFF/XAD-2 OVS,

226-30-16

60 1 1 OSHA CSI

GC/ECD

NC $102 Also see Chlorinated Pesticide Profile.

Heptane

142-82-5

T-01

Charcoal, 226-01

4 - 10 0.01 - 0.2 10 NIOSH 1500

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

2-Heptanone

110-43-0

$- See Methyl n-amyl Ketone

Heptyl Acetate

90438-79-2

T-01

Charcoal, 226-01

5 - 10 0.05 - 0.2 5 NIOSH 1450M

GC/FID

A $56 Component of DuPont products Axarel TM and Optisol In-

Line.

Heptyl Alcohol

70914-20-4

T-01

Charcoal, 226-01

5 - 10 0.05 - 0.2 5 NIOSH 1402 GC/FID A $56 Component of Optisol TM - a DuPont product

Heptyl Alcohol + Isomers

70914-20-4

T-01

Charcoal, 226-01

5 - 10 0.05 - 0.2 5 NIOSH 1402M

GC/FID

D $56 Component of Optisol TM - a DuPont product

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Hexachlorocyclopentadi-

ene

77-47-4

T-116,

2 tubes in series

Porapak-T, 226-116

TWA 6-90

STEL 6

TWA 0.01-0.2

STEL 0.2

0.03 NIOSH 2518

GC/ECD

NC $102 Cap tubes separately after sampling. Store refrigerated in

dark.

1,1,1,3,3,3-

Hexachloropropane

3607-78-1

T-59-04

Porapak R, 226-59-04

1 - 10 0.01 - 0.2 0.1 NIOSH 2517

GC/ECD

NC $102

Hexamethylcyclotrisilox-

ane

541-5-9

T-09

Charcoal, 226-09

TWA 96

STEL 30

TWA 0.2

STEL 2.0

16 IHGC-P040

GC/FID

A $77 Store samples in freezer, ship cold overnight.

1,6-Hexamethylene

Diisocyanate

822-06-0

C-14

cassette or K-20 kit;

see comments at right

15 - 240 1 0.12 OSHA 42

HPLC/FL

O $116 Sample open faced. Refrigerate media before and after

sampling. Ship samples cold by overnight delivery. Testing

is for both 2,4- and 2,6-TDI isomers. Media is marked with

expiration date, and will ship with at least 1-month shelf

life (stored cold). See comments that follow regarding field

desorption of samples.

The OSHA National Emphasis Program (now closed)

specified field desorption immediately after sampling; the

intended purpose was improving recovery of collected

diisocyanates, particularly those in aerosol form. The K-20

kit includes C-14 cassette,V-04 vial with 3mL 90/10 (v/v)


instruction set, SDS for solution. Cold sample shipment

after extraction is not required, but extracted samples

should ship to lab as soon as possible. Extracts may be

stored in refrigeration for up to a week before shipment if

unavoidable. Dangerous goods shipping requirements

apply. Contact lab for more specifics.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Hexamethylene

Diisocyanate Homopolymer

28182-81-2

C-14

cassette or K-20 kit;

see comments at right

15 - 240 1 Max 2 OSHA PV2125

HPLC/UV



















Hexamethylenediamine

124-09-4

T-30-18

NITC-Treated XAD-2,

226-30-18

12 0.1 2 OSHA Stopgap

HPLC



1,b-Hexanedioldiacrylate

1348-33-4

T-110

Chromosorb 106,

226-110

48 Max 0.2 Max 20 OSHA PV2133

GC/FID

HH $56

n-Hexane

110-54-3

T-01

Charcoal, 226-01

4 - 10 0.01 - 0.2 10 NIOSH 1500

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Hexane, isomers, other

than n-Hexane

75-83-2; 79-29-8;

96-14-0; 107-83-5

T-01

Charcoal, 226-01

4 - 10 0.01 - 0.2 10 NIOSH 1500

GC/FID

A $77

M-3500

3M POVM, 3500


GC/FID

A $77

2-Hexanone

591-78-6

$- See Methyl butyl Ketone

Hexone

108-10-1

$- See Methyl Isobutyl ketone (MIBK)

Hexylene Glycol

107-41-5

T-01

Charcoal, 226-01

3 - 20 0.05 - 0.2 20 OSHA Stopgap

GC/FID

E $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

HFE 7100 $- See Perfluorobutyl Methyl Ether

High Flash Aromatic

Naphtha

N/A

$- See Aromatic 100

HMDI

5124-30-1

$- See Methylene Bis(4-Cyclohexylisocyanate).

Hydrazine

302-01-2

C-15


37mm, 3PC

240 1 0.1 OSHA 108

HPLC

NC $116 Preferred method. Store samples cold if not shipped

immediately. Samples are stable for up to 19 days at

ambient temperature (60 - 80°F).

T-42-02

H2SO4-treated Firebrick,

226-42-02

10 - 20 0.1 - 1.0 0.08 OSHA 20

HPLC

NC $116

Hydrobromic Acid

10035-10-6

$- See Hydrogen Bromide

Hydrocarbons, Total

as n-Hexane

N/A

T-01

Charcoal, 226-01

20 - 50 0.01 - 0.2 50 NIOSH 1500

GC/FID

A $77 Commonly used to measure Volatile Organic Compounds

(VOCs); instrument response to hexane is used for a

cumulative estimation of all compounds that 1) collect on

charcoal, 2) desorb in CS2, and 3) respond to FID under the

chromatographic conditions applied. Light hydrocarbons

may break through with high (>10L) air volumes.

M-3500

3M POVM, 3500

Up to 8 hours 0.032

(published rate

for hexane)

75 NIOSH 1500M

GC/FID






may break through with high (>10L) air volumes. Light

hydrocarbons may require sampling with 3M 3520.

M-01

SKC POVM, 575-001

Up to 8 hours 0.0143

(published rate

for hexane)

100 NIOSH 1500M

GC/FID






may require sampling with 3M 3520.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Hydrocarbons, Total as

n-Hexane, High Resolution

N/A

T-01

Charcoal, 226-01

5 - 20 0.01 - 0.2 20 NIOSH 1500

GC/FID





chromatographic conditions applied. The five most

abundant compounds will be identified as TICs (Tentatively

Identified Compounds, based upon GC-MS library search)

in samples that meet or exceed the FID LOQ.

M-3500

3M POVM, 3500

Up to 8 hours 0.032 (pub-

lished rate for

hexane)

30 NIOSH 1500M

GC/FID









M-01

SKC POVM, 575-001

Up to 8 hours 0.0143

(published rate

for hexane)

40 NIOSH 1500M

GC/FID









Hydrochloric Acid

7647-01-0

$- See Hydrogen Chloride. Also see Acid Mist Profile.

Hydrogen Bromide

10035-10-6

C-68

Na2CO3-treated Quartz,

37mm, 3 PC

30-600 2.0 5 NIOSH 7907

IC/COND

SS Stable 1 week at 20°C, stable to at least 28 days at 4°C.

T-10-03

Prewashed Silica Gel

226-10-03

TWA 96

STEL 7.5

TWA 0.5 Max

STEL 0.5

5 OSHA ID 165SG

IC/COND

Samples are stable at least 21 days.

T-10-03


226-10-03

3 - 100 0.2 - 0.5 5 NIOSH 7903

IC

U $69 NIOSH now describes NIOSH Method 7903 as a “historical”

method and does not recommend its use, advocating

instead for a series of filter methods which provide

improved sensitivity and the opportunity for size-selective

sampling of aerosols. NIOSH’s intention is not to invalidate

results developed using NIOSH 7903 in the past, but to

instead transition users to the newer filter methods. See

Hydrogen Bromide. Also see Acid Mist Profile.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Hydrogen Chloride

7647-01-0

C-68

Na2CO3-treated Quartz,

37mm, 3 PC

30-600 2.0 10 NIOSH 7907

IC/COND

SS Stable 1 week at 20°C, stable to at least 28 days at 4°C.

T-10-03


226-10-03

TWA 96

STEL 7.5

TWA 0.5 Max

STEL 0.5

2.5 OSHA ID174SG

IC/COND

U $69 Samples are stable at ambient temperature for at least 21

days.

T-10-03


226-10-03

3 - 100 0.2 - 0.5 2.5 NIOSH 7903

IC







instead transition users to the newer filter methods. Also

see Acid Mist Profile. Synonyms: Hydrochloric acid, muriatic

acid.

Hydrogen Cyanide

74-90-8

T-28

Soda Lime, 226-28

2 - 90 0.2 2.6 NIOSH 6010M

ISE

NC $81 Before sampling, remove glass wool plug that precedes

glass fiber filters (holds filter in place at front of sorbent

during shipping). No need to replace the glass wool; only

used to keep the filter in place during shipping.

Hydrogen Fluoride

7664-39-3

T-10-03


226-10-03

3 - 100 0.2 - 0.3 5 NIOSH 7903

IC







instead transition users to the newer filter methods. See

also Fluorides, Gaseous for alternate filter/cassette

sampling method. Also see Acid Mist Profile.

C-13

MCE/Treated Backup,

37mm, 3PC

50 - 800 1 -2 5.3 NIOSH 7902

ISE

NC $69

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Hydrogen Peroxide

7722-84-1

IMP-13

Midget Fritted? Glass

Bubbler, 15 mL TiOSO4

reagent

100 0.5 2

(varies with

solution

volume)

OSHA VI-6

Color

NC $100 Request 20 mL sampling solution and one V-40 vial per

sample and blank from laboratory. Must send blank

solution for correction. Positive interferences can be

expected from any compounds that liberate H2O2 on acid

hydrolysis. Negative interferences are a function of the

reactivity of H2O2 with other compounds present in the air

samples. Dangerous goods shipping requirement. Sampling

solution shelf-life is 1 month. Samples are stable for 1

month after collection.

C-73

TiOSO4-treated

Quartz (2), 25mm

30 - 40 1 -2 LPM for

vapor and mist

4.5 OSHA 1019 NC After sampling, wrap cassette in aluminum foil to protect

from light. Foil-wrapped samples are stable at least 2

weeks. Submit samples to lab as soon as possible after

sampling. If delayed shipping is unavoidable, store samples

under refrigeration.

Hydrogen Sulfide

7783-06-4

T-177

Silvered Silica Gel,

226-177

TWA 12

STEL 7.5

0.05 Max

0.5 Max

8.8 OSHA 1008

IC

NC $116 Preferred method. Store media and samples cold, ship

overnight.

K-04

Low SO4 Charcoal (Lrg.

Orbo 34) + PTFE prefilter to

remove sulfate particulates

(if present)

2 - 40

(established at 10 ppm,

see notes at right)

0.1 - 1.5 7.1 NIOSH 6013

IC

NC $69 Do not send filter to lab unless measurement of particulate

sulfates/sulfides is required. Breakthrough volume

sampling in a low humidity 1 ppm atmosphere is 420 liters;

capacity increases in high humidity atmosphere.

Hydrogenated Terphenyl

61788-32-7

C-08

PTFE, 37mm, 2um, 3PC

30 Max 3 Max 100 OSHA Stopgap

GC/FID

NC $77 Immediately after sampling, transfer filter and backup pad

into small glass vial for shipping.

Hydroquinone

123-31-9

C-05


30 - 180 1.0 - 4.0 2 NIOSH 5004

HPLC

NC $116 Place filter in glass vial containing 10 ml of 1% acetic acid

immediately after sampling.

Hydroquinone monomethyl

ether

150-76-5

C-10

PVC, 37mm, 5um, 3PC

20 0.05 - 2 4 IH HPLC-P006

HPLC/UV

K $160

Hydroquinone (Vapor)

123-31-9

T-98


226-98


HPLC

NC $116

Hydroxy Ethyl Acrylate

818-61-1

T-15

Silica Gel, 226-15

TWA 30

STEL 7.50

TWA 0.25-0.5

STEL 0.5

6 IN-HOUSE

GC/FID

KK $77 Store in freezer after sampling. Ship cold overnight.

Hydroxy Ethyl Methacrylate

868-77-9

T-15

Silica Gel, 226-15

TWA 30

STEL 7.50

TWA 0.25-0.5

STEL 0.5

7 IN-HOUSE

GC/FID


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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

2-Hydroxypropyl Acrylate,

Mixture of Isomers

25584-83-2

T-15

Silica Gel, 226-15

TWA 30

STEL 7.50

TWA 0.05-0.5

STEL 0.5

6.2 IN-HOUSE

GC/FID


2-Hydroxypropyl

Methacrylate

27813-02-1

T-15

Silica Gel, 226-15

TWA 30

STEL 7.50

TWA 0.05-0.5

STEL 0.5

6 IN-HOUSE

GC/FID


Indeno(1,2,3-cd)pyrene

193-39-5

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC





delivery.

Indium Oxide

1312-43-2

C-05


2000 Max 4 2.4 NIOSH 7300M

ICP

T $77 NIOSH 7300 determines the amount of Indium metal.

Multiply Indium amount by 1.21 to obtain results expressed

as Indium Oxide.

Iodine

(NO iodide compounds

present)

7553-56-2

T-80

KOH-treated Anasorb 747,

226-80

2.5 - 7.5 (Ceiling) 0.5 OSHA ID212

IC

NC Call for

pricing

If relative humidity is >50% sample using alternate

impinger method to avoid iodine loss. See next entry if

particulate iodide compounds are present. Ship

immediately via overnight carrier. Efficient collection of 0.7

ppm atmosphere at 0.5 LPM for up to 30 minutes was

demonstrated. Analysis is subcontracted to outside

laboratory.Iodine

(iodide compounds present)

7553-56-2

T-142

PTFE/KOH-treated Anasorb

747 OVS,

226-142

2.5 - 7.5 (Ceiling) 0.5 OSHA ID212

IC

NC Call for

pricing

If relative humidity is >50% sample using alternate

impinger method to avoid iodine loss. This sampler

includes a prefilter to remove interfering iodide

compounds. Ship immediately via overnight carrier.

Efficient collection of 0.7 ppm atmosphere at 0.5 LPM for

up to 30 minutes was demonstrated. Samples are


IPDI

4098-71-9

$- See entry for Isophorone Diisocyanate.

Iron Oxide

1309-37-1

C-05


200 - 2000 1.0 - 4.0 2.86 NIOSH 7300

ICP

T $40 Limit air volume sampled as necessary to prevent

overloading filter.

Isoamyl Acetate

123-92-2

T-01

Charcoal, 226-01

1 -10 0.01 - 0.2 20 NIOSH 1450

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Isoamyl Alcohol

123-51-3

T-01

Charcoal, 226-01

1 -10 0.01 - 0.2 20 NIOSH 1402

GC/FID

D $56

M-3500

3M POVM, 3500


GC/FID

D $56

Isobornyl Acrylate

5888-33-5

T-01

Charcoal, 226-01

4 0.001 - 0.3 40 IHGC-P018

GC/FID

A $77

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Isobornyl Methacrylate

7534-94-3

T-01

Charcoal, 226-01

3 0.01-0.3 80 IHGC-P018

GC/FID

A $77

Isobutyl Acetate

110-19-0

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 20 NIOSH 1450

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.1 Proprietary

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77

Isobutyl Acrylate

106-63-8

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.3 Proprietary

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hrs (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77

Isobutyl Alcohol

78-83-1

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 10 NIOSH 1401

GC/FID

C $56

M-3500

3M POVM, 3500


GC/ FID

C $56

Isobutyryl Chloride

79-30-1

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



Isobutyl Isobutyrate

97-85-8

T-01

Charcoal, 226-01

10 0.2 5 OSHA PV2090

GC/FID

F $56

M-3500

3M POVM, 3500

Up to 8 hours 0.0255 7.5 OSHA PV2090M

GC/FID

A $56

Isobutyl Methacrylate

97-86-9

M-02

SKC POVM, 575-002

TWA 8 hrs (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03 - 0.2

STEL 0.2

1.2 Proprietary

IHGC-P029

GC/FID

A $77

Isobutyraldehyde

78-84-2

T-119


226-119

TWA 3-24

STEL 3

TWA 0.05-0.5

STEL 0.2

1 MOSH 2532M

HPLC/UV


potential interference. Large concentrations of the acetone

or MEK will compete with aldehyde and are therefore


and after sampling and ship overnight. Also see Aldehyde

Profile for additional compounds.

Isoflurane

26675-46-7

$- See Forane.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Isooctane

540-84-1

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 10 NIOSH 1500

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Isopentyl Acetate

123-92-2

$- See Isoamyl Acetate

Isophorone

78-59-1

T-81

Anasorb 747, 226-81

2 - 25 1 Max 50 NIOSH 2508M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Isophorone Diisocyanate

4098-71-9

K-20

GFF, 2PP-treated, 37mm,

3PC

15 - 240 1 0.2 OSHA 42

HPLC/FL



















Isophthalic Acid as

Particulate

121-91-5

C-11


5um, 2PC

100-480 1-4 50 NIOSH 0500

Gravimetric

NC $21 Not chemical specific.

Isoprene

78-79-5

T-73


226-73

TWA 3

STEL 0.75

0.05 2 OSHA 56

GC/FID

NC $56 Store in freezer after sampling. Ship cold overnight.

Isopropanol

67-63-0

$- See Isopropyl Alcohol

Isopropyl Acetate

108-21-4

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 20 NIOSH 1454

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Isopropyl Alcohol

67-63-0

T-01

Charcoal, 226-01

0.2 - 3 0.01 - 0.2 5 NIOSH 1400

GC/FID

A or B $56

M-3520



GC/FID

A or B $56 Limit sampling to 4 hours at high humidity (> 80% RH).

Isopropyl Benzene

98-82-8

$- See Cumene

Isopropylamine

75-31-0

T-30-18

NITC-Treated XAD-2,

226-30-18

TWA 20

STEL 1.5

TWA 0.1

STEL 0.1

4 OSHA Stopgap

HPLC/UV

NC $116 Store media cold before sampling. Samples stable at


Isopropyl Chloroformate

108-23-6

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



Isovaleraldehyde

590-86-3

T-119


226-119

2 - 30 0.2 - 1.0 1 TO-11

HPLC

N $116 Also see Aldehyde Profile. Any ketone or aldehyde will

react with the DNPH and is a potential interference. Large




ship overnight.

Kathon ® 886 Biocide

Mixture

N/A

T-99

GFF/Silica Gel OVS,

226-99

TWA 50

STEL 7.5

TWA 0.2

STEL 0.5

See

individual

compound

entries

IHHPLC-P008

HPLC/UV

JJ See individual

compound

entries

This product contains 2-Methyl-4-Isothiazolin-3-One (RH

573) and 5-Chloro-2-Methyl-4-Isothiazolin-3-One (RH 651).

Avoid and ensure that the outside of the OVS tube is not


containing this material as either a particulate or aerosol.

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Analyte CAS # Recommended MediaSuggested


Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Kathon ® 893 Biocide

26530-20-1

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0

0.6 IN-HOUSE

IHHPLC-P002

HPLC/UV

K $160 Avoid and ensure that the outside of the OVS tube is not


containing RH-287 as a particulate. This product contains 2-

N-Octyl-4-Isothiazolin-3-one.

Kathon ® 930 Microbiocide

64359-81-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0

0.5 IN-HOUSE

IHHPLC-P002

HPLC/UV

K $160 This product contains 4,5-Dichloro-2-N-Octyl-4-Isothiazolin-

3-one; also known as RH-287.

Kerosene

(Diesel fuel)

8008-20-6

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 NIOSH 1550

GC/FID

A $77 Submit 5 ml of bulk in separate shipment for reference. Can

also be used to measure jet fuels in air (JP-4 or JP-8).

M-3500

3M POVM, 3500


GC/FID

A $77

Lauryl Acrylate

2156-97-0

T-81

Anasorb 747,

226-81

TWA 10 TWA

0.03 - 0.2

3.4 IN-HOUSE

GC/FID

A $77

Lead

7439-92-1

C-05


400 - 2000 1.0 - 3.0 2 NIOSH 7300

ICP

T $40

C-05


400 - 2000 1.0 - 3.0 0.062 NIOSH 7300M

ICP/MS

T $46

Lead - Paint chips

7439-92-1

1 - 2 gm N/A 0.005% NIOSH 7082M

FLAA/ICP

T $28

Lead

Soil or Water

7439-29-1

$- See Environmental Directory of Services for detailed

information.

Lead

Wipes/Dust

7439-92-1

K-07

Ghost Wipe Kit

100 sq. cm. or 1 sq. ft. 2 NIOSH 7082

ICP-OES

T $28 Place folded wipe in special shipping/digestion container

supplied by the laboratory as Wipe Test Kit (K-07).

Ligroin

8032-32-4

$- See Naphtha or Petroleum Distillates

Lime

1305-78-8

C-11


5um, 2PC

480 1-4 50 NIOSH 0500

Gravimetric

$21 Not chemically specific.

Limonene

138-86-3

T-01

Charcoal, 226-01

10 - 25 0.2 Max 20 NIOSH 1552

GC/FID

A $56 Samples are stable at room temperature for at least 30

days.

Lithium

7439-93-2

C-05


50 - 2000 1.0 - 3.0 4 NIOSH 7300

ICP

T $40

Lithium Hydride

7580-67-8

C-05


160 - 2000 1.0 - 3.0 1.15 NIOSH 7300M

ICP

T $40 Total lithium reported as LiH.

Magnesium Fume

1309-48-4

C-05


50 - 1200 1.0 - 3.0 2 T $40 Magnesium oxide fume as magnesium.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

MAK

110-43-0

$- See Methyl n-Amyl Ketone

Maleic Acid

110-16-7

C-06

GFF, 37mm, 1um, 3PC

TWA 100-480

STEL 30

1-4 2 NIOSH P&CAM 302

HPLC/UV

NC $116

Maleic Anhydride

108-31-6

T-30-07

XAD-2, 226-30-07

20 0.1 2 OSHA 25

HPLC

NC $116 Tubes have short shelf-life; store cold. Include 226-30 tube

(T-30) in train between 226-30-07 tube and pump. Discard

226-30 tube after sampling. Wrap tubes with foil to protect

from light during sampling and shipping. Ship samples

refrigerated by overnight delivery. If maleic anhydride

exists in the air as particulates, sample using coated filters

per method OSHA 86. Any compound that will react with p-

anisidine and has the same retention time will interfere in

the spectral region of interest.

C-28

GFFs (2), amine-treated,

37mm, 4PC

140 0.5 2 OSHA 86

HPLC/UV

K $116 Preferred method. Sample closed-face. If maleic anhydride

exists in the air as particulates, sample using coated filters

per method OSHA 86. This method may also be used just

for vapors. Media has 1 month shelf life; Store in a

refrigerator and ship as soon as possible after sampling.

Manganese

7439-96-5

C-05


100 - 1000 1.0 - 3.0 0.05 NIOSH 7300M

ICP-MS

T $46

C-05


100 - 1000 1.0 - 3.0 2 NIOSH 7300M

ICP-OES

T $40

MBK

591-78-6

$- See Methyl butyl Ketone

4,4’-MDI

101-68-8

$- See Methylene Bisphenyl Diisocyanate.

MEK

78-93-3

$- See Methyl Ethyl Ketone.

MEK Peroxide

1338-23-4

T-93

XAD-4, 226-93

15 1 10 OSHA 77

HPLC/UV

NC $- Call lab prior to sampling. Freeze samples immediately after

sampling. Ship samples cold by overnight delivery. Samples

referred to outside laboratory for analysis.

Menthol

2216-51-5

T-10

Silica Gel, 226-10

10 - 20 0.1 5 SPM

GC/FID

NC $56

Mercaptopropyltrimeth-

oxysilane, Gamma

4420-74-0

O-202580

Specially Cleaned XAD-2,

O-202580

30 0.05-0.07 10 IHGC-P032

GC/FID

K $77 Ship sample by overnight delivery to the lab

in insulated container with cold pack.

Synonym: Silane A-189.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Mercury

7439-97-6

T-17-1A

Anasorb C300,

226-17-1A

20 - 100 0.15 - 0.25 0.025 NIOSH 6009

CVAA

NC $77 Tube samples are stable for 30 days at 25°C. Sample with

prefilter (C-05) in the presence particulates containing

mercury, or particulates containing Cr +6 or large amounts

of Ni +2. The prefilter may be tested for mercury

particulates if needed. Ship prefilter samples to lab as soon

as possible.

M-03

SKC Mercury PM,

SKC PN 520-02A

8 hours Max 0.02 0.1 OSHA ID140M

CVAA

NC $77 PN 520-02A is the consumable sorbent capsule only;

passive monitor holders (SKC 520-03) are required, and are

available for $40 each.

Mercury Particulate

7439-97-6

C-05


100 - 1000 1.0 - 3.0 0.05 OSHA ID 145

CVAA

NC $77

Mercury Wipes Various K-07

Ghost Wipe Kit

100 cm2 0.075 EPA SW846 7471A

CVAA

NC $77

Mesityl Oxide

141-79-7

T-01

Charcoal, 226-01

1 - 25 0.01 - 0.2 20 NIOSH 1301

GC/FID

H $56

M-3500

3M POVM, 3500


GC/FID

H $56

Mesitylene

108-67-8

$- See 1,3,5-Trimethylbenzene

Metalworking Fluids

N/A

C-09

PTFE, Preweighed, 37mm,

2um, 2PC

500 - 1000 2 50 NIOSH 5524

Gravimetric with

Extraction

NC $98 Laboratory pre-washed and preweighed Teflon filters are

required; NIOSH 5524 Issue 2 (12/2014) recommends at

least 5 field blanks per sample set; pre-washing the Teflon

filters has minimized this need, though at least 1 field blank

is required. A special 3-piece cassette is required for

thoracic- range cyclone. Store samples cold if not shipped

immediately, analyze within 2 weeks of collection.

Applicable to mineral oils, semi-synthetics, and synthetic

fluids. Send small bulk sample (1 - 5 mL) of fluid for

solubility evaluation. Ship cold for overnight delivery.

Methacrylamide

79-39-0

IMP-14

MFGB, 20 mL DI Water

150 0.8 2 IHHPLC-P004

HPLC/UV

NC $160

Methacrylic Acid

79-41-4

T-49-108

Chromosorb 108,

226-49-108

TWA 5

STEL 1.5

TWA 0.03-0.3

STEL 0.1

4.5 Proprietary, IHHPLC-

P005 HPLC/UV

NC $160 Acrylic acid can be collected and analyzed along with

methacrylic acid by this method.

T-30-08(2)

Anasorb 708, 226-30-08,

2 in series

24 0.1 4 OSHA PV2005

HPLC/UV

K $160 Two identical tubes sampled in series. Acrylic acid may also

be tested along with methacrylic acid.

Methacroyl Chloride

920-46-7

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



B-Methallyl Chloride See 3-Chloro-2-methyl-1-propene

Methanol

67-56-1

$- See Methyl Alcohol

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1-Methoxy-2-Propanol

107-98-2

$- See Propylene Glycol Methyl Ether

1-Methoxy-2-Propanol

Acetate

108-65-6

$- See Propylene Glycol Methyl Ether Acetate

2-Methoxyethanol

109-86-4

T-01

Charcoal, 226-01

15 0.01 - 0.1 20 OSHA 79

GC/FID

E $56 Synonym: Methyl Cellosolve

M-3500

3M POVM, 3500


GC/FID

E $56

2-(2-Methoxyethoxy)

ethanol

111-77-3

$- See Diethylene Glycol Monomethyl Ether.

2-Methoxyethyl Acetate

110-49-6

T-01

Charcoal, 226-01

10 - 50 0.01 - 0.2 20 OSHA 79

GC/FID

E $56 Synonyms: Methyl Cellosolve Acetate, Ethylene Glycol

Monomethyl Ether Acetate.

M-3500

3M POVM, 3500


GC/FID

E $56 Synonyms: Methyl Cellosolve Acetate, Ethylene Glycol

Monomethyl Ether Acetate.

2-Methoxyethyl Ether

111-96-6

$- See Diethylene Glycol Dimethyl Ether

2-Methoxy-1-Methylethyl

Acetate

108-65-8

See Propylene Glycol Methyl Ether Acetate

Methyl 2 Cyanoacrylate

137-05-3

T-98


226-98

12 0.01 - 0.2 10 OSHA 55

HPLC

NC $116

Methyl Acetate

79-20-9

T-01

Charcoal, 226-01

2 - 10 0.01 - 0.2 20 NIOSH 1450M

GC/FID

A $56

M-3520

3M POVM 3520,

2-stage

2 hours Max 0.037 30 NIOSH 1450M

GC/FID

A $56

Methyl Acrylate

96-33-3

T-01

Charcoal, 226-01

5 Max 0.01 - 0.2 20 NIOSH 1459M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.3 Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min

0.016 2.6 Proprietary,

IHGC-P029

GC/FID

A $77

T-73

TBC-Treated charcoal, 226-

73

12 Max 0.05 Max 20 OSHA 92

GC/FID

A $56

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Methyl Alcohol

67-56-1

T-15

Silica Gel, 226-15

10 Max 0.02 - 0.2 20 NIOSH 2000

GC/FID

NC $56 Reduce air volume when sampled in high humidity

conditions. Store samples in refrigeration. Ship samples

cold for overnight delivery.

T-82 (2)

Anasorb 747, 226-82,

(2 in series)

TWA 3.0

STEL 0.75

0.05 Max

0.05

20 OSHA 91

GC/FID

NC $56

M-07

SKC POVM, 575-007


GC/FID

PP $56 Sampler includes (and requires) a secondary diffusion

barrier.

Methyl Amyl Alcohol

108-11-2

$- See Methyl Isobutyl Carbinol

Methyl t-Amyl Ether

994-05-8

$- See t-Amyl Methyl Ether

Methyl n-Amyl Ketone

110-43-0

T-01

Charcoal, 226-01

1 - 25 0.05 - 0.2 20 NIOSH 1301

GC/FID

A $56 Synonyms: Methyl pentyl ketone, heptan-2-one

M-3500

3M POVM, 3500


GC/FID

A $56

Methyl Bromide

74-83-9

T-83 (2)

Anasorb 747, 226-83

3 Max 0.05-0.2 10 PV2040

GC/FID

A $69 Two 226-83 tubes in series. Cap separately after sampling

and refrigerate immediately. Ship in an insulated container

with synthetic ice product and analyzed within two weeks

of sampling.

Methyl t-Butyl Ether

1634-04-4

T-09 (2)

Charcoal, 226-09,

2 in Series

2 - 96 0.1 - 0.2 20 NIOSH 1615

GC/FID

A $56 Sample with two tubes in series. Cap separately after

sampling. Smaller 226-01 tube can be used as second tube

in train.

M-3500

3M POVM, 3500


GC/FID

A $56

Methyl Butyl Ketone

591-78-6

T-01

Charcoal, 226-01

5 - 10 0.2 20 NIOSH 1300

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Methyl Carbitol

11-77-3

$- See Diethylene Glycol Monomethyl Ether.

Methyl Cellosolve

109-86-4

$- See 2-Methoxyethanol

Methyl Cellosolve Acetate

110-49-6

$- See 2-Methoxyethyl Acetate

Methyl Chloride

74-87-3

T-09

(2 in series) Charcoal,

226-09, 2 in Series

TWA 3

STEL 1.5

TWA 0.02-0.1

STEL 0.1

10 NIOSH 1001

GC/FID

I $56 Ship samples by overnight delivery to the lab in insulated

container with cold pack. Using 226-01

for second tube in series is acceptable.

Synonym: Chloromethane

Methyl Chloroform

71-55-6

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 10 NIOSH 1003

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Methyl Chloroformate

79-22-1

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



Methyl Cyclohexane

108-87-2

T-01

Charcoal, 226-01

4 - 10 0.01 - 0.2 20 NIOSH 1500

GC/FID

A $56

Methyl Ether

115-10-6

T-01

Charcoal, 226-01

3 Max 0.01 - 0.2 20 NIOSH 1610M

GC/FID

A $56 Stable in freezer for 14 days. Synonym: Dimethyl Ether

M-3520

3M POVM, 3520

2 Hours Max 0.033 30 NIOSH 1610M

GC/FID

A $56

Methyl Ether Hydroquinone See Hydroquinone nonmethylether

4- Methoxyphenol See Hydroquinone nonmethylether

Methyl Ethyl Ketone

78-93-3

T-10 (2)

Silica Gel, 226-10,

2 tubes in series

3 - 10 0.1 20 OSHA 16

GC/FID

NC $56 Sample with 2 tubes in series, cap separately after

sampling.

Synonym: 2- Butanone

T-01

Charcoal, 226-01

2 - 12 0.01 - 0.2 5 NIOSH S3

GC/FID

A $56 Ship refrigerated by overnight delivery.

T-81

Anasorb 747, 226-81

2 - 12 0.01 - 0.2 5 NIOSH 2500

GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1 Proprietary,

IHGC-P029

GC/FID

A $77

M-3500

3M POVM, 3500

Up to 8 hours 0.0363 7.5 OSHA 07M

GC/FID

A $56 Keep samples cold and expedite analysis for optimum

results.

M-02

SKC POVM, 575-002

15 - 480 min 0.02 2 Proprietary,

IHGC-P029

GC/FID

A $77

Methyl Ethyl Ketone

Peroxide

1338-23-4

$- See MEK Peroxide

Methyl Ethyl Ketoxime

96-29-7

T-10

Silica Gel, 226-10

TWA 24

STEL 7.5

TWA 0.05-0.2

STEL 0.5

5 IN-HOUSE

GC/FID

K $77 Refrigerate as soon as possible after collection. Ship cold by

overnight carrier.

Methyl Formate

107-31-3

T-83

Anasorb 747, 226-83

3 Max 0.05 Max 5 PV2041

GC/FID

NC $56

Methyl Hydrazine

60-34-4

C-15


37mm, 3PC

240 1 0.5 OSHA 108M

HPLC

NC $116

Methyl Isoamyl Ketone

110-12-3

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 20 NIOSH 1300M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Methyl Isobutyl Carbinol

108-11-2

T-01

Charcoal, 226-01

5 - 10 0.05 - 0.2 20 NIOSH 1402

GC/FID

NC $56 Store in freezer after sampling, ship overnight. Synonym:

Methyl Amyl Alcohol

M-3500

3M POVM, 3500


GC/FID

NC $56 Store in freezer after sampling, ship overnight. Synonym:

Methyl Amyl Alcohol

Methyl Isobutyl Ketone

(MIBK)

108-10-1

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 5 NIOSH 1300

GC/FID

A $56 Synonyms: Hexone, 4-Methyl-2-pentanone; Isobutyl methyl

ketone; MIBK. Store samples cold and ship cold overnight.

M-3500

3M POVM, 3500


GC/FID



T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1 Proprietary,

IHGC-P029

GC/FID



M-02

SKC POVM, 575-002


IHGC-P029

GC/FID



O-91

Carbosieve S-III, Orbo 91

10 Max 0.01 - 0.2 10 NIOSH 2555 GC/FID A $77 Synonyms: Hexone, 4-Methyl-2-pentanone; Isobutyl methyl


2-Methyl-4-Isothiazolin-3-

One (RH 573)

2682-20-4

T-99

GFF/Silica Gel OVS,

226-99

TWA 50

STEL 7.5

TWA 0.2

STEL 0.5

0.1 IHHPLC-P008

HPLC/UV

JJ $160 This chemical is one component of Kathon® 886 Biocide.

Also known as RH 573.

Methyl Mercaptan

74-93-1

C-48


37mm, 2PC,

SKC PN 225-9007

10-150 0.1-0.2 4 NIOSH 2542

GC/FPD

NC Call for

pricing

Store media cold before use. Protect samples from light

after sampling. Samples are stable for 15 days at 25°C.


Methyl

Mercaptopropionate

2935-90-2

T-47-01


TWA 6 max

STEL 3

TWA 0.05 - 0.2

STEL 0.2

1.3 IHGC-P032

GC/FID

K $77

Methyl Methacrylate

80-62-6

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1.1 Proprietary,

IHGC-P029

GC/FID

A $77

T-30-06

XAD-2, 226-30-06

1 - 8 0.01 - 0.05 20 NIOSH 2537

GC/FID

DD $56 Store in freezer and ship overnight on dry ice.

T-73


226-73

3 Max 0.01 - 0.05 20 OSHA 94

GC/FID

CC $56

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77 Preferred passive sampling method.

M-3500

3M POVM, 3500


GC/FID

A $56

Methyl Methanoate

107-31-3

$- See Methyl Formate

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Methyl Propyl Ketone

107-87-9

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 5 NIOSH 1300

GC/FID

A $56 Synonym: 2-Pentanone

M-3500

3M POVM, 3500


GC/FID

A $56

n-Methyl Pyrrolidone

(NMP)

872-50-4

T-01

Charcoal, 226-01

30 - 125 0.05 -0.2 20 NIOSH 1302

GC/FID

E $56 Protect from prolonged light exposure. Refrigerate samples

and ship cold overnight.

M-3500

3M POVM, 3500


GC/FID

E $56

Methyl Styrene (alpha)

98-83-9

T-01

Charcoal, 226-01

3 - 30 0.2 20 NIOSH 1501M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Methyl Styrene,

meta and para

25013-15-4

$- See Vinyl Toluene

2-Methyl-1,3- Butadiene

78-79-5

$- See Isoprene

4-Methyl-2- Pentanone

108-10-1

$- See Methyl Isobutyl ketone (MIBK)

2-Methyl-4-Isothiazolin-3-

One

2682-20-4

$- See Kathon 886 Biocide

Methylal

109-87-5

T-01

Charcoal, 226-01

1 - 3 0.01 - 0.2 20 NIOSH 1611

GC/FID

S $56 Also known as Dimethoxymethane

M-3520


1 Hour 0.0379 30 NIOSH 1611M

GC/FID

A $56

Methylamine

74-89-5

T-30-18

NITC-Treated XAD-2,

226-30-18

1-20 0.01-0.1 4 NIOSH 2540M

HPLC

N $116 Preferred method. Store media cold before sampling.

Samples stable ambient temperature for at least 15 days.

T-96


XAD-7, 226-96

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2

3 OSHA 40

HPLC

W $116

2-Methylbutyl Acetate

624-41-9

T-01

Charcoal, 226-01

TWA 10

STEL 3

TWA 0.01-0.2

STEL 0.2

20 NIOSH 1450

GC/FID

A $56

1-Methylbutyl Acetate

626-38-0

$- See sec-Amyl Acetate.

4,4’ Methylene bis (2-

Chloroaniline)

101-14-4

$- See MOCA

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Methylene Bisphenyl

Diisocyanate

101-68-8 (4,4’-MDI)

5873-54-1 (2,4’-MDI)

K-20

OSHA Isocyanate Kit for

Field Desorption (see

description at right)

15 - 240 1 0.12 OSHA 47

HPLC/FL











kit includes C-14 cassette, V-04 vial with 3mL 90/10 (v/v)








Methylene Bisphenyl

Diisocyanate, Polymeric

(PMDI), Air Sample

9016-87-9 and others

K-20




15 - 240 1 Variable OSHA 47

Mod. HPLC/FL

O $116 ($58 if

tested along

with MDI

monomer)

Sample open faced. Refrigerate media before and after


















Methylene Bisphenyl

Diisocyanate, Polymeric

(PMDI), Bulk Sample

Characterization

9016-87-9 and others

Vial 1-5 mL of un-diluted MDI/

PMDI product

Variable OSHA 47

Mod. HPLC/FL

O $158 Bulk sample of undiluted MDI/PMDI product is required.

Contact lab for specific instructions.

Methylene Chloride

75-09-2

See dichloromethane.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

4,4-Methylene Dianiline

101-77-9

K-13

C-15 (H2SO4 Treated GFF)

plus 2 vials with 2 ml DI

water for field transfer.

1000 Max 1.0 - 2.0 0.1 NIOSH 5029M

HPLC/UV

NC $102 Within 4 hours after sampling, transfer each filter to a

separate glass vial containing 2 ml deionized water.

Methylenebis(4-

Cyclohexylisocyanate)

5124-30-1

K-20




15 - 60 1 0.4 OSHA PV2092

HPLC



















n-(1-Methylethyl)-2-

Propanamine

108-18-9

See Diisopropylamine.

Methylolacrylamide

924-42-5

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1

1.5 IHHPLC-P003

HPLC/UV

NC $160 Acrylamide may also be tested along with n-

methylolacrylamide.

Synonym: N-(Hydroxymethyl)acrylamide.

2-Methyl-2,

4-Pentanediol

107-41-5

See Hexylene Glycol.

Methyltin Trichloride

993-16-8

T-30-16

GFF/XAD-2 OVS,

226-30-16

TWA 15-75

STEL 15 Max

TWA 0.25

STEL 1.0

0.1 NIOSH 5526

GC/FPD

NC Call for

pricing.


dedicated instrument; 3-sample minimum applies. Analysis

is also available for the following agents on one sample:

dimethyltin dichloride and trimethyltin chloride. Samples

are subcontracted to an outside laboratory.

MIAK

110-12-3

$- See methyl Isoamyl Ketone

MIBK See Methyl Isobutyl Ketone

Mineral Oil as particulate

8052-41-3

$- See Oil Mist

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Mineral Spirits

8052-41-3, 68551-17-7,

64741-65-7, others

T-01

Charcoal, 226-01

20 0.01 - 0.2 50 OSHA 48 GC/FID A $77

M-3500

3M POVM, 3500


GC/FID

A $77

MOCA

101-14-4

K-13

C-15 (H2SO4 Treated GFF)

plus 2 vials with 2 ml DI

water for field transfer.

100 Max 1.0 Max 0.1 OSHA 71M

(sampling)

NIOSH P&CAM

236M (analysis)

HPLC/UV

NC $116 Transfer each filter (using tweezers) to a separate glass vial

containing 2 mL DI water within 10 hours of sampling.

Extracted samples are stable at room temperature for at

least 2 weeks.

Mold Spore Count & ID

(Non-Viable) N/A

C-23

Air-O-Cell Cassette

150 15 Standard

Microscopy

NA

NC Call for

pricing

See Indoor Air Quality Profiles. Rush Turnaround requires

notification.

Mold Spore ID

(Non-Viable)

Bulk N/A

1X1 inch NA Presence/

Absence

Standard

Microscopy

NA

NC Call for

pricing

See Indoor Air Quality Profiles. Rush Turnaround requires

notification.

Molybdenum, Total

7439-98-7

C-05


50 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP-OES

T $40

Monochloroacetic Acid

79-11-8

T-47-01


10 - 100 0.05 - 0.2 1 NIOSH 2008

IC

V $69 Store samples cold and in the dark. Synonym: Chloroacetic

Acid.

Monochlorobenzene

108-90-7

$- See Chlorobenzene.

Morpholine

110-91-8

T-30-18

NITC-Treated XAD-2,

226-30-18


HPLC

N $116 Preferred Method. Store media cold before sampling.

Samples stable at ambient temperature for at least 15 days.

T-98


226-98

10 Max 0.1 Max OSHA PV2133

GC/FID

NC Call for

pricing

Store and ship cold after sampling. Samples are

subcontracted to an outside laboratory.

MPK

107-87-9

$- See Methyl Propyl Ketone.

MTBE

1634-04-4

$56 See Methyl t-Butyl Ether.

Naphtha, Petroleum (MW =

97.8-110)

8030-30-6

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 NIOSH 1550

GC/FID

A $77 Ship 5 ml pure distillate in separate shipment for reference.

M-3500

3M POVM 3500


GC/FID


Naphtha, VM & P

(MW = 118-130)

8032-32-4

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 NIOSH 1550

GC/FID


M-3500

3M POVM, 3500


GC/FID


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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Naphthalene

91-20-3

T-110

Chromosorb 106,

226-110

TWA 10 Max

STEL 3 Max

0.2 Max 5 OSHA 35

GC/FID

A $56

T-01

Charcoal, 226-01

30 0.2 Max 20 NIOSH 1501M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC

NC $116 See methods listed above for monitoring naphthalene

alone; this entry describes monitoring for a PAH Profile.





delivery.

Nickel

7440-02-2

C-05


400 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP-OES

T $40

C-05


400 - 1000 1.0 - 3.0 0.063 NIOSH 7300

ICP-OES

T $46

Nickel Carbonyl

(as Ni)

13463-39-3

O-304

Low-Nickel charcoal, ORBO

304,

Supelco PN 20041

10 - 80 0.05 - 0.2 0.03 NIOSH 6007M

ICP/MS

NC $77 MCEF prefilter (C-05) is required when nickel particulates

are present. Do not return filter after sampling.

Nicotine

54-11-5

T-93

XAD-4, 226-93

0.5 - 600 0.1 - 1 1 NIOSH 2551

GC/NPD

NC $127 Store cold and ship cold overnight, protect from light.

Stable for 2 weeks at 5°C.

T-93

XAD-4, 226-93

1-24 hours (duration limited

by sorbent capacity of

approx. 300 ug nicotine)

1.5 Max 0.2 ASTM D5075

GC/NPD

NC $127 Store samples in freezer, ship cold overnight. Stable for 8

weeks at -10ºC. Testing for 3-ethenylpyridine also available,

for Environmental Tobacco Smoke (ETS) monitoring.

Nitrates, Particulate

N/A

C-05


3 - 100 0.5 - 1.5 5 NIOSH 7903M

IC

U $69

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Nitric Acid

7697-37-2

C-68

Na2CO3-treated Quartz +

Quartz prefilter

30 - 600 2.0 5 NIOSH 7907

IC/COND

SS Samples require at least 4 days equilibration prior to

analysis.

T-10-03


226-10-03

TWA 96

STEL 7.5

TWA 0.5

STEL 0.5 Max

5 OSHA ID1655G

IC/COND

U

T-10-03


226-10-03

3 - 100 0.2 - 0.5 5 NIOSH 7903

IC








see Acid Mist Profile.

Nitric Oxide

(NO)

10102-44-0

T-40

TEA-treated Molecular

Sieve, 226-40

1.5 - 6 0.025 1.3 NIOSH 6014

Spec

NC $69 Third tube in train of three (TEA tube for NO2, followed by

oxidizer tube, followed by TEA tube for NO). Discard

oxidizer tube after sampling. NO is tested only from the

third tube in train. Store tubes cold. Samples are stable at

ambient temperature for at least 7 days. Inorganic nitrites

cause positive interference.

p-Nitroaniline

100-01-6

C-05


TWA 480

STEL 60

TWA 1-4

STEL 4

10 NIOSH 5033

HPLC/UV

NC $116 Note: This method is applicable to p-nitroaniline aerosol

but not for environments where vapor may be present.

Nitrobenzene

98-95-3

T-10

Silica Gel, 226-10

10 - 150 0.01 - 1.0 5 NIOSH 2005

GC/FID

K $56

Nitroethane

79-24-3

T-30-06 (2)

XAD-2, 226-30-06

3 0.01-0.05 40 NIOSH 2526

GC/FID

NC $56 Two 226-30-06 tubes in series.

Nitrogen Dioxide

10102-44-0

T-40-02


Sieve, 226-40-02

1.5 - 6

(see notes at right regarding

improved sensitivity)

0.025 - 0.2 2 NIOSH 6014

Spec

NC $69 The NO2 TLV has been lowered since publication of NIOSH

Method 6014, which describes validation performed in

NIOSH 2nd Edition Method S320. This validation

demonstrated efficient collection at a rate of 0.064 L/min

for 180 minutes (11.5 L) in at atmosphere of 11.6 ppm

NO2/84% RH. Two tubes may be sampled in series for

indication of breakthrough. Store tubes cold before

sampling. Samples are stable at ambient temperature for at

least 7 days. No oxidizer tube needed.

M-04

SKC NO2 & SO2 Passive

Sampler, UMEx-200

15 min. up to 24 hours 0.0173 1.0 SKC #40108 rev.

1102

IC/COND

SS $69 May be tested for sulfur dioxide also. Samples are stable

for 3 weeks at ambient temperature. Return sampler to

aluminized pouch and seal for storage and shipping.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Nitrogen Dioxide/Nitric

Oxide (NO2 / NO)

N/A

T-40


Sieve, 226-40

1.5 - 6 0.025 NO 1.3

NO2 2.0

NIOSH 6014

Spec

NC $153 Three tubes in train are required (TEA tube for NO2,

followed by oxidizer tube, followed by TEA tube for NO).

Discard oxidizer tube after sampling. Since NO requires

oxidation before trapping, the notes above regarding

improved test sensitivity for NO2 do not apply. Store tubes

cold before sampling. Samples are stable at ambient

temperature for at least 7 days. Inorganic nitrites cause

positive interference.

Nitromethane

75-52-5

T-110

Chromosorb 106,

226-110

2.4 0.02 2 NIOSH 2527

GC/NPD

NC Call for

pricing

Rear sorbent section must be transferred to a vial

immediately after sampling. Samples are subcontracted to

an outside laboratory.

2-Nitropropane

79-46-9

T-110

Chromosorb 106,

226-110

3 0.01-0.05 1.4 NIOSH 2528

GC/FID

NC $56

1-Nitropyrene

5522-43-0

C-06

GFF, 37mm, 1um, 3PC

960 2 Max 1 OSHA 58M

HPLC

MM $116

Nonyl Acetate

143-13-5

IMP-07

MFGB, Methanol

10 0.05 - 0.1 300 NIOSH 1450M

GC/FID

A $56 Part of Optisol Rotary. DuPont product.

Nonylphenol

84852-15-3

T-95

XAD-7, 226-95

24 Max 0.1 Max 100 OSHA PV2085M

HPLC/UV

K $160 Mixed isomer CAS #25154-52-3.

Nuisance Particulates,

Respirable

N/A

$- See Particulates, Respirable.

Nuisance Particulates, Total

N/A


Octamethylcyclotetrasi-

loxane

556-67-2

T-09

Charcoal, 226-09

TWA 96

STEL 30

TWA 0.2

STEL 2.0

16 IHGC-P040

GC/FID

A $77 Store samples in freezer, ship cold overnight.

n-Octane

111-65-9

T-01

Charcoal, 226-01

3 - 10 0.01 - 0.2 20 NIOSH 1500

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

n-Octylamine

111-86-4

T-93

XAD-4, 226-93

TWA 96

STEL 9

TWA 0.2

STEL 0.6

40 IHGC-P023

GC/FID

K $77 Store samples in chemical refrigerator if not immediately

shipped for analysis.

T-30-18

NITC-Treated XAD-2,

226-30-18

10 0.1 Max 0.4 NIOSH 2540M HPLC NC $116 Store media cold before sampling. Samples stable at


t-Octylamine

107-45-9

T-93

XAD-4, 226-93

TWA 96

STEL 9

TWA 0.2

STEL 0.6

86 IHGC-P023

GC/FID



2-N-Octyl-4-Isothiazolin- 3-

One

26530-20-1

T-99

GFF/Silica Gel OVS,

226-99

TWA 96

STEL 15

TWA 0.2

STEL 1.0

0.6 IHHPLC-P002

HPLC/UV

K $160 Note: STEL samples may have to be repeated several times

in succession with the SAME tube in order to achieve

adequate sensitivity. Store samples in chemical refrigerator

if not immediately shipped for analysis.

Synonym: Kathon ® 893 Biocide, RH 287.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Oil Mist,

Custom

8012-95-1

C-11


5um

100 - 500 1.0 - 3.0 50 NIOSH 5026

FTIR

NC $127 Unweighed media may be used if total particulate results

are not required (C-05 or C-10). Ship a 5 ml bulk sample of

undiluted oil (not emulsion) separately for standardization.

Oil must be Freon 113 soluble.

Oil Mist,

Mineral

8012-95-1

C-11


5um

100 - 500 1.0 - 3.0 50 NIOSH 5026

FTIR

NC $77 Unweighed media (C-05 or C-10) may be used if total

particulate results are not required. Commercial white

mineral oil will be used as reference.

Oil Mist,

as Particulate

8012-95-1

C-11


5um

50 -1000 1.0 - 3.0 50 NIOSH 0500

Gravimetric

NC $21 Other non-oil particulates will positively interfere.

Optisol Inline

70914-20-4

$- See Heptyl Alcohol and Heptyl Acetate entries.

Optisol Rotary

143-13-5

$- See Nonyl Acetate and Benzyl Alcohol entries.

Oxalic Acid as Particulate

144-62-7

C-11


5um, 2PC

TWA 480-960

STEL 60

1-4 50 NIOSH 0500

Gravimetric


Oxone™,

measured as Sulfate Ion

10361-76-9

C-05


30 - 480 0.5 - 2.0 5 OSHA ID 113

IC

U $79 Oxone is DuPont's trade name for the potassium salt of

peroxymonosulfuric acid. This procedure uses a modifi-

cation of OSHA Method 113 (Sulfuric Acid

sampling/analysis) for filter sampling of oxone, followed by

reduction to sulfate and analysis by Ion

Chromatography/Conductivity Detection. The sulfate

measurement is mathematically converted to an Oxone

equivalent.

10,10-Oxybisphenoxarsine

58-36-6

C-05


TWA 480

STEL 60

TWA 1-4

STEL 4

0.05

as Arsenic

NIOSH 7901

GFAA

NC $51 On Analysis Request form specify “Arsenic-GFAA” analysis

(GFAA stands for Graphite Furnace Atomic Absorption and

provides a lower limit of quantitation than standard ICP

analysis) and request results reported as micrograms and

mg/M3 Oxybisphenoxyarsine, 10, 10’-. (To convert Arsenic

results to Oxybisphenoxyarsine, 10, 10’- (C24H16A- s2O3;

molecular weight 502.2) in the same units, multiply by

3.35). Note: This test is not chemically specific in that all

sources of Arsenic will contribute to the total result.

Ozone

10028-15-6

C-22

GFFs (2), nitrite-treated,

37mm, 2PC

TWA 90

STEL 22.5

TWA 0.25 - 0.5

STEL 1.5

6.25 OSHA ID 214

IC

NC $69 May be sampled up to 480 minutes at 0.25 LPM. Store and

ship media cold. Media has very short shelf life (<5 weeks).

Minimum order of 10 units. Sulfur dioxide gas and airborne

particulate nitrate salts are positive interferences. If SO2 is

known to be present, it can be eliminated by preceding the

filter with an oxidizer tube. Field blank is imperative (two

treated filters per cassette).

PAH Profile

N/A

$- See Polynuclear Aromatic Hydrocarbons

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

PAH Profile - Selected

Analytes N/A

$- See Polynuclear Aromatic Hydrocarbons - Selected

Analytes.

Paraffin Wax Fumes

8002-74-2

C-06

GFF, 37mm, 1um, 3PC

200 - 600 1 100 OSHA PV2047

GC/FID

NC $77

Particle Characterization/

ID

N/A

1 - 10 grams NA NA EPA/600/M4- 82-

620, Dec. 1982

PLM

NC $102 Morphological examination by PLM. Also see indoor air

quality profiles. Sample types include mini-vac samples,

scrapings, bulk materials in sealed bags, tape lifts, or MCEF

filters.

Particle Sizing, Bulks

N/A

$- Optical microscopy. Please see Section V.5 for details on

multiple size ranges & pricing.

Particulate Matter, <10

microns

N/A

X-13

Hi-Vol GFF, Pre- weighed,

8”x10”, 1um

1585 cubic meter 28 1 mg 40CFR Pt 50

App B Gravimetric

NC $38 Size-selective sampler is required, sampling at the

manufacturer’s specified flow rate. This listing is for a 1

CFM PM10 high volume sampler.

Particulate Matter, <10

microns

N/A

C-40

PEM Sampler PTFE,

Preweighed, 2um

(Anaslide), Serialized

2000

(see notes at right)

Specific to

impactor used

50 EPA IP-10A

Gravimetric

NC $38 This listing is for the SKC PEM PM10 series of impactors,

available for various sampling rates. Air volume of 2000

liters provides testing sensitivity down to 0.050 mg/M3.

Particulate Matter, Total

Suspended

(High Vol Sampler) N/A

X-13

Hi-Vol GFF, Preweighed,

8”x10”, 1um

1585 cubic meter 28 1 mg 40CFR Pt 50

App B Gravimetric

NC $38 Requires high volume sampler at 28 LPM. Filter can also be

analyzed for Lead (Pb) particulates.

Particulates,

Not Otherwise Classified

N/A


Particulate Size Estimate

(Bulk, Surface or Air)

2 Ranges

10 grams <2.5 mm,

≥2.5 mm or

<10 mm,

≥10 mm

Call for

pricing.

Samples are subcontracted to an outside laboratory.



3 Ranges

10 grams <2.5 mm,

≥2.5 mm or

<10 mm,

≥10 mm

Call for

pricing.


Particulates, Inhalable

N/A

SKC IOM Sampler

with preweighed

cassette/filter *

960 2.0 500 NIOSH 0500M

GRAV

NA *Preweighed filters/cassettes can be provided with PVC or

PTFE filters, and stainless steel or plastic cassettes. Filter

and cassette choice may depend upon any additional

testing to be performed on the sample. Call lab to discuss

specific situation.

Particulates, Respirable

N/A

C-11 or C-12

PVC, Preweighed, 5um

170 - 1000 See comments 50 NIOSH 0600

Gravimetric

$21 Sampling rate and cassette type vary with cyclone type. SKC

Aluminum Cyclone, 2.5 LPM, C-12 (3-piece cassette). Nylon

Dorr-Oliver Cyclone, 1.7 LPM, C-11 (2-piece cassette).

...........................................

Synonyms: Respirable Particulates Not Otherwise

Regulated, Nuisance Respirable Dust.

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"Respirable Silica"



Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Particulates, Total

N/A

C-11


5um, 2PC

50 - 1000 1.0 - 2.0 50 NIOSH 0500

Gravimetric

$21 Three (3) piece preweighed PVC cassette (C-12) is also

suitable. ....

Synonyms: Particulates Not Otherwise Regulated (PNOR),

Nuisance Dust.

Particulates, Total

N/A

C-04


Matched-weight

50 - 1000 1.0 - 2.0 100 NIOSH 0500

Gravimetric

$21 Matched weight MCE filter; does not require preweighing.

Filter can also be analyzed for metals. Synonyms:

Particulates Not Otherwise Regulated (PNOR), Nuisance

Dust.

Particulates, PM10

N/A

See Particulate matter <10 microns

PCB Caulk/Oil/Water/Soil See Environmental Directory of Services.

PCB

Vapor & Particulate

N/A

$- See Polychlorinated Biphenyls - Vapor & Particulate

PCB

Wipe

N/A

X-PCB

Paper filter, 7cm,

hexane-moistened

100 cm2 2 ug/ wipe SW-846 8082

GC/ECD

S $102 Also See Environmental Directory of Services.

Pentachlorophenol

87-86-5

T-57


50 - 100 0.2 - 0.5 2 OSHA 39M

HPLC

K $116

n-Pentane

109-66-0

T-01

Charcoal, 226-01

2 0.05 - 0.1 10 NIOSH 1500

GC/FID

A $56

M-3520


Up to 4 hours 15 NIOSH 1500M

GC/FID

A $56

2,4-Pentanedione

123-54-6

$- See Acetylacetone

1-Pentanol

71-41-0

$- See Amyl Alcohol.

2-Pentanone

107-87-9

$- See Methyl Propyl Ketone.

1-Pentyl Acetate

628-63-7

$- See n-Amyl Acetate.

2-Pentyl Acetate

626-38-0

$- See sec-Amyl Acetate.

Perchloroethylene

127-18-4

$- See Tetrachloroethylene.

Perfluoro Pentane

138495-42-8

$- See Decafluoropentane.

Perfluorobutyl Methyl Ether

Isomer mixture

(163702-07-6 &

163702-08-7)

O-91

Carbosieve S-III, Orbo 91


GC/FID

F $56 Store and ship samples cold, analyze ASAP.

Synonym: HFE-7100.

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Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Petroleum Distillates

Customer-provided bulk as

reference standard

General Term

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 NIOSH 1550

GC/FID

A $77 Send 5 ml pure distillate separately for standardization. If

no pure distillate bulk is available, see “Petroleum

Distillates, Best-Fit” below.

Petroleum Distillates,

Best-Fit

[No pure distillate bulk

available as reference

standard]

General Term

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 NIOSH 1550

GC/FID

A $127 Sample chromatographic peak pattern is compared to in-

house multi-component hydrocarbon mixtures (Stoddard

Solvent, VM&P Naphtha, Mineral Spirits, etc.) to identify

best available reference standard. If no match is found,

results are reported as Total Hydrocarbons as Hexane.

Petroleum Ether

8032-32-4

$- See Naphtha or Petroleum Distillates

PGME

107-98-2

$- See Propylene Glycol Methyl Ether

PGMEA

108-65-6

$- See Propylene Glycol Methyl Ether Acetate

Phenanthrene

85-01-8

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC





delivery.

Phenol

108-95-2

T-95

XAD-7, 226-95


HPLC/UV

K $116 Cresols may also be tested from the same sample.

Phenothiazine

92-84-2

C-06

GFF, 37mm, 1um, 3PC

TWA 100

STEL 15

TWA 1.0

STEL 1.0

30 IHGC-P031

GC/FID

NC $77

2-Phenoxyethanol

122-99-6

T-01

Charcoal, 226-01

10 Max 0.2 Max 10 OSHA CSI

GC/FID

E $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Phenyl Chloroformate

1885-14-9

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID



4-Phenyl Cyclohexene

4994-16-5

T-01

Charcoal, 226-01

24 - 100 0.2 0.15 OSHA 7

GC/MS

A $56 Carpet gas irritant.

Phenyl Ether

101-84-8

T-01

Charcoal, 226-01

10 - 50 0.2 10 NIOSH 1617

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Phenyl Ether / Diphenyl Mix

(eutectic mixture)

101-84-8 & 92-52-4

T-10

Silica Gel, 226-10

1 - 40 0.01 - 0.2 2 ug for each

compound

NIOSH 2013

GC/FID

NC $112 Analyzed and reported separately as Phenyl Ether and

Diphenyl. …………………………………… ….

Synonym: Dowtherm A™

Phenyl Glycidyl Ether

122-60-1

T-01

Charcoal, 226-01

80 - 150 0.1 - 1.0 20 NIOSH 1619

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

m-Phenylenediamine

108-45-2

C-15 GFFs (2),

H2SO4-treated, 37mm, 3PC

100 1 1.3 OSHA 87

HPLC

NC $116 p-Phenylenediamine is reported on 226-30-18

Phosgene

75-44-5

T-153


226-153

TWA 48

STEL 3

TWA 0.1

STEL 0.2

5 AIHAJ 12/1986,

pp.742-746

GC/FID


Samples must arrive at lab within 10 days of sampling. This

method is not sensitive enough to meet NIOSH ceiling REL -

0.2 ppm.T-117

HMP-Treated XAD-2,

226-117

100 - 240 0.5 - 1.0 OSHA 61

GC/NPD

NC Call for

pricing


Phosphine

7803-51-2

C-9018

GFF/ HgCl2-treated

Polyester, 37mm, 3PC, SKC

PN 225-9018

TWA 240 Max

STEL 30

TWA 1.0 Max

STEL 2

11 OSHA 1003

ICP

NC Call for

pricing

Special order media - call at least one week in advance.

Minimum order of 10 units. Must submit blank.

Phosphoric Acid

7664-38-2

C-05


30 - 960 0.5 - 1.5 10 OSHA ID 111

IC

U $69 Transfer filter to vial within 1 hour of sampling.

T-10-03


226-10-03

3 - 100 0.5 10 NIOSH 7903

IC









T-10-03


226-10-03

TWA 96

STEL 7.5

TWA 0.5 Max

STEL 0.5

10 OSHA ID1655G

IC/COND

U

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Phosphorus

(applicable to non-volatile

phosphorus-

containing compounds)

C-05


100 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP

T $40 Not suitable for sampling/analysis of elemental yellow or

white phosphorus.

Phosphorus Trichloride

7719-12-2

IMP-14

MFGB, 15 mL DI Water

25 0.05-0.2 Approx. 7 NIOSH 6402M

ICP

$77

o-Phthalaldehyde

643-79-8

T-119


226-119

480 Max 0.03 - 1 0.4 JEM,2008, v10.

p1337

HPLC/ UV

NC $116 Store media and samples cold, ship cold overnight. Ozone

may interfere - use ozone scrubber in known ozone


and deplete the DNPH, and is a potential interference.

Media contains residual acetonitrile which could interfere

with acetonitrile monitoring. Also see Aldehyde profile.

Phthalic Anhydride

85-44-9

C-28

GFFs (2), veratrylamine-

treated, 37mm, 4PC

75 - 100 1.0 Max 2 OSHA 90

HPLC

O $116 Sample open faced. Store media cold. Store samples cold if

not shipped to lab immediately. Media shelf life is 1 month.

Pivaloyl Chloride

3282-30-2

T-153


226-153

TWA 48 TWA

STEL 3 STEL

TWA 0.1 TWA

STEL 0.2 STEL

5 AIHAJ 12/1986,

pp.742-746 GC/FID



Synonym: Trimethylacetyl chloride

PIXE SCAN AIR

N/A

C-05


100 - 1000 1.0 - 2.0 NA SPM

PIXE

NC $- Covers element range of sodium to uranium. Samples are

subcontracted to outside laboratory. Analyzed by proton

induced x-ray emission spectroscopy.

PIXE SCAN BULK

N/A

N/A N/A NA SPM

PIXE

NC $- Good scan for unknown bulk materials for elemental

composition. Subcontracted to outside laboratory.

Platinum

7440-06-4

C-05


20 - 1000 1 - 3 2 NIOSH 7300M

ICP

OO $40

Platinum,

Soluble Compounds

Various

C-05


500 - 1000 1 - 3 0.1 NIOSH

S191 ICP/MS

J $75

PM10

N/A

$- See Particulate Matter, <10 microns.

Polychlorinated Biphenyls

- Caulk (PCBs)

See Environmental Testing Directory


Oil (PCBs)

See Environmental Testing Directory

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment


Vapor & Particulate (PCBs)

N/A

K-02

Swinnex GFF +

226-39 + vial

50 0.05 - 0.2

(see notes at

right)

0.2 NIOSH 5503

GC/ECD

NC $153 Transfer filter and Teflon ring to a glass vial immediately

after sampling. At low concentrations samples may be

collected at 1 lpm for up to 24 hours. Sample volume of

>200 liters will measure down to the NIOSH REL = 1 ug/M3.

Polynuclear Aromatic

Hydrocarbons

N/A

K-06

PTFE + ORBO 43

200 - 1000 2 Varies NIOSH 5506

HPLC

N $284 Wrap cassettes in aluminum foil if sampling in bright

sunlight. Transfer filter to glass vial immediately after

sampling, and wrap the vial and tube with aluminum foil to

protect from light. Ship samples cold for overnight delivery.

Profile includes Acenaphthene, Acenaphthylene,

Anthracene, Benzo(k)fluoranthene, Benzo(g,h,i)perylene,

Benzo(a) pyrene, Benz(a)anthracene,

Benzo(b)fluoranthene, Chrysene, Dibenz(a,h)anthracene,

Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene,

Naphthalene, Phenanthrene, Pyrene.


Hydrocarbons

Selected Analytes

N/A

C-06

GFF, 37mm, 1um, 3PC

960 2 Varies OSHA 58

HPLC

MM $226 Transfer filters to glass vials after sampling and wrap with

aluminum foil to protect from light. Ship samples by

overnight delivery. Analytes includes Anthracene, Benzo(a)

pyrene, Chrysene, Phenanthrene, Pyrene.

Potassium

7440-09-7

C-05


50 - 1000 1.0 - 3.0 7 NIOSH 7300M

ICP

T $40 Elemental potassium analysis can be used to determine

equivalent concentrations of potassium compounds.

Potassium Borohydride

13762-51-1

C-05


TWA 48-480

STEL 45

TWA 1-3

STEL 3

10 NIOSH 7300M

ICP

$40 On Analysis Request form specify “Boron” analysis and

request results reported as Potassium Borohydride (To

convert Boron results to Potassium Borohydride in the

same units, multiply Boron analysis results by 10. Note: This

test is not chemically specific in that all sources of Boron

will contribute to the total result).

Potassium Hydroxide,

measured as Alkaline dust

1310-58-3

C-66

PTFE, 1um, 37mm, 2PC

70 - 1000 1.0 - 4.0 60 NIOSH 7401

Titration

NC $69 Also see entry for Alkaline Dust. This test provides a single

cumulative measure of all alkaline aerosols present in the

exposure; e.g., sodium hydroxide, potassium hydroxide,

sodium bicarbonate, calcium carbonate, etc. The acid-base

titration test is not compound-specific, but the result will

be expressed in terms of the alkaline compound identified

on the test request form. Acid compounds present in the

sampling environment will be negative interferences in the

measurement.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Potassium Hydroxide (by

elemental potassium

analysis with KOH-

equivalent calculation)

1310-58-3

C-05


50 - 1000 1.0 - 3.0 3.6 NIOSH 7300M

ICP/MS

T $46 Elemental analysis for potassium is performed, and a

potassium hydroxide equivalent result is calculated. Other

potassium compounds are a positive interference. Mineral

acids will not interfere.

Potassium Persulfate,

As Persulfate

7727-21-1

C-05


TWA 480-960

STEL 60

TWA 1-4

STEL 4

0.5 NIOSH 7300

ICP

$40 Wen submitting samples specify analysis for “Potassium

Persulfate, AS PERSULFATE” in order to have results

reported correctly as persulfate. This test is not chemically

specific; all sources of Potassium will contribute to the total

result.

Primene 81R® Amine

68955-53-3

T-93

XAD-4, 226-93

TWA 10

STEL 3

0.025-0.2 13 IN-HOUSE

GC/FID



2-Propanol See Isopropanol.

2-Propenol

107-18-6

$- See Allyl Alcohol.

Propionaldehyde

123-38-6

T-119


226-119

1 - 30 0.05 - 0.5 0.5 TO-11

HPLC




potential negative interferences. Refrigerate before and

after sampling and ship overnight. Also see aldehyde

profiles.

Propionic Acid

79-09-4

T-10-03


226-10-03

1 - 24 0.05 - 0.2 10 NIOSH 2011M

IC/Cond.

V $69

1-Propoxy-2-Propanol

30136-13-1

$- See Propylene Glycol Propyl Ether.

2-Propoxyethanol See Ethylene glycol monopropyl ether

n-Propyl Acetate

109-60-4

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 10 NIOSH 1450

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

n-Propyl Alcohol

71-23-8

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 20 NIOSH 1401

GC/FID

C $56 Synonyms: 1-Propyl alcohol, 1-Propanol.

M-3500

3M POVM, 3500


GC/FID

C $56 Synonyms: 1-Propyl alcohol, 1-Propanol.

Propyl Bromide

106-94-5

$- See 1-Bromopropane

2-Propylbromide

75-26-3

$- See 2-Bromopropane

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Propylene Dichloride

78-87-5

T-81

Anasorb 747, 226-81

1 - 3.5 0.01 - 0.2 20 NIOSH 1013M

GC/FID

NC $77 Synonym: 1,2-Dichloropropane.

M-3500

3M POVM, 3500


GC/FID

NC $77 Synonym: 1,2-Dichloropropane.

Propylene Glycol

57-55-6

T-57


5 - 60 0.5 - 2.0 20 NIOSH 5523

GC/FID

K $77 Also see Glycol Profile.

Propylene Glycol

n-Butyl Ether

5131-66-8

T-01

Charcoal, 226-01

5 - 10 0.1 20 OSHA 99M

GC/FID

E $56 Synonyms: 1-Butoxy-2-Propanol, also DOWANOL® PnB

M-3500

3M POVM, 3500


GC/FID

E $56 Synonym: 1-Butoxy-2-propranol

Propylene Glycol Methyl

Ether

107-98-2

T-01

Charcoal, 226-01

5 - 10 0.1 20 OSHA 99

GC/FID

E $56 Synonyms: 1-Methoxy-2-Propanol, PGME.

M-3500

3M POVM, 3500


GC/FID

E $56 Synonyms: 1-Methoxy-2-Propanol, PGME.

Propylene Glycol Methyl

Ether Acetate

108-65-6

T-01

Charcoal, 226-01

5 - 10 0.2 20 OSHA 99

GC/FID

E $56 Synonyms: 1-Methoxy-2-Propyl Acetate, PGMEA, Dowanol

PMA

M-3500

3M POVM, 3500


GC/FID

E $56 Synonyms: 1-Methoxy-2-Propyl Acetate, PGMEA.

Propylene Glycol Propyl

Ether

1569-01-3

T-01

Charcoal, 226-01

10 0.1 20 OSHA 7

GC/FID

E $56 Synonyms: n-Propoxypropanol, 1-Propoxy-2-Propanol,

Propasol P.

Propylene Oxide

75-56-9

T-01

Charcoal, 226-01

5 0.05 - 0.2 20 NIOSH 1612

GC/FID

A $56

M-3520



GC/FID

A $56

Pseudocumene

95-63-6

$- See 1,2,4-Trimethylbenzene.

Pyrene

129-00-1

K-06

PTFE + ORBO 43

200-1000 2 3 NIOSH 5506

HPLC





delivery.

Pyrethrum

8003-34-7

C-06

GFF, 37mm, 1um, 3PC

20 - 400 1.0 - 4.0 0.2 NIOSH 5008

HPLC

NC $116

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Pyridine

110-86-1

T-01

Charcoal, 226-01

18 - 150 0.01 - 1.0 10 NIOSH 1613

GC/FID

I $56

Pyrrolidine

123-75-1

T-30-18

NITC-Treated XAD-2,

226-30-18

1 - 20 0.01 - 0.1 2 NIOSH 2540M

HPLC

N $160 Contact laboratory before sampling and/or sending

samples. Ship samples immediately after sampling (next

day delivery).

Quartz

14808-60-7

$- See Silica - Crystalline Profile

Quinone

106-51-4

T-30

XAD-2 Tube, 226-30

TWA 24

STEL 3

TWA 0.01-0.2

STEL 0.2

2 NIOSH S181M

HPLC/UV

NC $116 Samples must be analyzed within 7 days.

Refractory Ceramic Fibers

N/A

$- See Fiber Count, Total - “A” counting rules.

Refrigerant 11

75-69-4

$- See Trichlorofluoromethane.

Refrigerant 113

76-13-1

$- See 1,1,2-Trichloro-1,2,2-Trifluoroethane.

Refrigerant 114

76-14-2

$- See 1,2-Dichloro-1,1,2,2-Tetrafluoroethane.

Refrigerant 12

75-71-8

$- See Dichlorodifluoromethane.

Refrigerant 123

306-83-2

$- See 2,2-Dichloro-1,1,1-Trifluoroethane.

Refrigerant 134a

811-97-2

$- See 1,1,1,2-Tetrafluoroethane.

Refrigerant 141b

1717-00-6

$- See 1,1-Dichloro-1-Fluoroethane.

Refrigerant 21

75-43-4

$- See Dichlorofluoromethane. Note low recommended air

volumes.

Refrigerant 22

75-45-6

$- See Chlorodifluoromethane.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Refrigerant 225 ca & cb

135151-96-1

T-09 (2)

Charcoal, 226-09

1 - 4 0.01 - 0.05 20 NIOSH 1018M

GC/FID

I $76 Each component (ca & cb) reported separately. Two (2)

tubes in series. Second tube can be smaller 226-01. Also

known as HCFC 225, AK-225 (TM) and

dichloropentafluoropropane. HCFC-225 ca =

3,3-dichloro-1,1,1,2,2-pentafluoropropane (CAS 422-

56-0), HCFC-225cb = 1,3-dichloro-1,1,2,2,3-

pentafluoropropane (CAS 507-55-1).M-3520



GC/FID

l $76 Each component (ca & cb) reported separately. Also known

as HCFC 225, AK-225 (TM) and

dichloropentafluoropropane. HCFC-225 ca = 3,3-dichloro-

1,1,1,2,2-pentafluoropropane (CAS 422-56-

0), HCFC-225cb = 1,3-dichloro-1,1,2,2,3-

pentafluoropropane (CAS 507-55-1).

Refrigerant 43

138495-42-8


Resorcinal

108-46-3

T-57

13 mm GFF + 200/100

XAD-7 OVS, 226-57

60 Max 1 Max 50 OSHA PV2053

GC/FID

K $110

Rhodium

7440-16-6

C-05

MCEF, 37mm, 0.8um,

3PC

960 Max 2 Max 2 NIOSH 7300M

ICP-OES

T

Rhodium, water-soluble

compounds

NA

C-05

MCEF, 37mm, 0.8um,

3PC

960 Max 2 Max 0.05 NIOSH

7300M

J

Ribavirin

36791-04-5

C-06

GFF, 37mm, 1um, 3PC

40 - 1000 1.0 - 3.0 1 NIOSH 5027

HPLC

NC $116 Not chemically specific.

Sebacic Acid

as Particulate

111-20-6

C-11


5um, 2PC

100-480 1-4 50 NIOSH 0500

Gravimetric

NC $21

Selenium

7782-49-2

C-05

MCEF, 37mm, 0.8um,

3PC

40 - 1000 1.0 - 3.0 1 NIOSH 7300

ICP-OES

T $40

C-05

MCEF, 37mm, 0.8um,

3PC

40 - 1000 1.0 - 3.0 0.125 NIOSH 7300

ICP-MS

T $46

Sevin/Carbaryl

63-25-2

T-30-16

GFF/XAD-2 OVS,

226-30-16

60 Max 1.0 Max 5 OSHA 63

HPLC/UV

NC $116

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Sevoflurane

28523-86-6

T-81

Anasorb 747, 226-81


GC/FID

CC $77

M-02

SKC POVM, 575-002

See note at right 40 OSHA 103M

GC/FID

A $77 Not recommended due to reverse diffusion.

M-3520



GC/FID

A $77

Silane

A-189

See entry for Mercaptopropyltrimethoxysilane, Gamma

Silica - Amorphous

(Diatomaceous Earth), Total

7631-86-9

C-11 or C-12


5um, 2PC

816-1320 2-4 NIOSH 7501

XRD

NC Call for

pricing


Silica - Amorphous (Fume),

Respirable

69012-64-2

C-12


5um, 3PC

816-1300 Dependent on

cyclone type

NIOSH 7501

XRD

NC Call for

pricing

Silica - Cristobalite

14464-46-1

$- See Silica, Crystalline Profile

Silica - Crystalline Profile

Multiple

C-11 or C-12


5um, 2PC

816-1200 See comments 5

(each

polymorph)

NIOSH 7500

XRD

NC $98 *Sampling rate is dependent on cyclone used - SKC

Aluminum Cyclone - 2.5 LPM, Nylon Dorr-Oliver Cyclone -

1.7 LPM. Preweighed PVC filters are specified so that

overall filter loading can be addressed correctly during

sample prep. Samples are stable (no stated hold time limit).

Profile includes gravimetric analysis, quartz (14808-60-7),

cristobalite (14464-46-1), and tridymite (15468-32-3).

Interferences include any compound that has a diffraction

line that coincides with the primary or secondary lines of

quartz. Common interferences are bauxite, mica, potash,

feldspar, graphite, and zircon.

Silica - Crystalline Bulk

Multiple

Vial or bag 2 - 5 gms N/A 1.0% NIOSH 7500

XRD

NC $134 Profile includes quartz (14808-60-7), cristobalite (14464-46-

1), and tridymite (15468-32-3). Interferences include any

compound that has a diffraction line that coincides with

the primary or secondary lines of quartz. Common

interferences are bauxite, mica, potash, feldspar, graphite,

and zircon.

Silica - Fused, Respirable

60676-86-0

C-12


5um, 3PC

800-1300 Dependent on

cyclone type

5 NIOSH 7501

XRD

NC $- Samples are subcontracted to outside laboratory.

Silica - Quartz

14808-60-7

$- See Silica, Crystalline Profile

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Silicon Tetrahydride

(Silane)

7803-52-3

IMP-15

MFGB, 15 mL 0.01N KOH

380 - 400 0.8 1 NIOSH 7300M

ICP

NC $40 Analysis is for dissolved silicon. Since the Midget Fritted

Glass Bubbler (MFGB) is glass, creation and submission of a

field blank is critical; maintain the field blank solution in the

MFGB for same duration as samples. Transfer to plastic vial

immediately after sampling. All other hydrolyzable silicon

hydrides will interfere, as will soluble particulate silicates.

Also submit a portion of unused collecting solution for

testing as a Reagent Blank.

Silver, Metal and Soluble

Compounds

7440-22-4

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 2000 1.0 - 3.0 1 NIOSH 7300

ICP

T $40

C-05

MCEF, 37mm, 0.8um,

3PC

51 - 2000 1.0 - 3.0 0.025 NIOSH 7300M

ICP/MS

T $46

Skane M-8 (R) Biocide

26530-20-1

$- See Kathon 893™ Biocide.

Sodium

7440-23-5

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0 - 3.0 2.5 NIOSH 7300M

ICP

T $40 Blank is important to correct for amount of sodium found

in MCE filters.

Sodium Bisulfite

as Particulate

7631-90-5

C-11 or C-12


5um, 2PC

960-1920 2-4 50 NIOSH 0500

Gravimetric

NC $21 Not chemically specific.

Sodium Borohydride

16940-66-2

C-05

MCEF, 37mm, 0.8um,

3PC

TWA 48-480

STEL 45

TWA 1-3

STEL 3

7 NIOSH 7300M

ICP for B

T $77 On Analysis Request form specify “Boron” analysis and

request results reported as Sodium Borohydride (To

convert Boron results to Sodium Borohydride in the same

units, multiply Boron analysis results by 3.5. Note: This test

is not chemically specific in that all sources of Boron will

contribute to the total result).

Sodium Cyanoborohydride

25895-60-7

C-05

MCEF, 37mm, 0.8um,

3PC

TWA 48-480

STEL 45

TWA 1-3

STEL 3

12 NIOSH 7300M

ICP for B

T $77 On Analysis Request form specify “Boron” analysis and

request results reported as Sodium Cyanoborohydride (To

convert Boron results to Sodium Cyanoborohydride in the

same units, multiply Boron analysis results by 5.83. Note:

This test is not chemically specific in that all sources of

Boron will contribute to the total result).

V01 06.2017

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Sodium Hydride

7646-69-7

C-08


TWA 480

STEL 60

TWA 1-4

STEL 4

0.25 NIOSH 7300M

ICP

T $77 Note: Obtain low sodium (pre-rinsed) Teflon filters from

lab. Submit 3 blanks along with each group of samples in

order to adequately correct for sodium background and

avoid false positives. Request analysis for “sodium”, to be

reported as “sodium hydride". The ACGIH states that if

instantaneous monitoring is not feasible, ceiling values

“can be assessed by sampling over a period that should not

exceed 15 minutes, except for those substances that may

cause immediate irritation when exposures are short.” Not

chemically specific.

Sodium Hydrosulfite

as Particulate

7775-14-6

C-11


5um, 2PC

TWA 100-480

STEL 60

1-4 50 NIOSH 0500

Gravimetric

NC $21 Analysis is not compound-specific.

Sodium Hydroxide,

measured as Alkaline Dust

1310-73-2

C-66

PTFE, 1um, 37mm, 2PC

45 - 1000 1.0 - 4.0 40 NIOSH 7401

Titration

NC $69 Also see Alkaline Dust as NaOH. This test provides a single

cumulative measure of all alkaline aerosols present in the

exposure; e.g., sodium hydroxide, potassium hydroxide,

sodium bicarbonate, calcium carbonate, etc. The acid-base

titration test is not compound-specific, but the result will

be expressed in terms of the alkaline compound identified

on the test request form. Acid compounds present in the

sampling environment will be negative interferences in the

measurement.

Sodium Hydroxide

(calculated from measured

sodium concentration)

1310-73-2

C-05


50 - 1000 1.0 - 3.0 4.5 NIOSH 7300M

ICP

T $40 Elemental analysis for sodium is performed, and a sodium

hydroxide equivalent result is calculated. Other sodium

compounds are a positive interference. Mineral acids will

not interfere.

Sodium Persulfate,

as Persulfate

7775-27-1

C-08


TWA 480-960

STEL 60

TWA 1-4

STEL 4

40 NIOSH 7300

ICP

T $40 Request analysis of “Sodium Persulfate, AS PERSULFATE” in

order to have results reported correctly as persulfate (To

convert “Sodium” results to “Sodium Persulfate, as

Persulfate”, multiply by 4.18).

Solder Operations Profile

N/A

C-05

MCEF, 37mm, 0.8um,

3PC

480 - 960 1.0 - 3.0 Varies OSHA ID-206

ICP

NC $127 Includes Antimony, Beryllium, Cadmium, Copper, Lead,

Silver, Tin, Zinc Oxide. 960 liters needed to determine silver

at the TLV.

Solvesso 100

N/A

$- See Aromatic 100

Solvesso 150

N/A

$- See Aromatic 150

V01 06.2017

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Stearic Acid

as Particulate

57-11-4

C-11


5um, 2PC

100-480 1-4 50 NIOSH 0500

Gravimetric

$21 Test is not chemically specific.

Stoddard Solvent

8052-41-3

T-01

Charcoal, 226-01

1 - 20 0.01 - 0.2 50 OSHA 48

GC/FID

A $77 Ship a 5 ml bulk sample separately.

M-3500

3M POVM, 3500


GC/FID

A $77 Ship a 5 ml bulk sample separately.

Strontium

7789-06-2

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0-3.0 2 NIOSH 7300M

ICP

T $40

Strontium Chromate

(as Cr VI)

133-82-0

$- See Chromium, Hexavalent.

Styrene

100-42-5

T-01

Charcoal, 226-01

5 - 15 0.05 - 0.2 40 NIOSH 1501

GC/FID

A $56

T-73


226-73

0.75 - 15 0.05 - 0.2 40 OSHA 89M

GC/FID

CC $56 Recommended method due to improved desorption

efficiency.

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10 STEL

3

TWA 0.03-0.2

STEL 0.2

3.1 Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hrs (Max)

STEL 15 min


IHGC-P029

GC/FID

A $77

Sulfate Particulate

N/A

C-05

MCEF, 37mm, 0.8um,

3PC

30 - 100 0.5 - 1.5 5 NIOSH 6004

IC

U $69 Test is not compound-specific; all water soluble sulfates,

including sulfuric acid, are measured.

Sulfur Dioxide

7446-09-5

K-05

KOH-treated Anasorb 747,

226-80

12-24 0.1 8.33 OSHA ID 200

IC

NC $69 Do not return pre-filter for analysis unless soluble sulfate

particulates are needed. Extra charge applies.

C-25

MCE/Na2CO3-treated filter,

37mm, 4PC

22.5-200 0.5 - 1.5 7 NIOSH 6004

IC

NC $69 15 minute sample at 1.5 LPM measures down to 0.12 ppm

SO , approx. 50% of ACGIH STELTLV.2

Sulfur Dioxide

7446-09-5

M-UMEX-200

SKC UMEX SO2/ NO2

PM 500-100

15 min - 8 hrs 0.0151 2 SKC #40108

rev. 1102

IC/COND

NC $69 Samples may be tested for nitrogen dioxide also. Return to

aluminized pouch after sampling and seal for storage and

shipping. Samples are stable at ambient temperature for at

least 3 weeks after sampling.

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Sulfur Dioxide & Particulate

Water Soluble Sulfates

7446-09-5

C-25

MCE/Na-2CO3-treated

filter, 37mm, 4PC

22.5 -200 0.5 - 1.5 7 NIOSH 6004

IC

NC $116 Sulfur trioxide gas, if present in dry atmospheres, may give

a positive interfere. Built-in prefilter may be tested for

water-soluble sulfate/sulfite particulates if needed.

Sulfur Hexafluoride

2551-62-4

Call lab - NIOSH S244

GC/MS

Call for

pricing

WARNING - DO NOT SHIP BY AIR. Samples are


Sulfuric Acid

7664-93-9

C-05

MCEF, 37mm, 0.8um,

3PC

30 - 480 0.5 - 2.0 5 OSHA ID 113

IC

U $69 Recommended method. Transfer filter to V-15 vial within 1

hour of sampling.

T-10-03


226-10-03

30 - 100 0.2 - 0.5 5 NIOSH 7903

IC









T-10-03


226-10-03

TWA 96

STEL 7.5

TWA 0.5 Max

STEL 0.5

5 OSHA ID1655G

IC/COND

U

Talc

Respirable Fraction

(containing no asbestos,

Crystalline silica <1%)

14807-96-6

*C-11 or C-12

*PVC, Preweighed, 37mm,

5um, 2PC

*816 - 1300 *See

comments

100 NIOSH 7500

Mod. XRD

W $98 *Cassette type (2- or 3-piece) and sampling rate is

dependent on cyclone used - SKC Aluminum Cyclone - 2.5

LPM, Nylon Dorr-Oliver Cyclone - 1.7 LPM. Gravimetric

analysis alone may be sufficient for assessment. Any

mineral having similar x-ray diffraction spectra may

interfere.

TAME

994-05-8

$- See t-Amyl Methyl Ether

TCE

79-01-6

$- See Trichloroethylene

TDI, 2,4 & 2,6

584-84-9

$- See Toluene Diisocyanate

Tellurium

13494-80-9

C-05

MCEF, 37mm, 0.8um,

3PC

80 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP

T $40

p-Tert-Butyl Toluene

98-51-1

T-01

Charcoal, 226-01

10 - 30 0.01 - 0.2 20 NIOSH 1501 GC/FID A $56

1,1,2,2-Tetrabromoethane

79-27-6

T-10

Silica Gel, 226-10

50 - 100 0.2 - 1.0 20 NIOSH 2003 GC/FID W $56

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,1,2,2-Tetrachloroethane

79-34-5

M-3500

3M POVM, 3500


GC/FID

A $77 Synonym: Acetylene Trichloride.

M-01

SKC POVM, 575-001

8 Hrs 0.012 40 NIOSH 1019M

GC/FID

A $77

T-81

Anasorb 747, 226-81

3 - 30 0.01-0.2 20 NIOSH 1019

GC/FID

A $77

Tetrachloroethylene

127-18-4

T-01

Charcoal, 226-01

0.2 - 40 0.01 - 0.2 20 NIOSH 1003 GC/FID A $56 Synonyms: Perchloroethylene, Trerachloroethene

M-3500

3M POVM, 3500


GC/FID

A $56

Tetraethyl Lead

(as Pb)

78-00-2

T-16

Charcoal, 226-16

30 - 200 0.01 - 1.0 0.8 Ethyl Corp. Method

ICP/OES

NC $77 Needs prefilter if airborne particulate lead is present;

contact lab for this prefilter. All other volatile lead organic

vapors will interfere.

T-01

Charcoal, 226-01

480 Max 1.0 Max 0.8 OSHA Stopgap

Modified

ICP/OES

NC $77 Needs prefilter (C-06) if airborne particulate lead is present;

contact lab for this prefilter. All other volatile lead organic

vapors will interfere.

1,1,1,2-Tetrafluoroethane

811-97-2

T-01 (2 in series)

Charcoal, 226-01,

2 in series

0.5 - 2.0 0.01 - 0.035 50 NIOSH 1020M

GC/FID

A $77 Cap tubes separately after sampling. ……… ……..

Synonym: Refrigerant 134a.

Tetrahydrofuran (THF)

109-99-9

T-01

Charcoal, 226-01

1 - 9 0.01 - 0.2 10 NIOSH 1609

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Tetramethylsuccino Nitrile

3333-52-6

T-01

Charcoal, 226-01

55 Max 0.05 - 1.0 10 NIOSH S155

GC/FID

A $77 Synonym: TMSN.

TGIC

2451-62-9

$- See Triglycidyl Isocyanurate.

Thallium

7440-28-0

C-05

MCEF, 37mm, 0.8um,

3PC

80 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP

T $40

C-05

MCEF, 37mm, 0.8um,

3PC

80 - 1000 1.0 - 3.0 0.025 NIOSH 7300M

ICP/MS

T $46

Tin

7440-31-5

C-05

MCEF, 37mm, 0.8um,

3PC

20 - 1000 2.0 2 OSHA ID 125

ICP-OES

EE $40

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Tin

Total Organotin Compounds

as Tin

Various

T-30-16

GFF/XAD-2 OVS,

226-30-16

50 - 500 1.5 Max 0.5 NIOSH 5504M

GFAA

NC $237 Store samples cold and ship cold by overnight delivery. The

organotin compound being monitored must be identified

to the laboratory, and a reference standard must be

available for the testing. Additional charges may apply for

procurement of the reference standard, or it may be

necessary for the customer to provide a small portion (1 - 2

grams) of the relatively-pure organotin compound along

with the known purity. A 3-sample-minimum charge

applies for this test. Samples are extracted with an

acidified organic solvent, and the extracts are tested for

dissolved tin, but the testing is not compound-specific. This

method will not work for the most volatile organotin

compounds; see separate entries for methyltin trichloride,

dimethyltin dichloride, and trimethytin chloride by NIOSH

5526.

Titanium

7440-32-6

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0 - 3.0 2 OSHA ID 125

ICP

EE $40

Titanium Dioxide

13463-67-7

C-05

MCEF, 37mm, 0.8um,

3PC

100 - 1000 2 3.3 OSHA ID 125

ICP

EE $40 Analysis is for Total Titanium, with calculated equivalent as

TiO2 reported.

TMSN

3333-52-6

$- See Tetramethyl Succinonitrile

Toluene

108-88-3

T-01

Charcoal, 226-01

2 - 15 0.02 - 0.2 10 NIOSH 1501

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

TWA 0.03-0.2

STEL 0.2

1 Proprietary,

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002


IHGC-P029

GC/FID

A $77

V01 06.2017

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Toluene Diisocyanate,

2,4 & 2,6

584-84-9 & 91-08-7

K-20


Field Desorption

(see description at right).

15 - 240 0.2 - 1.0 0.12 OSHA 42

HPLC/FL



















o-Toluidine

95-53-4

T-10

Silica Gel, 226-10

10 - 150 0.02 - 1 20 NIOSH 2002

GC/FID

M $56

Total Hydrocarbons, as

n-Hexane (VOCs)

N/A

$- See Hydrocarbons, Total as n-Hexane

Total Hydrocarbons, as

n-Hexane, High Resolution

N/A

$- See Hydrocarbons, Total as n-Hexane - High Resolution.

Tribromomethane

75-25-2

$- See Bromoform.

Tributyl phosphate

126-73-8

C-05

MCEF, 37mm, 0.8um,

3PC

90 1.5 2 NIOSH 5034

GC/MS

NC Call for

pricing

Samples subcontracted to outside laboratory.

1,2,4-Trichlorobenzene

120-82-1

K-11

C-45 Cassette + 226-30-04

tube, Tubing Adapter and

15mL Vial

3 - 12 0.01 - 0.2 0.1 NIOSH 5517

GC/ECD

S $102 Transfer filter to vial after sampling; cassette may be

omitted if no aerosols are present. Samples are stable at

least 13 days at ambient temperature.

1,1,1-Trichloroethane

71-55-6

$- See methyl chloroform

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,1,2-Trichloroethane

79-00-5

T-01

Charcoal, 226-01

2 - 10 0.01 - 0.2 10 NIOSH 1003M

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Trichloroethene

79-01-6

$- See trichloroethylene.

Trichloroethylene

79-01-6

T-01

Charcoal, 226-01

1 - 30 0.01 - 0.2 10 NIOSH 1022M

GC/FID

A $56

M-3500

M POVM, 3500


GC/FID

A $56

Trichlorofluoromethane

75-69-4

T-09

Charcoal, 226-09

0.3 - 7 0.01 - 0.05 50 NIOSH 1006

GC/FID

A $77 Ship cold overnight. ………………….. …………. ….

Synonym: Refrigerant 11.

1,1,2-Trichloro-1,2,2-

trifluoroethane

76-13-1

T-01

Charcoal, 226-01

0.1 - 3 0.01 - 0.05 20 NIOSH 1020

GC/FID

A $77

M-3520


1 Hour 0.0291 30 NIOSH 1020M

GC/FID

A $77

Triethanolamine

102-71-6

C-06

GFF, 37mm, 1um, 3PC

120 1 40 OSHA PV2141

GC/FID

NC $77

Triethylamine

121-44-8

T-10-06


226-10-06

TWA 10

STEL 3

0.2 Max 20 OSHA PV2060M

IC

NC $102 Submit for analysis as soon as possible after sampling. If

delay is unavoidable, store cold and ship cold by overnight

delivery.

T-98


226-98

20 Max 0.2 Max 20 OSHA PV2060M

IC



delivery. A minimum volume of 3 Liters is required for STEL

sampling.

Triethylene Glycol

112-27-6

T-57


60 - 200 0.5 - 1.0 20 NIOSH 5523

GC/FID

JJ $77 Also see Glycol Profile.

Triethylenetetramine

112-24-3

T-30-18

NITC-Treated XAD-2,

226-30-18

10 Max 0.1 Max 10 OSHA 60

HPLC/UV



Trifluoroacetic Acid

76-05-1

T-10-03


226-10-03


IC

U $69

1,3,5-Triglycidyl

Isocyanurate

2451-62-9

C-51

GFF, HBr Treated, 37mm,

2PC

60 Max 1 Max 1.5 OSHA PV2055M

HPLC

NC $141 Synonym: 1,3,5-Triglycidyl-s-triazinetrione, TRIG

Triisobutyl Phosphate

126-71-6

T-10-03


226-10-03

60 - 120 0.15 - 0.3 IN-HOUSE

GC/MS

NC Call for

pricing


V01 06.2017

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Triisopropanolamine as

Particulate

122-20-3

C-11


5um, 2PC

TWA 100-480

STEL 60

TWA 1-4

STEL 4

50 NIOSH 0500

Gravimetric


Trimellitic Anhydride

552-30-7

C-28 GFFs (2),

amine-treated, 37mm, 4PC

30 - 480 2 Max 0.5 OSHA 98M

HPLC/UV

NC $116 Sample open-face. Media has 1-month shelf life. Store in

refrigeration and ship as soon as possible after sampling.

1,2,3-Trimethyl Benzene

526-73-8

T-01

Charcoal, 226-01

10 - 30 0.01 - 0.2 10 NIOSH 1501

GC/FID

A $56

M-3500

3M POVM, 3500

Up to 8 hours 15 NIOSH 1501

GC/FID

A $56


95-63-6

T-01

Charcoal, 226-01

10 - 30 0.01 - 0.2 10 NIOSH 1501

GC/FID

A $56 Synonym: Pseudocumene

M-3500

3M POVM, 3500

Up to 8 hours 0.0244 15 NIOSH 1501

GC/FID

A $56


108-67-8

T-01

Charcoal, 226-01

10 - 30 0.01 - 0.2 10 NIOSH 1501

GC/FID

A $56 Synonym: Mesitylene

M-3500

3M POVM, 3500

Up to 8 hours 0.0263 15 NIOSH 1501 GC/FID A $56

2,2,4-Trimethyl Pentane

540-84-1

$- See Isooctane.

Trimethylamine

75-50-3

T-10-06


226-10-06

5 - 10 0.05 - 0.1 4 NIOSH 6016M

IC



delivery.

T-98


226-98

TWA 20 Max

STEL 3.0

TWA 0.05-0.2

STEL 0.2

4 OSHA PV2060

IC



delivery.

Trimethylolpropane

Triacrylate

15625-89-5

T-95

XAD-7, 226-95

10 0.02 3.5 OSHA CSI

HPLC/UV

NC Call for

pricing


2,4,4-Trimethylpentene

25157-70-8

$- See Diisobutylene.

Trimethyltin Chloride

1066-45-1

T-30-16

GFF/XAD-2 OVS,

226-30-16

TWA 15-75

STEL 15 (Max)

TWA 0.25

STEL 1.0

0.1 NIOSH 5526

GC/FPD

NC Call for

pricing


dedicated instrument and there is a 3 sample minimum.

Analysis available for the following agents on one sample:

methyltin dichloride, dimethyltin dichloride, and

trimethyltin chloride. Samples are subcontracted to outside

laboratory.

Triorthocresyl Phosphate

78-30-8

C-05

MCEF, 37mm, 0.8um,

3PC

150 1.5 Max 2 NIOSH S209M

GC/MS

NC $160

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

1,1,1 Tris(hydroxymethyl)

Propane

77-99-6

See Trimethylolpropane Triacrylate.

Tungsten, Total

7440-33-7

C-05

MCEF, 37mm, 0.8um,

3PC

960 Max 2 10 OSHA ID213

ICP-OES

NC $81 Sample can also be tested for cobalt, otherwise sample

other metals separately.

Turpentine

8006-64-2

T-01

Charcoal, 226-01

1 - 10 0.01 - 0.2 100 NIOSH 1551 GC/FID A $77 Measures principle isomers of pinene.

Uranium

7440-61-1

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0 - 3.0 2 NIOSH 7300M

ICP-OES

T $40

Vanadium

7440-62-2

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0 - 3.0 2 NIOSH 7300M

ICP

T $40

C-05

MCEF, 37mm, 0.8um,

3PC

50 - 1000 1.0 - 3.0 0.125 NIOSH 7300M

ICP-MS

T $46

Vanadium Pentoxide

1314-62-1

C-05

MCEF, 37mm, 0.8um,

3PC

300 - 1000 1.7 - 2.0 1.43 NIOSH S388M

ICP

NC $56 Test is for vanadium that is extractable in a weak alkaline

solution, expressed as V205.

Vertrel XF (DuPont Product)

138495-42-8


Vinyl Acetate

108-05-4

M-02

SKC POVM, 575-002

30 min - 8 hours 0.02 2.9 Proprietary,

IHGC-P029

GC/FID

A $77 If samples will not be shipped within 24 hours after

sampling, store samples in a chemical freezer (<0 C) until

shipment. Ship samples refrigerated by overnight delivery.

T-81

Anasorb 747, 226-81

TWA 10

STEL 3 STEL

TWA 0.03-0.2

STEL 0.2

1.6 Proprietary,

IHGC-P029

GC/FID

A $77 If samples will not be shipped within 24 hours after

sampling, store samples in a chemical freezer (<0 C) until

shipment. Ship samples refrigerated by overnight delivery.

O-92

Carboxen 564, ORBO 92

24 0.1 20 OSHA 51

GC/FID

E $56 Samples stable up to 18 days when stored cold.

M-3500

3M POVM, 3500


GC/FID

A $56 Store samples cold, ship cold overnight to expedite

analysis.

Vinyl Chloride

75-01-4

T-01 (2)

Charcoal, 226-01

0.7 - 5.0 0.05 2 NIOSH 1007

GC/FID

A $77 Ship samples refrigerated by overnight delivery. Synonyms:

Chloroethene, Chloroethylene

M-3520


2 hours 0.0408 3 NIOSH 1007M

GC/FID

A $77 Ship samples refrigerated by overnight delivery.

O-91

Carbosieve S-III,Orbo 91

3 0.05 3 OSHA 75

GC/FID

F $77

M-N566


N566


GC/FID

RR $77

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Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

4-Vinyl-1-cyclohexene

100-40-3

T-01

Charcoal, 226-01

10 0.2 Max 1.1 OSHA 07

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

3-Vinyl Pyridine $- See 3-Ethenyl Pyridine.

n-Vinyl 2-Pyrrolidone (NVP)

88-12-0

T-01

Charcoal, 226-01

12 0.1 20 NIOSH 1302M

GC/FID

E $56

Vinyl Toluene

25013-15-4

T-01

Charcoal, 226-01

10 - 24 0.01 - 0.2 100 NIOSH 1501

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

Vinylidene Chloride

75-35-4

$- See 1,1-Dichloroethylene.

VM & P Naphtha

8032-32-4

$- See Naphtha, VM&P.

Volatile Organic

Compounds N/A

$- See Hydrocarbons, Total as n-Hexane.

Welding Fume Particulates

N/A

C-04


Matched-weight

200 - 1000 1 - 3 100 NIOSH 0500

Gravimetric

$21 Matched weight filter allows for metals analysis.

Welding Fumes Profile

Air

N/A

C-04


Matched-weight

200 Liters, 480 Liters needed

to allow detection of

Cadmium at OSHA action

level

1.0 - 2.0 Varies by

element

OSHA ID-125

ICP

EE $196 Profile includes Aluminum, Antimony, Beryllium, Cadmium,

Chromium, Cobalt, Copper, Iron, Lead, Manganese,

Molybdenum, Nickel, Titanium, Vanadium, Zinc & Total

Particulates.


Bulk

N/A

Vial or Bag NA NA Varies by

element

OSHA ID-125

ICP



Molybdenum, Nickel, Titanium, Vanadium, Zinc


Wipe

N/A

K-07

Ghost Wipe Kit

100 sq cm NA Varies by

element

OSHA ID-125

ICP



Molybdenum, Nickel, Titanium, Vanadium, Zinc. Use

“Ghost” wipe.

Wood Dust

N/A

C-11


5um, 2PC

100 - 500 1.5 - 2.0 50 NIOSH 0500

Gravimetric

$21 Includes total airborne particulates. No speciation possible

as to wood dust type.

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ccatlyn

Line


Suggested


samplers) Volume, L

Sampling

Rate, LPM

Reporting

Limit (µg)

Method

Technique

Lab

Code

Unit Cost

USDGeneral Comment

Xylene

all isomers

1330-20-7

T-01

Charcoal, 226-01

2 - 30 0.02 - 0.2 5 NIOSH 1501

GC/FID

A $56

M-3500

3M POVM, 3500


GC/FID

A $56

T-81

Anasorb 747, 226-81

TWA 10

STEL 3

0.03-0.2 3 Proprietary

IHGC-P029

GC/FID

A $77

M-02

SKC POVM, 575-002

TWA 8 hr (Max)

STEL 15 min

0.014 6 Proprietary

IHGC-P029

GC/FID

A $77 Samples are subcontracted to outside laboratory.

m-Xylenediamine

1477-55-0

C-15


37mm, 3PC

TWA 100

STEL 15

TWA 1.0

STEL 1.0

0.2 OSHA Method

105M

HPLC/UV

NC $116

Xylidine (Mixed Isomers)

1300-73-8 also 95-68-1

T-10

Silica Gel, 226-10

TWA 96

STEL 7.5

TWA 0.2

STEL 0.5

12 NIOSH 2002

GC/FID

NC Call for

pricing


2,4-Xylidine

1300-73-8

T-10

Silica Gel, 226-10

TWA 96

STEL 7.5

TWA 0.2

STEL 0.5

12 NIOSH 2002

GC/FID

NC Call for

pricing


2,5-Xylidine

95-78-3

T-10

Silica Gel, 226-10

TWA 96

STEL 7.5

TWA 0.2

STEL 0.5

12 NIOSH 2002

GC/FID

NC Call for

pricing


Zinc and Zinc Compounds

7440-66-6

C-05


20 - 1000 1.0 - 3.0 2 NIOSH 7300

ICP

T $40 Other forms of zinc including metallic zinc and zinc salts can

interfere. Total Zinc as ZnO.

Zinc Oxide

1314-13-2

C-05


20 - 1000 1.0 - 3.0 2.6 NIOSH 7300

ICP

T $40 Same species of zirconium may not be solubilized by this

procedure.

Zirconium

7440-67-7

C-05


20 - 1000 1.5 2 NIOSH 7300

ICP

T $40

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2.3 Profiles

Profile Analytes Media VolumeSampling

RateMethod Technique Price

Acrylate Monomer Profile Anasorb 747

Tube (226-81)

3 - 12 Liters 0.02 - 0.2

LPM

Proprietary

IH- GC-P029

GC/FID $116

SKC 575-002 PM 8 hours Max Various

3M POVM 3500 8 hours Max Various

Aldehyde Profile Acetaldehyde, Acrolein, Butyraldehyde, Formaldehyde,

Glutaraldehyde, Isovaleraldehyde

DNPH Tube,

226-119

16 - 30 Liters 0.2 - 1.0

LPM

EPA TO- 11 HPLC/UV $254

UMEX-100 Up to 8 hours - - EPA TO- 11M HPLC/UV $254

Aromatic Hydrocarbon Profile Benzene, Chlorobenzene, Cumene,

o-Dichlorobenzene, p-Dichlorobenzene, Ethyl Benzene,

alpha-Methyl Styrene, Naphthalene, para-tert-Butyl

Toluene, Styrene, Toluene, Vinyl Toluene, Xylene

Charcoal Tube,

T-01, 226-01

10 Liters 0.1 - 0.5

LPM

NIOSH 1501 GC/FID $150

3M 3500/3520,

SKC 575-001

8 hours Max Various NIOSH 1501M GC/FID $150

BTEX Profile Benzene, Ethyl Benzene, Toluene, Xylene,

Total Hydrocarbons as Hexane

Charcoal Tube,

T-01, 226-01

5 - 15 Liters 0.05 - 0.2

LPM

NIOSH 1501 GC/FID $127

3M 3500/3520,

SKC 575-001,

Assay N521

8 hours Max Various NIOSH 1501M GC/FID $127

Chlorinated Pesticide Profile Aldrin, alpha-BHC, beta-BHC, gamma-BHC (Lindane), alpha-

Chlordane, gamma-Chlordane, 4,4-DDD, 4,4- DDE, 4,4-DDT,

Dieldrin, Endosulfan I, Endosulfan II, Endosulfan Sulfate,

Endrin, Heptachlor, Heptachlor Epoxide, Methoxychlor

OVS 226-30-16 or

ORBO 49P

60 - 1000 Liters 1 LPM OSHA 67M GC/ECD $416

Diisocyanate Profile HDI, MDI, 2,4-TDI, 2,6-TDI, IPDI Coated GFF (2 PP) 15 - 240 Liters 0.2 - 1.0

LPM

OSHA

Methods

42 & 47

HPLC/FL $226

Analytics was a pioneer with the concept of IH profiles to better offer our clients an affordable approach to large scale IH testing. Our profiles include organics (29 solvents), PAHs (16 analytes),

welding fumes (15 metals plus particulates), crystalline silica (3 most common), and customized profiles to meet your specific testing requirements. Analytics can also customize a profile to

meet your specific requirements while at the same time, saving you money. Please do not hesitate to contact Analytics about setting up your customized profile.

Preferred active sampling method. For STEL sampling, collect a 15-minute sample at 1 LPM. Ozone may interfere - use ozone scrubber in known ozone contaminated areas. Any ketone or aldehyde will react

with the DNPH and is a potential interference. Large concentrations of acetone or MEK will compete with the aldehyde and are therefore potential negative interferences. Refrigerate before and after sampling

and ship overnight. Media contains residual acetonitrile which could interfere with acetonitrile monitoring.

Methyl Acrylate, n-Butyl Acrylate, N-Butyl Methacrylate,

Ethyl Acrylate, Methyl Methacrylate

Sample open faced. Refrigerate media before and after sampling. Ship samples cold by overnight delivery. Testing is for both 2,4- and 2,6-TDI isomers. Media is marked with expiration date,

and will ship with at least 1-month shelf life (stored cold). See comments that follow regarding field desorption of samples.

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Glycol Profile Butylene Glycol, Diethylene Glycol, Propylene Glycol,

Triethylene Glycol, Ethylene Glycol

OVS tube SKC

226-57

5 – 60 Liters 0.5 – 2.0

LPM

NIOSH 5523 GC $116

Inorganic Acid Profile Hydrobromic Acid, Hydrochloric Acid, Hydrofluoric Acid,

Nitric Acid, Phosphoric Acid, Sulfuric Acid

SKC 226-10-03 100 Liters 0.3 LPM

Max

NIOSH 7903 IC $208

K-08, Whatman

Smear Tab kit

100 cm2 or 1 ft2 - - NIOSH 7903M IC $208

Non-Viable Airborne

Particulate Profile

Non-Viable Fungal Spore Count plus ID of:

Glass Fibers, Cellulosic Fibers, Insect parts, Pollen, Animal

Hair, Fly Ash, Quartz/Sand, Synthetic Fibers, Asbestos,

Calcite, Plant Fibers, Other Fibers/Particles

Zefon Sampling

Cassette

(Air-O- Cell

cassette)

150 Liters 15 LPM Call for Pricing

Organic Solvent Profile Acetone, Benzene, Butyl Acetate, Chlorobenzene,

Cyclohexanone, Decane, 1,2-Dichloroethane, 1,4-Dioxane,

Ethyl Acetate, Ethyl Benzene, Heptane, Hexane, Isooctane,

Methyl Ethyl Ketone, Methyl Isobutyl Ketone, Methylene

Chloride, m-Xylene, n-Propyl Acetate, Octane, Pentane,

Perchloroethylene, Styrene, Tetrahydrofuran, THC as

Hexane, Toluene, 1,1,1-Trichloroethane, Trichloroethylene,

1,2,4-Trimethylbenzene, o-Xylene, p-Xylene

Charcoal Tube,

T-01, 226-01

3 – 10 Liters 0.02 - 0.1

LPM

OSHA 7M GC/FID $196

3M 3500/3520,

SKC 575-001

8 hours Max

(sampler capacity

may be exceeded

for more volatile

compounds in

higher

concentration

atmospheres)

Various NIOSH 1501M GC/FID $196

Store samples cold, and ship samples cold overnight.

NIOSH now describes NIOSH Method 7903 as a “historical” method and does not recommend its use, advocating instead for a series of filter methods which provide improved sensitivity and

the opportunity for size-selective sampling of aerosols. NIOSH’s intention is not to invalidate results developed using NIOSH 7903 in the past, but to instead transition users to the newer filter

methods.

For optimum results keep samples cold and ship cold by overnight delivery (for ketone compounds).

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Hydrocarbons

Acenaphthene, Acenaphthylene, Anthracene, Benzo(k)

fluoranthene, Benzo(g,h,i)perylene, Benzo(a)pyrene,

Benz(a)anthracene, Benzo(b)fluoranthene, Chrysene,

Dibenz(a,h)anthracene, Fluoranthene, Fluorene,

Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene,

Pyrene

PTFE Filter and

Orbo 43 or XAD-2

200 - 1000 Liters 2.0 LPM NIOSH 5506 HPLC/UV

& FL

$284

Selected Polynuclear

Aromatic Hydrocarbons

Anthracene, Benzo(a)pyrene, Chrysene, Phenanthrene,

Pyrene

GFF 960 Liters 2.0 LPM OSHA 58 HPLC/UV

& FL

$226

Solder Operations Profile Antimony, Beryllium, Cadmium, Copper, Lead, Silver, Tin,

Zinc Oxide

0.8µ MCEF 480 Liters,

960 if silver is

determined at TLV

1.0-2.0

LPM

OSHA ID-206 ICP $127

Toxic Metal Profile Arsenic, Beryllium, Cadmium, Chromium, Lead, Vanadium 0.8µ 37mm MCEF 400 Liters 1.0 – 3.0

LPM

NIOSH 7300M ICP $127

Welding Fume Metals Profile

– Air

Aluminum, Antimony, Beryllium, Cadmium, Chromium,

Cobalt, Copper, Iron, Lead, Manganese, Molybdenum,

Nickel, Titanium, Vanadium, Zinc and Total Particulates.

0.8µm MCEF,

C-04 (includes

gravimetric

analysis) or C-05

(no gravimetric

analysis)

200 Liters, 480

Liters needed to

allow detection of

Cadmium at OSHA

action level

1.0-2.0

LPM

OSHA ID- 125G ICP $196


– Bulk



Nickel, Titanium, Vanadium, Zinc

Approximately 2

grams into a

plastic vial or bag

N/A N/A OSHA ID- 125G ICP $226


– Wipe



Nickel, Titanium, Vanadium, Zinc

“Ghost” wipe. Place

into a glass or

plastic vial after

sampling.

100 cm2 or 1 ft2 N/A OSHA ID- 125G ICP $226

Transfer filters to glass vials after sampling and wrap with aluminum foil to protect from light. Ship samples by overnight delivery.

Transfer filter to glass vial immediately after sampling, and wrap the vial and tube with aluminum foil to protect from light. Ship samples cold for overnight delivery. Profile includes

Acenaphthene, Acenaphthylene, Anthracene, Benzo(k)fluoranthene, Benzo(g,h,i)perylene, Benzo(a)pyrene, Benz(a)anthracene, Benzo(b)fluoranthene, Chrysene, Dibenz(a,h)anthracene,

Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene.

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2.4 Media Table

Part Number Media DescriptionUnit of

Measure

CASSETTES

C-01 MCEF, 25mm, 0.8um, 3PC, long cowl, C-01 EACH

C-02 MCEF, 25mm, 0.45um, 3PC, long cowl, C-02 EACH

C-03 MCEF, 37mm, 0.45um, 3PC, C-03 EACH

C-04 MCEF, 37mm, 0.8um, 3PC, Matched- weight, C-04 EACH


C-06 GFF, 37mm, 1um, 3PC, C-06 EACH

C-07 GFF, 13mm, 1um, 2PC Swinnex, C-07 EACH

C-08 PTFE, 37mm, 2um, 3PC, C-08 EACH

C-09 PTFE, Preweighed, 37mm, 2um, 2PC, Serialized, C-09 EACH

C-10 PVC, 37mm, 5um, 3PC, C-10 EACH

C-11 PVC, Preweighed, 37mm, 5um, 2PC, Serialized, C-11 EACH


C-13 MCE/Treated Backup, 37mm, 3PC, C-13 EACH

C-14 GFF, 2PP-treated, 37mm, 3PC, C-14 EACH

C-15 GFFs (2), H2SO4-treated, 37mm, 3PC, C-15 EACH

C-16 Ag/PTFE, Cl2 / Br2 Sampler, 25mm, 3PC, C-16 EACH

C-18 MCEF/Treated Backup, 37mm, 3PC, C-18 EACH

C-19 PTFE, Preweighed, 25mm, 0.5um, C-19 EACH

C-20 GFFs(2), DNPH-treated, 37mm, 4PC, C-20 Box of 10

C-21 PTFE, 25mm, 0.45um, 2PC, C-21 EACH

C-22 GFFs (2), nitrite-treated, 37mm, 2PC, C-22 Box of 10

C-23 Air-O-Cell Cassette, C-23 EACH

C-25 MCE/Na2CO3-treated filter, 37mm, 4PC, C-25 EACH



C-28 GFFs (2), amine-treated, 37mm, 4PC, C-28 EACH

C-29 PTFE, 25mm, 0.5um, 3PC long cowl, PPBU, C-29 EACH

C-30 PVC, Preweighed, 5um, 47mm, (Anaslide), Serialized, C-30 EACH

C-31 IOM Cassette, plastic, SKC PN 225-71A EACH

C-32 IOM Wash&Load, PVC, 5um, 25mm EACH

C-33 IOM Wash&Load, MCE, 0.8um, 25mm EACH

In many cases for general analysis, our sample media can be provided at no additional cost. Call the lab for

pricing information.

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Measure

CASSETTES

C-35 IOM Sampler & Cassette, SKC PN 225-70A EACH

C-39 PTFE, Preweighed, 2um, 37mm (Anaslide), Serialized, C-39 EACH

C-40 PEM Sampler PTFE, Preweighed, 2um(A- naslide), Serialized, C-

40

EACH

C-41 PVC, 25mm, 5um, 2PC, C-41 EACH

C-42 PVC, prewashed 37mm, 5um, 2PC, C-42 EACH

C-43 Quartz, NaOH-treated, 37mm, 2PC, C-43 EACH

C-44 GFF Type A/B, 37mm, 1um, 3PC, C-44 EACH

C-45 PTFE 13mm Swinnex, 0.5um, C-45 EACH

C-46 PTFE, 37mm, 2um + support spacer, 2PC, C-46 EACH

C-47 Quartz, heat-treated, 37mm, 3PC, SKC PN 225-401 EACH

C-48 GFF, Hg Acetate-Treated, 37mm, 2PC, SKC PN 225-9007 or

equiv.(provided by subcontract lab)

EACH

C-49 GFF (2 in series), 2PP-treated, 37mm, 4PC, C-49 EACH

C-50 MCEF Prefilter, 37mm, 0.8um, 2PC, PPBU EACH

C-51 GFF, HBr Treated, 37mm, 2PC, C-51 EACH

C-52 IOM Cassette Preweight, PVC, 5um, 25mm EACH

C-53 PVC, 37mm, 5um, Quartz support, 2PC, C-53 EACH

C-54 PVC,Preweighed,5um, 25mm, in Anaslide filter holder,

Serialized, C-54

EACH

C-55 GFF, Sulfur-treated (ST-GFF), 37mm, 2PC, C-54 EACH

C-56 GFFs(2), 37mm, 4PC, C-56 EACH

C-57 PRE-RINSED 37mm GFF EACH

C-58 IOM WASH & LOAD W/GFF EACH

C-59 PTFE,1um,25mm,2PC conductive goblet, [SKC 225-1725] EACH

C-61 PVC,5um,37mm,Preweighed,over 0.8um MCE filter,2-PC, C-61 EACH

C-62 PTFE,2um,25mm,3PC conductive goblet,[SKC MRK-005]

MERCK-ONLY PART

EACH

C-63 PVC ACCU-CAP,Preweighed,5.0um, 37mm,2PC,Serialized, C-63 EACH

C-64 GFFs (2), veratrylamine-treated, 25mm in IOM, C-64 Each

C-65 PTFE, Pre-weighed, 47mm, 2um, PMP support ring, in Anaslide,

Serialized, C-65

Each

C-66 PTFE, 1um, 37mm, 2PC, C-66 Each

C-9018 GFF/ HgCl2-treated Polyester, 37mm, 3PC,

SKC PN 225-9018

Box of 10

C-MCE-NN MCE, Low Metals, 37mm, 0.8um, 2PC, C-MCE-NN EACH

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Measure

CASSETTES

X-12 Hi-Vol GFF, 8”x10”, 1um EACH

X-13 Hi-Vol GFF, Preweighed, 8”x10”, 1um, Serialized EACH

IMPINGER SOLUTIONS

IMP-01 Impinger, 0.1N KOH MLS

IMP-02 Impinger, 1% Sodium Bisulfite MLS

IMP-03 Isocyanate Train, MAMA Impinger/Filter SET

IMP-04 Impinger, 0.02% KI in NaHCO3/Na2CO3 MLS

IMP-05 Impinger, 0.01N NaOH MLS

IMP-06 MFGB, 0.1N KOH MLS

IMP-07 MFGB, Methanol MLS

IMP-08 Impinger, 0.1N NH4F MLS

IMP-09 Impinger, NaHCO3/Na2CO3 MLS

IMP-10 Impinger, Isopropanol MLS

IMP-11 Impinger, DI Water MLS

IMP-12 MFGB, 15 mL 0.1N KOH + 5um PVC prefilter cassette + vial SET

IMP-13 Impinger, TiOSO4 reagent MLS

IMP-14 MFGB, DI Water MLS

IMP-15 MFGB, 0.01N KOH MLS

IMP-16 MFGB, Isopropanol MLS

BOTTLES/VIALS

1OZUP 1 oz Nalgene, Unpreserved EACH

15UG 15ml Clear Glass Unpreserved EACH

40UG 40ml Clear Glass Unpreserved EACH

V-02 2 mL glass vial, teflon-lined cap, Unpreserved EACH




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SAMPLING KITS, AIR &

WIPES & BAGS

– IH

K-01 Dialysis water sampling kit

K-02 Swinnex GFF+ 226-39 SET

K-03 LAL water sampling kit EACH

K-04 Low SO4 Charcoal, Orbo 34 (LG) SET

K-05 KOH-treated Anasorb 747, 226-80 + PTFE Pre-filter EACH

K-06 PTFE + ORBO 43 EACH

K-07 Ghost Wipe Kit EACH

K-08 Whatman SmearTab Kit EACH

K-09 Impinger, 0.1N KOH EACH

K-10 Swinnex GFF + 226-10 EACH

K-11 Swinnex PTFE + 226-30-04 EACH

K-12 Methanol-moistened cotton-fabric swab EACH

K-13 C-15 (H2SO4 Treated GFF) plus 2 vials with 2 ml DI water for

field transfer.

EACH

K-19 Texwipe 714A swabs(2)+16mL plastic screw-cap tube EACH

K-20 OSHA Isocyanate Kit, Field Desorption Each

X-01 Paper filter, 7cm EACH

X-10 1L Tedlar Bag EACH

X-11 Ghost Wipe Only EACH

X-19 1L Foil bag EACH

X-20 5L Tedlar Bag EACH

X-PCB Paper filter, 7cm, hexane-wetted EACH

DIFFUSIVE SAMPLERS –

BADGES

M-01 SKC POVM, 575-001 EACH

M-02 SKC POVM, 575-002 EACH

M-03 SKC Mercury PM, SKC PN 520-02A EACH

M-03-A SKC Mercury PM Holder for 520-02A EACH

M-04 SKC Formaldehyde PEL PM, 526-200 EACH

M-05 SKC Formaldehyde STEL PM, 526-201 EACH

M-06 SKC Ethylene Oxide PM, 575-005 EACH

M-3500 3M POVM 3500 EACH

M-3500-C 3M POVM 3500, Case of 50 CASE of 50

M-3520 3M POVM 3520, 2-stage EACH

M-3520-C 3M POVM 3520, 2-stage, Case of 50 CASE of 50

M-3721 3M Formaldehyde PM 3721 EACH

M-3721-C 3M Formaldehyde PM 3721, Case of 5 CASE of 5

M-N521 Assay N521 TraceAir POVM EACH

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DIFFUSIVE SAMPLERS –

BADGES

M-ATN571 Assay Aldehyde PM ATN571 EACH

M-N584 Assay Ammonia PM ATN584 EACH

M-N586 Assay Ozone PM N586, Case CASE of 10

UMEX-100 SKC UMEX Aldehyde PM 500-100 EACH

UMEX-200 SKC UMEX SO2&NO2 PM 500-200 EACH

UMEX-400 SKC UMEX Amine PM 500-400 EACH

TUBES – IH

O-23 Supelpak 20N, ORBO 23 EACH

O-24 Supelpak 20N, ORBO 24 EACH

O-34 Low Sulfate charcoal, ORBO 34 EACH

O-43 Supelpak 20U, ORBO 43 EACH

O-44 Supelpak 20E, ORBO 44 EACH

O-49 Supelpak 20P, ORBO 49P EACH

O-53 Specially-cleaned silica gel, ORBO 53 EACH

O-90 Carbonxen 564, ORBO 90 EACH

O-91 Carbosieve S-III,Orbo 91 EACH

O-92 Carbonxen 564, ORBO 92 EACH

O-304 Low-Nickel charcoal, ORBO 304 EACH

O-306 Petroleum Charcoal, ORBO 306 EACH

O-202580 Specially Cleaned XAD-2, O-202580 EACH

T-00-IAQ Thermal Desorption Tube, Multi-bed EACH

T-01 Charcoal, 226-01 EACH


T-10 Silica Gel, 226-10 EACH

T-10-03 Prewashed Silica Gel, 226-10-03 EACH

T-10-04 Silica Gel, 226-10-04 EACH

T-10-06 H2SO4-Treated Silica Gel, 226-10-06 EACH

T-15 Silica Gel, 226-15 EACH


T-17-1A Anasorb C300, 226-17-1A EACH

T-28 Soda Lime, 226-28 EACH

T-29 Anasorb 747, 226-29 EACH

T-30 XAD-2 Tube, 226-30 EACH

T-30-04 XAD-2, 226-30-04 EACH

T-30-06 XAD-2, 226-30-06 EACH

T-30-07 XAD-2, 226-30-07 EACH

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Measure

TUBES – IH

T-30-08 Anasorb 708, 226-30-08 EACH

T-30-16 GFF/XAD-2 OVS, 226-30-16 EACH

T-30-18 NITC-Treated XAD-2, 226-30-18 EACH

T-35-01 Tenax, 226-35-01 EACH

T-35-03 Tenax, 226-35-03 EACH

T-39 Florisil, 226-39 EACH

T-40 TEA-treated Molecular Seive(2 tubes), with Oxidizer tube, 226-

40

EACH

T-40-02 TEA-treated Molecular Seive, 226-40-02 EACH

T-42-02 H2SO4-treated Firebrick, 226-42-02 EACH

T-44 Drying Tube, 226-44 EACH

T-47-01 Silica Gel, 226-47-01 EACH

T-49-108 Chromosorb 108, 226-49-108 EACH

T-54 HMP-treated XAD-2, 226-54 EACH

T-56 GFF/Tenax OVS, 226-56 EACH

T-57 GFF/XAD-7 OVS, 226-57 EACH

T-58 GFF/XAD-2 OVS, 226-58 EACH

T-59-04 Porapak R, 226-59-04 EACH

T-67 KOH-treated Charcoal, 226-67 EACH

T-73 TBC-Treated charcoal, 226-73 EACH

T-80 KOH-treated Anasorb 747, 226-80 EACH

T-81 Anasorb 747, 226-81A EACH

T-82 Anasorb 747, 226-82, (2 in series) EACH

T-83 Anasorb 747, 226-83 EACH

T-89 TCP-treated XAD-4, 226-89 EACH

T-93 XAD-4, 226-93 EACH

T-94 XAD-7, 226-94 EACH

T-95 XAD-7, 226-95 EACH

T-96 NBD-chloride-treated XAD-7, 226-96 EACH

T-97 XAD-7 (3 Tubes, PCP Sampler), 226-97 EACH

T-98 H3PO4-treated XAD-7, 226-98 EACH

T-99 GFF/Silica Gel OVS, 226-99 EACH

T-107 Chromosorb 102, 226-107 EACH

T-110 Chromosorb 106, 226-110 EACH

T-111 Chromosorb 106, 226-111 SET

T-114 Porapak-P, 226-114 EACH

T-115 Porapak-Q, 226-115 EACH

T-116 Porapak-T, 226-116 EACH

T-117 HMP XAD-2, 226-117 EACH

T-119 DNPH-Treated Silica Gel, 226-119 EACH

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Measure

TUBES – IH

T-120 DNPH-Treated Silica Gel, 226-120, with ozone scrubber EACH

T-121 Anasorb CMS, 226-121 EACH

T-142 KOH-treated carbon beads, OVS-type with PTFE

pre-filter, 226-142

EACH

T-151 Oxidizer-Treated Charcoal, 226-151 EACH

T-153 Amine-treated XAD-2, 226-153 EACH

T-177 Silvered Silica Gel, 226-177 EACH

T-178 HBR-treated Anasorb 747, 226-178 PAIR

T-183 Silica Gel+GFF,washed/baked,226-183, 2 in series EACH

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V02-25-13 Page 1 800-888-8061

III. Pharmaceutical Testing ServicesAnalytics works with pharmaceutical companies to first develop and then routinely monitor personal exposure and equipment clearance testing. These proprietary methods are developed by Analytics using similar OSHA/NIOSH methods and then adapting these existing methods to the unique nature of the active ingredients required for your company. The entire process is made simple by Analytics’ R&D Staff and only requires minimum input by your company to establish the Occupational Exposure Limit (OEL) and to provide a small portion of the active ingredient required for analysis. The protocol we develop can be used to analyze air exposure samples, as well as samples for wipe clearance and bulk material testing. Analytics also provides containment testing of your entire production process based on the analysis of surrogates such as lactose, naproxen, acetaminophen, and mannitol. Analytics currently has over 200 proprietary and over-the-counter active pharmaceutical ingredients (API) that we analyze routinely.

Compound Media ng/ Sample

Method

5-Fluorouracil J 10 HPLC-UV Acetaminophen E, J 1000 HPLC-UV Acetylsalicylic acid E, J 2000 HPLC-UV Aciclovir E, J 9000 HPLC-UV Acitretin J 50 HPLC-UV Actinomycin D Wipe 100 HPLC-UV Amitriptylene E, J, A 100 HPLC-UV Amoxicillin E, J 100 HPLC-UV Amphotericin B J 400 HPLC-UV Anagrelide Hydrochloride N 70 HPLC-UV Atracurium besylate E, J 600 HPLC-UV Atropine Sulfate H 125 HPLC-UV Azothioprine I/Wipe 100/1000 HPLC-UV Bendamustine H/Wipe 100/1000 HPLC-UV Benzoate A 10 HPLC-UV Bromocriptine mesylate E 500 HPLC-UV Bupropion HCl E, J 400 HPLC-UV Butalbital E 2000 HPLC-UV Butoconazole Nitrate A 500 HPLC-UV Capsaicin J 20 HPLC-UV Capecitabine E, J 100 HPLC-UV Cefaclor Wipe 200 HPLC-UV Cefamandole Nafate Wipe 100 HPLC-UV Cefazolin Sodium Wipe 100 HPLC-UV Ceftazidime Wipe 100 HPLC-UV Ceftriaxone sodium N/A N/A HPLC-UV Cefuroxime Axetil Wipe 100 HPLC-UV Cefuroxime Sodium Wipe 200 HPLC-UV Cephalexin Wipe 100 HPLC-UV Cephalothin Wipe 300 HPLC-UV Chlordiazepoxide E, J 40 HPLC-UV Chlormadinone Acetate A 50 HPLC-UV Chlorohydrine A 1000 HPLC-UV Clenbuterol E, J 20 HPLC-UV Clidinium bromide E, J 2000 HPLC-UV Clobetasol propionate E, J 100 HPLC-UV Clonazepam E, J 200 HPLC-UV Clozapine base E 780 HPLC-UV Cyclophosphamide E, J, A 8000 HPLC-UV Cyclosporin A E 500 HPLC-UV


Method

Darifenacin F 125 HPLC-UV Desogestrel E 20 HPLC-UV Diatrizoic Acid E 156 HPLC-UV Digoxin N/Wipe 150 HPLC-UV Dihydrocapsaicin J 20 HPLC-UV Doxifl Uridine J 25 HPLC-UV Doxycline Hyclate F 500 HPLC-UV Ethinyl Estradiol E/Wipe 10/60 HPLC-FL Etretinate K 50 HPLC-UV Floxuridine J 50 HPLC-UV Flucytosine J 40 HPLC-UV Fludrocortisone Acetate H 10 HPLC-UV Flumethasone A 10 HPLC-UV Fluocinolone Acetonide A 20 HPLC-UV Fluocinonide A 20 HPLC-UV Fluorescein L 625 OD Fluorouracil (5-) E, J 100 HPLC-UV Flurazepam E, J 200 HPLC-UV Fluticasone Propionate E, J 2000 HPLC-UV Ganciclovir Sodium A 100 HPLC-UV Hydrazoic Acid M 50 (300) HPLC-UV Hydrocodone J 200 HPLC-UV Hydrocodone Bitartrate J 200 HPLC-UV Insulin F 2000 HPLC-UV Isotretinoin J 100 HPLC-UV Ketorolac Tromethamine A 100 HPLC-UV Labetalol E, J 1000 HPLC-UV Lactose A/ Wipe 2 IC Laidlomycin A 400 HPLC-UV Laidlomycin Propionate A 400 HPLC-UV Lamivudine E, J 1000 HPLC-UV Lansoprazole E 30 HPLC-UV Lasalocid E, J 800 HPLC-UV Levonorgestrel E 10 HPLC-UV Mannitol A/Wipe 1 IC Mestranol E, J 80 HPLC-UV Methamphetamine E, J 200 HPLC-UV Methylphenidate E, J 200 HPLC-UV Methylphenidate (dex-) E, J 200 HPLC-UV Mivacurium HCl E, J 800 HPLC-UV

118

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Method

Morphine Sulfate E, J 100 HPLC-UV Mycophenolate Mofetil A 200 HPLC-UV Nadolol E, J 10 HPLC-UV Naproxen A 2 HPLC-FL Naproxen Sodium A/Wipe 2 HPLC-FL Nicardipine Hydrochloride A 1000 HPLC-UV Norethindrone A 10 HPLC-UV Norethindrone Acetate E/Wipe 30 HPLC-UV Norgestimate E 10 HPLC-UV Orlistat B 1000 HPLC-UV Oseltamivir E, J 100 HPLC-UV Oxfendazole A 1000 HPLC-UV Oxytetracycline F 2500 HPLC-UV Pergolide Mesylate E 8.5 HPLC-FL Pilocarpine HCl E 600 HPLC-UV Prasterone (DHEA, dehydroepiandrosterone)

E 100 HPLC-UV

Procainamide HCl E, J 100 HPLC-UV Procarbazine Hydrochloride

J 100 HPLC-UV

Progesterone A 10 HPLC-UV Pyridostigmine Bromide E, J 200 HPLC-UV Ramoxifen Citrate G 200 HPLC-UV Ranitidine HCl J 400 HPLC-UV Ranolazine Free Base A 500 HPLC-UV Ranolazine Hydrochloride A 500 HPLC-UV Retinol O 100 HPLC-UV Ribavirin H 30 HPLC-UV Rifaximin E 17,000 HPLC-UV Salinomycin Sodium J 500 HPLC-UV Sertindole E 200 HPLC-UV Sumatriptan Succinate E, J 1000 HPLC-UV Temazepam E 500 HPLC-UV Testosterone Propionate A 10 HPLC-UV Tezacytabine (FMdC) J 20 HPLC-UV Thalidomide C 30 HPLC-UV Ticlopidine Hydrochloride A 200 HPLC-UV Tobramycin E 2000 HPLC-UV Tolcapone B 5000 HPLC-UV Trenbolone Acetate A 5 HPLC-UV Tretinoin, Vesanoid J 50 HPLC-UV Triamcinolone K 50 HPLC-UV Valaciclovir J 3000 HPLC-UV Verapamil J 200 HPLC-UV Vitamin D3 D 120 HPLC-UV Warfarin E 50 HPLC-UV Zalcitabine A 100 HPLC-UV Zidovudine E, J 3000 HPLC-UV Zopiclone E 38 HPLC-UV

Media Codes:

A - 37 mm glass filter type A/E (1μm) and pad in polystyrene cassette B - 37 mm quartz filter (1μm) and pad in polystyrene cassette C - Two 37 mm quartz filters (1μm) in polystyrene cassette D - 37 mm Teflon filter (1μm) and pad in polycarbonate cassette E - 37 mm Teflon filter (1μm) and pad in polypropylene cassette F - 37 mm Teflon filter (1μm) and pad in 3-piece polypropylene cassette G - 37 mm Teflon filter (1μm) and glass fi lter type A/E as support pad in polypropylene cassette H - 25 mm Teflon filter (1μm) and pad in polypropylene cassette I - 37 mm Teflon filter (0.45μm) and pad in polypropylene cassette J - 37 mm Teflon filter (1μm) and pad in polystyrene cassette K - 37 mm Teflon filter (0.5μm) and pad in polystyrene cassette L - Two 37 mm quartz filters (1μm) in polypropylene cassette N - Two 37 mm glass filter type A/E (1μm) in polystyrene cassette O - 25 mm impregnated Teflon filter (1μm) in IOM cassette

119

IV. Environmental Services and Fees

1. IntroductionWith more than twenty years of laboratory experience, Analytics continues its tradition of excellence in analytical services. By combining scientific expertise, state of the art instrumentation and leading edge information management systems, Analytics is committed to delivering to our clients the highest quality analytical laboratory service and data. From sample receipt to results delivery, remaining responsive to client needs is the center of our focus.

2. Standard Turnaround TimeAnalytics standard turnaround time for most environmental analyses is 5 business days from sample receipt in the laboratory. Emailed, faxed or verbal results are available by the close of business on the due date. A hard copy of the report will follow by mail.

3. Billing and Rush MultipliersClients may request monthly billing or individual invoices by sample group. Billing by sample group is assumed unless otherwise requested. Billing terms are payable upon receipt. Acceptable forms of payment include check, money order, wire transfer, VisaTM, MasterCardTM, DiscoverTM or American ExpressTM.

Samples requiring rush turnaround time must be scheduled prior to sample submission. The following charges will apply:

3 Day Turnaround Time 1.5 x price 2 Day Turnaround Time 1.75 x price 1 Day Turnaround Time 2.00 x price Same Day Turnaround Time 3.00 x price Weekend Analysis 3.00 x price + $300 Holiday Analysis 3.00 x price + $300

4. Deliverable MultipliersUnit prices are for a Level 1 data package. Analytics can provide Level 2, 3, CLP-like, and custom formats (see Section 9 for details of data package deliverable). The following charges apply to the data package requested:

Level 2 10% Level 3 15% CLP-Like 20% Custom Package Call for Pricing

5. CertificationsAnalytics seeks specific certifications as our business strategies require that we gain them. Our laboratory is certified by some of the most prestigious environmental oversight agencies including the National Environmental Laboratory Accreditation Conference (NELAC). We are currently approved as an environmental laboratory in conformance with the NELAC standards through the Commonwealth of Virginia for the following categories: Potable Water, Non-Potable Water and Solid and Hazardous Waste. Certification under the NELAC program provides for reciprocity to all NELAC authorized states, which includes FL, IL, KS, LA, MN, NH, NY, OR, PA, TX, and UT. A complete listing of our state and federal certifications can be found on our website at www.analyticscorp.com

120

http://www.analyticscorp.com/

6. Sample Containers/Shipping KitsWe will provide and ship the appropriate sample supplies/containers by non-priority status to clients within the continental United States at no charge with one exception: Nitric acid preserved containers are classified as a hazardous shipment and appropriate charges will be applied. Clients requesting overnight delivery of supplies and those outside the continental U.S. will be invoiced for the associated charges when applicable. Due to the changes in shipping regulations, Nitric acid preserved sampling containers cannot be shipped overnight. It is the client’s responsibility to ensure proper sampling, packing, and return shipping to the laboratory under proper storage/preservation conditions.

7. Sample Kit/Cooler Return PolicyWe will provide and ship (by non-priority status) the appropriate sample containers in a sample kit or cooler. We request that the kits/coolers be returned to us within 30 days. Please notify your Client Services Representative if you cannot meet this deadline. Clients will be billed for any unreturned kits/coolers, inserts, packing material, and bottles. The value of the kits and coolers ranges between $50 and $250.

8. Sample Kit/Cooler TemperaturesWhen samples arrive at the laboratory, the temperature of each shipping container is measured and recorded. Samples should be packed such that they maintain a temperature range of 2-6°C during shipment. To ensure shipment at the proper temperature, we recommend using bags of ice rather than ice packs or artificial coolants. Guidance addressing temperature varies by state, regulatory program, and client-specific quality assurance plans.

9. Sample Collection and Preservation GuidelinesPreservatives must be added in the field at the time of sample collection unless sample containers are pre-preserved. Preservatives should be recorded on the Chain-of-Custody (COC) form in the "Preservative" column on a per sample basis. For certain methods and parameters, the laboratory verifies upon receipt that the sample pH falls within an acceptable range. Improperly preserved samples or samples with pH values outside of the specified range are noted in the sample container receipt form. The client is contacted and given the option of re-sampling, directing the laboratory to preserve the sample in-house, or processing the sample as it was received, and recorded on the COC.

When obtaining aqueous samples for the determination of volatile organics, the collector should ensure the absence of headspace by filling the 40-ml bottle to the top. This procedure should produce a positive meniscus across the surface of the vial. The Teflon-lined septum should be placed gently over the sample surface, with the Teflon side down, and the top screwed firmly on over the septum. A proper seal should be verified by inverting the sealed bottle and gently tapping on the sides with your finger, ensuring that no air bubbles appear.

If applicable, the collector should designate which samples are to be used for Quality

121

Control. For these designated samples, the recommended sample weight or volume should be doubled. If sufficient sample is not available to the laboratory, QC requirements may not be achievable. Excess sample will unnecessarily increase shipping costs.

Sampling and Shipping Guidelines:

Bottles: • Do not open any bottles until you actually put your sample in them - this

prevents contamination.• Do not substitute your own bottles or interchange any lids or labels on our

bottles.• Securely repack all bottles provided. Otherwise, bottle breakage may occur.• Do not rinse bottles prior to sample collection. Rinsing will contaminate them

and remove preservative. Some states may require that non-preservedcontainers be rinsed with sample water before collection.

Ice/Blue Ice: • A wet ice slurry is ideal for sample collection and the use of blue ice is

discouraged and not allowed by some state certifying bodies. • If you must use blue ice, freeze in a standard freezer for at least 12 hours and no

more than 18 hours prior to sampling. Do not freeze the blue ice using dry ice. This freezes your sample and breaks bottles.

• Do not freeze the sample itself.• Please repack the blue ice with red caps upward. Otherwise, your sample results

may not be accurate or bottle breakage may occur during shipment.

Sample Records: • Two types of labels will be supplied: a return shipping label and a sufficient

number of sample identification labels. On the sample identification labels, please complete all sections of the label to eliminate the possibility of samples being mixed up. A Chain-of-Custody record and packing list are also provided.

• Provide as much identifying information about your company on the COC,including your account number, as possible. Analytics processes thousands ofsamples a year—often from several plants of the same company, and very oftenon the same day!

10. How to Submit a Sample

1. Complete all the pertinent information on the chain of custody (COC) about yourcompany and the project. Please include the state where the samples werecollected. A COC can be found on our website at www.analyticscorp.com/forms.

a. Sample Identification: A unique sample description that will appear on thereport. Date and time collected should always be recorded.

b. Grab or Composite: Indicate whether the sample is a grab (taken at one timefrom a single location) or a composite (taking multiple samples andcombining them into one).

c. Matrix: Mark the type of sample and number of containers. If applicable,indicate whether the water is a groundwater, waste water, or drinking water.

d. Analyses Requested: Write the analysis name or abbreviation. Clearlyindicate the analyses needed on every sample.

e. Preservative: Please indicate what preservative was used, if any.f. Turnaround Time: Indicate whether the samples are to be analyzed on a

normal (5 working days) or rush basis. To assist the lab in scheduling, you can

122

also include the date you need results. All rush work should be prescheduled. Also indicate if you would like preliminary results phoned, emailed or faxed to you, and include the number or email address.

g. Data Package Options: When a detailed data packaged is required, indicatethe type of data package and if site QC is being submitted.

h. Relinquished by/Received by: Each time there is a change in the samplescustody, this section must be signed by the person relinquishing and the person receiving the samples. Chain-of-custody seals for the sample containers and the outside of the package are available upon request.

2. Each sample bottle must be clearly labeled and cross-referenced on your chain ofcustody.

3. Samples which may present health hazards, such as those containing high levels oftoxic materials, MUST be clearly marked.

4. If accurate and detailed information is not available, it will delay sample processingand possibly inhibit meeting your reporting date.

11. Reports and DeliverablesAnalytical reports convey to the client all of the information that is needed to evaluate the analytical results and draw conclusions about the levels those samples represent. Unless a specific format is requested, the standard laboratory procedure is to report Level 1 results to the limit of quantitation (LOQ). In many instances, it is possible to estimate to a value below the LOQ, if lower values are needed. These estimates are made to the method detection limit (MDL). Values reported below the LOQ are flagged with a “J” to indicate that the value is estimated.

A typical Level 1 analytical report will include the following:

1. Laboratory name, address, telephone number, and certification/ID number2. Client name and/or site name3. Date and time of sample collection or pickup4. Date and time of sample receipt, extraction, and analysis5. Laboratory sample ID number6. Customer sample ID number7. Method reference (EPA, Standard Methods, etc.)8. Sample type9. Requested analytes10. Analytical results with units of measurement11. Reporting limits12. Data qualifier code(s) if needed13. Remarks about sample irregularities or problem in analysis14. Initials of laboratory analyst, signature of lab director or designee

123

Detailed data packages are also available, upon request, which document QA/QC in addition to the sample analyses for each batch of samples. For data package purposes, a batch is defined as the samples listed on a COC and is generally less than 20 field samples. If you request site-specific QA/QC samples, one sample in each batch must be submitted in triplicate in order to meet volume requirements. An additional charge for these samples will be incurred if less than 10 samples are submitted. If your data package does not require site-specific QC, you will not be charged for laboratory batch QC samples. The turnaround time for extended data packages is contingent upon the level of the data package.

Analytics can provide our clients any report format since all laboratory data is stored and generated from a common database. In order to meet both regulatory agency and client requirements, we are constantly updating our data package formats. If you need additional modifications to the report formats listed below, please contact our customer service department or your project manager. A description of our most commonly requested reports are as follows:

Organics Data Packages

Data Requirements 1 2 3 4 EPA-CLP Equivalent Forms Case Narrative X X NA Cross Reference Sample ID/Client ID X X Cover Page Sample Result Summary X X X X 1A, 1B,C, 1D Surrogate Recovery X X X 2A, 2B, 2C, 2D, 2E, 2F Matrix Spike/Matrix Spike Duplicate Recovery X X X 3A, 3B, 3C, 3D, 3E Laboratory Control Sample X X X NA Method Blank Summary X X 4A, 4B, 4C Method Blank Results X X 1A, 1B,C, 1D Instrument Performance Check (Tune Report) X X 5A, 5B Initial Calibration Data X X 6A, 6B, 6C, 6D, 6E, 6F, 6G Continuing Calibration Check X X 7A, 7B, 7C, 7D, 7E Internal Standard Area and RT Summary X X 8A, 8B, 8C, 8D Raw Data X NA External Chain-of-Custody X X X X NA Internal Custody Tracking Documentation X NA

Inorganics Data Packages

Data Requirements 1 2 3 4 EPA-CLP Equivalent Forms Case Narrative X X NA Cross Reference Sample ID/Client ID X X Cover Page Sample Result Summary X X X X 1 Initial Calibration X X 2A Continuing Calibration Verification X X 2A Method Blank Results X X 3 ICP Interference Check Sample X X 4 Matrix Spike Sample Recovery X X X 5A, 5B Duplicates X X X 6 Laboratory Control Sample X X X 7 Raw Data X NA External Chain-of-Custody X X X X NA Internal Custody Tracking Documentation X X NA

X = Offered as part of QC Package * = Only offered if requested

124

12. Alphabetical Listing of Methods

Analytics is pleased to offer an extensive array of environmental analyses, including most EPA, RCRA, UST, TCLP, drinking water and wastewater methods. Specific analytical tests are listed in the following sections. Lists of tests are presented by an alphabetical list by analyte. Please note that for most tests Analytics does not require a minimum sample fee. Volume discounts are available depending on the scope of your project. Please contact our sales department or your project manager for details.

Each COC submitted is considered a Work Order (WO), therefore a separate report package is prepared for each COC submitted unless otherwise requested.

125

Alphabetical Listing

of

Environmental Tests

V01 06.2017 Toll Free: 800-888-8061 Find more info at www.analyticscorp.com 126

Analyte Name Method Matrix Container Preservation Holding TimeQuantitation

Limits (mg/L)

Unit PriceComments

Acidity SM2310BDrinking Water /

Water

250 mL Plastic,

No HeadspaceCool < 6 ºC 14 days 5.00 $29

Alcohol Profile EPA 8015 Water 40 mL Vial Cool < 6 ºC 7 days 10.0 $104 Ethanol, Methanol, Isopropanol

Alcohol Profile EPA 8015Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC 14 days 10.0 mg/kg $104 Ethanol, Methanol, Isopropanol

Alkalinity, Total SM2320BDrinking Water /

Water

250 mL Plastic,


Alkalinity - Bicarbonate SM2320BDrinking Water /

Water

250 mL Plastic,


Alkalinity - Carbonate SM2320BDrinking Water /

Water

250 mL Plastic,


Alkalinity - Hydroxide SM2320BDrinking Water /

Water

250 mL Plastic,


Aggressive Water Index Calculation Drinking Water250 mL Plastic,

No Headspace/ 500mL

250 mL plastic

unpreserved /

500mL plastic

HNO3 preserved

14 days N/A $29Calculation based on Field pH, Alkalinity

and Calcium Hardness

Ammonia-N SM4500NH3G Water 500 mL PlasticCool < 6 ºC;

H2SO428 days 0.10 $35

Anion Profile - inclusive

(Br, Cl, F, NO2, NO3, PO4, SO4)EPA 300.0

Drinking Water /

Water125 mL Plastic Cool < 6 ºC

28 days -

48 hours for

NO2, NO3,

o-Phos

0.1 - 1.0 $127

Anion Profile - inclusive

(Br, Cl, F, NO2, NO3, PO4, SO4)EPA 300.0 Mod.

Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC

28 days -

48 hours for

NO2, NO3,

o-Phos

1.0-10.0 ug/g $127

BOD (Biochemical Oxygen

Demand)SM5210B Water 1 L Plastic Cool < 6 ºC 48 hours 2 $29

Bromide EPA 300.0Drinking Water /

Water125 mL Plastic Cool < 6 ºC 28 days 0.50 $41

Bromide EPA 300.0 Mod.Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 28 days 5.0 ug/g $41

Nominal limit for soils. Final Detection

limit adjusted for sample weight and

percent moisture.

BTEX EPA 8021 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

1-5 ug/L $64

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Limits (mg/L)

Unit PriceComments

BTEX EPA 8021Solid / Soil /

Waste4 oz Glass Jar Cool < 6 ºC 14 days 1.0 mg/Kg $64



percent moisture.

BTEX + MTBE EPA 8021 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

1-5 ug/L $69

BTEX + MTBE EPA 8021Solid / Soil /




percent moisture.

BTEX + MTBE +

NaphthaleneEPA 8021 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

1-5 ug/L $69

BTEX + MTBE +

NaphthaleneEPA 8021

Solid / Soil /




percent moisture.

Benzene, Toluene,

EthylbenzeneEPA 602 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

1-5 ug/L $64 Used for Discharge (Clean Water Act)

BTEX EPA 524.2 Drinking Water (3) 40 mL VialsCool < 6 ºC, HCl,

Ascorbic Acid14 days 2.0-5.0 ug/L $191

BTU ASTM D 240 Water 8 oz Glass Jar Cool < 6 ºC 28 days Call for limitsCall for

pricing

BTU ASTM D 240Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 28 days Call for limits

Call for

pricing

Carbon Call for Method Water

Carbon Call for MethodSolid / Soil /

Waste

Carbon Dioxide (CO) SM4500CO2Drinking Water /

Water

250 mL Glass,

No HeadspaceCool < 6 ºC Immediately 10.00 $46

Call for container, preservation, limits and pricing


V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

CBOD (Carbonaceous Bio-

chemical Oxygen Demand)SM5210B Water 1L Plastic Cool < 6 ºC 48 Hours 2 $46

Chloride EPA 300.0Drinking Water /


Chloride EPA 300 Mod.Solid / Soil /


Chlorine, Residual SM4500ClGDrinking Water /

Water

250 mL Amber Glass,

Zero HeadspaceCool < 6 ºC Immediately 0.20 $29

Chlorine, Free SM4500ClGDrinking Water /

Water

250 mL Amber Glass,


COD (Chemical Oxygen

Demand)EPA 410.4 Water 250 mL Plastic

Cool < 6 ºC;

H2SO428 days 20.0 $29

Coliform - E. Coli,

Presence/Absence

SM9223B

(Colisure)Drinking Water Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

30 Hours Present / Absent $58

E. Coli, MPNSM9223

ColisureDrinking Water Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

30 Hours < 1 MPN/100 mL $58

E. Coli, MPNSM9223

ColisureWastewater Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

8 Hours < 1 MPN/100 mL $58

Coliform - Fecal, (MPN) SM9221E Water Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

8 Hours 2 CFU/mL MPN $58

Coliform - Total,

Presence/ Absence

SM9223

ColisureDrinking Water Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

30 Hours Present / Absent $58

Coliform, Total (MPN)SM9223

Colilert 18Drinking Water

Cool < 10 ºC;

Sodium

Thiosulfate

30 Hours < 1 MPN/100 mL $58

Color SM2120BDrinking Water /

Water125 mL Plastic Cool < 6 ºC 24 hours 5 CU $18

Conductivity SM2510B Drinking Water 125 mL Plastic Cool < 6 ºC 28 days N/A $18

Conductivity EPA 120.1 Water 125 mL Plastic Cool < 6 ºC 28 days N/A $18

Corrosivity (pH meter) SM4500H+B Water 125 mL Plastic Cool < 6 ºC Immediately N/A $18

Corrosivity (pH meter) EPA 9045CSolid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC Immediately N/A $18

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Cyanide, Amenable SM4500CNGDrinking Water /

Water500 mL Plastic

Cool < 6 ºC

NaOH14 days 0.02 $46

Cyanide, Total SM4500CN C&EDrinking Water /

Water500 mL Plastic

Cool < 6 ºC

NaOH14 days 0.02 $46

Cyanide, Total EPA 9010C/9014Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC 14 days 1.00 mg/Kg $46

Density ASTM D1475 Waste / Oil / Pant 8 oz Wide Mouth Jar Cool < 6 ºC 7 days N/A $46

Dissolved Organic Carbon SM5310CDrinking Water /

Water250 mL Amber Glass

Cool < 6 ºC

H2SO428 Days 1.00 $46

Dissolved Organic Carbon EPA 9060A ModSolid / Soil /

Waste2 oz Wide Mouth Jar Cool < 6 ºC 28 Days 10.0 mg/Kg $46

Diesel Range Organics (DRO) EPA 8015 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.50 $76

Diesel Range Organics (DRO) EPA 8015Solid / Soil /




percent moisture.

EDB/DBCP EPA 8011 Water (3) 40 mL Vials Cool < 6 ºC; HCl 14 days 0.05 ug/L $76

Endotoxin

Manufacturer

Analytics SOP

ENVWC-023-LAL

Drinking Water /

Water

Sterile / Pyrogen Free

Plastic TubeCool < 6 ºC Not Specified 0.05 EU/mL $46

Ethylene Dibromide, 1,2-Di-

bromo-3-chloropropane, 1,2,3-

Trichloropropane

EPA 504.1 Drinking Water (3) 40 mL VialsCool < 6 ºC,

Na2S2O314 days 0.05 ug/L $69

Ethylene Glycol EPA 8015 Water 40 mL Vial Cool < 6 ºC 7 days 10.0 $104

Ethylene Glycol EPA 8015Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC 14 days 10.0 mg/kg $104



percent moisture.

Extractable Organic Halides

(EOX)EPA 9020

Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC 14 days Call for limits

Call for

pricing

Flashpoint, Liquids by Closed

CupASTM D93 Water

250 mL Amber Glass,

or plasticCool < 6 ºC 7 days > 75ºC $46

Flashpoint, Liquids by Closed

CupASTM D93

Solid / Soil /

Waste8 oz Wide Mouth Jar Cool < 6 ºC 7 days > 75ºC $46

Fluoride EPA 300.0Drinking Water /


V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Fluoride EPA 300.0 Mod.Solid / Soil /


Formaldehyde EPA 8315 Water 1 Liter Amber Glass Cool < 6 ºC 3 days 100 ug/L $208

Formaldehyde EPA 8315Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 14 days 0.100 mg/kg $208



percent moisture.

Free Liquids EPA 9095A Water 8 oz Jar Cool < 6 ºC 7 days + / - $46

Free Liquids EPA 9095ASolid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 7 days + / - $46

Fuels - Fingerprinting EPA 8015 Mod Water (2) 1 L Amber Glass Cool < 6 ºC 7 days N/A $133Compared to in house Fuels. Reported

as a distillation range comparison.

Fuels - Fingerprinting EPA 8015 ModSolid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 14 days N/A $133

Compared to in house Fuels. Reported

as a distillation range comparison.

Gasoline Range Organics

(GRO)EPA 8015 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

500 ug/L $64

Gasoline Range Organics

(GRO)EPA 8015

Solid / Soil /




percent moisture.

Glycol Profile EPA 8015 Water 40 mL Vial Cool < 6 ºC 7 days 10.0 $104

Ethylene Glycol, Propylene Glycol,

Diethylene Glycol, Dipropylene Glycol,

Triethylene Glycol

Glycol Profile EPA 8015Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC 14 days 10.0 mg/kg $104



percent moisture

Haloacetic Acids

(HAA)EPA 552.2 Drinking Water

Hardness, Total SM2340C Drinking Water 250 mL Plastic HNO3 180 days 10.0 $29

Hardness, Total EPA 200.7 Water 250 mL Plastic HNO3 180 days 0.05 $23

Herbicides - Chlorinated EPA 515 Drinking Water (2) 1 L Amber Glass Cool < 6 ºC 7 days Call for limitsCall for

pricing

Herbicides - Chlorinated EPA 8151A Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 2.00 $341


V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Herbicides - Chlorinated EPA 8151 Soil 8 oz Glass Jar Cool < 6 ºC 14 days Call for limitsCall for

pricing

Heterotrophic Plate Count

(HPC)SM9215B Drinking Water Sterile Container

Cool < 10 ºC;

Sodium

Thiosulfate

8 Hours 1 CFU/mL $58 HPC Agar 48 hour incubation

Heterotrophic Plate Count

(HPC)SM9215B Drinking Water Sterile Container

Cool < 10 ºC ;

Sodium

Thiosulfate

8 Hours 1 CFU/mL $58 R2A Agar 7 day incubation

Hexavalent Chromium SM3500CrB Water 250 mL Plastic Cool < 6 ºC 24 hours 0.02 $58

Hexavalent Chromium SM3500CrB Water250 mL Plastic

pH 9.3-9.7

Ammonium

Sulfate Buffer28 days 0.02 $58

Hydrazine ASTM D385 Water 500 mL Plastic Cool < 6 ºC 7 days Call for limitsCall for

pricing

Hydrogen Sulfide SM4500S2H Water 500 mL Plastic Cool < 6 ºC 7 Days 2.00 $46Calculation based on pH, Conductivity

and Total Sulfide

Ignitability by Closed Cup ASTM D93 Water250 mL Amber Glass,

or plasticCool < 6 ºC 7 days > 60ºC $53

Ignitability by Closed Cup ASTM D93Solid / Soil /

Waste8 oz Wide Mouth Jar Cool < 6 ºC 7 days > 60ºC $53

LAL

(Limulus Amebocyte Lysate)

Manufacturer

Analytics SOP

ENVWC-023-LAL

Drinking Water /

Water

Sterile / Pyrogen Free

Plastic TubeCool < 6 ºC Not Specified 0.05 EU/mL $46

Langlier Saturation Index Calculation Drinking Water

250 mL Plastic,

No Headspace /

1000mL/ 500mL

250 mL plastic

unpreserved

/1000mL plastic

unpreserved

500mL plastic

HNO3 preserved

14 days N/A $29

Calculation based on Field

Temperature, Field pH, Alkalinity, TDS

and Calcium Hardness

Lead EPA 200.7 Water 500 mL Plastic HNO3 180 days 0.05 $23

Lead EPA 6010 Water 500 mL Plastic HNO3 180 days 0.05 $23

Lead EPA 6010Solid / Soil /

Waste4 oz Wide Mouth Jar None 180 days 4 ug/g $23

Lead EPA 200.8 Drinking Water 500 mL Plastic HNO3 180 days 0.0025 $29

MBAS (Surfactants) SM5540CDrinking Water/

Water1000 mL plastic Cool < 6 ºC 48 hours 0.10 $76

Mercury EPA 245.2Drinking Water/

Water500 mL plastic HNO3 28 days 0.0002 $35

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Mercury EPA 7470 Water 500 mL plastic HNO3 28 days 0.0002 $35

Mercury EPA 7471Solid / Soil /

Waste4 oz Glass Jar HNO3 28 days 0.025 mg/Kg $35

Metals - Appendix IXEPA 6010 / EPA

7470Water 500 mL Plastic HNO3

6 months / 28

days for

Mercury

0.05; Hg 0.0005 $203

Antimony, Arsenic, Barium, Beryllium,

Cadmium, Chromium, Cobalt, Copper,

Lead, Molybdenum, Nickel, Selenium,

Silver, Thallium, Tin, Vanadium, Zinc,

Mercury

Metals - Appendix IXEPA 6010 / EPA

7471

Solid / Soil /

Waste4 oz Wide Mouth Jars None

6 months /

28 days for

Mercury

4 ug/g

Hg 0.025ug/g$203


Cadmium, Chromium, Cobalt, Copper,

Lead, Molybdenum, Nickel, Selenium,

Silver, Thallium, Tin, Vanadium, Zinc,

Mercury

Metals - Priority Pollutant List

(PPL)

EPA 200.7 / EPA

245.2Water 500 mL Plastic HNO3

6 months /

28 days for

Mercury

0.05; Hg 0.0002 $145

Antimony, Arsenic, Beryllium,

Cadmium, Chromium, Copper, Lead,

Nickel, Selenium, Silver, Thallium, Zinc,

Mercury

3

Metals - Priority Pollutant List

(PPL)

EPA 6010 / EPA

7471

Solid / Soil /

Waste4 oz Glass Jar None

6 months /

28 days for

Mercury

4 ug/g

Hg 0.025ug/g$145

Antimony, Arsenic, Beryllium,


Nickel, Selenium, Silver, Thallium, Zinc,

Mercury

Metals - RCRA (8)EPA 6010 / EPA


6 months /

28 days for

Mercury

0.05; Hg 0.0005 $104Arsenic, Barium, Cadmium, Chromium,

Lead, Selenium, Silver, Mercury

Metals - RCRA (8)EPA 6010 / EPA

7471

Solid / Soil /

Waste4 oz Wide Mouth Jars None

6 months /

28 days for

Mercury

4 ug/g

Hg 0.025ug/g$104

Arsenic, Barium, Cadmium, Chromium,

Lead, Selenium, Silver, Mercury

Metals - Target Analyte List

(TAL)

EPA 6010 / EPA


6 months /

28 days for

Mercury

0.05; Hg 0.0005 $203

Aluminum, Antimony, Arsenic, Barium,

Beryllium, Cadmium, Calcium,

Chromium, Cobalt, Copper, Iron, Lead,

Magnesium, Manganese, Molybdenum,

Nickel, Potassium, Selenium, Silver,

Thallium, Vanadium, Zinc, Mercury

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Metals - Target Analyte List

(TAL)

EPA 6010 / EPA

7471

Solid / Soil /

Waste4 oz Glass Jar None

6 months /

28 days for

Mercury

4 ug/g

Hg 0.025ug/g$203






Thallium, Vanadium, Zinc, Mercury

Metals by ICP EPA 200.7Drinking Water /

Water500 mL Plastic HNO3 6 months 0.05 - 0.25 $23 Individual Elements

Metals by ICP EPA 6010 Water 500 mL Plastic HNO3 6 months 0.05 - 0.25 $23 Individual Elements

Metals by ICP EPA 6010Solid / Soil /

Waste4 oz Glass Jar None 6 months 4 ug/g $23 Individual Elements

Metals by ICP/MS EPA 200.8Drinking Water /

Water500 mL Plastic HNO3 6 months 0.0025 - 0.010 $29 Individual Elements

Nitrate, as Nitrogen (NO3) EPA 300.0Drinking Water /

Water125 mL Plastic Cool < 6 ºC 48 hours 0.11 $46

Nitrate-Nitrite, as Nitrogen SM4500NO3FDrinking Water /

Water250 mL Plastic

Cool < 6 ºC

H2SO428 days 0.05 $46

Nitrite, as Nitrogen EPA 300.0Drinking Water /


Nitrite, as Nitrogen SM4500NO2BDrinking Water /


Nitrogen, TotalEPA351.2 /

SM4500NO3FWater 250 mL Plastic

Cool < 6 ºC;

H2SO428 days 0.25 $104

Sum of the Total Kjeldahl Nitrogen and

Nitrate-Nitrite Analysis.

Oil and Grease -Total EPA 1664 Water (2) 1 L Amber GlassCool < 6 ºC; HCL

or H2SO428 days 5.00 $81 Hexane extractable materials (HEM)

Oil and Grease -TPH EPA 1664 Water (2) 1 L Amber GlassCool < 6 ºC; HCL

or H2SO428 days 5.00 $92

Silica gel treated hexane extracted

materials (HEM-SGT or HEM-TPH)

Oil and Grease -AV EPA 1664 Water (2) 1 L Amber GlassCool < 6 ºC; HCL

or H2SO428 days 5.00 $173

If requested individually, AV is

determined from Total Oil & Grease -

TPH Oil & Grease

Oxygen, Dissolved SM4500OGDrinking Water /

Water

250mL Amber Glass,


PAHs - Polynuclear Aromatic

HydrocarbonsEPA 550 Drinking Water (2) 1 L Amber Glass Cool < 6 ºC 7 days Call for limits

Call for

pricing


HydrocarbonsEPA 610 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 20 ug/L $173 Used for Discharge (Clean Water Act)


HydrocarbonsEPA 8100

Solid / Soil /

Waste8 oz Wide Mouth Jars Cool < 6 ºC 14 days 1.00 mg/Kg $173



percent moisture.

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments


HydrocarbonsEPA 8270 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 10 ug/L $226



Solid / Soil /

Waste8 oz Wide Mouth Jars Cool < 6 ºC 14 days

0.333 - 0.666

mg/Kg$226



percent moisture.


HydrocarbonsEPA 8310 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.2-2.0 ug/L $173



Solid / Soil /

Waste8 oz Wide Mouth Jars Cool < 6 ºC 14 days 0.01 - 0.05 mg/Kg $173



percent moisture.

PCB (Polychlorinated

Biphenyls)EPA 508 Drinking Water (2) 1 L Amber Glass Cool < 6 ºC 1 year Call for limits

Call for

pricing


Biphenyls)EPA 608 Water (2) 1 L Amber Glass Cool < 6 ºC 1 year 2.00 ug/L $87 Used for Discharge (Clean Water Act)


Biphenyls)EPA 8082 Water (2) 1 L Amber Glass Cool < 6 ºC 1 year 1.00 ug/L $87


Biphenyls)EPA 8082 Wipe Call for PCB wipe kit Cool < 6 ºC 1 year 2 ug/Wipe $87


Biphenyls)EPA 8082

Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 1 year 0.500 mg/Kg $87



percent moisture.


Biphenyls)EPA 8082 Bulk / Caulk 4 oz Glass Jar Cool < 6 ºC 1 year 0.500 mg/Kg $104


Biphenyls)EPA 8082 Bulk / Caulk 4 oz Glass Jar Cool < 6 ºC 1 year Call for limits

Call for

pricing

EPA regions that require soxhlet

extraction for the preparation

procedure EPA 3540C.

Percent Ash ASTM D482Solid / Soil /

Waste4 oz Glass Jar Cool < 6 ºC 14 days Call for limits

Call for

pricing

Percent MoistureEPA 3550 Sec.

7.2Soil 4 oz Glass Jar Cool < 6 ºC 14 days 0.5% $12

Percent SolidsEPA 3550 Sec.

7.2Soil 4 oz Glass Jar Cool < 6 ºC 14 days 0.5% $12

Percent Solids SM2540G Sludge 8 oz glass Jar Cool < 6 ºC 14 days 0.5% $18

Percent Water (Karl Fischer) ASTM D1744 Waste / Oil / Pant 4 oz Glass Jar Cool < 6 ºC 14 days Call for limitsCall for

pricing

Pesticides - Chlorinated EPA 508 Drinking Water (2) 1 L Amber Glass Cool < 6 ºC 7 days Call for limitsCall for

pricing

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Pesticides - Chlorinated EPA 608 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.1-10 ug/L $145 Used for Discharge (Clean Water Act)

Pesticides - Chlorinated EPA 8081 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.1-10 ug/L $145

Pesticides - Chlorinated EPA 8081Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 14 days 0.02 - 0.2 mg/Kg $145



percent moisture.

pH SM4500H+BDrinking Water /

Water125 mL Plastic Cool < 6 ºC Immediately N/A $29

Phenol, Total (Phenolics) EPA 420.1 Water (2) 1 L Amber GlassCool < 6 ºC;

H2SO428 days 0.005 - 0.05 $87

Phenol, Total (Phenolics) EPA 9065 Solid/Waste 8 oz Glass JarCool < 6 ºC;

H2SO428 days 0.005 - 0.05 $87

Phosphorate, Ortho (as

Phosphorus)EPA 300.0

Drinking Water /


Phosphorate, Ortho (as

Phosphorus)

EPA 365 as

HACH 8048Drinking Water 125 mL Plastic Cool < 6 ºC 48 hours 0.020 $29

Phosphorus, Total SM4500 PEH Water 250 mL PlasticCool < 6 ºC;

H2SO428 days 0.020 $46

Reactivity (Cyanides/ Sulfides) EPA Chapter 7 Water 500 mL PlasticCool < 6 ºC;

NaOH7 days 200 $87

Reactivity (Cyanides/ Sulfides) EPA Chapter 7Solid / Soil /

Waste8 oz Glass Jar Cool < 6 ºC 14 days 200 mg/Kg $87

Resistivity EPA 120.1 Water 125 mL Plastic Cool < 6 ºC 28 days N/A $18

Semivolatiles EPA 525 Drinking Water (2) 1 L Amber Glass Cool < 6 ºC 7 days Call for limitsCall for

pricing

Semivolatiles EPA 625 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 20-40 ug/L $226 Used for Discharge (Clean Water Act)

Semivolatiles EPA 8270 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 10-40 ug/L $226

Semivolatiles EPA 8270Solid / Soil /

Waste8 oz Wide Mouth Jar Cool < 6 ºC 14 days

0.333 - 0.666

mg/Kg$226



percent moisture.

Semivolatiles - Tentatively

Identified Compounds

(TICs) Library Search

EPA 625 /EPA

8270N/A N/A N/A N/A N/A $46

If requested, TICs must be accompanied

by a corresponding analysis, either EPA

625 or EPA 8270.

Settleable Solids (SS) SM2540F Water 1 L Plastic Cool < 6 ºC 48 hours 0.10 mL/L $18

Silicates (Silica) EPA 200.7Drinking Water /

Water500 mL Plastic HNO3 6 months 0.05 $46

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Solids, Total (TS) SM2540BDrinking Water /

Water1 L Plastic Cool < 6 ºC 7 days 10.0 $18

Solids, Total (TS) SM2540G Solid / Sludge 16 oz Glass Jar Cool < 6 ºC 7 days 0.01 % $18

Solids, Total Dissolved (TDS) SM2540CDrinking Water /

Water1 L Plastic Cool < 6 ºC 7 days 10.0 $18

Solids, Total Suspended (TSS) SM2540D Water 1 L Plastic Cool < 6 ºC 7 days 1.00 $18

Solids, Total Fixed (TFS) SM2540E Water 1 L Plastic Cool < 6 ºC 7 days 1.00 % $18

Solids, Total Fixed (TFS) SM2540G Solid / Sludge 16 oz Glass Jar Cool < 6 ºC 7 days 1.00 % $18

Solids, Total Volatiles (TVS) SM2540E Water 1 L Plastic Cool < 6 ºC 7 days 1.00 % $18

Solids, Total Volatiles (TVS) SM2540G Solid / Sludge 16 oz Glass Jar Cool < 6 ºC 7 days 1.00 % $18

Specific Conductance SM2510B Drinking Water 125 mL Plastic Cool < 6 ºC 28 days N/A $18

Specific Conductance EPA 120.1 Water 125 mL Plastic Cool < 6 ºC 28 days N/A $18

Specific Gravity ASTM D1475 Waste / Oil / Pant 8 oz Wide Mouth Jar Cool < 6 ºC 7 days N/A $46

Sulfate EPA 300.0Drinking Water /


Sulfate EPA 300 Mod.Solid / Soil /


Sulfide SM4500S2FDrinking Water /

Water500 mL Plastic

Cool < 6 ºC; Zinc

acetate plus

NaOH

7 days 2.00 $29

Sulfite SM4500SO3BDrinking Water /

Water250 mL Plastic Cool < 6 ºC Immediately 2.00 $29

Sulfur EPA 200.7 Water 500 mL Plastic HNO3 180 days Call for limitsCall for

pricing

Sulfur EPA 6010 Water 500 mL Plastic HNO3 180 days Call for limitsCall for

pricing

Sulfur EPA 6010Solid / Soil /

Waste4 oz Wide Mouth Jar None 180 days Call for limits

Call for

pricing

Surfactants (MBAS) SM5540CDrinking Water /


Suitability Call for Method Drinking Water

TCLP Herbicides

[excludes extractions]EPA 8151 Water

(2) 1 Liter Amber Glass

w/Teflon Lined CapCool < 6 ºC

14 days

to TCLP

Extraction

0.05 $162


V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

TCLP Herbicides

[excludes extractions]EPA 8151

Solid / Soil /

Waste

8 oz. Wide Mouth

Glass w/Teflon Lined

Cap

Cool < 6 ºC

14 days

to TCLP

Extraction

0.05 $162

TCLP Metals

[excludes extractions]EPA 6010/7470 Water 500 mL Plastic Cool < 6 ºC

6 months

(Hg-28 days)

to TCLP

Extraction

0.5 - 10.0 $104

TCLP Metals

[excludes extractions]EPA 6010/7470

Solid / Soil /

Waste4 oz Wide Mouth Jar Cool < 6 ºC

6 months

(Hg-28 days)

to TCLP

Extraction

0.5 - 10.0 $104

TCLP Pesticides

[excludes extractions]EPA 8081 Water



14 days

to TCLP

Extraction

0.001 - 0.1 $145

TCLP Pesticides

[excludes extractions]EPA 8081

Solid / Soil /

Waste

8 oz. Glass w/ Teflon

Lined CapCool < 6 ºC

14 days

to TCLP

Extraction

0.001 - 0.1 $145

TCLP Semivolatiles [excludes

extractions]EPA 8270 Water



14 days

to TCLP

Extraction

0.100 $226

TCLP Semivolatiles [excludes

extractions]EPA 8270

Solid / Soil /

Waste

8 oz. Glass w/ Teflon

Lined CapCool < 6 ºC

14 days

to TCLP

Extraction

0.100 $226

TCLP Volatiles EPA 8260 Water (3) 40 mL Vials Cool < 6 ºC; 14 days 0.050 - 0.250 $145

TCLP- Volatiles

(includes ZHE)EPA 8260/ZHE

Solid / Soil /

Waste4 oz. Wide Mouth Jar Cool < 6 ºC;

14 days

to TCLP

Extraction

0.050 - 0.250 $226

TCLP- Extraction only

(non-VOA)EPA 1311 N/A N/A N/A

14 days;

6 months

Metals

(Hg-28 days)

to TCLP

Extraction

N/A $69

Temperature (Field) SM2550B Various 125 mL Plastic N/A Immediately N/A $12 Field measurement only

THM (THM) EPA 524.2 Drinking Water (3) 40 mL VialsCool < 6 ºC, HCl,

Ascorbic acid14 days 2.00 - 5.00 ug/L $191

Chloroform, Chlorodibromomethane,

Dibromochloromethane, Bromoform

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Total Trihalomethanes (TTHM) EPA 524.2 Drinking Water (3) 40 mL VialsCool < 6 ºC, HCl,

Ascorbic Acid14 days 2.00 - 5.00 ug/L $191

Chloroform, Chlorodibromomethane,

Dibromochloromethane, Bromoform

Total Halides

(TX)EPA 9020 Oil 4 oz Glass Jar Cool < 6 ºC; 14 days Call for limits

Call for

pricing

Total Kjeldahl Nitrogen (TKN) EPA 351.2 Water 250 mL PlasticCool < 6 ºC;

H2SO428 days 0.25 $46

Total NitrogenEPA351.2 /

SM4500NO3FWater 250 mL Plastic

Cool < 6 ºC

H2SO428 days 0.25 $104

Sum of the Total Kjeldahl Nitrogen and

Nitrate-Nitrite Analysis.

Total Organic Carbon

(TOC)SM5310C

Drinking Water /

Water250 mL Amber Glass

Cool < 6 ºC;

H2SO428 Days 1.00 $46

Total Organic Carbon

(TOC)EPA 9060

Solid / Soil /

Waste250 mL Amber Glass Cool < 6 ºC; 28 days 10.0 mg/kg $46

Total Organic Halides

(TOX)EPA 9020 Water 250 mL Amber Glass

Cool < 6 ºC

H2SO47 days Call for limits

Call for

pricing

Toxicity - Acute

Toxicity - Chronic

TPH-DRO EPA 8015 Water (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.50 $76

TPH-DRO EPA 8015Solid / Soil /




percent moisture

TPH-GRO EPA 8015 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

500 ug/L $64

TPH-GRO EPA 8015Solid / Soil /




percent moisture

TPH-HEM 1664 Water (2) 1 L Amber Glass Cool < 6 ºC

HCL or H2SO428 days 5 mg/L $92

Call for Container, Preservation and Pricing

Call for Container, Preservation and Pricing

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Limits (mg/L)

Unit PriceComments

TPH - Leachable HEM O&G1664/ ASTM

D3987Solids 8 oz Glass Jar Cool < 6 ºC 28 days 5 mg/L $145

Leachable TPH includes ASTM D3987

tumble

Turbidity EPA 180.1Drinking Water /

Water125 mL Plastic Cool < 6 ºC 48 hours 1 NTU $18

Viscosity ASTM D2196 Liquids

Call for container,

preservation, limits

and pricing

Volatiles EPA 524.2 Drinking Water (3) 40 mL VialsCool < 6 ºC, HCl,

Ascorbic Acid14 days 2.00 - 5.00 ug/L $191

Volatiles EPA 624 Water (3) 40 mL Vials HCl 14 days 2-10 ug/L $145 Used for Discharge (Clean Water Act)

Volatiles EPA 8260 Water (3) 40 mL Vials HCl 14 days 1.00-25 ug/L $145

Volatiles EPA 8260Solid / Soil /

Waste4 oz Glass Jar Cool < 6 ºC 14 days 0.050 - 1.25 mg/Kg $145



percent moisture

Volatiles - Aromatic

(BTEX, MTBE, Naphthalene)EPA 8021 Water (3) 40 mL Vials Cool < 6 ºC, HCl

14 days

preserved /

7 days

unpreserved

1-5 ug/L $69

Volatiles - Aromatic

(BTEX, MTBE, Naphthalene)EPA 8021

Solid / Soil /




percent moisture

Volatiles - Tentatively

Identified Compounds (TICs)

Library Search

Various N/A N/A N/A N/A N/A $29

If requested, TICs must be accompanied

by a corresponding analysis, either EPA

624 or EPA 8260

Volatile Suspended Solids

(VSS)SM2540E Water 1 L Plastic Cool < 6 ºC 7 days 1.00 $18

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Limits (mg/L)

Unit PriceComments

TCL & TAL Pkg. - Full,

(VOA, SVOA, Pest/PCB,

Metals and Cn)

EPA 8260Remediation/

Ground Water(3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 1.00 - 10.0 ug/L $866 Volatiles

EPA 8270 (2) 1 L Amber Glass Cool < 6 ºC 7 days 10.0 - 40.0 ug/L Semivolatiles

EPA 8081 (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.100 - 2.00 ug/L Pesticides

EPA 8082 (2) 1 L Amber Glass Cool < 6 ºC 1 year 1.00 ug/L PCBs (Polychlorinated Biphenyls)

EPA 6010 500 mL PlasticCool < 6 ºC

HNO36 months 0.05 - 0.5






Thallium, Vanadium, Zinc

EPA 7470 28 days 0.0005 Mercury

SM4500CN C&E 500 mL PlasticCool < 6 ºC

NaOH14 days 0.02 Cyanide

TCL & TAL Pkg. - Full,

(VOA, SVOA, Pest/PCB,

Metals and Cn)

EPA 8260Solid / Soil /

Waste4 oz Glass Jar Cool < 6 ºC 14 days 0.05 - 0.5 mg/Kg $866 Volatiles

EPA 8270 (2) 8 oz Glass Jars 14 days0.333 - 0.666

mg/KgSemivolatiles

EPA 8081 14 days0.020 - 0.200

mg/KgPesticides

EPA 8082 1 year 0.500 mg/Kg PCBs (Polychlorinated Biphenyls)

EPA 6010 6 months 4.00 ug/g






Thallium, Vanadium, Zinc

EPA 7470 28 days 0.025 ug/g Mercury

SM4500CN C&E 14 days 1.00 mg/Kg Cyanide

Profiles

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Limits (mg/L)

Unit PriceComments


Waste4 oz Glass Jar Cool < 6 ºC 14 days 0.05-1.25 $751

TCLP tumbling (leaching) procedure

performed by EPA 1311

EPA 8270 (2) 8 oz Glass Jars 14 days 0.1

EPA 8081 14 days 0.001-0.010

EPA 8151 14 days 0.05

EPA 6010 6 months 0.100 - 10.0

EPA 7470 28 days 0.002

TCLP - Full, (VOA, SVOA,

Pest, Herb, Metals includes

extraction)


Ground Water(3) 40mL VOA Vials Cool < 6 ºC 14 days 0.05-1.25 $751



EPA 8270 1 L Amber Glass Cool < 6 ºC 14 days 0.1

EPA 8081 1 L Amber Glass Cool < 6 ºC 14 days 0.001-0.010


EPA 6010 500 mL Plastic Cool < 6 ºC 6 months 0.100 - 10.0

EPA 7470 500 mL Plastic Cool < 6 ºC 28 days 0.002

TCLP - Full + RIC, (VOA,

SVOA, Pest, Herb, Metals,

Reactivity, Ignitability,

Corrosivity - includes

extraction)


Waste4 oz Glass Jar Cool < 6 ºC 14 days 0.05-1.25 $866



EPA 8270 (2) 8 oz Glass Jars 14 days 0.1

EPA 8081 14 days 0.001-0.010

EPA 8151 14 days 0.05

EPA 6010 6 months 0.100 - 10.0

EPA 7470 28 days 0.002

Chapter 7 14 days 200 mg/Kg

ASTM D93 14 days > 60ºC

EPA 9040C 14 days NA

TCLP - Full, (VOA, SVOA,

Pest, Herb, Metals - includes

extraction)

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Limits (mg/L)

Unit PriceComments

TCLP - Full + RIC, (VOA,

SVOA, Pest, Herb, Metals,

Reactivity, Ignitability,

Corrosivity - includes

extraction)


Ground Water(3) 40mL VOA Vials Cool < 6 ºC 14 days 0.05-1.25 $866




EPA 8081 1 L Amber Glass Cool < 6 ºC 14 days 0.001-0.010


EPA 6010 500 mL Plastic Cool < 6 ºC 6 months 0.100 - 10.0

EPA 7470 500 mL Plastic Cool < 6 ºC 28 days 0.002

Chapter 7 500 mL Plastic Cool < 6 ºC 14 days 200

ASTM D93 14 days > 60ºC

EPA 9040C 14 days NA

Priority Pollutants - Full, (VOA,

BNA, Pest/PCB, and Metals

and CN)

EPA 624 Water (3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 2.00 - 10.0 ug/L $693 Volatiles

EPA 625 (2) 1 L Amber Glass Cool < 6 ºC 7 days 20.0 - 40.0 ug/L Semivolatiles

EPA 608 (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.100 - 2.00 ug/L Pesticides / PCBs

EPA 200.7 500 mL PlasticCool < 6 ºC

HNO36 months 0.05 - 0.5 Metals

EPA 245.2 28 days 0.0002 Mercury

SM4500CN C& E 500 mL PlasticCool < 6 ºC


Total Toxic Organics

(TTO)EPA 624 Water (3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 0.002 - 0.010 $145

Total Toxic Organics generally includes

EPA 624, 625 and 608; components are

priced individually

EPA 625 (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.010 - 0.020 $226

EPA 608 (2) 1 L Amber Glass Cool < 6 ºC 7 days 0.005 - 0.008 $145

Primary Inorganics

(Safe Drinking Water Act)EPA 200.8 Drinking Water 500 mL Plastic

Cool < 6 ºC

HNO3

6 months

(Hg - 28 days)0.0025 - 0.010 $295



Mercury, Selenium, Thallium

EPA 300.0 125mL Plastic Cool < 6 ºC 48 hours 0.100 - 0.16 Fluoride, Nitrate, Nitrite

SM4500CNC & E 500 mL PlasticCool < 6 ºC


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Limits (mg/L)

Unit PriceComments

Secondary Inorganics

(Safe Drinking Water Act)EPA 200.7 Drinking Water 500 mL Plastic

Cool < 6 ºC

HNO336 months 0.050 $243

Aluminum, Iron, Manganese, Silver,

Zinc

SM2120B 500 mL Plastic Cool < 6 ºC 48 hours 5 CU Color

EPA 300.0 125mL Plastic Cool < 6 ºC 28 days 0.250 - 0.500 Chloride, Fluoride, Sulfate

SM5540C 1000 mL Plastic Cool < 6 ºC 48 hours 0.100 MBAS

SM4500H+B 125mL Plastic Cool < 6 ºC Immediately N/A pH

SM2540C 1000 mL Plastic Cool < 6 ºC 7 days 10 Total Dissolved Solids

Primary Metals Only (SDWA) EPA 200.8 Drinking Water 500 mL PlasticCool < 6 ºC

HNO3

6 months

(Hg - 28 days)0.0025 - 0.010 $231



Mercury, Selenium, Thallium

Secondary Metals Only

(SDWA)EPA 200.7 Drinking Water 500 mL Plastic

Cool < 6 ºC

HNO36 months 0.050 $110

Aluminum, Iron, Manganese, Silver,

Zinc

Hazardous Waste Profile A EPA 8021Solid / Soil /


Benzene, Toluene, Ethylbenzene,

Xylenes

EPA 9040C (2) 16 oz Glass Jars Immediately N/A Corrosivity

ASTM D93 14 days 75ºC Flashpoint

EPA 9095A 14 days N/A Free Liquids


EPA 3550 Sec 7.2 14 days N/A Percent Moisture

Chapter 7 14 days 200 mg/Kg Reactivity

EPA 6010 6 months 0.100 - 10.0TCLP Metals: Arsenic, Barium,

Cadmium, Chromium, Lead, Selenium

EPA 7470 28 days 0.002 TCLP Mercury

EPA 8015 14 days 10 mg/Kg Diesel Range Organics (DRO)

EPA 8015 14 days 10 mg/Kg Gasoline Range Organics (GRO)

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Hazardous Waste Profile A EPA 8021Remediation/

Aqueous Liquid(3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 1.00 - 10.0 ug/L $578


Xylenes

EPA 9040C 125 mL Plastic Cool < 6 ºC 14 days N/A Corrosivity

ASTM D93 500 mL Plastic 14 days 75oC Flashpoint

EPA 9095A 500 mL Plastic 14 days N/A Free Liquids

EPA 8082A(2) 1 Liter Amber Glass

w/Teflon Lined Cap1 year 1.00 ug/L PCBs (Polychlorinated Biphenyls)

SM2540B 500 mL Plastic 14 days N/A Percent Solids / Moisture

Chapter 7 500 mL Plastic 14 days 200.000 Reactivity

EPA 6010 500 mL Plastic 14 days 0.100 - 10.0TCLP Metals: Arsenic, Barium,



EPA 8015(2) 1 Liter Amber Glass

w/Teflon Lined Cap7 days 0.500 Diesel Range Organics (DRO)

EPA 8015 (3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 500 ug/L Gasoline Range Organics (GRO)

Hazardous Waste Profile B EPA 8021Solid / Soil /



Xylenes

EPA 9095A(2) 16 oz

Glass Jars14 days N/A Free Liquids


EPA 3550 Sec 7.2 14 days N/A Percent Moisture

EPA 6010 6 months 0.100 - 10.0TCLP Metals: Arsenic, Barium,



EPA 8015 14 days 10 mg/Kg Diesel Range Organics (DRO)

EPA 8015 14 days 10 mg/Kg Gasoline Range Organics (GRO)

V01 06.2017Toll Free: 800-888-8061



Limits (mg/L)

Unit PriceComments

Hazardous Waste Profile B EPA 8021Remediation/

Aqueous Liquid(3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 1.00 - 10.0 ug/L $485


Xylenes

EPA 9095A 500 mL Plastic Cool < 6 ºC 14 days N/A Free Liquids


w/Teflon Lined Cap1 year 1.00 ug/L PCBs (Polychlorinated Biphenyls)

SM2540B 500 mL Plastic 14 days N/A Percent Solids / Moisture

EPA 6010 500 mL Plastic 14 days 0.100 - 10.0TCLP Metals: Arsenic, Barium,




w/Teflon Lined Cap7 days 0.500 Diesel Range Organics (DRO)

EPA 8015 (3) 40mL VOA Vials Cool < 6 ºC; HCl 14 days 500 ug/L Gasoline Range Organics (GRO)

Sample Preparation Fee Various Solid VariousSee Specific

Analyte Method

See Specific

Analyte

Method

N/A $29

Sample preparation fee applied if a

sample matrix requires further

reduction prior to analysis. Client

notification by Analytics required.

Miscellaneous

V01 06.2017Toll Free: 800-888-8061


V. Miscellaneous Services and Fees

1. Introduction

By providing these more specialized analyses, Analytics has found that it truly

provides our clients a full-service “one stop shop” for their analytical testing needs

and requirements. Miscellaneous Services are the remaining laboratory analyses that

are less commonly run and do not necessarily conform to the traditional industrial

hygiene or environmental testing section of our service directory. The analyses

contained in the section are:

• Microbiology: Bacteria in Air

• Microbiology: Bacteria in Water

• Microbiology: Fungal

• Air Quality Testing

Since Analytics performs a wide array of analytical methodologies in-house, we do not

normally subcontract any samples. If, however, we do not run the analysis, then the

use of a qualified laboratory for subcontracted analytical services must be agreed to

by Analytics’ client before the analyses take place. By providing subcontract services,

Analytics can serve as your “one-stop shop” for all your testing needs.

Samples that require analysis by a subcontract laboratory for capability, test

verification, or workload purposes are subcontracted whenever possible to a

laboratory which is deemed competent by Analytics based upon accreditation and

work history (for instance, IH sample subcontracting will be to an AIHA-accredited lab

whenever feasible). Customer acceptance of subcontracting, in writing whenever

possible, is obtained before subcontracting, and the subcontract laboratory is

prominently identified in reporting of results. Analytics remains responsible for

subcontracted testing unless the customer or a regulatory authority has specified

the subcontract laboratory to be employed.

Analytics completes a separate chain-of-custody (COC) document to accompany the

samples to the subcontract laboratory. Upon receipt of the data, the laboratory

director and/or project manager reviews the results prior to sending the data. Any

problems encountered with subcontracted analyses should be communicated to the

project manager at Analytics. Analytics will then contact our subcontract laboratory

so the project manager remains the sole contact.

147

V 2. Microbiology: Bacteria in AirTest Procedure Method of Analysis Sampling Media Sampling Rate Suggested Air

Volume, L

Unit Cost

Total Bacterial Count, Air Visual Plate CountContact Customer Service for

Media Requirements

For Andersen Impactor:

28.3 L/min100-300 Call for Pricing

Total Bacterial Count, Air with

Identification

(Specify No. to ID)

Visual Plate Count

and Laboratory

Identification

Contact Customer Service for

Media Requirements



V 3 Microbiology: Bacteria in WaterParameter Method Sample Container Preservative Holding Time Cost

Total Bacterial Count, Bulk Visual Plate Count Bulk Material N/A N/A Call for Pricing

Total Bacterial Count, Bulk with

Identification (Specify No. to ID)

Visual Plate Count

and Laboratory

Identification

Bulk Material N/A N/A Call for Pricing

Total Bacterial Count, Water Visual Plate Count100 mL of water in sterile

container, refrigeratedNA2S2O3 24 hours Call for Pricing

Total Bacterial Count, Water with


Visual Plate Count

and Laboratory

Identification

100 mL of water in sterile

container, refrigeratedNA2S2O3 24 hours Call for Pricing

Total Bacterial Count, Wipe Visual Plate Count Wipe Specimen 163100 N/A 24 hours Call for Pricing

Total Bacterial Count, Wipe with


Visual Plate Count

and Laboratory

Identification

Wipe Specimen 163100 N/A 24 hours Call for Pricing

Total Coliform SM9221B 120 mL sterile plastic NA2S2O3 24 hours Call for Pricing

Total Coliform MPN (For bacteria

counts)SM9221C 120 mL sterile plastic NA2S2O3 24 hours Call for Pricing

Fecal Coliform MPN SM9221C 120 mL sterile plastic NA2S2O3 8 hours Call for Pricing

Fecal Steptococcus MPN SM9230B 120 mL sterile plastic NA2S2O3 8 hours Call for Pricing

Fecal Enterococcus MPN SM9230B 120 mL sterile plastic NA2S2O3 8 hours Call for Pricing

Heterotrophic Plate Count SM9215B 100 mL in sterile container NA2S2O3 8 hours Call for Pricing

Legionella Culture and ID 100 mL in sterile container NA2S2O3 24 hours Call for Pricing

V01 06.2017

Toll Free: 800-888-8061


Fungal - Viable / Cultured

Test Procedure Method of Analysis Sampling Media Sampling RateSuggested Air

Volume, LUnit Cost

Total Fungal Count, Air Visual Plate CountContact Customer Service for

Media Requirements



Total Fungal Count, Air with


Visual Plate Count

and Laboratory

Identification

Contact Customer Service for

Media Requirements



Total Fungal Count, Bulk Visual Plate Count Bulk Material N/A N/A Call for Pricing

Total Fungal Count, Bulk with


Visual Plate Count

and Laboratory

Identification

Bulk Material N/A N/A Call for Pricing

Total Fungal Count, Water Visual Plate Count100 mL of water in sterile

container, refrigeratedN/A N/A Call for Pricing

Total Fungal Count, Water with


Visual Plate Count

and Laboratory

Identification

100 mL of water in sterile

container, refrigeratedN/A N/A Call for Pricing

Total Fungal Count, Wipe Visual Plate Count Wipe Specimen 163100 N/A N/A Call for Pricing

Total Fungal Count, Wipe with


Visual Plate Count

and Laboratory

Identification

Wipe Specimen 163100 N/A N/A Call for Pricing

Fungal - Non-Viable / Direct Analysis

Test Procedure Method of Analysis Sampling Media Sampling RateSuggested Air

Volume, LUnit Cost

Mold Spore Count & ID (Air) Standard Microscopy Air-O-Cell Cassette 15 LPM 150 Call for Pricing

Mold Spore ID (Bulk) Standard Microscopy Zip-Loc Bag 1x1 Inch N/A Call for Pricing

Mold Spore Count/ID and Particulate

ProfileStandard Microscopy Air-O-Cell Cassette 15 LPM 150 Call for Pricing

V01 06.2017

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V 5. Air Quality Testing

Method Compounds Sampling Approach Instrumentation Detection Limit Unit Price

TO-4 PCBs, 4,4-DDE, DDT, DDD Filter and PUF absorbent trap GC/MS or GC/FID/ECD 0.2 pg/m3 – 200 ng/m3 Call for Pricing

TO-8 Cresol/Phenol Midget impingers HPLC 1-250 ppb Call for Pricing

TO-14 Toluene, Benzene, Chlorobenzene Evacuated stainless steel canister GC/MS or GC/FID/ECD 0.2-25 ppbv Call for Pricing

TO-15 Methanol, Benzene, Xylene, Nitrobenzene Specially prepared canisters GC/MS 0.2-25 ppbv Call for Pricing

TO-17Alcohols, Ketones, Benzene, Toluene, o-

Xylene, ChlorobenzeneMulti-Bed Sorbent Tube GC/MS 0.2-25 ppbv Call for Pricing



Standard Microscopy

2 Ranges: <2.5 µm, ≥2.5 μm or

<10 μm, ≥10 μm

Bulk – Sealable glass or plastic vials

Surface - micro-vac on MCEF.

Air - MCEF

N/A N/A Call for Pricing



Standard Microscopy

2 Ranges: <2.5 µm, ≥2.5 μm or

<10 μm, ≥10 μm

Bulk – Sealable glass or plastic vials

Surface - micro-vac on MCEF.

Air - MCEF

N/A N/A Call for Pricing

Particle/Fiber Characterization

& IdentificationStandard Microscopy

Mini-vac samples, scrapings, bulk

materials in sealed bags, tape lifts, or

MCEF filters

N/A N/A $102

V01 06.2017Toll Free: 800-888-8061


VI. Service Guide Summary

1. Standard Terms and Conditions

Unless otherwise agreed to in a formal contract, services provided by Analytics Corporation are limited to the terms and conditions stated below.

Confidentiality – Strict confidentiality is maintained in all business dealings with clients. Confidentiality agreements are therefore willingly provided. In instances where information is subpoenaed by and must be released to a regulatory or legal body, the client is promptly notified. Likewise, the client agrees to respect all such relationships of trust. Client agrees it will not use Analytics’ name and/or data in any manner which might cause harm to Analytics’ business and/or reputation. Under no circumstances is the name Analytics Corporation (Analytics) to be published without written approval.

No verbal results, preliminary or final reports, copies of reports, or electronic deliverables will be sent to anyone other than the client unless the client formally requests us to do so in writing. Contracts – All contracts are subject to review and approval and must be signed by a corporate officer. Payment Terms – Payment in advance is required for all clients except those who establish credit with our company. For clients with approved credit, our standard terms due upon receipt, after which time a 1% per month late charge or maximum amount permitted by law (if less) is added to all unpaid balances. Any deviation in payment terms must be agreed to in writing. Analytics has the right to ask for payment in advance, if the established payment terms are not adhered to. Analytics reserves the right to cease all work in the event the client does not pay its invoices. In the event of default in payment for services rendered, the client is responsible for reasonable collection and/or legal fees.

Billing – All fees are billed directly to the client. Third party billing will not be accepted without a statement, signed by the third party, which acknowledges and accepts payment responsibility. All paperwork submitted with a sample describes the testing desired, and any changes must be submitted in writing. If changes are made after the original request is initiated or has been completed, the client must accept payment responsibility. Analytics is not responsible for holding times that are exceeded due to such changes. All changes should be faxed to: “CLIENT SERVICES - URGENT”.

Rush Analyses – A surcharge is added to the agreed upon fee if rush analysis is requested. The surcharge will depend upon the turnaround time requested. Rush analysis is offered contingent upon availability and pre-arrangement with Client Services or your project manager.

Hazard Communication – It is the client’s responsibility to information the laboratory of any hazardous characteristics known or suspected about the sample based on the collection site or circumstances. Information on hazard prevention and personal protection should also be provided to Analytics.

Delivery of Samples – Upon timely delivery of samples, Analytics will use best efforts to meet mutually agreed upon turnaround times. The risk of loss or damage to the sample during shipment remains with the client. Analytics will advise the client of samples that are missing or received in damaged, contaminated, or improperly preserved condition. The risk of loss or damage to the sample will be assumed by Analytics at the time possession of the sample is delivered to an employee.

151

Analytics reserves the right to refuse or to rescind acceptance of any samples, which in the judgment of Analytics is likely to pose any unreasonable risk in handling and/or analysis.

The client aggress that any sample containing any hazardous substance which is to be delivered to Analytics is labeled, packaged, manifested, transported, and delivered to Analytics in accordance with the most current state and federal regulations. These regulations include, but are not limited to OSHA, EPA, TSCA, RCRA, DOT, FDA and applicable federal, state, and local agencies.

Sample Containers – Analytics will provide sample containers/media upon request. Analytics reserves the right to charge a fee for sample containers/media. Containers, media, and packaging not returned after thirty days will be assessed a fee based on cost plus 25%.

Retention of Samples – After the analytical results have been reported, samples are routinely retained in our storage facilities for 30 days. Prior arrangements must be made if samples are to be held for periods longer than this. Analytics may charge a monthly fee for long-term storage.

Quality Assurance – Analytics will perform services consistent with our Quality Assurance Program Plans (QAPP) and our Standard Operating Procedures. (SOPs). It is the responsibility of the client to confirm that our standard practices meet the needs of the client prior to placing an order for work. In the event the client desires an alternative to these standard practices, such request must be made in writing prior to samples acceptance.

Retention of Reports – Unless otherwise agreed to in writing, Analytics will retain copies of analytics reports for a period of five (5) years, after which the reports may be destroyed. If the client requests additional copies of the analytical reports during the retention period, an additional charge may apply for preparation and printing.

Reports – Analytics prohibits the use of its name in connection with any unauthorized use of its reports. Special Reports – Additional charges may be necessary for customized reports which differ significantly from the Analytics’ standard report. Additional charges may apply for specific QA/QC report formats for data packages and/or electronic deliverables. Please call for specific charges.

Hazardous Waste – Unused portions of samples found or suspected to be hazardous according to state or federal guidelines may be returned to the client upon completion of the analytical work. These include samples known or suspected to contain hazardous materials as defined by state or federal regulatory agencies. The cost of returning the sample may be invoiced to the client. The sample and portions thereof remain the property of the client at all times.

Litigation – All costs associated with compliance to any subpoena or other official request for documents, for testimony in a court of law, or for any other purpose relating to work performed by Analytics in connection with work performed for that client, shall be paid by the client. Such costs shall include, but are not limited to, hourly charge for persons involved in responding to subpoenas, travel and accommodations, mileage, attorney’s preparation of testifier and advice of counsel in connection with response to subpoenas, and all other expenses deemed reasonable and associated with said litigation.

152

Indemnification, Liability, and Insurance – Analytics agrees to indemnify, defend, and save the client, its officers, directors, employees, agents, and representatives harmless from all losses, expenses, demands, and claims made against the clients, its officers, directors, employees, agents, and representatives because of any personal injuries, death, or property damage to the extent caused by the negligence or willful misconduct of Analytics, its employees, agents, or representatives in connection with the performance of services under this agreement, except to the extent such losses, expenses, demands, or claims occur as a result of the negligent or willful acts or omissions of the client, its officers, directors, employees, agents, and representatives; however, such indemnification and damages shall, in the aggregate, be limited to an amount equal to the lesser of (a) damages suffered by the client as a direct result thereof, or (b) the total amount paid by the client to Analytics for the work herein covered. Analytics will, if requested by the client, furnish certificates of insurance from its carrier(s) evidencing appropriate insurance coverage.

Warranty and Limits of Liability – In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other warranties, expressed or implied. We disclaim any other warranties, expressed or implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall Analytics be liable for indirect, special, consequential, or incidental damages including, but not limited to, damages for loss of profit or goodwill regardless of the negligence (either sole or concurrent) of Analytics and whether Analytics has been informed of the possibility of such damages. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Analytics which includes any conditions that vary from the above described Standard Terms and Conditions, and Analytics hereby objects to any conflicting terms contained in any acceptance or order submitted by client.

Equal Opportunity/Affirmative Action Notice – Analytics Corporation is an equal opportunity/affirmative action employer and complies with all the regulations of executive order 11246 and the regulations promulgated there under.

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